atomer analysis tests consulting

8/8/2019 ATOMER Analysis Tests Consulting

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ATOMERATOMERANALYSISANALYSIS -- TESTSTESTS

CONSULTING IN MATERIALSCONSULTING IN MATERIALS

& CHEMISTRY& CHEMISTRY

ATOMER

www.atomer.frwww.atomer.frcontact@[email protected]


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TheTheanalysisanalysis engineering divisionengineering division

AnalysisAnalysisininallallitsitsformsforms

ATOMER

TheThe entireentire rangerange ofofthethe latestlatest technologytechnology as moreas more

conventionalconventional situations insituations in thethe mostmost diversediverse

AnalysisAnalysissatisfyingsatisfyingstandards ASTM, ISO, DIN, ...standards ASTM, ISO, DIN, ...

Reverse engineeringReverse engineering

FindFinda contaminant or additivea contaminant or additive

AnalysisAnalysisfor expertise infor expertise inlitigationlitigationwww.atomer.frwww.atomer.frcontact@[email protected]


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AppropriateAppropriateandandeffective solutionseffective solutions

ATOMER

RatesRatesveryverycompetitivecompetitive

TotalTotalconfidentialityconfidentiality

PersonalizedPersonalizedsupportsupport

TimelinessTimelinessofofcustomercustomer

PerformancePerformanceanalysisanalysis




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EquipmentEquipmentperformanceperformanceandandskillsskills

ininsamplingsamplingandandinterpretationinterpretation

ATOMER




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SeparativeSeparativemethodsmethodsforforsamplesamplepreparationpreparation: filtration,: filtration,precipitationprecipitation,, fractionationfractionation,, variousvariouschromatographieschromatographies

SpectroscopicSpectroscopicmethodsmethods::multinuclearmultinuclearNMR, FTIR,NMR, FTIR,UVUV--visiblevisible, Raman, MS, RX, ESCA, ..., Raman, MS, RX, ESCA, ...

ColorimetricColorimetricassaysassaysandandvariousvariousteststests

ElectrochemicalElectrochemicalmethodsmethods

TheThemethodsmethodsavailableavailabletotothetheanalystanalystareare::

ATOMERwww.atomer.frwww.atomer.frcontact@[email protected]


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CHROMATOGRAPHY :CHROMATOGRAPHY :

ThinThinLayerLayerChromatographyChromatography(HPTLC)(HPTLC)



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VACCUM FILTRATION POLYMERSVACCUM FILTRATION POLYMERS

PRECIPITATIONPRECIPITATION



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ROTATIVEROTATIVEEVAPORATIONEVAPORATION



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SOXHLET EXTRACTIONSOXHLET EXTRACTION

ATOMER


S C OSCO


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SPECTROSCOPY :SPECTROSCOPY :

FTIRFTIR withwithmanymanyaccessoriesaccessories

Diamond ATR Specular reflexion

vertical ATR with variable angle

KRS-5 crystalPERKIN-ELMER FTIR spectrometer

4949//spectrumspectrum


SPECTROSCOPYSPECTROSCOPY


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SPECTROSCOPY :SPECTROSCOPY :

UVUV--VISIBLE (AdditivesVISIBLE (Additivesresearchresearch& quantification)& quantification)

ATOMERSpectrophotometer UV-visible LAMBDA 35


QUANTITATIVEQUANTITATIVE COLORIMETRYCOLORIMETRY


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QUANTITATIVEQUANTITATIVECOLORIMETRY :COLORIMETRY :

ATOMER

PrecisionPrecisionspectrocolorimetryspectrocolorimetrydesigneddesignedforforthethemeasurementmeasurement

ofofliquidliquidandandtransparenttransparentcoloredcoloredplastics ...plastics ...

StandardsStandardsmethodsmethods::IodineIodineindex, Gardner,index, Gardner, HazenHazen((PtPt--CoCo))KlettKlett,, SayboltSaybolt, ASTM D, ASTM D--1500,1500, LovibondLovibond,, LyLy,, LrLr, (, (TxTx,,TyTy,,TzTz))(X,Y,Z),(X,Y,Z), LabLab**--CIE,CIE,


QUALITATIVESQUALITATIVES COLORIMETRIC TESTSCOLORIMETRIC TESTS


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ATOMER

polyurethane

White cloud

Filter paper

QUALITATIVESQUALITATIVESCOLORIMETRIC TESTSCOLORIMETRIC TESTS


QUALITATIVESQUALITATIVES COLORIMETRIC TESTSCOLORIMETRIC TESTS


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ATOMER

Specific reactive

Violet : 1,5-NDI

Red-brown :2,4 & 2,6-TDI

2,4-TDI dimerized

Yellow : 4,4-MDI

Red : TMP & TDI

addition products

Uncolored :

aliphaticisocyanates

QUALITATIVESQUALITATIVESCOLORIMETRIC TESTSCOLORIMETRIC TESTS


PhysicalPhysical andand mechcanicalmechcanical tests :tests :


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Thermal &Thermal & thermothermo--mechanicalmechanicalmethodsmethods: DSC, TMA, ATG,: DSC, TMA, ATG,DMA, HDT,DMA, HDT,

MechanicalMechanicaltests :tests :TensileTensile, flexion, compression, flexion, compression

RheologicalRheologicalmethodsmethods::viscosimetersviscosimeters,, rheometersrheometers,,

FireFire--SmokeSmoketeststests

PhysicalPhysicalandandmechcanicalmechcanicaltests :tests :


HeatHeat DeflectionDeflection TemperatureTemperature (HDT)(HDT)


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HeatHeatDeflectionDeflectionTemperatureTemperature(HDT)(HDT)


MeltMelt FluidFluid Index (MFI)Index (MFI)


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MeltMeltFluidFluidIndex (MFI)Index (MFI)


MECHANICAL TESTS :MECHANICAL TESTS :


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MECHANICAL TESTS :MECHANICAL TESTS :TENSILETENSILE--COMPRESSIONCOMPRESSION--FLEXIONFLEXION

Extensometer ZWICK 1455

TENSILE &TENSILE &COMPRESSIONCOMPRESSIONTESTSTESTS

4545/ 5/ 5piecespieces


MECHANICAL TESTS :MECHANICAL TESTS :


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ATOMER

Extensometer INSTRON 5867. Extensometer INSTRON 5544.

MECHANICAL TESTS :MECHANICAL TESTS :TENSILETENSILE--COMPRESSIONCOMPRESSION--FLEXIONFLEXION


MECHANICAL TESTSMECHANICAL TESTS ::


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MECHANICAL TESTSMECHANICAL TESTS::

TESTS STANDARDS OFFTESTS STANDARDS OFF--MAKING PIECESMAKING PIECES


RESILIENT TESTSRESILIENT TESTS


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RESILIENT TESTSRESILIENT TESTS

1 Joule / 4 J / 7,5 Jwww.atomer.frwww.atomer.frcontact@[email protected]

HARDNESSHARDNESS


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HARDNESSHARDNESS

ShoreShoreA & DA & D

PersozPersoz


HARDNESSHARDNESS


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HARDNESSHARDNESS

VickersVickers


TestingTestingofofnanonano--indentationindentationwithwiththetheNano indenter XPNano indenter XP


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gg

Measuring the hardness and modulus of elasticity (including dynamic modules)

The measurement by nano-indentation is to implement and monitor expenses as low as afew tens of micro-Newtons (N) and up to several hundred Millinewton (mN) with an

accuracy N

The advantage of the instrument of nano-indentation is its ability to measure with

nanometer resolution, depth of penetration up to a few tens of nm with an accuracy


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ABRASION RESISTANCEABRASION RESISTANCE

CircularCircularTaberTaber

LinearLinearTaberTaber


RHEOLOGY :RHEOLOGY :


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ATOMER

RHEOMETERRHEOMETER


RHEOLOGY :RHEOLOGY :


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O OGBROOKFIELD VISCOSIMETERBROOKFIELD VISCOSIMETER

ATOMER


KINETIC RHEOLOGY :KINETIC RHEOLOGY :


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PENDULAR VISCOSIMETERPENDULAR VISCOSIMETER

ATOMER


POLYMERS THERMAL ANALYSISPOLYMERS THERMAL ANALYSIS


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(DIFFERENTIAL SCANNING CALORIMETRY)(DIFFERENTIAL SCANNING CALORIMETRY)




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* Identify the softening point of a material ;* Compare the effects of additives on the material ;

* Determine the glass transition temperature (Tg) ;

* Determine the degree of crystallinity and melting temperature (Tm) ;

* Determine the minimum temperature in the manufacturing process of a material ;* Determine the amount of energy needed to melt the material ;

* Quantify the material specific heat (Cp) ;

* Run a test of stability in oxygen, OIT: Oxidation Induction Time ;

* Understand and quantify the kinetics of reaction of thermosetting material during its

cooking ;* Compare the doneness of a material relative to another ;

* Characterize material when it reacts under ultraviolet light ;

* Characterize material at its cooking temperature ;

* Determine the crystallization temperature (Tc) during cooling.

ATOMER

Some applications of thermal analysis by differential scanning calorimetry in

the field of plastics and polymers :





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Thermogram of a thermoset polymer and measure its

glass transition temperature (Tg)





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Thermogram of the reaction of a mixture of monomers(thermosetting) and partial and total integration of the exothermic

reaction of polymerization (crosslinking)





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OIT : Oxidation Induction Time





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ATOMER

(THERMOGRAVIMETRIC ANALYSIS)(THERMOGRAVIMETRIC ANALYSIS)




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(THERMOGRAVIMETRIC ANALYSIS)(THERMOGRAVIMETRIC ANALYSIS)

ATOMER

* Determine the amount of filler material in weight percent ;

* Determine the amount of ash material in weight percent ;

* Characterize the mass loss of a material over a range of temperature ;

* Characterize the mass loss vs material. time at a given temperature ;

* Quantifying the loss of water, solvent, or plasticizer or additive in a certainrange of temperature ;

* Examine the properties of flame retardant material ;

* Examine the combustion properties of a material.

Some applications of the TGA in plastics arelisted below :


ACCELERATED PHOTOAGEINGACCELERATED PHOTOAGEING(Q UV S )


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(Q(Q--UV + Spray)UV + Spray)

ATOMER

Simulation of energy rays of the solar spectrum. Programming

condensation temperature cycles (simulation of the morning dew) andUV, water spray to test the degradation produced by rain, perfectly

simulates the thermal shockwww.atomer.frwww.atomer.frcontact@[email protected]

ACCELERETED PHOTOAGEINGACCELERETED PHOTOAGEING

(SUNTEST)(SUNTEST)


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(SUNTEST)(SUNTEST)


DETERMINATION OF LIQUIDS MOISTUREDETERMINATION OF LIQUIDS MOISTURE

(KARL FISCHER(KARL FISCHER COULOMETRY)COULOMETRY)


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(KARL FISCHER(KARL FISCHER COULOMETRY)COULOMETRY)

ATOMER


FIREFIRESMOCK TESTSSMOCK TESTS


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METALLOGRAPHYMETALLOGRAPHY


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WebsiteWebsite::www.atomer.frwww.atomer.fr


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atomer analysis tests consulting

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