ar202627c '6 northeastern analytical corporation test report no. nac91l-3927 ciba-geigy...

LABORATORY DEUVERABLES

THIS FORM MUST BE COMPLETED BY THE LABORATORY ORENVIRONMENTAL CONSULTANT AND ACCOMPANY ALL DATA SUBMISSIONS

The following laboratory deliverable* shall be included in the data submission. All deviations from the acceptedmethodology and procedures, or performance values outride acceptable ranges shall b« summarized in the Non-Caniormance Summary. Attachment 2 of the Draft SCHA Sampling Plan Guide (ESPG) provides runner details a befollowed. The document shall b« bound and paginated, contain a Cable of contents, and all pages shall be legible,Incomplete packages will be returned or held without review until the data pactage is completed.

Check ifComplete

L Cover Page, Format; and Laboratory Certification (Include Cross Reference Tableof Field ID. * and Laboratory ID. #)

DL Chain of Custody

HL Summary Sheets Listing Analytical Results Including QA Data Infbrmation(set Attached Form and ESPG Attachment 1&2.CJ

IV. • Laboratory Chronicle and Methodology Summary including Sampling HoldingTime Check

V. Initial Calibration and Continuing Calibration

VL Tune Summary (MS)

VTL Blanks (Method,

VTTL Surrogate Recovery Summary

DC. ' Chromatographx Labefled/Campound Identification

X. Minimum Detection Limits (Lower than Action Level if Clean Zone Sample -and consistent with method guidelines)

XL Non-Conferraance Summary

Laboratory Director or EavironmenoTConsultants Signature

AR202627

MOP_ Northeastern Analytical Corp.

ANALYTICAL REPORT

for

CIBA-GEIGY CORPORATIONEngineering DepartmentJames & Water StreetsNewport, DE 19804

Attention: Mr. Kenneth Taft

TEST REPORT NO. NAC91L-3927

Client NAG DateDesignation Designation Received Matrix

006 91L-3927 12-17-91 Aqueous

Laboratory Name: Northeastern Analytical Corp.

Certification No: 03117________ ______

Name: Paul P. Painter

Title: Laboratory Director

Date: December 31. 1991

AR202628

Analysis, Sampling and Testing for the Environmental and Safety ProfessionalEveaham Corporate Centar, 4 East Stow Road, Marlton, New Jersey 08053 (609J 985-80OO FAX (609) 985-9700

\J G rNORTHEASTERN ANALYTICAL CORPORATION

Test Report No. NAC91L-3927Ciba-Geigy Corporation

TABLE OF CONTENTS

Page No.

I. Sampling Information . . . . . . . . . . . . . 3

II. Chain of Custody Documentation . . . . . . . . 4-9

III. Method Summary . . . . . . . . . . . . . . . . 10

IV. Laboratory Chronicle . . . . . . . . . . . . . 11

V. Analysis Conformance/Non-ConformanceSummary Format . . . . . . . . . . . . . . . 12

VI. Analytical Results . . . . . . . . . . . . . . 13-15

VII. Quality Assurance Data . . . . . . . . . . . . 16

VIII. statement of Authentication . . . . . . . . . 17

File: 28L\TEST\91L-3927

AR202629

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NORTHEASTERN ANALYTICAL CORPORATIONTest Report No. NAC91L-3927

Ciba-Geigy Corporation

I. SAMPLING INFORMATION

Not submitted.

AR202630

,1NORTHEASTERN ANALYTICAL CORPORATION


II. CHAIN OF CUSTODY DOCUMENTATION

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NORTHEASTERN ANALYTICAL CORPORATION

Test Report No. _/'

Parameter Sam?!e Preparation Chemat

3.9.

t.2. Adds3. Pestfcttts4.5. PCB'S

7. Volatile*1 TOC9. TOXiau.

U.14.

15.

_______pnnti

1. 3ase. Neutrals .:. Acids __________

Pesticides ___.______..-t. HerBtcides _____________5. PCB'S _.________6. Metal* Z

M rint D.i:.'



III. METHOD SUMMARY

Metals

This is a procedure used to determine metals concentra-tions in aqueous matrices. It , involves an acidicdigestion under oxidizing conditions of approximately 25milliliters of sample. Nitric and hydrochloric acids aswell as hydrogen peroxide are employed in the digestion.The digested sample is filtered and diluted to 25milliliters. The analysis is performed by ICP andfurnace atomic absorption. Reference methods are 1988CLP Statement of Work for Inorganics and EPA Methods forthe Chemical Analysis of Water and Wastes, Revised, March1983.

Cyanide

An aliquot of sample is acidified under analysis condi-tions liberating cyanide as HCN. A distillation followsleaving behind interferences and scrubbing the distilledHCN in sodium hydroxide solution. An aliquot of the NaOHsolution is analyzed colorimetrically for cyanide ion.Reference method is EPA Methods for the Chemical Analysisof Water and Wastes, Revised, March 1983, Method 335.2.

AR202637

o - iNORTHEASTERN ANALYTICAL CORPORATION


IV. LABORATORY CHRONICLE

A. Date of Sampling; 12-16-91

B. Date of Receipt/Refrigeration: 12-17-91

C. Date of Analysis;

Parameter Hold Time Analyzed Analyzed

Metals 6 Months 12-28 & 12-30-91Mercury 28 Days 12-30-91Cyanide 14 Days 12-30-91

AR202638

V. ANALYSIS CONFORMANCE/NON-CONFORMANCE SUMMARY FORMAT

NO. Yg|

GC/MS Tune Specifications

a. BFB passed ___ __b. DFTPP passed ___ ___

2. GC/MS Tuning Frequency - Performed every 12 hours

3. GC/MS Calibration - Initial Calibration performedwithin 30 days before sample analysis and continuingcalibration performed within 24 hours beforesample analysis

4. GC/MS Calibration Requirementsa. Calibration Check Compoundsb. System Performance Check Compounds

5. Blank Contamination - List compounds for each fraction

a. VOA Fractionb. 8/N Fractionc. Acid Fraction

6. Surrogate Recoveries Meet Criteria(If not met; list those compounds and tha'rrecoveries which fall outside the acceptable range)

a. VOA Fractionb. B/N Fractionc. Acid Fraction

7. Fjctractton Holding Time Met

Comment: ______

8. Analysis Holding Time Met

Comment: _____

Additional Comments:

)Laboratory Director: \ /) n V\S QccfeL- Date:———-

HR2Q263

cNORTHEASTERN ANALYTICAL CORPORATION

REPORT OF METALS ANALYSIS

Client: CIBA-GEIGY CORPORATION Report #: 91L 3927Sample ID: 006 NAG ID: 3927 - 1

UNITS: ug/1

ELEMENT MDL CONC

ALUMINUM 200 1100ANTIMONY 10 UARSENIC 10 ' UBARIUM 200 UBERYLLIUM 5.0 UCADMIUM 5.0 UCALCIUM 5000 86000CHROMIUM 10 UCOBALT 50 UCOPPER 25 UIRON 100 4400LEAD 5.0 UMAGNESIUM 5000 27000MANGANESE 15 2600MERCURY 0.20 UNICKEL 40 UPOTASSIUM 5000 9000SELENIUM 5.0 USILVER 10 USODIUM 5000 130000THALLIUM 10 UVANADIUM 50 UZINC 20 7700

U - Indicates element was analyzed for but not detectedbased on necessary concentrations/dilutions.

MDL - Method detection limit as the minimumof a substance that can be measured and reportedwith 99% confidence.

CONC - Concentration of analyte.



Client: CIBA-GEIGY CORPORATION Report #: 91L 3927Sample ID: METHOD BLANK WATER NAG ID: 3927 - MBW

UNITS: ug/1

ELEMENT MDL CONC

ALUMINUM 200 UANTIMONY 10 UARSENIC 10 UBARIUM 200 UBERYLLIUM 5.0 UCADMIUM 5.0 UCALCIUM 5000 UCHROMIUM 10 UCOBALT 50 UCOPPER 25 UIRON 100 ULEAD 5.0 UMAGNESIUM 5000 UMANGANESE 15 UMERCURY 0.20 UNICKEL 40 UPOTASSIUM 5000 USELENIUM 5.0 USILVER 10 USODIUM 5000 UTHALLIUM 10 UVANADIUM 50 UZINC 20 U


MDL - Method detection limit as the minimum concen6ra«JM>» 0 *+ Iof a substance that can be measured and reportedwith 99% confidence.

CONC - Concentration of analyte.



VI. ANALYTICAL RESULTS (Continued)

Parameter

Sample . DetectionDesignation Cyanide Limit

91L-3927 ND 20Method Blank ND 10

Units (ug/1) (ug/1)

NO: Not Detected.

C '6NORTHEASTERN ANALYTICAL CORPORATION


VII. QUALITY ASSURANCE DATA

Matrix Spike and Matrix Spike Duplicate Recoveries

Sample Amount of Initial % Duplicate Relative %Parameter Spiked Spike, ug Recovery % Recovery Difference

Aluminum 3915-2 50 80 84 4.9Antimony 3901-2 1.2 ** ** **Arsenic 3901-2 0.50 49* 45* 8.5*Barium 3915-2 50 ' 87 88 1.1Beryllium 3915-2 1.2 72 74 2.7Cadmium 3915-2 1.2 68 74 8.4calcium Control 120 98 —— ——Chromium 3915-2 5.0 91 92 . 1 . 1Cobalt 3915-2 12 100 103 3.0Copper 3915-2 6.2 90 94 4.3Iron 3915-2 25 97 100 3.0Lead 3901-2 0.50 72 70 2.8Magnesium Control 120 95 —— ——Manganese 3915-2 12 90 91 1.1Mercury 3901-4 0.20 119 119 0Nickel 3915-2 12 75 79 5.2Potassium Control 120 85 —— ——Selenium 3901-2 0.25 *** *** ***Sodium Control 120 86 —— ——Silver 3915-2 55 81 87 7.4Thallium 3901-2 0.62 43 42 2.4Vanadium 3915-2 12 94 94 0Zinc 3915-2 12 88 89 1.1Cyanide 3918-1 39 92 95 3.2

*: Due to the matrix interference in the sample, the matrix spikes for Arsenic were outside laboratory controllimits. However, the control sample demonstrated acceptable recovery.

**: Du« to the high level of analyte in the sample, the matrix spikes for Antimony were not recovered.However, the control sample demonstrated acceptable recovery.

***: Due to the Matrix interference in the sample, the matrix spikes for Selenium were not recovered. However,the control sample demonstrated acceptable recovery.

RR2026143

p •



VIII. STATEMENT OF AUTHENTICATION

LABORATORY AUTHENTICATION STATEMENT FOR NJPDESCOMPLIANCE MONITORING

I certify under penalty of law, where applicable, thislaboratory meets the Laboratory Performance Standards andQuality Control requirements specified in N.J.A.C. 7:18, 40CFR 136 for Water and Wastewater Analyses and sw 846 forSolid Waste Analyses. I have personally examined and amfamiliar with the information contained in this report, andthat, based on my inquiry of those individuals immediatelyresponsible for obtaining the information, I believe thesubmitted information is true, accurate, complete, and meetsthe standards specified in N.J.A.C. 7:18, 40 CFR 136, and/orSW 846. I am aware that there are significant Penalties forsubmitting false information, including the possibility of afine and imprisonment.

Paul P. PainterLaboratory Director

AR2026t*i*

#CIBA-GEIGY CORP.Newport, Delaware

Outfall & Seep Sampling ProgramBy Northeastern Analytical Corp.

November 15, 1991

Sample Points

* 009 Outfall.

* OF-6 Abandoned Outfall, flow from within and around pipe.

* GWS Composite 1, seep points OA, OB, 1, 2, 3, 4, 5 & 6.No flow from GWS 7.

* 006 Outfall, tide entered pipe and prevented samplecompletion.

* GWS Composite 2, seep points, 11, 12 & 13.No flow from GWS 8, 9 & 10.

* GWS Composite 3, seep point 17.No flow from GWS 14, 15, 16, 18, 19 & 20.

* GWS Composite 4, seep points 22 & 23.

* GWS Composite 5, seep point 26.No flow from GWS 25.

* 001 Outfall.

* 008 Outfall.

jkt/doc29

355V

LABORATORY DEL1VERABLES

THIS FORM MUST BE COMPLETED BY THE LABORATORY ORENVIRONMENTAL CONSULTANT AND ACCOMPANY ALL DATA SUBMISSIONS

The following laboratory deliverable* shall be included in the data submission. All deviations from the acceptedmethodology »nd procedures, or performance values outside acceptable ranges shall be summarized in the Non-Conformance Summary. Attachment 2 of the Draft ECRA Sampling Plan Guide (ESPG) provides further details to befollowed. The document shall b« bound and paginated, contain a table of contents, and ail pages snail be legible.Incomplete package* will be returned or held without review until die data paclage is completed.

Check ifComplete

L Cover Page, Format; and Laboratory Certification (Include Cross Reference Tableof Field LD. * and Laboratory LD. #)

0. Chain of Custody

m. Summary Sheets Listing Analytical Results Including QA Data Information(see Attached Form and ESPG Attachment 1&2LCJ

IV. • Laboratory Chronicle and Methodology Summary including Sampling HoldingTime Check

V. Initial Calibration and Continuing Calibration

VL Tune Summary (MS)

VTL Blank (Method, BeH Trip)

VIE. Surrogate Recovery Summary

Df, ' Chromatographs Labelled/Compound Identification

X. Minimum Detection Limits (Lower than Action Level if Clean Zone Sample •and consistent wim method guidelines)

XL Non-Confbrmance Summary

Laboratory Director or Environmental DattConsultants Signature

MOP Northeastern Analytical Corp.

ANALYTICAL REPORT

for

CIBA-GEIGY CORPORATION/DELAWAREEngineering DepartmentJames & Water StreetsNewport, DE 19804

Attention: Mr. Kenneth Taft

TEST,REPORT NO. NAC91L-3551

PROJECT: Outfalls & Composites

Sample NAG DateLocation Designation Sampled • Matrix

001 Outfall 91L-3551-1 11-15-91 Aqueous006 Outfall 91L-3551-2 11-15-91 Aqueous008 Outfall 91L-3551-3 11-15-91 Aqueous009 Outfall 91L-3551-4 11-15-91 AqueousGWS Composite 1 91L-3551-5 11-15-91 AqueousGWS Composite 2 91L-3551-6 11-15-91 AqueousGWS Composite 3 91L-3551-7 11-15-91 AqueousGWS Composite 4 91L-3551-8 11-15-91 AqueousGWS Composite 5 91L-3551-9 11-15-91 AqueousOF-6 Outfall 91L-3551-10 11-15-91 AqueousTrip Blank 91L-3551-11 11-15-91 Aqueous

Laboratory Name: Northeastern Analytical Corp

Certification No: 03117________________

AJLName: Paul P. Painter

Title: Laboratory Director

Date: December 18. 1991

Analysis, Sampling and Testing for the Environmental and Safety Professions!Evesham Corporate Center. 4 East Stow Road. Marlton, New Jersey 08053 [60S] 985-8000 FAX (609] 985-9700



TABLE OF CONTENTS

Page No.

I. Sampling Information . . . . . . . . . . . . . 3

II. Chain of Custody Documentation . . . . . . . . 4-7

III. Method Summary . . . . . . . . . . . . . . . . 8-9

IV. Laboratory Chronicle . . . . . . . . . . . . . 10

V. Analysis Conformance/Non-ConformanceSummary Format . . . . . . . . . . . . . . . 11

VI. Analytical Results . . . . . . . . . . . . . . 12 - 116

VII. Quality Assurance Data . . . . . . . . . . . . 117 - 133

VIII. Statement of Authentication . . . . . . . . . 134

Appendix 1: Volatile Organic and SemivolatileOrganic Compounds Data Package 135 - 753

Sample Identification91L-3551-1 Sample Data Package91L-3551-2 Sample Data Package91L-3551-3 Sample Data Package91L-3551-4 Sample Data Package91L-3551-5 Sample Data Package91L-3551-6 Sample Data Package91L-3551-7 Sample Data Package91L-3551-8 Sample Data Package91L-3551-9 Sample Data Package91L-3551-10 Sample Data Package91L-3551-11 Sample Data PackageGC/MS Tune and Mass Calibration SummaryInitial Calibration SummaryContinuing Calibration SummaryGC/MS Quality Assurance DataMethod Blank Summary

Appendix 2; Pesticide and PCB Chromatograms

File: 28L\TEST\91L-3551



I. SAMPLING INFORMATION

Sampling was conducted on November 15, 1991 by NortheasternAnalytical Corporation (NAC) personnel in accordance with theguidelines as outlined in the NJDEP Field Sampling Manual1986. Sample locations were identified by markers installedby Ciba-geigy Corporation of Newport.

Sample locations consisted of five (5) outfall discharges andsix (6) ground water seepage discharges.

Sample designations and descriptions are as follows:

NAC SAMPLENUMBER DESIGNATION DESCRIPTION

91L-3551-1 Outfall 001 Flowing Discharge91L-3551-2 Outfall 006 Flowing Discharge

( aborted due torising of tide)

91L-3551-3 Outfall 008 Flowing Discharge91L-3551-4 Outfall 009 Flowing Discharge91L-3551-5 GWS Comp. 1 Composite of the

following: OA, OB,1, 2, 3, 4, F, 6, 7(No flow from 7)

91L-3551-6 GWS Comp. 2 Composite of thefollowing: 8, 9,10, 11, 12, 13 (Noflow from 16, 18,19, or 20)

91L-3551-7 GWS Comp. 3 Composite of thefollowing: 16, 17,18, 19, or 20)

91L-3551-8 GWS Comp. 4 Composite of thefollowing: 21, 22,23, 24 (No flow from21 or 24)

91L-3551-9 GWS Comp. 5 Composite of 25 and26 (NO flOW/NOSample)

91L-3551-10 Outfall Of 6 *

*: Sample collected front ground water seepage from within and around discharge pipe. NortheasternAnalytical Corporation (NAC) was unable to determine actual source of discharge. A D O fl O £ I



II. CHAIN OF CUSTODY DOCUMENTATION

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/-. K-lUs. 7NORTHEASTERN ANALYTICAL CORPORATION

Test Report No.

3.

9.

Parameter Sample Preparation Chemm;

Vame /"please pnnt) Signature__ , 7, v_ )

t. Base/Neutrals -Uv^ VC^AT. C At, T" K,> .-•-• Acids -ZTcy ^Cftx.^ri L-L -r- £. . ."A,

.\ '.V Pesticides -jc^-^?e// d'-'o».•i. Herbicides ____________5. PCB's jl<6. Meuls

Paramettf AnaMt

Name) fpteaaa priaty~N Si|n«nife> -— Da;.-s fi —J &?:

1. 3«ac/N«atnli2. Adds3. Pesddda4. Htrbttdcs5. PCB's6. Mttals "tJe- V-au- Vgaf- ___ SH\. j *n —~ nzn~ —/———/T. Volstito A/vfaxx' MAKTiJ :z ^~/7 ^ '^ a ti: 2!c sj:7/yS. TOC _______________ ______________ ________9. TOX ^___________' ^-^_________ ________10. PtMHOk (MCJ_> —

U. cyuidc (toal) Ta -P—— j13. __________ _14. ___________ ____

15. _______'

NORTHEASTERN ANALYTICAL CORPORATION °^ UTest Report No. NAC91L-3551


III. METHOD SUMMARY

Puraeables by GC/MS

EPA Method 624 - This is a purge and trap gas chromato-graph/mass spectrometer (GC/MS) method. The organiccompounds are separated by the gas chromatograph anddetected using the mass spectrometer. Federal Register,Vol. 40, No. 136, July, 1988.

An HP5890/5970 GC/MS was used with a packed column of 1%SP-1000 on Carbopack B.

Method detection limits are as stated.

Semivolatiles by GC/MS

EPA Method 625 - This is a gas chromatograph/mass spec-trometer (GC/MS) method applicable to the determinationof a number of organic compounds that are partitioned inan organic solvent and amenable to gas chromatography.Federal Register, Vol. 40, No. 136, July, 1988.

An HP5890/5970B GC/MS was used with a Rtx-5 fused silicacapillary column.

Method detection limits are as stated.

AR202651*



III. METHOD SUMMARY (Continued)

Metals

This is a procedure used to determine metals concentra-tions in aqueous matrices. It involves an acidicdigestion under oxidizing conditions of approximately 25milliliters of sample. Nitric and hydrochloric acids aswell as hydrogen peroxide are employed in the digestion.The digested sample is filtered and diluted to 25milliliters. The analysis is performed by ICP andfurnace atomic absorption. Reference methods are 1988CLP Statement of Work for Inorganics and EPA Methods forthe Chemical Analysis of Water and Wastes, Revised, March1983.

Cyanide

An aliquot of sample is acidified under analysis condi-tions liberating cyanide as HCN. A distillation followsleaving behind interferences and scrubbing the distilledHCN in sodium hydroxide solution. An aliquot of the NaOHsolution is analyzed colorimetrically for cyanide ion.Reference method is EPA Methods for the Chemical Analysisof Water and Wastes, Revised, March 1983, Method 335.2.

Pesticides/PCB's

EPA Method 608 - This method covers the determination ofpesticides and polychlorinated biphenyls (PCB's) insamples by extraction/concentration with organic solventsand subsequent qualification/quantification by GasChromatography. The gas chromatograph utilizes anelectron capture detector (BCD) which is applicable forthe determination of the compounds listed for this methodin the U.S.E.P.A. Manual entitled "Methods for OrganicChemical Analysis of Municipal and IndustrialWastewater".

AR202655

r> •' -\b_ J



IV. LABORATORY CHRONICLE

A. Date of Sampling: 11-15-91

B. Date of Receipt/Refrigeration; 11-15-91

C. Date of Analysis;

Hold Date DateParameter Time Extracted Analyzed

Volatile Organics 14 Days NA 11-19, 11-26 &11-27-91

Semivolatile Organics 7 Days 11-22-91 11-27-91• Re-extraction NA 11-29 & 12-03 & 12-06-91

12-04-91Metals 6 Months NA 11-27 & 11-30-91Mercury 28 Days NA 11-27-91Cyanide 14 Days NA 11-27-91

NA: Not Applicable.

AR202656

V. ANALYSIS CONFORMANCE/NON-CONFORMANCE SUMMARY FORMAT

NO Yes

1. GC/MS Tune Specifications

a. BFB passed ___ Xb. DFTPP passed ___ X

2. GC/MS Tuning Frequency - Performed every 12 hours ___ _X_

3. GC/MS Calibration - Initial Calibration performedwithin 30 days before sample analysis and continuingcalibration performed within 24 hours beforesample analysis ___ _X_

4. GC/MS Calibration Requirementsa. Calibration Check Compounds ___ _X_b. System Performance Check Compounds ___ _X_

5. Blank Contamination - List compounds for each fraction

a. VOA Fraction _______________________________b. B/N Fraction bis(2-Ethy1hexytlphthalatec. Acid Fraction ___________________

6. Surrogate Recoveries Meet Criteria X ___(If not met; list those compounds and theirrecoveries which fall outside the acceptable range)

a. VOA Fraction Toluene-dS: m. 1.2-Dtohtofoethene: 115_______________b. B/N Fraction Nitrobenzene-d5: 30. Phenol-d6: 0.1.3.5. 2-Fluorophenol-. 0.4.18.20. 2.4.6-

Tribromophenol 0,1,5. Terphenvi-d-14: 143__________________________c. Acid Fraction ___________________________________________

7. Extraction Holding Time Met ___ X

Comment: Sample 91L-3551 -3 was re-extracted for Semivolatile Oraanics analysis on 11 -29-91due to surrogate recovery failure. Original extraction was on 11 -22-91, Samples 91L-3551 -5, -8and -9 were re-extracted for Semivolatile Organlcs analysis on 11 -29-91 due to surrogate recoveryfailure. Repeat analyses also hod surrogates outside QC Limits, therefore initial results have beenprovided. Sample 3551 -10 was re-extracted for Semrvotatile Organics analysis on 12-4-91 due tosample matrix Interference. Original extraction was on 11 -22-91. Sample 91 L-3551 -2 hassurrogates outside QC Limits. Samples was not re-extracted due to insufficient sample.______

8. Analysis Holding Time Met

Comment: _______

AR202657Laboratory Director: V XA/lou>U-x Date:

P •; 2NORTHEASTERN ANALYTICAL CORPORATION

VOLATILE ORGANIC ANALYSIS DATA SHEET

B SAMPLE ID:91L-3551-1 LAB FILE ID:>C1626DATE RECEIVED:11/15/91 DATE ANALYZED:911127

SAMPLE WT/VOL:5ML LEVEL:LOW

CAS NO. MDL CONC. ug/L

74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 1 J67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane ' 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U~9-ol-6 Trichloroethene 5 3 J24-48-1 Dibromochloromethane 5 U9-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 76/79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not DetectedJ; below the limits of reliable quantitation

AR202658

NORTHEASTERN ANALYTICAL CORPORATION ," "1VOLATILE UNKNOWN IDENTIFICATION U i. O

"AB SAMPLE ID:91L-3551-1 LAB FILE ID:>C1626

DATE RECEIVED: 1 1/1 5/91 DATE ANALYZED: 91 1 1 27'


COMPOUND RET TIME CONC

1.1,2 & 1,4-Dichlorobenzenes 34.98 10 ug/L J

J; Estimated Concentration

AR202659

NORTHEASTERN ANALYTICAL CORPORATION C ,_. 4


B SAMPLE ID:91L-3551-2 LAB FILE ID:>C1643

DATE RECEIVED:11/15/91 ' , DATE ANALYZED:911127

SAMPLE WT/VOL:2ML/5ML LEVEL:LOW


74-87-3 Chloromethane 25 U74-83-9 Bromomethane 25 U75-01-4 Vinyl Chloride 25 U75-00-3 Chloroethane 25 U75-09-2 Methylene Chloride 13 U67-64-1 Acetone 25 U75-15-0 Carbon Disulfide 13 U75-35-4 1,1-Dichloroethene 13 U75-34-3 1,1-Dichloroethane 13 U156-60-5 Trans-l,2-Dichloroethene 13 2567-66-3 Chloroform 13 7 J107-06-2 1,2-Dichloroethane 13 U78-93-3 2-Butanone 25 U71-55-6 1,1,1-Trichloroethane 13 U56-23-5 Carbon Tetrachloride 13 U108-05-4 Vinyl Acetate 25 U75-27-4 Bromodichloromethane 13 U78-87-5 !<2-Dichl9ropropane 13 U"0061-01-5 cis-l,3-Dichloropropene 13 U9-01-6 Trichloroethene 13 3124-48-1 Dibromochloromethane 13 U79-00-5 1,1,2-Trichloroethane 13 U71-43-2 Benzene 13 U10061-02-6 trans-i,3-Dichloropropene 13 U75-25-2 Bromoform 13 U591-78-6 2-Hexanone 25 U108-10-1 4-Methyl-2-Pentanone 25 U127-18-4 Tetrachloroethene 13 47079-34-5 1,1,2,2-Tetrachloroethane 13 U108-88-3 Toluene 13 U108-90-7 Chlorobenzene 13 U100-41-4 Ethylbenzene 13 U100-42-5 Styrene 13 U133-02-7 o&p Xylenes . 25 U108-38-3 m-Xylene 13 U


AR202660

NORTHEASTERN ANALYTICAL CORPORATION <_, .VOLATILE UNKNOWN IDENTIFICATION

,AB SAMPLE ID:91L-3551~2 LAB FILE ID:>C1643

DATE RECEIVED:11/15/91 DATE ANALYZED:911127

SAMPLE WT/VOL:2ML/5ML ' LEVEL:LOW




AR20266I

NORTHEASTERN ANALYTICAL CORPORATION '-' - u





GAS NO. MDL CONC. ug/L

74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 4 J67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-1.3-Dichloropropene 5 U9-01-6 Trichioroethene 5 U124-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U


HR202662

C. 7NORTHEASTERN ANALYTICAL CORPORATION ~ 'VOLATILE UNKNOWN IDENTIFICATION

,AB SAMPLE ID:91L-3551-3 LAB FILE ID:>C1627




I.Silane, fluorotrimethyl- (8CI9CI) 7.26 6 ug/L J


AR202663

NORTHEASTERN ANALYTICAL CORPORATION U *• Cf




SAMPLE WT/VOL.-5ML LEVEL: LOW


74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 u75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 1075-15-0 carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 . U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-1.3-Dichloropropene 5 U"9-01-6 Trichloroethene 5 U24-48-1 Dibromochloromethane 5 U9-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not Detected

AR20266i*

NORTHEASTERN ANALYTICAL CORPORATION C 1VOLATILE UNKNOWN IDENTIFICATION

LAB SAMPLE ID:91L-3551-4 LAB FILE ID:>C1628




I.Silane, fluorotrimethyl- (8CI9CI) 7.26 6 ug/L J


AR202665

NORTHEASTERN ANALYTICAL CORPORATION !^ - J


LAB SAMPLE ID:91L-3551-5 LAB FILE ID:>A3740


SAMPLE WT/VOL.-5ML LEVEL: LOW


74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 2 J75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 3367-66-3 Chloroform 5 1 J107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 u108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-1.3-Dichloropropene 5 U(79-01-6 Trichloroethene 5 19124-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone .10 u108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 16079-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 u108-38-3 m-Xylene 5 U


AR202666

***' " ._>

NORTHEASTERN ANALYTICAL CORPORATION U _j_VOLATILE UNKNOWN IDENTIFICATION







AR202667

NORTHEASTERN ANALYTICAL CORPORATION C C 2VOLATILE ORGANIC ANALYSIS DATA SHEET

B SAMPLE ID.-91L-3551-6 LAB FILE ID:>A3741DATE RECEIVED:11/15/91 DATE ANALYZED:911126



74-87-3 Chloromethane 50 U74-83-9 Bromomethane 50 U75-01-4 Vinyl Chloride 50 5475-00-3 Chloroethane 50 U75-09-2 Methylene Chloride 25 U67-64-1 Acetone 50 U75-15-0 Carbon Disulfide 25 U75-35-4 1,1-Dichloroethene 25 u75-34-3 1,1-Dichloroethane 25 U156-60-5 Trans-l,2-Dichloroethene 25 8767-66-3 Chloroform 25 5 J107-06-2 1,2-Dichloroethane 25 U78-93-3 2-Butanone 50 U71-55-6 1,1,1-Trichloroethane ' 25 U56-23-5 Carbon Tetrachloride 25 U108-05-4 Vinyl Acetate 50 U75-27-4 Bromodichloromethane 25 U78-87-5 l,2-Dichl9ropropane 25 U10061-01-5 cis-1.3-Dichloropropene 25 U"9-01-6 Trichloroethene 25 25. 24-48-1 Dibromochloromethane 25 U79-00-5 1,1,2-Trichloroethane 25 U71-43-2 Benzene 25 U10061-02-6 trans-l,3-Dichloropropene 25 U75-25-2 Bromoform 25 U591-78-6 2-Hexanone 50 Ulos-io-i 4-Methyl-2-Pentanone 50 U127-18-4 Tetrachloroethene 25 14079-34-5 1,1,2,2-Tetrachloroethane 25 U108-88-3 Toluene • 25 U108-90-7 Chlorobenzene 25 1400100-41-4 Ethylbenzene 25 U100-42-5 Styrene 25 U133-02-7 o&p Xylenes 50 U108-38-3 m-Xylene 25 U


AR202668

NORTHEASTERN ANALYTICAL CORPORATION f• "VOLATILE UNKNOWN IDENTIFICATION ;— L J





1.1,2 & 1,4~Dichlorobenzenes 34.86 670 ug/L J


AR202669

NORTHEASTERN ANALYTICAL CORPORATION CC4VOLATILE ORGANIC ANALYSIS DATA SHEET

B SAMPLE 10:911-3551-7 LAB FILE ID:>C1618


SAMPLE WT/VOL:2.5ML/5ML LEVEL:LOW


74-87-3 Chloromethane 20 u74-83-9 Bromomethane 20 U75-01-4 Vinyl Chloride 20 10 J75-00-3 Chloroethane 20 u75-09-2 Methylene Chloride 10 U67-64-1 Acetone 20 U75-15-0 Carbon Disulfide 10 U75-35-4 1,1-Dichloroethene 10 U75-34-3 1,1-Dichloroethane 10 U156-60-5 Trans-l,2-Dichloroethene 10 1267-66-3 Chloroform 10 u107-06-2 1,2-Dichloroethane 10 U78-93-3 2-Butanone 20 U71-55-6 1,1,1-Trichloroethane 10 U56-23-5 Carbon Tetrachloride 10 u108-05-4 Vinyl Acetate 20 U75-27-4 Bromodichloromethane 10 U78-87-5 l,2-Dichl9ropropane 10 U"0061-01-5 cis-l,3-Dichloropropene 10 u9-01-6 Trichloroethene 10 U124-48-1 Dibromochloromethane 10 U79-00-5 1,1,2-Trichloroethane 10 u71-43-2 .Benzena 10 3810061-02-6 trans-l,3-Dichloropropene 10 U75-25-2 Bromoform 10 U591-78-6 2-Hexanone 20 U108-10-1 4-Methyl-2-Pentanone 20 U127-18-4 Tetrachloroethene 10 U79-34-5 1,1,2,2-Tetrachloroethane 10 U108-88-3 Toluene 10 U108-90-7 Chlorobenzene 10 570100-41-4 Ethylbenzene 10 2 J100-42-5 styrene 10 u133-02-7 o&p Xylenes . 20 U108-38-3 m-Xylene 10 U


AR202670

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE UNKNOWN IDENTIFICATION

LAB SAMPLE ID:911-3551-7 LAB FILE ID:>C1618


SAMPLE WT/VOL:2.5ML/5ML LEVEL:LOW


1.Unknown 34.97 30 ug/L J


AR20267I

NORTHEASTERN ANALYTICAL CORPORATION •-• .-, U


B SAMPLE ID:91L-3551-8 LAB FILE ID:>C1629 ,




74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 1575-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 19067-66-3 Chloroform 5 3 J107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 uios-05-4 Vinyl Acetate 10 u75-27-4 Bromodichloromethane 5 U78-87-5 l,2-Dichl9ropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 Uk79-ol-6 Trichloroethene 5 376.24-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 710061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 7579-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 160100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U


AR202672

NORTHEASTERN ANALYTICAL CORPORATION C 7VOLATILE UNKNOWN IDENTIFICATION

LAB SAMPLE ID:91L-3551-8 LAB FILE ID:>C1629

DATE RECEIVED:11/15/91 DATE ANALYZED:9111 2





HR202673

NORTHEASTERN ANALYTICAL CORPORATION '-•-<J


B SAMPLE ID:91L-3551-9 LAB FILE ID:>C1620DATE RECEIVED:11/15/91 DATE ANALYZED:911126

SAMPLE WT/VOL:250UL/5ML LEVEL:LOW


74-87-3 Chloromethane 200 U74-83-9 Bromomethane 200 U75-01-4 Vinyl Chloride 200 U75-00-3 Chloroethane 200 U75-09-2 Methylene Chloride 100 U67-64-1 Acetone 200 U75-15-0 Carbon Disulfide 100 U75-35-4 1,1-Dichloroethene 100 U75-34-3 1,1-Dichloroethane 100 U156-60-5 Trans-l,2-Dichloroethene 100 28067-66-3 Chloroform 100 57 J107-06-2 1,2-Dichloroethane 100 U78-93-3 2-Butanone 200 U71-55-6 1,1,1-Trichloroethane 100 U56-23-5 carbon Tetrachloride 100 370108-05-4 Vinyl Acetate 200 U75-27-4 Bromodichloromethane 100 U78-87-5 l,2-Dichl9ropropane 100 U10061-01-5 cis-1.3-Dichloropropene 100 U.79-01-6 Trichloroethene 100 31 J24-48-1 Dibromochloromethane 100 U'79-00-5 1,1,2-Trichloroethane 100 U71-43-2 Benzene 100 U10061-02-6 trans-l,3-Dichloropropene 100 U75-25-2 Bromoform 100 U591-78-6 2-Hexanone 200 U108-10-1 4-Methyl-2-Pentanone 200 U127-18-4 Tetrachloroethene 100 240079-34-5 1,1,2,2-Tetrachloroethane 100 U108-88-3 Toluene 100 U108-90-7 Chlorobenzene 100 240100-41-4 Ethylbenzene 100 U100-42-5 Styrene 100 U133-02-7 o&p Xylenes 200 U108-38-3 m-Xylene 100 U


AR20267I*

NORTHEASTERN ANALYTICAL CORPORATION f -_VOLATILE UNKNOWN IDENTIFICATION •-> <~ J

"_AB SAMPLE ID:91L-3551~9 LAB FILE ID:>C1620

DATE RECEIVED: 1 1 /1 5 / 91 DATE ANALYZED: 9111 26"

SAMPLE WT/VOL:250UL/5ML LEVEL:LOW


1.1,2 & 1,4-Dichlorobenzene 34.88 3800 ug/L J


AR202675


VOLATILE ORGANIC ANALYSIS DATA SHEET 'J ~ JLAB SAMPLE ID:91L-3551-10 LAB FILE ID:>A3766




74-87-3 Chloromethane 50 U74-83-9 Bromomethane 50 U75-01-4 Vinyl Chloride 50 15 J75-00-3 Chloroethane 50 U75-09-2 Methylene Chloride 25 U.67-64-1 Acetone 50 U75-15-0 Carbon Disulfide 25 U75-35-4 1,1-Dichloroethene 25 U75-34-3 I,l-Dichlor9ethane 25 U156-60-5 Trans-l,2-Dichloroethene 25 6667-66-3 Chloroform 25 U107-06-2 1,2-Dichloroethane 25 U78-93-3 2-Butanone 50 U71-55-6 1,1,1-Trichloroethane 25 U56-23-5 Carbon Tetrachloride 25 U108-05-4 Vinyl Acetate 50 U75-27-4 Bromodichloromethane 25 U78-87-5 1,2-Dichloropropane 25 U10061-01-5 cis-l,3-Dichloropropene 25 U(79-01-6 Trichloroethene 25 U24-48-1 Dibromochloromethane 25 U79-00-5 1,1,2-Trichloroethane 25 U71-43-2 Benzene 25 3410061-02-6 trans-l,3-Dichloropropene 25 U75-25-2 Bromoform 25 U591-78-6 2-Hexanone -50 U108-10-1 4-Methyl-2-Pentanone 50 U127-18-4 Tetracnloroethene 25 U79-34-5 1,1,2,2-Tetrachloroethane 25 U108-88-3 Toluene 25 8 J108-90-7 Chlorobenzene 25 510100-41-4 Ethylbenzene 25 . U100-42-5 Styrene 25 U133-02-7 o&p Xylenes 50 U108-38-3 m-Xylene 25 U


AR202676

NORTHEASTERN ANALYTICAL CORPORATION „VOLATILE UNKNOWN IDENTIFICATION ^







AR202677

NORTHEASTERN ANALYTICAL CORPORATION r'" *>VOLATILE ORGANIC ANALYSIS DATA SHEET v <•

B SAMPLE ID.-91L-3551-11 LAB FILE ID:>C1508




74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 3875-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 I,l-Dichlor9ethane 5 u156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform _ . 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 u71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U179-01-6 Trichloroethene 5 U, 24-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene • 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not Detected

AR202678

NORTHEASTERN ANALYTICAL CORPORATION CCCVOLATILE UNKNOWN IDENTIFICATION

-,AB SAMPLE ID: 91 L-3551-11 LAB FILE ID:>C1508

DATE RECEIVED: 11/1 5/91 DATE ANALYZED: 911 11 9'


COMPOUND RET TIME(MIN) CONC

NONE FOUND


VOLATILE ORGANIC ANALYSIS DATA SHEET CC<_'

LAB SAMPLE ID:METHOD BLANK LAB FILE ID:>C16389111271049

DATE RECEIVED:NA DATE ANALYZED:911127SAMPLE WT/VOL.-5.0ML LEVEL: LOW


74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 u75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 l,l-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 u67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 u56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 u78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U79-01-6 Trichloroethene 5 U124-48-1 Dibromochlororaethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetracnloroethene 5 u79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 u100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene " 5 U

U; Not Detected

AR202680

NORTHEASTERN ANALYTICAL CORPORATION < ' '}VOLATILE UNKNOWN IDENTIFICATION


DATE RECEIVED:NA DATE ANALYZED:9111 27

SAMPLE WT/VOL:5.0ML LEVEL:LOW


NONE FOUND

AR20268I

NORTHEASTERN ANALYTICAL CORPORATION f, " 2-1 w OVOLATILE ORGANIC ANALYSIS DATA SHEET


DATE RECEIVED:NA DATE ANALYZED:911126SAMPLE WT/VOL:5ML LEVEL:LOW


74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U(79-01-6 Trichloroethene 5 U124-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U-133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not Detected

AR202682

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE UNKNOWN IDENTIFICATION r, r -;

LAB SAMPLE ID:METHOD BLANK LAB FILE Iof>C1624

DATE RECEIVED:NA 233° DATE ANALYZED:91112



NONE FOUND

AR202683




DATE RECEIVED:NA DATE ANALYZED:911126



74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 u78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 u75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U179-01-6 Trichloroethene 5 U124-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not Detected

NORTHEASTERN ANALYTICAL CORPORATION C v^ 3VOLATILE UNKNOWN IDENTIFICATION





NONE FOUND

AR202685


I VOLATILE ORGANIC ANALYSIS DATA SHEET C • J





74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U_79-01-6 Trichloroethene 5 U24-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Broraoform 5 u591-78-6 2-Hexanone .10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 u100-42-5 styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 U

U; Not Detected

AR202686

NORTHEASTERN ANALYTICAL CORPORATION _ .,tVOLATILE UNKNOWN IDENTIFICATIION A





NONE FOUND

AR202687

C*2NORTHEASTERN ANALYTICAL CORPORATION

VOLATILE ORGANIC ANALYSIS DATA SHEETLAB SAMPLE ID:METHOD BLANK LAB FILE ID:>A3762

9111271321DATE RECEIVED:NA DATE ANALYZED:911127



74-87-3 Chloromethane 10 U74-83-9 Bromomethane 10 U75-01-4 vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 I,l-Dichlor9ethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform • 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 u71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 U108-05-4 Vinyl Acetate 10 u75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U10061-01-5 cis-l,3-Dichloropropene 5 U(79-01-6 Trichloroethene 5 U124-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene - 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene ' 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes 10 U108-38-3 m-Xylene 5 u

U; Not Detected

AR202688

NORTHEASTERN ANALYTICAL CORPORATION ,' ' "VOLATILE UNKNOWN IDENTIFICATIION - "* *-

LAB SAMPLE ID:METHOD BLANK LAB FILE ID:>A37629111271321

DATE RECEIVED:NA DATE ANALYZED:911 1 2



NONE FOUND

AR202689

NORTHEASTERN ANALYTICAL CORPORATION t,


B SAMPLE ID:METHOD BLANK LAB FILE ID:>A37359111261117




74-87-3 Chloromethane 10 U74-83-9 Broraomethane 10 U75-01-4 Vinyl Chloride 10 U75-00-3 Chloroethane 10 U75-09-2 Methylene Chloride 5 U67-64-1 Acetone 10 U75-15-0 Carbon Disulfide 5 U75-35-4 1,1-Dichloroethene 5 U75-34-3 1,1-Dichloroethane 5 U156-60-5 Trans-l,2-Dichloroethene 5 U67-66-3 Chloroform 5 U107-06-2 1,2-Dichloroethane 5 U78-93-3 2-Butanone 10 U71-55-6 1,1,1-Trichloroethane 5 U56-23-5 Carbon Tetrachloride 5 u108-05-4 Vinyl Acetate 10 U75-27-4 Bromodichloromethane 5 U78-87-5 1,2-Dichloropropane 5 U"0061-01-5 cis-l,3-Dichloropropene 5 U9-01-6 Trichloroethene v 5 U24-48-1 Dibromochloromethane 5 U79-00-5 1,1,2-Trichloroethane 5 U71-43-2 Benzene 5 U10061-02-6 trans-l,3-Dichloropropene 5 U75-25-2 Bromoform 5 U591-78-6 2-Hexanone 10 U108-10-1 4-Methyl-2-Pentanone 10 U127-18-4 Tetrachloroethene 5 U79-34-5 1,1,2,2-Tetrachloroethane 5 U108-88-3 Toluene 5 U108-90-7 Chlorobenzene 5 U100-41-4 Ethylbenzene 5 U100-42-5 Styrene 5 U133-02-7 o&p Xylenes • 10 U108-38-3 m-Xylene 5 U

U; Not Detected

AR202690

NORTHEASTERN ANALYTICAL CORPORATION f' 'VOLATILE UNKNOWN IDENTIFICATION


DATE RECEIVED:NA DATE ANALYZED: 9111 2'



NONE FOUND

ftR20269l


VOLATILE METHOD BLANK SUMMARY SHEET


MATRIX:AQUEOUS LEVEL:LOW

DATE ANALYZED:11/27/91 TIME ANALYZED:10:49

This method blank applies to the following Samples, MS and MSD

LAB SAMPLE ID LAB FILE ID INJECT DATE AND TIME

91L-3551-2 >C1643 11/27/91 17:09

AR202692

NORTHEASTERN ANALYTICAL CORPORATION /-, . ~'i (



MATRIX:AQUEOUS LEVEL:LOWDATE ANALYZED:11/26/91 TIME ANALYZED:23:30



91L-3551-1 >C1626 11/27/91 01:10

91L-3551-3 >C1627 11/27/91 02:0091L-3551-4 >C1628 11/27/91 02:50

91L-3551-8 >C1629 11/27/91 03:40

AR202693

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE METHOD BLANK SUMMARY SHEET

£AB SAMPLE ID:METHOD BLANK LAB FILE ID:>C1615





91L-3551-7 >C1618 11/26/91 17:30

91L-3551-9 >C1620 11/26/91 19:38

AR20269I*








91L-3551-11 >C1508 11/19/91 20:02

AR202695

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE METHOD BLANK SUMMARY SHEET



DATE ANALYZED:11/27/91 ' TIME ANALYZED:13:21



91L-3551-10 >A3766 11/27/91 17:53

AR202696

NORTHEASTERN ANALYTICAL CORPORATIONt * h

VOLATILE METHOD BLANK SUMMARY SHEET "

LAB SAMPLE ID:METHOD BLANK LAB FILE ID:>A3735MATRIX:AQUEOUS LEVEL:LOW




91L-3551-5 >A3740 11/26/91 16:54

91L-3551-6 >A3741 11/26/91 17:57

AR202697


SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET tj 2

}LAB SAMPLE ID:91L3551-1 LAB FILE ID:>D7741

DATE EXTRACTED:11/22/91 DATE ANALYZED:911127

SAMPLE WT/VOL:1000/1ML LEVEL:LOW

GAS NO. MDL CONC.UG/L

108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 U106-46-7 1,4-Dichlorobenzene 10 U100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 5 J95-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine ' 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 U111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 U87-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 u95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-NitroanIline 50 U


AR202698

NORTHEASTERN ANALYTICAL CORPORATION C O 3

SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET

LAB SAMPLE ID:91L3551-1 LAB FILE ID:>D7741




83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 U100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 U84-74-2 Di-n-Butylphthalate 10 U206-44-0 Fluoranthene 10 U129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate . 10 10 B218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,i)Perylene 10 U

B: Cone, of Bis(2-Ethylhexyl)Phthalate 4 ug/1 IN METHOD BLANK(1) - Cannot be separated from DiphenylamineU; Not Detected

AR202699

NORTHEASTERN ANALYTICAL CORPORATIONSEMIUOLATILE UNKNOWN IDENTIFICATION C o 4


DATE EXTRACTED: 11/22/91 DATE ANALYZED : 91112."

SAMPLE UiT/UOL: 1000/1ML LEUEL:LOW


l.Ethene, tetrachloro- C9CIJ 4.78 14UG/L J


AR202700

NORTHEASTERN ANALYTICAL CORPORATION r ' ",V <v «J




SAMPLE WT/VOL:500/.5ML LEVEL:LOW

CAS NO. MDL CONC.UG/L

108-95-2 Phenol • 10 3 J111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 U106-46-7 1,4-Dichlorobenzene 10 3 J100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 3995-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 . U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nltrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 7111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 U87-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroanlline 50 U


AR20270I

NORTHEASTERN ANALYTICAL CORPORATIONf •":»

SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET "^ °



SAMPLE WT/VOL:500/.5ML LEVEL:LOW


83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate • 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 U100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 U84-74-2 Di-n-Butylphthalate 10 U206-44-0 Fluoranthene 10 U'129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 15 B218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,i)Perylene 10 U

B: Cone, of Bis(2-Ethylhexyl)Phthalate 4 ug/1 IN METHOD BLANK(1) - Cannot be separated from DiphenylamineU; Not Detected

AR202702

NORTHEASTERN ANALYTICAL CORPORATION C C 7SEMIUOLATILE UNKNOWN IDENTIFICATION



SAMPLE UT/UOL:500/.5ML LEUEL:LOW


l.Ethene, tetrachloro- (9CI) 4.75 41UG/L J

2.Unknoujn 7.93 5UG/L 3

3.Unknown Aromatic * 17.80 110UG/L 3

4. Benzene, l/l'-oxybis- C9CI) 18.24 250UG/L 3

5.Unknown 23.74 4UG/L 3

6.Unknown 26.10 5UG/L J

7.Hexadecanoic acid C9CI) 26.33 5UG/L 3

f Estimated Concentration

AR202703

NORTHEASTERN ANALYTICAL CORPORATION £ r; g


'LAB SAMPLE iD:9iL355i-3R LAB FILE io:>D7778DATE EXTRACTED:11/29/91 DATE ANALYZED:911203



108-95-2 Phenol 20 U111-44-4 bis(2-Chloroethyl)ether 20 U95-57-8 2-Chlorophenol 20 U541-73-1 1,3-Dichlorobenzene 20 U106-46-7 1,4-Dichlorobenzene 20 U100-51-6 Benzyl Alcohol 20 U95-50-1 1,2-Dichlorobenzene 20 U95-48-7 2-Methylphenol 20 U39638-32-9 bis(2-Chloroisopropyl)ether 20 U106-44-5 4-Methylphenol 20 U621-64-7 N-Nitroso-di-n-propylamine 20 U67-72-1 Hexachloroethane 20 U98-95-3 Nitrobenzene 20 U78-59-1 Isophorone 20 U88-75-5 2-Nitrophenol 20 U105-67-9 2,4-Dimethylphenol 20 U65-85-0 Benzoic Acid 100 U111-91-1 bis(-2-Chloroethoxy)Methane 20 U120-83-2 2,4-Dichlorophenol 20 U120-82-1 1,2,4-Trichlorobenzene 20 U91-20-3 Naphthalene 20 U .106-47-8 4-Chloroaniline 20 U87-68-3 Hexachlorobutadiene 20 U59-50-7 4-Chloro-3-methylphenol 20 U91-57-6 2-Methylnaphthalene 20 U ,77-47-4 Hexachlorocyclopentadiene 20 U88-06-2 2,4,6-Trichlorophenol 20 U95-95-4 2,4,5-Trichlorophenol 100 U91-58-7 2-Chloronaphthalene 20 U88-74-4 2-Nitroaniline 100 U131-11-3 Dimethylphthalate 20 U208-96-8 Acenaphthylene 20 U99-09-2 3-Nitroaniline 100 U

U; Not Detected

AR202701*


SEMI -VOLATILE ORGANIC ANALYSIS DATA SHEET

LAB SAMPLE ID: 91L3551-3R LAB FILE ID:>D7778

DATE EXTRACTED: 11/2 9/91 DATE ANALYZED: 911203

SAMPLE WT/VOL:500/1ML LEVEL: LOW

GAS NO. MDL CONC. UG/L

83-32-9 Acenaphthene ' 20 U51-28-5 2,4-Dinitrophenol 100 U100-02-7 4-Nitrophenol 100 U132-64-9 Dibenzofuran 20 U121-14-2 2,4-Dinitrotoluene 20 U606-20-2 2 , 6-Dinitrotoluene 20 U84-66-2 Diethylphthalate 20 U7005-72-3 4-Chlorophenyl-phenylether 20 U86-73-7 Fluorene 20 U100-01-6 4-Nitroaniline 100 U534-52-1 4,6-Dinitro-2-methylphenol 100 . U86-30-6 N-Nitrosodiphenylamine (1) 20 U101-55-3 4-Bromophenyl-phenylether 20 U118-74-1 Hexachlorobenzene 20 U87-86-5 Pentachlorophenol 100 U85-01-8 Phenanthrene 20 U120-12-7 Anthracene 20 U84-74-2 Di-n-Butylphthalate 20 U206-44-0 Fluoranthene 20 U129-00-0 Pyrene 20 U85-68-7 Butylbenzylphthalate 20 U91-94-1 3,3'-Dichlorobenzidine 40 u56-55-3 Benzo( a) Anthracene 20 U117-81-7 Bis(2-Ethylhexyl)Phthalate 20 9 J B218-01-9 Chrysene 20 U117-84-0 Di-n-octylphthalate 20 U205-99-2 Benzo(b)fluoranthene 20 u207-08-9 Benzo (k) Fluoranthene 20 U50-32-8 Benzo (a) Pyrene 20 U193-39-5 Indeno(l, 2 ,3-cd) Pyrene 20 U53-70-3 Dibenzo( a, h) Anthracene 20 U191-24-2 Benzo (g,h, i) Perylene 20 U

B: Cone, of Bis(2-Ethylhexyl)Phthalate 6UG/L IN METHOD BLANK(1) - Cannot be separated from DiphenylamineU; Not Detected

J; below the limits of reliable quantitation

AR202705

NORTHEASTERN ANALYTICAL CORPORATION C (~"\SEI1IUOLATILE UNKNOWN IDENTIFICATION '->' U

LAB SAMPLE ID:91L3551-3R LAB FILE ID:>D7778

'DATE EXTRACTED:ll/29/91 DATE ANALYZED : 9 11203

SAMPLE WT/UOL-.500/1ML LEUEL:LOW


1.Naphthalene, 2-ethenyl- C9CI) ' 17.71 10UG/L 3

2.Benzene, l,l'-oxybis- C9CI) 18.11 59UG/L 3

3', Estimated Concentration

AR202706

NORTHEASTERN ANALYTICAL CORPORATIONL- L JL






108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 U106-46-7 1,4-Dichlorobenzene 10 U100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 U95-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 U111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 U87-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 u91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 u88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroaniline 50 U

U; Not Detected

AR202707

NORTHEASTERN ANALYTICAL CORPORATION f ~* ~SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET - c.'





83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol - 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene • 10 U100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U20-12-7 Anthracene 10 U4-74-2 Di-n-Butylphthalate 10 1 J206-44-0 Fluoranthene 10 U129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 4JB218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U2Q5-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,iJPerylene 10 U

B: Cone, of Bis(2-Ethylhexyl)Phthalate 4 ug/1 IN METHOD BLANK(1) - Cannot be separated from DiphenylamineU; Not DetectedJ; below the limits of reliable quantitation

AR202708

NORTHEASTERN ANALYTICAL CORPORATIONSEMI VOLATILE UNKNOWN IDENTIFICATION ^ "* 7- vj <Ji


DATE EXTRACTED:11/22/91 DATE ANALYZED:911II

SAMPLE WT/UOL:1000/1ML LEUEL:LOW



1.2.

3.

4.

5.

6.

Unknown s i lane

Unknown silane

Unknown silane

Unknown s i lane

Unknown s i lane

Unknown s i lane

34.

35.

37.

38.

39.

40.

54

81

01

14

35

76

5 UG/L

7UG/L

7UG/L

6UG/L

5UG/L

4UG/L

3

3

3

3

3

3

AR202709

NORTHEASTERN ANALYTICAL CORPORATION CG4






108-95-2 Phenol 100 U111-44-4 bis(2-Chloroethyl)ether 100 U95-57-8 2-Chlorophenol 100 U541-73-1 1,3-Dichlorobenzene 100 U106-46-7 1,4-Dichlorobenzene 100 U100-51-6 Benzyl Alcohol 100 U95-50-1 1,2-Dichlorobenzene 100 39 J95-48-7 2-Methylphenol 100 U39638-32-9 bis(2-Chloroisopropyl)ether 100 U106-44-5 4-Methylphenol 100 U621-64-7 N-Nitroso-di-n-propylamine 100 • U67-72-1 Hexachloroethane 100 U98-95-3 Nitrobenzene 100 U78-59-1 Isophorone 100 U88-75-5 2-Nitrophenpl 100 U105-67-9 2,4-Dimethylphenol 100 U65-85-0 Benzoic Acid 500 U111-91-1 bis(-2-Chloroethoxy)Methane 100 U120-83-2 2,4-Dichlorophenol 100 U120-82-1 1,2,4-Trichlorobenzene 100 U91-20-3 Naphthalene 100 U106-47-8 4-Chloroaniline 100 U87-68-3 Hexachlorobutadiene 100 U59-50-7 4-Chloro-3-methylphenol 100 U91-57-6 2-Methylnaphthalene 100 U77-47-4 Hexachlorocyclopentadiene • 100 U88-06-2 2,4,6-Trichlorophenol 100 U95-95-4 2,4,5-Trichlorophenol 500 U91-58-7 2-Chloronaphthalene 100 U88-74-4 2-Nitroaniline . 500 U131-11-3 Dimethylphthalate 100 U208-96-8 Acenaphthylene 100 U99-09-2 3-NitroanIline 500 U


AR2027IO

NORTHEASTERN ANALYTICAL CORPORATION ^ ~U






83-32-9 Acenaphthene 100 U51-28-5 2,4-Dinitrophenol 500 U100-02-7 4-Nitrophenol 500 U132-64-9 Dibenzofuran 100 U121-14-2 2,4-Dinitrotoluene 100 U606-20-2 2,6-Dinitrotoluene 100 U84-66-2 Diethylphthalate 100 U7005-72-3 4-Chlorophenyl-phenylether 100 U86-73-7 Fluorene 100 U100-01-6 4-Nitroaniline 500 U534-52-1 4,6-Dinitro-2-methylphenol 500 U86-30-6 N-Nitrosodiphenylamine (1) 100 U101-55-3 4-Bromophenyl-phenylather 100 U118-74-1 Hexachlorobenzene 100 U87-86-5 Pentachlorophenol 500 U85-01-8 Phenanthrene 100 U120-12-7 Anthracene 100 U84-74-2 Di-n-Butylphthalate 100 U206-44-0 Fluoranthene 100 U129-00-0 Pyrene 100 U85-68-7 Butylbenzylphthalate 100 U91-94-1 3,3'-Dichlorobenzidine 200 U56-55-3 Benzo(a)Anthracene 100 U117-81-7 Bis(2-Ethylhexyl)Phthalate 100 U218-01-9 Chrysene 100 U117-84-0 Di-n-octylphthalate 100 U205-99-2 Benzo(b)fluoranthene 100 U207-08-9 Benzo(k)Fluoranthene 100 U50-32-8 Benzo(a)Pyrene 100 U193-39-5 Indeno(1,2,3-cd)Pyrene 100 U53-70-3 Dibenzo(a,h)Anthracene 100 U191-24-2 Benzo(g,h,i)Perylene 100 U(1) - Cannot be separated from DiphenylamineU; Not Detected

AR2027II

OL cNORTHEASTERN ANALYTICAL CORPORATIONSEMI VOLATILE UNKNOWN IDENTIFICATION





l.Ethene, tetrachloro- (9CI) . 4.73 54UG/L J

2.1,1'-Biphenyl C9CI) 17.81 270UG/L 3

3.Benzene, l,l'-oxybis- C9CI) 18.21 750UG/L 3


AR202712

NORTHEASTERN ANALYTICAL CORPORATION OC?


LAB SAMPLE ID:9113551-6 LAB FILE ID:>B8538



GAS NO. MDL CONC. ug/1

108-95-2 Phenol 100 13 J111-44-4 bis(2-Chloroethyl)ether 100 U95-57-8 2-Chlorophenol 100 U541-73-1 1,3-Dichlorobenzene 100 U106-46-7 1,4-Dichlorobenzene 100 54 J100-51-6 Benzyl Alcohol 100 U95-50-1 1,2-Dichlorobenzene 100 21095-48-7 2-Methylphenol 100 U39638-32-9 bis(2-Chloroisopropyl)ether 100 U106-44-5 4-Methylphenol ' 100 U621-64-7 N-Nitroso-di-n-propylamine 100 U67-72-1 Hexachloroethane 100 U98-95-3 Nitrobenzene 100 U78-59-1 Isophorone 100 U88-75-5 2-Nitrophenol 100 U105-67-9 2,4-Dimethylphenol 100 U65-85-0 Benzoic Acid 500 U111-91-1 bis(-2-Chloroethoxy)Methane 100 U120-83-2 2,4-Dichlorophenol 100 U120-82-1 1,2,4-Trichlorobenzene 100 U91-20-3 Naphthalene 100 U106-47-8 4-Chloroaniline 100 14087-68-3 Hexachlorobutadiene 100 U59-50-7 4-Chloro-3-methylphenol 100 U91-57-6 2-Methylnaphthalene 100 11 J77-47-4 Hexachlorocyclopentadiene 100 U88-06-2 2,4,6-Trichlorophenol 100 U95-95-4 2,4,5-Trichlorophenol 500 U91-58-7 2-Chloronaphthalene ' 100 U88-74-4 2-Nitroaniline 500 U131-11-3 Dimethylphthalate 100 U208-96-8 Acenaphthylene 100 U99-09-2 3-Nitroaniline 500 U

U; Not Detected

J; below the limits of reliable quantitation

AR2027I3

NORTHEASTERN ANALYTICAL CORPORATION GG3


LAB SAMPLE 10:9113551-6 . LAB FILE ID:>B8538




83-32-9 Acenaphthene 100 U51-28-5 2,4-Dinitrophenol 500 U100-02-7 4-Nitrophenol 500 U132-64-9 Dibenzofuran 100 U121-14-2 2,4-Dinitrotoluene 100 U606-20-2 2,6-Dinitrotoluene 100 U84-66-2 Diethylphthalate 100 U7005-72-3 4-Chlorophenyl-phenylether 100 U86-73-7 Fluorene 100 u100-01-6 4-Nitroaniline 500 U534-52-1 4,6-Dinitro-2-methylphenol 500 • U86-30-6 N-Nitrosodiphenylamine (1) 100 U101-55-3 4-Bromophenyl-phenylether 100 U118-74-1 Hexachlorobenzene 100 U87-86-5 Pentachlorophenol 500 U85-01-8 Phenanthrene 100 U120-12-7 Anthracene 100 U84-74-2 Di-n-Butylphthalate 100 U206-44-0 Fluoranthene 100 u129-00-0 Pyrene 100 U85-68-7 Butylbenzylphthalate 100 U91-94-1 3,3'-Dichlorobenzidine 200 U56-55-3 Benzo(a)Anthracene 100 U117-81-7 Bis(2-Ethylhexyl)Phthalate 100 U218-01-9 Chrysene 100 U117-84-0 Di-n-octylphthalate 100 U205-99-2 Benzo(b)fluoranthene 100 U207-08-9 Benzo(k)Fluoranthene 100 u50-32-8 Benzo(a)Pyrene 100 U193-39-5 Indeno(1,2,3-cd)Pyrene 100 U53-70-3 Dibenzo(a,h)Anthracene 100 U191-24-2 Benzo (g,h,i)Perylene 100 U(1) - Cannot be separated from DiphenylamineU; Not Detected

AR2027H*

r'-NORTHEASTERN ANALYTICAL CORPORATION•SEMIVOLATILE UNKNOWN IDENTIFICATION

LAB SAMPLE 10:9113551-6 LAB FILE ID:>B8538




l.Ethene, tetrachloro- C9CI) 5.68 60 ug/l 3

2.Benzene, chloro- (8CI9CI) 6.73 360 ug/1 J

3.Aniline CACNM8CI) 10.32 86 ug/1 3

4.Ch1oroan i 1 ine isomer 13.82 41 ug/1 3

5.1,1'-Biphenyl C9CI) 19.80 1500 ug/1 3

6.Unknown 19.25 2500 ug/1 3

7.1,l'-Biphenyl, 2-phenoxy- (9CI) 27.91 100 ug/1 3

3f Estimated Concentration

AR2027I5

NORTHEASTERN ANALYTICAL CORPORATION C i 0






108-95-2 Phenol 100 10 J111-44-4 bis(2-Chloroethyl)ether 100 U95-57-8 2-Chlorophenol 100 U541-73-1 1,3-Dichlorobenzene 100 U106-46-7 1,4-Dichlorobenzene 100 U100-51-6 Benzyl Alcohol 100 U95-50-1 1,2-Dichlorobenzene 100 U95-48-7 2-Methylphenol 100 U39638-32-9 bis(2-Chloroisopropyl)ether 100 U106-44-5 4-Methylphenol 100 U621-64-7 N-Nitroso-di-n-propylamine 100 U67-72-1 Hexachloroethane 100 U98-95-3 Nitrobenzene 100 U78-59-1 Isophorone 100 U88-75-5 2-Nitrophenol 100 U105-67-9 2,4-Dimethylphenol 100 U65-85-0 Benzoic Acid 500 U111-91-1 bis(-2-Chloroethoxy)Methane 100 U120-83-2 2,4-Dichlorophenol 100 U120-82-1 1,2,4-Trichlorobenzene 100 U91-20-3 Naphthalene 100 U106-47-8 4-Chloroaniline 100 34087-68-3 Hexachlorobutadiene 100 U59-50-7 4-Chloro-3-methylphenol ioo U91-57-6 2-Methylnaphthalene 100 U77-47-4 Hexachlorocyclopentadiene 100 U88-06-2 2,4,6-Trichlorophenol 100 U95-95-4 2,4,5-Trichlorophenol 500 u91-58-7 2-Chloronaphthalene 100 U88-74-4 2-Nitroaniline 500 U131-11-3 Dimethylphthalate 100 U208-96-8 Acenaphthylene 100 U99-09-2 3-Nitroaniline 500 U


AR2027I6

C 7;NORTHEASTERN ANALYTICAL CORPORATION






83-32-9 Acenaphthene 100 U51-28-5 2,4-Dinitrophenol 500 U100-02-7 4-Nitrophenol 500 U132-64-9 Dibenzofuran 100 U121-14-2 2,4-Dinitrotoluene 100 U606-20-2 2,6-Dinitrotoluene 100 U84-66-2 Diethylphthalate 100 u7005-72-3 4-Chlorophenyl-phenylether 100 U86-73-7 Fluorene 100 U100-01-6 4-Nitroaniline 500 U534-52-1 4,6-Dinitro-2-methylphenol 500 U86-30-6 N-Nitrosodiphenylamine (1) 100 u101-55-3 4-Bromophenyl-phenylether 100 U118-74-1 Hexachlorobenzene 100 U87-86-5 Pentachlorophenol 500 U85-01-8 Phenanthrene 100 U120-12-7 Anthracene 100 U84-74-2 Di-n-Butylphthalate 100 U206-44-0 Fluoranthene 100 U129-00-0 Pyrene 100 U85-68-7 Butylbenzylphthalate 100 U91-94-1 3,3'-Dichlorobenzidine 200 U56-55-3 Benzo(a)Anthracene 100 U117-81-7 Bis(2-Ethylhexyl)Phthalate 100 U218-01-9 Chrysene 100 U117-84-0 Di-n-octylphthalate 100 U205-99-2 Benzo(b)fluoranthene 100 U207-08-9 Benzo(k)Fluoranthene 100 U50-32-8 Benzo(a)Pyrene 100 U193-39-5 Indeno(1,2,3-cd)Pyrene 100 U53-70-3 Dibenzo(a,h)Anthracene 100 U191-24-2 Benzo(g,h,i)Perylene 100 U(1) - Cannot be separated from DiphenylamineU; Not Detected

AR2027I7

NORTHEASTERN ANALYTICAL CORPORATIONSEMIUOLATILE UNKNOWN IDENTIFICATION CV'2

LAB SAMPLE ID:91L3551-7 LAB FILE ID:>D774S

DATE EXTRACTED:11/22/91 . DATE ANALYZED: 911127



1.Benzene, chloro- (8CI9CI) 5.81 230UG/L J

2.Benzene, l,l'-oxybis- C9CI) ' 18.22 1500UG/L 3

3.Unknown silane 34.52 65UG/L 3



3} Estimated Concentration

AR2027I8

NORTHEASTERN ANALYTICAL CORPORATION CY3






108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 4 J106-46-7 1,4-Dichlorobenzene 10 30100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 15095-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 2111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 9687-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroanlline 50 U


AR2027I9

NORTHEASTERN ANALYTICAL CORPORATION G V«±


B SAMPLE ID:91L3551-8 LAB FILE ID:>D7745

DATE EXTRACTED:11/22/91 . DATE ANALYZED:911127



83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 u100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (l) 10 U101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 U4-74-2 Di-n-Butylphthalate 10 U206-44-0 Fluoranthene 10 u129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 u117-81-7 Bis(2-Ethylhexyl)Phthalate 10 4 J B218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo (k) Fluoranthene 10 tr50-32-8 Benzo(a)Pyrene 10 u193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,i)Perylene 10 U


AR202720

NORTHEASTERN ANALYTICAL CORPORATIONSEMIUOLATILE UNKNOWN IDENTIFICATION




COMPOUND - RET TIME CONC

*

l.Ethene, tetrachloro- C9CI) 4.78 21UG/L J

2.Benzene, chldro- C8CI9CD 5.81 71UG/L 3

3.2,5-Cyclohexadiene-l,4-dione (9CI) 7.92 65UG/L 3

4.Unknown , 8.93 6UG/L 3

5.Aniline (ACNH8CI) 9.46 7UG/L 3



8.Methyl benzamine isomer 11.73 4UG/L 3

9.o-Chloroani1ine 12.93 19UG/L J

10.Benzene, 1,1'-oxybis- C9CI) 18.18 17UG/L 3

ll.Carbamic acid, phenyl-, ethyl ester C9CI 18.48 • 47UG/L J)


13.Carbamic acid, (4-chloropheny1)-, ethyl 21.72 19UG/L 3ester C9CI)


15.Urea, N,N'-diphony1- (9CI) 29.70 13UG/L J

3; Estimated Concentration

AR20272I







108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 24106-46-7 1,4-Dichlorobenzene 10 140100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 70095-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 • U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 3 J111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 5 J91-20-3 Naphthalene . 10 U106-47-8 4-Chloroaniline 10 2887-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 - 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroaniline 50 U


AR202722

r • ' NORTHEASTERN ANALYTICAL CORPORATION v » t'






83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene . 10 U100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Broraophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 1084-74-2 Di-n-Butylphthalate 10206-44-0 Fluoranthene 10129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 u91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 4 J218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,i)Perylene 10 U


AR202723

/•% t , ,-v

NORTHEASTERN ANALYTICAL CORPORATION (jSEMIVOLATILE UNKNOWN IDENTIFICATION

B SAMPLE ID,:91L3551-9 LAB FILE ID:>D7746




l.Ethene, tetrachloro- (9CI) 4.77 130UG/L J

2.Benzene, chloro- (8CI9CI) 5.82 110UG/L J

3.2,5-Cyclohexadiene-l,4-dione (9CI) 7.98 92UG/L J4.Unknown 8.18 4UG/L J


6.Unknown 8.61 5UG/L J7.Unknown 8.97 5UG/L J

8.Aniline (ACN)(SCI) 9.50 5UG/L J

pnknown 11.01 8UG/L J^Chloroaniline isomer 12.97 7UG/L J^ <

ll.Carbamic acid, phenyl-, methyl ester (9C 17.14 17UG/L JI)

12.Unknown Aromatic 17.82 22UG/L J13.Benzene, l,l'-oxybis- (9CI) 18.24 92UG/L J

14.Carbamic acid, phenyl-, ethyl ester (9CI 18.51 32UG/L J)

15.Unknown 20.25 4UG/L C

AR202721*

r ' •-.NORTHEASTERN ANALYTICAL CORPORATION v < JSEMIVOLATILE UNKNOWN IDENTIFICATION

B SAMPLE ID:91L3551-9 LAB FILE ID:>D7746




16.Unknown 20.56 5UG/L J17.Carbamic acid, (4-chlorophenyl)-, ethyl 21.75 11UG/L Jester (9CI)


19.Urea, N,N'-diphenyl- (9CI) 29.74 11UG/L J


AR202725



LAB SAMPLE .ID:91L3551-10R LAB FILE ID:>D7806




108-95-2 Phenol 400 U111-44-4 bis(2-Chloroethyl)ether 400 U95-57-8 2-Chlorophenol 400 U541-73-1 1,3-Dichlorobenzene 400 U106-46-7 1,4-Dichlorobenzene 400 44 J100-51-6 Benzyl Alcohol 400 U95-50-1 1,2-Dichlorobenzene 400 130 J95-48-7 2-Methylphenol 400 U39638-32-9 bis(2-Chloroisopropyl)ether 400 U106-44-5 4-Methylphenol 400 U621-64-7 N-Nitroso-di-n-propylamine 400 • U67-72-1 Hexachloroethane 400 U98-95-3 Nitrobenzene 400 U78-59-1 Isophorone 400 U88-75-5 2-Nitrophenol 400 U105-67-9 2,4-Dimethylphenol 400 U65-85-0 Benzoic Acid 2000 U111-91-1 bis(-2-Chloroethoxy)Methane 400 U120-83-2 2,4-Dichlorophenol 400 U120-82-1 1,2,4-Trichlorobenzene 400 U91-20-3 Naphthalene 400 U106-47-8 4-Chloroaniline 400 U87-68-3 Hexachlorobutadiene 400 U59-50-7 4-Chloro-3-methylphenol 400 U91-57-6 2-Methylnaphthalene 400 U77-47-4 Hexachlorocyclopentadiene 400 U88-06-2 2,4,6-Trichlorophenol 400 U95-95-4 2,4,5-Trichlorophenol 2000 U91-58-7 2-Chloronaphthalene 400 U88-74-4 2-Nitroaniline 2000 U131-11-3 Dimethylphthalate 400 U208-96-8 Acenaphthylene 400 U99-09-2 3-Nitroaniline 2000 U


AR202726

NORTHEASTERN ANALYTICAL CORPORATION f -t- jr.SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET

LAB. SAMPLE ID:91L3551-10R LAB FILE ID:>D7806




83-32-9 Acenaphthene 400 U51-28-5 2,4-Dinitrophenol 2000 U100-02-7 4-Nitrophenol 2000 U132-64-9 Dibenzofuran 400 U121-14-2 2,4-Dinitrotoluene 400 U606-20-2 2,6-Dinitrotoluene 400 U84-66-2 Diethylphthalate 400 U7005-72-3 4-Chlorophenyl-phenylether 400 U86-73-7 Fluorene 400 U100-01-6 4-Nitroaniline 2000 U534-52-1 4,6-Dinitro-2-methylphenol 2000 U86-30-6 N-Nitrosodiphenylamine (1) 400 U101-55-3 4-Bromophenyl-phenylether 400 U118-74-1 Hexachlorobenzene 400 U87-86-5 Pentachlorophenol 2000 U85-01-8 Phenanthrene 400 U120-12-7 Anthracene 400 U84-74-2 Di-n-Butylphthalate• 400 U206-44-0 Fluoranthene 400 U129-00-0 Pyrene 400 U85-68-7 Butylbenzylphthalate 400 U91-94-1 3,3'-Dichlorobenzidine 800 U56-55-3 Benzo(a)Anthracene 400 U117-81-7 Bis(2-Ethylhexyl)Phthalate 400 110 J B218-01-9 Chrysene 400 U117-84-0 Di-n-octylphthalate 400 U205-99-2 Benzo(b)fluoranthene 400 U207-08-9 Benzo(k)Fluoranthene 400 U50-32-8 Benzo(a)Pyrene 400 U193-39-5 Indeno(1,2,3-cd)Pyrene 400 U53-70-3 Dibenzo(a,h)Anthracene 400 U191-24-2 Benzo(g,h,i)Perylene 400 U

B: Cone, of Bis(2-Ethylhexyl)Phthalate 6UG/L IN METHOD BLANK(1) - Cannot be separated from DiphenylamineU; Not DetectedJ; below the limits of reliable quantitation

AR202727

CC2NORTHEASTERN ANALYTICAL CORPORATIONSEMIUOLATILE UNKNOWN IDENTIFICATION

LttB SAMPLE ID:91L3551-10R LAB FILE ID:>07806

DATE EXTRACTED: 12/04/91 _ DATE ANALYZED:9112 Do

SAMPLE WT/UOL:25ML/1ML LEMEL:LOW


1. Benzene, chloro- C.8CI9CI) 5.77 250UG/L J

2.Unknown aromatic 17.68 3000UG/L 3

3.Benzene, l,l'-oxybis- (9CI) ' 13.12 6800UG/L 3


AR202728

NORTHEASTERN ANALYTICAL CORPORATIONf ~O

SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET "WO

LAB SAMPLE ID:BLK#l-377 LAB FILE ID:>B84999111251841




108-95-2 Phenol ' 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 u541-73-1 1,3-Dichlorobenzene . 10 U106-46-7 1,4-Dichlorobenzene 10 U100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 U95-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nltrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 U111-91-1 bis(-2-Chloroethoxy)Methane 10 u120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 u87-68-3 Hexachlorobutadiene 10 u59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 ' u91-58-7 2-Chloronaphthalene 10 u88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate 10 U208-96-8 Acenaphthylene 10 u99-09-2 3-Nitroaniline 50 u

U; Not Detected

BR202729


SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET Jw^

iAB SAMPLE ID:BLK#l-377 LAB FILE ID:>B84999111251841

DATE' EXTRACTED:11/22/91 DATE ANALYZED:911125



83-32-9 Acenaphthene . 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 u84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 U100-01-6 4-Nitroaniline • 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (l) 10 • u101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 u34-74-2 Di-n-Butylphthalate 10 U206-44-0 Fluoranthene 10 U129-00-0 , Pyrene 10 u85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 u56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 4 J218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 u191-24-2 Benzo(g,h,i)Perylene 10 u(1)- Cannot be separated from DiphenylamineU; Not DetectedJ; below the limits of reliable quantitation

AR202730

NORTHEASTERN ANALYTICAL CORPORATIONSEMI VOLATILE UNKNOWN. IDENTIFICATION C*^





1.3-Penten-2-one C8CI9CH 4.10 5 ug/1 3

2.Unknown 5,24 8 ug/1 J


AR20273I


SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET t^O

LAB SAMPLE ID:BLK #2 -380 LAB FILE ID:>D77769112031128




108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 U106-46-7 1,4-Dichlorobenzene 10 U100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 U95-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene . 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 U111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 U87-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 U131-11-3 Dimethylphthalate • 10 U208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroaniline 50 U

U; Not Detected

AR202732


SEMI -VOLATILE ORGANIC ANALYSIS DATA SHEET "'7

B SAMPLE ID:BLK #2 -380 LAB FILE ID:>D77769112031128


SAMPLE WT/VOL:1000/1ML LEVEL': LOW


83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 U100-01-6 4-Nitroaniline 50 U534-52-1 . 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Bromophenyl-phenylether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 U4-74-2 Di-n-Butylphthalate 10 U'206-44-0 Fluoranthene 10 U129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 6 J218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 u53-70-3 Dibenzo(a,h)Anthracene 10 U191-24-2 Benzo(g,h,i)Perylene 10 U(1)- Cannot be separated from DiphenylamineU; Not DetectedJ; below the limits of reliable quantitation

AR202733

NORTHEASTERN ANALYTICAL CORPORATION fSEMIUOLATILE UNKNOWN IDENTIFICATION b

LAB SAMPLE ID:BLK *2 -380 LAB FILE ID :>9112031128

DATE EXTRACTED: 11/29/91 DATE ANALYZED : 9 1 120'

SAMPLE WT/UOL: 1000/1ML LEUEL:LOW


NONE FOUND

AR202731*

NORTHEASTERN ANALYTICAL CORPORATIONC"'3SEMI-VOLATILE ORGANIC ANALYSIS DATA SHEET ^J





108-95-2 Phenol 10 U111-44-4 bis(2-Chloroethyl)ether 10 U95-57-8 2-Chlorophenol 10 U541-73-1 1,3-Dichlorobenzene 10 U106-46-7 1,4-Dichlorobenzene 10 U100-51-6 Benzyl Alcohol 10 U95-50-1 1,2-Dichlorobenzene 10 U95-48-7 2-Methylphenol 10 U39638-32-9 bis(2-Chloroisopropyl)ether . 10 U106-44-5 4-Methylphenol 10 U621-64-7 N-Nitroso-di-n-propylamine 10 U67-72-1 Hexachloroethane 10 U98-95-3 Nitrobenzene 10 U78-59-1 Isophorone 10 U88-75-5 2-Nitrophenol 10 U105-67-9 2,4-Dimethylphenol 10 U65-85-0 Benzoic Acid 50 . U111-91-1 bis(-2-Chloroethoxy)Methane 10 U120-83-2 2,4-Dichlorophenol 10 U120-82-1 1,2,4-Trichlorobenzene 10 U91-20-3 Naphthalene 10 U106-47-8 4-Chloroaniline 10 U87-68-3 Hexachlorobutadiene 10 U59-50-7 4-Chloro-3-methylphenol 10 U91-57-6 2-Methylnaphthalene 10 U77-47-4 Hexachlorocyclopentadiene 10 U88-06-2 2,4,6-Trichlorophenol 10 U95-95-4 2,4,5-Trichlorophenol 50 U91-58-7 2-Chloronaphthalene 10 U88-74-4 2-Nitroaniline 50 u131-11-3 Dimethylphthalate 10 u208-96-8 Acenaphthylene 10 U99-09-2 3-Nitroanlline 50 u

U; Not Detected

AR202735

NORTHEASTERN ANALYTICAL CORPORATIONl/LU






83-32-9 Acenaphthene 10 U51-28-5 2,4-Dinitrophenol 50 U100-02-7 4-Nitrophenol 50 U132-64-9 Dibenzofuran 10 U121-14-2 2,4-Dinitrotoluene 10 U606-20-2 2,6-Dinitrotoluene 10 U84-66-2 Diethylphthalate 10 U7005-72-3 4-Chlorophenyl-phenylether 10 U86-73-7 Fluorene 10 U100-01-6 4-Nitroaniline 50 U534-52-1 4,6-Dinitro-2-methylphenol 50 U86-30-6 N-Nitrosodiphenylamine (1) 10 U101-55-3 4-Bromophenyl-phenyl-ether 10 U118-74-1 Hexachlorobenzene 10 U87-86-5 Pentachlorophenol 50 U85-01-8 Phenanthrene 10 U120-12-7 Anthracene 10 U84-74-2 Di-n-Butylphthalate 10 U206-44-0 Fluoranthene 10 U129-00-0 Pyrene 10 U85-68-7 Butylbenzylphthalate 10 U91-94-1 3,3'-Dichlorobenzidine 20 U56-55-3 Benzo(a)Anthracene 10 U117-81-7 Bis(2-Ethylhexyl)Phthalate 10 6 J218-01-9 Chrysene 10 U117-84-0 Di-n-octylphthalate 10 U205-99-2 Benzo(b)fluoranthene 10 U207-08-9 Benzo(k)Fluoranthene 10 U50-32-8 Benzo(a)Pyrene 10 U193-39-5 Indeno(1,2,3-cd)Pyrene 10 U53-70-3 Dibenzo(a,h)Anthracene 10 u191-24-2 Benzo(g,h,i)Perylene 10 U(l) - Cannot be separated from DiphenylamineU; Not DetectedJ; below the limits of reliable quantitation

SR202736

NORTHEASTERN ANALYTICAL CORPORATION f - vSEMIUOLATILE UNKNOWN IDENTIFICATION ^"--t





NONE FOUND

AR202737

NORTHEASTERN ANALYTICAL CORPORATION CC'2

SEMI-VOLATILE METHOD BLANK SUMMARY SHEET




EXTRACTION METHOD:CONT



91L3551-1 >D7741 11/27/91 13:18

91L3551-2 >D7742 11/27/91 14:11

91L3551-4 >D7744 11/27/91 16:07

91L3551-5 >D7747 11/27/91 'l8:47

9113551-6 >B8538 11/27/91 19:19

91L3551-7 >D7748 11/27/91 20:12

91L3551-8 >D7745 11/27/91 17:01

91L3551-9 >D7746 11/27/91 17:54

AR202738

NORTHEASTERN ANALYTICAL CORPORATION r?->

SEMI-VOLATILE METHOD BLANK SUMMARY SHEET




EXTRACTION METHOD:CONT



91L3551-3R >D7778 12/03/91 13:17

AR202739

NORTHEASTERN ANALYTICAL CORPORATION • .SEMI-VOLATILE METHOD BLANK SUMMARY SHEET




EXTRACTION METHODICONT



91L3551-10R ' >D7806 12/06/91 12:37

AR2027«40

CDNORTHEASTERN ANALYTICAL CORPORATION



Pesticides & Polychlorinated Biphenyls

Sample Designation

DetectionParameter 91L-3551-1 Limit

Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC . ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p«-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND " 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0

Units (ug/1) (ug/1)NO: Not Detected.




Pesticides & Polychlorinated Biphenyls (Continued)

Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND '0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan TI ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,

. as Aroclor 1016 ND 0.50

. as Aroclor 1221 .ND 0.50







AR20271*

97NORTHEASTERN ANALYTICAL CORPORATION'



Pesticides & Polychlorinated Biphenvls (Continued)

Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND ' 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


AR2Q27l*3





Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


AR2027UI*

99NORTHEASTERN ANALYTICAL CORPORATION



• . Pesticides & Polychlorinated Biphenyls (Continued)

Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND • 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0

Units (ug/1) (ug/1)

ND: Not Detected.

AR2027t*5

1C-0NORTHEASTERN ANALYTICAL CORPORATION

Test Report NO. NAC91L-3551Ciba-Geigy Corporation


• Pesticides & Polychlorinated Biphenyls (Continued)

Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND .0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0

Units (ug/1) (ug/1)ND: Not Detected.




• Pesticides & Polychlorinated Biphenvls (Continued)

Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ' ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND o.osoEndosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 -ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


flR2027i*7





Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND ' 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND 1.0Polychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


AR2027U8





Sample Designation


Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND l.oPolychlorinated Biphenyls,. as Aroclor 1016 ND 0.50, as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


AR2027t*9




Pesticides & Polychlorinated Biphenvls (Continued)

Sample Designation


Aldrin ND 1.0alpha BHC ND 1.0beta BHC ND 1.0gamma BHC ND 1.0delta BHC ND 1.0Chlordane ND ' 10Dieldrin ND 2.0p,p'-DDE ND 2.0p,p'-DDT ND 2.0p,p'-DDD ND 2.0Endosulfan I ND 1.0Endosulfan II ND 2.0Endosulfan Sulfate ND 2.0Endrin ND 2.0Endrin Aldehyde ND 1.0Heptachlor ND 1.0Heptachlor Epoxide ND 1.0Methoxychlor ND 0.30Toxaphene ND 20Polychlorinated Biphenyls,. as Aroclor 1016 ND 10. as Aroclor 1221 ND 10. as Aroclor 1232 ND 10. as Aroclor 1242 ND 10. as Aroclor 1248 ND 10. as Aroclor 1254 288 20. as Aroclor 1260 ND 20


AR202750





Sample Designation

DetectionParameter Method Blank Limit

Aldrin ND 0.050alpha BHC ND 0.050beta BHC ND 0.050gamma BHC ND 0.050delta BHC ND 0.050Chlordane ND 0.50Dieldrin ND 0.10p,p'-DDE ND 0.10p,p'-DDT ND 0.10p,p'-DDD ND 0.10Endosulfan I ND 0.050Endosulfan II ND 0.10Endosulfan Sulfate ND 0.10Endrin ND 0.10Endrin Aldehyde ND 0.050Heptachlor ND 0.050Heptachlor Epoxide ND 0.050Methoxychlor ND 0.30Toxaphene ND i.oPolychlorinated Biphenyls,. as Aroclor 1016 ND 0.50. as Aroclor 1221 ND 0.50. as Aroclor 1232 ND 0.50. as Aroclor 1242 ND . 0.50. as Aroclor 1248 ND 0.50. as Aroclor 1254 ND 1.0. as Aroclor 1260 ND 1.0


AR20275I



Client: CIBA-GEIGY CORPORATION Report #: 91L 3551Sample ID: 001 OUTFALL Nac ID: 3551-1

UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 200 UARSENIC 10 UBARIUM 3800BERYLLIUM 5.0 UCALCIUM 25000CADMIUM 110COBALT 50 UCHROMIUM 10 UCOPPER 25 UIRON 330MERCURY 2.0POTASSIUM 5000 UMAGNESIUM 8500MANGANESE 360SODIUM 27000NICKEL 56LEAD 12ANTIMONY " 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 410Q ,


—AR2Q2752




UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 200 UARSENIC 10 UBARIUM 1700-BERYLLIUM 5.0 UCALCIUM 49000CADMIUM 19COBALT 50 UCHROMIUM 10 UCOPPER 64IRON 38000MERCURY 4.0POTASSIUM 9900MAGNESIUM 8000MANGANESE 4800SODIUM 66000NICKEL 40 ULEAD 5.0 UANTIMONY 20SELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 3000 t





UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 1400ARSENIC 33BARIUM 2400BERYLLIUM 5.0 UCALCIUM 73000CADMIUM 5.0COBALT 50 UCHROMIUM 10 ' UCOPPER 25 UIRON 3300MERCURY 0.20 UPOTASSIUM 14000MAGNESIUM 14000MANGANESE 350SODIUM 100000NICKEL 40 ULEAD 5.0 UANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 2800


AR20275I4



Client: CIBA-GEIGY CORPORATION Report #: 91L 3551Sample ID: GWS COMPOSITE 1 Nac ID: 3551-5

UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 4900ARSENIC 11BARIUM 440BERYLLIUM 5.0 UCALCIUM 30000CADMIUM 15COBALT 74CHROMIUM 11COPPER 77IRON 19000MERCURY 0.20 UPOTASSIUM 5000MAGNESIUM 14000MANGANESE 2700SODIUM 47000NICKEL 40 ULEAD 10ANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC ,4100


——————————————————————flR2Q2755

^.-J




UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 1900ARSENIC 10 UBARIUM 3000BERYLLIUM 5.0 UCALCIUM 25000CADMIUM 32COBALT 50 UCHROMIUM 11COPPER 25 UIRON 24000MERCURY 0.20 UPOTASSIUM 9800MAGNESIUM 9500MANGANESE 1800SODIUM 130000NICKEL 40 ULEAD 33ANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 1600


AR202756




UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 6500ARSENIC 50BARIUM 700BERYLLIUM 5.0 UCALCIUM 51000CADMIUM 6600COBALT 50 UCHROMIUM 65COPPER 230IRON 81000MERCURY 71POTASSIUM 16000MAGNESIUM 10000MANGANESE 2800SODIUM 280000NICKEL 40 ULEAD 7800ANTIMONY' 10 USELENIUM 5.0 UTHALLIUM 29VANADIUM 78ZINC 47000t


*$ -t_: /

- 112NORTHEASTERN ANALYTICAL CORPORATION



UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 1200ARSENIC 10 UBARIUM 430BERYLLIUM 5.0 UCALCIUM 58000CADMIUM 130COBALT 150CHROMIUM 10 UCOPPER 34IRON 12000MERCURY 0.20 UPOTASSIUM 8800MAGNESIUM 10000MANGANESE 9500SODIUM 160000NICKEL 43LEAD 5.0 UANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 63000


AR202750M 202.15*




UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 7900ARSENIC 15BARIUM 200 UBERYLLIUM 5.0 UCALCIUM 73000CADMIUM 1200COBALT 220CHROMIUM 10 UCOPPER 62IRON 50000MERCURY 2.0POTASSIUM 11000MAGNESIUM 16000MANGANESE 16000SODIUM 160000NICKEL 87LEAD 140ANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 150000




Client: CIBA-GEIGY CORPORATION Report #: 91L 3551Sample ID: OF-6 OUTFALL Nac ID: 3551-10

UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 23000ARSENIC 130BARIUM 200BERYLLIUM 5.0 UCALCIUM 61000CADMIUM 25COBALT 50 UCHROMIUM 24COPPER 25 UIRON 63000MERCURY 0.20 UPOTASSIUM 11000MAGNESIUM 11000MANGANESE 2100SODIUM 130000NICKEL 40 ULEAD 21ANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 18000


-. -.ONORTHEASTERN ANALYTICAL CORPORATION


Client: CIBA-GEIGY CORPORATION Report #: 91L 3551Sample ID: METHOD BLANK WATER Nac ID: 3551-MBW

UNITS: ug/1

ELEMENT CONC FLAG

SILVER 10 UALUMINUM 200 UARSENIC 10 UBARIUM 200 UBERYLLIUM - 5 . 0 UCALCIUM 5000 UCADMIUM 5.0 UCOBALT 50 UCHROMIUM 10 UCOPPER 25 UIRON 100 UMERCURY 0.20 UPOTASSIUM 5000 UMAGNESIUM 5000 UMANGANESE 15 USODIUM 5000 UNICKEL 40 ULEAD 5.0 UANTIMONY 10 USELENIUM 5.0 UTHALLIUM 10 UVANADIUM 50 UZINC 20 U


AR20276I

1*.NORTHEASTERN ANALYTICAL CORPORATION ••Test Report No. NAC91L-3551



Parameter

Sample DetectionDesignation Cyanide ' Limit

91L-3551-1 ND 2091L-3551-3 ND 2091L-3551-4 ND 2091L-3551-5 ND 2091L-3551-6 ND 2091L-3551-7 26 2091L-3551-8 ND 2091L-3551-9 ND 2091L-3551-10 ND 20Method Blank ND 10

Units (ug/1) (ug/1)

NO: Not Detected.

AR202762

NORTHEASTERN ANALYTICAL CORPORATION A fVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY

* INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLORO

BENZENE ETHENE(88-110) (86-115) (76-114)

>C1626 11/27/91 91L-3551-1 97 96 101

>C1643 11/27/91 91L-3551-2 101 93 94

>C1627 11/27/91 91L-3551-3 103 93 108

>C1628 11/27/91 91L-3551-4 102 97 108

>A3740 11/26/91 91L-3551-5 100 92 94

>A3741 11/26/91 91L-3551-6 95 93 92

>C1618 11/26/91 911-3551-7 111* 103 102

>C1629 11/27/91 91L-3551-8 110 103 115*

>C1620 11/26/91 91L-3551-9 100 94 109>A3766 11/27/91 91L-3551-10 94 89 90

>C1508 11/19/91 91L-3551-11 99 95 109

AR202763

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY

* INDICATES RECOVERY OUTSIDE OF RANGE i*

INSTRUMENT CDATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLORO

• BENZENE ETHENE(88-110) (86-115) (76-114)

>C1638 11/27/91 METHOD BLANK 99 92 98

AR20276I*

NORTHEASTERN ANALYTICAL CORPORATION ' .VOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY ~~"

* INDICATES RECOVERY OUTSIDE OF RANGEINSTRUMENT C

DATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLOROBENZENE ETHENE

(88-110) (86-115) (76-114)

>C1624 11/26/91 METHOD BLANK 98 92 101

AR202765

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY ''

-i-

* INDICATES RECOVERY OUTSIDE OF RANGE

INSTRUMENT CDATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLORO

BENZENE ETHENE(88-110) (86-115) (76-114)

>C1615 11/26/91 METHOD BLANK 104 94 101

AR202766

NORTHEASTERN ANALYTICAL CORPORATIONVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY JL. -v JL

* ' INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLORO

BENZENE ETHENE(88-110) (86-115) (76-114)

>C1502 11/19/91 METHOD BLANK 104 96 99

AR202767

NORTHEASTERN ANALYTICAL CORPORATION -L. VOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY

* INDICATES RECOVERY OUTSIDE OF RANGE

INSTRUMENT ADATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLORO

BENZENE ETHENE(88-110) (86-115) (76-114)

>A3762 11/27/91 METHOD BLANK 100 , 98 98

AR202768

NORTHEASTERN ANALYTICAL CORPORATION , _VOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY .i. 3

* INDICATES RECOVERY OUTSIDE OF RANGEINSTRUMENT A

DATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLOROBENZENE ETHENE

(88-110) (86-115) (76-114)>A3735 11/26/91 METHOD BLANK 96 96 96

AR202769

NORTHEASTERN ANALYTICAL CORPORATION "• ' AVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY - -*

* INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID TOLUENE-d8 BROMOFLOURO 1,2-DICHLOR

BENZENE ETHENE(88-110) (86-115) (76-114)

>C1692 12/03/91 91L-3534-7MS A 99 95 91

>C1693 12/03/91 91L-3534-7MSD 97 98 99

AR202770

NORTHEASTERN ANALYTICAL CORPORATION .. .SEMIVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY JL . i

* INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID NBZ FBP TPH PHL 2FP TBP

>D7741 11/27/91 91L3551-1 77 89 81 24 18* 51

>D7742 11/27/91 91L3551-2 63 69 72 5* 4* 5*

>D7778 12/03/91 91L3551-3R 95 90 103 65 54 70

>D7744 11/27/91 91L3551-4 71 79 75 47 43 54

>D7747 11/27/91 91L3551-5 30* 86 80 0* 0* 0*

>B8538 11/27/91 9113551-6 61 84 67 38 33 43

>D7748 11/27/91 91L3551-7 4.3 86 70 24 20* 15

>D7745 11/27/91 91L3551-8 82 85 81 3* 0* 0*

>D7746 11/27/91 91L3551-9 89 91 93 1* 0* 1*

>D7806 12/06/91 91L3551-10R 101 96 122 66 67 72

QC LIMITS(NBZ)=Nitrobenzene-d5 (35-114)(FBP)=2-Fluorobiphenyl (43-116)(TPH)=Terphenyl-d-14 (33-141)(PHL)=Phenol-d6 (10-94)(2FP)=2-Fuorophenol (21-100)(TBP)=2,4,6-Tribromophenol (10-123)

AR20277

NORTHEASTERN ANALYTICAL CORPORATION .. .. 0SEMIVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY - O

* •INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID NBZ FBP TPH PHL 2FP TBP

>B8499 11/25/91 BLK#l-377 85 101 143* 49 52 82


AR202772

NORTHEASTERN ANALYTICAL CORPORATIONSEMIVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY

* INDICATES RECOVERY OUTSIDE OF RANGE~t+ *•,

INSTRUMENT DDATA FILE DATE SAMPLE ID NBZ FBP TPH PHL 2FP TBP

>D7807 12/06/91 BLK #1 -381 100 105 121 69 74 70

QC LIMITS(NBZ)=Nitrobenzene-d5 (35-114)(FBP)=2-Fluorobiphenyl (43-116)(TPH)=Terphenyl-d-14 (33-141)(PHL)=Phenol-d6 (10-94)(2FP)=2-Fuorophenol (21-100)(TBP)=2,4,6-Tribromophenol , (10-123)

AR202773

NORTHEASTERN ANALYTICAL CORPORATIONSEMIVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY

* INDICATES RECOVERY OUTSIDE OF RANGE —

INSTRUMENT DDATA FILE DATE SAMPLE ID NBZ FBP TPH PHL 2FP TBP

>D7776 12/03/91 BLK #2 -380 94 89 102 86 73 85


AR20277k

NORTHEASTERN ANALYTICAL CORPORATIONSEMIVOLATILE AQUEOUS SURROGATE SPIKE PERCENT RECOVERY -

* INDICATES RECOVERY OUTSIDE OF RANGEDATA FILE DATE SAMPLE ID NBZ FBP TPH PHL 2FP TBP

>D7730 11/27/91 91L3638-2MS 86 89 87 41 43 50

>D7731 11/27/91 91L3638-2MSD 88 85 99 49 51 56


AR202775

-»• <~> (J



VII. QUALITY ASSURANCE DATA (Continued)

Pesticide & PCS Surrogate Recoveries

% Recovery

SampleDesignation Dibutylchlorendate

91L-3551-1 6391L-3551-2 6191L-3551-3 6991L-3551-4 8191L-3551-5 8591L-3551-6 5991L-3551-7 9291L-3551-8 6491L-3551-9 9,391L-3551-10 '*Method Blank 8991L-3249-1S 3491L-3249-1SD 28

QC Limits (19-164)

*: No surrogate recovery due to dilution.

AR202776



VII. QUALITY ASSURANCE DATA (Continued)

Matrix Spike and Matrix Spike Duplicate Recoveries

Sample Amount of Initial % Duplicate Relative %Parameter Spiked Spike, ug Recovery % Recovery Difference

Aldrin 3249-1 0.10 73 74 1.4gamma-BHC 3249-1 0.10 72 80 11Dieldrin 3249-1 0.20 68 72 5.7p,p'-DDT 3249-1 0.60 68 71 4.3Endrin 3249-1 0.20 50 55 9.5Heptachlor 3249-1 0.10 70 78 11Aluminum 3534-1 50 91 93 2.2Antimony 3551-1 1.2 67 63 6.2Arsenic 3551-1 0.50 117 118 85Barium 3534-1 50 97 98 1.0Beryllium 3534-1 1.2 94 94 0Cadmium 3534-1 1.2 84 78 7.4Calcium Control 120 120 —— ——Chromium 3534-1 5.0 96 92 4.2Cobalt 3534-1 12 106 100 5.8Copper 3534-1 6.2 88 86 2.3Iron 3534-1 25 93 92 1.1Lead 3551-1 0.50 108 105 2.8Magnesium Control 120 86 —— ——Manganese 3534-1 12 83 83 0Mercury 3551-3 0.10 107 111 3.7Nickel 3534-1 12 91 93 2.2Potassium 3534-1 120 89 —— ——Selenium 3551-1 0.25 95 . 104 9.0Sodium Control 120 88 —— ——Silver 3534-1 55 84 84 0Thallium 3551-1 0.62 88 91 3.3Vanadium 3534-1 12 99 99 0Zinc 3534-1 12 87 88 1.1Cyanide 3534-1 44 91 95 4.3

AR202777

NORTHEASTERN ANALYTICAL CORPORATIONAQUEOUS VOLATILE MATRIX SPIKE AND MATRIX SPIKE DUPLICATE

SAMPLE NAME:91L-3534-7 ANALYSIS DATE: 12/03/9

BATCH NO:362

COMPOUND SPIKE MS MSD SAM MS% MSD% RPDADDED CONC CONC CONC REC REC

1,1-Dichloroethene 50 41 45 ND 82 90 9Trichloroethene 50 45 44 ND 90 88 2Benzene 50 46 45 ND 92 90 2

Toluene 50 40 40 ND 80 80 0

Chlorobenzene 50 41 41 ND 82 82 0

UNITS OF CONCENTRATION ARE UG/L

QC LIMITS %REC RPD1,1-Dichloroethene 61-145 14Trichloroethene 71-120 14Benzene 76-127 11Toluene ' 76-125 13Chlorobenzene 75-130 13* INDICATES RECOVERY OUTSIDE OF LIMITS

RPD: 0 OUT OF 5 OUTSIDE OF LIMITSSPIKE RECOVERY: 0 OUT OF 10 OUTSIDE OF LIMITS

PAGE 1 OF 1

AR202778

NORTHEASTERN ANALYTICAL CORPORATIONAQUEOUS SEMIVOLATILE MATRIX SPIKE AND MATRIX SPIKE DUPLICATE

SAMPLE NAME:91L3638-2 ANALYSIS DATE:11/27/91

BATCH NO:377

COMPOUND SPIKE MS MSD SAM MS% MSD% RPDADDED CONC CONC CONC REC REC

Phenol 100 42 46 ND 42 46 9

2-Chlorophenol 100 57 62 ND 57 62 8

1,4-Dichlorobenzene 50 34 36 ND 68 72 6

N-Nitroso-di-n-propylamine 50 35 34 ND 70 68 31,2,4-Trichlorobenzene 50 23 27 ND 46 54 164-Chloro-3-methylphenol 100 44 57 ND 44 57 26Acenaphthene 50 26 26 ND 52 52 0

4-Nitrophenol 100 30 39 ND 30 39 26

2,4-Dinitrotoluene 50 29 32 ND 58 64 10^entachlorophenol 100 55 60 ND 55 60 9

Pyrene 50 49 52 ND 98 104 6

UNITS OF CONCENTRATION ARE UG/L

QC LIMITS %REC RPDPhenol 12- 89 422-Chlorophenol 27-123 401,4-Dichlorobenzene 36- 97 28N-Nitros9-di-n-propylamine 41-116 381,2,4-Trichlorobenzene 39- 98 284-Chloro-3-methylphenol 23-97 42Acenaphthene 46-118 314-Nitrophenol 10- 80 502,4-Dinitrotoluene 24-96 38Pentachlorophenol 9-103 50Pyrene 26-127 31* INDICATES RECOVERY OUTSIDE OF LIMITS

RPD: 0 OUT OF 11 OUTSIDE OF LIMITSSPIKE RECOVERY: o our OF 22 OUTSIDE OF LIMITSNOTE: DILUTION FACTOR NOT USED IN CALCULATING RECOVERIES

PAGE 1 OF 1AR202779



VIII. STATEMENT OF AUTHENTICATION

LABORATORY AUTHENTICATION STATEMENT FOR NJPDESCOMPLIANCE MONITORING

I certify under penalty of law, where applicable, thislaboratory meets the Laboratory Performance Standards andQuality Control requirements specified in N.J.A.C. 7:18, 40CFR 136 for Water and Wastewater Analyses and SW 846 forSolid Waste Analyses. I have personally examined and amfamiliar with the information contained in this report, andthat, based on my inquiry of those individuals immediatelyresponsible for obtaining the information, I believe thesubmitted information is true, accurate, complete, and meetsthe standards specified in N.J.A.C. 7:18, 40 CFR 136, and/orSW 846. I am aware that there are significant Penalties forsubmitting false information, including the possibility of afine and imprisonment.

Paul P. PainterLaboratory Director

AR202780

ar202627c '6 northeastern analytical corporation test report no. nac91l-3927 ciba-geigy...

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