appendix a3 raw chemical data - pops) toolkit pdr...n/a form 1a pesticide analysis report axys...

Appendix A3

Raw Chemical Data

Organo Chlorine Pesticide

Analysis Report

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration; X = result reported separately.

Approved by: ___________Jason MacKenzie___________ QA/QC Chemist

For Axys Internal Use Only [ XSL Template: Pest1A.xsl; Created: 14-Nov-2008 09:32:25; Application: XMLTransformer-1.9.15;Report Filename: Pest_PEST_HI_E1HI_L11831-1_Form1A_CL81_334S22_SJ925679.html; Workgroup: WG26811; Design ID: 595 ]

These pages are part of a larger report that may contain information necessary for full data evaluation. Results reported relate only to the sample tested.

AXYS METHOD MLA-028 Rev 05 CLIENT SAMPLE NO.08LAO029ASample Collection:N/A

Form 1APESTICIDE ANALYSIS REPORT

AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811

Project No. POP1406

Contract No.: 2607 Lab Sample I.D.: L11831-1

Matrix: TISSUE Sample Size: 10.2 g (wet)

Sample Receipt Date: 07-Oct-2008 Initial Calibration Date: BRACKETING CAL

Extraction Date: 24-Oct-2008 Instrument ID: HR GC/MS

Analysis Date: 31-Oct-2008 Time: 00:07:31 GC Column ID: DB5

Extract Volume (uL): 40 Sample Data Filename: CL81_334 S: 22

Injection Volume (uL): 1.0 Blank Data Filename: CL81_334 S: 21

Dilution Factor: N/A Opening Cal. Data Filename:Closing Cal. Data Filename:

CL81_334 S: 17CL81_334 S: 26

Concentration Units: ng/g (wet weight basis) % Lipid: 1.34

COMPOUND CAS NO. LAB FLAG 1 CONC.FOUND

DETECTIONLIMIT

ION ABUND.RATIO

RRT

Hexachlorobenzene 118-74-1 0.502 0.0049 1.28 1.000HCH, alpha 319-84-6 ND 0.0061HCH, beta 319-85-7 ND 0.0049HCH, gamma 58-89-9 ND 0.0049HCH, delta 319-86-8 XHeptachlor 76-44-8 ND 0.0049Aldrin 309-00-2 ND 0.0049Chlordane, oxy- 27304-13-8 NDR 0.078 0.0049 1.11 1.001Chlordane, gamma (trans) 5103-74-2 0.030 0.0049 1.09 1.001Chlordane, alpha (cis) 5103-71-9 0.245 0.0049 1.08 1.026Nonachlor, trans- 39765-80-5 0.337 0.0049 1.20 1.001Nonachlor, cis- 5103-73-1 0.231 0.0049 1.16 1.0012,4'-DDD 53-19-0 ND 0.00974,4'-DDD 72-54-8 1.14 0.0109 1.62 1.0002,4'-DDE 3424-82-6 ND 0.00714,4'-DDE 72-55-9 5.14 0.0075 1.65 1.0002,4'-DDT 789-02-6 ND 0.01744,4'-DDT 50-29-3 0.383 0.0197 1.77 1.001Mirex 2385-85-5 0.010 0.0049 0.55 1.001

Page 1 of 1 (WG26811 - Pest_PEST_HI_E1HI_L11831-1_Form1A_CL81_334S22_SJ925679.html)

(1) Where applicable, custom lab flags have been used on this report; X = result reported separately.(2) R% = percent recovery.


For Axys Internal Use Only [ XSL Template: Pest2.xsl; Created: 14-Nov-2008 09:32:25; Application: XMLTransformer-1.9.15;Report Filename: Pest_PEST_HI_E1HI_L11831-1_Form2_CL81_334S22_SJ925679.html; Workgroup: WG26811; Design ID: 595 ]


AXYS METHOD MLA-028 Rev 05 CLIENT SAMPLE NO.08LAO029ASample Collection:N/A

Form 2PESTICIDE ANALYSIS REPORT


Project No. POP1406


Matrix: TISSUE Sample Size: 10.2 g (wet)

Sample Receipt Date: 07-Oct-2008 Initial Calibration Date: BRACKETING CAL






CL81_334 S: 17CL81_334 S: 26

Concentration Units: ng absolute % Lipid: 1.34

LABELED COMPOUND LABFLAG 1

SPIKECONC.

CONC.FOUND

R(%) 2 ION ABUND.RATIO

RRT

13C-Hexachlorobenzene 16.0 9.32 58.3 1.34 0.79013C-beta-HCH 16.0 13.4 83.8 0.77 0.82413C-gamma-HCH 16.0 12.3 76.8 0.79 0.83313C-delta-HCH X13C-Heptachlor 16.0 13.8 86.1 1.17 0.96513C-Aldrin 16.0 12.8 80.0 1.65 1.03013C-Chlordane, oxy 16.0 15.9 99.3 1.41 1.11013C-Chlordane, gamma (trans) 16.0 10.8 67.3 1.24 0.83913C-Nonachlor, trans- 16.0 11.2 70.1 1.35 0.86713C-Nonachlor, cis- 16.0 11.7 73.2 1.25 0.95613C-2,4'-DDE 16.0 10.2 63.9 1.51 0.84613C-4,4'-DDE 40.6 29.9 73.6 1.51 0.89113C-4,4'-DDD 16.0 13.1 82.1 1.60 0.95013C-2,4'-DDT 16.0 12.3 76.7 1.57 0.95413C-4,4'-DDT 19.8 17.1 86.3 1.61 0.99613C-Mirex 16.0 11.8 73.5 1.26 1.085

Page 1 of 1 (WG26811 - Pest_PEST_HI_E1HI_L11831-1_Form2_CL81_334S22_SJ925679.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Pest1A.xsl; Created: 14-Nov-2008 09:32:25; Application: XMLTransformer-1.9.15;Report Filename: Pest_PEST_HI_E1HI_WG26811-101_Form1A_CL81_334S21_SJ925678.html; Workgroup: WG26811; Design ID: 595 ]


AXYS METHOD MLA-028 Rev 05 CLIENT SAMPLE NO.Lab BlankSample Collection:N/A

Form 1APESTICIDE ANALYSIS REPORT


Project No. N/A

Contract No.: 2607 Lab Sample I.D.: WG26811-101

Matrix: TISSUE Sample Size: 10.0 g

Sample Receipt Date: N/A Initial Calibration Date: BRACKETING CAL






CL81_334 S: 17CL81_334 S: 26

Concentration Units: ng/g

COMPOUND CAS NO. LAB FLAG 1 CONC.FOUND

DETECTIONLIMIT

ION ABUND.RATIO

RRT

Hexachlorobenzene 118-74-1 ND 0.0050HCH, alpha 319-84-6 ND 0.0050HCH, beta 319-85-7 ND 0.0050HCH, gamma 58-89-9 ND 0.0050HCH, delta 319-86-8 XHeptachlor 76-44-8 ND 0.0050Aldrin 309-00-2 ND 0.0050Chlordane, oxy- 27304-13-8 ND 0.0050Chlordane, gamma (trans) 5103-74-2 ND 0.0050Chlordane, alpha (cis) 5103-71-9 ND 0.0050Nonachlor, trans- 39765-80-5 ND 0.0050Nonachlor, cis- 5103-73-1 ND 0.00502,4'-DDD 53-19-0 ND 0.01184,4'-DDD 72-54-8 ND 0.01332,4'-DDE 3424-82-6 ND 0.00634,4'-DDE 72-55-9 ND 0.00782,4'-DDT 789-02-6 ND 0.01874,4'-DDT 50-29-3 ND 0.0228Mirex 2385-85-5 ND 0.0050

Page 1 of 1 (WG26811 - Pest_PEST_HI_E1HI_WG26811-101_Form1A_CL81_334S21_SJ925678.html)

(1) Where applicable, custom lab flags have been used on this report; X = result reported separately.(2) R% = percent recovery.


For Axys Internal Use Only [ XSL Template: Pest2.xsl; Created: 14-Nov-2008 09:32:25; Application: XMLTransformer-1.9.15;Report Filename: Pest_PEST_HI_E1HI_WG26811-101_Form2_CL81_334S21_SJ925678.html; Workgroup: WG26811; Design ID: 595 ]



Form 2PESTICIDE ANALYSIS REPORT


Project No. N/A


Matrix: TISSUE Sample Size: 10.0 g

Sample Receipt Date: N/A Initial Calibration Date: BRACKETING CAL






CL81_334 S: 17CL81_334 S: 26

Concentration Units: ng absolute


SPIKECONC.

CONC.FOUND

R(%) 2 ION ABUND.RATIO

RRT

13C-Hexachlorobenzene 16.0 7.20 45.0 1.36 0.78913C-beta-HCH 16.0 9.81 61.3 0.79 0.82313C-gamma-HCH 16.0 11.2 70.2 0.80 0.83313C-delta-HCH X13C-Heptachlor 16.0 10.7 66.7 1.36 0.96413C-Aldrin 16.0 10.4 64.7 1.56 1.03013C-Chlordane, oxy 16.0 13.6 85.1 1.63 1.11013C-Chlordane, gamma (trans) 16.0 14.0 87.5 1.31 0.83813C-Nonachlor, trans- 16.0 13.3 83.3 1.27 0.86713C-Nonachlor, cis- 16.0 14.0 87.3 1.12 0.95513C-2,4'-DDE 16.0 12.9 80.7 1.52 0.84613C-4,4'-DDE 40.6 34.6 85.1 1.52 0.89013C-4,4'-DDD 16.0 14.9 93.1 1.57 0.94913C-2,4'-DDT 16.0 15.3 95.3 1.59 0.95413C-4,4'-DDT 19.8 19.0 95.7 1.59 0.99613C-Mirex 16.0 13.9 86.6 1.29 1.085

Page 1 of 1 (WG26811 - Pest_PEST_HI_E1HI_WG26811-101_Form2_CL81_334S21_SJ925678.html)

(1) Where applicable, custom lab flags have been used on this report; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Pest8A.xsl; Created: 14-Nov-2008 09:32:25; Application: XMLTransformer-1.9.15;Report Filename: Pest_PEST_HI_E1HI_WG26811-102_Form8A_SJ925676.html; Workgroup: WG26811; Design ID: 595 ]


AXYS METHOD MLA-028 Rev 05Form 8A

PESTICIDE ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 OPR Data Filename: CL81_334 S: 18

Matrix: TISSUE Lab Sample I.D.: WG26811-102

Extraction Date: 24-Oct-2008 Analysis Date: 30-Oct-2008 Time: 21:38:50

ALL CONCENTRATIONS REPORTED ON THIS FORM ARE CONCENTRATIONS IN EXTRACT, BASED ON 100 uL EXTRACT.

COMPOUND CAS NO. LABFLAG 1

IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)

OPR CONC.LIMITS(ng/mL)

%RECOVERY

Hexachlorobenzene 118-74-1 1.24 80.0 79.0 56.0 - 104 98.8HCH, alpha 319-84-6 0.77 160 127 112 - 208 79.3HCH, beta 319-85-7 0.77 160 157 112 - 208 98.1HCH, gamma 58-89-9 0.79 160 162 112 - 208 101HCH, delta 319-86-8 XHeptachlor 76-44-8 1.20 81.0 81.9 56.7 - 105 101Aldrin 309-00-2 1.58 160 149 112 - 208 93.2Chlordane, oxy- 27304-13-8 1.52 160 147 112 - 208 91.6Chlordane, gamma (trans) 5103-74-2 1.17 160 152 112 - 208 94.8Chlordane, alpha (cis) 5103-71-9 1.23 160 153 112 - 208 95.5Nonachlor, trans- 39765-80-5 1.14 160 162 112 - 208 101Nonachlor, cis- 5103-73-1 1.16 160 170 112 - 208 1062,4'-DDD 53-19-0 1.66 82.0 81.3 57.4 - 107 99.14,4'-DDD 72-54-8 1.68 82.0 77.2 57.4 - 107 94.22,4'-DDE 3424-82-6 1.64 82.0 80.1 57.4 - 107 97.74,4'-DDE 72-55-9 1.69 80.0 81.4 56.0 - 104 1022,4'-DDT 789-02-6 1.79 82.0 82.2 57.4 - 107 1004,4'-DDT 50-29-3 1.76 81.0 74.7 56.7 - 105 92.2Mirex 2385-85-5 0.47 81.0 79.9 56.7 - 105 98.6

Page 1 of 1 (WG26811 - Pest_PEST_HI_E1HI_WG26811-102_Form8A_SJ925676.html)

(1) Where applicable, custom lab flags have been used on this report; X = result reported separately.


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AXYS METHOD MLA-028 Rev 05Form 8B

PESTICIDE ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 OPR Data Filename: CL81_334 S: 18

Matrix: TISSUE Lab Sample I.D.: WG26811-102

Extraction Date: 24-Oct-2008 Analysis Date: 30-Oct-2008 Time: 21:38:50

ALL CONCENTRATIONS REPORTED ON THIS FORM ARE CONCENTRATIONS IN EXTRACT, BASED ON 100 uL EXTRACT.

LABELEDCOMPOUND

CAS NO. LABFLAG 1

IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

13C-Hexachlorobenzene 1.31 160 74.7 32.0-240 46.713C-beta-HCH 0.80 160 97.7 48.0-240 61.113C-gamma-HCH 0.79 160 112 47.9-240 69.913C-delta-HCH X13C-Heptachlor 1.28 160 115 48.0-240 71.613C-Aldrin 1.51 160 108 48.0-240 67.713C-Chlordane, oxy 1.52 160 135 48.0-320 84.513C-Chlordane, gamma (trans) 1.29 160 139 48.0-320 86.813C-Nonachlor, trans- 1.26 160 127 48.0-240 79.613C-Nonachlor, cis- 1.33 160 135 48.0-240 84.513C-2,4'-DDE 1.54 160 132 64.0-240 82.213C-4,4'-DDE 1.49 406 308 163-610 75.813C-4,4'-DDD 1.63 160 140 64.0-240 87.513C-2,4'-DDT 1.61 160 149 64.0-240 93.313C-4,4'-DDT 1.57 198 200 79.4-298 10113C-Mirex 1.31 160 141 48.0-240 88.2

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PCB Analysis Report

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; C = co-eluting congener; D = dilution data.(2) Concentrations that do not meet quantification criteria are not included in the TEQ calculations.


For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 01-Dec-2008 18:10:50; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_L11830-2_TEQ_SJ934801.html; Workgroup: WG26760; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.08LAO010BForm 1C

PCB CONGENER TEQ ANALYSIS REPORTAXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811

Sample Collection: N/A

Contract No.: 2607 Project No. POP1406

Matrix: SOIL Lab Sample I.D.: L11830-2

Sample Size: 9.79 g (dry) GC Column ID(s): SPB OCTYL

Concentration Units: pg/g (dry weight basis) Sample Data Filename(s): PB8B_315 S: 6PB8C_452 S: 3

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 1998TEF

ND=0 ND=1/2 DL ND=DL

3,3',4,4'-TeCB 77 662 2.08 0.0001 6.62e-02 6.62e-023,4,4',5-TeCB 81 17.9 2.07 0.0001 1.79e-03 1.79e-032,3,3',4,4'-PeCB 105 1600 6.14 0.0001 1.60e-01 1.60e-012,3,4,4',5-PeCB 114 59.8 6.21 0.0005 2.99e-02 2.99e-022,3',4,4',5-PeCB 118 7970 5.82 0.0001 7.97e-01 7.97e-012',3,4,4',5-PeCB 123 172 6.03 0.0001 1.72e-02 1.72e-023,3',4,4',5-PeCB 126 637 6.83 0.1 6.37e+01 6.37e+012,3,3',4,4',5-HxCB 156 156 + 157 C 15000 9.69 0.0005 7.50e+00 7.50e+002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 14000 7.24 0.00001 1.40e-01 1.40e-013,3',4,4',5,5'-HxCB 169 ND 521 0.01 0.00e+00 2.61e+002,3,3',4,4',5,5'-HpCB 189 9190 29.3 0.0001 9.19e-01 9.19e-01

TOTAL TEQ 73.3 75.9TEQ

COMPOUND IUPACNO.

COELUTIONS LABFLAG 1

CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 662 2.08 0.0001 6.62e-02 6.62e-023,4,4',5-TeCB 81 17.9 2.07 0.0003 5.37e-03 5.37e-032,3,3',4,4'-PeCB 105 1600 6.14 0.00003 4.80e-02 4.80e-022,3,4,4',5-PeCB 114 59.8 6.21 0.00003 1.79e-03 1.79e-032,3',4,4',5-PeCB 118 7970 5.82 0.00003 2.39e-01 2.39e-012',3,4,4',5-PeCB 123 172 6.03 0.00003 5.16e-03 5.16e-033,3',4,4',5-PeCB 126 637 6.83 0.1 6.37e+01 6.37e+012,3,3',4,4',5-HxCB 156 156 + 157 C 15000 9.69 0.00003 4.50e-01 4.50e-012,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 14000 7.24 0.00003 4.20e-01 4.20e-013,3',4,4',5,5'-HxCB 169 ND 521 0.03 0.00e+00 7.82e+002,3,3',4,4',5,5'-HpCB 189 9190 29.3 0.00003 2.76e-01 2.76e-01

TOTAL TEQ 65.2 73.0

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For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 01-Dec-2008 18:10:50; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_L11830-5_TEQ_SJ934802.html; Workgroup: WG26760; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.08LAO032BForm 1C




Matrix: SOIL Lab Sample I.D.: L11830-5

Sample Size: 10.1 g (dry) GC Column ID(s): SPB OCTYL

Concentration Units: pg/g (dry weight basis) Sample Data Filename(s): PB8B_315 S: 7PB8C_452 S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 1998TEF


3,3',4,4'-TeCB 77 6350 18.8 0.0001 6.35e-01 6.35e-013,4,4',5-TeCB 81 426 18.1 0.0001 4.26e-02 4.26e-022,3,3',4,4'-PeCB 105 33000 0.820 0.0001 3.30e+00 3.30e+002,3,4,4',5-PeCB 114 2070 12.2 0.0005 1.04e+00 1.04e+002,3',4,4',5-PeCB 118 125000 0.820 0.0001 1.25e+01 1.25e+012',3,4,4',5-PeCB 123 1010 12.5 0.0001 1.01e-01 1.01e-013,3',4,4',5-PeCB 126 ND 10.4 0.1 0.00e+00 5.20e-012,3,3',4,4',5-HxCB 156 156 + 157 C 105000 40.7 0.0005 5.25e+01 5.25e+012,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 41100 29.4 0.00001 4.11e-01 4.11e-013,3',4,4',5,5'-HxCB 169 ND 524 0.01 0.00e+00 2.62e+002,3,3',4,4',5,5'-HpCB 189 21900 26.6 0.0001 2.19e+00 2.19e+00


COMPOUND IUPACNO.


CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 6350 18.8 0.0001 6.35e-01 6.35e-013,4,4',5-TeCB 81 426 18.1 0.0003 1.28e-01 1.28e-012,3,3',4,4'-PeCB 105 33000 0.820 0.00003 9.90e-01 9.90e-012,3,4,4',5-PeCB 114 2070 12.2 0.00003 6.21e-02 6.21e-022,3',4,4',5-PeCB 118 125000 0.820 0.00003 3.75e+00 3.75e+002',3,4,4',5-PeCB 123 1010 12.5 0.00003 3.03e-02 3.03e-023,3',4,4',5-PeCB 126 ND 10.4 0.1 0.00e+00 5.20e-012,3,3',4,4',5-HxCB 156 156 + 157 C 105000 40.7 0.00003 3.15e+00 3.15e+002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 41100 29.4 0.00003 1.23e+00 1.23e+003,3',4,4',5,5'-HxCB 169 ND 524 0.03 0.00e+00 7.86e+002,3,3',4,4',5,5'-HpCB 189 21900 26.6 0.00003 6.57e-01 6.57e-01

TOTAL TEQ 10.6 19.0


(1) Where applicable, custom lab flags have been used on this report; ND = not detected.(2) All header information pertains to the initial instrumental analysis of the sample extract. Additional sample datafiles listed refer to secondary analysisof the sample extract.


For Axys Internal Use Only [ XSL Template: .xsl; Created: 01-Dec-2008 18:00:57; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_WG26760-101_Form1AHT_SJ931178.html; Workgroup: WG26760; Design ID: 925 ]



Form 1AHOMOLOGUE TOTAL PCB ANALYSIS REPORT


Project No. N/A


Matrix: SOLID Sample Size: 10.0 g

Sample Receipt Date: N/A Initial Calibration Date: 22-Oct-2008


Analysis Date: 15-Nov-2008 Time: 01:16:25 GC Column ID: SPB OCTYL

Extract Volume (uL): 20 Sample Data Filename: PB8C_447A S: 4

Injection Volume (uL): 1.0 Blank Data Filename: PB8C_447A S: 4

Dilution Factor: N/A Cal. Ver. Data Filename: PB8C_447A S: 1

Concentration Units: pg/g

PCB HOMOLOGUE GROUP LABFLAG 1

CONC.FOUND

Total Monochloro Biphenyls ND

Total Dichloro Biphenyls 1.21

Total Trichloro Biphenyls 1.85

Total Tetrachloro Biphenyls 10.5

Total Pentachloro Biphenyls 27.6

Total Hexachloro Biphenyls 49.4

Total Heptachloro Biphenyls 32.2

Total Octachloro Biphenyls 6.89

Total Nonachloro Biphenyls 0.186

Decachloro Biphenyl 0.250

TOTAL PCBs 130

Page 1 of 1 (WG26760 - 1668_PCB1668_HomTotals-TEQs_WG26760-101_Form1AHT_SJ931178.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; C = co-eluting congener.(2) Concentrations that do not meet quantification criteria are not included in the TEQ calculations.


For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 01-Dec-2008 18:10:50; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_WG26760-101_TEQ_SJ931178.html; Workgroup: WG26760; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.Lab BlankForm 1C



Contract No.: 2607 Project No. N/A

Matrix: SOLID Lab Sample I.D.: WG26760-101

Sample Size: 10.0 g GC Column ID(s): SPB OCTYL

Concentration Units: pg/g Sample Data Filename(s): PB8C_447A S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 1998TEF


3,3',4,4'-TeCB 77 0.441 0.0595 0.0001 4.41e-05 4.41e-053,4,4',5-TeCB 81 ND 0.0600 0.0001 0.00e+00 3.00e-062,3,3',4,4'-PeCB 105 2.91 0.0829 0.0001 2.91e-04 2.91e-042,3,4,4',5-PeCB 114 0.186 0.0822 0.0005 9.30e-05 9.30e-052,3',4,4',5-PeCB 118 5.66 0.0802 0.0001 5.66e-04 5.66e-042',3,4,4',5-PeCB 123 ND 0.0831 0.0001 0.00e+00 4.16e-063,3',4,4',5-PeCB 126 ND 0.0863 0.1 0.00e+00 4.32e-032,3,3',4,4',5-HxCB 156 156 + 157 C 1.30 0.0662 0.0005 6.50e-04 6.50e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 0.373 0.0550 0.00001 3.73e-06 3.73e-063,3',4,4',5,5'-HxCB 169 ND 0.0585 0.01 0.00e+00 2.93e-042,3,3',4,4',5,5'-HpCB 189 0.223 0.0500 0.0001 2.23e-05 2.23e-05

TOTAL TEQ 0.00167 0.00628TEQ

COMPOUND IUPACNO.


CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 0.441 0.0595 0.0001 4.41e-05 4.41e-053,4,4',5-TeCB 81 ND 0.0600 0.0003 0.00e+00 9.00e-062,3,3',4,4'-PeCB 105 2.91 0.0829 0.00003 8.73e-05 8.73e-052,3,4,4',5-PeCB 114 0.186 0.0822 0.00003 5.58e-06 5.58e-062,3',4,4',5-PeCB 118 5.66 0.0802 0.00003 1.70e-04 1.70e-042',3,4,4',5-PeCB 123 ND 0.0831 0.00003 0.00e+00 1.25e-063,3',4,4',5-PeCB 126 ND 0.0863 0.1 0.00e+00 4.32e-032,3,3',4,4',5-HxCB 156 156 + 157 C 1.30 0.0662 0.00003 3.90e-05 3.90e-052,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 0.373 0.0550 0.00003 1.12e-05 1.12e-053,3',4,4',5,5'-HxCB 169 ND 0.0585 0.03 0.00e+00 8.78e-042,3,3',4,4',5,5'-HpCB 189 0.223 0.0500 0.00003 6.69e-06 6.69e-06

TOTAL TEQ 0.000364 0.00557

Page 1 of 1 (WG26760 - 1668_PCB1668_HomTotals-TEQs_WG26760-101_TEQ_SJ931178.html)


Form 1APCB CONGENER ANALYSIS REPORT


Project No. N/A










COMPOUND IUPACNO.

CO-ELUTIONS LABFLAG 1

CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 NDR 0.064 0.0500 2.27 1.0003-MoCB 2 ND 0.05004-MoCB 3 NDR 0.108 0.0500 7.18 1.000

2,2'-DiCB 4 ND 0.1082,3-DiCB 5 ND 0.07542,3'-DiCB 6 NDR 0.106 0.0672 1.31 1.1782,4-DiCB 7 ND 0.06932,4'-DiCB 8 0.133 0.0613 1.56 1.2112,5-DiCB 9 ND 0.06722,6-DiCB 10 ND 0.06613,3'-DiCB 11 0.974 0.0702 1.67 0.9693,4-DiCB 12 12 + 13 C ND 0.06963,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.06684,4'-DiCB 15 0.100 0.0742 1.57 1.000

2,2',3-TriCB 16 NDR 0.086 0.0500 1.55 1.1652,2',4-TriCB 17 NDR 0.072 0.0500 1.33 1.1382,2',5-TriCB 18 18 + 30 C 0.176 0.0500 1.19 1.1142,2',6-TriCB 19 ND 0.05002,3,3'-TriCB 20 20 + 28 C 0.482 0.0500 0.93 0.8482,3,4-TriCB 21 21 + 33 C ND 0.05002,3,4'-TriCB 22 0.230 0.0500 0.92 0.8722,3,5-TriCB 23 ND 0.05002,3,6-TriCB 24 ND 0.05002,3',4-TriCB 25 ND 0.05002,3',5-TriCB 26 26 + 29 C NDR 0.078 0.0500 0.86 1.3032,3',6-TriCB 27 ND 0.05002,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 0.354 0.0500 1.13 0.8362,4',6-TriCB 32 0.063 0.0500 1.13 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 0.05003,3',4-TriCB 35 ND 0.05003,3',5-TriCB 36 ND 0.05003,4,4'-TriCB 37 0.541 0.0500 0.93 1.0013,4,5-TriCB 38 ND 0.0500

Page 1 of 4 (WG26760 - 1668_PCB1668_PCBTF_WG26760-101_Form1A_PB8C_447AS4_SJ931178.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.05002,2',3,3'-TeCB 40 40 + 41 + 71 C 0.704 0.0500 0.76 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.270 0.0500 0.72 1.3142,2',3,5-TeCB 43 ND 0.05002,2',3,5'-TeCB 44 44 + 47 + 65 C NDR 0.911 0.0500 0.92 1.2872,2',3,6-TeCB 45 45 + 51 C 0.115 0.0500 0.69 1.1492,2',3,6'-TeCB 46 ND 0.05002,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 0.132 0.0500 0.79 1.2752,2',4,5'-TeCB 49 49 + 69 C 0.345 0.0500 0.81 1.2602,2',4,6-TeCB 50 50 + 53 C ND 0.05002,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 0.657 0.0500 0.80 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 0.05002,3,3',4-TeCB 55 ND 0.05772,3,3',4'-TeCB 56 1.37 0.0593 0.84 0.9052,3,3',5-TeCB 57 ND 0.05422,3,3',5'-TeCB 58 ND 0.05872,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.073 0.0500 1.42 1.3032,3,4,4'-TeCB 60 0.707 0.0588 0.67 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 3.37 0.0553 0.76 0.8752,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 0.05362,3,4',6-TeCB 64 0.441 0.0500 0.82 1.3502,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 1.96 0.0543 0.76 0.8842,3',4,5-TeCB 67 NDR 0.057 0.0500 0.42 0.8572,3',4,5'-TeCB 68 ND 0.05372,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.05302,3',5',6-TeCB 73 ND 0.05002,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 0.441 0.0595 0.88 1.0013,3',4,5-TeCB 78 ND 0.05623,3',4,5'-TeCB 79 ND 0.05003,3',5,5'-TeCB 80 ND 0.05313,4,4',5-TeCB 81 ND 0.0600

2,2',3,3',4-PeCB 82 0.663 0.0500 1.62 0.9332,2',3,3',5-PeCB 83 83 + 99 C 1.96 0.0500 1.47 0.8852,2',3,3',6-PeCB 84 0.729 0.0500 1.53 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 0.845 0.0500 1.41 0.9202,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 2.79 0.0500 1.59 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C NDR 0.313 0.0500 1.19 1.1542,2',3,4,6'-PeCB 89 ND 0.05002,2',3,4',5-PeCB 90 90 + 101 + 113 C 3.69 0.0500 1.65 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 0.511 0.0500 1.62 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 1.95 0.0500 1.41 1.1202,2',3,5,6'-PeCB 94 ND 0.05002,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.05002,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.05002,2',4,6,6'-PeCB 104 ND 0.05002,3,3',4,4'-PeCB 105 2.91 0.0829 1.66 1.0002,3,3',4,5-PeCB 106 ND 0.07252,3,3',4',5-PeCB 107 107 + 124 C NDR 0.165 0.0792 1.09 0.9902,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 0.388 0.0738 1.42 0.9982,3,3',4',6-PeCB 110 110 + 115 C 5.30 0.0500 1.55 0.9242,3,3',5,5'-PeCB 111 ND 0.05002,3,3',5,6-PeCB 112 ND 0.05002,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 0.186 0.0822 1.73 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 5.66 0.0802 1.48 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 0.05002,3',4,5',6-PeCB 121 ND 0.05002',3,3',4,5-PeCB 122 ND 0.08192',3,4,4',5-PeCB 123 ND 0.08312',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 ND 0.08633,3',4,5,5'-PeCB 127 ND 0.0741

2,2',3,3',4,4'-HxCB 128 128 + 166 C 1.75 0.0660 1.16 0.9592,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 12.0 0.0651 1.24 0.9292,2',3,3',4,5'-HxCB 130 0.533 0.0833 1.38 0.9132,2',3,3',4,6-HxCB 131 NDR 0.083 0.0789 1.49 1.1602,2',3,3',4,6'-HxCB 132 3.94 0.0827 1.34 1.1742,2',3,3',5,5'-HxCB 133 NDR 0.088 0.0763 0.93 1.1922,2',3,3',5,6-HxCB 134 134 + 143 C 0.424 0.0789 1.40 1.1392,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 3.00 0.0500 1.31 1.1032,2',3,3',6,6'-HxCB 136 1.01 0.0500 1.33 1.0232,2',3,4,4',5-HxCB 137 0.308 0.0790 1.33 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR 0.084 0.0707 2.00 1.1532,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 2.52 0.0726 1.32 0.9032,2',3,4,5,6-HxCB 142 ND 0.08052,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 0.421 0.0500 1.23 1.1212,2',3,4,6,6'-HxCB 145 ND 0.05002,2',3,4',5,5'-HxCB 146 1.24 0.0686 1.28 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 8.50 0.0714 1.29 1.1332,2',3,4',5,6'-HxCB 148 ND 0.05002,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 0.05002,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 0.05002,2',4,4',5,5'-HxCB 153 153 + 168 C 10.1 0.0591 1.22 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 ND 0.05002,3,3',4,4',5-HxCB 156 156 + 157 C 1.30 0.0662 1.21 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 1.12 0.0509 1.16 0.9382,3,3',4,5,5'-HxCB 159 NDR 0.222 0.0541 1.43 0.9812,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 0.05232,3,3',4',5,5'-HxCB 162 ND 0.05522,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 0.901 0.0544 1.22 0.9212,3,3',5,5',6-HxCB 165 ND 0.06302,3,4,4',5,6-HxCB 166 128 + 166 C128


(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration; C = co-eluting congener.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 17:59:29; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26760-101_Form1A_PB8C_447AS4_SJ931178.html; Workgroup: WG26760; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 0.373 0.0550 1.21 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 ND 0.0585

2,2',3,3',4,4',5-HpCB 170 4.13 0.0500 1.06 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C 1.25 0.0500 1.01 1.1622,2',3,3',4,5,5'-HpCB 172 0.658 0.0500 1.04 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 4.37 0.0500 1.04 1.1332,2',3,3',4,5',6-HpCB 175 0.172 0.0500 0.97 1.1022,2',3,3',4,6,6'-HpCB 176 0.486 0.0500 0.97 1.0342,2',3,3',4',5,6-HpCB 177 2.35 0.0500 1.09 1.1452,2',3,3',5,5',6-HpCB 178 NDR 0.746 0.0500 1.28 1.0852,2',3,3',5,6,6'-HpCB 179 1.62 0.0500 1.10 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C 8.70 0.0500 1.04 0.9102,2',3,4,4',5,6-HpCB 181 ND 0.05002,2',3,4,4',5,6'-HpCB 182 ND 0.05002,2',3,4,4',5',6-HpCB 183 183 + 185 C 2.82 0.0500 1.07 1.1272,2',3,4,4',6,6'-HpCB 184 ND 0.05002,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND 0.05002,2',3,4',5,5',6-HpCB 187 4.59 0.0500 1.01 1.1102,2',3,4',5,6,6'-HpCB 188 ND 0.05002,3,3',4,4',5,5'-HpCB 189 0.223 0.0500 0.94 1.0002,3,3',4,4',5,6-HpCB 190 0.860 0.0500 1.14 0.9472,3,3',4,4',5',6-HpCB 191 NDR 0.176 0.0500 0.83 0.9172,3,3',4,5,5',6-HpCB 192 ND 0.05002,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 1.98 0.0500 0.82 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR 0.730 0.0500 1.03 0.9462,2',3,3',4,4',5,6'-OcCB 196 1.04 0.0500 0.94 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C NDR 0.309 0.0500 1.26 1.0462,2',3,3',4,5,5',6-OcCB 198 198 + 199 C 2.08 0.0500 0.88 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 0.230 0.0500 0.93 1.0232,2',3,3',5,5',6,6'-OcCB 202 NDR 0.338 0.0500 0.72 1.0012,2',3,4,4',5,5',6-OcCB 203 1.40 0.0500 0.89 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND 0.05002,3,3',4,4',5,5',6-OcCB 205 0.161 0.0500 0.82 1.001

2,2',3,3',4,4',5,5',6-NoCB 206 NDR 0.643 0.0815 0.93 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 NDR 0.083 0.0587 0.50 1.0202,2',3,3',4,5,5',6,6'-NoCB 208 0.186 0.0610 0.76 1.001

2,2',3,3',4,4',5,5',6,6'-DeCB 209 0.250 0.0500 0.68 1.000


(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; C = co-eluting congener.(3) R% = percent recovery of labeled compounds.


For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 01-Dec-2008 17:59:29; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26760-101_Form2_PB8C_447AS4_SJ931178.html; Workgroup: WG26760; Design ID: 925 ]



Form 2PCB CONGENER ANALYSIS REPORT


Project No. N/A









Concentration Units: pg absolute

LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND

R(%) 3 IONABUND.RATIO

RRT

13C12-2-MoCB 1L 2000 938 46.9 3.19 0.71813C12-4-MoCB 3L 2000 962 48.1 3.20 0.858

13C12-2,2'-DiCB 4L 2000 1040 52.2 1.57 0.87313C12-4,4'-DiCB 15L 2000 1370 68.7 1.57 1.256

13C12-2,2',6-TriCB 19L 2000 1030 51.7 1.05 1.07313C12-3,4,4'-TriCB 37L 2000 1740 87.2 1.04 1.092

13C12-2,2',6,6'-TeCB 54L 2000 1070 53.4 0.81 0.81013C12-3,3',4,4'-TeCB 77L 2000 2020 101 0.78 1.39713C12-3,4,4',5-TeCB 81L 2000 1990 99.4 0.77 1.374

13C12-2,2',4,6,6'-PeCB 104L 2000 1210 60.4 1.60 0.80813C12-2,3,3',4,4'-PeCB 105L 2000 2010 100 1.56 1.20013C12-2,3,4,4',5-PeCB 114L 2000 1970 98.4 1.56 1.17813C12-2,3',4,4',5-PeCB 118L 2000 1980 99.1 1.54 1.16113C12-2',3,4,4',5-PeCB 123L 2000 1970 98.6 1.57 1.15113C12-3,3',4,4',5-PeCB 126L 2000 2200 110 1.56 1.301

13C12-2,2',4,4',6,6'-HxCB 155L 2000 1180 58.9 1.24 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 4000 3370 84.3 1.26 1.10713C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 2000 1680 83.8 1.25 1.07813C12-3,3',4,4',5,5'-HxCB 169L 2000 1750 87.6 1.24 1.191

13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1690 84.4 1.05 0.89713C12-2,2',3,4,4',5,5'-HpCB 180L 2000 1660 83.1 1.05 0.87313C12-2,2',3,4',5,6,6'-HpCB 188L 2000 1310 65.7 1.06 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L 2000 2010 100 1.02 0.959

13C12-2,2',3,3',5,5',6,6'-OcCB 202L 2000 1220 61.0 0.89 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L 2000 1680 84.0 0.91 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L 2000 1420 71.1 0.79 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L 2000 1410 70.7 0.78 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L 2000 1200 59.8 1.19 1.075

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1390 69.3 1.04 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1590 79.6 1.60 1.087

13C12-2,2',3,3',5,5',6-HpCB 178L 2000 1430 71.5 1.04 1.011

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTF_WG26760-101_Form2_PB8C_447AS4_SJ931178.html)

(1) Where applicable, custom lab flags have been used on this report; N = authentic recovery is not within method/contract control limits; C = co-elutingcongener.


For Axys Internal Use Only [ XSL Template: Form16688A.xsl; Created: 01-Dec-2008 17:59:29; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26760-102_Form8A_SJ931175.html; Workgroup: WG26760; Design ID: 925 ]



PCB CONGENER ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 Lab Sample I.D.: WG26760-102

Matrix: SOLID Initial Calibration Date: 22-Oct-2008



Extract Volume (uL): 20 OPR Data Filename: PB8C_447A S: 2



CONCENTRATIONS REPORTED ARE CONCENTRATIONS IN EXTRACT, BASED ON A 20 uL EXTRACT VOLUME.

COMPOUND IUPACNO.


IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

2-MoCB 1 2.93 50.0 49.5 25.0 - 75.0 98.94-MoCB 3 3.00 50.0 50.4 25.0 - 75.0 1012,2'-DiCB 4 1.49 50.0 49.3 25.0 - 75.0 98.54,4'-DiCB 15 1.53 50.0 50.4 25.0 - 75.0 1012,2',6-TriCB 19 1.06 50.0 51.9 25.0 - 75.0 1043,4,4'-TriCB 37 1.03 50.0 54.9 25.0 - 75.0 1102,2',6,6'-TeCB 54 0.82 50.0 51.4 25.0 - 75.0 1033,3',4,4'-TeCB 77 0.79 50.0 55.1 25.0 - 75.0 1103,4,4',5-TeCB 81 0.79 50.0 55.9 25.0 - 75.0 1122,2',4,6,6'-PeCB 104 1.57 50.0 51.0 25.0 - 75.0 1022,3,3',4,4'-PeCB 105 N 1.54 50.0 78.4 25.0 - 75.0 1572,3,4,4',5-PeCB 114 1.57 50.0 58.1 25.0 - 75.0 1162,3',4,4',5-PeCB 118 N 1.56 50.0 106 25.0 - 75.0 2122',3,4,4',5-PeCB 123 1.57 50.0 59.0 25.0 - 75.0 1183,3',4,4',5-PeCB 126 1.59 50.0 55.7 25.0 - 75.0 1112,2',4,4',6,6'-HxCB 155 1.26 50.0 50.9 25.0 - 75.0 1022,3,3',4,4',5-HxCB 156 156 + 157 C 1.27 100 110 50.0 - 150 1102,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 1.27 50.0 55.4 25.0 - 75.0 1113,3',4,4',5,5'-HxCB 169 1.27 50.0 52.4 25.0 - 75.0 1052,2',3,4',5,6,6'-HpCB 188 1.04 50.0 51.7 25.0 - 75.0 1032,3,3',4,4',5,5'-HpCB 189 1.02 50.0 54.7 25.0 - 75.0 1092,2',3,3',5,5',6,6'-OcCB 202 0.88 50.0 52.8 25.0 - 75.0 1062,3,3',4,4',5,5',6-OcCB 205 0.89 50.0 53.2 25.0 - 75.0 1062,2',3,3',4,4',5,5',6-NoCB 206 0.79 50.0 52.8 25.0 - 75.0 1062,2',3,3',4,5,5',6,6'-NoCB 208 0.79 50.0 51.5 25.0 - 75.0 1032,2',3,3',4,4',5,5',6,6'-DeCB 209 0.69 50.0 49.0 25.0 - 75.0 98.0

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTF_WG26760-102_Form8A_SJ931175.html)

(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; V = surrogate recovery is not within method/contract control limits; C = co-elutingcongener.


For Axys Internal Use Only [ XSL Template: Form16688B.xsl; Created: 01-Dec-2008 17:59:29; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26760-102_Form8B_SJ931175.html; Workgroup: WG26760; Design ID: 925 ]











LABELEDCOMPOUND

IUPACNO. 1

CO-ELUTIONS

LABFLAG2

IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

13C12-2-MoCB 1L 3.25 100 37.0 15.0 - 140 37.013C12-4-MoCB 3L 3.19 100 45.3 15.0 - 140 45.313C12-2,2'-DiCB 4L 1.58 100 50.3 30.0 - 140 50.313C12-4,4'-DiCB 15L 1.58 100 70.4 30.0 - 140 70.413C12-2,2',6-TriCB 19L 1.06 100 52.7 30.0 - 140 52.713C12-3,4,4'-TriCB 37L 1.07 100 101 30.0 - 140 10113C12-2,2',6,6'-TeCB 54L 0.81 100 73.5 30.0 - 140 73.513C12-3,3',4,4'-TeCB 77L 0.80 100 98.0 30.0 - 140 98.013C12-3,4,4',5-TeCB 81L 0.78 100 92.7 30.0 - 140 92.713C12-2,2',4,6,6'-PeCB 104L 1.61 100 72.0 30.0 - 140 72.013C12-2,3,3',4,4'-PeCB 105L 1.59 100 137 30.0 - 140 13713C12-2,3,4,4',5-PeCB 114L 1.59 100 131 30.0 - 140 13113C12-2,3',4,4',5-PeCB 118L 1.59 100 130 30.0 - 140 13013C12-2',3,4,4',5-PeCB 123L 1.58 100 133 30.0 - 140 13313C12-3,3',4,4',5-PeCB 126L V 1.56 100 148 30.0 - 140 14813C12-2,2',4,4',6,6'-HxCB 155L 1.25 100 47.8 30.0 - 140 47.813C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 1.27 200 174 60.0 - 280 86.813C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 1.27 100 85.6 30.0 - 140 85.613C12-3,3',4,4',5,5'-HxCB 169L 1.27 100 95.6 30.0 - 140 95.613C12-2,2',3,4',5,6,6'-HpCB 188L 1.05 100 41.6 30.0 - 140 41.613C12-2,3,3',4,4',5,5'-HpCB 189L 1.04 100 108 30.0 - 140 10813C12-2,2',3,3',5,5',6,6'-OcCB 202L 0.91 100 41.7 30.0 - 140 41.713C12-2,3,3',4,4',5,5',6-OcCB 205L 0.92 100 78.2 30.0 - 140 78.213C12-2,2',3,3',4,4',5,5',6-NoCB 206L 0.77 100 65.9 30.0 - 140 65.913C12-2,2',3,3',4,5,5',6,6'-NoCB 208L 0.79 100 60.9 30.0 - 140 60.913C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L 1.17 100 57.6 30.0 - 140 57.6

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 1.05 100 102 40.0 - 125 10213C12-2,3,3',5,5'-PeCB 111L 1.62 100 81.5 40.0 - 125 81.513C12-2,2',3,3',5,5',6-HpCB 178L 1.06 100 65.2 40.0 - 125 65.2

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTF_WG26760-102_Form8B_SJ931175.html)

(1) Where applicable, custom lab flags have been used on this report; D = dilution data; C = co-eluting congener; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-2_Form1A_PB8B_315S6_SJ934848.html; Workgroup: WG26760; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.08LAO010BSample Collection:N/A



Project No. POP1406

Contract No.: 2607 Lab Sample I.D.: L11830-2 NK

Matrix: SOIL Sample Size: 9.79 g (dry)

Sample Receipt Date: 07-Oct-2008 Initial Calibration Date: 19-Nov-2008



Extract Volume (uL): 4000 Sample Data Filename: PB8B_315 S: 6


Dilution Factor: 20 Cal. Ver. Data Filename: PB8B_315 S: 1

Concentration Units: pg/g (dry weight basis) % Moisture: 24.7

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,3',4,4'-TeCB 77 X3,4,4',5-TeCB 81 X

2,3,3',4,4'-PeCB 105 X2,3,4,4',5-PeCB 114 X2,3',4,4',5-PeCB 118 X2',3,4,4',5-PeCB 123 X3,3',4,4',5-PeCB 126 X

2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 X3,3',4,4',5,5'-HxCB 169 X

2,2',3,3',4,4',5-HpCB 170 D 311000 21.0 1.05 1.0002,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 650000 14.7 1.05 1.0002,3,3',4,4',5,5'-HpCB 189 X2,3,3',4',5,5',6-HpCB 193 180 + 193 C180

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_L11830-2_Form1A_PB8B_315S6_SJ934848.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; C = co-eluting congener; OLR = exceeds calibrated linearrange, see dilution data.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-2_Form1A_PB8C_452S3_SJ934801.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406



Sample Receipt Date: 07-Oct-2008 Initial Calibration Date: 22-Oct-2008



Extract Volume (uL): 200 Sample Data Filename: PB8C_452 S: 3


Dilution Factor: N/A Cal. Ver. Data Filename: PB8C_452 S: 1


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,3',4,4'-TeCB 77 662 2.08 0.75 1.0003,4,4',5-TeCB 81 17.9 2.07 0.72 1.001

2,3,3',4,4'-PeCB 105 1600 6.14 1.72 1.0002,3,4,4',5-PeCB 114 59.8 6.21 1.47 1.0002,3',4,4',5-PeCB 118 7970 5.82 1.52 1.0002',3,4,4',5-PeCB 123 172 6.03 1.40 1.0003,3',4,4',5-PeCB 126 637 6.83 1.48 1.000

2,3,3',4,4',5-HxCB 156 156 + 157 C 15000 9.69 1.25 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 14000 7.24 1.26 1.0003,3',4,4',5,5'-HxCB 169 ND 521

2,2',3,3',4,4',5-HpCB 170 OLR2,2',3,4,4',5,5'-HpCB 180 180 + 193 C OLR2,3,3',4,4',5,5'-HpCB 189 9190 29.3 1.02 1.0002,3,3',4',5,5',6-HpCB 193 180 + 193 C180

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_L11830-2_Form1A_PB8C_452S3_SJ934801.html)

(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; C = co-eluting congener; X = result reported separately.(3) R% = percent recovery of labeled compounds.


For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-2_Form2_PB8B_315S6_SJ934848.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406









Concentration Units: pg absolute % Moisture: 24.7

LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-3,3',4,4'-TeCB 77L X13C12-3,4,4',5-TeCB 81L X

13C12-2,3,3',4,4'-PeCB 105L X13C12-2,3,4,4',5-PeCB 114L X13C12-2,3',4,4',5-PeCB 118L X13C12-2',3,4,4',5-PeCB 123L X13C12-3,3',4,4',5-PeCB 126L X

13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L X13C12-3,3',4,4',5,5'-HxCB 169L X

13C12-2,2',3,3',4,4',5-HpCB 170L X13C12-2,2',3,4,4',5,5'-HpCB 180L X13C12-2,3,3',4,4',5,5'-HpCB 189L X

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L X13C12-2,2',3,3',5,5',6-HpCB 178L X

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For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-2_Form2_PB8C_452S3_SJ934801.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-3,3',4,4'-TeCB 77L 2000 1960 97.8 0.76 1.39713C12-3,4,4',5-TeCB 81L 2000 2010 101 0.78 1.374

13C12-2,3,3',4,4'-PeCB 105L 2000 1770 88.5 1.54 1.20013C12-2,3,4,4',5-PeCB 114L 2000 1720 86.0 1.58 1.17913C12-2,3',4,4',5-PeCB 118L 2000 1810 90.5 1.52 1.16213C12-2',3,4,4',5-PeCB 123L 2000 1830 91.3 1.54 1.15113C12-3,3',4,4',5-PeCB 126L 2000 1800 89.8 1.58 1.301

13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 4000 1940 48.4 1.31 1.10713C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 2000 999 50.0 1.20 1.07713C12-3,3',4,4',5,5'-HxCB 169L 2000 1070 53.5 1.19 1.190

13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1440 71.9 1.10 1.17513C12-2,2',3,4,4',5,5'-HpCB 180L 2000 1710 85.4 1.14 1.14313C12-2,3,3',4,4',5,5'-HpCB 189L 2000 1110 55.5 1.05 1.255

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L 2000 1750 87.4 1.62 1.08813C12-2,2',3,3',5,5',6-HpCB 178L 2000 1230 61.6 1.03 1.011

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_L11830-2_Form2_PB8C_452S3_SJ934801.html)

(1) Where applicable, custom lab flags have been used on this report; D = dilution data; C = co-eluting congener; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-5_Form1A_PB8B_315S7_SJ934849.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,3',4,4'-TeCB 77 X3,4,4',5-TeCB 81 X

2,3,3',4,4'-PeCB 105 D 33000 0.820 1.58 1.0002,3,4,4',5-PeCB 114 X2,3',4,4',5-PeCB 118 D 125000 0.820 1.57 1.0002',3,4,4',5-PeCB 123 X3,3',4,4',5-PeCB 126 X

2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 X3,3',4,4',5,5'-HxCB 169 X

2,2',3,3',4,4',5-HpCB 170 D 679000 0.191 1.05 1.0012,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 1520000 0.196 1.04 1.0002,3,3',4,4',5,5'-HpCB 189 X2,3,3',4',5,5',6-HpCB 193 180 + 193 C180

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_L11830-5_Form1A_PB8B_315S7_SJ934849.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration; C = co-eluting congener; OLR = exceeds calibrated linear range, see dilutiondata.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-5_Form1A_PB8C_452S4_SJ934802.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,3',4,4'-TeCB 77 6350 18.8 0.77 1.0003,4,4',5-TeCB 81 426 18.1 0.81 1.000

2,3,3',4,4'-PeCB 105 OLR2,3,4,4',5-PeCB 114 2070 12.2 1.54 1.0002,3',4,4',5-PeCB 118 OLR2',3,4,4',5-PeCB 123 1010 12.5 1.61 1.0013,3',4,4',5-PeCB 126 NDR 2230 10.4 1.51 1.000

2,3,3',4,4',5-HxCB 156 156 + 157 C 105000 40.7 1.27 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 41100 29.4 1.26 1.0003,3',4,4',5,5'-HxCB 169 ND 524

2,2',3,3',4,4',5-HpCB 170 OLR2,2',3,4,4',5,5'-HpCB 180 180 + 193 C OLR2,3,3',4,4',5,5'-HpCB 189 21900 26.6 1.04 1.0002,3,3',4',5,5',6-HpCB 193 180 + 193 C180

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Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-3,3',4,4'-TeCB 77L X13C12-3,4,4',5-TeCB 81L X

13C12-2,3,3',4,4'-PeCB 105L X13C12-2,3,4,4',5-PeCB 114L X13C12-2,3',4,4',5-PeCB 118L X13C12-2',3,4,4',5-PeCB 123L X13C12-3,3',4,4',5-PeCB 126L X

13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L X13C12-3,3',4,4',5,5'-HxCB 169L X

13C12-2,2',3,3',4,4',5-HpCB 170L X13C12-2,2',3,4,4',5,5'-HpCB 180L X13C12-2,3,3',4,4',5,5'-HpCB 189L X

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L X13C12-2,2',3,3',5,5',6-HpCB 178L X

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For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_L11830-5_Form2_PB8C_452S4_SJ934802.html; Workgroup: WG26760; Design ID: 925 ]





Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-3,3',4,4'-TeCB 77L 2000 2150 107 0.77 1.40313C12-3,4,4',5-TeCB 81L 2000 2250 113 0.77 1.379

13C12-2,3,3',4,4'-PeCB 105L 2000 2490 124 1.53 1.20113C12-2,3,4,4',5-PeCB 114L 2000 2310 115 1.58 1.18013C12-2,3',4,4',5-PeCB 118L 2000 2620 131 1.55 1.16313C12-2',3,4,4',5-PeCB 123L 2000 2430 122 1.58 1.15313C12-3,3',4,4',5-PeCB 126L 2000 2680 134 1.60 1.302


13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1030 51.3 1.18 1.17313C12-2,2',3,4,4',5,5'-HpCB 180L 2000 945 47.2 1.12 1.14213C12-2,3,3',4,4',5,5'-HpCB 189L 2000 1460 72.9 1.05 1.253

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L 2000 1720 85.9 1.61 1.08913C12-2,2',3,3',5,5',6-HpCB 178L 2000 996 49.8 1.08 1.011

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_L11830-5_Form2_PB8C_452S4_SJ934802.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; C = co-eluting congener.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_WG26760-101_Form1A_PB8C_447AS4_SJ934800.html; Workgroup: WG26760; Design ID: 925 ]





Project No. N/A










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,3',4,4'-TeCB 77 0.441 0.0595 0.88 1.0013,4,4',5-TeCB 81 ND 0.0600

2,3,3',4,4'-PeCB 105 2.91 0.0829 1.66 1.0002,3,4,4',5-PeCB 114 0.186 0.0822 1.73 1.0012,3',4,4',5-PeCB 118 5.66 0.0802 1.48 1.0002',3,4,4',5-PeCB 123 ND 0.08313,3',4,4',5-PeCB 126 ND 0.0863

2,3,3',4,4',5-HxCB 156 156 + 157 C 1.30 0.0662 1.21 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 0.373 0.0550 1.21 1.0003,3',4,4',5,5'-HxCB 169 ND 0.0585

2,2',3,3',4,4',5-HpCB 170 4.36 0.0500 1.06 1.0012,2',3,4,4',5,5'-HpCB 180 180 + 193 C 10.5 0.0500 1.04 1.0002,3,3',4,4',5,5'-HpCB 189 0.223 0.0500 0.94 1.0002,3,3',4',5,5',6-HpCB 193 180 + 193 C180

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Project No. N/A










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-3,3',4,4'-TeCB 77L 2000 2020 101 0.78 1.39713C12-3,4,4',5-TeCB 81L 2000 1990 99.4 0.77 1.374

13C12-2,3,3',4,4'-PeCB 105L 2000 2010 100 1.56 1.20013C12-2,3,4,4',5-PeCB 114L 2000 1970 98.4 1.56 1.17813C12-2,3',4,4',5-PeCB 118L 2000 1980 99.1 1.54 1.16113C12-2',3,4,4',5-PeCB 123L 2000 1970 98.6 1.57 1.15113C12-3,3',4,4',5-PeCB 126L 2000 2200 110 1.56 1.301


13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1480 74.0 1.05 1.17513C12-2,2',3,4,4',5,5'-HpCB 180L 2000 1490 74.5 1.05 1.14313C12-2,3,3',4,4',5,5'-HpCB 189L 2000 2040 102 1.02 1.256

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L 2000 1590 79.6 1.60 1.08713C12-2,2',3,3',5,5',6-HpCB 178L 2000 1430 71.5 1.04 1.011

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_WG26760-101_Form2_PB8C_447AS4_SJ934800.html)

(1) Where applicable, custom lab flags have been used on this report; N = authentic recovery is not within method/contract control limits; C = co-elutingcongener.


For Axys Internal Use Only [ XSL Template: Form16688A.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_WG26760-102_Form8A_SJ934799.html; Workgroup: WG26760; Design ID: 925 ]











COMPOUND IUPACNO.


IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

3,3',4,4'-TeCB 77 0.79 50.0 55.1 25.0 - 75.0 1103,4,4',5-TeCB 81 0.79 50.0 55.9 25.0 - 75.0 1122,3,3',4,4'-PeCB 105 N 1.54 50.0 78.4 25.0 - 75.0 1572,3,4,4',5-PeCB 114 1.57 50.0 58.1 25.0 - 75.0 1162,3',4,4',5-PeCB 118 N 1.56 50.0 106 25.0 - 75.0 2122',3,4,4',5-PeCB 123 1.57 50.0 59.0 25.0 - 75.0 1183,3',4,4',5-PeCB 126 1.59 50.0 55.7 25.0 - 75.0 1112,3,3',4,4',5-HxCB 156 156 + 157 C 1.27 100 110 50.0 - 150 1102,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 1.27 50.0 55.4 25.0 - 75.0 1113,3',4,4',5,5'-HxCB 169 1.27 50.0 52.4 25.0 - 75.0 1052,2',3,3',4,4',5-HpCB 170 N 1.04 50.0 79.1 25.0 - 75.0 1582,2',3,4,4',5,5'-HpCB 180 180 + 193 C N 1.04 50.0 120 25.0 - 75.0 2412,3,3',4,4',5,5'-HpCB 189 1.02 50.0 54.7 25.0 - 75.0 1092,3,3',4',5,5',6-HpCB 193 180 + 193 C180

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_WG26760-102_Form8A_SJ934799.html)

(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; V = surrogate recovery is not within method/contract control limits; C = co-elutingcongener.


For Axys Internal Use Only [ XSL Template: Form16688B.xsl; Created: 01-Dec-2008 18:00:30; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTOX_WG26760-102_Form8B_SJ934799.html; Workgroup: WG26760; Design ID: 925 ]











LABELEDCOMPOUND

IUPACNO. 1

CO-ELUTIONS

LABFLAG2

IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

13C12-3,3',4,4'-TeCB 77L 0.80 100 98.0 30.0 - 140 98.013C12-3,4,4',5-TeCB 81L 0.78 100 92.7 30.0 - 140 92.713C12-2,3,3',4,4'-PeCB 105L 1.59 100 137 30.0 - 140 13713C12-2,3,4,4',5-PeCB 114L 1.59 100 131 30.0 - 140 13113C12-2,3',4,4',5-PeCB 118L 1.59 100 130 30.0 - 140 13013C12-2',3,4,4',5-PeCB 123L 1.58 100 133 30.0 - 140 13313C12-3,3',4,4',5-PeCB 126L V 1.56 100 148 30.0 - 140 14813C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 1.27 200 174 60.0 - 280 86.813C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 1.27 100 85.6 30.0 - 140 85.613C12-3,3',4,4',5,5'-HxCB 169L 1.27 100 95.6 30.0 - 140 95.613C12-2,2',3,3',4,4',5-HpCB 170L 1.04 100 75.9 30.0 - 140 75.913C12-2,2',3,4,4',5,5'-HpCB 180L 1.05 100 73.7 30.0 - 140 73.713C12-2,3,3',4,4',5,5'-HpCB 189L V 1.04 100 142 30.0 - 140 142

CLEANUP STANDARD

13C12-2,3,3',5,5'-PeCB 111L 1.62 100 81.5 40.0 - 125 81.513C12-2,2',3,3',5,5',6-HpCB 178L 1.06 100 65.2 40.0 - 125 65.2

Page 1 of 1 (WG26760 - 1668_PCB1668_PCBTOX_WG26760-102_Form8B_SJ934799.html)

Dioxin/Furan (PCDD/F) Analysis

Report

(1) Where applicable, custom lab flags have been used on this report.(2) For contract CV specifications, see Section 10.5.4, Method 1613.

Approved by: ___________Robert Tones___________ QA/QC Chemist

For Axys Internal Use Only [ XSL Template: Form3A.xsl; Created: 11-Dec-2008 11:45:47; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_06-Nov-2008_DB83__Form3A_GS29846.html; Workgroup: WG26805; Design ID: 988 ]


PCDD/PCDF INITIAL CALIBRATION RELATIVE RESPONSES


CS0 Data Filename: N/A

Initial Calibration Date: 06-Nov-2008 CS1 Data Filename: DB83_249E S: 2

Instrument ID: HR GC/MS CS2 Data Filename: DB83_249E S: 9

GC Column ID: DB225 CS3 Data Filename: DB83_249E S: 8

CS4 Data Filename: DB83_249E S: 6



RELATIVE RESPONSE (RR)CS0 CS1 CS2 CS3 CS4 CS5 CS6 MEAN

RRCV

(%RSD)2COMPOUND LAB

FLAG 1

2,3,7,8-TCDF 0.77 0.71 0.74 0.74 0.76 0.75 3.14

Page 1 of 1 (WG26805 - 1613_DIOXINS_06-Nov-2008_DB83__Form3A_GS29846.html)

(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits from Table 9, Method 1613.


For Axys Internal Use Only [ XSL Template: Form3C.xsl; Created: 11-Dec-2008 11:45:47; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_06-Nov-2008_DB83__Form3C_GS29846.html; Workgroup: WG26805; Design ID: 988 ]

AXYS METHOD MLA-017 Rev 14Form 3C

PCDD/PCDF INITIAL CALIBRATION ION ABUNDANCE RATIOS



Initial Calibration Date: 06-Nov-2008 CS1 Data Filename: DB83_249E S: 2

Instrument ID: HR GC/MS CS2 Data Filename: DB83_249E S: 9

GC Column ID: DB225 CS3 Data Filename: DB83_249E S: 8




ION ABUNDANCE RATIOCS0 CS1 CS2 CS3 CS4 CS5 CS6

COMPOUND LABFLAG 1

M/Z'sFORMINGRATIO 2

QCLIMITS3

2,3,7,8-TCDF M/M+2 0.84 0.69 0.75 0.74 0.75 0.65-0.89

Page 1 of 1 (WG26805 - 1613_DIOXINS_06-Nov-2008_DB83__Form3C_GS29846.html)

(1) Where applicable, custom lab flags have been used on this report.(2) For contract CV specifications, see Section 10.5.4, Method 1613.(3) Alternate confirmation and quantitation ions used for native and labeled PECDD.(4) Response ratios are calculated relative to the labeled analogs of the other two HXCDDs (Section 17.1.2, Method 1613).(5) Response ratios are calculated relative to the labeled analog of OCDD (Section 17.1.1, Method 1613).

Approved by: ___________Leanne Henley___________ QA/QC Chemist

For Axys Internal Use Only [ XSL Template: Form3A.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_25-Oct-2008_DX8M__Form3A_GS29844.html; Workgroup: WG26805; Design ID: 988 ]





Initial Calibration Date: 25-Oct-2008 CS1 Data Filename: DX8M_084B S: 3

Instrument ID: HR GC/MS CS2 Data Filename: DX8M_084B S: 2

GC Column ID: DB5 CS3 Data Filename: DX8M_084B S: 1

CS4 Data Filename: DX8M_084B S: 6




RRCV

(%RSD)2COMPOUND LAB

FLAG 1

2,3,7,8-TCDD 1.01 1.04 0.91 1.02 1.01 1.00 5.321,2,3,7,8-PECDD 3 0.94 0.96 0.94 0.94 0.94 0.94 1.001,2,3,4,7,8-HXCDD 0.87 0.93 0.86 0.88 0.86 0.88 3.581,2,3,6,7,8-HXCDD 0.84 0.80 0.82 0.81 0.81 0.81 1.711,2,3,7,8,9-HXCDD 4 0.85 0.89 0.85 0.85 0.84 0.86 2.241,2,3,4,6,7,8-HPCDD 1.08 1.09 1.02 1.05 1.06 1.06 2.69OCDD 1.00 1.02 0.97 0.99 0.95 0.99 2.932,3,7,8-TCDF 0.89 0.90 0.88 0.88 0.87 0.89 1.261,2,3,7,8-PECDF 1.02 1.02 1.03 1.01 1.00 1.02 1.142,3,4,7,8-PECDF 0.99 1.03 1.00 1.01 1.00 1.01 1.711,2,3,4,7,8-HXCDF 1.19 1.15 1.15 1.15 1.13 1.15 1.891,2,3,6,7,8-HXCDF 1.12 1.14 1.13 1.11 1.12 1.12 1.061,2,3,7,8,9-HXCDF 0.99 1.00 0.93 1.01 0.99 0.98 3.002,3,4,6,7,8-HXCDF 1.05 1.07 1.02 1.03 1.02 1.04 1.991,2,3,4,6,7,8-HPCDF 1.40 1.40 1.33 1.36 1.33 1.36 2.451,2,3,4,7,8,9-HPCDF 1.22 1.30 1.21 1.23 1.20 1.23 3.20OCDF 5 1.05 1.08 1.02 1.10 1.06 1.06 2.78

Page 1 of 1 (WG26805 - 1613_DIOXINS_25-Oct-2008_DX8M__Form3A_GS29844.html)

(1) Where applicable, custom lab flags have been used on this report.(2) For assignment of labeled compounds to internal standards, see Table 2. For contract CV specifications, see Section 10.6.3, Method 1613.(3) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form3B.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_25-Oct-2008_DX8M__Form3B_GS29844.html; Workgroup: WG26805; Design ID: 988 ]












RRCV

(%RSD)2LABELED COMPOUND LAB

FLAG 1

13C-2,3,7,8-TCDD 1.11 1.10 1.09 1.14 1.21 1.13 4.4713C-1,2,3,7,8-PECDD 3 0.77 0.77 0.75 0.81 0.91 0.80 8.0413C-1,2,3,4,7,8-HXCDD 0.95 0.94 1.00 0.98 1.00 0.97 2.7313C-1,2,3,6,7,8-HXCDD 1.08 1.10 1.06 1.11 1.09 1.09 1.8613C-1,2,3,4,6,7,8-HPCDD 0.79 0.82 0.84 0.79 0.81 0.81 2.1713C-OCDD 0.77 0.80 0.82 0.77 0.88 0.81 5.6413C-2,3,7,8-TCDF 1.70 1.70 1.65 1.79 1.80 1.73 3.7313C-1,2,3,7,8-PECDF 1.22 1.22 1.18 1.29 1.43 1.27 7.8013C-2,3,4,7,8-PECDF 1.15 1.16 1.12 1.22 1.34 1.20 7.3413C-1,2,3,4,7,8-HXCDF 1.11 1.11 1.13 1.15 1.18 1.14 2.5513C-1,2,3,6,7,8-HXCDF 1.33 1.31 1.30 1.38 1.32 1.32 2.2713C-1,2,3,7,8,9-HXCDF 1.03 1.05 1.05 1.06 1.08 1.06 1.8413C-2,3,4,6,7,8-HXCDF 1.15 1.16 1.18 1.20 1.18 1.17 1.7113C-1,2,3,4,6,7,8-HPCDF 0.92 0.93 0.93 0.93 0.95 0.93 1.4213C-1,2,3,4,7,8,9-HPCDF 0.80 0.81 0.81 0.80 0.84 0.81 2.03

CLEANUP

37CL-2,3,7,8-TCDD 1.27 1.27 1.13 1.24 1.33 1.25 6.19

Page 1 of 1 (WG26805 - 1613_DIOXINS_25-Oct-2008_DX8M__Form3B_GS29844.html)

(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits from Table 9, Method 1613.(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form3C.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_25-Oct-2008_DX8M__Form3C_GS29844.html; Workgroup: WG26805; Design ID: 988 ]

AXYS METHOD MLA-017 Rev 14Form 3C











COMPOUND LABFLAG 1

M/Z'sFORMINGRATIO 2

QCLIMITS3

2,3,7,8-TCDD M/M+2 0.78 0.80 0.78 0.78 0.77 0.65-0.891,2,3,7,8-PECDD 4 M/M+2 0.62 0.62 0.62 0.62 0.62 0.51-0.701,2,3,4,7,8-HXCDD M+2/M+4 1.21 1.24 1.22 1.23 1.23 1.05-1.431,2,3,6,7,8-HXCDD M+2/M+4 1.30 1.22 1.23 1.23 1.23 1.05-1.431,2,3,7,8,9-HXCDD M+2/M+4 1.22 1.23 1.24 1.22 1.22 1.05-1.431,2,3,4,6,7,8-HPCDD M+2/M+4 1.00 1.03 1.02 1.04 1.02 0.88-1.20OCDD M+2/M+4 0.87 0.86 0.88 0.89 0.87 0.76-1.022,3,7,8-TCDF M/M+2 0.77 0.78 0.76 0.77 0.77 0.65-0.891,2,3,7,8-PECDF M+2/M+4 1.50 1.54 1.53 1.52 1.55 1.32-1.782,3,4,7,8-PECDF M+2/M+4 1.53 1.49 1.56 1.55 1.54 1.32-1.781,2,3,4,7,8-HXCDF M+2/M+4 1.20 1.24 1.24 1.28 1.23 1.05-1.431,2,3,6,7,8-HXCDF M+2/M+4 1.24 1.24 1.24 1.21 1.25 1.05-1.431,2,3,7,8,9-HXCDF M+2/M+4 1.22 1.25 1.24 1.24 1.25 1.05-1.432,3,4,6,7,8-HXCDF M+2/M+4 1.26 1.25 1.24 1.23 1.24 1.05-1.431,2,3,4,6,7,8-HPCDF M+2/M+4 1.07 1.03 1.03 1.04 1.04 0.88-1.201,2,3,4,7,8,9-HPCDF M+2/M+4 1.04 1.05 1.05 1.04 1.06 0.88-1.20OCDF M+2/M+4 0.94 0.90 0.90 0.91 0.91 0.76-1.02

Page 1 of 1 (WG26805 - 1613_DIOXINS_25-Oct-2008_DX8M__Form3C_GS29844.html)

(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits from Table 9, Method 1613.(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form3D.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_25-Oct-2008_DX8M__Form3D_GS29844.html; Workgroup: WG26805; Design ID: 988 ]

AXYS METHOD MLA-017 Rev 14Form 3D











LABELED COMPOUND LABFLAG1

M/Z'sFORMINGRATIO 2

QCLIMITS3

13C-2,3,7,8-TCDD M/M+2 0.78 0.79 0.78 0.80 0.78 0.65-0.8913C-1,2,3,7,8-PECDD 4 M/M+2 0.62 0.62 0.64 0.63 0.63 0.51-0.7013C-1,2,3,4,7,8-HXCDD M+2/M+4 1.26 1.28 1.26 1.32 1.26 1.05-1.4313C-1,2,3,6,7,8-HXCDD M+2/M+4 1.25 1.25 1.26 1.16 1.24 1.05-1.4313C-1,2,3,4,6,7,8-HPCDD M+2/M+4 1.03 1.03 1.05 1.05 1.04 0.88-1.2013C-OCDD M+2/M+4 0.89 0.88 0.90 0.89 0.90 0.76-1.0213C-2,3,7,8-TCDF M/M+2 0.79 0.79 0.78 0.79 0.78 0.65-0.8913C-1,2,3,7,8-PECDF M+2/M+4 1.54 1.57 1.55 1.57 1.55 1.32-1.7813C-2,3,4,7,8-PECDF M+2/M+4 1.56 1.54 1.55 1.54 1.56 1.32-1.7813C-1,2,3,4,7,8-HXCDF M/M+2 0.52 0.52 0.51 0.52 0.52 0.43-0.5913C-1,2,3,6,7,8-HXCDF M/M+2 0.51 0.51 0.52 0.51 0.52 0.43-0.5913C-1,2,3,7,8,9-HXCDF M/M+2 0.52 0.52 0.52 0.52 0.52 0.43-0.5913C-2,3,4,6,7,8-HXCDF M/M+2 0.52 0.52 0.52 0.52 0.52 0.43-0.5913C-1,2,3,4,6,7,8-HPCDF M/M+2 0.45 0.45 0.46 0.45 0.45 0.37-0.5113C-1,2,3,4,7,8,9-HPCDF M/M+2 0.45 0.45 0.45 0.46 0.45 0.37-0.51

Page 1 of 1 (WG26805 - 1613_DIOXINS_25-Oct-2008_DX8M__Form3D_GS29844.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration.(2) Contract-required limits for RRTs and ion abundance ratios are specified in Tables 2 and 9, respectively, Method 1613.(3) Alternate confirmation and quantitation ions used for native and labeled PECDD.

Approved by: ___________Teresa Rawsthorne___________ QA/QC Chemist

For Axys Internal Use Only [ XSL Template: Form1A.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613DB5_L11830-3_Form1A_DX8M_098S10_SJ933028.html; Workgroup: WG26805; Design ID: 988 ]

These pages are part of a larger report that may contain information necessary for full data evaluation. Results reported relate only to the sample tested. Results are compliant with NELAP wherespecific accreditation is held.


Form 1APCDD/PCDF ANALYSIS REPORT


Project No. POP1406


Matrix: ASH Sample Size: 4.48 g (dry)



Analysis Date: 19-Nov-2008 Time: 03:15:30 GC Column ID: DB5

Extract Volume (uL): 20 Sample Data Filename: DX8M_098 S: 10

Injection Volume (uL): 1.0 Blank Data Filename: DX8M_098 S: 5

Dilution Factor: N/A Cal. Ver. Data Filename: DX8M_098 S: 1


COMPOUND LAB FLAG 1 CONCENTRATIONFOUND

DETECTIONLIMIT

ION ABUND.RATIO 2

RRT 2

2,3,7,8-TCDD NDR 0.125 0.112 0.24 1.0011,2,3,7,8-PECDD 3 ND 0.1121,2,3,4,7,8-HXCDD ND 0.1121,2,3,6,7,8-HXCDD 0.130 0.112 1.08 1.0001,2,3,7,8,9-HXCDD 0.192 0.112 1.07 1.0001,2,3,4,6,7,8-HPCDD 1.61 0.112 1.08 1.000OCDD 6.41 0.112 0.87 1.0002,3,7,8-TCDF 0.872 0.112 0.80 1.0021,2,3,7,8-PECDF NDR 0.161 0.112 2.00 1.0022,3,4,7,8-PECDF NDR 0.260 0.112 2.17 1.0011,2,3,4,7,8-HXCDF NDR 0.210 0.112 1.50 1.0001,2,3,6,7,8-HXCDF 0.176 0.112 1.07 1.0001,2,3,7,8,9-HXCDF ND 0.1122,3,4,6,7,8-HXCDF 0.240 0.112 1.09 1.0001,2,3,4,6,7,8-HPCDF 0.713 0.112 1.17 1.0001,2,3,4,7,8,9-HPCDF ND 0.112OCDF 0.445 0.112 0.84 1.002TOTAL TETRA-DIOXINS 2.28 0.112TOTAL PENTA-DIOXINS 1.11 0.112TOTAL HEXA-DIOXINS 1.91 0.112TOTAL HEPTA-DIOXINS 2.94 0.112TOTAL TETRA-FURANS 5.22 0.112TOTAL PENTA-FURANS 1.64 0.112TOTAL HEXA-FURANS 1.31 0.112TOTAL HEPTA-FURANS 1.02 0.112

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_L11830-3_Form1A_DX8M_098S10_SJ933028.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required limits for percent recovery (R) are specified in Section 9.3.3, Method 1613.(3) Contract-required limits for RRTs and ion abundance ratios are specified in Tables 2 and 9, respectively, Method 1613. NOTE: There is no ionabundance ratio for 37Cl4-2,3,7,8-TCDD(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form2.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613DB5_L11830-3_Form2_DX8M_098S10_SJ933028.html; Workgroup: WG26805; Design ID: 988 ]



Form 2PCDD/PCDF ANALYSIS REPORT


Project No. POP1406











SPIKECONC.

CONC.FOUND

R(%) 2 ION ABUND.RATIO 3

RRT 3

13C-2,3,7,8-TCDD 2000 1190 59.5 0.79 1.01313C-1,2,3,7,8-PECDD 4 2000 1450 72.6 0.63 1.38313C-1,2,3,4,7,8-HXCDD 2000 1330 66.6 1.26 0.98713C-1,2,3,6,7,8-HXCDD 2000 1360 68.2 1.24 0.99013C-1,2,3,4,6,7,8-HPCDD 2000 1360 68.2 0.96 1.09413C-OCDD 4000 2360 58.9 0.89 1.17713C-2,3,7,8-TCDF 2000 1080 54.1 0.75 0.96613C-1,2,3,7,8-PECDF 2000 1260 63.2 1.53 1.28413C-2,3,4,7,8-PECDF 2000 1340 67.1 1.50 1.35113C-1,2,3,4,7,8-HXCDF 2000 1200 59.9 0.51 0.95413C-1,2,3,6,7,8-HXCDF 2000 1280 63.8 0.51 0.95813C-1,2,3,7,8,9-HXCDF 2000 1220 61.0 0.51 1.00513C-2,3,4,6,7,8-HXCDF 2000 1220 61.0 0.52 0.98013C-1,2,3,4,6,7,8-HPCDF 2000 1220 60.8 0.45 1.06213C-1,2,3,4,7,8,9-HPCDF 2000 1240 61.9 0.44 1.104

CLEANUP STANDARD

37CL-2,3,7,8-TCDD 200 127 63.5 1.014

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_L11830-3_Form2_DX8M_098S10_SJ933028.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration.(2) Contract-required limits for RRTs and ion abundance ratios are specified in Tables 2 and 9, respectively, Method 1613.(3) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form1A.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613DB5_WG26805-101_Form1A_DX8M_098S5_SJ933026.html; Workgroup: WG26805; Design ID: 988 ]





Project No. N/A











DETECTIONLIMIT

ION ABUND.RATIO 2

RRT 2

2,3,7,8-TCDD ND 0.07141,2,3,7,8-PECDD 3 ND 0.07141,2,3,4,7,8-HXCDD ND 0.07141,2,3,6,7,8-HXCDD ND 0.07141,2,3,7,8,9-HXCDD ND 0.07141,2,3,4,6,7,8-HPCDD NDR 0.187 0.0714 1.34 1.000OCDD 1.15 0.0714 0.94 1.0002,3,7,8-TCDF ND 0.07141,2,3,7,8-PECDF ND 0.07142,3,4,7,8-PECDF ND 0.07141,2,3,4,7,8-HXCDF ND 0.07141,2,3,6,7,8-HXCDF ND 0.07141,2,3,7,8,9-HXCDF ND 0.07142,3,4,6,7,8-HXCDF ND 0.07141,2,3,4,6,7,8-HPCDF 0.075 0.0714 0.97 1.0001,2,3,4,7,8,9-HPCDF ND 0.0714OCDF NDR 0.268 0.0714 0.56 1.002TOTAL TETRA-DIOXINS ND 0.0714TOTAL PENTA-DIOXINS ND 0.0714TOTAL HEXA-DIOXINS ND 0.0714TOTAL HEPTA-DIOXINS 0.207 0.0714TOTAL TETRA-FURANS ND 0.0714TOTAL PENTA-FURANS ND 0.0714TOTAL HEXA-FURANS ND 0.0714TOTAL HEPTA-FURANS 0.075 0.0714

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_WG26805-101_Form1A_DX8M_098S5_SJ933026.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required limits for percent recovery (R) are specified in Section 9.3.3, Method 1613.(3) Contract-required limits for RRTs and ion abundance ratios are specified in Tables 2 and 9, respectively, Method 1613. NOTE: There is no ionabundance ratio for 37Cl4-2,3,7,8-TCDD(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form2.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613DB5_WG26805-101_Form2_DX8M_098S5_SJ933026.html; Workgroup: WG26805; Design ID: 988 ]



Form 2PCDD/PCDF ANALYSIS REPORT


Project No. N/A











SPIKECONC.

CONC.FOUND

R(%) 2 ION ABUND.RATIO 3

RRT 3

13C-2,3,7,8-TCDD 2000 1040 51.9 0.80 1.01313C-1,2,3,7,8-PECDD 4 2000 1310 65.6 0.63 1.38313C-1,2,3,4,7,8-HXCDD 2000 1140 57.0 1.27 0.98713C-1,2,3,6,7,8-HXCDD 2000 1290 64.7 1.25 0.99013C-1,2,3,4,6,7,8-HPCDD 2000 1300 65.2 0.98 1.09413C-OCDD 4000 2130 53.3 0.89 1.17713C-2,3,7,8-TCDF 2000 975 48.7 0.73 0.96513C-1,2,3,7,8-PECDF 2000 1220 60.8 1.53 1.28413C-2,3,4,7,8-PECDF 2000 1250 62.5 1.50 1.35113C-1,2,3,4,7,8-HXCDF 2000 1100 55.2 0.51 0.95413C-1,2,3,6,7,8-HXCDF 2000 1150 57.4 0.52 0.95813C-1,2,3,7,8,9-HXCDF 2000 1150 57.3 0.52 1.00513C-2,3,4,6,7,8-HXCDF 2000 1160 57.8 0.51 0.98013C-1,2,3,4,6,7,8-HPCDF 2000 1160 57.8 0.45 1.06213C-1,2,3,4,7,8,9-HPCDF 2000 1170 58.4 0.44 1.103

CLEANUP STANDARD

37CL-2,3,7,8-TCDD 200 114 56.9 1.014

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_WG26805-101_Form2_DX8M_098S5_SJ933026.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required Ion Abundance Ratios are specified in Table 9, Method 1613.(3) Contract-required concentration range as determined from the percent of the test concentration in Table 6, Method 1613, under OPR.(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


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PCDD/PCDF ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 OPR Data Filename: DX8M_098 S: 2


Extraction Date: 22-Oct-2008 Analysis Date: 18-Nov-2008 Time: 19:59:35

ALL CONCENTRATIONS REPORTED ON THIS FORM ARE CONCENTRATIONS IN EXTRACT, BASED ON A 20 uL EXTRACT VOLUME.

COMPOUNDLAB

FLAG 1ION ABUND.

RATIO 2SPIKE CONC.

(ng/mL)

CONC.FOUND(ng/mL)

OPR CONC.LIMITS 3

(ng/mL) % RECOVERY

2,3,7,8-TCDD 0.78 10.6 9.87 7.10 - 16.7 93.11,2,3,7,8-PECDD 4 0.63 56.6 49.5 39.6 - 80.4 87.51,2,3,4,7,8-HXCDD 1.22 59.2 50.9 41.4 - 97.1 85.91,2,3,6,7,8-HXCDD 1.24 51.8 52.2 39.4 - 69.4 1011,2,3,7,8,9-HXCDD 1.25 56.7 50.9 36.3 - 91.9 89.81,2,3,4,6,7,8-HPCDD 1.04 50.0 43.8 35.0 - 70.0 87.5OCDD 0.88 108 90.8 84.2 - 155 84.22,3,7,8-TCDF 0.78 10.9 10.4 8.18 - 17.2 95.91,2,3,7,8-PECDF 1.54 50.0 42.3 40.0 - 67.0 84.72,3,4,7,8-PECDF 1.54 50.0 42.9 34.0 - 80.0 85.81,2,3,4,7,8-HXCDF 1.25 54.4 47.3 39.2 - 72.9 87.01,2,3,6,7,8-HXCDF 1.24 50.0 43.8 42.0 - 65.0 87.71,2,3,7,8,9-HXCDF 1.26 50.0 50.8 39.0 - 65.0 1022,3,4,6,7,8-HXCDF 1.24 53.1 49.6 37.2 - 82.8 93.51,2,3,4,6,7,8-HPCDF 1.04 50.0 51.0 41.0 - 61.0 1021,2,3,4,7,8,9-HPCDF 1.04 50.0 46.4 39.0 - 69.0 92.7OCDF 0.90 109 90.5 68.4 - 185 83.4

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_WG26805-105_Form8A_SJ933022.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required Ion Abundance Ratios are specified in Table 9, Method 1613.(3) Contract-required concentration limits for OPR as specified in Table 6, Method 1613. Labeled compound concentrations limits are based on requiredpercent recovery (Section 15.5, Method 1613).(4) Alternate confirmation and quantitation ions used for native and labeled PECDD.


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PCDD/PCDF ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 OPR Data Filename: DX8M_098 S: 2


Extraction Date: 22-Oct-2008 Analysis Date: 18-Nov-2008 Time: 19:59:35

ALL CONCENTRATIONS REPORTED ON THIS FORM ARE CONCENTRATIONS IN EXTRACT, BASED ON A 20 uL EXTRACT VOLUME.

LABELEDCOMPOUND

LABFLAG 1

ION ABUND.RATIO 2

SPIKE CONC.(ng/mL)

CONC.FOUND(ng/mL)

OPR CONC.LIMITS 3

(ng/mL) % RECOVERY

13C-2,3,7,8-TCDD 0.80 100 41.6 20.0-175 41.613C-1,2,3,7,8-PECDD 4 0.64 100 50.6 21.0-227 50.613C-1,2,3,4,7,8-HXCDD 1.24 100 49.3 21.0-193 49.313C-1,2,3,6,7,8-HXCDD 1.24 100 49.9 25.0-163 49.913C-1,2,3,4,6,7,8-HPCDD 0.97 100 52.8 26.0-166 52.813C-OCDD 0.89 200 102 26.0-397 50.913C-2,3,7,8-TCDF 0.77 100 37.5 22.0-152 37.513C-1,2,3,7,8-PECDF 1.54 100 50.0 21.0-192 50.013C-2,3,4,7,8-PECDF 1.53 100 49.7 13.0-328 49.713C-1,2,3,4,7,8-HXCDF 0.50 100 45.4 19.0-202 45.413C-1,2,3,6,7,8-HXCDF 0.51 100 48.7 21.0-159 48.713C-1,2,3,7,8,9-HXCDF 0.52 100 46.8 17.0-205 46.813C-2,3,4,6,7,8-HXCDF 0.52 100 46.4 22.0-176 46.413C-1,2,3,4,6,7,8-HPCDF 0.45 100 49.0 21.0-158 49.013C-1,2,3,4,7,8,9-HPCDF 0.44 100 50.9 20.0-186 50.9

CLEANUP STANDARD

37CL-2,3,7,8-TCDD 10.0 4.93 3.10-19.1 49.3

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB5_WG26805-105_Form8B_SJ933022.html)

(1) Where applicable, custom lab flags have been used on this report; NDR = peak detected but did not meet quantification criteria, result reportedrepresents the estimated maximum possible concentration.(2) Contract-required limits for RRTs and ion abundance ratios are specified in Tables 2 and 9, respectively, Method 1613.


For Axys Internal Use Only [ XSL Template: Form1A.xsl; Created: 11-Dec-2008 11:45:47; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613DB225_L11830-3_Form1A_DB83_264AS7_SJ933120.html; Workgroup: WG26805; Design ID: 988 ]





Project No. POP1406






Extract Volume (uL): 20 Sample Data Filename: DB83_264A S: 7

Injection Volume (uL): 2.0 Blank Data Filename: N/A

Dilution Factor: N/A Cal. Ver. Data Filename: DB83_264A S: 2



DETECTIONLIMIT

ION ABUND.RATIO 2

RRT 2

2,3,7,8-TCDF NDR 0.581 0.112 0.50 0.999

Page 1 of 1 (WG26805 - 1613_DIOXINS_1613DB225_L11830-3_Form1A_DB83_264AS7_SJ933120.html)

(1) Where applicable, custom lab flags have been used on this report; ND = not detected.(2) Concentrations that do not meet quantification criteria are not included in the TEQ calculations.


For Axys Internal Use Only [ XSL Template: TEQ.xsl; Created: 11-Dec-2008 11:46:18; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613-TEQ_L11830-3_TEQ_SJ933120.html; Workgroup: WG26805; Design ID: 988 ]


AXYS METHOD MLA-017 Rev 14 CLIENT SAMPLE NO.08LAO016BPCDD/PCDF ANALYSIS TEQ DATA REPORT




Matrix: ASH Lab Sample I.D.: L11830-3

Sample Size: 4.48 g (dry) GC Column ID(s): DB225DB5

Concentration Units: pg/g (dry weight basis) Sample Data Filenames: DB83_264A S: 7DX8M_098 S: 10

TEQCOMPOUND LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 1998TEF


2,3,7,8-TCDD ND 0.112 1 0.00e+00 5.60e-021,2,3,7,8-PECDD ND 0.112 1 0.00e+00 5.60e-021,2,3,4,7,8-HXCDD ND 0.112 0.1 0.00e+00 5.60e-031,2,3,6,7,8-HXCDD 0.130 0.112 0.1 1.30e-02 1.30e-021,2,3,7,8,9-HXCDD 0.192 0.112 0.1 1.92e-02 1.92e-021,2,3,4,6,7,8-HPCDD 1.61 0.112 0.01 1.61e-02 1.61e-02OCDD 6.41 0.112 0.0001 6.41e-04 6.41e-042,3,7,8-TCDF ND 0.112 0.1 0.00e+00 5.60e-031,2,3,7,8-PECDF ND 0.112 0.05 0.00e+00 2.80e-032,3,4,7,8-PECDF ND 0.112 0.5 0.00e+00 2.80e-021,2,3,4,7,8-HXCDF ND 0.112 0.1 0.00e+00 5.60e-031,2,3,6,7,8-HXCDF 0.176 0.112 0.1 1.76e-02 1.76e-021,2,3,7,8,9-HXCDF ND 0.112 0.1 0.00e+00 5.60e-032,3,4,6,7,8-HXCDF 0.240 0.112 0.1 2.40e-02 2.40e-021,2,3,4,6,7,8-HPCDF 0.713 0.112 0.01 7.13e-03 7.13e-031,2,3,4,7,8,9-HPCDF ND 0.112 0.01 0.00e+00 5.60e-04OCDF 0.445 0.112 0.0001 4.45e-05 4.45e-05


COMPOUND LABFLAG 1

CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


2,3,7,8-TCDD ND 0.112 1 0.00e+00 5.60e-021,2,3,7,8-PECDD ND 0.112 1 0.00e+00 5.60e-021,2,3,4,7,8-HXCDD ND 0.112 0.1 0.00e+00 5.60e-031,2,3,6,7,8-HXCDD 0.130 0.112 0.1 1.30e-02 1.30e-021,2,3,7,8,9-HXCDD 0.192 0.112 0.1 1.92e-02 1.92e-021,2,3,4,6,7,8-HPCDD 1.61 0.112 0.01 1.61e-02 1.61e-02OCDD 6.41 0.112 0.0003 1.92e-03 1.92e-032,3,7,8-TCDF ND 0.112 0.1 0.00e+00 5.60e-031,2,3,7,8-PECDF ND 0.112 0.03 0.00e+00 1.68e-032,3,4,7,8-PECDF ND 0.112 0.3 0.00e+00 1.68e-021,2,3,4,7,8-HXCDF ND 0.112 0.1 0.00e+00 5.60e-031,2,3,6,7,8-HXCDF 0.176 0.112 0.1 1.76e-02 1.76e-021,2,3,7,8,9-HXCDF ND 0.112 0.1 0.00e+00 5.60e-032,3,4,6,7,8-HXCDF 0.240 0.112 0.1 2.40e-02 2.40e-021,2,3,4,6,7,8-HPCDF 0.713 0.112 0.01 7.13e-03 7.13e-031,2,3,4,7,8,9-HPCDF ND 0.112 0.01 0.00e+00 5.60e-04OCDF 0.445 0.112 0.0003 1.34e-04 1.34e-04

TOTAL TEQ 0.0991 0.253

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(1) Where applicable, custom lab flags have been used on this report; ND = not detected.(2) Concentrations that do not meet quantification criteria are not included in the TEQ calculations.


For Axys Internal Use Only [ XSL Template: TEQ.xsl; Created: 11-Dec-2008 11:46:18; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_1613-TEQ_WG26805-101_TEQ_SJ933026.html; Workgroup: WG26805; Design ID: 988 ]


AXYS METHOD MLA-017 Rev 14 CLIENT SAMPLE NO.Lab BlankPCDD/PCDF ANALYSIS TEQ DATA REPORT





Sample Size: 7.00 g GC Column ID: DB5

Concentration Units: pg/g Sample Data Filename: DX8M_098 S: 5

TEQCOMPOUND LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 1998TEF


2,3,7,8-TCDD ND 0.0714 1 0.00e+00 3.57e-021,2,3,7,8-PECDD ND 0.0714 1 0.00e+00 3.57e-021,2,3,4,7,8-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,6,7,8-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8,9-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,4,6,7,8-HPCDD ND 0.0714 0.01 0.00e+00 3.57e-04OCDD 1.15 0.0714 0.0001 1.15e-04 1.15e-042,3,7,8-TCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8-PECDF ND 0.0714 0.05 0.00e+00 1.79e-032,3,4,7,8-PECDF ND 0.0714 0.5 0.00e+00 1.79e-021,2,3,4,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,6,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8,9-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-032,3,4,6,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,4,6,7,8-HPCDF 0.075 0.0714 0.01 7.50e-04 7.50e-041,2,3,4,7,8,9-HPCDF ND 0.0714 0.01 0.00e+00 3.57e-04OCDF ND 0.0714 0.0001 0.00e+00 3.57e-06


COMPOUND LABFLAG 1

CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


2,3,7,8-TCDD ND 0.0714 1 0.00e+00 3.57e-021,2,3,7,8-PECDD ND 0.0714 1 0.00e+00 3.57e-021,2,3,4,7,8-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,6,7,8-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8,9-HXCDD ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,4,6,7,8-HPCDD ND 0.0714 0.01 0.00e+00 3.57e-04OCDD 1.15 0.0714 0.0003 3.45e-04 3.45e-042,3,7,8-TCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8-PECDF ND 0.0714 0.03 0.00e+00 1.07e-032,3,4,7,8-PECDF ND 0.0714 0.3 0.00e+00 1.07e-021,2,3,4,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,6,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,7,8,9-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-032,3,4,6,7,8-HXCDF ND 0.0714 0.1 0.00e+00 3.57e-031,2,3,4,6,7,8-HPCDF 0.075 0.0714 0.01 7.50e-04 7.50e-041,2,3,4,7,8,9-HPCDF ND 0.0714 0.01 0.00e+00 3.57e-04OCDF ND 0.0714 0.0003 0.00e+00 1.07e-05

TOTAL TEQ 0.00110 0.114

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AXYS METHOD MLA-017 Rev 14Form 5

PCDD/PCDF RT WINDOW AND ISOMER SPECIFICITY STANDARDSAXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811

Instrument ID: HR GC/MS Initial Calibration Date: 06-Nov-2008

RT Window Data Filename: Analysis Date: Time:

DB-5 IS Data Filename: Analysis Date: Time:

DB-225 IS Data Filename: DB83_249E S: 1 Analysis Date: 06-Nov-2008 Time: 12:43:06

DB225 RT WINDOW DEFINING STANDARDS RESULT

ISOMERS ABSOLUTERT

1,3,6,8-TCDD (F) N/A1,2,8,9-TCDD (L) N/A

1,2,4,7,9-PECDD (F) N/A1,2,3,8,9-PECDD (L) N/A

1,2,4,6,7,9-HXCDD (F) N/A1,2,3,4,6,7-HXCDD (L) N/A

1,2,3,4,6,7,9-HPCDD (F) N/A1,2,3,4,6,7,8-HPCDD (L) N/A

ISOMERS ABSOLUTERT

1,3,6,8-TCDF (F) N/A1,2,8,9-TCDF (L) N/A

1,3,4,6,8-PECDF (F) N/A1,2,3,8,9-PECDF (L) N/A

1,2,3,4,6,8-HXCDF (F) N/A1,2,3,4,8,9-HXCDF (L) N/A

1,2,3,4,6,7,8-HPCDF (F) N/A1,2,3,4,7,8,9-HPCDF (L) N/A

(F) = First eluting isomer (DB-5); (L) = Last eluting isomer (DB-5)

ISOMER SPECIFICITY (IS) TEST STANDARDS RESULT

Isomers % Valley HeightBetween Compared

Peaks

1,2,3,4-TCDD1,2,7,8-TCDD

N/A

1,2,7,8-TCDD1,4,7,8-TCDD

N/A

1,4,7,8-TCDD1,2,3,7-TCDD

N/A

1,2,3,7-TCDD1,2,3,8-TCDD

N/A


Peaks

1,2,3,8-TCDD2,3,7,8-TCDD

N/A

2,3,4,7-TCDF2,3,7,8-TCDF

12

2,3,7,8-TCDF1,2,3,9-TCDF

6.6

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Instrument ID: HR GC/MS Initial Calibration Date: 06-Nov-2008

RT Window Data Filename: Analysis Date: Time:


DB-225 IS Data Filename: DB83_264A S: 1 Analysis Date: 18-Nov-2008 Time: 08:37:25


ISOMERS ABSOLUTERT

1,3,6,8-TCDD (F) N/A1,2,8,9-TCDD (L) N/A

1,2,4,7,9-PECDD (F) N/A1,2,3,8,9-PECDD (L) N/A

1,2,4,6,7,9-HXCDD (F) N/A1,2,3,4,6,7-HXCDD (L) N/A

1,2,3,4,6,7,9-HPCDD (F) N/A1,2,3,4,6,7,8-HPCDD (L) N/A

ISOMERS ABSOLUTERT

1,3,6,8-TCDF (F) N/A1,2,8,9-TCDF (L) N/A

1,3,4,6,8-PECDF (F) N/A1,2,3,8,9-PECDF (L) N/A

1,2,3,4,6,8-HXCDF (F) N/A1,2,3,4,8,9-HXCDF (L) N/A

1,2,3,4,6,7,8-HPCDF (F) N/A1,2,3,4,7,8,9-HPCDF (L) N/A




Peaks

1,2,3,4-TCDD1,2,7,8-TCDD

N/A

1,2,7,8-TCDD1,4,7,8-TCDD

N/A

1,4,7,8-TCDD1,2,3,7-TCDD

N/A

1,2,3,7-TCDD1,2,3,8-TCDD

N/A


Peaks

1,2,3,8-TCDD2,3,7,8-TCDD

N/A

2,3,4,7-TCDF2,3,7,8-TCDF

11

2,3,7,8-TCDF1,2,3,9-TCDF

14

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Instrument ID: HR GC/MS Initial Calibration Date: 25-Oct-2008

RT Window Data Filename: DX8M_084B S: 1 Analysis Date: 25-Oct-2008 Time: 11:44:02

DB-5 IS Data Filename: DX8M_084B S: 1 Analysis Date: 25-Oct-2008 Time: 11:44:02



ISOMERS ABSOLUTERT

1,3,6,8-TCDD (F) 22:541,2,8,9-TCDD (L) 28:16

1,2,4,7,9-PECDD (F) 32:021,2,3,8,9-PECDD (L) 37:05

1,2,4,6,7,9-HXCDD (F) 40:021,2,3,4,6,7-HXCDD (L) 42:40

1,2,3,4,6,7,9-HPCDD (F) 45:461,2,3,4,6,7,8-HPCDD (L) 46:41

ISOMERS ABSOLUTERT

1,3,6,8-TCDF (F) 21:221,2,8,9-TCDF (L) 28:07

1,3,4,6,8-PECDF (F) 28:501,2,3,8,9-PECDF (L) 37:07

1,2,3,4,6,8-HXCDF (F) 38:591,2,3,4,8,9-HXCDF (L) 43:01

1,2,3,4,6,7,8-HPCDF (F) 45:191,2,3,4,7,8,9-HPCDF (L) 47:05




Peaks

1,2,3,4-TCDD1,2,7,8-TCDD

0

1,2,7,8-TCDD1,4,7,8-TCDD

0

1,4,7,8-TCDD1,2,3,7-TCDD

0

1,2,3,7-TCDD1,2,3,8-TCDD

DB-5 column;co-elute as per

Figure 6 in Method


Peaks

1,2,3,8-TCDD2,3,7,8-TCDD

18

2,3,4,7-TCDF2,3,7,8-TCDF

N/A

2,3,7,8-TCDF1,2,3,9-TCDF

N/A

Page 1 of 1 (WG26805 - 1613_DIOXINS__DX8M_084BS1_Form5_SJ924704.html)

Approved by: ___________Shelley Facchin___________ QA/QC Chemist

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Instrument ID: HR GC/MS Initial Calibration Date: 25-Oct-2008

RT Window Data Filename: DX8M_098 S: 1 Analysis Date: 18-Nov-2008 Time: 19:04:35

DB-5 IS Data Filename: DX8M_098 S: 1 Analysis Date: 18-Nov-2008 Time: 19:04:35



ISOMERS ABSOLUTERT

1,3,6,8-TCDD (F) 22:531,2,8,9-TCDD (L) 28:14

1,2,4,7,9-PECDD (F) 31:591,2,3,8,9-PECDD (L) 37:02

1,2,4,6,7,9-HXCDD (F) 40:011,2,3,4,6,7-HXCDD (L) 42:40

1,2,3,4,6,7,9-HPCDD (F) 45:461,2,3,4,6,7,8-HPCDD (L) 46:40

ISOMERS ABSOLUTERT

1,3,6,8-TCDF (F) 21:201,2,8,9-TCDF (L) 28:04

1,3,4,6,8-PECDF (F) 28:471,2,3,8,9-PECDF (L) 37:05

1,2,3,4,6,8-HXCDF (F) 38:581,2,3,4,8,9-HXCDF (L) 43:00

1,2,3,4,6,7,8-HPCDF (F) 45:171,2,3,4,7,8,9-HPCDF (L) 47:05




Peaks

1,2,3,4-TCDD1,2,7,8-TCDD

0

1,2,7,8-TCDD1,4,7,8-TCDD

0

1,4,7,8-TCDD1,2,3,7-TCDD

0

1,2,3,7-TCDD1,2,3,8-TCDD

DB-5 column;co-elute as per

Figure 6 in Method


Peaks

1,2,3,8-TCDD2,3,7,8-TCDD

22

2,3,4,7-TCDF2,3,7,8-TCDF

N/A

2,3,7,8-TCDF1,2,3,9-TCDF

N/A

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(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits as specified in Table 9, Method 1613.(4) Contract-required concentration range as determined from the percent of the test concentration in Table 6, Method 1613, under VER.


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PCDD/PCDF CALIBRATION VERIFICATIONAXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811

Initial Calibration Date: 06-Nov-2008 VER Data Filename: DB83_264A S: 2

Instrument ID: HR GC/MS Analysis Date: 18-Nov-2008

GC Column ID: DB225 Analysis Time: 09:13:00

LABFLAG 1

MZ'sFORMINGRATIO 2

IONABUND.RATIO

QCLIMITS 3

CONC.FOUND(ng/mL)

CONC.RANGE

(ng/mL) 4

COMPOUND

2,3,7,8-TCDF M/M+2 0.76 0.65-0.89 9.97 9.1 - 13

Page 1 of 1 (WG26805 - 1613_DIOXINS_DB83_264AS2__Form4A_SJ933117.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required limits for Relative Retention Times (RRT) as specified in Table 2, Method 1613.


For Axys Internal Use Only [ XSL Template: Form6A.xsl; Created: 11-Dec-2008 11:45:47; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_DB83_264AS2__Form6A_SJ933117.html; Workgroup: WG26805; Design ID: 988 ]


PCDD/PCDF RELATIVE RETENTION TIMESAXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811

Initial Calibration Date: 06-Nov-2008 VER Data Filename: DB83_264A S: 2



LABFLAG 1

RETENTIONTIME

REFERENCE

RRT RRTQC

LIMITS 2

COMPOUND

2,3,7,8-TCDF 13C-2,3,7,8-TCDF 1.001 0.999-1.003

Page 1 of 1 (WG26805 - 1613_DIOXINS_DB83_264AS2__Form6A_SJ933117.html)

(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits as specified in Table 9, Method 1613.(4) Contract-required concentration range as determined from the percent of the test concentration in Table 6, Method 1613, under VER.(5) Alternate confirmation and quantitation ions used for native and labeled PECDD.


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Initial Calibration Date: 25-Oct-2008 VER Data Filename: DX8M_098 S: 1



LABFLAG 1

MZ'sFORMINGRATIO 2

IONABUND.RATIO

QCLIMITS 3

CONC.FOUND(ng/mL)

CONC.RANGE

(ng/mL) 4

COMPOUND

2,3,7,8-TCDD M/M+2 0.78 0.65-0.89 10.6 8.6 - 14.21,2,3,7,8-PECDD 5 M/M+2 0.61 0.51-0.70 51.0 41 - 67.61,2,3,4,7,8-HXCDD M+2/M+4 1.23 1.05-1.43 53.4 44 - 72.31,2,3,6,7,8-HXCDD M+2/M+4 1.22 1.05-1.43 55.5 43 - 711,2,3,7,8,9-HXCDD M+2/M+4 1.22 1.05-1.43 54.5 44 - 65.91,2,3,4,6,7,8-HPCDD M+2/M+4 1.03 0.88-1.20 46.3 41 - 55.1OCDD M+2/M+4 0.88 0.76-1.02 97.5 79 - 1262,3,7,8-TCDF M/M+2 0.77 0.65-0.89 10.9 9 - 12.81,2,3,7,8-PECDF M+2/M+4 1.55 1.32-1.78 45.7 38 - 55.22,3,4,7,8-PECDF M+2/M+4 1.57 1.32-1.78 46.9 39 - 57.31,2,3,4,7,8-HXCDF M+2/M+4 1.24 1.05-1.43 50.8 45 - 561,2,3,6,7,8-HXCDF M+2/M+4 1.23 1.05-1.43 45.6 42 - 54.21,2,3,7,8,9-HXCDF M+2/M+4 1.24 1.05-1.43 49.9 47 - 58.82,3,4,6,7,8-HXCDF M+2/M+4 1.26 1.05-1.43 51.9 47 - 60.41,2,3,4,6,7,8-HPCDF M+2/M+4 1.03 0.88-1.20 50.3 45 - 551,2,3,4,7,8,9-HPCDF M+2/M+4 1.06 0.88-1.20 49.0 43 - 58OCDF M+2/M+4 0.91 0.76-1.02 98.9 66 - 165

Page 1 of 1 (WG26805 - 1613_DIOXINS_DX8M_098S1__Form4A_SJ933021.html)

(1) Where applicable, custom lab flags have been used on this report.(2) See Table 8, Method 1613, for m/z specifications.(3) Ion Abundance Ratio Control Limits as specified in Table 9, Method 1613.(4) Contract-required concentration range as determined from the percent of the test concentration in Table 6, Method 1613, under VER.(5) Alternate confirmation and quantitation ions used for native and labeled PECDD.(6) No ion abundance ratio for 37Cl4-2,3,7,8-TCDD; concentration reported.


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LABFLAG 1

MZ'sFORMINGRATIO 2

IONABUND.RATIO

QCLIMITS 3

CONC.FOUND(ng/mL)

CONC.RANGE

(ng/mL) 4

LABELED COMPOUND

13C-2,3,7,8-TCDD M/M+2 0.80 0.65-0.89 98.4 82 - 12113C-1,2,3,7,8-PECDD 5 M/M+2 0.63 0.51-0.70 105 62 - 16013C-1,2,3,4,7,8-HXCDD M+2/M+4 1.25 1.05-1.43 94.5 85 - 11713C-1,2,3,6,7,8-HXCDD M+2/M+4 1.24 1.05-1.43 97.5 85 - 11813C-1,2,3,4,6,7,8-HPCDD M+2/M+4 0.97 0.88-1.20 106 72 - 13813C-OCDD M+2/M+4 0.89 0.76-1.02 204 96 - 41513C-2,3,7,8-TCDF M/M+2 0.77 0.65-0.89 98.9 71 - 14013C-1,2,3,7,8-PECDF M+2/M+4 1.52 1.32-1.78 102 76 - 13013C-2,3,4,7,8-PECDF M+2/M+4 1.50 1.32-1.78 102 77 - 13013C-1,2,3,4,7,8-HXCDF M/M+2 0.51 0.43-0.59 90.5 76 - 13113C-1,2,3,6,7,8-HXCDF M/M+2 0.51 0.43-0.59 94.7 70 - 14313C-1,2,3,7,8,9-HXCDF M/M+2 0.52 0.43-0.59 94.7 74 - 13513C-2,3,4,6,7,8-HXCDF M/M+2 0.51 0.43-0.59 92.9 73 - 13713C-1,2,3,4,6,7,8-HPCDF M/M+2 0.45 0.37-0.51 96.9 78 - 12913C-1,2,3,4,7,8,9-HPCDF M/M+2 0.44 0.37-0.51 101 77 - 129

CLEANUP STANDARD

37CL-2,3,7,8-TCDD 6 9.78 7.9 - 12.7

Page 1 of 1 (WG26805 - 1613_DIOXINS_DX8M_098S1__Form4B_SJ933021.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required limits for Relative Retention Times (RRT) as specified in Table 2, Method 1613.(3) Alternate confirmation and quantitation ions used for native and labeled PECDD.


For Axys Internal Use Only [ XSL Template: Form6A.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_DX8M_098S1__Form6A_SJ933021.html; Workgroup: WG26805; Design ID: 988 ]






LABFLAG 1

RETENTIONTIME

REFERENCE

RRT RRTQC

LIMITS 2

COMPOUND

2,3,7,8-TCDD 13C-2,3,7,8-TCDD 1.001 0.999-1.0021,2,3,7,8-PECDD 3 13C-1,2,3,7,8-PECDD 1.000 0.999-1.0021,2,3,4,7,8-HXCDD 13C-1,2,3,4,7,8-HXCDD 1.000 0.999-1.0011,2,3,6,7,8-HXCDD 13C-1,2,3,6,7,8-HXCDD 1.000 0.998-1.0041,2,3,7,8,9-HXCDD 13C-1,2,3,6,7,8-HXCDD 1.000 1.000-1.0191,2,3,4,6,7,8-HPCDD 13C-1,2,3,4,6,7,8-HPCDD 1.000 0.999-1.001OCDD 13C-OCDD 1.000 0.999-1.0012,3,7,8-TCDF 13C-2,3,7,8-TCDF 1.001 0.999-1.0031,2,3,7,8-PECDF 13C-1,2,3,7,8-PECDF 1.001 0.999-1.0022,3,4,7,8-PECDF 13C-2,3,4,7,8-PECDF 1.000 0.999-1.0021,2,3,4,7,8-HXCDF 13C-1,2,3,4,7,8-HXCDF 1.000 0.999-1.0011,2,3,6,7,8-HXCDF 13C-1,2,3,6,7,8-HXCDF 1.000 0.997-1.0051,2,3,7,8,9-HXCDF 13C-1,2,3,7,8,9-HXCDF 1.000 0.999-1.0012,3,4,6,7,8-HXCDF 13C-2,3,4,6,7,8-HXCDF 1.000 0.999-1.0011,2,3,4,6,7,8-HPCDF 13C-1,2,3,4,6,7,8-HPCDF 1.000 0.999-1.0011,2,3,4,7,8,9-HPCDF 13C-1,2,3,4,7,8,9-HPCDF 1.000 0.999-1.001OCDF 13C-OCDD 1.002 0.999-1.008

Page 1 of 1 (WG26805 - 1613_DIOXINS_DX8M_098S1__Form6A_SJ933021.html)

(1) Where applicable, custom lab flags have been used on this report.(2) Contract-required limits for Relative Retention Times (RRT) as specified in Table 2, Method 1613.


For Axys Internal Use Only [ XSL Template: Form6B.xsl; Created: 11-Dec-2008 11:45:11; Application: XMLTransformer-1.9.16;Report Filename: 1613_DIOXINS_DX8M_098S1__Form6B_SJ933021.html; Workgroup: WG26805; Design ID: 988 ]






LABFLAG 1

RETENTIONTIME

REFERENCE

RRT RRTQC

LIMITS 2

LABELED COMPOUND

13C-2,3,7,8-TCDD 13C-1,2,3,4-TCDD 1.013 0.976-1.04313C-1,2,3,7,8-PECDD 13C-1,2,3,4-TCDD 1.387 1.000-1.56713C-1,2,3,4,7,8-HXCDD 13C-1,2,3,7,8,9-HXCDD 0.987 0.977-1.00013C-1,2,3,6,7,8-HXCDD 13C-1,2,3,7,8,9-HXCDD 0.990 0.981-1.00313C-1,2,3,4,6,7,8-HPCDD 13C-1,2,3,7,8,9-HXCDD 1.094 1.086-1.11013C-OCDD 13C-1,2,3,7,8,9-HXCDD 1.178 1.032-1.31113C-2,3,7,8-TCDF 13C-1,2,3,4-TCDD 0.966 0.923-1.10313C-1,2,3,7,8-PECDF 13C-1,2,3,4-TCDD 1.286 1.000-1.42513C-2,3,4,7,8-PECDF 13C-1,2,3,4-TCDD 1.355 1.011-1.52613C-1,2,3,4,7,8-HXCDF 13C-1,2,3,7,8,9-HXCDD 0.954 0.944-0.97013C-1,2,3,6,7,8-HXCDF 13C-1,2,3,7,8,9-HXCDD 0.958 0.949-0.97513C-1,2,3,7,8,9-HXCDF 13C-1,2,3,7,8,9-HXCDD 1.005 0.977-1.04713C-2,3,4,6,7,8-HXCDF 13C-1,2,3,7,8,9-HXCDD 0.980 0.959-1.02113C-1,2,3,4,6,7,8-HPCDF 13C-1,2,3,7,8,9-HXCDD 1.062 1.043-1.08513C-1,2,3,4,7,8,9-HPCDF 13C-1,2,3,7,8,9-HXCDD 1.104 1.057-1.151

CLEANUP STANDARD

37CL-2,3,7,8-TCDD 13C-1,2,3,4-TCDD 1.014 0.989-1.052

Page 1 of 1 (WG26805 - 1613_DIOXINS_DX8M_098S1__Form6B_SJ933021.html)

CALUX Analysis Report (PCDD/F and

Dioxin-like PCB TEQs)

2008.10.01Hiyoshi Corporation

Final report (Lao PDR)

The World Bank

TERMS OF REFERENCECAMBODIA, LAO PDR, MALAYSIA, AND THAILAND

BIOMONITORING OF POPs AND POPs-LIKE CHEMICALS -

PCDDs/Fs DL-PCBs DXNs LOD LOQ PCDDs/Fs DL-PCBs DXNs PCDDs/Fs DL-PCBs DXNs

1 08Lao001A Soil 3.14 4.7 0 4.7 0.50 1.0 1.1 0 1.1 1.0 0 1.02 08Lao002A Soil 3.21 3.5 2.0 5.5 0.49 1.0 0.80 5.1 5.9 0.74 5.3 6.03 08Lao003A Soil 2.45 38 4.7 42 0.64 1.3 8.7 12 21 8.1 12 204 08Lao004A Soil 2.88 4.9 1.8 6.6 0.54 1.1 1.1 4.5 5.6 1.0 4.6 5.75 08Lao005A Soil 2.58 6.1 5.1 11 0.61 1.2 1.4 13 14 1.3 13 156 08Lao006A Soil 2.21 2.3 (0.97) 2.3 0.71 1.4 0.52 (2.5) 3.0 0.48 (2.6) 3.17 08Lao007A Sediment 2.80 9.7 1.1 11 0.56 1.1 2.2 3.7 5.9 2.4 2.3 4.78 08Lao008A Soil 3.13 7.9 0 7.9 0.50 1.0 1.8 0 1.8 1.7 0 1.79 08Lao009A Soil 3.49 13 14 27 2.2 4.5 3.0 35 38 2.8 36 39

10 08Lao010A Soil 2.73 336 9.3 346 0.57 1.1 78 24 101 72 25 9711 08Lao011A Soil 3.26 22 5.1 28 0.48 1.0 5.2 13 18 4.8 13 1812 08Lao012A Soil 3.27 23 2.5 26 0.48 1.0 5.4 6.4 12 5.0 6.6 1213 08Lao013A Sediment 1.62 43 7.0 50 0.97 1.9 9.9 18 28 10 14 2514 08Lao014A Soil 2.68 83 60 143 2.9 5.8 19 152 171 18 158 17615 08Lao015A Soil 3.43 40 14 53 2.3 4.6 9.1 35 44 8.5 37 4516 08Lao016A Soil 3.37 77 9.3 86 2.3 4.6 18 23 41 17 24 4117 08Lao017A Soil 2.86 15 2.6 18 1.1 2.2 3.5 6.6 10 3.2 6.9 1018 08Lao019A Soil 2.96 3.2 0 3.2 1.1 2.1 0.75 0 0.75 0.69 0 0.6919 08Lao020A Soil 3.13 22 (1.5) 22 1.0 2.0 5.0 (3.8) 8.8 4.7 (3.9) 8.620 08Lao021A Soil 3.08 4.1 3.4 7.5 1.0 2.0 0.95 8.5 9.5 0.88 8.8 9.721 08Lao022A Soil 2.90 4.4 0 4.4 1.1 2.2 1.0 0 1.0 0.95 0 0.9522 08Lao023A Soil 3.03 8.7 3.4 12 0.51 1.0 2.0 8.7 11 1.9 9.0 1123 08Lao025A Soil 3.29 3.6 0 3.6 0.47 0.9 0.84 0 0.84 0.78 0 0.7824 08Lao026A Sediment 1.54 4.2 0 4.2 1.0 2.0 0.95 0 0.95 1.0 0 1.025 08Lao027A Soil 3.14 3.7 (0.65) 3.7 0.50 1.0 0.86 (1.6) 2.5 0.80 (1.7) 1.426 08Lao028A Soil 3.48 6.8 3.8 11 0.45 0.9 1.6 9.5 11 1.4 9.9 1127 08Lao032A Soil 3.48 308 96 404 0.90 1.8 71 243 314 66 253 31928 08Lao033A Soil 3.07 10 15 25 1.0 2.0 2.3 39 41 2.2 40 43

①PCDD/Fs ②DL-PCBs ③DXNs ④PCDD/Fs ⑤DL-PCBs ⑥DXNsSoil 0.231 2.53 ①＋② 0.214 2.63 ④＋⑤

Sediment 0.226 3.21 ①＋② 0.244 2.04 ④＋⑤

*　"0" represent below detection limit (LOD)**　number in bracket represent the number below quantification limit and above detection limit which has been converted into DXNs

Final report (Soil＆Sediment)－１

Conversion factor

***　Average of quantified and measured toxic equivalent value and calculate standard deviation and coefficient of variation(CV) from standard curve obtained from 5 time measured adjusted standard for detection limit and create quality profile. Detection

WHO-TEF1998 WHO-TEF2006

pg-TEQ(WHO1998)/g pg-TEQ(WHO2006)/g

Sample No. Sample type Sample

volume(g)pgCALUX-TEQ/g

CALUX Raw Date

****　Guideline for quality control of dioxin environmental measurement, March 3, 2006 by Ministry of the Environment, was used to set quantification limit and detection limit was

Conversion factor

WHO-TEF1998

Final report (Soil)－２

WHO-TEF2006

020406080

100120140160180200220240260280300320340

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Sample No.

CA

LUX

(pg-

TEQ

/g)

PCDDs/FsDL-PCBsDXNs

020406080

100120140160180200220240260280300320340

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Sample No.

CA

LUX

(pg-

TEQ

/g)

PCDDs/FsDL-PCBsDXNs

PCDDs/Fs DL-PCBs DXNs LOD LOQ

108Lao018A　　　　　　　　　　　

　 0.0625 0 0 0 25 50

*　"0" represent below detection limit (LOD)**　number in bracket represent the number below quantification limit and above detection limit which has been converted into DXNs

Final report (Water)

pgCALUX-TEQ/l

CALUX Raw Date

****　Guideline for quality control of dioxin environmental measurement, March 3, 2006 by Ministry of the Environment, was used to set quantification limit and detection limit was

***　Average of quantified and measured toxic equivalent value and calculate standard deviation and coefficient of variation(CV) from standard curve obtained from 5 time measured adjusted standard for detection limit and create quality profile. Detection

Sample No. Sample type

Sample volume(ｌ)

Blood PCB Chemistry

(1) Where applicable, custom lab flags have been used on this report.(2) All header information pertains to the initial instrumental analysis of the sample extract. Additional sample datafiles listed refer to secondary analysisof the sample extract.


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AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.08LAO-B01Sample Collection:N/A



Project No. POP1406

Contract No.: 2607 Lab Sample I.D.: L11590-1 L

Matrix: BLOOD Sample Size: 40.8 g (wet)

Sample Receipt Date: 15-Aug-2008 Initial Calibration Date: 30-Jul-2008

Extraction Date: 03-Sep-2008 Instrument ID: HR GC/MS

Analysis Date: 04-Oct-2008 Time: 13:54:05 GC Column ID: SPB OCTYL

Extract Volume (uL): 20 Sample Data Filename(s): PB8B_261 S: 6, PB8B_269A S: 4

Injection Volume (uL): 1.0 Blank Data Filename: PB8B_261 S: 5

Dilution Factor: N/A Cal. Ver. Data Filename: PB8B_261 S: 1

Concentration Units: pg/g (wet weight basis) % Lipid: 0.39


CONC.FOUND

Total Monochloro Biphenyls 2.11




Total Pentachloro Biphenyls 183

Total Hexachloro Biphenyls 385

Total Heptachloro Biphenyls 173




TOTAL PCBs 853

Page 1 of 1 (WG26343 - 1668_PCB1668_HomTotals-TEQs_L11590-1_Form1AHT_SJ910828.html)



For Axys Internal Use Only [ XSL Template: .xsl; Created: 28-Oct-2008 07:16:20; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_L11590-1_Form1AHT_SJ910828_Lipid.html; Workgroup: WG26343; Design ID: 925 ]





Project No. POP1406


Matrix: BLOOD Sample Size: 0.161 g (lipid)







Concentration Units: pg/g (lipid weight basis) % Lipid: 0.39


CONC.FOUND

Total Monochloro Biphenyls 535

Total Dichloro Biphenyls 1030

Total Trichloro Biphenyls 2940

Total Tetrachloro Biphenyls 7300




Total Octachloro Biphenyls 14600

Total Nonachloro Biphenyls 1560

Decachloro Biphenyl 387

TOTAL PCBs 216000

Page 1 of 1 (WG26343 - 1668_PCB1668_HomTotals-TEQs_L11590-1_Form1AHT_SJ910828_Lipid.html)



For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 15-Oct-2008 10:22:59; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_L11590-1_TEQ_SJ910828.html; Workgroup: WG26343; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.08LAO-B01Form 1C




Matrix: BLOOD Lab Sample I.D.: L11590-1 L

Sample Size: 40.8 g (wet) GC Column ID(s): SPB OCTYL

Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_261 S: 6PB8B_269A S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 1.69 0.0580 0.0001 1.69e-04 1.69e-043,4,4',5-TeCB 81 1.69 0.0556 0.0003 5.07e-04 5.07e-042,3,3',4,4'-PeCB 105 25.1 0.195 0.00003 7.53e-04 7.53e-042,3,4,4',5-PeCB 114 4.26 0.182 0.00003 1.28e-04 1.28e-042,3',4,4',5-PeCB 118 93.0 0.182 0.00003 2.79e-03 2.79e-032',3,4,4',5-PeCB 123 2.31 0.188 0.00003 6.93e-05 6.93e-053,3',4,4',5-PeCB 126 1.89 0.211 0.1 1.89e-01 1.89e-012,3,3',4,4',5-HxCB 156 156 + 157 C 33.3 0.0492 0.00003 9.99e-04 9.99e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 11.4 0.0385 0.00003 3.42e-04 3.42e-043,3',4,4',5,5'-HxCB 169 1.41 0.0588 0.03 4.23e-02 4.23e-022,3,3',4,4',5,5'-HpCB 189 3.30 0.0894 0.00003 9.90e-05 9.90e-05

TOTAL TEQ 0.237 0.237




For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 15-Oct-2008 10:22:59; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_L11590-1_TEQ_SJ910828_Lipid.html; Workgroup: WG26343; Design ID: 925 ]







Sample Size: 0.161 g (lipid) GC Column ID(s): SPB OCTYL

Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_261 S: 6PB8B_269A S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 428 14.7 0.0001 4.28e-02 4.28e-023,4,4',5-TeCB 81 428 14.1 0.0003 1.28e-01 1.28e-012,3,3',4,4'-PeCB 105 6360 49.4 0.00003 1.91e-01 1.91e-012,3,4,4',5-PeCB 114 1080 46.1 0.00003 3.24e-02 3.24e-022,3',4,4',5-PeCB 118 23600 46.1 0.00003 7.08e-01 7.08e-012',3,4,4',5-PeCB 123 585 47.6 0.00003 1.76e-02 1.76e-023,3',4,4',5-PeCB 126 479 53.4 0.1 4.79e+01 4.79e+012,3,3',4,4',5-HxCB 156 156 + 157 C 8430 12.5 0.00003 2.53e-01 2.53e-012,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 2890 9.75 0.00003 8.67e-02 8.67e-023,3',4,4',5,5'-HxCB 169 357 14.9 0.03 1.07e+01 1.07e+012,3,3',4,4',5,5'-HpCB 189 836 22.6 0.00003 2.51e-02 2.51e-02

TOTAL TEQ 60.1 60.1

Page 1 of 1 (WG26343 - 1668_PCB1668_HomTotals-TEQs_L11590-1_TEQ_SJ910828_Lipid.html)








Project No. POP1406

Contract No.: 2607 Lab Sample I.D.: L11590-2 Li





Extract Volume (uL): 20 Sample Data Filename(s): PB8B_261A S: 1, PB8B_269A S: 5





CONC.FOUND











TOTAL PCBs 2750









Project No. POP1406






Extract Volume (uL): 20 Sample Data Filename(s): PB8B_261A S: 1, PB8B_269A S: 5





CONC.FOUND











TOTAL PCBs 580000










Matrix: BLOOD Lab Sample I.D.: L11590-2 Li


Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_261A S: 1PB8B_269A S: 5

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 2.27 0.0722 0.0001 2.27e-04 2.27e-043,4,4',5-TeCB 81 2.24 0.0693 0.0003 6.72e-04 6.72e-042,3,3',4,4'-PeCB 105 29.9 0.139 0.00003 8.97e-04 8.97e-042,3,4,4',5-PeCB 114 8.41 0.135 0.00003 2.52e-04 2.52e-042,3',4,4',5-PeCB 118 124 0.136 0.00003 3.72e-03 3.72e-032',3,4,4',5-PeCB 123 3.39 0.140 0.00003 1.02e-04 1.02e-043,3',4,4',5-PeCB 126 3.09 0.156 0.1 3.09e-01 3.09e-012,3,3',4,4',5-HxCB 156 156 + 157 C 93.7 0.0770 0.00003 2.81e-03 2.81e-032,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 27.3 0.0578 0.00003 8.19e-04 8.19e-043,3',4,4',5,5'-HxCB 169 ND 3.01 0.03 0.00e+00 4.52e-022,3,3',4,4',5,5'-HpCB 189 12.6 0.155 0.00003 3.78e-04 3.78e-04

TOTAL TEQ 0.319 0.364










Matrix: BLOOD Lab Sample I.D.: L11590-2 Li


Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_261A S: 1PB8B_269A S: 5

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 479 15.2 0.0001 4.79e-02 4.79e-023,4,4',5-TeCB 81 473 14.6 0.0003 1.42e-01 1.42e-012,3,3',4,4'-PeCB 105 6310 29.3 0.00003 1.89e-01 1.89e-012,3,4,4',5-PeCB 114 1770 28.5 0.00003 5.31e-02 5.31e-022,3',4,4',5-PeCB 118 26200 28.7 0.00003 7.86e-01 7.86e-012',3,4,4',5-PeCB 123 715 29.5 0.00003 2.15e-02 2.15e-023,3',4,4',5-PeCB 126 652 32.9 0.1 6.52e+01 6.52e+012,3,3',4,4',5-HxCB 156 156 + 157 C 19800 16.2 0.00003 5.94e-01 5.94e-012,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 5760 12.2 0.00003 1.73e-01 1.73e-013,3',4,4',5,5'-HxCB 169 ND 635 0.03 0.00e+00 9.53e+002,3,3',4,4',5,5'-HpCB 189 2660 32.7 0.00003 7.98e-02 7.98e-02

TOTAL TEQ 67.3 76.8









Project No. POP1406






Extract Volume (uL): 20 Sample Data Filename(s): PB8B_261A S: 2, PB8B_270B S: 3





CONC.FOUND









Total Nonachloro Biphenyls ND


TOTAL PCBs 750









Project No. POP1406











CONC.FOUND











TOTAL PCBs 210000












Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_261A S: 2PB8B_270B S: 3

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 1.10 0.110 0.0001 1.10e-04 1.10e-043,4,4',5-TeCB 81 1.00 0.105 0.0003 3.00e-04 3.00e-042,3,3',4,4'-PeCB 105 8.12 0.0986 0.00003 2.44e-04 2.44e-042,3,4,4',5-PeCB 114 2.39 0.0924 0.00003 7.17e-05 7.17e-052,3',4,4',5-PeCB 118 28.4 0.0966 0.00003 8.52e-04 8.52e-042',3,4,4',5-PeCB 123 0.987 0.101 0.00003 2.96e-05 2.96e-053,3',4,4',5-PeCB 126 1.21 0.108 0.1 1.21e-01 1.21e-012,3,3',4,4',5-HxCB 156 156 + 157 C 20.4 0.0799 0.00003 6.12e-04 6.12e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 5.68 0.0600 0.00003 1.70e-04 1.70e-043,3',4,4',5,5'-HxCB 169 ND 0.996 0.03 0.00e+00 1.49e-022,3,3',4,4',5,5'-HpCB 189 3.03 0.0493 0.00003 9.09e-05 9.09e-05

TOTAL TEQ 0.123 0.138












Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_261A S: 2PB8B_270B S: 3

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 34.6 38.8









Project No. POP1406











CONC.FOUND










Decachloro Biphenyl ND

TOTAL PCBs 773









Project No. POP1406











CONC.FOUND











TOTAL PCBs 245000












Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_261A S: 3PB8B_270B S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 0.657 0.657












Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_261A S: 3PB8B_270B S: 4

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 209 209









Project No. POP1406






Extract Volume (uL): 20 Sample Data Filename(s): PB8B_262 S: 4, PB8B_270B S: 5





CONC.FOUND











TOTAL PCBs 264









Project No. POP1406











CONC.FOUND











TOTAL PCBs 63400












Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_262 S: 4PB8B_270B S: 5

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 0.280 0.280












Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_262 S: 4PB8B_270B S: 5

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 67.4 67.4









Project No. POP1406











CONC.FOUND











TOTAL PCBs 358









Project No. POP1406











CONC.FOUND











TOTAL PCBs 99300













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 1.61 0.0606 0.0001 1.61e-04 1.61e-043,4,4',5-TeCB 81 1.51 0.0595 0.0003 4.53e-04 4.53e-042,3,3',4,4'-PeCB 105 5.48 0.0530 0.00003 1.64e-04 1.64e-042,3,4,4',5-PeCB 114 1.80 0.0494 0.00003 5.40e-05 5.40e-052,3',4,4',5-PeCB 118 13.5 0.0498 0.00003 4.05e-04 4.05e-042',3,4,4',5-PeCB 123 1.47 0.0507 0.00003 4.41e-05 4.41e-053,3',4,4',5-PeCB 126 1.83 0.0597 0.1 1.83e-01 1.83e-012,3,3',4,4',5-HxCB 156 156 + 157 C 8.80 0.0341 0.00003 2.64e-04 2.64e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 2.91 0.0268 0.00003 8.73e-05 8.73e-053,3',4,4',5,5'-HxCB 169 ND 1.43 0.03 0.00e+00 2.15e-022,3,3',4,4',5,5'-HpCB 189 2.01 0.0567 0.00003 6.03e-05 6.03e-05

TOTAL TEQ 0.185 0.206













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 51.2 57.1









Project No. POP1406











CONC.FOUND











TOTAL PCBs 168









Project No. POP1406











CONC.FOUND











TOTAL PCBs 49800













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 0.0783 0.0001 0.00e+00 3.92e-063,4,4',5-TeCB 81 ND 0.0702 0.0003 0.00e+00 1.05e-052,3,3',4,4'-PeCB 105 2.64 0.0605 0.00003 7.92e-05 7.92e-052,3,4,4',5-PeCB 114 0.400 0.0559 0.00003 1.20e-05 1.20e-052,3',4,4',5-PeCB 118 8.25 0.0563 0.00003 2.48e-04 2.48e-042',3,4,4',5-PeCB 123 0.133 0.0555 0.00003 3.99e-06 3.99e-063,3',4,4',5-PeCB 126 ND 0.0691 0.1 0.00e+00 3.46e-032,3,3',4,4',5-HxCB 156 156 + 157 C 3.35 0.0196 0.00003 1.01e-04 1.01e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 1.12 0.0149 0.00003 3.36e-05 3.36e-053,3',4,4',5,5'-HxCB 169 ND 0.110 0.03 0.00e+00 1.65e-032,3,3',4,4',5,5'-HpCB 189 ND 0.0591 0.00003 0.00e+00 8.87e-07

TOTAL TEQ 0.000477 0.00560













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 23.2 0.0001 0.00e+00 1.16e-033,4,4',5-TeCB 81 ND 20.8 0.0003 0.00e+00 3.12e-032,3,3',4,4'-PeCB 105 783 18.0 0.00003 2.35e-02 2.35e-022,3,4,4',5-PeCB 114 119 16.6 0.00003 3.57e-03 3.57e-032,3',4,4',5-PeCB 118 2450 16.7 0.00003 7.35e-02 7.35e-022',3,4,4',5-PeCB 123 39.5 16.5 0.00003 1.19e-03 1.19e-033,3',4,4',5-PeCB 126 ND 20.5 0.1 0.00e+00 1.03e+002,3,3',4,4',5-HxCB 156 156 + 157 C 994 5.82 0.00003 2.98e-02 2.98e-022,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 332 4.42 0.00003 9.96e-03 9.96e-033,3',4,4',5,5'-HxCB 169 ND 32.6 0.03 0.00e+00 4.89e-012,3,3',4,4',5,5'-HpCB 189 ND 17.5 0.00003 0.00e+00 2.63e-04

TOTAL TEQ 0.142 1.66









Project No. POP1406











CONC.FOUND











TOTAL PCBs 319









Project No. POP1406











CONC.FOUND











TOTAL PCBs 90200













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 0.0653 0.0001 0.00e+00 3.27e-063,4,4',5-TeCB 81 ND 0.0623 0.0003 0.00e+00 9.35e-062,3,3',4,4'-PeCB 105 4.60 0.0624 0.00003 1.38e-04 1.38e-042,3,4,4',5-PeCB 114 0.822 0.0588 0.00003 2.47e-05 2.47e-052,3',4,4',5-PeCB 118 17.2 0.0598 0.00003 5.16e-04 5.16e-042',3,4,4',5-PeCB 123 ND 0.0595 0.00003 0.00e+00 8.93e-073,3',4,4',5-PeCB 126 ND 0.0739 0.1 0.00e+00 3.70e-032,3,3',4,4',5-HxCB 156 156 + 157 C 8.79 0.0500 0.00003 2.64e-04 2.64e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 3.02 0.0377 0.00003 9.06e-05 9.06e-053,3',4,4',5,5'-HxCB 169 ND 0.195 0.03 0.00e+00 2.93e-032,3,3',4,4',5,5'-HpCB 189 1.07 0.0482 0.00003 3.21e-05 3.21e-05

TOTAL TEQ 0.00107 0.00770













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 18.5 0.0001 0.00e+00 9.25e-043,4,4',5-TeCB 81 ND 17.6 0.0003 0.00e+00 2.64e-032,3,3',4,4'-PeCB 105 1300 17.7 0.00003 3.90e-02 3.90e-022,3,4,4',5-PeCB 114 233 16.7 0.00003 6.99e-03 6.99e-032,3',4,4',5-PeCB 118 4870 16.9 0.00003 1.46e-01 1.46e-012',3,4,4',5-PeCB 123 ND 16.9 0.00003 0.00e+00 2.54e-043,3',4,4',5-PeCB 126 ND 20.9 0.1 0.00e+00 1.05e+002,3,3',4,4',5-HxCB 156 156 + 157 C 2490 14.2 0.00003 7.47e-02 7.47e-022,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 855 10.7 0.00003 2.57e-02 2.57e-023,3',4,4',5,5'-HxCB 169 ND 55.2 0.03 0.00e+00 8.28e-012,3,3',4,4',5,5'-HpCB 189 303 13.7 0.00003 9.09e-03 9.09e-03










Project No. POP1406











CONC.FOUND











TOTAL PCBs 700









Project No. POP1406











CONC.FOUND











TOTAL PCBs 200000













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 0.0694 0.0001 0.00e+00 3.47e-063,4,4',5-TeCB 81 ND 0.0618 0.0003 0.00e+00 9.27e-062,3,3',4,4'-PeCB 105 6.33 0.0980 0.00003 1.90e-04 1.90e-042,3,4,4',5-PeCB 114 2.34 0.0900 0.00003 7.02e-05 7.02e-052,3',4,4',5-PeCB 118 27.8 0.0936 0.00003 8.34e-04 8.34e-042',3,4,4',5-PeCB 123 0.321 0.0940 0.00003 9.63e-06 9.63e-063,3',4,4',5-PeCB 126 ND 0.114 0.1 0.00e+00 5.70e-032,3,3',4,4',5-HxCB 156 156 + 157 C 25.4 0.0161 0.00003 7.62e-04 7.62e-042,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 6.55 0.0125 0.00003 1.97e-04 1.97e-043,3',4,4',5,5'-HxCB 169 ND 0.301 0.03 0.00e+00 4.52e-032,3,3',4,4',5,5'-HpCB 189 2.64 0.0721 0.00003 7.92e-05 7.92e-05

TOTAL TEQ 0.00214 0.0124













TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 19.9 0.0001 0.00e+00 9.95e-043,4,4',5-TeCB 81 ND 17.7 0.0003 0.00e+00 2.66e-032,3,3',4,4'-PeCB 105 1810 28.1 0.00003 5.43e-02 5.43e-022,3,4,4',5-PeCB 114 670 25.8 0.00003 2.01e-02 2.01e-022,3',4,4',5-PeCB 118 7960 26.8 0.00003 2.39e-01 2.39e-012',3,4,4',5-PeCB 123 92.0 26.9 0.00003 2.76e-03 2.76e-033,3',4,4',5-PeCB 126 ND 32.7 0.1 0.00e+00 1.64e+002,3,3',4,4',5-HxCB 156 156 + 157 C 7280 4.61 0.00003 2.18e-01 2.18e-012,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 1880 3.58 0.00003 5.64e-02 5.64e-023,3',4,4',5,5'-HxCB 169 ND 86.2 0.03 0.00e+00 1.29e+002,3,3',4,4',5,5'-HpCB 189 756 20.7 0.00003 2.27e-02 2.27e-02










Project No. POP1406





Analysis Date: 30-Sep-2008 Time: 06:57:29 GC Column ID: SPB OCTYL


Injection Volume (uL): 1.0 Blank Data Filename: PB8B_253A S: 5




CONC.FOUND











TOTAL PCBs 1050









Project No. POP1406











CONC.FOUND











TOTAL PCBs 272000










Matrix: BLOOD Lab Sample I.D.: L11590-10


Concentration Units: pg/g (wet weight basis) Sample Data Filename(s): PB8B_254 S: 9

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 0.682 0.682










Matrix: BLOOD Lab Sample I.D.: L11590-10


Concentration Units: pg/g (lipid weight basis) Sample Data Filename(s): PB8B_254 S: 9

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF



TOTAL TEQ 176 176




For Axys Internal Use Only [ XSL Template: .xsl; Created: 28-Oct-2008 07:16:20; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_WG26343-101_Form1AHT_SJ910826.html; Workgroup: WG26343; Design ID: 925 ]





Project No. N/A

Contract No.: 2607 Lab Sample I.D.: WG26343-101 L

Matrix: BLOOD Sample Size: 40.0 g

Sample Receipt Date: N/A Initial Calibration Date: 30-Jul-2008








CONC.FOUND











TOTAL PCBs 3.86

Page 1 of 1 (WG26343 - 1668_PCB1668_HomTotals-TEQs_WG26343-101_Form1AHT_SJ910826.html)



For Axys Internal Use Only [ XSL Template: 1668TEQ.xsl; Created: 15-Oct-2008 10:22:59; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_HomTotals-TEQs_WG26343-101_TEQ_SJ910826.html; Workgroup: WG26343; Design ID: 925 ]


AXYS METHOD MLA-010 Rev 09 CLIENT SAMPLE NO.Lab BlankForm 1C




Matrix: BLOOD Lab Sample I.D.: WG26343-101 L

Sample Size: 40.0 g GC Column ID(s): SPB OCTYL

Concentration Units: pg/g Sample Data Filename(s): PB8B_261 S: 5

TEQCOMPOUND IUPAC

NO.COELUTIONS LAB

FLAG 1CONC.FOUND

DETECTIONLIMIT

WHO 2005TEF


3,3',4,4'-TeCB 77 ND 0.0326 0.0001 0.00e+00 1.63e-063,4,4',5-TeCB 81 ND 0.0336 0.0003 0.00e+00 5.04e-062,3,3',4,4'-PeCB 105 ND 0.0149 0.00003 0.00e+00 2.24e-072,3,4,4',5-PeCB 114 ND 0.0137 0.00003 0.00e+00 2.06e-072,3',4,4',5-PeCB 118 ND 0.0145 0.00003 0.00e+00 2.18e-072',3,4,4',5-PeCB 123 ND 0.0153 0.00003 0.00e+00 2.30e-073,3',4,4',5-PeCB 126 ND 0.0170 0.1 0.00e+00 8.50e-042,3,3',4,4',5-HxCB 156 156 + 157 C 0.069 0.0125 0.00003 2.07e-06 2.07e-062,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 0.022 0.0125 0.00003 6.60e-07 6.60e-073,3',4,4',5,5'-HxCB 169 ND 0.0261 0.03 0.00e+00 3.92e-042,3,3',4,4',5,5'-HpCB 189 0.026 0.0125 0.00003 7.80e-07 7.80e-07

TOTAL TEQ 0.000004 0.00125

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Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 0.913 0.0230 2.97 1.0013-MoCB 2 ND 0.02374-MoCB 3 1.20 0.0261 3.09 1.001

2,2'-DiCB 4 0.959 0.0847 1.59 1.0022,3-DiCB 5 ND 0.05282,3'-DiCB 6 ND 0.04892,4-DiCB 7 ND 0.05012,4'-DiCB 8 1.18 0.0449 1.59 1.2092,5-DiCB 9 ND 0.04882,6-DiCB 10 ND 0.05093,3'-DiCB 11 0.596 0.0477 1.65 0.9693,4-DiCB 12 12 + 13 C ND 0.04753,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.04754,4'-DiCB 15 1.34 0.0495 1.59 1.001

2,2',3-TriCB 16 0.066 0.0235 0.98 1.1672,2',4-TriCB 17 NDR 0.045 0.0218 0.87 1.1402,2',5-TriCB 18 18 + 30 C 0.976 0.0189 1.16 1.1142,2',6-TriCB 19 1.07 0.0241 1.08 1.0022,3,3'-TriCB 20 20 + 28 C 4.06 0.0208 1.05 0.8472,3,4-TriCB 21 21 + 33 C 0.166 0.0200 1.03 0.8572,3,4'-TriCB 22 NDR 0.075 0.0228 0.70 0.8712,3,5-TriCB 23 1.03 0.0225 1.11 1.2832,3,6-TriCB 24 ND 0.01722,3',4-TriCB 25 ND 0.01932,3',5-TriCB 26 26 + 29 C NDR 0.059 0.0215 1.25 1.3022,3',6-TriCB 27 ND 0.01542,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1.51 0.0199 1.03 0.8362,4',6-TriCB 32 NDR 0.049 0.0216 1.37 1.1992',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 1.06 0.0223 1.02 1.2743,3',4-TriCB 35 ND 0.01903,3',5-TriCB 36 ND 0.01903,4,4'-TriCB 37 1.67 0.0224 1.06 1.0013,4,5-TriCB 38 ND 0.0191

Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_261S6_SJ910828.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.01992,2',3,3'-TeCB 40 40 + 41 + 71 C 1.12 0.0163 0.74 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 0.054 0.0167 1.40 1.3122,2',3,5-TeCB 43 0.020 0.0193 0.85 1.2452,2',3,5'-TeCB 44 44 + 47 + 65 C 1.75 0.0153 0.80 1.2852,2',3,6-TeCB 45 45 + 51 C ND 0.01792,2',3,6'-TeCB 46 ND 0.02022,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 0.031 0.0169 2.07 1.2732,2',4,5'-TeCB 49 49 + 69 C 1.06 0.0146 0.77 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 0.056 0.0177 0.63 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 1.72 0.0162 0.76 1.2332,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1.16 0.0128 0.84 1.0012,3,3',4-TeCB 55 ND 0.05262,3,3',4'-TeCB 56 1.31 0.0524 0.86 0.9052,3,3',5-TeCB 57 ND 0.05202,3,3',5'-TeCB 58 ND 0.05342,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.090 0.0127 0.98 1.3022,3,4,4'-TeCB 60 1.01 0.0522 0.87 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 12.0 0.0506 0.79 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 0.090 0.0502 0.83 0.8652,3,4',6-TeCB 64 0.127 0.0122 0.76 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 4.07 0.0493 0.81 0.8852,3',4,5-TeCB 67 ND 0.04752,3',4,5'-TeCB 68 NDR 0.080 0.0514 0.41 0.8322,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.05122,3',5',6-TeCB 73 ND 0.01342,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 1.69 0.0580 0.79 1.0003,3',4,5-TeCB 78 ND 0.04843,3',4,5'-TeCB 79 ND 0.04073,3',5,5'-TeCB 80 ND 0.04623,4,4',5-TeCB 81 1.69 0.0556 0.78 1.001

2,2',3,3',4-PeCB 82 NDR 0.073 0.0162 1.06 0.9332,2',3,3',5-PeCB 83 83 + 99 C 39.7 0.0153 1.56 0.8862,2',3,3',6-PeCB 84 NDR 0.091 0.0172 3.04 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 2.17 0.0125 1.50 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1.61 0.0130 1.52 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.01562,2',3,4,6'-PeCB 89 ND 0.01592,2',3,4',5-PeCB 90 90 + 101 + 113 C 3.18 0.0133 1.61 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 0.805 0.0155 1.63 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 2.59 0.0153 1.58 1.1202,2',3,5,6'-PeCB 94 ND 0.01732,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01222,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.01482,2',4,6,6'-PeCB 104 0.827 0.0122 1.58 1.0012,3,3',4,4'-PeCB 105 25.1 0.195 1.56 1.0002,3,3',4,5-PeCB 106 ND 0.1672,3,3',4',5-PeCB 107 107 + 124 C ND 0.1822,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 1.26 0.157 1.69 0.9972,3,3',4',6-PeCB 110 110 + 115 C 4.03 0.0122 1.58 0.9262,3,3',5,5'-PeCB 111 0.046 0.0122 1.68 0.9462,3,3',5,6-PeCB 112 ND 0.01222,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 4.26 0.182 1.46 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 93.0 0.182 1.58 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 0.080 0.0122 2.03 0.9592,3',4,5',6-PeCB 121 NDR 0.027 0.0122 1.04 1.2002',3,3',4,5-PeCB 122 ND 0.1882',3,4,4',5-PeCB 123 2.31 0.188 1.39 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 1.89 0.211 1.50 1.0003,3',4,5,5'-PeCB 127 ND 0.165

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 0.566 0.0122 1.19 1.0002,3,3',4,4',5-HxCB 156 156 + 157 C 33.3 0.0492 1.28 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128


(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration; C = co-eluting congener; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_261S6_SJ910828.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 11.4 0.0385 1.29 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X

2,2',3,3',4,4',5-HpCB 170 X2,2',3,3',4,4',6-HpCB 171 171 + 173 C X2,2',3,3',4,5,5'-HpCB 172 X2,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 X2,2',3,3',4,5',6-HpCB 175 X2,2',3,3',4,6,6'-HpCB 176 X2,2',3,3',4',5,6-HpCB 177 X2,2',3,3',5,5',6-HpCB 178 X2,2',3,3',5,6,6'-HpCB 179 X2,2',3,4,4',5,5'-HpCB 180 180 + 193 C X2,2',3,4,4',5,6-HpCB 181 X2,2',3,4,4',5,6'-HpCB 182 X2,2',3,4,4',5',6-HpCB 183 183 + 185 C X2,2',3,4,4',6,6'-HpCB 184 X2,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 X2,2',3,4',5,5',6-HpCB 187 X2,2',3,4',5,6,6'-HpCB 188 X2,3,3',4,4',5,5'-HpCB 189 X2,3,3',4,4',5,6-HpCB 190 X2,3,3',4,4',5',6-HpCB 191 X2,3,3',4,5,5',6-HpCB 192 X2,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 X2,2',3,3',4,4',5,6-OcCB 195 X2,2',3,3',4,4',5,6'-OcCB 196 X2,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C X2,2',3,3',4,5,5',6-OcCB 198 198 + 199 C X2,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 X2,2',3,3',5,5',6,6'-OcCB 202 X2,2',3,4,4',5,5',6-OcCB 203 X2,2',3,4,4',5,6,6'-OcCB 204 X2,3,3',4,4',5,5',6-OcCB 205 X

2,2',3,3',4,4',5,5',6-NoCB 206 X2,2',3,3',4,4',5,6,6'-NoCB 207 X2,2',3,3',4,5,5',6,6'-NoCB 208 X

2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 231 5.82 2.97 1.0013-MoCB 2 ND 6.004-MoCB 3 304 6.61 3.09 1.001

2,2'-DiCB 4 243 21.4 1.59 1.0022,3-DiCB 5 ND 13.42,3'-DiCB 6 ND 12.42,4-DiCB 7 ND 12.72,4'-DiCB 8 299 11.4 1.59 1.2092,5-DiCB 9 ND 12.42,6-DiCB 10 ND 12.93,3'-DiCB 11 151 12.1 1.65 0.9693,4-DiCB 12 12 + 13 C ND 12.03,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 12.04,4'-DiCB 15 339 12.5 1.59 1.001

2,2',3-TriCB 16 16.7 5.95 0.98 1.1672,2',4-TriCB 17 NDR 11.4 5.52 0.87 1.1402,2',5-TriCB 18 18 + 30 C 247 4.79 1.16 1.1142,2',6-TriCB 19 271 6.10 1.08 1.0022,3,3'-TriCB 20 20 + 28 C 1030 5.27 1.05 0.8472,3,4-TriCB 21 21 + 33 C 42.0 5.06 1.03 0.8572,3,4'-TriCB 22 NDR 19.0 5.77 0.70 0.8712,3,5-TriCB 23 261 5.70 1.11 1.2832,3,6-TriCB 24 ND 4.362,3',4-TriCB 25 ND 4.892,3',5-TriCB 26 26 + 29 C NDR 14.9 5.44 1.25 1.3022,3',6-TriCB 27 ND 3.902,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 382 5.04 1.03 0.8362,4',6-TriCB 32 NDR 12.4 5.47 1.37 1.1992',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 268 5.65 1.02 1.2743,3',4-TriCB 35 ND 4.813,3',5-TriCB 36 ND 4.813,4,4'-TriCB 37 423 5.67 1.06 1.0013,4,5-TriCB 38 ND 4.84

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COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 5.042,2',3,3'-TeCB 40 40 + 41 + 71 C 284 4.13 0.74 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 13.7 4.23 1.40 1.3122,2',3,5-TeCB 43 5.06 4.89 0.85 1.2452,2',3,5'-TeCB 44 44 + 47 + 65 C 443 3.87 0.80 1.2852,2',3,6-TeCB 45 45 + 51 C ND 4.532,2',3,6'-TeCB 46 ND 5.122,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 7.85 4.28 2.07 1.2732,2',4,5'-TeCB 49 49 + 69 C 268 3.70 0.77 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 14.2 4.48 0.63 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 436 4.10 0.76 1.2332,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 294 3.24 0.84 1.0012,3,3',4-TeCB 55 ND 13.32,3,3',4'-TeCB 56 332 13.3 0.86 0.9052,3,3',5-TeCB 57 ND 13.22,3,3',5'-TeCB 58 ND 13.52,3,3',6-TeCB 59 59 + 62 + 75 C NDR 22.8 3.22 0.98 1.3022,3,4,4'-TeCB 60 256 13.2 0.87 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 3040 12.8 0.79 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 22.8 12.7 0.83 0.8652,3,4',6-TeCB 64 32.2 3.09 0.76 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 1030 12.5 0.81 0.8852,3',4,5-TeCB 67 ND 12.02,3',4,5'-TeCB 68 NDR 20.3 13.0 0.41 0.8322,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 13.02,3',5',6-TeCB 73 ND 3.392,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 428 14.7 0.79 1.0003,3',4,5-TeCB 78 ND 12.33,3',4,5'-TeCB 79 ND 10.33,3',5,5'-TeCB 80 ND 11.73,4,4',5-TeCB 81 428 14.1 0.78 1.001

2,2',3,3',4-PeCB 82 NDR 18.5 4.10 1.06 0.9332,2',3,3',5-PeCB 83 83 + 99 C 10100 3.87 1.56 0.8862,2',3,3',6-PeCB 84 NDR 23.0 4.36 3.04 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 550 3.17 1.50 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 408 3.29 1.52 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 3.952,2',3,4,6'-PeCB 89 ND 4.032,2',3,4',5-PeCB 90 90 + 101 + 113 C 805 3.37 1.61 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 204 3.93 1.63 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 656 3.87 1.58 1.1202,2',3,5,6'-PeCB 94 ND 4.382,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 3.092,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 3.752,2',4,6,6'-PeCB 104 209 3.09 1.58 1.0012,3,3',4,4'-PeCB 105 6360 49.4 1.56 1.0002,3,3',4,5-PeCB 106 ND 42.32,3,3',4',5-PeCB 107 107 + 124 C ND 46.12,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 319 39.8 1.69 0.9972,3,3',4',6-PeCB 110 110 + 115 C 1020 3.09 1.58 0.9262,3,3',5,5'-PeCB 111 11.6 3.09 1.68 0.9462,3,3',5,6-PeCB 112 ND 3.092,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 1080 46.1 1.46 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 23600 46.1 1.58 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 20.3 3.09 2.03 0.9592,3',4,5',6-PeCB 121 NDR 6.84 3.09 1.04 1.2002',3,3',4,5-PeCB 122 ND 47.62',3,4,4',5-PeCB 123 585 47.6 1.39 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 479 53.4 1.50 1.0003,3',4,5,5'-PeCB 127 ND 41.8

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 143 3.09 1.19 1.0002,3,3',4,4',5-HxCB 156 156 + 157 C 8430 12.5 1.28 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128




For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_261S6_SJ910828_Lipid.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 2890 9.75 1.29 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406

Contract No.: 2607 Lab Sample I.D.: L11590-1 LW





Extract Volume (uL): 200 Sample Data Filename: PB8B_269A S: 4




COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 X3-MoCB 2 X4-MoCB 3 X

2,2'-DiCB 4 X2,3-DiCB 5 X2,3'-DiCB 6 X2,4-DiCB 7 X2,4'-DiCB 8 X2,5-DiCB 9 X2,6-DiCB 10 X3,3'-DiCB 11 X3,4-DiCB 12 12 + 13 C X3,4'-DiCB 13 12 + 13 C123,5-DiCB 14 X4,4'-DiCB 15 X

2,2',3-TriCB 16 X2,2',4-TriCB 17 X2,2',5-TriCB 18 18 + 30 C X2,2',6-TriCB 19 X2,3,3'-TriCB 20 20 + 28 C X2,3,4-TriCB 21 21 + 33 C X2,3,4'-TriCB 22 X2,3,5-TriCB 23 X2,3,6-TriCB 24 X2,3',4-TriCB 25 X2,3',5-TriCB 26 26 + 29 C X2,3',6-TriCB 27 X2,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 X2,4',6-TriCB 32 X2',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 X3,3',4-TriCB 35 X3,3',5-TriCB 36 X3,4,4'-TriCB 37 X3,4,5-TriCB 38 X

Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_269AS4_SJ912363.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 X2,2',3,3'-TeCB 40 40 + 41 + 71 C X2,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 X2,2',3,5-TeCB 43 X2,2',3,5'-TeCB 44 44 + 47 + 65 C X2,2',3,6-TeCB 45 45 + 51 C X2,2',3,6'-TeCB 46 X2,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 X2,2',4,5'-TeCB 49 49 + 69 C X2,2',4,6-TeCB 50 50 + 53 C X2,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 X2,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 X2,3,3',4-TeCB 55 X2,3,3',4'-TeCB 56 X2,3,3',5-TeCB 57 X2,3,3',5'-TeCB 58 X2,3,3',6-TeCB 59 59 + 62 + 75 C X2,3,4,4'-TeCB 60 X2,3,4,5-TeCB 61 61 + 70 + 74 + 76 C X2,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 X2,3,4',6-TeCB 64 X2,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 X2,3',4,5-TeCB 67 X2,3',4,5'-TeCB 68 X2,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 X2,3',5',6-TeCB 73 X2,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 X3,3',4,5-TeCB 78 X3,3',4,5'-TeCB 79 X3,3',5,5'-TeCB 80 X3,4,4',5-TeCB 81 X

2,2',3,3',4-PeCB 82 X2,2',3,3',5-PeCB 83 83 + 99 C X2,2',3,3',6-PeCB 84 X2,2',3,4,4'-PeCB 85 85 + 116 + 117 C X2,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C X2,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C X2,2',3,4,6'-PeCB 89 X2,2',3,4',5-PeCB 90 90 + 101 + 113 C X2,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 X2,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C X2,2',3,5,6'-PeCB 94 X2,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 X2,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 X2,2',4,6,6'-PeCB 104 X2,3,3',4,4'-PeCB 105 X2,3,3',4,5-PeCB 106 X2,3,3',4',5-PeCB 107 107 + 124 C X2,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 X2,3,3',4',6-PeCB 110 110 + 115 C X2,3,3',5,5'-PeCB 111 X2,3,3',5,6-PeCB 112 X2,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 X2,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 X2,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 X2,3',4,5',6-PeCB 121 X2',3,3',4,5-PeCB 122 X2',3,4,4',5-PeCB 123 X2',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 X3,3',4,5,5'-PeCB 127 X

2,2',3,3',4,4'-HxCB 128 128 + 166 C D 7.66 0.0970 1.38 0.9592,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 136 0.0913 1.27 0.9282,2',3,3',4,5'-HxCB 130 D 3.45 0.115 1.16 0.9132,2',3,3',4,6-HxCB 131 ND D 0.1062,2',3,3',4,6'-HxCB 132 NDR D 1.37 0.114 0.99 1.1752,2',3,3',5,5'-HxCB 133 D 1.96 0.103 1.17 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.1082,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 3.77 0.0703 1.24 1.1032,2',3,3',6,6'-HxCB 136 NDR D 0.185 0.0520 0.97 1.0242,2',3,4,4',5-HxCB 137 D 7.58 0.109 1.20 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C D 0.972 0.0993 1.30 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 D 1.60 0.105 1.36 0.9042,2',3,4,5,6-HxCB 142 ND D 0.1072,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 0.07302,2',3,4,6,6'-HxCB 145 ND D 0.05512,2',3,4',5,5'-HxCB 146 D 16.3 0.0940 1.32 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 3.75 0.0993 1.21 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.07242,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.05482,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.04852,2',4,4',5,5'-HxCB 153 153 + 168 C D 148 0.0831 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 7.48 0.0728 1.29 0.9382,3,3',4,5,5'-HxCB 159 ND D 0.07732,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.07992,3,3',4',5,5'-HxCB 162 NDR D 0.184 0.0801 3.16 0.9892,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR D 0.474 0.0802 1.01 0.9222,3,3',5,5',6-HxCB 165 ND D 0.08882,3,4,4',5,6-HxCB 166 128 + 166 C128


(1) Where applicable, custom lab flags have been used on this report; ND = not detected; NDR = peak detected but did not meet quantification criteria,result reported represents the estimated maximum possible concentration; D = dilution data; C = co-eluting congener; X = result reported separately.


For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_269AS4_SJ912363.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 D 1.41 0.0588 1.21 1.000

2,2',3,3',4,4',5-HpCB 170 D 35.9 0.0548 1.07 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 3.47 0.0615 1.13 1.1632,2',3,3',4,5,5'-HpCB 172 D 3.75 0.0600 0.92 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 1.58 0.0590 1.17 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 0.599 0.0590 1.34 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 0.04552,2',3,3',4',5,6-HpCB 177 D 6.37 0.0544 1.06 1.1452,2',3,3',5,5',6-HpCB 178 D 3.78 0.0581 0.90 1.0852,2',3,3',5,6,6'-HpCB 179 D 0.546 0.0430 1.03 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 67.4 0.0452 1.08 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.178 0.0570 2.02 1.1572,2',3,4,4',5,6'-HpCB 182 NDR D 0.651 0.0558 0.61 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 11.8 0.0575 1.05 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 0.04362,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.04652,2',3,4',5,5',6-HpCB 187 D 24.8 0.0582 1.06 1.1102,2',3,4',5,6,6'-HpCB 188 D 0.684 0.0447 1.14 1.0012,3,3',4,4',5,5'-HpCB 189 D 3.30 0.0894 1.00 1.0002,3,3',4,4',5,6-HpCB 190 D 8.36 0.0411 1.04 0.9472,3,3',4,4',5',6-HpCB 191 D 1.56 0.0438 1.10 0.9172,3,3',4,5,5',6-HpCB 192 ND D 0.04902,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 14.0 0.0417 0.89 0.9912,2',3,3',4,4',5,6-OcCB 195 D 4.36 0.0495 0.80 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 7.42 0.0772 0.91 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.06782,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 17.0 0.0803 0.97 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.406 0.0668 1.55 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 2.75 0.0735 0.93 1.0002,2',3,4,4',5,5',6-OcCB 203 D 10.9 0.0737 0.84 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 0.06752,3,3',4,4',5,5',6-OcCB 205 D 1.42 0.0381 0.86 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 4.22 0.348 0.85 1.0012,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 0.499 0.317 0.98 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 D 1.93 0.272 0.88 1.001

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 1.53 0.0471 0.78 1.000





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT




Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_269AS4_SJ912363_Lipid.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C D 1940 24.6 1.38 0.9592,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 34400 23.1 1.27 0.9282,2',3,3',4,5'-HxCB 130 D 874 29.1 1.16 0.9132,2',3,3',4,6-HxCB 131 ND D 26.82,2',3,3',4,6'-HxCB 132 NDR D 347 28.9 0.99 1.1752,2',3,3',5,5'-HxCB 133 D 496 26.1 1.17 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 27.32,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 955 17.8 1.24 1.1032,2',3,3',6,6'-HxCB 136 NDR D 46.8 13.2 0.97 1.0242,2',3,4,4',5-HxCB 137 D 1920 27.6 1.20 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C D 246 25.1 1.30 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 D 405 26.6 1.36 0.9042,2',3,4,5,6-HxCB 142 ND D 27.12,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 18.52,2',3,4,6,6'-HxCB 145 ND D 14.02,2',3,4',5,5'-HxCB 146 D 4130 23.8 1.32 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 950 25.1 1.21 1.1332,2',3,4',5,6'-HxCB 148 ND D 18.32,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 13.92,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 12.32,2',4,4',5,5'-HxCB 153 153 + 168 C D 37500 21.0 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 1890 18.4 1.29 0.9382,3,3',4,5,5'-HxCB 159 ND D 19.62,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 20.22,3,3',4',5,5'-HxCB 162 NDR D 46.6 20.3 3.16 0.9892,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR D 120 20.3 1.01 0.9222,3,3',5,5',6-HxCB 165 ND D 22.52,3,4,4',5,6-HxCB 166 128 + 166 C128




For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form1A_PB8B_269AS4_SJ912363_Lipid.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 D 357 14.9 1.21 1.000

2,2',3,3',4,4',5-HpCB 170 D 9090 13.9 1.07 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 879 15.6 1.13 1.1632,2',3,3',4,5,5'-HpCB 172 D 950 15.2 0.92 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 400 14.9 1.17 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 152 14.9 1.34 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 11.52,2',3,3',4',5,6-HpCB 177 D 1610 13.8 1.06 1.1452,2',3,3',5,5',6-HpCB 178 D 957 14.7 0.90 1.0852,2',3,3',5,6,6'-HpCB 179 D 138 10.9 1.03 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 17100 11.4 1.08 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 45.1 14.4 2.02 1.1572,2',3,4,4',5,6'-HpCB 182 NDR D 165 14.1 0.61 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 2990 14.6 1.05 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 11.02,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 11.82,2',3,4',5,5',6-HpCB 187 D 6280 14.7 1.06 1.1102,2',3,4',5,6,6'-HpCB 188 D 173 11.3 1.14 1.0012,3,3',4,4',5,5'-HpCB 189 D 836 22.6 1.00 1.0002,3,3',4,4',5,6-HpCB 190 D 2120 10.4 1.04 0.9472,3,3',4,4',5',6-HpCB 191 D 395 11.1 1.10 0.9172,3,3',4,5,5',6-HpCB 192 ND D 12.42,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 3550 10.6 0.89 0.9912,2',3,3',4,4',5,6-OcCB 195 D 1100 12.5 0.80 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 1880 19.5 0.91 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 17.22,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 4300 20.3 0.97 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 103 16.9 1.55 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 696 18.6 0.93 1.0002,2',3,4,4',5,5',6-OcCB 203 D 2760 18.7 0.84 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 17.12,3,3',4,4',5,5',6-OcCB 205 D 360 9.65 0.86 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 1070 88.1 0.85 1.0012,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 126 80.3 0.98 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 D 489 68.9 0.88 1.001

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 387 11.9 0.78 1.000




For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form2_PB8B_261S6_SJ910828.html; Workgroup: WG26343; Design ID: 925 ]





Project No. POP1406









Concentration Units: pg absolute % Lipid: 0.39

LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 608 30.4 3.19 0.71813C12-4-MoCB 3L 2000 752 37.6 3.19 0.858

13C12-2,2'-DiCB 4L 2000 1000 50.1 1.67 0.87313C12-4,4'-DiCB 15L 2000 1560 77.8 1.64 1.255

13C12-2,2',6-TriCB 19L 2000 1340 66.8 1.06 1.07213C12-3,4,4'-TriCB 37L 2000 1560 77.9 1.07 1.091

13C12-2,2',6,6'-TeCB 54L 2000 1270 63.6 0.82 0.81113C12-3,3',4,4'-TeCB 77L 2000 1880 94.0 0.82 1.39613C12-3,4,4',5-TeCB 81L 2000 1890 94.6 0.83 1.372

13C12-2,2',4,6,6'-PeCB 104L 2000 1620 81.2 1.60 0.80813C12-2,3,3',4,4'-PeCB 105L 2000 1770 88.6 1.64 1.19913C12-2,3,4,4',5-PeCB 114L 2000 1850 92.3 1.63 1.17913C12-2,3',4,4',5-PeCB 118L 2000 1870 93.4 1.65 1.16213C12-2',3,4,4',5-PeCB 123L 2000 1880 93.9 1.62 1.15113C12-3,3',4,4',5-PeCB 126L 2000 1770 88.6 1.62 1.301

13C12-2,2',4,4',6,6'-HxCB 155L 2000 1760 88.1 1.21 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 4000 3470 86.8 1.23 1.10813C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 2000 1750 87.5 1.21 1.07813C12-3,3',4,4',5,5'-HxCB 169L X

13C12-2,2',3,3',4,4',5-HpCB 170L X13C12-2,2',3,4,4',5,5'-HpCB 180L X13C12-2,2',3,4',5,6,6'-HpCB 188L X13C12-2,3,3',4,4',5,5'-HpCB 189L X

13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1810 90.7 1.07 0.92413C12-2,3,3',5,5'-PeCB 111L 2000 1960 97.8 1.63 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X

Page 1 of 1 (WG26343 - 1668_PCB1668_PCBTF_L11590-1_Form2_PB8B_261S6_SJ910828.html)

(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; D = dilution data; C = co-eluting congener; X = result reported separately.(3) R% = percent recovery of labeled compounds.


For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-1_Form2_PB8B_269AS4_SJ912363.html; Workgroup: WG26343; Design ID: 925 ]





Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L X13C12-4-MoCB 3L X

13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X

13C12-2,2',6-TriCB 19L X13C12-3,4,4'-TriCB 37L X

13C12-2,2',6,6'-TeCB 54L X13C12-3,3',4,4'-TeCB 77L X13C12-3,4,4',5-TeCB 81L X

13C12-2,2',4,6,6'-PeCB 104L X13C12-2,3,3',4,4'-PeCB 105L X13C12-2,3,4,4',5-PeCB 114L X13C12-2,3',4,4',5-PeCB 118L X13C12-2',3,4,4',5-PeCB 123L X13C12-3,3',4,4',5-PeCB 126L X

13C12-2,2',4,4',6,6'-HxCB 155L D 2000 2040 102 1.17 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C D 4000 3500 87.4 1.23 1.10713C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L D 2000 1740 86.8 1.21 1.07813C12-3,3',4,4',5,5'-HxCB 169L D 2000 2720 136 1.27 1.191

13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 2010 100 1.12 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 1750 87.7 1.09 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1250 62.4 1.09 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 2150 108 1.03 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1270 63.6 0.94 0.81713C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1570 78.3 0.89 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 2060 103 0.75 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 2350 118 0.82 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 2020 101 1.25 1.074

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L X13C12-2,3,3',5,5'-PeCB 111L X

13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2300 115 0.99 1.012

Page 1 of 1 (WG26343 - 1668_PCB1668_PCBTF_L11590-1_Form2_PB8B_269AS4_SJ912363.html)




Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 1.41 0.0667 3.00 1.0003-MoCB 2 ND 0.06984-MoCB 3 1.47 0.0781 3.46 1.001


2,2',3-TriCB 16 ND 0.06902,2',4-TriCB 17 ND 0.06402,2',5-TriCB 18 18 + 30 C 1.48 0.0554 1.02 1.1142,2',6-TriCB 19 1.56 0.0697 1.00 1.0022,3,3'-TriCB 20 20 + 28 C 13.8 0.0503 1.07 0.8482,3,4-TriCB 21 21 + 33 C 0.160 0.0484 1.07 0.8572,3,4'-TriCB 22 NDR 0.087 0.0550 0.52 0.8732,3,5-TriCB 23 1.64 0.0543 1.00 1.2832,3,6-TriCB 24 ND 0.05042,3',4-TriCB 25 ND 0.04662,3',5-TriCB 26 26 + 29 C ND 0.05192,3',6-TriCB 27 ND 0.04502,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 2.20 0.0481 1.09 0.8372,4',6-TriCB 32 ND 0.05222',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 1.78 0.0539 1.03 1.2743,3',4-TriCB 35 ND 0.04583,3',5-TriCB 36 ND 0.04593,4,4'-TriCB 37 2.16 0.0531 1.07 1.0013,4,5-TriCB 38 ND 0.0461


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.04812,2',3,3'-TeCB 40 40 + 41 + 71 C 1.63 0.0388 0.76 1.3352,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 ND 0.03982,2',3,5-TeCB 43 ND 0.04602,2',3,5'-TeCB 44 44 + 47 + 65 C 3.62 0.0364 0.76 1.2852,2',3,6-TeCB 45 45 + 51 C NDR 0.083 0.0426 1.15 1.1492,2',3,6'-TeCB 46 ND 0.04802,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 0.048 0.0402 0.25 1.2732,2',4,5'-TeCB 49 49 + 69 C 1.90 0.0348 0.73 1.2592,2',4,6-TeCB 50 50 + 53 C ND 0.04202,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 3.17 0.0384 0.73 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1.69 0.0304 0.71 1.0012,3,3',4-TeCB 55 ND 0.06552,3,3',4'-TeCB 56 2.11 0.0653 0.80 0.9052,3,3',5-TeCB 57 ND 0.06472,3,3',5'-TeCB 58 ND 0.06652,3,3',6-TeCB 59 59 + 62 + 75 C 0.120 0.0301 0.70 1.3022,3,4,4'-TeCB 60 5.01 0.0650 0.83 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 50.5 0.0631 0.80 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 0.287 0.0625 0.98 0.8652,3,4',6-TeCB 64 NDR 0.254 0.0285 0.98 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 13.9 0.0614 0.78 0.8852,3',4,5-TeCB 67 ND 0.05922,3',4,5'-TeCB 68 0.404 0.0640 0.71 0.8322,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.06372,3',5',6-TeCB 73 ND 0.03202,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 2.27 0.0722 0.86 1.0003,3',4,5-TeCB 78 ND 0.06033,3',4,5'-TeCB 79 ND 0.05073,3',5,5'-TeCB 80 ND 0.05763,4,4',5-TeCB 81 2.24 0.0693 0.80 1.001

2,2',3,3',4-PeCB 82 ND 0.05432,2',3,3',5-PeCB 83 83 + 99 C 36.9 0.0515 1.59 0.8862,2',3,3',6-PeCB 84 0.094 0.0577 1.38 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 2.60 0.0422 1.61 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 2.18 0.0435 1.73 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C NDR 0.083 0.0524 0.94 1.1542,2',3,4,6'-PeCB 89 ND 0.05352,2',3,4',5-PeCB 90 90 + 101 + 113 C 6.57 0.0448 1.58 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 1.92 0.0520 1.60 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 3.21 0.0516 1.50 1.1202,2',3,5,6'-PeCB 94 ND 0.05822,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.02662,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.04962,2',4,6,6'-PeCB 104 1.31 0.0233 1.47 1.0012,3,3',4,4'-PeCB 105 29.9 0.139 1.59 1.0012,3,3',4,5-PeCB 106 ND 0.1232,3,3',4',5-PeCB 107 107 + 124 C ND 0.1332,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 2.16 0.115 1.60 0.9972,3,3',4',6-PeCB 110 110 + 115 C 4.11 0.0373 1.60 0.9252,3,3',5,5'-PeCB 111 0.176 0.0371 1.43 0.9452,3,3',5,6-PeCB 112 ND 0.03752,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 8.41 0.135 1.60 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 124 0.136 1.57 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 0.247 0.0354 1.71 0.9582,3',4,5',6-PeCB 121 NDR 0.043 0.0393 2.88 1.1992',3,3',4,5-PeCB 122 ND 0.1382',3,4,4',5-PeCB 123 3.39 0.140 1.55 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 3.09 0.156 1.54 1.0003,3',4,5,5'-PeCB 127 NDR 0.505 0.121 1.96 1.042







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 27.3 0.0578 1.26 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 297 14.1 3.00 1.0003-MoCB 2 ND 14.74-MoCB 3 310 16.5 3.46 1.001


2,2',3-TriCB 16 ND 14.62,2',4-TriCB 17 ND 13.52,2',5-TriCB 18 18 + 30 C 312 11.7 1.02 1.1142,2',6-TriCB 19 329 14.7 1.00 1.0022,3,3'-TriCB 20 20 + 28 C 2910 10.6 1.07 0.8482,3,4-TriCB 21 21 + 33 C 33.8 10.2 1.07 0.8572,3,4'-TriCB 22 NDR 18.4 11.6 0.52 0.8732,3,5-TriCB 23 346 11.5 1.00 1.2832,3,6-TriCB 24 ND 10.62,3',4-TriCB 25 ND 9.832,3',5-TriCB 26 26 + 29 C ND 10.92,3',6-TriCB 27 ND 9.492,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 464 10.1 1.09 0.8372,4',6-TriCB 32 ND 11.02',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 375 11.4 1.03 1.2743,3',4-TriCB 35 ND 9.663,3',5-TriCB 36 ND 9.683,4,4'-TriCB 37 456 11.2 1.07 1.0013,4,5-TriCB 38 ND 9.72


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 10.12,2',3,3'-TeCB 40 40 + 41 + 71 C 344 8.18 0.76 1.3352,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 ND 8.402,2',3,5-TeCB 43 ND 9.702,2',3,5'-TeCB 44 44 + 47 + 65 C 764 7.68 0.76 1.2852,2',3,6-TeCB 45 45 + 51 C NDR 17.5 8.99 1.15 1.1492,2',3,6'-TeCB 46 ND 10.12,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 10.1 8.48 0.25 1.2732,2',4,5'-TeCB 49 49 + 69 C 401 7.34 0.73 1.2592,2',4,6-TeCB 50 50 + 53 C ND 8.862,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 669 8.10 0.73 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 357 6.41 0.71 1.0012,3,3',4-TeCB 55 ND 13.82,3,3',4'-TeCB 56 445 13.8 0.80 0.9052,3,3',5-TeCB 57 ND 13.62,3,3',5'-TeCB 58 ND 14.02,3,3',6-TeCB 59 59 + 62 + 75 C 25.3 6.35 0.70 1.3022,3,4,4'-TeCB 60 1060 13.7 0.83 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 10700 13.3 0.80 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 60.5 13.2 0.98 0.8652,3,4',6-TeCB 64 NDR 53.6 6.01 0.98 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 2930 13.0 0.78 0.8852,3',4,5-TeCB 67 ND 12.52,3',4,5'-TeCB 68 85.2 13.5 0.71 0.8322,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 13.42,3',5',6-TeCB 73 ND 6.752,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 479 15.2 0.86 1.0003,3',4,5-TeCB 78 ND 12.73,3',4,5'-TeCB 79 ND 10.73,3',5,5'-TeCB 80 ND 12.23,4,4',5-TeCB 81 473 14.6 0.80 1.001

2,2',3,3',4-PeCB 82 ND 11.52,2',3,3',5-PeCB 83 83 + 99 C 7780 10.9 1.59 0.8862,2',3,3',6-PeCB 84 19.8 12.2 1.38 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 548 8.90 1.61 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 460 9.18 1.73 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C NDR 17.5 11.1 0.94 1.1542,2',3,4,6'-PeCB 89 ND 11.32,2',3,4',5-PeCB 90 90 + 101 + 113 C 1390 9.45 1.58 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 405 11.0 1.60 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 677 10.9 1.50 1.1202,2',3,5,6'-PeCB 94 ND 12.32,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 5.612,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 10.52,2',4,6,6'-PeCB 104 276 4.92 1.47 1.0012,3,3',4,4'-PeCB 105 6310 29.3 1.59 1.0012,3,3',4,5-PeCB 106 ND 25.92,3,3',4',5-PeCB 107 107 + 124 C ND 28.12,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 456 24.3 1.60 0.9972,3,3',4',6-PeCB 110 110 + 115 C 867 7.87 1.60 0.9252,3,3',5,5'-PeCB 111 37.1 7.83 1.43 0.9452,3,3',5,6-PeCB 112 ND 7.912,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 1770 28.5 1.60 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 26200 28.7 1.57 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 52.1 7.47 1.71 0.9582,3',4,5',6-PeCB 121 NDR 9.07 8.29 2.88 1.1992',3,3',4,5-PeCB 122 ND 29.12',3,4,4',5-PeCB 123 715 29.5 1.55 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 652 32.9 1.54 1.0003,3',4,5,5'-PeCB 127 NDR 107 25.5 1.96 1.042







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 5760 12.2 1.26 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C D 5.77 0.103 1.21 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 376 0.0970 1.29 0.9282,2',3,3',4,5'-HxCB 130 D 11.1 0.122 1.17 0.9132,2',3,3',4,6-HxCB 131 ND D 0.1132,2',3,3',4,6'-HxCB 132 D 1.10 0.121 1.21 1.1742,2',3,3',5,5'-HxCB 133 D 8.14 0.109 1.24 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C NDR D 0.190 0.114 1.76 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 8.54 0.0761 1.11 1.1032,2',3,3',6,6'-HxCB 136 NDR D 0.171 0.0563 1.92 1.0232,2',3,4,4',5-HxCB 137 D 15.5 0.115 1.21 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C D 0.725 0.106 1.19 1.1532,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 0.1112,2',3,4,5,6-HxCB 142 ND D 0.1142,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 D 0.153 0.0790 1.26 1.1212,2',3,4,6,6'-HxCB 145 ND D 0.05962,2',3,4',5,5'-HxCB 146 D 65.7 0.0998 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 5.00 0.106 1.34 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.07832,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.05932,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.05252,2',4,4',5,5'-HxCB 153 153 + 168 C D 490 0.0883 1.27 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 9.71 0.0773 1.33 0.9382,3,3',4,5,5'-HxCB 159 NDR D 0.160 0.0821 4.95 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.08492,3,3',4',5,5'-HxCB 162 ND D 0.08512,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 1.05 0.0853 1.23 0.9222,3,3',5,5',6-HxCB 165 NDR D 0.189 0.0943 2.11 0.8782,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 ND D 3.01

2,2',3,3',4,4',5-HpCB 170 D 192 0.0666 1.03 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 18.1 0.0748 1.03 1.1622,2',3,3',4,5,5'-HpCB 172 D 25.9 0.0730 1.01 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 1.94 0.0717 1.16 1.1322,2',3,3',4,5',6-HpCB 175 D 2.38 0.0718 1.13 1.1022,2',3,3',4,6,6'-HpCB 176 NDR D 0.066 0.0553 2.19 1.0342,2',3,3',4',5,6-HpCB 177 D 30.5 0.0662 1.03 1.1452,2',3,3',5,5',6-HpCB 178 D 27.2 0.0707 1.08 1.0842,2',3,3',5,6,6'-HpCB 179 D 0.754 0.0523 0.90 1.0092,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 391 0.0550 1.02 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.395 0.0693 1.21 1.1562,2',3,4,4',5,6'-HpCB 182 NDR D 1.39 0.0678 1.40 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 41.8 0.0699 1.04 1.1262,2',3,4,4',6,6'-HpCB 184 NDR D 0.084 0.0530 0.65 1.0242,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.05652,2',3,4',5,5',6-HpCB 187 D 128 0.0708 1.02 1.1092,2',3,4',5,6,6'-HpCB 188 NDR D 0.953 0.0514 0.89 1.0002,3,3',4,4',5,5'-HpCB 189 D 12.6 0.155 1.07 1.0012,3,3',4,4',5,6-HpCB 190 D 37.9 0.0500 1.02 0.9472,3,3',4,4',5',6-HpCB 191 D 6.69 0.0533 1.08 0.9172,3,3',4,5,5',6-HpCB 192 ND D 0.05962,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 86.7 0.0913 0.87 0.9912,2',3,3',4,4',5,6-OcCB 195 D 25.0 0.108 0.92 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 37.5 0.0890 0.83 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.07812,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 103 0.0926 0.88 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 D 1.82 0.0771 0.89 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 14.2 0.0821 0.88 1.0002,2',3,4,4',5,5',6-OcCB 203 D 66.4 0.0850 0.92 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 0.07782,3,3',4,4',5,5',6-OcCB 205 D 3.69 0.0836 0.89 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 13.5 0.346 0.78 1.0012,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 1.22 0.312 0.64 1.0202,2',3,3',4,5,5',6,6'-NoCB 208 D 6.20 0.266 0.75 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 4.83 0.0678 0.67 1.000





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C D 1220 21.7 1.21 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 79300 20.5 1.29 0.9282,2',3,3',4,5'-HxCB 130 D 2340 25.7 1.17 0.9132,2',3,3',4,6-HxCB 131 ND D 23.82,2',3,3',4,6'-HxCB 132 D 232 25.5 1.21 1.1742,2',3,3',5,5'-HxCB 133 D 1720 23.0 1.24 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C NDR D 40.1 24.0 1.76 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 1800 16.1 1.11 1.1032,2',3,3',6,6'-HxCB 136 NDR D 36.1 11.9 1.92 1.0232,2',3,4,4',5-HxCB 137 D 3270 24.3 1.21 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C D 153 22.4 1.19 1.1532,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 23.42,2',3,4,5,6-HxCB 142 ND D 24.02,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 D 32.3 16.7 1.26 1.1212,2',3,4,6,6'-HxCB 145 ND D 12.62,2',3,4',5,5'-HxCB 146 D 13900 21.1 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 1050 22.4 1.34 1.1332,2',3,4',5,6'-HxCB 148 ND D 16.52,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 12.52,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 11.12,2',4,4',5,5'-HxCB 153 153 + 168 C D 103000 18.6 1.27 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 2050 16.3 1.33 0.9382,3,3',4,5,5'-HxCB 159 NDR D 33.8 17.3 4.95 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 17.92,3,3',4',5,5'-HxCB 162 ND D 18.02,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 222 18.0 1.23 0.9222,3,3',5,5',6-HxCB 165 NDR D 39.9 19.9 2.11 0.8782,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 ND D 635

2,2',3,3',4,4',5-HpCB 170 D 40500 14.0 1.03 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 3820 15.8 1.03 1.1622,2',3,3',4,5,5'-HpCB 172 D 5460 15.4 1.01 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 409 15.1 1.16 1.1322,2',3,3',4,5',6-HpCB 175 D 502 15.1 1.13 1.1022,2',3,3',4,6,6'-HpCB 176 NDR D 13.9 11.7 2.19 1.0342,2',3,3',4',5,6-HpCB 177 D 6430 14.0 1.03 1.1452,2',3,3',5,5',6-HpCB 178 D 5740 14.9 1.08 1.0842,2',3,3',5,6,6'-HpCB 179 D 159 11.0 0.90 1.0092,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 82500 11.6 1.02 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 83.3 14.6 1.21 1.1562,2',3,4,4',5,6'-HpCB 182 NDR D 293 14.3 1.40 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 8820 14.7 1.04 1.1262,2',3,4,4',6,6'-HpCB 184 NDR D 17.7 11.2 0.65 1.0242,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 11.92,2',3,4',5,5',6-HpCB 187 D 27000 14.9 1.02 1.1092,2',3,4',5,6,6'-HpCB 188 NDR D 201 10.8 0.89 1.0002,3,3',4,4',5,5'-HpCB 189 D 2660 32.7 1.07 1.0012,3,3',4,4',5,6-HpCB 190 D 8000 10.5 1.02 0.9472,3,3',4,4',5',6-HpCB 191 D 1410 11.2 1.08 0.9172,3,3',4,5,5',6-HpCB 192 ND D 12.62,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 18300 19.3 0.87 0.9912,2',3,3',4,4',5,6-OcCB 195 D 5270 22.8 0.92 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 7910 18.8 0.83 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 16.52,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 21700 19.5 0.88 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 D 384 16.3 0.89 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 3000 17.3 0.88 1.0002,2',3,4,4',5,5',6-OcCB 203 D 14000 17.9 0.92 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 16.42,3,3',4,4',5,5',6-OcCB 205 D 778 17.6 0.89 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 2850 73.0 0.78 1.0012,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 257 65.8 0.64 1.0202,2',3,3',4,5,5',6,6'-NoCB 208 D 1310 56.1 0.75 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 1020 14.3 0.67 1.000









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 699 35.0 3.21 0.71913C12-4-MoCB 3L 2000 789 39.5 3.17 0.857

13C12-2,2'-DiCB 4L 2000 1050 52.4 1.64 0.87313C12-4,4'-DiCB 15L 2000 1300 65.1 1.61 1.253

13C12-2,2',6-TriCB 19L 2000 1250 62.3 1.05 1.07213C12-3,4,4'-TriCB 37L 2000 1410 70.5 1.05 1.090





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1810 90.3 1.05 0.92413C12-2,3,3',5,5'-PeCB 111L 2000 1950 97.4 1.63 1.087

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X




13C12-2,2',4,4',6,6'-HxCB 155L D 2000 2060 103 1.28 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C D 4000 3290 82.3 1.31 1.10813C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L D 2000 1690 84.4 1.28 1.07813C12-3,3',4,4',5,5'-HxCB 169L D 2000 2620 131 1.24 1.191

13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 1960 97.8 1.09 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 1700 85.2 1.07 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1280 64.2 1.04 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 2060 103 1.00 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1310 65.7 0.84 0.81713C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1470 73.3 0.89 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1880 94.2 0.76 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 2230 111 0.75 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1870 93.7 1.23 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2430 121 1.02 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 0.504 0.0835 3.10 1.0013-MoCB 2 ND 0.08284-MoCB 3 0.587 0.0883 3.47 1.000


2,2',3-TriCB 16 NDR 0.078 0.0669 1.66 1.1652,2',4-TriCB 17 NDR 0.075 0.0621 0.82 1.1392,2',5-TriCB 18 18 + 30 C 0.735 0.0537 1.05 1.1132,2',6-TriCB 19 0.661 0.0671 1.07 1.0012,3,3'-TriCB 20 20 + 28 C 6.34 0.0569 1.04 0.8482,3,4-TriCB 21 21 + 33 C NDR 0.198 0.0547 0.74 0.8572,3,4'-TriCB 22 NDR 0.072 0.0622 2.31 0.8722,3,5-TriCB 23 0.619 0.0614 1.04 1.2832,3,6-TriCB 24 ND 0.04892,3',4-TriCB 25 ND 0.05282,3',5-TriCB 26 26 + 29 C NDR 0.059 0.0588 0.85 1.3022,3',6-TriCB 27 ND 0.04372,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1.14 0.0544 1.04 0.8372,4',6-TriCB 32 ND 0.05912',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 0.655 0.0609 1.11 1.2743,3',4-TriCB 35 ND 0.05183,3',5-TriCB 36 ND 0.05193,4,4'-TriCB 37 0.974 0.0618 1.02 1.0013,4,5-TriCB 38 ND 0.0521


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.05452,2',3,3'-TeCB 40 40 + 41 + 71 C 0.779 0.0361 0.77 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 ND 0.03712,2',3,5-TeCB 43 ND 0.04292,2',3,5'-TeCB 44 44 + 47 + 65 C 1.98 0.0339 0.77 1.2872,2',3,6-TeCB 45 45 + 51 C ND 0.03972,2',3,6'-TeCB 46 ND 0.04472,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.03752,2',4,5'-TeCB 49 49 + 69 C 0.815 0.0324 0.85 1.2592,2',4,6-TeCB 50 50 + 53 C 0.068 0.0392 0.78 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 1.78 0.0358 0.80 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 0.738 0.0271 0.75 1.0012,3,3',4-TeCB 55 ND 0.09782,3,3',4'-TeCB 56 NDR 0.846 0.0975 0.92 0.9052,3,3',5-TeCB 57 ND 0.09672,3,3',5'-TeCB 58 ND 0.09942,3,3',6-TeCB 59 59 + 62 + 75 C 0.122 0.0281 0.74 1.3032,3,4,4'-TeCB 60 1.46 0.0971 0.87 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 14.3 0.0942 0.80 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 0.191 0.0933 0.66 0.8642,3,4',6-TeCB 64 0.250 0.0266 0.69 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 0.03932,2',3,3',5-PeCB 83 83 + 99 C 16.5 0.0372 1.56 0.8852,2',3,3',6-PeCB 84 NDR 0.147 0.0417 1.23 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 1.11 0.0305 1.70 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1.30 0.0315 1.63 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.03782,2',3,4,6'-PeCB 89 ND 0.03872,2',3,4',5-PeCB 90 90 + 101 + 113 C 3.95 0.0324 1.59 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 1.02 0.0376 1.61 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 2.68 0.0373 1.58 1.1202,2',3,5,6'-PeCB 94 ND 0.04202,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.02122,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT








COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 5.68 0.0600 1.31 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 141 23.4 3.10 1.0013-MoCB 2 ND 23.24-MoCB 3 164 24.7 3.47 1.000


2,2',3-TriCB 16 NDR 21.9 18.7 1.66 1.1652,2',4-TriCB 17 NDR 21.0 17.4 0.82 1.1392,2',5-TriCB 18 18 + 30 C 206 15.0 1.05 1.1132,2',6-TriCB 19 185 18.8 1.07 1.0012,3,3'-TriCB 20 20 + 28 C 1780 15.9 1.04 0.8482,3,4-TriCB 21 21 + 33 C NDR 55.5 15.3 0.74 0.8572,3,4'-TriCB 22 NDR 20.2 17.4 2.31 0.8722,3,5-TriCB 23 173 17.2 1.04 1.2832,3,6-TriCB 24 ND 13.72,3',4-TriCB 25 ND 14.82,3',5-TriCB 26 26 + 29 C NDR 16.5 16.5 0.85 1.3022,3',6-TriCB 27 ND 12.22,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 319 15.2 1.04 0.8372,4',6-TriCB 32 ND 16.62',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 184 17.1 1.11 1.2743,3',4-TriCB 35 ND 14.53,3',5-TriCB 36 ND 14.53,4,4'-TriCB 37 273 17.3 1.02 1.0013,4,5-TriCB 38 ND 14.6


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 15.32,2',3,3'-TeCB 40 40 + 41 + 71 C 218 10.1 0.77 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 ND 10.42,2',3,5-TeCB 43 ND 12.02,2',3,5'-TeCB 44 44 + 47 + 65 C 555 9.50 0.77 1.2872,2',3,6-TeCB 45 45 + 51 C ND 11.12,2',3,6'-TeCB 46 ND 12.52,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 10.52,2',4,5'-TeCB 49 49 + 69 C 228 9.08 0.85 1.2592,2',4,6-TeCB 50 50 + 53 C 19.1 11.0 0.78 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 499 10.0 0.80 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 207 7.59 0.75 1.0012,3,3',4-TeCB 55 ND 27.42,3,3',4'-TeCB 56 NDR 237 27.3 0.92 0.9052,3,3',5-TeCB 57 ND 27.12,3,3',5'-TeCB 58 ND 27.92,3,3',6-TeCB 59 59 + 62 + 75 C 34.2 7.87 0.74 1.3032,3,4,4'-TeCB 60 409 27.2 0.87 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 4010 26.4 0.80 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 53.5 26.1 0.66 0.8642,3,4',6-TeCB 64 70.0 7.45 0.69 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 11.02,2',3,3',5-PeCB 83 83 + 99 C 4620 10.4 1.56 0.8852,2',3,3',6-PeCB 84 NDR 41.2 11.7 1.23 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 311 8.55 1.70 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 364 8.83 1.63 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 10.62,2',3,4,6'-PeCB 89 ND 10.82,2',3,4',5-PeCB 90 90 + 101 + 113 C 1110 9.08 1.59 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 286 10.5 1.61 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 751 10.5 1.58 1.1202,2',3,5,6'-PeCB 94 ND 11.82,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 5.942,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT








COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 1590 16.8 1.31 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406






Extract Volume (uL): 200 Sample Data Filename: PB8B_270B S: 3


Dilution Factor: 10 Cal. Ver. Data Filename: PB8B_270B S: 1


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT




Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_L11590-3_Form1A_PB8B_270BS3_SJ913109.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 1.66 0.326 1.03 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 95.2 0.322 1.31 0.9282,2',3,3',4,5'-HxCB 130 NDR D 3.13 0.402 1.84 0.9132,2',3,3',4,6-HxCB 131 ND D 0.3622,2',3,3',4,6'-HxCB 132 NDR D 1.07 0.397 0.91 1.1742,2',3,3',5,5'-HxCB 133 D 1.97 0.357 1.17 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.3662,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 4.25 0.0886 1.13 1.1032,2',3,3',6,6'-HxCB 136 NDR D 0.255 0.0671 0.69 1.0242,2',3,4,4',5-HxCB 137 D 4.12 0.378 1.37 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 0.3402,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 NDR D 1.63 0.350 1.93 0.9042,2',3,4,5,6-HxCB 142 ND D 0.3742,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 D 0.114 0.0901 1.17 1.1202,2',3,4,6,6'-HxCB 145 ND D 0.07192,2',3,4',5,5'-HxCB 146 D 15.1 0.332 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 3.22 0.331 1.23 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.09162,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.06822,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.06382,2',4,4',5,5'-HxCB 153 153 + 168 C D 122 0.285 1.26 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 NDR D 2.89 0.257 1.49 0.9382,3,3',4,5,5'-HxCB 159 ND D 0.2732,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.2662,3,3',4',5,5'-HxCB 162 ND D 0.2842,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 0.693 0.277 1.13 0.9212,3,3',5,5',6-HxCB 165 ND D 0.3012,3,4,4',5,6-HxCB 166 128 + 166 C128




For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-3_Form1A_PB8B_270BS3_SJ913109.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 50.3 0.126 1.10 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 5.36 0.131 1.02 1.1622,2',3,3',4,5,5'-HpCB 172 D 6.51 0.132 1.18 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 2.16 0.124 0.98 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 0.738 0.120 1.26 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 0.08962,2',3,3',4',5,6-HpCB 177 D 10.9 0.122 0.98 1.1452,2',3,3',5,5',6-HpCB 178 D 7.64 0.122 0.95 1.0852,2',3,3',5,6,6'-HpCB 179 D 1.01 0.0870 0.98 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 120 0.105 1.03 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.531 0.124 0.54 1.1562,2',3,4,4',5,6'-HpCB 182 D 0.493 0.120 1.14 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 15.9 0.119 1.02 1.1262,2',3,4,4',6,6'-HpCB 184 NDR D 0.128 0.0874 0.52 1.0242,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.09612,2',3,4',5,5',6-HpCB 187 D 40.3 0.115 1.02 1.1102,2',3,4',5,6,6'-HpCB 188 NDR D 0.345 0.0691 1.70 1.0002,3,3',4,4',5,5'-HpCB 189 D 3.03 0.0493 1.18 1.0012,3,3',4,4',5,6-HpCB 190 D 10.4 0.0961 0.98 0.9472,3,3',4,4',5',6-HpCB 191 D 2.58 0.0969 1.00 0.9172,3,3',4,5,5',6-HpCB 192 ND D 0.1072,3,3',4',5,5',6-HpCB 193 180 + 193 C180


2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 3.53 0.405 0.96 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 0.594 0.318 0.41 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 1.54 0.295 0.62 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 1.86 0.0712 0.75 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT




Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_L11590-3_Form1A_PB8B_270BS3_SJ913109_Lipid.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 465 91.3 1.03 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 26700 90.2 1.31 0.9282,2',3,3',4,5'-HxCB 130 NDR D 877 113 1.84 0.9132,2',3,3',4,6-HxCB 131 ND D 1012,2',3,3',4,6'-HxCB 132 NDR D 300 111 0.91 1.1742,2',3,3',5,5'-HxCB 133 D 552 100 1.17 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 1032,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 1190 24.8 1.13 1.1032,2',3,3',6,6'-HxCB 136 NDR D 71.4 18.8 0.69 1.0242,2',3,4,4',5-HxCB 137 D 1150 106 1.37 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 95.32,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 NDR D 457 98.1 1.93 0.9042,2',3,4,5,6-HxCB 142 ND D 1052,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 D 31.9 25.2 1.17 1.1202,2',3,4,6,6'-HxCB 145 ND D 20.12,2',3,4',5,5'-HxCB 146 D 4230 93.0 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C D 902 92.7 1.23 1.1332,2',3,4',5,6'-HxCB 148 ND D 25.72,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 19.12,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 17.92,2',4,4',5,5'-HxCB 153 153 + 168 C D 34200 79.9 1.26 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 NDR D 810 72.0 1.49 0.9382,3,3',4,5,5'-HxCB 159 ND D 76.52,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 74.52,3,3',4',5,5'-HxCB 162 ND D 79.62,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 194 77.6 1.13 0.9212,3,3',5,5',6-HxCB 165 ND D 84.32,3,4,4',5,6-HxCB 166 128 + 166 C128




For Axys Internal Use Only [ XSL Template: Form16681A.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-3_Form1A_PB8B_270BS3_SJ913109_Lipid.html; Workgroup: WG26343; Design ID: 925 ]


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 14100 35.3 1.10 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 1500 36.7 1.02 1.1622,2',3,3',4,5,5'-HpCB 172 D 1820 37.0 1.18 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 605 34.7 0.98 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 207 33.6 1.26 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 25.12,2',3,3',4',5,6-HpCB 177 D 3050 34.2 0.98 1.1452,2',3,3',5,5',6-HpCB 178 D 2140 34.2 0.95 1.0852,2',3,3',5,6,6'-HpCB 179 D 283 24.4 0.98 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 33600 29.4 1.03 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 149 34.7 0.54 1.1562,2',3,4,4',5,6'-HpCB 182 D 138 33.6 1.14 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 4460 33.3 1.02 1.1262,2',3,4,4',6,6'-HpCB 184 NDR D 35.9 24.5 0.52 1.0242,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 26.92,2',3,4',5,5',6-HpCB 187 D 11300 32.2 1.02 1.1102,2',3,4',5,6,6'-HpCB 188 NDR D 96.7 19.4 1.70 1.0002,3,3',4,4',5,5'-HpCB 189 D 849 13.8 1.18 1.0012,3,3',4,4',5,6-HpCB 190 D 2910 26.9 0.98 0.9472,3,3',4,4',5',6-HpCB 191 D 723 27.2 1.00 0.9172,3,3',4,5,5',6-HpCB 192 ND D 30.02,3,3',4',5,5',6-HpCB 193 180 + 193 C180


2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 989 113 0.96 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 NDR D 166 89.1 0.41 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 431 82.7 0.62 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 521 19.9 0.75 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 496 24.8 3.32 0.71713C12-4-MoCB 3L 2000 675 33.8 3.20 0.858

13C12-2,2'-DiCB 4L 2000 916 45.8 1.64 0.87313C12-4,4'-DiCB 15L 2000 1450 72.6 1.63 1.254

13C12-2,2',6-TriCB 19L 2000 1260 63.0 1.03 1.07213C12-3,4,4'-TriCB 37L 2000 1440 71.9 1.07 1.091





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1830 91.4 1.05 0.92413C12-2,3,3',5,5'-PeCB 111L 2000 1970 98.6 1.64 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X




For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_L11590-3_Form2_PB8B_270BS3_SJ913109.html; Workgroup: WG26343; Design ID: 925 ]





Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X




13C12-2,2',4,4',6,6'-HxCB 155L D 2000 1920 96.1 1.24 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C D 4000 3230 80.9 1.27 1.10813C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L D 2000 1620 80.9 1.22 1.07813C12-3,3',4,4',5,5'-HxCB 169L D 2000 2220 111 1.20 1.191

13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 2220 111 0.99 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 2010 100 1.08 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1620 81.2 1.14 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 1920 96.0 1.05 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1490 74.7 0.87 0.81713C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1600 80.1 0.90 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1850 92.5 0.85 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 2160 108 0.83 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1880 94.2 1.14 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2180 109 1.12 1.012

Page 1 of 1 (WG26343 - 1668_PCB1668_PCBTF_L11590-3_Form2_PB8B_270BS3_SJ913109.html)




Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 2.80 0.0845 3.08 1.0013-MoCB 2 ND 0.09024-MoCB 3 3.25 0.102 3.28 1.000


2,2',3-TriCB 16 0.067 0.0503 1.09 1.1662,2',4-TriCB 17 0.057 0.0467 1.18 1.1382,2',5-TriCB 18 18 + 30 C 2.71 0.0404 1.02 1.1142,2',6-TriCB 19 3.16 0.0558 1.12 1.0012,3,3'-TriCB 20 20 + 28 C 11.8 0.0573 1.03 0.8482,3,4-TriCB 21 21 + 33 C 0.204 0.0552 0.97 0.8572,3,4'-TriCB 22 ND 0.06272,3,5-TriCB 23 3.16 0.0619 0.95 1.2832,3,6-TriCB 24 ND 0.03682,3',4-TriCB 25 ND 0.05322,3',5-TriCB 26 26 + 29 C 0.068 0.0593 0.99 1.3022,3',6-TriCB 27 ND 0.03282,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 4.34 0.0549 1.03 0.8372,4',6-TriCB 32 ND 0.05952',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 3.31 0.0614 1.08 1.2733,3',4-TriCB 35 ND 0.05223,3',5-TriCB 36 ND 0.05233,4,4'-TriCB 37 5.07 0.0600 1.05 1.0013,4,5-TriCB 38 ND 0.0526


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.05492,2',3,3'-TeCB 40 40 + 41 + 71 C 3.13 0.0398 0.77 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.062 0.0408 0.69 1.3122,2',3,5-TeCB 43 ND 0.04722,2',3,5'-TeCB 44 44 + 47 + 65 C 4.56 0.0373 0.82 1.2852,2',3,6-TeCB 45 45 + 51 C NDR 0.051 0.0437 0.96 1.1502,2',3,6'-TeCB 46 ND 0.04922,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.04132,2',4,5'-TeCB 49 49 + 69 C 3.23 0.0357 0.76 1.2592,2',4,6-TeCB 50 50 + 53 C ND 0.04312,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 4.65 0.0395 0.78 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 3.63 0.0334 0.78 1.0022,3,3',4-TeCB 55 ND 0.08822,3,3',4'-TeCB 56 4.36 0.0879 0.83 0.9052,3,3',5-TeCB 57 ND 0.08722,3,3',5'-TeCB 58 ND 0.08962,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.043 0.0309 2.32 1.3042,3,4,4'-TeCB 60 2.33 0.0875 0.83 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 10.9 0.0849 0.81 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 0.215 0.0842 0.91 0.8652,3,4',6-TeCB 64 0.228 0.0293 0.71 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 9.13 0.0827 0.81 0.8852,3',4,5-TeCB 67 ND 0.07982,3',4,5'-TeCB 68 0.280 0.0862 0.78 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.08592,3',5',6-TeCB 73 ND 0.03282,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 5.16 0.0969 0.83 1.0003,3',4,5-TeCB 78 ND 0.08133,3',4,5'-TeCB 79 ND 0.06833,3',5,5'-TeCB 80 ND 0.07753,4,4',5-TeCB 81 5.02 0.0899 0.86 1.001

2,2',3,3',4-PeCB 82 ND 0.03622,2',3,3',5-PeCB 83 83 + 99 C 12.3 0.0343 1.59 0.8862,2',3,3',6-PeCB 84 NDR 0.056 0.0384 2.71 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 1.08 0.0281 1.51 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 3.65 0.0290 1.61 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C 0.050 0.0348 1.67 1.1542,2',3,4,6'-PeCB 89 ND 0.03562,2',3,4',5-PeCB 90 90 + 101 + 113 C 7.71 0.0298 1.57 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 1.23 0.0346 1.62 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 5.17 0.0343 1.55 1.1202,2',3,5,6'-PeCB 94 ND 0.03872,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01872,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C 4.08 0.0412 1.23 0.9602,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 90.7 0.0406 1.27 0.9292,2',3,3',4,5'-HxCB 130 2.99 0.0504 1.32 0.9142,2',3,3',4,6-HxCB 131 ND 0.05082,2',3,3',4,6'-HxCB 132 1.39 0.0517 1.21 1.1742,2',3,3',5,5'-HxCB 133 1.34 0.0465 1.18 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C NDR 0.195 0.0478 1.69 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 10.3 0.0148 1.24 1.1032,2',3,3',6,6'-HxCB 136 0.243 0.0120 1.24 1.0242,2',3,4,4',5-HxCB 137 2.84 0.0461 1.23 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR 0.188 0.0449 1.70 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 3.93 0.0447 1.30 0.9042,2',3,4,5,6-HxCB 142 ND 0.04822,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 NDR 0.266 0.0151 0.99 1.1222,2',3,4,6,6'-HxCB 145 ND 0.01232,2',3,4',5,5'-HxCB 146 13.7 0.0420 1.28 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 5.75 0.0452 1.24 1.1332,2',3,4',5,6'-HxCB 148 ND 0.01492,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 0.01212,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 0.01202,2',4,4',5,5'-HxCB 153 153 + 168 C 108 0.0362 1.26 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 1.57 0.0120 1.36 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 21.3 0.0436 1.26 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 3.97 0.0321 1.26 0.9382,3,3',4,5,5'-HxCB 159 0.180 0.0352 1.08 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 0.03432,3,3',4',5,5'-HxCB 162 ND 0.03502,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 2.41 0.0351 1.30 0.9222,3,3',5,5',6-HxCB 165 NDR 0.044 0.0395 0.76 0.8792,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 7.68 0.0335 1.24 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 3.86 0.0400 1.29 1.000




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 889 26.8 3.08 1.0013-MoCB 2 ND 28.64-MoCB 3 1030 32.4 3.28 1.000


2,2',3-TriCB 16 21.3 16.0 1.09 1.1662,2',4-TriCB 17 18.1 14.8 1.18 1.1382,2',5-TriCB 18 18 + 30 C 861 12.8 1.02 1.1142,2',6-TriCB 19 1000 17.7 1.12 1.0012,3,3'-TriCB 20 20 + 28 C 3750 18.2 1.03 0.8482,3,4-TriCB 21 21 + 33 C 64.8 17.5 0.97 0.8572,3,4'-TriCB 22 ND 19.92,3,5-TriCB 23 1000 19.7 0.95 1.2832,3,6-TriCB 24 ND 11.72,3',4-TriCB 25 ND 16.92,3',5-TriCB 26 26 + 29 C 21.6 18.8 0.99 1.3022,3',6-TriCB 27 ND 10.42,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1380 17.4 1.03 0.8372,4',6-TriCB 32 ND 18.92',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 1050 19.5 1.08 1.2733,3',4-TriCB 35 ND 16.63,3',5-TriCB 36 ND 16.63,4,4'-TriCB 37 1610 19.1 1.05 1.0013,4,5-TriCB 38 ND 16.7


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 17.42,2',3,3'-TeCB 40 40 + 41 + 71 C 994 12.6 0.77 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 19.7 13.0 0.69 1.3122,2',3,5-TeCB 43 ND 15.02,2',3,5'-TeCB 44 44 + 47 + 65 C 1450 11.8 0.82 1.2852,2',3,6-TeCB 45 45 + 51 C NDR 16.2 13.9 0.96 1.1502,2',3,6'-TeCB 46 ND 15.62,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 13.12,2',4,5'-TeCB 49 49 + 69 C 1030 11.3 0.76 1.2592,2',4,6-TeCB 50 50 + 53 C ND 13.72,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 1480 12.5 0.78 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1150 10.6 0.78 1.0022,3,3',4-TeCB 55 ND 28.02,3,3',4'-TeCB 56 1380 27.9 0.83 0.9052,3,3',5-TeCB 57 ND 27.72,3,3',5'-TeCB 58 ND 28.52,3,3',6-TeCB 59 59 + 62 + 75 C NDR 13.7 9.81 2.32 1.3042,3,4,4'-TeCB 60 740 27.8 0.83 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 3460 27.0 0.81 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 68.3 26.7 0.91 0.8652,3,4',6-TeCB 64 72.4 9.30 0.71 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 2900 26.3 0.81 0.8852,3',4,5-TeCB 67 ND 25.32,3',4,5'-TeCB 68 88.9 27.4 0.78 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 27.32,3',5',6-TeCB 73 ND 10.42,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 1640 30.8 0.83 1.0003,3',4,5-TeCB 78 ND 25.83,3',4,5'-TeCB 79 ND 21.73,3',5,5'-TeCB 80 ND 24.63,4,4',5-TeCB 81 1590 28.5 0.86 1.001

2,2',3,3',4-PeCB 82 ND 11.52,2',3,3',5-PeCB 83 83 + 99 C 3910 10.9 1.59 0.8862,2',3,3',6-PeCB 84 NDR 17.8 12.2 2.71 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 343 8.92 1.51 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1160 9.21 1.61 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C 15.9 11.1 1.67 1.1542,2',3,4,6'-PeCB 89 ND 11.32,2',3,4',5-PeCB 90 90 + 101 + 113 C 2450 9.46 1.57 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 391 11.0 1.62 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 1640 10.9 1.55 1.1202,2',3,5,6'-PeCB 94 ND 12.32,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 5.942,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C 1300 13.1 1.23 0.9602,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 28800 12.9 1.27 0.9292,2',3,3',4,5'-HxCB 130 949 16.0 1.32 0.9142,2',3,3',4,6-HxCB 131 ND 16.12,2',3,3',4,6'-HxCB 132 441 16.4 1.21 1.1742,2',3,3',5,5'-HxCB 133 425 14.8 1.18 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C NDR 61.9 15.2 1.69 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 3270 4.70 1.24 1.1032,2',3,3',6,6'-HxCB 136 77.2 3.81 1.24 1.0242,2',3,4,4',5-HxCB 137 902 14.6 1.23 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR 59.7 14.3 1.70 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 1250 14.2 1.30 0.9042,2',3,4,5,6-HxCB 142 ND 15.32,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 NDR 84.5 4.79 0.99 1.1222,2',3,4,6,6'-HxCB 145 ND 3.912,2',3,4',5,5'-HxCB 146 4350 13.3 1.28 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 1830 14.4 1.24 1.1332,2',3,4',5,6'-HxCB 148 ND 4.732,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 3.842,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 3.812,2',4,4',5,5'-HxCB 153 153 + 168 C 34300 11.5 1.26 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 499 3.81 1.36 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 6760 13.8 1.26 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 1260 10.2 1.26 0.9382,3,3',4,5,5'-HxCB 159 57.2 11.2 1.08 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 10.92,3,3',4',5,5'-HxCB 162 ND 11.12,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 765 11.1 1.30 0.9222,3,3',5,5',6-HxCB 165 NDR 14.0 12.5 0.76 0.8792,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 2440 10.6 1.24 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 1230 12.7 1.29 1.000




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X

2,2',3,3',4,4',5-HpCB 170 D 37.1 0.0905 1.02 0.9372,2',3,3',4,4',6-HpCB 171 171 + 173 C D 3.82 0.0940 0.90 1.1632,2',3,3',4,5,5'-HpCB 172 D 4.79 0.0944 1.02 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 3.16 0.0886 1.17 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 0.555 0.0856 1.61 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 0.06422,2',3,3',4',5,6-HpCB 177 D 9.87 0.0876 0.93 1.1452,2',3,3',5,5',6-HpCB 178 D 6.18 0.0876 0.90 1.0852,2',3,3',5,6,6'-HpCB 179 D 1.20 0.0623 0.97 1.0092,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 89.2 0.0751 1.01 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.096 0.0891 4.44 1.1562,2',3,4,4',5,6'-HpCB 182 D 2.04 0.0857 0.94 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 15.0 0.0851 1.13 1.1262,2',3,4,4',6,6'-HpCB 184 ND D 0.06262,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.06892,2',3,4',5,5',6-HpCB 187 D 33.0 0.0824 0.98 1.1102,2',3,4',5,6,6'-HpCB 188 D 1.64 0.0586 1.05 1.0002,3,3',4,4',5,5'-HpCB 189 D 6.04 0.0994 0.98 1.0002,3,3',4,4',5,6-HpCB 190 D 6.12 0.0688 0.99 0.9472,3,3',4,4',5',6-HpCB 191 D 1.69 0.0694 1.18 0.9182,3,3',4,5,5',6-HpCB 192 ND D 0.07682,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 21.4 0.0821 0.91 0.9912,2',3,3',4,4',5,6-OcCB 195 D 4.46 0.0960 0.98 0.9462,2',3,3',4,4',5,6'-OcCB 196 D 8.94 0.0986 1.01 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.07792,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 13.9 0.103 0.91 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.419 0.0777 0.60 1.0222,2',3,3',5,5',6,6'-OcCB 202 NDR D 4.71 0.0961 1.04 1.0002,2',3,4,4',5,5',6-OcCB 203 D 8.63 0.0945 0.99 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 0.07962,3,3',4,4',5,5',6-OcCB 205 D 3.39 0.0685 0.78 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 5.10 0.583 0.74 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 0.4842,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 2.42 0.464 0.93 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 2.88 0.0678 0.81 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT









COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 11800 28.7 1.02 0.9372,2',3,3',4,4',6-HpCB 171 171 + 173 C D 1210 29.8 0.90 1.1632,2',3,3',4,5,5'-HpCB 172 D 1520 30.0 1.02 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 1000 28.1 1.17 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 176 27.2 1.61 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 20.42,2',3,3',4',5,6-HpCB 177 D 3130 27.8 0.93 1.1452,2',3,3',5,5',6-HpCB 178 D 1960 27.8 0.90 1.0852,2',3,3',5,6,6'-HpCB 179 D 381 19.8 0.97 1.0092,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 28300 23.8 1.01 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 30.5 28.3 4.44 1.1562,2',3,4,4',5,6'-HpCB 182 D 648 27.2 0.94 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 4760 27.0 1.13 1.1262,2',3,4,4',6,6'-HpCB 184 ND D 19.92,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 21.92,2',3,4',5,5',6-HpCB 187 D 10500 26.2 0.98 1.1102,2',3,4',5,6,6'-HpCB 188 D 521 18.6 1.05 1.0002,3,3',4,4',5,5'-HpCB 189 D 1920 31.6 0.98 1.0002,3,3',4,4',5,6-HpCB 190 D 1940 21.8 0.99 0.9472,3,3',4,4',5',6-HpCB 191 D 537 22.0 1.18 0.9182,3,3',4,5,5',6-HpCB 192 ND D 24.42,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 6800 26.1 0.91 0.9912,2',3,3',4,4',5,6-OcCB 195 D 1420 30.5 0.98 0.9462,2',3,3',4,4',5,6'-OcCB 196 D 2840 31.3 1.01 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 24.72,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 4410 32.7 0.91 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 133 24.7 0.60 1.0222,2',3,3',5,5',6,6'-OcCB 202 NDR D 1500 30.5 1.04 1.0002,2',3,4,4',5,5',6-OcCB 203 D 2740 30.0 0.99 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 25.32,3,3',4,4',5,5',6-OcCB 205 D 1080 21.8 0.78 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 1620 185 0.74 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 1542,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 768 147 0.93 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 914 21.5 0.81 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 430 21.5 3.24 0.71813C12-4-MoCB 3L 2000 506 25.3 3.28 0.858

13C12-2,2'-DiCB 4L 2000 704 35.2 1.60 0.87313C12-4,4'-DiCB 15L 2000 1090 54.4 1.60 1.254

13C12-2,2',6-TriCB 19L 2000 954 47.7 1.03 1.07213C12-3,4,4'-TriCB 37L 2000 1190 59.3 1.01 1.092





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1640 82.1 1.06 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1930 96.3 1.64 1.087

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X




13C12-2,2',4,4',6,6'-HxCB 155L X13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L X13C12-3,3',4,4',5,5'-HxCB 169L X

13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 1170 58.6 1.13 0.89713C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 1210 60.6 1.03 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1030 51.6 1.07 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 1590 79.6 1.10 0.959

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 998 49.9 0.79 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1440 72.2 0.88 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1380 69.0 0.85 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 1400 70.0 0.86 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1490 74.3 1.17 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2280 114 1.09 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 1.36 0.0473 3.47 1.0013-MoCB 2 ND 0.04914-MoCB 3 1.54 0.0571 3.01 1.001


2,2',3-TriCB 16 NDR 0.075 0.0499 2.27 1.1662,2',4-TriCB 17 NDR 0.069 0.0445 0.39 1.1382,2',5-TriCB 18 18 + 30 C 1.34 0.0375 1.04 1.1142,2',6-TriCB 19 1.45 0.0446 1.19 1.0012,3,3'-TriCB 20 20 + 28 C 4.26 0.0319 1.09 0.8482,3,4-TriCB 21 21 + 33 C ND 0.03132,3,4'-TriCB 22 NDR 0.075 0.0351 0.73 0.8712,3,5-TriCB 23 1.51 0.0342 1.14 1.2832,3,6-TriCB 24 ND 0.03282,3',4-TriCB 25 ND 0.02872,3',5-TriCB 26 26 + 29 C NDR 0.075 0.0327 0.78 1.3022,3',6-TriCB 27 ND 0.03172,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1.97 0.0301 1.04 0.8372,4',6-TriCB 32 NDR 0.040 0.0312 0.53 1.1992',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 1.46 0.0335 1.11 1.2753,3',4-TriCB 35 ND 0.03073,3',5-TriCB 36 ND 0.03113,4,4'-TriCB 37 2.16 0.0401 1.04 1.0013,4,5-TriCB 38 ND 0.0311


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.03172,2',3,3'-TeCB 40 40 + 41 + 71 C 1.38 0.0325 0.79 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 0.044 0.0337 2.34 1.3112,2',3,5-TeCB 43 ND 0.03772,2',3,5'-TeCB 44 44 + 47 + 65 C 2.12 0.0298 0.84 1.2852,2',3,6-TeCB 45 45 + 51 C 0.077 0.0337 0.75 1.1482,2',3,6'-TeCB 46 ND 0.03792,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 0.039 0.0333 1.03 1.2732,2',4,5'-TeCB 49 49 + 69 C 1.40 0.0282 0.84 1.2592,2',4,6-TeCB 50 50 + 53 C ND 0.03262,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 2.06 0.0305 0.75 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1.56 0.0215 0.85 1.0002,3,3',4-TeCB 55 ND 0.05312,3,3',4'-TeCB 56 1.75 0.0527 0.76 0.9042,3,3',5-TeCB 57 ND 0.05142,3,3',5'-TeCB 58 ND 0.05442,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.062 0.0248 0.95 1.3012,3,4,4'-TeCB 60 0.534 0.0525 0.73 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 3.31 0.0500 0.79 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 0.053 0.0504 1.51 0.8642,3,4',6-TeCB 64 NDR 0.121 0.0238 0.90 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 2.70 0.0484 0.81 0.8842,3',4,5-TeCB 67 ND 0.04662,3',4,5'-TeCB 68 0.143 0.0504 0.65 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.05032,3',5',6-TeCB 73 ND 0.02552,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 2.25 0.0618 0.70 1.0003,3',4,5-TeCB 78 ND 0.04943,3',4,5'-TeCB 79 NDR 0.071 0.0427 0.64 0.9723,3',5,5'-TeCB 80 ND 0.04703,4,4',5-TeCB 81 2.14 0.0548 0.78 1.000

2,2',3,3',4-PeCB 82 ND 0.04272,2',3,3',5-PeCB 83 83 + 99 C 4.34 0.0418 1.69 0.8862,2',3,3',6-PeCB 84 ND 0.04512,2',3,4,4'-PeCB 85 85 + 116 + 117 C NDR 0.261 0.0332 2.00 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1.93 0.0355 1.56 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.04152,2',3,4,6'-PeCB 89 ND 0.04302,2',3,4',5-PeCB 90 90 + 101 + 113 C 2.75 0.0355 1.52 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 0.382 0.0410 2.09 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 2.37 0.0408 1.56 1.1202,2',3,5,6'-PeCB 94 ND 0.04552,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.02462,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.03762,2',4,6,6'-PeCB 104 1.16 0.0206 1.42 1.0012,3,3',4,4'-PeCB 105 3.51 0.0889 1.57 1.0012,3,3',4,5-PeCB 106 ND 0.07242,3,3',4',5-PeCB 107 107 + 124 C ND 0.07762,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 0.134 0.0715 1.91 0.9972,3,3',4',6-PeCB 110 110 + 115 C 2.17 0.0295 1.62 0.9252,3,3',5,5'-PeCB 111 ND 0.02972,3,3',5,6-PeCB 112 ND 0.02902,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 1.95 0.0792 1.55 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 7.52 0.0813 1.57 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 0.02822,3',4,5',6-PeCB 121 ND 0.03132',3,3',4,5-PeCB 122 ND 0.07922',3,4,4',5-PeCB 123 1.59 0.0835 1.58 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 2.31 0.0982 1.75 1.0003,3',4,5,5'-PeCB 127 ND 0.0728







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 2.62 0.0374 1.35 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 327 11.4 3.47 1.0013-MoCB 2 ND 11.84-MoCB 3 370 13.7 3.01 1.001


2,2',3-TriCB 16 NDR 18.0 12.0 2.27 1.1662,2',4-TriCB 17 NDR 16.6 10.7 0.39 1.1382,2',5-TriCB 18 18 + 30 C 322 9.01 1.04 1.1142,2',6-TriCB 19 348 10.7 1.19 1.0012,3,3'-TriCB 20 20 + 28 C 1020 7.67 1.09 0.8482,3,4-TriCB 21 21 + 33 C ND 7.522,3,4'-TriCB 22 NDR 18.0 8.44 0.73 0.8712,3,5-TriCB 23 363 8.22 1.14 1.2832,3,6-TriCB 24 ND 7.882,3',4-TriCB 25 ND 6.902,3',5-TriCB 26 26 + 29 C NDR 18.0 7.86 0.78 1.3022,3',6-TriCB 27 ND 7.622,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 473 7.23 1.04 0.8372,4',6-TriCB 32 NDR 9.61 7.50 0.53 1.1992',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 351 8.05 1.11 1.2753,3',4-TriCB 35 ND 7.383,3',5-TriCB 36 ND 7.473,4,4'-TriCB 37 519 9.64 1.04 1.0013,4,5-TriCB 38 ND 7.47


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 7.622,2',3,3'-TeCB 40 40 + 41 + 71 C 332 7.81 0.79 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 10.6 8.10 2.34 1.3112,2',3,5-TeCB 43 ND 9.062,2',3,5'-TeCB 44 44 + 47 + 65 C 510 7.16 0.84 1.2852,2',3,6-TeCB 45 45 + 51 C 18.5 8.10 0.75 1.1482,2',3,6'-TeCB 46 ND 9.112,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 9.37 8.00 1.03 1.2732,2',4,5'-TeCB 49 49 + 69 C 336 6.78 0.84 1.2592,2',4,6-TeCB 50 50 + 53 C ND 7.842,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 495 7.33 0.75 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 375 5.17 0.85 1.0002,3,3',4-TeCB 55 ND 12.82,3,3',4'-TeCB 56 421 12.7 0.76 0.9042,3,3',5-TeCB 57 ND 12.42,3,3',5'-TeCB 58 ND 13.12,3,3',6-TeCB 59 59 + 62 + 75 C NDR 14.9 5.96 0.95 1.3012,3,4,4'-TeCB 60 128 12.6 0.73 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 796 12.0 0.79 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 12.7 12.1 1.51 0.8642,3,4',6-TeCB 64 NDR 29.1 5.72 0.90 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 649 11.6 0.81 0.8842,3',4,5-TeCB 67 ND 11.22,3',4,5'-TeCB 68 34.4 12.1 0.65 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 12.12,3',5',6-TeCB 73 ND 6.132,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 541 14.9 0.70 1.0003,3',4,5-TeCB 78 ND 11.93,3',4,5'-TeCB 79 NDR 17.1 10.3 0.64 0.9723,3',5,5'-TeCB 80 ND 11.33,4,4',5-TeCB 81 514 13.2 0.78 1.000

2,2',3,3',4-PeCB 82 ND 10.32,2',3,3',5-PeCB 83 83 + 99 C 1040 10.0 1.69 0.8862,2',3,3',6-PeCB 84 ND 10.82,2',3,4,4'-PeCB 85 85 + 116 + 117 C NDR 62.7 7.98 2.00 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 464 8.53 1.56 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 9.972,2',3,4,6'-PeCB 89 ND 10.32,2',3,4',5-PeCB 90 90 + 101 + 113 C 661 8.53 1.52 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 91.8 9.85 2.09 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 570 9.81 1.56 1.1202,2',3,5,6'-PeCB 94 ND 10.92,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 5.912,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 9.042,2',4,6,6'-PeCB 104 279 4.95 1.42 1.0012,3,3',4,4'-PeCB 105 844 21.4 1.57 1.0012,3,3',4,5-PeCB 106 ND 17.42,3,3',4',5-PeCB 107 107 + 124 C ND 18.72,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 32.2 17.2 1.91 0.9972,3,3',4',6-PeCB 110 110 + 115 C 522 7.09 1.62 0.9252,3,3',5,5'-PeCB 111 ND 7.142,3,3',5,6-PeCB 112 ND 6.972,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 469 19.0 1.55 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 1810 19.5 1.57 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 6.782,3',4,5',6-PeCB 121 ND 7.522',3,3',4,5-PeCB 122 ND 19.02',3,4,4',5-PeCB 123 382 20.1 1.58 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 555 23.6 1.75 1.0003,3',4,5,5'-PeCB 127 ND 17.5







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 630 8.99 1.35 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 0.269 0.0540 11.08 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 20.2 0.0533 1.29 0.9282,2',3,3',4,5'-HxCB 130 NDR D 0.882 0.0665 1.48 0.9132,2',3,3',4,6-HxCB 131 ND D 0.05992,2',3,3',4,6'-HxCB 132 NDR D 0.161 0.0657 0.44 1.1752,2',3,3',5,5'-HxCB 133 NDR D 0.484 0.0590 1.71 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.06062,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C NDR D 2.06 0.0861 1.57 1.1032,2',3,3',6,6'-HxCB 136 ND D 0.06532,2',3,4,4',5-HxCB 137 NDR D 0.715 0.0625 1.75 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 0.05622,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 NDR D 0.533 0.0579 2.38 0.9032,2',3,4,5,6-HxCB 142 ND D 0.06192,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 0.08772,2',3,4,6,6'-HxCB 145 ND D 0.06992,2',3,4',5,5'-HxCB 146 D 3.89 0.0550 1.28 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 1.56 0.0548 1.85 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.08912,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.06632,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.06212,2',4,4',5,5'-HxCB 153 153 + 168 C D 24.3 0.0472 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 0.724 0.0425 1.06 0.9382,3,3',4,5,5'-HxCB 159 ND D 0.04512,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.04412,3,3',4',5,5'-HxCB 162 NDR D 0.080 0.0470 0.21 0.9882,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 0.342 0.0458 1.13 0.9212,3,3',5,5',6-HxCB 165 ND D 0.04982,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 D 1.59 0.0385 1.05 1.000

2,2',3,3',4,4',5-HpCB 170 D 17.8 0.101 0.98 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C NDR D 1.45 0.105 1.60 1.1622,2',3,3',4,5,5'-HpCB 172 D 2.71 0.105 0.97 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 0.238 0.0987 3.39 1.1332,2',3,3',4,5',6-HpCB 175 ND D 0.09542,2',3,3',4,6,6'-HpCB 176 ND D 0.07152,2',3,3',4',5,6-HpCB 177 D 2.59 0.0976 1.04 1.1462,2',3,3',5,5',6-HpCB 178 D 2.54 0.0977 1.07 1.0852,2',3,3',5,6,6'-HpCB 179 ND D 0.06952,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 38.6 0.0837 1.03 0.9102,2',3,4,4',5,6-HpCB 181 ND D 0.09932,2',3,4,4',5,6'-HpCB 182 D 1.46 0.0955 1.17 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 4.33 0.0949 1.00 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 0.06982,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.07672,2',3,4',5,5',6-HpCB 187 D 11.7 0.0918 1.06 1.1102,2',3,4',5,6,6'-HpCB 188 D 1.06 0.0601 0.92 1.0012,3,3',4,4',5,5'-HpCB 189 D 2.47 0.0489 1.03 1.0002,3,3',4,4',5,6-HpCB 190 D 3.21 0.0767 1.20 0.9472,3,3',4,4',5',6-HpCB 191 ND D 0.07732,3,3',4,5,5',6-HpCB 192 ND D 0.08562,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 9.11 0.0670 0.89 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 1.40 0.0783 1.05 0.9442,2',3,3',4,4',5,6'-OcCB 196 D 4.39 0.115 0.80 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.09052,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 12.4 0.120 0.91 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.172 0.0903 0.37 1.0222,2',3,3',5,5',6,6'-OcCB 202 D 2.05 0.0952 0.89 1.0002,2',3,4,4',5,5',6-OcCB 203 D 4.60 0.110 0.99 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 0.09252,3,3',4,4',5,5',6-OcCB 205 D 1.74 0.0595 0.91 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 2.25 0.394 0.98 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 0.3232,2',3,3',4,5,5',6,6'-NoCB 208 D 1.61 0.312 0.87 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 1.73 0.0542 0.83 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 64.7 13.0 11.08 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 4850 12.8 1.29 0.9282,2',3,3',4,5'-HxCB 130 NDR D 212 16.0 1.48 0.9132,2',3,3',4,6-HxCB 131 ND D 14.42,2',3,3',4,6'-HxCB 132 NDR D 38.7 15.8 0.44 1.1752,2',3,3',5,5'-HxCB 133 NDR D 116 14.2 1.71 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 14.62,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C NDR D 495 20.7 1.57 1.1032,2',3,3',6,6'-HxCB 136 ND D 15.72,2',3,4,4',5-HxCB 137 NDR D 172 15.0 1.75 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 13.52,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 NDR D 128 13.9 2.38 0.9032,2',3,4,5,6-HxCB 142 ND D 14.92,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 21.12,2',3,4,6,6'-HxCB 145 ND D 16.82,2',3,4',5,5'-HxCB 146 D 935 13.2 1.28 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 375 13.2 1.85 1.1332,2',3,4',5,6'-HxCB 148 ND D 21.42,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 15.92,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 14.92,2',4,4',5,5'-HxCB 153 153 + 168 C D 5840 11.3 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 174 10.2 1.06 0.9382,3,3',4,5,5'-HxCB 159 ND D 10.82,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 10.62,3,3',4',5,5'-HxCB 162 NDR D 19.2 11.3 0.21 0.9882,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 82.2 11.0 1.13 0.9212,3,3',5,5',6-HxCB 165 ND D 12.02,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 X2,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 D 382 9.25 1.05 1.000

2,2',3,3',4,4',5-HpCB 170 D 4280 24.3 0.98 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C NDR D 348 25.2 1.60 1.1622,2',3,3',4,5,5'-HpCB 172 D 651 25.2 0.97 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 57.2 23.7 3.39 1.1332,2',3,3',4,5',6-HpCB 175 ND D 22.92,2',3,3',4,6,6'-HpCB 176 ND D 17.22,2',3,3',4',5,6-HpCB 177 D 622 23.5 1.04 1.1462,2',3,3',5,5',6-HpCB 178 D 610 23.5 1.07 1.0852,2',3,3',5,6,6'-HpCB 179 ND D 16.72,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 9280 20.1 1.03 0.9102,2',3,4,4',5,6-HpCB 181 ND D 23.92,2',3,4,4',5,6'-HpCB 182 D 351 23.0 1.17 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 1040 22.8 1.00 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 16.82,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 18.42,2',3,4',5,5',6-HpCB 187 D 2810 22.1 1.06 1.1102,2',3,4',5,6,6'-HpCB 188 D 255 14.4 0.92 1.0012,3,3',4,4',5,5'-HpCB 189 D 594 11.8 1.03 1.0002,3,3',4,4',5,6-HpCB 190 D 772 18.4 1.20 0.9472,3,3',4,4',5',6-HpCB 191 ND D 18.62,3,3',4,5,5',6-HpCB 192 ND D 20.62,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 2190 16.1 0.89 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 336 18.8 1.05 0.9442,2',3,3',4,4',5,6'-OcCB 196 D 1060 27.6 0.80 0.9152,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 21.82,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 2980 28.8 0.91 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 41.3 21.7 0.37 1.0222,2',3,3',5,5',6,6'-OcCB 202 D 493 22.9 0.89 1.0002,2',3,4,4',5,5',6-OcCB 203 D 1110 26.4 0.99 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND D 22.22,3,3',4,4',5,5',6-OcCB 205 D 418 14.3 0.91 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 541 94.7 0.98 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 77.62,2',3,3',4,5,5',6,6'-NoCB 208 D 387 75.0 0.87 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 416 13.0 0.83 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 562 28.1 3.24 0.71813C12-4-MoCB 3L 2000 667 33.3 3.15 0.858

13C12-2,2'-DiCB 4L 2000 901 45.1 1.60 0.87413C12-4,4'-DiCB 15L 2000 1160 57.9 1.63 1.255

13C12-2,2',6-TriCB 19L 2000 1150 57.7 1.03 1.07213C12-3,4,4'-TriCB 37L 2000 1340 66.9 1.05 1.092



13C12-2,2',4,4',6,6'-HxCB 155L 2000 1700 85.1 1.22 0.78613C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 2000 1580 78.8 1.23 1.07813C12-3,3',4,4',5,5'-HxCB 169L X


13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1930 96.7 1.04 0.92413C12-2,3,3',5,5'-PeCB 111L 2000 1960 98.2 1.63 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X




13C12-2,2',4,4',6,6'-HxCB 155L X13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L X13C12-3,3',4,4',5,5'-HxCB 169L D 2000 2160 108 1.20 1.191

13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 1950 97.6 1.07 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 1750 87.3 0.99 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1270 63.3 1.11 0.71113C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 1840 92.2 1.13 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1330 66.7 0.89 0.81713C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1450 72.5 0.90 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1680 83.9 0.76 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 1880 93.9 0.80 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1750 87.6 1.17 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2170 108 1.02 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 0.908 0.0417 3.12 1.0003-MoCB 2 ND 0.04374-MoCB 3 1.07 0.0515 3.35 1.000


2,2',3-TriCB 16 0.057 0.0363 0.96 1.1652,2',4-TriCB 17 NDR 0.047 0.0324 0.72 1.1382,2',5-TriCB 18 18 + 30 C 0.942 0.0273 1.11 1.1142,2',6-TriCB 19 1.08 0.0359 1.11 1.0012,3,3'-TriCB 20 20 + 28 C 3.64 0.0223 1.08 0.8482,3,4-TriCB 21 21 + 33 C 0.112 0.0219 1.11 0.8562,3,4'-TriCB 22 NDR 0.056 0.0245 1.28 0.8712,3,5-TriCB 23 1.09 0.0239 1.06 1.2832,3,6-TriCB 24 ND 0.02382,3',4-TriCB 25 ND 0.02012,3',5-TriCB 26 26 + 29 C 0.056 0.0228 0.89 1.3002,3',6-TriCB 27 ND 0.02312,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1.37 0.0210 1.03 0.8362,4',6-TriCB 32 0.035 0.0218 1.08 1.1972',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 1.12 0.0235 1.04 1.2733,3',4-TriCB 35 ND 0.02153,3',5-TriCB 36 ND 0.02183,4,4'-TriCB 37 1.51 0.0265 1.07 1.0013,4,5-TriCB 38 ND 0.0217


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.02212,2',3,3'-TeCB 40 40 + 41 + 71 C 1.15 0.0242 0.83 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 0.036 0.0252 1.45 1.3122,2',3,5-TeCB 43 ND 0.02812,2',3,5'-TeCB 44 44 + 47 + 65 C 2.07 0.0222 0.77 1.2862,2',3,6-TeCB 45 45 + 51 C ND 0.02522,2',3,6'-TeCB 46 ND 0.02832,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.02492,2',4,5'-TeCB 49 49 + 69 C 1.15 0.0211 0.82 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 0.026 0.0244 4.80 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 1.71 0.0227 0.79 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1.17 0.0169 0.84 1.0012,3,3',4-TeCB 55 ND 0.05582,3,3',4'-TeCB 56 1.50 0.0555 0.77 0.9042,3,3',5-TeCB 57 ND 0.05402,3,3',5'-TeCB 58 ND 0.05722,3,3',6-TeCB 59 59 + 62 + 75 C 0.078 0.0185 0.82 1.3032,3,4,4'-TeCB 60 0.699 0.0553 0.81 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 3.84 0.0526 0.80 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 0.053 0.0530 1.42 0.8652,3,4',6-TeCB 64 0.119 0.0178 0.85 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 2.98 0.0509 0.79 0.8852,3',4,5-TeCB 67 ND 0.04902,3',4,5'-TeCB 68 0.108 0.0530 0.75 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.05292,3',5',6-TeCB 73 ND 0.01902,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 1.61 0.0606 0.77 1.0013,3',4,5-TeCB 78 ND 0.05203,3',4,5'-TeCB 79 NDR 0.047 0.0449 0.49 0.9723,3',5,5'-TeCB 80 ND 0.04953,4,4',5-TeCB 81 1.51 0.0595 0.82 1.000

2,2',3,3',4-PeCB 82 ND 0.03492,2',3,3',5-PeCB 83 83 + 99 C 9.14 0.0342 1.52 0.8862,2',3,3',6-PeCB 84 NDR 0.049 0.0369 2.43 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 0.650 0.0271 1.62 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1.45 0.0290 1.63 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.03402,2',3,4,6'-PeCB 89 ND 0.03522,2',3,4',5-PeCB 90 90 + 101 + 113 C 2.76 0.0290 1.61 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 0.438 0.0335 1.43 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 1.76 0.0334 1.53 1.1202,2',3,5,6'-PeCB 94 ND 0.03722,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01212,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.03072,2',4,6,6'-PeCB 104 0.958 0.0116 1.67 1.0012,3,3',4,4'-PeCB 105 5.48 0.0530 1.50 1.0012,3,3',4,5-PeCB 106 ND 0.04432,3,3',4',5-PeCB 107 107 + 124 C ND 0.04742,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 0.287 0.0437 1.67 0.9972,3,3',4',6-PeCB 110 110 + 115 C 2.22 0.0241 1.57 0.9252,3,3',5,5'-PeCB 111 0.040 0.0243 1.69 0.9452,3,3',5,6-PeCB 112 ND 0.02372,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 1.80 0.0494 1.66 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 13.5 0.0498 1.58 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 0.048 0.0231 1.16 0.9582,3',4,5',6-PeCB 121 ND 0.02562',3,3',4,5-PeCB 122 ND 0.04842',3,4,4',5-PeCB 123 1.47 0.0507 1.53 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 1.83 0.0597 1.76 1.0013,3',4,5,5'-PeCB 127 NDR 0.075 0.0445 2.07 1.041







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 2.91 0.0268 1.32 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 252 11.6 3.12 1.0003-MoCB 2 ND 12.14-MoCB 3 296 14.3 3.35 1.000


2,2',3-TriCB 16 15.8 10.1 0.96 1.1652,2',4-TriCB 17 NDR 13.0 8.98 0.72 1.1382,2',5-TriCB 18 18 + 30 C 261 7.56 1.11 1.1142,2',6-TriCB 19 299 9.95 1.11 1.0012,3,3'-TriCB 20 20 + 28 C 1010 6.18 1.08 0.8482,3,4-TriCB 21 21 + 33 C 31.0 6.07 1.11 0.8562,3,4'-TriCB 22 NDR 15.5 6.79 1.28 0.8712,3,5-TriCB 23 302 6.62 1.06 1.2832,3,6-TriCB 24 ND 6.592,3',4-TriCB 25 ND 5.572,3',5-TriCB 26 26 + 29 C 15.5 6.32 0.89 1.3002,3',6-TriCB 27 ND 6.402,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 380 5.82 1.03 0.8362,4',6-TriCB 32 9.70 6.04 1.08 1.1972',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 310 6.51 1.04 1.2733,3',4-TriCB 35 ND 5.963,3',5-TriCB 36 ND 6.043,4,4'-TriCB 37 418 7.34 1.07 1.0013,4,5-TriCB 38 ND 6.01


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 6.122,2',3,3'-TeCB 40 40 + 41 + 71 C 319 6.71 0.83 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 9.98 6.98 1.45 1.3122,2',3,5-TeCB 43 ND 7.792,2',3,5'-TeCB 44 44 + 47 + 65 C 574 6.15 0.77 1.2862,2',3,6-TeCB 45 45 + 51 C ND 6.982,2',3,6'-TeCB 46 ND 7.842,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 6.902,2',4,5'-TeCB 49 49 + 69 C 319 5.85 0.82 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 7.20 6.76 4.80 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 474 6.29 0.79 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 324 4.68 0.84 1.0012,3,3',4-TeCB 55 ND 15.52,3,3',4'-TeCB 56 416 15.4 0.77 0.9042,3,3',5-TeCB 57 ND 15.02,3,3',5'-TeCB 58 ND 15.82,3,3',6-TeCB 59 59 + 62 + 75 C 21.6 5.13 0.82 1.3032,3,4,4'-TeCB 60 194 15.3 0.81 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 1060 14.6 0.80 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 NDR 14.7 14.7 1.42 0.8652,3,4',6-TeCB 64 33.0 4.93 0.85 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 826 14.1 0.79 0.8852,3',4,5-TeCB 67 ND 13.62,3',4,5'-TeCB 68 29.9 14.7 0.75 0.8312,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 14.72,3',5',6-TeCB 73 ND 5.262,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 446 16.8 0.77 1.0013,3',4,5-TeCB 78 ND 14.43,3',4,5'-TeCB 79 NDR 13.0 12.4 0.49 0.9723,3',5,5'-TeCB 80 ND 13.73,4,4',5-TeCB 81 418 16.5 0.82 1.000

2,2',3,3',4-PeCB 82 ND 9.672,2',3,3',5-PeCB 83 83 + 99 C 2530 9.48 1.52 0.8862,2',3,3',6-PeCB 84 NDR 13.6 10.2 2.43 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 180 7.51 1.62 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 402 8.04 1.63 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 9.422,2',3,4,6'-PeCB 89 ND 9.752,2',3,4',5-PeCB 90 90 + 101 + 113 C 765 8.04 1.61 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 121 9.28 1.43 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 488 9.25 1.53 1.1202,2',3,5,6'-PeCB 94 ND 10.32,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 3.352,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 8.512,2',4,6,6'-PeCB 104 265 3.21 1.67 1.0012,3,3',4,4'-PeCB 105 1520 14.7 1.50 1.0012,3,3',4,5-PeCB 106 ND 12.32,3,3',4',5-PeCB 107 107 + 124 C ND 13.12,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 79.5 12.1 1.67 0.9972,3,3',4',6-PeCB 110 110 + 115 C 615 6.68 1.57 0.9252,3,3',5,5'-PeCB 111 11.1 6.73 1.69 0.9452,3,3',5,6-PeCB 112 ND 6.572,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 499 13.7 1.66 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 3740 13.8 1.58 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 13.3 6.40 1.16 0.9582,3',4,5',6-PeCB 121 ND 7.092',3,3',4,5-PeCB 122 ND 13.42',3,4,4',5-PeCB 123 407 14.0 1.53 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 507 16.5 1.76 1.0013,3',4,5,5'-PeCB 127 NDR 20.8 12.3 2.07 1.041







COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 806 7.43 1.32 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 1.36 0.0884 1.51 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 37.3 0.0873 1.32 0.9282,2',3,3',4,5'-HxCB 130 D 0.914 0.109 1.33 0.9132,2',3,3',4,6-HxCB 131 ND D 0.09812,2',3,3',4,6'-HxCB 132 NDR D 0.177 0.108 0.63 1.1752,2',3,3',5,5'-HxCB 133 D 0.594 0.0966 1.06 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.09922,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 2.03 0.106 1.31 1.1042,2',3,3',6,6'-HxCB 136 ND D 0.08042,2',3,4,4',5-HxCB 137 D 1.43 0.102 1.28 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 0.09202,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 D 0.918 0.0948 1.06 0.9032,2',3,4,5,6-HxCB 142 ND D 0.1012,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 0.1082,2',3,4,6,6'-HxCB 145 ND D 0.08612,2',3,4',5,5'-HxCB 146 NDR D 5.25 0.0900 1.05 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 2.05 0.0897 1.57 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.1102,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.08162,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.07642,2',4,4',5,5'-HxCB 153 153 + 168 C D 42.8 0.0773 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 1.69 0.0696 1.18 0.9372,3,3',4,5,5'-HxCB 159 ND D 0.07382,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.07212,3,3',4',5,5'-HxCB 162 ND D 0.07682,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 ND D 0.07502,3,3',5,5',6-HxCB 165 ND D 0.08142,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 25.7 0.111 0.98 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 2.35 0.115 0.97 1.1622,2',3,3',4,5,5'-HpCB 172 D 3.25 0.116 1.17 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 0.412 0.109 1.29 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 0.469 0.105 1.44 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 0.07862,2',3,3',4',5,6-HpCB 177 D 5.49 0.107 1.03 1.1452,2',3,3',5,5',6-HpCB 178 D 2.85 0.107 1.07 1.0852,2',3,3',5,6,6'-HpCB 179 NDR D 0.181 0.0764 3.16 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 55.9 0.0920 1.03 0.9102,2',3,4,4',5,6-HpCB 181 ND D 0.1092,2',3,4,4',5,6'-HpCB 182 NDR D 1.10 0.105 1.60 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 9.02 0.104 0.96 1.1262,2',3,4,4',6,6'-HpCB 184 ND D 0.07672,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.08442,2',3,4',5,5',6-HpCB 187 D 19.4 0.101 1.04 1.1102,2',3,4',5,6,6'-HpCB 188 NDR D 0.596 0.0641 0.88 1.0012,3,3',4,4',5,5'-HpCB 189 D 2.01 0.0567 0.90 1.0012,3,3',4,4',5,6-HpCB 190 D 5.34 0.0843 1.16 0.9462,3,3',4,4',5',6-HpCB 191 D 1.34 0.0850 1.12 0.9172,3,3',4,5,5',6-HpCB 192 ND D 0.09412,3,3',4',5,5',6-HpCB 193 180 + 193 C180


2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 1.92 0.452 0.61 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 0.3692,2',3,3',4,5,5',6,6'-NoCB 208 D 1.35 0.357 0.85 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 1.36 0.0793 0.93 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 377 24.5 1.51 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 10300 24.2 1.32 0.9282,2',3,3',4,5'-HxCB 130 D 253 30.2 1.33 0.9132,2',3,3',4,6-HxCB 131 ND D 27.22,2',3,3',4,6'-HxCB 132 NDR D 49.0 29.9 0.63 1.1752,2',3,3',5,5'-HxCB 133 D 165 26.8 1.06 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 27.52,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 562 29.4 1.31 1.1042,2',3,3',6,6'-HxCB 136 ND D 22.32,2',3,4,4',5-HxCB 137 D 396 28.3 1.28 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 25.52,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 D 254 26.3 1.06 0.9032,2',3,4,5,6-HxCB 142 ND D 28.02,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 29.92,2',3,4,6,6'-HxCB 145 ND D 23.92,2',3,4',5,5'-HxCB 146 NDR D 1450 24.9 1.05 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 568 24.9 1.57 1.1332,2',3,4',5,6'-HxCB 148 ND D 30.52,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 22.62,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 21.22,2',4,4',5,5'-HxCB 153 153 + 168 C D 11900 21.4 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 468 19.3 1.18 0.9372,3,3',4,5,5'-HxCB 159 ND D 20.42,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 20.02,3,3',4',5,5'-HxCB 162 ND D 21.32,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 ND D 20.82,3,3',5,5',6-HxCB 165 ND D 22.62,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 7120 30.8 0.98 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 651 31.9 0.97 1.1622,2',3,3',4,5,5'-HpCB 172 D 901 32.1 1.17 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 114 30.2 1.29 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 130 29.1 1.44 1.1022,2',3,3',4,6,6'-HpCB 176 ND D 21.82,2',3,3',4',5,6-HpCB 177 D 1520 29.6 1.03 1.1452,2',3,3',5,5',6-HpCB 178 D 790 29.6 1.07 1.0852,2',3,3',5,6,6'-HpCB 179 NDR D 50.2 21.2 3.16 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 15500 25.5 1.03 0.9102,2',3,4,4',5,6-HpCB 181 ND D 30.22,2',3,4,4',5,6'-HpCB 182 NDR D 305 29.1 1.60 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C D 2500 28.8 0.96 1.1262,2',3,4,4',6,6'-HpCB 184 ND D 21.32,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 23.42,2',3,4',5,5',6-HpCB 187 D 5380 28.0 1.04 1.1102,2',3,4',5,6,6'-HpCB 188 NDR D 165 17.8 0.88 1.0012,3,3',4,4',5,5'-HpCB 189 D 557 15.7 0.90 1.0012,3,3',4,4',5,6-HpCB 190 D 1480 23.4 1.16 0.9462,3,3',4,4',5',6-HpCB 191 D 371 23.6 1.12 0.9172,3,3',4,5,5',6-HpCB 192 ND D 26.12,3,3',4',5,5',6-HpCB 193 180 + 193 C180


2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 532 125 0.61 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 1022,2',3,3',4,5,5',6,6'-NoCB 208 D 374 98.9 0.85 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 377 22.0 0.93 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 646 32.3 3.16 0.71813C12-4-MoCB 3L 2000 745 37.2 3.23 0.858

13C12-2,2'-DiCB 4L 2000 1010 50.6 1.64 0.87313C12-4,4'-DiCB 15L 2000 1380 69.0 1.63 1.254

13C12-2,2',6-TriCB 19L 2000 1250 62.7 1.04 1.07213C12-3,4,4'-TriCB 37L 2000 1480 74.1 1.04 1.091





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1910 95.7 1.06 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1920 96.1 1.61 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X





13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 2230 112 0.97 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 2060 103 0.98 0.87113C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1390 69.6 1.10 0.71113C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 1800 89.9 0.97 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1460 73.2 0.82 0.81613C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1430 71.4 0.85 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1600 80.0 0.85 1.04313C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 1950 97.4 0.81 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1690 84.5 1.19 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2330 117 1.03 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 NDR 0.066 0.0542 4.89 1.0013-MoCB 2 ND 0.05574-MoCB 3 ND 0.0640

2,2'-DiCB 4 ND 0.1432,3-DiCB 5 ND 0.09582,3'-DiCB 6 ND 0.08562,4-DiCB 7 ND 0.09112,4'-DiCB 8 NDR 0.143 0.0785 1.80 1.2092,5-DiCB 9 ND 0.08852,6-DiCB 10 ND 0.09653,3'-DiCB 11 0.581 0.0848 1.73 0.9703,4-DiCB 12 12 + 13 C ND 0.08463,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.08494,4'-DiCB 15 ND 0.0922

2,2',3-TriCB 16 NDR 0.117 0.0469 0.76 1.1662,2',4-TriCB 17 0.082 0.0418 1.16 1.1382,2',5-TriCB 18 18 + 30 C 0.212 0.0352 0.91 1.1142,2',6-TriCB 19 ND 0.04492,3,3'-TriCB 20 20 + 28 C 5.37 0.0378 1.01 0.8472,3,4-TriCB 21 21 + 33 C 0.225 0.0372 1.07 0.8562,3,4'-TriCB 22 ND 0.04162,3,5-TriCB 23 ND 0.04052,3,6-TriCB 24 ND 0.03082,3',4-TriCB 25 ND 0.03412,3',5-TriCB 26 26 + 29 C NDR 0.067 0.0388 0.69 1.3022,3',6-TriCB 27 ND 0.02982,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 0.355 0.0357 1.02 0.8362,4',6-TriCB 32 NDR 0.073 0.0371 0.82 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 0.03983,3',4-TriCB 35 ND 0.03653,3',5-TriCB 36 ND 0.03703,4,4'-TriCB 37 NDR 0.066 0.0463 1.23 1.0013,4,5-TriCB 38 ND 0.0369


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.03762,2',3,3'-TeCB 40 40 + 41 + 71 C 0.129 0.0362 0.83 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.108 0.0376 0.75 1.3122,2',3,5-TeCB 43 ND 0.04202,2',3,5'-TeCB 44 44 + 47 + 65 C 0.723 0.0333 0.87 1.2872,2',3,6-TeCB 45 45 + 51 C ND 0.03762,2',3,6'-TeCB 46 ND 0.04232,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.03722,2',4,5'-TeCB 49 49 + 69 C 0.199 0.0315 0.79 1.2602,2',4,6-TeCB 50 50 + 53 C ND 0.03642,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 0.648 0.0340 0.87 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 0.02372,3,3',4-TeCB 55 ND 0.06732,3,3',4'-TeCB 56 ND 0.06692,3,3',5-TeCB 57 ND 0.06522,3,3',5'-TeCB 58 ND 0.06902,3,3',6-TeCB 59 59 + 62 + 75 C 0.088 0.0276 0.89 1.3022,3,4,4'-TeCB 60 0.704 0.0667 0.79 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 4.17 0.0635 0.78 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 0.06402,3,4',6-TeCB 64 0.196 0.0266 0.70 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 1.90 0.0614 0.75 0.8852,3',4,5-TeCB 67 ND 0.05912,3',4,5'-TeCB 68 ND 0.06402,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.06392,3',5',6-TeCB 73 ND 0.02842,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 ND 0.07833,3',4,5-TeCB 78 ND 0.06273,3',4,5'-TeCB 79 ND 0.05413,3',5,5'-TeCB 80 ND 0.05973,4,4',5-TeCB 81 ND 0.0702

2,2',3,3',4-PeCB 82 ND 0.03032,2',3,3',5-PeCB 83 83 + 99 C 4.50 0.0297 1.57 0.8862,2',3,3',6-PeCB 84 NDR 0.061 0.0321 2.23 1.1642,2',3,4,4'-PeCB 85 85 + 116 + 117 C 0.316 0.0236 1.72 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 0.211 0.0252 1.71 0.9012,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.02952,2',3,4,6'-PeCB 89 ND 0.03062,2',3,4',5-PeCB 90 90 + 101 + 113 C 0.777 0.0252 1.47 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 0.245 0.0291 1.21 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 0.503 0.0290 1.45 1.1212,2',3,5,6'-PeCB 94 ND 0.03242,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01812,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.02672,2',4,6,6'-PeCB 104 ND 0.01512,3,3',4,4'-PeCB 105 2.64 0.0605 1.53 1.0002,3,3',4,5-PeCB 106 ND 0.04962,3,3',4',5-PeCB 107 107 + 124 C ND 0.05312,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 0.176 0.0490 0.99 0.9972,3,3',4',6-PeCB 110 110 + 115 C 0.562 0.0210 1.64 0.9252,3,3',5,5'-PeCB 111 NDR 0.023 0.0211 2.21 0.9452,3,3',5,6-PeCB 112 ND 0.02062,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 0.400 0.0559 1.68 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 8.25 0.0563 1.59 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 0.02002,3',4,5',6-PeCB 121 0.038 0.0222 1.68 1.1992',3,3',4,5-PeCB 122 ND 0.05432',3,4,4',5-PeCB 123 0.133 0.0555 1.70 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 ND 0.06913,3',4,5,5'-PeCB 127 ND 0.0499

2,2',3,3',4,4'-HxCB 128 128 + 166 C 1.06 0.0186 1.23 0.9602,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 23.1 0.0191 1.26 0.9292,2',3,3',4,5'-HxCB 130 0.837 0.0246 1.26 0.9132,2',3,3',4,6-HxCB 131 ND 0.02382,2',3,3',4,6'-HxCB 132 0.252 0.0247 1.24 1.1742,2',3,3',5,5'-HxCB 133 NDR 0.481 0.0220 1.55 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND 0.02352,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 0.807 0.0180 1.25 1.1032,2',3,3',6,6'-HxCB 136 0.054 0.0142 1.18 1.0232,2',3,4,4',5-HxCB 137 1.11 0.0226 1.29 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR 0.086 0.0215 1.52 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 0.405 0.0213 1.40 0.9042,2',3,4,5,6-HxCB 142 ND 0.02442,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND 0.01842,2',3,4,6,6'-HxCB 145 ND 0.01562,2',3,4',5,5'-HxCB 146 3.73 0.0199 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 0.559 0.0217 1.12 1.1332,2',3,4',5,6'-HxCB 148 ND 0.01832,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 0.01442,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 0.01372,2',4,4',5,5'-HxCB 153 153 + 168 C 29.2 0.0175 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 0.020 0.0117 1.18 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 3.35 0.0196 1.28 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 0.978 0.0154 1.23 0.9382,3,3',4,5,5'-HxCB 159 NDR 0.023 0.0153 0.87 0.9812,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 0.01692,3,3',4',5,5'-HxCB 162 ND 0.01542,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 0.184 0.0166 1.23 0.9212,3,3',5,5',6-HxCB 165 NDR 0.028 0.0184 2.03 0.8782,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2'-DiCB 4 ND 42.42,3-DiCB 5 ND 28.42,3'-DiCB 6 ND 25.42,4-DiCB 7 ND 27.02,4'-DiCB 8 NDR 42.4 23.3 1.80 1.2092,5-DiCB 9 ND 26.32,6-DiCB 10 ND 28.63,3'-DiCB 11 172 25.2 1.73 0.9703,4-DiCB 12 12 + 13 C ND 25.13,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 25.24,4'-DiCB 15 ND 27.4

2,2',3-TriCB 16 NDR 34.7 13.9 0.76 1.1662,2',4-TriCB 17 24.3 12.4 1.16 1.1382,2',5-TriCB 18 18 + 30 C 62.9 10.4 0.91 1.1142,2',6-TriCB 19 ND 13.32,3,3'-TriCB 20 20 + 28 C 1590 11.2 1.01 0.8472,3,4-TriCB 21 21 + 33 C 66.8 11.0 1.07 0.8562,3,4'-TriCB 22 ND 12.32,3,5-TriCB 23 ND 12.02,3,6-TriCB 24 ND 9.142,3',4-TriCB 25 ND 10.12,3',5-TriCB 26 26 + 29 C NDR 19.9 11.5 0.69 1.3022,3',6-TriCB 27 ND 8.842,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 105 10.6 1.02 0.8362,4',6-TriCB 32 NDR 21.7 11.0 0.82 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 11.83,3',4-TriCB 35 ND 10.83,3',5-TriCB 36 ND 11.03,4,4'-TriCB 37 NDR 19.6 13.7 1.23 1.0013,4,5-TriCB 38 ND 10.9


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 11.22,2',3,3'-TeCB 40 40 + 41 + 71 C 38.3 10.7 0.83 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 32.0 11.2 0.75 1.3122,2',3,5-TeCB 43 ND 12.52,2',3,5'-TeCB 44 44 + 47 + 65 C 215 9.88 0.87 1.2872,2',3,6-TeCB 45 45 + 51 C ND 11.22,2',3,6'-TeCB 46 ND 12.62,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 11.02,2',4,5'-TeCB 49 49 + 69 C 59.1 9.35 0.79 1.2602,2',4,6-TeCB 50 50 + 53 C ND 10.82,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 192 10.1 0.87 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 7.032,3,3',4-TeCB 55 ND 20.02,3,3',4'-TeCB 56 ND 19.92,3,3',5-TeCB 57 ND 19.32,3,3',5'-TeCB 58 ND 20.52,3,3',6-TeCB 59 59 + 62 + 75 C 26.1 8.19 0.89 1.3022,3,4,4'-TeCB 60 209 19.8 0.79 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 1240 18.8 0.78 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 19.02,3,4',6-TeCB 64 58.2 7.89 0.70 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 564 18.2 0.75 0.8852,3',4,5-TeCB 67 ND 17.52,3',4,5'-TeCB 68 ND 19.02,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 19.02,3',5',6-TeCB 73 ND 8.432,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 ND 23.23,3',4,5-TeCB 78 ND 18.63,3',4,5'-TeCB 79 ND 16.13,3',5,5'-TeCB 80 ND 17.73,4,4',5-TeCB 81 ND 20.8

2,2',3,3',4-PeCB 82 ND 8.992,2',3,3',5-PeCB 83 83 + 99 C 1340 8.81 1.57 0.8862,2',3,3',6-PeCB 84 NDR 18.1 9.53 2.23 1.1642,2',3,4,4'-PeCB 85 85 + 116 + 117 C 93.8 7.00 1.72 0.9192,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 62.6 7.48 1.71 0.9012,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 8.752,2',3,4,6'-PeCB 89 ND 9.082,2',3,4',5-PeCB 90 90 + 101 + 113 C 231 7.48 1.47 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 72.7 8.64 1.21 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 149 8.61 1.45 1.1212,2',3,5,6'-PeCB 94 ND 9.612,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 5.372,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 7.922,2',4,6,6'-PeCB 104 ND 4.482,3,3',4,4'-PeCB 105 783 18.0 1.53 1.0002,3,3',4,5-PeCB 106 ND 14.72,3,3',4',5-PeCB 107 107 + 124 C ND 15.82,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 52.2 14.5 0.99 0.9972,3,3',4',6-PeCB 110 110 + 115 C 167 6.23 1.64 0.9252,3,3',5,5'-PeCB 111 NDR 6.83 6.26 2.21 0.9452,3,3',5,6-PeCB 112 ND 6.112,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 119 16.6 1.68 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 2450 16.7 1.59 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 5.932,3',4,5',6-PeCB 121 11.3 6.59 1.68 1.1992',3,3',4,5-PeCB 122 ND 16.12',3,4,4',5-PeCB 123 39.5 16.5 1.70 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 ND 20.53,3',4,5,5'-PeCB 127 ND 14.8

2,2',3,3',4,4'-HxCB 128 128 + 166 C 315 5.52 1.23 0.9602,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 6850 5.67 1.26 0.9292,2',3,3',4,5'-HxCB 130 248 7.30 1.26 0.9132,2',3,3',4,6-HxCB 131 ND 7.062,2',3,3',4,6'-HxCB 132 74.8 7.33 1.24 1.1742,2',3,3',5,5'-HxCB 133 NDR 143 6.53 1.55 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND 6.972,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 239 5.34 1.25 1.1032,2',3,3',6,6'-HxCB 136 16.0 4.21 1.18 1.0232,2',3,4,4',5-HxCB 137 329 6.71 1.29 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR 25.5 6.38 1.52 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 120 6.32 1.40 0.9042,2',3,4,5,6-HxCB 142 ND 7.242,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND 5.462,2',3,4,6,6'-HxCB 145 ND 4.632,2',3,4',5,5'-HxCB 146 1110 5.91 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 166 6.44 1.12 1.1332,2',3,4',5,6'-HxCB 148 ND 5.432,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 4.272,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 4.072,2',4,4',5,5'-HxCB 153 153 + 168 C 8660 5.19 1.28 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 5.93 3.47 1.18 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 994 5.82 1.28 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 290 4.57 1.23 0.9382,3,3',4,5,5'-HxCB 159 NDR 6.83 4.54 0.87 0.9812,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 5.012,3,3',4',5,5'-HxCB 162 ND 4.572,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 54.6 4.93 1.23 0.9212,3,3',5,5',6-HxCB 165 NDR 8.31 5.46 2.03 0.8782,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 332 4.42 1.08 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 ND 32.6




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT









COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 8.68 0.0854 1.06 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C NDR D 0.872 0.0887 1.43 1.1622,2',3,3',4,5,5'-HpCB 172 D 1.53 0.0891 0.90 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 0.245 0.0836 1.02 1.1342,2',3,3',4,5',6-HpCB 175 D 0.157 0.0808 0.93 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 0.06062,2',3,3',4',5,6-HpCB 177 D 1.93 0.0827 1.11 1.1452,2',3,3',5,5',6-HpCB 178 D 1.33 0.0827 1.08 1.0852,2',3,3',5,6,6'-HpCB 179 NDR D 0.069 0.0588 1.79 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 22.6 0.0709 1.08 0.9102,2',3,4,4',5,6-HpCB 181 ND D 0.08412,2',3,4,4',5,6'-HpCB 182 ND D 0.08092,2',3,4,4',5',6-HpCB 183 183 + 185 C D 3.43 0.0804 1.03 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 0.05912,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.06502,2',3,4',5,5',6-HpCB 187 D 7.70 0.0777 1.04 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 0.05782,3,3',4,4',5,5'-HpCB 189 NDR D 0.548 0.0591 0.72 1.0002,3,3',4,4',5,6-HpCB 190 D 1.75 0.0650 0.91 0.9472,3,3',4,4',5',6-HpCB 191 D 0.468 0.0655 0.92 0.9182,3,3',4,5,5',6-HpCB 192 ND D 0.07252,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 4.81 0.0681 0.95 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 1.61 0.0797 1.19 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 2.18 0.0873 0.79 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C NDR D 0.127 0.0690 0.54 1.0452,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 5.26 0.0912 0.89 1.1142,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.082 0.0688 0.06 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 0.883 0.0804 0.77 1.0002,2',3,4,4',5,5',6-OcCB 203 D 4.19 0.0837 0.82 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 0.07052,3,3',4,4',5,5',6-OcCB 205 NDR D 0.171 0.0577 1.36 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 0.935 0.517 1.47 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 0.4302,2',3,3',4,5,5',6,6'-NoCB 208 ND D 0.421

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 0.597 0.0563 0.90 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT









COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 2580 25.3 1.06 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C NDR D 259 26.3 1.43 1.1622,2',3,3',4,5,5'-HpCB 172 D 454 26.4 0.90 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 D 72.7 24.8 1.02 1.1342,2',3,3',4,5',6-HpCB 175 D 46.6 24.0 0.93 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 18.02,2',3,3',4',5,6-HpCB 177 D 573 24.5 1.11 1.1452,2',3,3',5,5',6-HpCB 178 D 395 24.5 1.08 1.0852,2',3,3',5,6,6'-HpCB 179 NDR D 20.5 17.4 1.79 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 6710 21.0 1.08 0.9102,2',3,4,4',5,6-HpCB 181 ND D 25.02,2',3,4,4',5,6'-HpCB 182 ND D 24.02,2',3,4,4',5',6-HpCB 183 183 + 185 C D 1020 23.9 1.03 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 17.52,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 19.32,2',3,4',5,5',6-HpCB 187 D 2280 23.1 1.04 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 17.22,3,3',4,4',5,5'-HpCB 189 NDR D 163 17.5 0.72 1.0002,3,3',4,4',5,6-HpCB 190 D 519 19.3 0.91 0.9472,3,3',4,4',5',6-HpCB 191 D 139 19.4 0.92 0.9182,3,3',4,5,5',6-HpCB 192 ND D 21.52,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 1430 20.2 0.95 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 478 23.7 1.19 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 647 25.9 0.79 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C NDR D 37.7 20.5 0.54 1.0452,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 1560 27.1 0.89 1.1142,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 24.3 20.4 0.06 1.0232,2',3,3',5,5',6,6'-OcCB 202 D 262 23.9 0.77 1.0002,2',3,4,4',5,5',6-OcCB 203 D 1240 24.8 0.82 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 20.92,3,3',4,4',5,5',6-OcCB 205 NDR D 50.7 17.1 1.36 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 NDR D 277 153 1.47 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 1282,2',3,3',4,5,5',6,6'-NoCB 208 ND D 125

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 177 16.7 0.90 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 457 22.9 3.21 0.71813C12-4-MoCB 3L 2000 597 29.8 3.11 0.858

13C12-2,2'-DiCB 4L 2000 803 40.1 1.62 0.87313C12-4,4'-DiCB 15L 2000 1240 61.8 1.65 1.255

13C12-2,2',6-TriCB 19L 2000 1160 57.8 1.04 1.07213C12-3,4,4'-TriCB 37L 2000 1380 68.8 1.06 1.092





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1780 89.2 1.02 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1870 93.3 1.62 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X




13C12-2,2',4,4',6,6'-HxCB 155L X13C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C X13C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L X13C12-3,3',4,4',5,5'-HxCB 169L X


13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1310 65.4 0.86 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1690 84.6 0.85 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1770 88.4 0.84 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 1970 98.3 0.78 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1990 99.3 1.28 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2390 120 0.99 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2'-DiCB 4 ND 0.08872,3-DiCB 5 ND 0.06382,3'-DiCB 6 ND 0.05712,4-DiCB 7 ND 0.06072,4'-DiCB 8 NDR 0.089 0.0523 1.24 1.2082,5-DiCB 9 ND 0.05902,6-DiCB 10 ND 0.06433,3'-DiCB 11 0.648 0.0565 1.75 0.9703,4-DiCB 12 12 + 13 C ND 0.05643,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.05664,4'-DiCB 15 ND 0.0635

2,2',3-TriCB 16 NDR 0.043 0.0357 1.38 1.1672,2',4-TriCB 17 NDR 0.061 0.0318 1.51 1.1392,2',5-TriCB 18 18 + 30 C NDR 0.091 0.0268 1.51 1.1132,2',6-TriCB 19 ND 0.03242,3,3'-TriCB 20 20 + 28 C 1.76 0.0263 1.09 0.8472,3,4-TriCB 21 21 + 33 C NDR 0.080 0.0259 1.26 0.8562,3,4'-TriCB 22 NDR 0.030 0.0290 0.66 0.8722,3,5-TriCB 23 ND 0.02822,3,6-TriCB 24 ND 0.02342,3',4-TriCB 25 ND 0.02372,3',5-TriCB 26 26 + 29 C ND 0.02702,3',6-TriCB 27 ND 0.02272,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 0.109 0.0249 0.89 0.8362,4',6-TriCB 32 ND 0.02582',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 0.02773,3',4-TriCB 35 ND 0.02543,3',5-TriCB 36 ND 0.02573,4,4'-TriCB 37 ND 0.03303,4,5-TriCB 38 ND 0.0257


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.02622,2',3,3'-TeCB 40 40 + 41 + 71 C 0.069 0.0235 0.72 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 0.042 0.0245 0.62 1.3122,2',3,5-TeCB 43 ND 0.02732,2',3,5'-TeCB 44 44 + 47 + 65 C 0.541 0.0216 0.83 1.2872,2',3,6-TeCB 45 45 + 51 C 0.086 0.0245 0.89 1.1482,2',3,6'-TeCB 46 ND 0.02752,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.02422,2',4,5'-TeCB 49 49 + 69 C NDR 0.102 0.0205 0.93 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 0.029 0.0237 0.40 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 0.428 0.0221 0.78 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 0.01552,3,3',4-TeCB 55 ND 0.05802,3,3',4'-TeCB 56 ND 0.05762,3,3',5-TeCB 57 ND 0.05622,3,3',5'-TeCB 58 ND 0.05942,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.040 0.0180 1.30 1.3022,3,4,4'-TeCB 60 0.578 0.0574 0.74 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 5.14 0.0547 0.78 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 0.05512,3,4',6-TeCB 64 0.077 0.0173 0.67 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 0.02602,2',3,3',5-PeCB 83 83 + 99 C 8.34 0.0255 1.61 0.8862,2',3,3',6-PeCB 84 NDR 0.031 0.0275 0.85 1.1622,2',3,4,4'-PeCB 85 85 + 116 + 117 C 0.512 0.0203 1.54 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 0.241 0.0217 1.65 0.9012,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C NDR 0.036 0.0254 2.25 1.1542,2',3,4,6'-PeCB 89 ND 0.02632,2',3,4',5-PeCB 90 90 + 101 + 113 C 0.951 0.0216 1.63 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 0.412 0.0250 1.55 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 0.559 0.0249 1.47 1.1202,2',3,5,6'-PeCB 94 ND 0.02782,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01482,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.02292,2',4,6,6'-PeCB 104 ND 0.01262,3,3',4,4'-PeCB 105 4.60 0.0624 1.62 1.0002,3,3',4,5-PeCB 106 ND 0.05242,3,3',4',5-PeCB 107 107 + 124 C ND 0.05622,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 0.272 0.0518 1.42 0.9972,3,3',4',6-PeCB 110 110 + 115 C 0.715 0.0180 1.59 0.9262,3,3',5,5'-PeCB 111 NDR 0.029 0.0181 0.73 0.9462,3,3',5,6-PeCB 112 ND 0.01772,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 0.822 0.0588 1.35 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 17.2 0.0598 1.57 1.0012,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 0.01722,3',4,5',6-PeCB 121 ND 0.01912',3,3',4,5-PeCB 122 ND 0.05742',3,4,4',5-PeCB 123 NDR 0.248 0.0595 2.26 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 NDR 0.095 0.0739 1.02 1.0003,3',4,5,5'-PeCB 127 NDR 0.081 0.0527 2.05 1.041

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 ND 0.01162,3,3',4,4',5-HxCB 156 156 + 157 C 8.79 0.0500 1.21 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 3.02 0.0377 1.26 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2'-DiCB 4 ND 25.12,3-DiCB 5 ND 18.12,3'-DiCB 6 ND 16.22,4-DiCB 7 ND 17.22,4'-DiCB 8 NDR 25.2 14.8 1.24 1.2082,5-DiCB 9 ND 16.72,6-DiCB 10 ND 18.23,3'-DiCB 11 184 16.0 1.75 0.9703,4-DiCB 12 12 + 13 C ND 16.03,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 16.04,4'-DiCB 15 ND 18.0

2,2',3-TriCB 16 NDR 12.2 10.1 1.38 1.1672,2',4-TriCB 17 NDR 17.3 9.01 1.51 1.1392,2',5-TriCB 18 18 + 30 C NDR 25.8 7.59 1.51 1.1132,2',6-TriCB 19 ND 9.182,3,3'-TriCB 20 20 + 28 C 498 7.45 1.09 0.8472,3,4-TriCB 21 21 + 33 C NDR 22.7 7.33 1.26 0.8562,3,4'-TriCB 22 NDR 8.50 8.21 0.66 0.8722,3,5-TriCB 23 ND 7.992,3,6-TriCB 24 ND 6.632,3',4-TriCB 25 ND 6.712,3',5-TriCB 26 26 + 29 C ND 7.652,3',6-TriCB 27 ND 6.432,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 30.9 7.05 0.89 0.8362,4',6-TriCB 32 ND 7.312',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 7.843,3',4-TriCB 35 ND 7.193,3',5-TriCB 36 ND 7.283,4,4'-TriCB 37 ND 9.353,4,5-TriCB 38 ND 7.28


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 7.422,2',3,3'-TeCB 40 40 + 41 + 71 C 19.5 6.66 0.72 1.3362,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 NDR 11.9 6.94 0.62 1.3122,2',3,5-TeCB 43 ND 7.732,2',3,5'-TeCB 44 44 + 47 + 65 C 153 6.12 0.83 1.2872,2',3,6-TeCB 45 45 + 51 C 24.4 6.94 0.89 1.1482,2',3,6'-TeCB 46 ND 7.792,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 6.852,2',4,5'-TeCB 49 49 + 69 C NDR 28.9 5.81 0.93 1.2592,2',4,6-TeCB 50 50 + 53 C NDR 8.21 6.71 0.40 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 121 6.26 0.78 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 4.392,3,3',4-TeCB 55 ND 16.42,3,3',4'-TeCB 56 ND 16.32,3,3',5-TeCB 57 ND 15.92,3,3',5'-TeCB 58 ND 16.82,3,3',6-TeCB 59 59 + 62 + 75 C NDR 11.3 5.10 1.30 1.3022,3,4,4'-TeCB 60 164 16.3 0.74 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 1460 15.5 0.78 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 15.62,3,4',6-TeCB 64 21.8 4.90 0.67 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 7.362,2',3,3',5-PeCB 83 83 + 99 C 2360 7.22 1.61 0.8862,2',3,3',6-PeCB 84 NDR 8.78 7.79 0.85 1.1622,2',3,4,4'-PeCB 85 85 + 116 + 117 C 145 5.75 1.54 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 68.3 6.15 1.65 0.9012,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C NDR 10.2 7.19 2.25 1.1542,2',3,4,6'-PeCB 89 ND 7.452,2',3,4',5-PeCB 90 90 + 101 + 113 C 269 6.12 1.63 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 117 7.08 1.55 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 158 7.05 1.47 1.1202,2',3,5,6'-PeCB 94 ND 7.872,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 4.192,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 6.492,2',4,6,6'-PeCB 104 ND 3.572,3,3',4,4'-PeCB 105 1300 17.7 1.62 1.0002,3,3',4,5-PeCB 106 ND 14.82,3,3',4',5-PeCB 107 107 + 124 C ND 15.92,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 77.0 14.7 1.42 0.9972,3,3',4',6-PeCB 110 110 + 115 C 202 5.10 1.59 0.9262,3,3',5,5'-PeCB 111 NDR 8.21 5.13 0.73 0.9462,3,3',5,6-PeCB 112 ND 5.012,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 233 16.7 1.35 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 4870 16.9 1.57 1.0012,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 4.872,3',4,5',6-PeCB 121 ND 5.412',3,3',4,5-PeCB 122 ND 16.32',3,4,4',5-PeCB 123 NDR 70.2 16.9 2.26 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 NDR 26.9 20.9 1.02 1.0003,3',4,5,5'-PeCB 127 NDR 22.9 14.9 2.05 1.041

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 ND 3.292,3,3',4,4',5-HxCB 156 156 + 157 C 2490 14.2 1.21 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 855 10.7 1.26 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 0.958 0.141 1.01 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 47.0 0.140 1.31 0.9282,2',3,3',4,5'-HxCB 130 D 1.55 0.176 1.10 0.9132,2',3,3',4,6-HxCB 131 ND D 0.1682,2',3,3',4,6'-HxCB 132 D 0.298 0.179 1.17 1.1742,2',3,3',5,5'-HxCB 133 NDR D 0.781 0.163 1.72 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.1692,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 1.93 0.0852 1.17 1.1032,2',3,3',6,6'-HxCB 136 NDR D 0.140 0.0629 0.47 1.0242,2',3,4,4',5-HxCB 137 D 2.15 0.174 1.40 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 0.1572,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 0.1612,2',3,4,5,6-HxCB 142 ND D 0.1662,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 0.08522,2',3,4,6,6'-HxCB 145 ND D 0.06772,2',3,4',5,5'-HxCB 146 D 7.29 0.142 1.40 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 0.926 0.156 1.82 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.08752,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 NDR D 0.071 0.0652 0.83 1.0132,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.06022,2',4,4',5,5'-HxCB 153 153 + 168 C D 49.5 0.125 1.25 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 1.69 0.111 1.20 0.9382,3,3',4,5,5'-HxCB 159 ND D 0.1182,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 0.1212,3,3',4',5,5'-HxCB 162 ND D 0.1192,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 0.177 0.117 1.24 0.9212,3,3',5,5',6-HxCB 165 ND D 0.1362,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 25.1 0.0936 1.08 0.9352,2',3,3',4,4',6-HpCB 171 171 + 173 C D 2.51 0.0992 1.03 1.1632,2',3,3',4,5,5'-HpCB 172 D 3.64 0.0986 1.16 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 0.642 0.0929 0.76 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 0.246 0.0937 3.45 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 0.07302,2',3,3',4',5,6-HpCB 177 D 5.01 0.0927 1.06 1.1452,2',3,3',5,5',6-HpCB 178 D 2.94 0.0959 0.99 1.0852,2',3,3',5,6,6'-HpCB 179 D 0.237 0.0707 1.05 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 49.6 0.0789 1.05 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.190 0.0943 1.93 1.1562,2',3,4,4',5,6'-HpCB 182 ND D 0.09302,2',3,4,4',5',6-HpCB 183 183 + 185 C D 7.53 0.0936 0.94 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 0.07162,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.07532,2',3,4',5,5',6-HpCB 187 D 15.5 0.0895 1.07 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 0.05742,3,3',4,4',5,5'-HpCB 189 D 1.07 0.0482 1.10 1.0002,3,3',4,4',5,6-HpCB 190 D 5.10 0.0708 0.92 0.9462,3,3',4,4',5',6-HpCB 191 D 1.19 0.0726 1.11 0.9172,3,3',4,5,5',6-HpCB 192 ND D 0.08102,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 5.75 0.0513 0.88 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 2.33 0.0611 1.11 0.9442,2',3,3',4,4',5,6'-OcCB 196 D 3.99 0.116 0.91 0.9142,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.09782,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 11.4 0.120 0.87 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.487 0.0971 0.71 1.0222,2',3,3',5,5',6,6'-OcCB 202 NDR D 1.14 0.0903 1.29 1.0002,2',3,4,4',5,5',6-OcCB 203 D 6.70 0.111 0.96 0.9182,2',3,4,4',5,6,6'-OcCB 204 ND D 0.09882,3,3',4,4',5,5',6-OcCB 205 D 0.293 0.0549 0.82 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 1.63 0.357 0.66 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 0.3052,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 0.611 0.295 0.55 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 0.666 0.0841 0.66 1.000





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 271 39.9 1.01 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 13300 39.6 1.31 0.9282,2',3,3',4,5'-HxCB 130 D 439 49.8 1.10 0.9132,2',3,3',4,6-HxCB 131 ND D 47.62,2',3,3',4,6'-HxCB 132 D 84.4 50.7 1.17 1.1742,2',3,3',5,5'-HxCB 133 NDR D 221 46.2 1.72 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C ND D 47.92,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C D 547 24.1 1.17 1.1032,2',3,3',6,6'-HxCB 136 NDR D 39.6 17.8 0.47 1.0242,2',3,4,4',5-HxCB 137 D 609 49.3 1.40 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND D 44.52,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 45.62,2',3,4,5,6-HxCB 142 ND D 47.02,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 24.12,2',3,4,6,6'-HxCB 145 ND D 19.22,2',3,4',5,5'-HxCB 146 D 2060 40.2 1.40 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 262 44.2 1.82 1.1332,2',3,4',5,6'-HxCB 148 ND D 24.82,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 NDR D 20.1 18.5 0.83 1.0132,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 17.02,2',4,4',5,5'-HxCB 153 153 + 168 C D 14000 35.4 1.25 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 479 31.4 1.20 0.9382,3,3',4,5,5'-HxCB 159 ND D 33.42,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND D 34.32,3,3',4',5,5'-HxCB 162 ND D 33.72,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 D 50.1 33.1 1.24 0.9212,3,3',5,5',6-HxCB 165 ND D 38.52,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 7110 26.5 1.08 0.9352,2',3,3',4,4',6-HpCB 171 171 + 173 C D 711 28.1 1.03 1.1632,2',3,3',4,5,5'-HpCB 172 D 1030 27.9 1.16 0.8962,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 182 26.3 0.76 1.1332,2',3,3',4,5',6-HpCB 175 NDR D 69.7 26.5 3.45 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 20.72,2',3,3',4',5,6-HpCB 177 D 1420 26.3 1.06 1.1452,2',3,3',5,5',6-HpCB 178 D 833 27.2 0.99 1.0852,2',3,3',5,6,6'-HpCB 179 D 67.1 20.0 1.05 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 14000 22.3 1.05 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 53.8 26.7 1.93 1.1562,2',3,4,4',5,6'-HpCB 182 ND D 26.32,2',3,4,4',5',6-HpCB 183 183 + 185 C D 2130 26.5 0.94 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 20.32,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 21.32,2',3,4',5,5',6-HpCB 187 D 4390 25.3 1.07 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 16.32,3,3',4,4',5,5'-HpCB 189 D 303 13.7 1.10 1.0002,3,3',4,4',5,6-HpCB 190 D 1440 20.1 0.92 0.9462,3,3',4,4',5',6-HpCB 191 D 337 20.6 1.11 0.9172,3,3',4,5,5',6-HpCB 192 ND D 22.92,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 1630 14.5 0.88 0.9912,2',3,3',4,4',5,6-OcCB 195 NDR D 660 17.3 1.11 0.9442,2',3,3',4,4',5,6'-OcCB 196 D 1130 32.9 0.91 0.9142,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 27.72,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 3230 34.0 0.87 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 138 27.5 0.71 1.0222,2',3,3',5,5',6,6'-OcCB 202 NDR D 323 25.6 1.29 1.0002,2',3,4,4',5,5',6-OcCB 203 D 1900 31.4 0.96 0.9182,2',3,4,4',5,6,6'-OcCB 204 ND D 28.02,3,3',4,4',5,5',6-OcCB 205 D 83.0 15.5 0.82 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 D 462 101 0.66 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 ND D 86.42,2',3,3',4,5,5',6,6'-NoCB 208 NDR D 173 83.5 0.55 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 D 189 23.8 0.66 1.000









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 656 32.8 3.17 0.71813C12-4-MoCB 3L 2000 743 37.2 3.24 0.858

13C12-2,2'-DiCB 4L 2000 1030 51.6 1.63 0.87313C12-4,4'-DiCB 15L 2000 1390 69.7 1.62 1.255

13C12-2,2',6-TriCB 19L 2000 1260 63.2 1.04 1.07213C12-3,4,4'-TriCB 37L 2000 1440 72.1 1.08 1.092





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1850 92.4 1.06 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1920 96.2 1.61 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X





13C12-2,2',3,3',4,4',5-HpCB 170L D 2000 2850 142 1.05 0.89613C12-2,2',3,4,4',5,5'-HpCB 180L D 2000 2620 131 1.03 0.87113C12-2,2',3,4',5,6,6'-HpCB 188L D 2000 1750 87.3 1.03 0.71113C12-2,3,3',4,4',5,5'-HpCB 189L D 2000 2180 109 1.08 0.958

13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1730 86.7 0.91 0.81713C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1650 82.5 0.89 1.010

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 1860 93.0 0.80 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 2150 108 0.81 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 1850 92.5 1.26 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2220 111 1.14 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 ND 0.04393-MoCB 2 ND 0.04564-MoCB 3 ND 0.0531

2,2'-DiCB 4 ND 0.09722,3-DiCB 5 ND 0.06402,3'-DiCB 6 ND 0.05722,4-DiCB 7 ND 0.06092,4'-DiCB 8 ND 0.05252,5-DiCB 9 ND 0.05922,6-DiCB 10 ND 0.06453,3'-DiCB 11 0.577 0.0567 1.57 0.9693,4-DiCB 12 12 + 13 C ND 0.05663,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.05684,4'-DiCB 15 ND 0.0612

2,2',3-TriCB 16 NDR 0.036 0.0269 0.61 1.1662,2',4-TriCB 17 ND 0.02402,2',5-TriCB 18 18 + 30 C NDR 0.098 0.0202 0.83 1.1132,2',6-TriCB 19 NDR 0.039 0.0279 1.91 1.0022,3,3'-TriCB 20 20 + 28 C 3.69 0.0284 1.11 0.8472,3,4-TriCB 21 21 + 33 C NDR 0.111 0.0279 1.31 0.8572,3,4'-TriCB 22 ND 0.03132,3,5-TriCB 23 ND 0.03052,3,6-TriCB 24 ND 0.01772,3',4-TriCB 25 ND 0.02562,3',5-TriCB 26 26 + 29 C ND 0.02912,3',6-TriCB 27 NDR 0.021 0.0171 1.89 1.1512,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 0.157 0.0268 0.97 0.8362,4',6-TriCB 32 ND 0.02792',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 0.02993,3',4-TriCB 35 ND 0.02743,3',5-TriCB 36 ND 0.02783,4,4'-TriCB 37 ND 0.03353,4,5-TriCB 38 ND 0.0277


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.02822,2',3,3'-TeCB 40 40 + 41 + 71 C 0.079 0.0191 0.69 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.047 0.0199 0.84 1.3112,2',3,5-TeCB 43 ND 0.02222,2',3,5'-TeCB 44 44 + 47 + 65 C 0.521 0.0176 0.88 1.2872,2',3,6-TeCB 45 45 + 51 C NDR 0.040 0.0199 1.04 1.1472,2',3,6'-TeCB 46 ND 0.02232,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 0.025 0.0196 0.95 1.2742,2',4,5'-TeCB 49 49 + 69 C NDR 0.113 0.0166 1.07 1.2602,2',4,6-TeCB 50 50 + 53 C NDR 0.023 0.0192 1.36 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 0.426 0.0180 0.82 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 0.01382,3,3',4-TeCB 55 ND 0.06162,3,3',4'-TeCB 56 ND 0.06122,3,3',5-TeCB 57 ND 0.05972,3,3',5'-TeCB 58 ND 0.06322,3,3',6-TeCB 59 59 + 62 + 75 C NDR 0.045 0.0146 0.60 1.3022,3,4,4'-TeCB 60 1.11 0.0610 0.77 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 19.5 0.0581 0.79 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 0.092 0.0586 0.78 0.8642,3,4',6-TeCB 64 0.087 0.0141 0.79 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 0.02132,2',3,3',5-PeCB 83 83 + 99 C 11.7 0.0209 1.61 0.8862,2',3,3',6-PeCB 84 ND 0.02252,2',3,4,4'-PeCB 85 85 + 116 + 117 C 0.671 0.0166 1.67 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 0.207 0.0177 1.40 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.02072,2',3,4,6'-PeCB 89 ND 0.02152,2',3,4',5-PeCB 90 90 + 101 + 113 C 1.08 0.0177 1.52 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 0.377 0.0205 1.82 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 0.663 0.0204 1.56 1.1212,2',3,5,6'-PeCB 94 ND 0.02282,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01152,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.01882,2',4,6,6'-PeCB 104 ND 0.01152,3,3',4,4'-PeCB 105 6.33 0.0980 1.55 1.0012,3,3',4,5-PeCB 106 ND 0.08242,3,3',4',5-PeCB 107 107 + 124 C ND 0.08842,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 0.386 0.0814 2.00 0.9972,3,3',4',6-PeCB 110 110 + 115 C 0.592 0.0147 1.37 0.9262,3,3',5,5'-PeCB 111 0.040 0.0149 1.41 0.9462,3,3',5,6-PeCB 112 ND 0.01452,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 2.34 0.0900 1.53 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 27.8 0.0936 1.59 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 0.037 0.0141 1.54 0.9592,3',4,5',6-PeCB 121 ND 0.01562',3,3',4,5-PeCB 122 ND 0.09022',3,4,4',5-PeCB 123 0.321 0.0940 1.65 1.0012',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 ND 0.1143,3',4,5,5'-PeCB 127 ND 0.0829

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 NDR 0.030 0.0115 0.97 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 25.4 0.0161 1.23 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 6.55 0.0125 1.32 1.0012,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 ND 12.63-MoCB 2 ND 13.14-MoCB 3 ND 15.2

2,2'-DiCB 4 ND 27.82,3-DiCB 5 ND 18.32,3'-DiCB 6 ND 16.42,4-DiCB 7 ND 17.42,4'-DiCB 8 ND 15.02,5-DiCB 9 ND 17.02,6-DiCB 10 ND 18.53,3'-DiCB 11 165 16.2 1.57 0.9693,4-DiCB 12 12 + 13 C ND 16.23,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 16.34,4'-DiCB 15 ND 17.5

2,2',3-TriCB 16 NDR 10.3 7.71 0.61 1.1662,2',4-TriCB 17 ND 6.882,2',5-TriCB 18 18 + 30 C NDR 28.1 5.79 0.83 1.1132,2',6-TriCB 19 NDR 11.2 7.99 1.91 1.0022,3,3'-TriCB 20 20 + 28 C 1060 8.14 1.11 0.8472,3,4-TriCB 21 21 + 33 C NDR 31.8 7.99 1.31 0.8572,3,4'-TriCB 22 ND 8.972,3,5-TriCB 23 ND 8.742,3,6-TriCB 24 ND 5.072,3',4-TriCB 25 ND 7.332,3',5-TriCB 26 26 + 29 C ND 8.342,3',6-TriCB 27 NDR 6.02 4.90 1.89 1.1512,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 45.0 7.68 0.97 0.8362,4',6-TriCB 32 ND 7.992',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 8.573,3',4-TriCB 35 ND 7.853,3',5-TriCB 36 ND 7.963,4,4'-TriCB 37 ND 9.603,4,5-TriCB 38 ND 7.94


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 8.082,2',3,3'-TeCB 40 40 + 41 + 71 C 22.6 5.47 0.69 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 13.5 5.70 0.84 1.3112,2',3,5-TeCB 43 ND 6.362,2',3,5'-TeCB 44 44 + 47 + 65 C 149 5.04 0.88 1.2872,2',3,6-TeCB 45 45 + 51 C NDR 11.5 5.70 1.04 1.1472,2',3,6'-TeCB 46 ND 6.392,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 7.16 5.62 0.95 1.2742,2',4,5'-TeCB 49 49 + 69 C NDR 32.4 4.76 1.07 1.2602,2',4,6-TeCB 50 50 + 53 C NDR 6.59 5.50 1.36 1.1112,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 122 5.16 0.82 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 3.952,3,3',4-TeCB 55 ND 17.62,3,3',4'-TeCB 56 ND 17.52,3,3',5-TeCB 57 ND 17.12,3,3',5'-TeCB 58 ND 18.12,3,3',6-TeCB 59 59 + 62 + 75 C NDR 12.9 4.18 0.60 1.3022,3,4,4'-TeCB 60 318 17.5 0.77 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 5590 16.6 0.79 0.8772,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 26.4 16.8 0.78 0.8642,3,4',6-TeCB 64 24.9 4.04 0.79 1.3482,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 ND 6.102,2',3,3',5-PeCB 83 83 + 99 C 3350 5.99 1.61 0.8862,2',3,3',6-PeCB 84 ND 6.452,2',3,4,4'-PeCB 85 85 + 116 + 117 C 192 4.76 1.67 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 59.3 5.07 1.40 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 5.932,2',3,4,6'-PeCB 89 ND 6.162,2',3,4',5-PeCB 90 90 + 101 + 113 C 309 5.07 1.52 0.8702,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 NDR 108 5.87 1.82 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 190 5.84 1.56 1.1212,2',3,5,6'-PeCB 94 ND 6.532,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 3.292,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 5.392,2',4,6,6'-PeCB 104 ND 3.292,3,3',4,4'-PeCB 105 1810 28.1 1.55 1.0012,3,3',4,5-PeCB 106 ND 23.62,3,3',4',5-PeCB 107 107 + 124 C ND 25.32,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 NDR 111 23.3 2.00 0.9972,3,3',4',6-PeCB 110 110 + 115 C 170 4.21 1.37 0.9262,3,3',5,5'-PeCB 111 11.5 4.27 1.41 0.9462,3,3',5,6-PeCB 112 ND 4.152,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 670 25.8 1.53 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 7960 26.8 1.59 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 10.6 4.04 1.54 0.9592,3',4,5',6-PeCB 121 ND 4.472',3,3',4,5-PeCB 122 ND 25.82',3,4,4',5-PeCB 123 92.0 26.9 1.65 1.0012',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 ND 32.73,3',4,5,5'-PeCB 127 ND 23.7

2,2',3,3',4,4'-HxCB 128 128 + 166 C X2,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C X2,2',3,3',4,5'-HxCB 130 X2,2',3,3',4,6-HxCB 131 X2,2',3,3',4,6'-HxCB 132 X2,2',3,3',5,5'-HxCB 133 X2,2',3,3',5,6-HxCB 134 134 + 143 C X2,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C X2,2',3,3',6,6'-HxCB 136 X2,2',3,4,4',5-HxCB 137 X2,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C X2,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 X2,2',3,4,5,6-HxCB 142 X2,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 X2,2',3,4,6,6'-HxCB 145 X2,2',3,4',5,5'-HxCB 146 X2,2',3,4',5,6-HxCB 147 147 + 149 C X2,2',3,4',5,6'-HxCB 148 X2,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 X2,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 X2,2',4,4',5,5'-HxCB 153 153 + 168 C X2,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 NDR 8.59 3.29 0.97 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 7280 4.61 1.23 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 X2,3,3',4,5,5'-HxCB 159 X2,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 X2,3,3',4',5,5'-HxCB 162 X2,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 X2,3,3',5,5',6-HxCB 165 X2,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 1880 3.58 1.32 1.0012,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 X




2,2',3,3',4,4',5,5',6,6'-DeCB 209 X





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 0.833 0.0700 0.81 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 106 0.0694 1.28 0.9282,2',3,3',4,5'-HxCB 130 D 3.11 0.0872 1.24 0.9132,2',3,3',4,6-HxCB 131 ND D 0.08352,2',3,3',4,6'-HxCB 132 NDR D 0.374 0.0885 1.53 1.1732,2',3,3',5,5'-HxCB 133 NDR D 2.55 0.0810 1.58 1.1902,2',3,3',5,6-HxCB 134 134 + 143 C ND D 0.08362,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C NDR D 1.54 0.107 1.03 1.1022,2',3,3',6,6'-HxCB 136 ND D 0.07882,2',3,4,4',5-HxCB 137 D 5.48 0.0860 1.24 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR D 0.117 0.0778 1.62 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 0.07982,2',3,4,5,6-HxCB 142 ND D 0.08212,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 0.1072,2',3,4,6,6'-HxCB 145 ND D 0.08492,2',3,4',5,5'-HxCB 146 D 18.9 0.0703 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 0.763 0.0773 1.65 1.1332,2',3,4',5,6'-HxCB 148 ND D 0.1102,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 0.08172,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 0.07542,2',4,4',5,5'-HxCB 153 153 + 168 C D 129 0.0618 1.25 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 1.58 0.0550 1.29 0.9382,3,3',4,5,5'-HxCB 159 ND D 0.05842,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 D 0.123 0.0600 1.33 0.8882,3,3',4',5,5'-HxCB 162 ND D 0.05882,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR D 0.217 0.0579 1.82 0.9212,3,3',5,5',6-HxCB 165 ND D 0.06762,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 50.0 0.0955 1.04 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 5.01 0.101 1.07 1.1632,2',3,3',4,5,5'-HpCB 172 D 7.41 0.101 0.95 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 0.104 0.0948 3.76 1.1332,2',3,3',4,5',6-HpCB 175 D 0.609 0.0957 1.11 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 0.07462,2',3,3',4',5,6-HpCB 177 D 7.88 0.0946 0.96 1.1452,2',3,3',5,5',6-HpCB 178 D 7.86 0.0979 1.10 1.0852,2',3,3',5,6,6'-HpCB 179 D 0.133 0.0722 1.03 1.0112,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 106 0.0805 1.04 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 0.160 0.0963 0.48 1.1562,2',3,4,4',5,6'-HpCB 182 ND D 0.09492,2',3,4,4',5',6-HpCB 183 183 + 185 C D 11.0 0.0955 1.10 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 0.07312,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 0.07692,2',3,4',5,5',6-HpCB 187 D 34.2 0.0913 1.05 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 0.06932,3,3',4,4',5,5'-HpCB 189 D 2.64 0.0721 1.06 1.0002,3,3',4,4',5,6-HpCB 190 D 9.46 0.0723 1.07 0.9472,3,3',4,4',5',6-HpCB 191 NDR D 1.79 0.0741 1.37 0.9182,3,3',4,5,5',6-HpCB 192 ND D 0.08272,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 17.5 0.0682 0.90 0.9912,2',3,3',4,4',5,6-OcCB 195 D 6.52 0.0812 0.93 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 9.95 0.123 0.94 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 0.1042,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 25.1 0.128 0.95 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 0.449 0.104 1.94 1.0232,2',3,3',5,5',6,6'-OcCB 202 NDR D 3.19 0.111 0.72 1.0012,2',3,4,4',5,5',6-OcCB 203 D 15.3 0.118 0.97 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 0.1052,3,3',4,4',5,5',6-OcCB 205 D 0.630 0.0669 0.79 1.001

2,2',3,3',4,4',5,5',6-NoCB 206 D 3.99 0.372 0.80 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 D 0.398 0.300 0.82 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 D 1.24 0.276 0.87 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 0.832 0.0468 0.55 1.000





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT





COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR D 239 20.1 0.81 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C D 30400 19.9 1.28 0.9282,2',3,3',4,5'-HxCB 130 D 891 25.0 1.24 0.9132,2',3,3',4,6-HxCB 131 ND D 23.92,2',3,3',4,6'-HxCB 132 NDR D 107 25.4 1.53 1.1732,2',3,3',5,5'-HxCB 133 NDR D 731 23.2 1.58 1.1902,2',3,3',5,6-HxCB 134 134 + 143 C ND D 23.92,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C NDR D 441 30.7 1.03 1.1022,2',3,3',6,6'-HxCB 136 ND D 22.62,2',3,4,4',5-HxCB 137 D 1570 24.6 1.24 0.9182,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C NDR D 33.5 22.3 1.62 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 ND D 22.92,2',3,4,5,6-HxCB 142 ND D 23.52,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND D 30.72,2',3,4,6,6'-HxCB 145 ND D 24.32,2',3,4',5,5'-HxCB 146 D 5410 20.1 1.29 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C NDR D 219 22.1 1.65 1.1332,2',3,4',5,6'-HxCB 148 ND D 31.52,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND D 23.42,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND D 21.62,2',4,4',5,5'-HxCB 153 153 + 168 C D 37000 17.7 1.25 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 X2,3,3',4,4',5-HxCB 156 156 + 157 C X2,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 D 453 15.8 1.29 0.9382,3,3',4,5,5'-HxCB 159 ND D 16.72,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 D 35.2 17.2 1.33 0.8882,3,3',4',5,5'-HxCB 162 ND D 16.82,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR D 62.2 16.6 1.82 0.9212,3,3',5,5',6-HxCB 165 ND D 19.42,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 D 14300 27.4 1.04 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C D 1440 28.9 1.07 1.1632,2',3,3',4,5,5'-HpCB 172 D 2120 28.9 0.95 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR D 29.8 27.2 3.76 1.1332,2',3,3',4,5',6-HpCB 175 D 174 27.4 1.11 1.1032,2',3,3',4,6,6'-HpCB 176 ND D 21.42,2',3,3',4',5,6-HpCB 177 D 2260 27.1 0.96 1.1452,2',3,3',5,5',6-HpCB 178 D 2250 28.0 1.10 1.0852,2',3,3',5,6,6'-HpCB 179 D 38.1 20.7 1.03 1.0112,2',3,4,4',5,5'-HpCB 180 180 + 193 C D 30400 23.1 1.04 0.9102,2',3,4,4',5,6-HpCB 181 NDR D 45.8 27.6 0.48 1.1562,2',3,4,4',5,6'-HpCB 182 ND D 27.22,2',3,4,4',5',6-HpCB 183 183 + 185 C D 3150 27.4 1.10 1.1272,2',3,4,4',6,6'-HpCB 184 ND D 20.92,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND D 22.02,2',3,4',5,5',6-HpCB 187 D 9800 26.2 1.05 1.1102,2',3,4',5,6,6'-HpCB 188 ND D 19.92,3,3',4,4',5,5'-HpCB 189 D 756 20.7 1.06 1.0002,3,3',4,4',5,6-HpCB 190 D 2710 20.7 1.07 0.9472,3,3',4,4',5',6-HpCB 191 NDR D 513 21.2 1.37 0.9182,3,3',4,5,5',6-HpCB 192 ND D 23.72,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 D 5010 19.5 0.90 0.9912,2',3,3',4,4',5,6-OcCB 195 D 1870 23.3 0.93 0.9452,2',3,3',4,4',5,6'-OcCB 196 D 2850 35.2 0.94 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND D 29.82,2',3,3',4,5,5',6-OcCB 198 198 + 199 C D 7190 36.7 0.95 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 NDR D 129 29.8 1.94 1.0232,2',3,3',5,5',6,6'-OcCB 202 NDR D 914 31.8 0.72 1.0012,2',3,4,4',5,5',6-OcCB 203 D 4380 33.8 0.97 0.9202,2',3,4,4',5,6,6'-OcCB 204 ND D 30.12,3,3',4,4',5,5',6-OcCB 205 D 180 19.2 0.79 1.001

2,2',3,3',4,4',5,5',6-NoCB 206 D 1140 107 0.80 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 D 114 85.9 0.82 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 D 355 79.1 0.87 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 NDR D 238 13.4 0.55 1.000









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 578 28.9 3.23 0.71813C12-4-MoCB 3L 2000 706 35.3 3.27 0.858

13C12-2,2'-DiCB 4L 2000 963 48.2 1.60 0.87313C12-4,4'-DiCB 15L 2000 1510 75.4 1.64 1.255

13C12-2,2',6-TriCB 19L 2000 1270 63.6 1.04 1.07213C12-3,4,4'-TriCB 37L 2000 1530 76.4 1.05 1.092





13C12-2,2',3,3',5,5',6,6'-OcCB 202L X13C12-2,3,3',4,4',5,5',6-OcCB 205L X

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L X13C12-2,2',3,3',4,5,5',6,6'-NoCB 208L X

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L X

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1790 89.6 1.04 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1950 97.3 1.63 1.088

13C12-2,2',3,3',5,5',6-HpCB 178L X









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT


13C12-2,2'-DiCB 4L X13C12-4,4'-DiCB 15L X






13C12-2,2',3,3',5,5',6,6'-OcCB 202L D 2000 1550 77.5 0.84 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L D 2000 1830 91.4 0.89 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L D 2000 2140 107 0.78 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L D 2000 2500 125 0.81 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L D 2000 2230 111 1.21 1.075

CLEANUP STANDARD


13C12-2,2',3,3',5,5',6-HpCB 178L D 2000 2340 117 1.04 1.012





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 3.36 0.0246 3.33 1.0003-MoCB 2 0.039 0.0263 3.48 0.9884-MoCB 3 3.85 0.0297 3.23 1.001

2,2'-DiCB 4 3.59 0.0852 1.63 1.0002,3-DiCB 5 ND 0.05272,3'-DiCB 6 NDR 0.053 0.0478 3.72 1.1762,4-DiCB 7 ND 0.04912,4'-DiCB 8 3.32 0.0444 1.64 1.2072,5-DiCB 9 ND 0.04642,6-DiCB 10 ND 0.04603,3'-DiCB 11 0.910 0.0507 1.73 0.9693,4-DiCB 12 12 + 13 C 0.091 0.0506 1.60 0.9843,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.04894,4'-DiCB 15 4.37 0.0541 1.60 1.000

2,2',3-TriCB 16 0.051 0.0306 1.10 1.1662,2',4-TriCB 17 NDR 0.042 0.0261 0.76 1.1382,2',5-TriCB 18 18 + 30 C 2.37 0.0222 1.06 1.1142,2',6-TriCB 19 3.78 0.0311 1.09 1.0022,3,3'-TriCB 20 20 + 28 C 14.9 0.0153 1.07 0.8472,3,4-TriCB 21 21 + 33 C NDR 0.172 0.0154 1.48 0.8572,3,4'-TriCB 22 0.128 0.0171 1.20 0.8722,3,5-TriCB 23 2.86 0.0162 1.09 1.2842,3,6-TriCB 24 ND 0.01972,3',4-TriCB 25 NDR 0.023 0.0140 0.71 0.8252,3',5-TriCB 26 26 + 29 C NDR 0.081 0.0153 1.34 1.3022,3',6-TriCB 27 ND 0.01842,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 3.89 0.0147 1.06 0.8362,4',6-TriCB 32 0.038 0.0145 0.96 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 2.88 0.0159 1.10 1.2753,3',4-TriCB 35 ND 0.01663,3',5-TriCB 36 ND 0.01523,4,4'-TriCB 37 5.13 0.0164 1.06 1.0013,4,5-TriCB 38 ND 0.0154


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.01532,2',3,3'-TeCB 40 40 + 41 + 71 C 2.83 0.0147 0.78 1.3382,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.080 0.0159 0.73 1.3132,2',3,5-TeCB 43 ND 0.01722,2',3,5'-TeCB 44 44 + 47 + 65 C 4.30 0.0137 0.80 1.2862,2',3,6-TeCB 45 45 + 51 C 0.033 0.0155 0.78 1.1502,2',3,6'-TeCB 46 NDR 0.026 0.0178 1.02 1.1622,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 0.01522,2',4,5'-TeCB 49 49 + 69 C 2.78 0.0130 0.78 1.2612,2',4,6-TeCB 50 50 + 53 C 0.031 0.0148 0.86 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 3.80 0.0139 0.77 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 3.98 0.0146 0.81 1.0022,3,3',4-TeCB 55 ND 0.05022,3,3',4'-TeCB 56 4.62 0.0513 0.85 0.9042,3,3',5-TeCB 57 ND 0.05132,3,3',5'-TeCB 58 ND 0.05232,3,3',6-TeCB 59 59 + 62 + 75 C 0.076 0.0129 0.88 1.3032,3,4,4'-TeCB 60 4.99 0.0508 0.82 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 25.4 0.0493 0.83 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 0.303 0.0499 0.81 0.8642,3,4',6-TeCB 64 0.207 0.0129 0.83 1.3502,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 NDR 0.062 0.0200 2.46 0.9342,2',3,3',5-PeCB 83 83 + 99 C 24.9 0.0187 1.55 0.8862,2',3,3',6-PeCB 84 0.075 0.0212 1.60 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 1.30 0.0157 1.59 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 4.47 0.0158 1.58 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 0.01962,2',3,4,6'-PeCB 89 ND 0.01952,2',3,4',5-PeCB 90 90 + 101 + 113 C 6.05 0.0166 1.54 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 1.13 0.0191 1.55 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 4.54 0.0193 1.57 1.1202,2',3,5,6'-PeCB 94 ND 0.02152,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01292,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.01772,2',4,6,6'-PeCB 104 2.94 0.0129 1.60 1.0012,3,3',4,4'-PeCB 105 19.7 0.106 1.59 1.0002,3,3',4,5-PeCB 106 ND 0.09102,3,3',4',5-PeCB 107 107 + 124 C ND 0.09412,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 1.18 0.0819 1.34 0.9972,3,3',4',6-PeCB 110 110 + 115 C 5.43 0.0137 1.60 0.9252,3,3',5,5'-PeCB 111 0.060 0.0138 1.38 0.9462,3,3',5,6-PeCB 112 ND 0.01342,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 5.80 0.0984 1.61 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 57.1 0.0975 1.60 1.0012,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 0.103 0.0132 2.07 0.9582,3',4,5',6-PeCB 121 ND 0.01472',3,3',4,5-PeCB 122 ND 0.09992',3,4,4',5-PeCB 123 4.58 0.0997 1.71 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 5.26 0.100 1.60 1.0013,3',4,5,5'-PeCB 127 0.143 0.0918 1.58 1.042

2,2',3,3',4,4'-HxCB 128 128 + 166 C 1.98 0.0455 1.23 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 139 0.0468 1.27 0.9282,2',3,3',4,5'-HxCB 130 4.20 0.0601 1.30 0.9132,2',3,3',4,6-HxCB 131 ND 0.05762,2',3,3',4,6'-HxCB 132 0.613 0.0612 1.21 1.1742,2',3,3',5,5'-HxCB 133 1.91 0.0564 1.29 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C 0.122 0.0559 1.29 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 6.18 0.0129 1.25 1.1032,2',3,3',6,6'-HxCB 136 0.154 0.0129 1.35 1.0242,2',3,4,4',5-HxCB 137 4.53 0.0535 1.28 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C 0.316 0.0517 1.18 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 1.52 0.0558 1.31 0.9042,2',3,4,5,6-HxCB 142 ND 0.05712,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 0.122 0.0129 1.05 1.1212,2',3,4,6,6'-HxCB 145 ND 0.01292,2',3,4',5,5'-HxCB 146 16.8 0.0505 1.27 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 5.11 0.0527 1.25 1.1332,2',3,4',5,6'-HxCB 148 ND 0.01292,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 0.01292,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 0.01292,2',4,4',5,5'-HxCB 153 153 + 168 C 157 0.0443 1.29 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 2.16 0.0129 1.23 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 27.5 0.0521 1.27 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 3.69 0.0378 1.25 0.9382,3,3',4,5,5'-HxCB 159 NDR 0.056 0.0385 1.56 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 0.04282,3,3',4',5,5'-HxCB 162 ND 0.03942,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR 0.394 0.0419 0.98 0.9222,3,3',5,5',6-HxCB 165 ND 0.04842,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 10.0 0.0400 1.28 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 5.01 0.0387 1.28 1.000

2,2',3,3',4,4',5-HpCB 170 51.4 0.0129 1.05 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C 5.94 0.0129 1.06 1.1622,2',3,3',4,5,5'-HpCB 172 6.70 0.0129 1.04 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 0.819 0.0129 1.08 1.1332,2',3,3',4,5',6-HpCB 175 0.958 0.0129 1.02 1.1022,2',3,3',4,6,6'-HpCB 176 ND 0.01292,2',3,3',4',5,6-HpCB 177 15.4 0.0129 1.06 1.1452,2',3,3',5,5',6-HpCB 178 7.34 0.0129 1.04 1.0852,2',3,3',5,6,6'-HpCB 179 0.373 0.0129 1.00 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C 116 0.0129 1.04 0.9102,2',3,4,4',5,6-HpCB 181 0.179 0.0129 1.18 1.1562,2',3,4,4',5,6'-HpCB 182 2.55 0.0129 1.06 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C 23.0 0.0129 1.05 1.1272,2',3,4,4',6,6'-HpCB 184 0.050 0.0129 1.13 1.0252,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND 0.01292,2',3,4',5,5',6-HpCB 187 45.7 0.0129 1.05 1.1102,2',3,4',5,6,6'-HpCB 188 2.35 0.0129 1.08 1.0002,3,3',4,4',5,5'-HpCB 189 6.39 0.0314 1.02 1.0002,3,3',4,4',5,6-HpCB 190 8.24 0.0129 1.05 0.9472,3,3',4,4',5',6-HpCB 191 1.95 0.0129 1.09 0.9172,3,3',4,5,5',6-HpCB 192 ND 0.01292,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 21.3 0.0284 0.88 0.9912,2',3,3',4,4',5,6-OcCB 195 6.26 0.0302 0.88 0.9452,2',3,3',4,4',5,6'-OcCB 196 11.1 0.0129 0.90 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND 0.01292,2',3,3',4,5,5',6-OcCB 198 198 + 199 C 18.7 0.0129 0.90 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 0.970 0.0129 0.93 1.0232,2',3,3',5,5',6,6'-OcCB 202 5.20 0.0129 0.87 1.0002,2',3,4,4',5,5',6-OcCB 203 11.5 0.0129 0.91 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND 0.01292,3,3',4,4',5,5',6-OcCB 205 4.15 0.0274 0.84 1.001

2,2',3,3',4,4',5,5',6-NoCB 206 6.41 0.0459 0.79 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 0.539 0.0370 0.84 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 3.25 0.0365 0.81 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 3.18 0.0129 0.72 1.001





Project No. POP1406










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 866 6.34 3.33 1.0003-MoCB 2 10.1 6.78 3.48 0.9884-MoCB 3 993 7.66 3.23 1.001

2,2'-DiCB 4 926 22.0 1.63 1.0002,3-DiCB 5 ND 13.62,3'-DiCB 6 NDR 13.7 12.3 3.72 1.1762,4-DiCB 7 ND 12.72,4'-DiCB 8 856 11.4 1.64 1.2072,5-DiCB 9 ND 12.02,6-DiCB 10 ND 11.93,3'-DiCB 11 235 13.1 1.73 0.9693,4-DiCB 12 12 + 13 C 23.5 13.0 1.60 0.9843,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 12.64,4'-DiCB 15 1130 13.9 1.60 1.000

2,2',3-TriCB 16 13.1 7.89 1.10 1.1662,2',4-TriCB 17 NDR 10.8 6.73 0.76 1.1382,2',5-TriCB 18 18 + 30 C 611 5.72 1.06 1.1142,2',6-TriCB 19 975 8.02 1.09 1.0022,3,3'-TriCB 20 20 + 28 C 3840 3.94 1.07 0.8472,3,4-TriCB 21 21 + 33 C NDR 44.3 3.97 1.48 0.8572,3,4'-TriCB 22 33.0 4.41 1.20 0.8722,3,5-TriCB 23 737 4.18 1.09 1.2842,3,6-TriCB 24 ND 5.082,3',4-TriCB 25 NDR 5.93 3.61 0.71 0.8252,3',5-TriCB 26 26 + 29 C NDR 20.9 3.94 1.34 1.3022,3',6-TriCB 27 ND 4.742,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 1000 3.79 1.06 0.8362,4',6-TriCB 32 9.80 3.74 0.96 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 742 4.10 1.10 1.2753,3',4-TriCB 35 ND 4.283,3',5-TriCB 36 ND 3.923,4,4'-TriCB 37 1320 4.23 1.06 1.0013,4,5-TriCB 38 ND 3.97


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 3.942,2',3,3'-TeCB 40 40 + 41 + 71 C 730 3.79 0.78 1.3382,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 20.6 4.10 0.73 1.3132,2',3,5-TeCB 43 ND 4.432,2',3,5'-TeCB 44 44 + 47 + 65 C 1110 3.53 0.80 1.2862,2',3,6-TeCB 45 45 + 51 C 8.51 4.00 0.78 1.1502,2',3,6'-TeCB 46 NDR 6.70 4.59 1.02 1.1622,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 ND 3.922,2',4,5'-TeCB 49 49 + 69 C 717 3.35 0.78 1.2612,2',4,6-TeCB 50 50 + 53 C 7.99 3.82 0.86 1.1122,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 980 3.58 0.77 1.2352,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 1030 3.76 0.81 1.0022,3,3',4-TeCB 55 ND 12.92,3,3',4'-TeCB 56 1190 13.2 0.85 0.9042,3,3',5-TeCB 57 ND 13.22,3,3',5'-TeCB 58 ND 13.52,3,3',6-TeCB 59 59 + 62 + 75 C 19.6 3.33 0.88 1.3032,3,4,4'-TeCB 60 1290 13.1 0.82 0.9112,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 6550 12.7 0.83 0.8762,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 78.1 12.9 0.81 0.8642,3,4',6-TeCB 64 53.4 3.33 0.83 1.3502,3,5,6-TeCB 65 44 + 47 + 65 C44


2,2',3,3',4-PeCB 82 NDR 16.0 5.16 2.46 0.9342,2',3,3',5-PeCB 83 83 + 99 C 6420 4.82 1.55 0.8862,2',3,3',6-PeCB 84 19.3 5.47 1.60 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C 335 4.05 1.59 0.9182,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C 1150 4.07 1.58 0.9022,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C ND 5.052,2',3,4,6'-PeCB 89 ND 5.032,2',3,4',5-PeCB 90 90 + 101 + 113 C 1560 4.28 1.54 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 291 4.92 1.55 0.8532,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C 1170 4.98 1.57 1.1202,2',3,5,6'-PeCB 94 ND 5.542,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 3.332,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 4.562,2',4,6,6'-PeCB 104 758 3.33 1.60 1.0012,3,3',4,4'-PeCB 105 5080 27.3 1.59 1.0002,3,3',4,5-PeCB 106 ND 23.52,3,3',4',5-PeCB 107 107 + 124 C ND 24.32,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 304 21.1 1.34 0.9972,3,3',4',6-PeCB 110 110 + 115 C 1400 3.53 1.60 0.9252,3,3',5,5'-PeCB 111 15.5 3.56 1.38 0.9462,3,3',5,6-PeCB 112 ND 3.452,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 1500 25.4 1.61 1.0012,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 14700 25.1 1.60 1.0012,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 NDR 26.6 3.40 2.07 0.9582,3',4,5',6-PeCB 121 ND 3.792',3,3',4,5-PeCB 122 ND 25.82',3,4,4',5-PeCB 123 1180 25.7 1.71 1.0002',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 1360 25.8 1.60 1.0013,3',4,5,5'-PeCB 127 36.9 23.7 1.58 1.042

2,2',3,3',4,4'-HxCB 128 128 + 166 C 510 11.7 1.23 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 35800 12.1 1.27 0.9282,2',3,3',4,5'-HxCB 130 1080 15.5 1.30 0.9132,2',3,3',4,6-HxCB 131 ND 14.82,2',3,3',4,6'-HxCB 132 158 15.8 1.21 1.1742,2',3,3',5,5'-HxCB 133 492 14.5 1.29 1.1912,2',3,3',5,6-HxCB 134 134 + 143 C 31.5 14.4 1.29 1.1402,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 1590 3.33 1.25 1.1032,2',3,3',6,6'-HxCB 136 39.7 3.33 1.35 1.0242,2',3,4,4',5-HxCB 137 1170 13.8 1.28 0.9192,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C 81.5 13.3 1.18 1.1522,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 392 14.4 1.31 0.9042,2',3,4,5,6-HxCB 142 ND 14.72,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 31.5 3.33 1.05 1.1212,2',3,4,6,6'-HxCB 145 ND 3.332,2',3,4',5,5'-HxCB 146 4330 13.0 1.27 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 1320 13.6 1.25 1.1332,2',3,4',5,6'-HxCB 148 ND 3.332,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 3.332,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 3.332,2',4,4',5,5'-HxCB 153 153 + 168 C 40500 11.4 1.29 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 557 3.33 1.23 1.0012,3,3',4,4',5-HxCB 156 156 + 157 C 7090 13.4 1.27 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 951 9.75 1.25 0.9382,3,3',4,5,5'-HxCB 159 NDR 14.4 9.93 1.56 0.9822,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 11.02,3,3',4',5,5'-HxCB 162 ND 10.22,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 NDR 102 10.8 0.98 0.9222,3,3',5,5',6-HxCB 165 ND 12.52,3,4,4',5,6-HxCB 166 128 + 166 C128






COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,3',4,4',5,5'-HxCB 167 2580 10.3 1.28 1.0002,3',4,4',5',6-HxCB 168 153 + 168 C1533,3',4,4',5,5'-HxCB 169 1290 9.98 1.28 1.000

2,2',3,3',4,4',5-HpCB 170 13300 3.33 1.05 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C 1530 3.33 1.06 1.1622,2',3,3',4,5,5'-HpCB 172 1730 3.33 1.04 0.8972,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 211 3.33 1.08 1.1332,2',3,3',4,5',6-HpCB 175 247 3.33 1.02 1.1022,2',3,3',4,6,6'-HpCB 176 ND 3.332,2',3,3',4',5,6-HpCB 177 3970 3.33 1.06 1.1452,2',3,3',5,5',6-HpCB 178 1890 3.33 1.04 1.0852,2',3,3',5,6,6'-HpCB 179 96.2 3.33 1.00 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C 29900 3.33 1.04 0.9102,2',3,4,4',5,6-HpCB 181 46.1 3.33 1.18 1.1562,2',3,4,4',5,6'-HpCB 182 657 3.33 1.06 1.1152,2',3,4,4',5',6-HpCB 183 183 + 185 C 5930 3.33 1.05 1.1272,2',3,4,4',6,6'-HpCB 184 12.9 3.33 1.13 1.0252,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND 3.332,2',3,4',5,5',6-HpCB 187 11800 3.33 1.05 1.1102,2',3,4',5,6,6'-HpCB 188 606 3.33 1.08 1.0002,3,3',4,4',5,5'-HpCB 189 1650 8.10 1.02 1.0002,3,3',4,4',5,6-HpCB 190 2120 3.33 1.05 0.9472,3,3',4,4',5',6-HpCB 191 503 3.33 1.09 0.9172,3,3',4,5,5',6-HpCB 192 ND 3.332,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 5490 7.32 0.88 0.9912,2',3,3',4,4',5,6-OcCB 195 1610 7.79 0.88 0.9452,2',3,3',4,4',5,6'-OcCB 196 2860 3.33 0.90 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND 3.332,2',3,3',4,5,5',6-OcCB 198 198 + 199 C 4820 3.33 0.90 1.1152,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 250 3.33 0.93 1.0232,2',3,3',5,5',6,6'-OcCB 202 1340 3.33 0.87 1.0002,2',3,4,4',5,5',6-OcCB 203 2960 3.33 0.91 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND 3.332,3,3',4,4',5,5',6-OcCB 205 1070 7.06 0.84 1.001

2,2',3,3',4,4',5,5',6-NoCB 206 1650 11.8 0.79 1.0002,2',3,3',4,4',5,6,6'-NoCB 207 139 9.54 0.84 1.0192,2',3,3',4,5,5',6,6'-NoCB 208 838 9.41 0.81 1.000

2,2',3,3',4,4',5,5',6,6'-DeCB 209 820 3.33 0.72 1.001









Project No. POP1406










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 721 36.0 3.24 0.71913C12-4-MoCB 3L 2000 812 40.6 3.25 0.858

13C12-2,2'-DiCB 4L 2000 825 41.2 1.61 0.87413C12-4,4'-DiCB 15L 2000 1110 55.3 1.60 1.254

13C12-2,2',6-TriCB 19L 2000 923 46.1 1.07 1.07213C12-3,4,4'-TriCB 37L 2000 1650 82.5 1.10 1.091

13C12-2,2',6,6'-TeCB 54L 2000 1050 52.6 0.81 0.81013C12-3,3',4,4'-TeCB 77L 2000 2110 105 0.82 1.39613C12-3,4,4',5-TeCB 81L 2000 2150 107 0.82 1.373

13C12-2,2',4,6,6'-PeCB 104L 2000 1130 56.6 1.60 0.80813C12-2,3,3',4,4'-PeCB 105L 2000 1840 92.0 1.60 1.19913C12-2,3,4,4',5-PeCB 114L 2000 1900 94.9 1.62 1.17813C12-2,3',4,4',5-PeCB 118L 2000 1950 97.5 1.61 1.16113C12-2',3,4,4',5-PeCB 123L 2000 1950 97.5 1.61 1.15113C12-3,3',4,4',5-PeCB 126L 2000 2000 100 1.60 1.300


13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1730 86.5 1.05 0.89713C12-2,2',3,4,4',5,5'-HpCB 180L 2000 1690 84.4 1.07 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L 2000 1470 73.7 1.06 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L 2000 1970 98.4 1.01 0.959

13C12-2,2',3,3',5,5',6,6'-OcCB 202L 2000 1750 87.5 0.91 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L 2000 1620 80.8 0.84 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L 2000 1650 82.5 0.77 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L 2000 1870 93.4 0.77 0.949

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L 2000 1630 81.5 1.19 1.075

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1820 90.8 1.10 0.92413C12-2,3,3',5,5'-PeCB 111L 2000 1970 98.5 1.62 1.087

13C12-2,2',3,3',5,5',6-HpCB 178L 2000 2170 109 1.07 1.012





Project No. N/A










COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2-MoCB 1 NDR 0.082 0.0288 2.48 1.0013-MoCB 2 NDR 0.056 0.0346 5.46 0.9884-MoCB 3 ND 0.0435

2,2'-DiCB 4 ND 0.1312,3-DiCB 5 ND 0.09922,3'-DiCB 6 ND 0.09182,4-DiCB 7 ND 0.09412,4'-DiCB 8 0.189 0.0842 1.53 1.2092,5-DiCB 9 ND 0.09162,6-DiCB 10 ND 0.09563,3'-DiCB 11 0.338 0.0896 1.52 0.9703,4-DiCB 12 12 + 13 C ND 0.08923,4'-DiCB 13 12 + 13 C123,5-DiCB 14 ND 0.08914,4'-DiCB 15 ND 0.103

2,2',3-TriCB 16 0.073 0.0291 1.04 1.1662,2',4-TriCB 17 NDR 0.075 0.0270 1.25 1.1382,2',5-TriCB 18 18 + 30 C 0.149 0.0233 1.02 1.1132,2',6-TriCB 19 NDR 0.045 0.0338 1.43 1.0022,3,3'-TriCB 20 20 + 28 C 0.264 0.0386 0.94 0.8472,3,4-TriCB 21 21 + 33 C 0.135 0.0371 0.99 0.8572,3,4'-TriCB 22 0.109 0.0422 1.09 0.8712,3,5-TriCB 23 ND 0.04162,3,6-TriCB 24 ND 0.02122,3',4-TriCB 25 ND 0.03582,3',5-TriCB 26 26 + 29 C 0.049 0.0399 0.88 1.3012,3',6-TriCB 27 ND 0.01902,4,4'-TriCB 28 20 + 28 C202,4,5-TriCB 29 26 + 29 C262,4,6-TriCB 30 18 + 30 C182,4',5-TriCB 31 0.210 0.0369 1.07 0.8362,4',6-TriCB 32 0.056 0.0400 1.20 1.1982',3,4-TriCB 33 21 + 33 C212',3,5-TriCB 34 ND 0.04133,3',4-TriCB 35 ND 0.03513,3',5-TriCB 36 ND 0.03523,4,4'-TriCB 37 0.046 0.0395 1.03 1.0003,4,5-TriCB 38 ND 0.0354

Page 1 of 4 (WG26343 - 1668_PCB1668_PCBTF_WG26343-101_Form1A_PB8B_261S5_SJ910826.html)

COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

3,4',5-TriCB 39 ND 0.03692,2',3,3'-TeCB 40 40 + 41 + 71 C NDR 0.119 0.0231 0.91 1.3372,2',3,4-TeCB 41 40 + 41 + 71 C402,2',3,4'-TeCB 42 0.039 0.0237 0.73 1.3112,2',3,5-TeCB 43 ND 0.02742,2',3,5'-TeCB 44 44 + 47 + 65 C 0.215 0.0216 0.74 1.2862,2',3,6-TeCB 45 45 + 51 C ND 0.02542,2',3,6'-TeCB 46 ND 0.02862,2',4,4'-TeCB 47 44 + 47 + 65 C442,2',4,5-TeCB 48 NDR 0.037 0.0239 1.17 1.2752,2',4,5'-TeCB 49 49 + 69 C NDR 0.112 0.0207 0.91 1.2602,2',4,6-TeCB 50 50 + 53 C NDR 0.035 0.0250 0.60 1.1132,2',4,6'-TeCB 51 45 + 51 C452,2',5,5'-TeCB 52 0.219 0.0229 0.75 1.2342,2',5,6'-TeCB 53 50 + 53 C502,2',6,6'-TeCB 54 ND 0.02172,3,3',4-TeCB 55 ND 0.03232,3,3',4'-TeCB 56 0.066 0.0322 0.85 0.9042,3,3',5-TeCB 57 ND 0.03192,3,3',5'-TeCB 58 ND 0.03282,3,3',6-TeCB 59 59 + 62 + 75 C 0.031 0.0179 0.86 1.3032,3,4,4'-TeCB 60 ND 0.03202,3,4,5-TeCB 61 61 + 70 + 74 + 76 C 0.226 0.0311 0.79 0.8752,3,4,6-TeCB 62 59 + 62 + 75 C592,3,4',5-TeCB 63 ND 0.03082,3,4',6-TeCB 64 NDR 0.073 0.0170 1.16 1.3492,3,5,6-TeCB 65 44 + 47 + 65 C44

2,3',4,4'-TeCB 66 NDR 0.115 0.0302 1.11 0.8852,3',4,5-TeCB 67 ND 0.02922,3',4,5'-TeCB 68 ND 0.03152,3',4,6-TeCB 69 49 + 69 C492,3',4',5-TeCB 70 61 + 70 + 74 + 76 C612,3',4',6-TeCB 71 40 + 41 + 71 C402,3',5,5'-TeCB 72 ND 0.03142,3',5',6-TeCB 73 ND 0.01902,4,4',5-TeCB 74 61 + 70 + 74 + 76 C612,4,4',6-TeCB 75 59 + 62 + 75 C592',3,4,5-TeCB 76 61 + 70 + 74 + 76 C613,3',4,4'-TeCB 77 ND 0.03263,3',4,5-TeCB 78 ND 0.02973,3',4,5'-TeCB 79 ND 0.02503,3',5,5'-TeCB 80 ND 0.02843,4,4',5-TeCB 81 ND 0.0336

2,2',3,3',4-PeCB 82 ND 0.02182,2',3,3',5-PeCB 83 83 + 99 C NDR 0.075 0.0207 2.23 0.8862,2',3,3',6-PeCB 84 0.036 0.0232 1.44 1.1632,2',3,4,4'-PeCB 85 85 + 116 + 117 C NDR 0.017 0.0169 2.82 0.9202,2',3,4,5-PeCB 86 86 + 87 + 97 + 108 + 119 + 125 C NDR 0.110 0.0175 1.97 0.9012,2',3,4,5'-PeCB 87 86 + 87 + 97 + 108 + 119 + 125 C862,2',3,4,6-PeCB 88 88 + 91 C 0.031 0.0210 1.73 1.1542,2',3,4,6'-PeCB 89 ND 0.02152,2',3,4',5-PeCB 90 90 + 101 + 113 C 0.171 0.0180 1.46 0.8692,2',3,4',6-PeCB 91 88 + 91 C882,2',3,5,5'-PeCB 92 ND 0.02092,2',3,5,6-PeCB 93 93 + 95 + 98 + 100 + 102 C NDR 0.186 0.0207 1.27 1.1212,2',3,5,6'-PeCB 94 ND 0.02342,2',3,5',6-PeCB 95 93 + 95 + 98 + 100 + 102 C932,2',3,6,6'-PeCB 96 ND 0.01252,2',3',4,5-PeCB 97 86 + 87 + 97 + 108 + 119 + 125 C862,2',3',4,6-PeCB 98 93 + 95 + 98 + 100 + 102 C932,2',4,4',5-PeCB 99 83 + 99 C832,2',4,4',6-PeCB 100 93 + 95 + 98 + 100 + 102 C932,2',4,5,5'-PeCB 101 90 + 101 + 113 C902,2',4,5,6'-PeCB 102 93 + 95 + 98 + 100 + 102 C93


COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT

2,2',4,5',6-PeCB 103 ND 0.02002,2',4,6,6'-PeCB 104 ND 0.01252,3,3',4,4'-PeCB 105 NDR 0.074 0.0149 1.07 1.0002,3,3',4,5-PeCB 106 ND 0.01332,3,3',4',5-PeCB 107 107 + 124 C ND 0.01442,3,3',4,5'-PeCB 108 86 + 87 + 97 + 108 + 119 + 125 C862,3,3',4,6-PeCB 109 ND 0.01252,3,3',4',6-PeCB 110 110 + 115 C NDR 0.142 0.0150 1.88 0.9252,3,3',5,5'-PeCB 111 ND 0.01492,3,3',5,6-PeCB 112 ND 0.01512,3,3',5',6-PeCB 113 90 + 101 + 113 C902,3,4,4',5-PeCB 114 NDR 0.026 0.0137 1.07 1.0002,3,4,4',6-PeCB 115 110 + 115 C1102,3,4,5,6-PeCB 116 85 + 116 + 117 C852,3,4',5,6-PeCB 117 85 + 116 + 117 C852,3',4,4',5-PeCB 118 NDR 0.102 0.0145 1.95 1.0002,3',4,4',6-PeCB 119 86 + 87 + 97 + 108 + 119 + 125 C862,3',4,5,5'-PeCB 120 ND 0.01422,3',4,5',6-PeCB 121 ND 0.01582',3,3',4,5-PeCB 122 ND 0.01492',3,4,4',5-PeCB 123 ND 0.01532',3,4,5,5'-PeCB 124 107 + 124 C1072',3,4,5,6'-PeCB 125 86 + 87 + 97 + 108 + 119 + 125 C863,3',4,4',5-PeCB 126 NDR 0.027 0.0170 1.80 1.0003,3',4,5,5'-PeCB 127 ND 0.0131

2,2',3,3',4,4'-HxCB 128 128 + 166 C NDR 0.029 0.0125 0.88 0.9582,2',3,3',4,5-HxCB 129 129 + 138 + 160 + 163 C 0.193 0.0125 1.32 0.9282,2',3,3',4,5'-HxCB 130 ND 0.01452,2',3,3',4,6-HxCB 131 ND 0.01462,2',3,3',4,6'-HxCB 132 NDR 0.060 0.0149 1.56 1.1742,2',3,3',5,5'-HxCB 133 ND 0.01342,2',3,3',5,6-HxCB 134 134 + 143 C ND 0.01382,2',3,3',5,6'-HxCB 135 135 + 151 + 154 C 0.068 0.0125 1.39 1.1042,2',3,3',6,6'-HxCB 136 0.024 0.0125 1.19 1.0242,2',3,4,4',5-HxCB 137 ND 0.01332,2',3,4,4',5'-HxCB 138 129 + 138 + 160 + 163 C1292,2',3,4,4',6-HxCB 139 139 + 140 C ND 0.01302,2',3,4,4',6'-HxCB 140 139 + 140 C1392,2',3,4,5,5'-HxCB 141 NDR 0.025 0.0129 1.44 0.9032,2',3,4,5,6-HxCB 142 ND 0.01392,2',3,4,5,6'-HxCB 143 134 + 143 C1342,2',3,4,5',6-HxCB 144 ND 0.01252,2',3,4,6,6'-HxCB 145 ND 0.01252,2',3,4',5,5'-HxCB 146 0.019 0.0125 1.12 0.8842,2',3,4',5,6-HxCB 147 147 + 149 C 0.145 0.0130 1.15 1.1332,2',3,4',5,6'-HxCB 148 ND 0.01252,2',3,4',5',6-HxCB 149 147 + 149 C1472,2',3,4',6,6'-HxCB 150 ND 0.01252,2',3,5,5',6-HxCB 151 135 + 151 + 154 C1352,2',3,5,6,6'-HxCB 152 ND 0.01252,2',4,4',5,5'-HxCB 153 153 + 168 C 0.166 0.0125 1.23 0.8992,2',4,4',5,6'-HxCB 154 135 + 151 + 154 C1352,2',4,4',6,6'-HxCB 155 ND 0.01252,3,3',4,4',5-HxCB 156 156 + 157 C 0.069 0.0125 1.41 1.0002,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3,3',4,4',6-HxCB 158 NDR 0.023 0.0125 0.86 0.9382,3,3',4,5,5'-HxCB 159 ND 0.01252,3,3',4,5,6-HxCB 160 129 + 138 + 160 + 163 C1292,3,3',4,5',6-HxCB 161 ND 0.01252,3,3',4',5,5'-HxCB 162 ND 0.01252,3,3',4',5,6-HxCB 163 129 + 138 + 160 + 163 C1292,3,3',4',5',6-HxCB 164 ND 0.01252,3,3',5,5',6-HxCB 165 ND 0.01252,3,4,4',5,6-HxCB 166 128 + 166 C128




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COMPOUND IUPACNO.


CONC.FOUND

REPORTINGLIMIT

IONABUND.RATIO

RRT


2,2',3,3',4,4',5-HpCB 170 0.086 0.0125 1.08 0.9362,2',3,3',4,4',6-HpCB 171 171 + 173 C NDR 0.023 0.0125 1.33 1.1622,2',3,3',4,5,5'-HpCB 172 ND 0.01252,2',3,3',4,5,6-HpCB 173 171 + 173 C1712,2',3,3',4,5,6'-HpCB 174 NDR 0.055 0.0125 0.53 1.1332,2',3,3',4,5',6-HpCB 175 ND 0.01252,2',3,3',4,6,6'-HpCB 176 ND 0.01252,2',3,3',4',5,6-HpCB 177 0.019 0.0125 0.91 1.1452,2',3,3',5,5',6-HpCB 178 ND 0.01252,2',3,3',5,6,6'-HpCB 179 NDR 0.022 0.0125 0.62 1.0102,2',3,4,4',5,5'-HpCB 180 180 + 193 C 0.152 0.0125 1.10 0.9102,2',3,4,4',5,6-HpCB 181 ND 0.01252,2',3,4,4',5,6'-HpCB 182 0.013 0.0125 0.89 1.1162,2',3,4,4',5',6-HpCB 183 183 + 185 C NDR 0.048 0.0125 1.31 1.1272,2',3,4,4',6,6'-HpCB 184 ND 0.01252,2',3,4,5,5',6-HpCB 185 183 + 185 C1832,2',3,4,5,6,6'-HpCB 186 ND 0.01252,2',3,4',5,5',6-HpCB 187 0.089 0.0125 0.95 1.1102,2',3,4',5,6,6'-HpCB 188 ND 0.01252,3,3',4,4',5,5'-HpCB 189 0.026 0.0125 1.01 1.0002,3,3',4,4',5,6-HpCB 190 ND 0.01252,3,3',4,4',5',6-HpCB 191 ND 0.01252,3,3',4,5,5',6-HpCB 192 ND 0.01252,3,3',4',5,5',6-HpCB 193 180 + 193 C180

2,2',3,3',4,4',5,5'-OcCB 194 0.070 0.0125 0.94 0.9912,2',3,3',4,4',5,6-OcCB 195 ND 0.01252,2',3,3',4,4',5,6'-OcCB 196 NDR 0.017 0.0125 0.58 0.9162,2',3,3',4,4',6,6'-OcCB 197 197 + 200 C ND 0.01252,2',3,3',4,5,5',6-OcCB 198 198 + 199 C ND 0.01252,2',3,3',4,5,5',6'-OcCB 199 198 + 199 C1982,2',3,3',4,5,6,6'-OcCB 200 197 + 200 C1972,2',3,3',4,5',6,6'-OcCB 201 ND 0.01252,2',3,3',5,5',6,6'-OcCB 202 NDR 0.017 0.0125 1.99 1.0002,2',3,4,4',5,5',6-OcCB 203 NDR 0.027 0.0125 0.39 0.9192,2',3,4,4',5,6,6'-OcCB 204 ND 0.01252,3,3',4,4',5,5',6-OcCB 205 NDR 0.016 0.0125 0.63 1.000

2,2',3,3',4,4',5,5',6-NoCB 206 ND 0.04782,2',3,3',4,4',5,6,6'-NoCB 207 ND 0.04342,2',3,3',4,5,5',6,6'-NoCB 208 ND 0.0417

2,2',3,3',4,4',5,5',6,6'-DeCB 209 0.049 0.0125 0.70 1.001




For Axys Internal Use Only [ XSL Template: Form16682.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26343-101_Form2_PB8B_261S5_SJ910826.html; Workgroup: WG26343; Design ID: 925 ]





Project No. N/A










LABELEDCOMPOUND

IUPACNO. 1


SPIKECONC.

CONC.FOUND


RRT

13C12-2-MoCB 1L 2000 498 24.9 3.21 0.71813C12-4-MoCB 3L 2000 496 24.8 3.29 0.858

13C12-2,2'-DiCB 4L 2000 745 37.3 1.59 0.87313C12-4,4'-DiCB 15L 2000 937 46.9 1.62 1.255

13C12-2,2',6-TriCB 19L 2000 975 48.8 1.06 1.07213C12-3,4,4'-TriCB 37L 2000 1290 64.3 1.05 1.092




13C12-2,2',3,3',4,4',5-HpCB 170L 2000 1860 92.8 1.04 0.89713C12-2,2',3,4,4',5,5'-HpCB 180L 2000 1920 95.8 1.06 0.87213C12-2,2',3,4',5,6,6'-HpCB 188L 2000 1800 89.8 1.04 0.71213C12-2,3,3',4,4',5,5'-HpCB 189L 2000 1910 95.4 1.05 0.959

13C12-2,2',3,3',5,5',6,6'-OcCB 202L 2000 1880 93.9 0.92 0.81813C12-2,3,3',4,4',5,5',6-OcCB 205L 2000 1860 92.8 0.88 1.009

13C12-2,2',3,3',4,4',5,5',6-NoCB 206L 2000 1870 93.7 0.81 1.04413C12-2,2',3,3',4,5,5',6,6'-NoCB 208L 2000 1910 95.5 0.80 0.950

13C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L 2000 1920 95.8 1.20 1.075

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 2000 1210 60.7 1.04 0.92513C12-2,3,3',5,5'-PeCB 111L 2000 1810 90.5 1.62 1.087

13C12-2,2',3,3',5,5',6-HpCB 178L 2000 2210 111 1.07 1.012

Page 1 of 1 (WG26343 - 1668_PCB1668_PCBTF_WG26343-101_Form2_PB8B_261S5_SJ910826.html)

(1) Where applicable, custom lab flags have been used on this report; C = co-eluting congener.


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PCB CONGENER ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 Lab Sample I.D.: WG26343-102 L

Matrix: BLOOD Initial Calibration Date: 30-Jul-2008



Extract Volume (uL): 20 OPR Data Filename: PB8B_261 S: 2




COMPOUND IUPACNO.


IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

2-MoCB 1 3.15 50.0 53.8 25.0 - 75.0 1084-MoCB 3 3.13 50.0 52.3 25.0 - 75.0 1052,2'-DiCB 4 1.54 50.0 52.8 25.0 - 75.0 1064,4'-DiCB 15 1.58 50.0 49.5 25.0 - 75.0 99.12,2',6-TriCB 19 1.07 50.0 53.3 25.0 - 75.0 1073,4,4'-TriCB 37 1.04 50.0 53.1 25.0 - 75.0 1062,2',6,6'-TeCB 54 0.76 50.0 50.2 25.0 - 75.0 1003,3',4,4'-TeCB 77 0.80 50.0 52.0 25.0 - 75.0 1043,4,4',5-TeCB 81 0.80 50.0 52.2 25.0 - 75.0 1042,2',4,6,6'-PeCB 104 1.59 50.0 48.2 25.0 - 75.0 96.42,3,3',4,4'-PeCB 105 1.57 50.0 50.6 25.0 - 75.0 1012,3,4,4',5-PeCB 114 1.54 50.0 48.1 25.0 - 75.0 96.32,3',4,4',5-PeCB 118 1.57 50.0 52.1 25.0 - 75.0 1042',3,4,4',5-PeCB 123 1.58 50.0 49.2 25.0 - 75.0 98.43,3',4,4',5-PeCB 126 1.57 50.0 49.5 25.0 - 75.0 98.92,2',4,4',6,6'-HxCB 155 1.28 50.0 45.9 25.0 - 75.0 91.92,3,3',4,4',5-HxCB 156 156 + 157 C 1.26 100 99.0 50.0 - 150 99.02,3,3',4,4',5'-HxCB 157 156 + 157 C1562,3',4,4',5,5'-HxCB 167 1.26 50.0 48.7 25.0 - 75.0 97.53,3',4,4',5,5'-HxCB 169 1.27 50.0 50.7 25.0 - 75.0 1012,2',3,4',5,6,6'-HpCB 188 1.07 50.0 46.0 25.0 - 75.0 92.02,3,3',4,4',5,5'-HpCB 189 1.00 50.0 51.4 25.0 - 75.0 1032,2',3,3',5,5',6,6'-OcCB 202 0.92 50.0 50.7 25.0 - 75.0 1012,3,3',4,4',5,5',6-OcCB 205 0.90 50.0 48.6 25.0 - 75.0 97.12,2',3,3',4,4',5,5',6-NoCB 206 0.79 50.0 51.7 25.0 - 75.0 1032,2',3,3',4,5,5',6,6'-NoCB 208 0.79 50.0 49.7 25.0 - 75.0 99.42,2',3,3',4,4',5,5',6,6'-DeCB 209 0.70 50.0 51.2 25.0 - 75.0 102

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(1) Suffix "L" indicates labeled compound.(2) Where applicable, custom lab flags have been used on this report; C = co-eluting congener.


For Axys Internal Use Only [ XSL Template: Form16688B.xsl; Created: 15-Oct-2008 10:21:32; Application: XMLTransformer-1.9.15;Report Filename: 1668_PCB1668_PCBTF_WG26343-102_Form8B_SJ910820.html; Workgroup: WG26343; Design ID: 925 ]



PCB CONGENER ONGOING PRECISION AND RECOVERY (OPR)AXYS ANALYTICAL SERVICES2045 MILLS RD., SIDNEY, B.C., CANADAV8L 5X2 TEL (250) 655-5800 FAX (250) 655-5811Contract No.: 2607 Lab Sample I.D.: WG26343-102 L

Matrix: BLOOD Initial Calibration Date: 30-Jul-2008



Extract Volume (uL): 20 OPR Data Filename: PB8B_261 S: 2




LABELEDCOMPOUND

IUPACNO. 1

CO-ELUTIONS

LABFLAG2

IONABUND.RATIO

SPIKECONC.(ng/mL)

CONC.FOUND(ng/mL)


%RECOVERY

13C12-2-MoCB 1L 3.19 100 22.5 15.0 - 140 22.513C12-4-MoCB 3L 3.12 100 24.0 15.0 - 140 24.013C12-2,2'-DiCB 4L 1.66 100 35.7 30.0 - 140 35.713C12-4,4'-DiCB 15L 1.63 100 54.1 30.0 - 140 54.113C12-2,2',6-TriCB 19L 1.06 100 50.7 30.0 - 140 50.713C12-3,4,4'-TriCB 37L 1.05 100 66.0 30.0 - 140 66.013C12-2,2',6,6'-TeCB 54L 0.83 100 46.9 30.0 - 140 46.913C12-3,3',4,4'-TeCB 77L 0.83 100 86.3 30.0 - 140 86.313C12-3,4,4',5-TeCB 81L 0.83 100 89.2 30.0 - 140 89.213C12-2,2',4,6,6'-PeCB 104L 1.60 100 72.3 30.0 - 140 72.313C12-2,3,3',4,4'-PeCB 105L 1.64 100 88.2 30.0 - 140 88.213C12-2,3,4,4',5-PeCB 114L 1.65 100 91.6 30.0 - 140 91.613C12-2,3',4,4',5-PeCB 118L 1.62 100 92.3 30.0 - 140 92.313C12-2',3,4,4',5-PeCB 123L 1.64 100 92.2 30.0 - 140 92.213C12-3,3',4,4',5-PeCB 126L 1.62 100 81.0 30.0 - 140 81.013C12-2,2',4,4',6,6'-HxCB 155L 1.21 100 90.2 30.0 - 140 90.213C12-2,3,3',4,4',5-HxCB 156L 156L + 157L C 1.23 200 173 60.0 - 280 86.313C12-2,3,3',4,4',5'-HxCB 157L 156L + 157L C156L13C12-2,3',4,4',5,5'-HxCB 167L 1.25 100 88.3 30.0 - 140 88.313C12-3,3',4,4',5,5'-HxCB 169L 1.19 100 90.4 30.0 - 140 90.413C12-2,2',3,4',5,6,6'-HpCB 188L 1.06 100 74.2 30.0 - 140 74.213C12-2,3,3',4,4',5,5'-HpCB 189L 1.05 100 91.5 30.0 - 140 91.513C12-2,2',3,3',5,5',6,6'-OcCB 202L 0.90 100 77.1 30.0 - 140 77.113C12-2,3,3',4,4',5,5',6-OcCB 205L 0.89 100 85.9 30.0 - 140 85.913C12-2,2',3,3',4,4',5,5',6-NoCB 206L 0.82 100 82.8 30.0 - 140 82.813C12-2,2',3,3',4,5,5',6,6'-NoCB 208L 0.80 100 86.5 30.0 - 140 86.513C12-2,2',3,3',4,4',5,5',6,6'-DeCB 209L 1.18 100 85.5 30.0 - 140 85.5

CLEANUP STANDARD

13C12-2,4,4'-TriCB 28L 1.06 100 70.3 40.0 - 125 70.313C12-2,3,3',5,5'-PeCB 111L 1.62 100 96.4 40.0 - 125 96.413C12-2,2',3,3',5,5',6-HpCB 178L 1.07 100 111 40.0 - 125 111

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appendix a3 raw chemical data - pops) toolkit pdr...n/a form 1a pesticide analysis report axys...

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