aparato cristalizar
DESCRIPTION
Descripcion de aparato para generar cristales en solución.TRANSCRIPT
-
inventory control Low-Cost Water-Bath Temperature CI
Gary D. Mercer Boise State University Boise, ID 83725
This article describes the construction of a temperature controller for the student laboratory that is low-cost, to- tally solid-state, and reasonably precise. When combined with a magnetic stirrer or small circulating pump, the unit will control a 1- to 4-L water bath with a precision of at least M.2 T over an ambient temperature range of 20-80 -C. The cost of construction, including the heater and en- closure, is less than $30. I have also found satisfactory re- sults using the wntroller for keeping a constant air tem- perature (M.2 ~ C ) in a closed chamber, although the controller was not specifically designed for this.
Construction The controller is constructed around the popular LM741
operational amplifier acting as a comparator to control the heater through an optocoupler with a triac. The heater is an inexpensive 200-W "coffee cup" heater generally avail- able at discount department stores. All electronic compo- nents are readily available from most electronics parts outlets.' Figure 1 shows the schematic diagram.
The heating coil and thermistor should be mounted to- gether to form a single unit. The leads of the thermistor should be soldered to the ends of a two-conductor cable. (Twenty-two gauge stranded speaker wire works well.)
'Possible sources are Radio Shack (local store); Jameco Electron- ics, 1355 Shoreway Road. Belmont. CA 94002 ($50.00 minimum order); or JDR Microdevices, 2233 Branham Lane, San Jose, CA 95124 ($10.00 minimum order).
Figure 1. Schematic diagram of the temperature controller
568 Journal of Chemical Education
edited by JOE RICH
Blackhawk Christian School 7400 East State Boulevard
Fort Wayne. IN 46815
Figure 2. Photograph showing the reiationship between the heater and the thermistor.
The connection is then insulated using 118-in. heat- shrink tubing so that one end covers the thermistor up to the tip and the other end is above the water line. The thermistor should he 0.5 cm from the heater coil and di- rectly above it for the most stable operation. These two should be taped or banded together at the handle of the heating coil so that they will not move relative to one an- other during use.
Figure 2 shows the heater-thehnistor assembly that I constructed. The figure also shows that the plug was re- moved from the end of the heater in my version. Then both its leads and the thermistor leads were wired to a 5-pin DIN connector.
The panel temperature control (5-kQ potentiometer) should be wired so that it will be at its lowest temperature setting when the control is in the extreme counter-clock- wise position. This can be done by connecting the thermis- tor lead to the right-hand terminal and by connecting the 4.7442 resistor to the left-hand terminal, as viewed from the shaft end.
Operation The controller is used with a magnetic stirrer or small
circulating pump, for example, a fish tank pump or an evaporative air-cooler pump. The bath vessel can be a large evaporating dish, a beaker, or a flat-bottom plastic bowl.
Before the controller can he used it must be calibrated. Immerse the heater and sensor in the water bath. Then turn the unit on, and set the panel temperature control to 50% of its maximum position. Then adjust the calibration trimmer (50-kR potentiometer) so that it regulates at 35 T. The controller will now show a usable temperature range of about 20-80 'C . The temperature range can be shifted by simply readjusting the calibration trimmer. The controller is now ready for use.
Modification for Air-Temperature Control Modification of the controller for controlling air temper-
ature is done by simply substituting a light bulb for the immersion heater and a fan for the stirrer. Again, the sys-
Dow
nloa
ded
by U
NIV
NA
CIO
NA
L A
UTO
NO
MA
MEX
ICO
on
Aug
ust 2
7, 2
015
| http:
//pubs
.acs.o
rg Pu
blic
atio
n D
ate:
July
1, 1
992
| doi: 1
0.1021
/ed069
p568
-
tern is set up so that the thermistor is reasonably close to Acknowledgment the light bulb (2-4 cm). For a cardboard-box enclosure (about 0.1 m3) that is kept at about 10 OC above ambient I would like to thank the College of Arts and Sciences at temperature, I found a 50-w bulb and a 4-in. "muffm" fan Boise State University for funding to complete this project to be quite adequate. through a minidevelopment grant program.
Volume 69 Number 7 July 1992 569
Dow
nloa
ded
by U
NIV
NA
CIO
NA
L A
UTO
NO
MA
MEX
ICO
on
Aug
ust 2
7, 2
015
| http:
//pubs
.acs.o
rg Pu
blic
atio
n D
ate:
July
1, 1
992
| doi: 1
0.1021
/ed069
p568