analytical test report silver haze orange tahoe · analysis method/sop: sop 8 results above 0.65...
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11119 SE Division St.
Portland, OR 97266
(503) 307-0096ORELAP #4096
OLCC #1002112892C Science First.
Analytical Test Report
Silver Haze Orange TahoeCloud 9
Laboratory ID: 1711103-01
Metrc Tag: 1A401030000985B000000713
Date Printed: 12/1/17
Date Sampled: 11/24/17
020-1002357FBBD
Batch ID: 0715
Potency Analysis
Analytical Method: De Backer, Journal of Chromatography b.2009. 11.004 -
SOP 19 & 20
Cannabinoids (% weight) Moisture Adjusted Notes
24.3 28.7THCA
< LOQ < LOQdelta 9-THC
0.959 1.13CBGA
< LOQ < LOQCBDA
< LOQ < LOQCBD
< LOQ < LOQCBN
< LOQ < LOQCBG
< LOQ < LOQCBC
Total THC
25.1 %
Total CBD
< LOQ %
MoistureAnalysis Method/SOP: SOP 7
Moisture: 15.4 %
Water Activity
Analysis Method/SOP: SOP 8 Results above 0.65 fail state testing requirements and will be highlighted Red.
Water Activity: 0.536 PASS
Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the
sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.
Chris Nielsen, Lab Director 12/1/2017Page 1 of 4
11119 SE Division St.
Portland, OR 97266
(503) 307-0096ORELAP #4096
OLCC #1002112892C Science First.
Analytical Test Report
Laboratory ID: 1711103-01
Cloud 9
Silver Haze Orange Tahoe
020-1002357FBBD
Terpene Analysis
Analysis Method/SOP: Terp
Analyte Result ug/g
alpha-Bisabolol < LOQ
Camphene < LOQ
delta-3-Carene < LOQ
beta-Caryophyllene 784.3
Caryophyllene Oxide < LOQ
p-Cymene < LOQ
Eucalyptol < LOQ
Geraniol < LOQ
Guaiol < LOQ
alpha-Humulene 215.1
Isopulegol < LOQ
Limonene 1594
Linalool 316.2
beta-Myrcene 685.4
Ocimene < LOQ
alpha-Pinene 178.6
beta-Pinene 253.0
gamma-Terpinene < LOQ
alpha-Terpinene < LOQ
Terpinolene < LOQ
cis-Nerolidol < LOQ
Total Terpenes 4114
Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the
sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.
Chris Nielsen, Lab Director 12/1/2017Page 2 of 4
11119 SE Division St.
Portland, OR 97266
(503) 307-0096ORELAP #4096
OLCC #1002112892C Science First.
Analytical Test Report
Laboratory ID: 1711103-01
Cloud 9
Silver Haze Orange Tahoe
020-1002357FBBD
Quality Control
Potency
Batch: B17K114 - Potency
Blank(B17K114-BLK1)
Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes
THCA 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
delta 9-THC 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBGA 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBDA 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBD 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBN 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBG 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
CBC 11/24/17 14:37 11/25/17 00:51< LOQ 0.110 %
LCS(B17K114-BS1)
% Recovery LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes
THCA 11/24/17 14:37 11/25/17 00:33102 0.110 % 80-120
delta 9-THC 11/24/17 14:37 11/25/17 00:33100 0.110 % 80-120
CBDA 11/24/17 14:37 11/25/17 00:33103 0.110 % 80-120
CBD 11/24/17 14:37 11/25/17 00:3397.2 0.110 % 80-120
Moisture Content
Batch: B17K115 - Grav
Blank(B17K115-BLK1)
Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes
Percent Moisture 11/24/17 18:56 11/24/17 18:560.0400 0.00 %
LCS(B17K115-BS1)
% Recovery LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes
Percent Moisture 11/24/17 18:56 11/24/17 18:560.00 % 70-130
Batch: B17K116 - WA
Blank(B17K116-BLK1)
Result LOQ Units Analyte Extracted Analyzed%Recovery Limits Notes
Water Activity 11/24/17 18:56 11/24/17 18:560.386 0.328 AW
Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the
sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.
Chris Nielsen, Lab Director 12/1/2017Page 3 of 4
11119 SE Division St.
Portland, OR 97266
(503) 307-0096ORELAP #4096
OLCC #1002112892C Science First.
Analytical Test Report
Laboratory ID: 1711103-01
Cloud 9
Silver Haze Orange Tahoe
020-1002357FBBD
Notes and Definitions
B Analyte detected in method blank, but not associated samples.
B2 Analyte detected in sample and associate methold blank.
C Interference due to co-elution.
D Initial result exceeded calibration range, reported data are based on analysis of a dilution.
H Non-homogenous samle matrix affecting RPD and/or QC.
I Manual Integration was performed.
L Duplicate sample relative precent difference (RPD) exceeds QC limits.
M Anomalous results due to matrix interference
P Peaks manually split.
Q1 QC out of limits but still oK
Q2 Quality Control outside QC limits. Data considered estimate.
Q3 CCV was above the acceptance criteria. Non-detect samples are considered acceptable.
Q4 CCV was below the acceptance criteria, however the sample still exceeds the regulatory limit.
R Marginal Exceedence.
U Reported result is an estimate. The analyte was detected above the calibration range.
X Problems with initial analysis, reported data are from reinjection of prepared sample.
<LOQ - Results below the Limit of Quantitation - Compound not detected
Sample tested in compliance with OAR 333-007 (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the
sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.
Chris Nielsen, Lab Director 12/1/2017Page 4 of 4
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Product identity:
Customer:
1711103-01 Silver Haze Orange Tahoe
11/24/17Sample Date:
17-002360-0013Laboratory ID:
Client/Metrc ID: 1A401030000620E000002140
Rose City Labs11119 SE Division St.Portland Oregon 97266United States
SubcontractGrower:
Matt BarnesRelinquished by:
18.8 °CTemp:
11.58 gWeight Received:
Sample Results
Pesticides Batch 1702363Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 12/1/17 12:00:00
LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes
Abamectin (sum) < LOQ 0.50 0.30 pass Acephate < LOQ 0.40 0.20 pass
Acequinocyl < LOQ 2.0 1.0 pass Acetamiprid < LOQ 0.20 0.10 pass
Aldicarb < LOQ 0.40 0.20 pass Azoxystrobin < LOQ 0.20 0.10 pass
Cyfluthrin (incl. Beta-Cyfl < LOQ 1.0 1.0 pass Bifenazate < LOQ 0.20 0.10 pass
Bifenthrin < LOQ 0.20 0.10 pass Boscalid < LOQ 0.40 0.10 pass
Carbaryl < LOQ 0.20 0.10 pass Carbofuran < LOQ 0.20 0.10 pass
Chlorantraniliprole < LOQ 0.20 0.10 pass Chlorfenapyr < LOQ 1.0 1.0 pass
Chlorpyrifos < LOQ 0.20 0.10 pass Clofentezine < LOQ 0.20 0.10 pass
Cypermethrin < LOQ 1.0 1.0 pass Daminozide < LOQ 1.0 1.0 pass
Diazinon < LOQ 0.20 0.10 pass Dichlorvos < LOQ 1.0 0.50 pass
Dimethoate < LOQ 0.20 0.10 pass Ethoprophos < LOQ 0.20 0.10 pass
Etofenprox < LOQ 0.40 0.10 pass Etoxazole < LOQ 0.20 0.10 pass
Fenoxycarb < LOQ 0.20 0.10 pass Fenpyroximate < LOQ 0.40 0.10 pass
Fipronil < LOQ 0.40 0.10 pass Flonicamid < LOQ 1.0 0.40 pass
Fludioxonil < LOQ 0.40 0.10 pass Hexythiazox < LOQ 1.0 0.40 pass
Imazalil < LOQ 0.20 0.10 pass Imidacloprid < LOQ 0.40 0.20 pass
Kresoxim-methyl < LOQ 0.40 0.10 pass Malathion < LOQ 0.20 0.10 pass
Metalaxyl < LOQ 0.20 0.10 pass Methiocarb < LOQ 0.20 0.10 pass
Methomyl < LOQ 0.40 0.20 pass Parathion-Methyl < LOQ 0.20 0.20 pass
MGK-264 < LOQ 0.20 0.10 pass Myclobutanil < LOQ 0.20 0.10 pass
Naled < LOQ 0.50 0.20 pass Oxamyl < LOQ 1.0 0.40 pass
Paclobutrazole < LOQ 0.40 0.20 pass Permethrin < LOQ 0.20 0.10 pass
Phosmet < LOQ 0.20 0.10 pass Piperonyl butoxide < LOQ 2.0 1.0 pass
Page 1 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Pesticides Batch 1702363Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 12/1/17 12:00:00
LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes
Prallethrin < LOQ 0.20 0.20 pass Propiconazole < LOQ 0.40 0.20 pass
Propoxur < LOQ 0.20 0.10 pass Pyrethrins < LOQ 1.0 0.50 pass
Pyridaben < LOQ 0.20 0.10 pass Spinosad < LOQ 0.20 0.10 pass
Spiromesifen < LOQ 0.20 0.10 pass Spirotetramat < LOQ 0.20 0.10 pass
Spiroxamine < LOQ 0.40 0.10 pass Tebuconazole < LOQ 0.40 0.20 pass
Thiacloprid < LOQ 0.20 0.10 pass Thiamethoxam < LOQ 0.20 0.10 pass
Trifloxystrobin < LOQ 0.20 0.10 pass
Page 2 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
AbbreviationsLimits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220Limit(s) of Quantitation (LOQ): The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be
reported with a specified degree of confidence.
Units of Measure
g = Gram
mg/kg = Milligram per kilogram
% wt = µg/g divided by 10,000
Derrick TannerGeneral Manager
Approved Signatory
Page 3 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Page 4 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Page 5 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Page 6 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Page 7 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Page 8 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400
12423 NE Whitaker WayPortland, OR 97230
503-254-1794
Job Number:
Report Date:
ORELAP#:
12/01/2017
OR100028
10:00Received: 11/27/17
17-002360
Purchase Order:Purchase Order:
Report#: 030913-00
Code Explanation
Q Matrix interferences affecting spike or surrogate recoveries.
Q1 Quality control result biased high. Only non-detect samples reported.
Q2 Quality control outside QC limits. Data considered estimate.
Q3 Sample concentration greater than four times the amount spiked.
Q4 Non-homogenous sample matrix, affecting RPD result and/or % recoveries.
Q5 Spike results above calibration curve.
Q6 Quality control outside QC limits. Data acceptable based on remaining QC.
R Relative percent difference (RPD) outside control limit.
R1 RPD non-calculable, as sample or duplicate results are less than five times the LOQ.
R2 Sample replicates RPD non-calculable, as only one replicate is within the analytical range.
LOQ1 Quantitation level raised due to low sample volume and/or dilution.
LOQ2 Quantitaion level raised due to matrix interference.
B Analyte detected in method blank, but not in associated samples.
B1 The sample concentration is greater than 5 times the blank concentration.
B2 The sample concentration is less than 5 times the blank concentration.
Explanation of QC Flag Comments:
Page 9 of 9Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.
Testing in accordance with: OAR 333-007-0400