analytical report 6greeleygov.com/docs/default-source/default...the test results in this report meet...

ANALYTICAL REPORTEurofins TestAmerica, Denver4955 Yarrow StreetArvada, CO 80002Tel: (303)736-0100

Laboratory Job ID: 280-132281-1Laboratory Sample Delivery Group: 191219024Client Project/Site: Boyd Lake WTP

For:Colorado Analytical Laboratories Inc10411 Heinz WayCommere City, Colorado 80640

Attn: Angela Forte

Authorized for release by:1/8/2020 10:31:10 AM

Elizabeth Hoerchler, Project Manager I(314)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Colorado Analytical Laboratories IncProject/Site: Boyd Lake WTP

Laboratory Job ID: 280-132281-1SDG: 191219024

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

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Case NarrativeClient: Colorado Analytical Laboratories Inc Job ID: 280-132281-1Project/Site: Boyd Lake WTP SDG: 191219024

Job ID: 280-132281-1

Laboratory: Eurofins TestAmerica, Denver

Narrative

CASE NARRATIVE

Client: Colorado Analytical Laboratories Inc

Project: Boyd Lake WTP

Report Number: 280-132281-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

RECEIPTThe samples were received on 12/19/2019; the samples arrived in good condition, properly preserved. The temperature of the coolers at

receipt was 20.5° C.

PAINT FILTERSamples 191219024-02 Boyd Lake WTP Sludge #1 (280-132281-1), 191219024-05 Boyd Lake WTP Sludge #2 (280-132281-2), 191219024-08 Boyd Lake WTP Sludge #3 (280-132281-3), 191219024-11 Boyd Lake WTP Sludge #4 (280-132281-4) and 191219024-14

Boyd Lake WTP Sludge Comp (280-132281-5) were analyzed for paint filter in accordance with EPA SW-846 Method 9095. The samples were analyzed on 12/30/2019.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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Definitions/GlossaryJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc

SDG: 191219024Project/Site: Boyd Lake WTP

GlossaryThese commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Detection SummaryJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


Client Sample ID: 191219024-02 Boyd Lake WTP Sludge #1 Lab Sample ID: 280-132281-1

Paint Filter

RL

mg/L

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1NO 9095A


Paint Filter

RL

mg/L


Total/NA1NO 9095A


Paint Filter

RL

mg/L


Total/NA1NO 9095A


Paint Filter

RL

mg/L


Total/NA1NO 9095A

Client Sample ID: 191219024-14 Boyd Lake WTP Sludge Comp

Lab Sample ID: 280-132281-5

Paint Filter

RL

mg/L


Total/NA1NO 9095A


This Detection Summary does not include radiochemical test results.

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Method SummaryJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


Method Method Description LaboratoryProtocol

SW8469095A Paint Filter TAL DEN

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL DEN = Eurofins TestAmerica, Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100


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Sample SummaryJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID

280-132281-1 191219024-02 Boyd Lake WTP Sludge #1 Solid 12/18/19 09:30 12/19/19 16:00




280-132281-5 191219024-14 Boyd Lake WTP Sludge Comp Solid 12/18/19 09:30 12/19/19 16:00


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Client Sample ResultsJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


General Chemistry

Lab Sample ID: 280-132281-1Client Sample ID: 191219024-02 Boyd Lake WTP Sludge #1Matrix: SolidDate Collected: 12/18/19 09:30

Date Received: 12/19/19 16:00RL MDL

Paint Filter NO mg/L 12/30/19 14:20 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier













Lab Sample ID: 280-132281-5Client Sample ID: 191219024-14 Boyd Lake WTP Sludge CompMatrix: SolidDate Collected: 12/18/19 09:30





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QC Sample ResultsJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


Method: 9095A - Paint Filter

Client Sample ID: 191219024-02 Boyd Lake WTP Sludge #1Lab Sample ID: 280-132281-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 481935

Paint Filter NO NO mg/L NC

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD


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QC Association SummaryJob ID: 280-132281-1Client: Colorado Analytical Laboratories Inc


General Chemistry

Analysis Batch: 481935

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 9095A280-132281-1 191219024-02 Boyd Lake WTP Sludge #1 Total/NA




Solid 9095A280-132281-5 191219024-14 Boyd Lake WTP Sludge Comp Total/NA

Solid 9095A280-132281-1 DU 191219024-02 Boyd Lake WTP Sludge #1 Total/NA


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Lab ChronicleClient: Colorado Analytical Laboratories Inc Job ID: 280-132281-1Project/Site: Boyd Lake WTP SDG: 191219024

Client Sample ID: 191219024-02 Boyd Lake WTP Sludge #1 Lab Sample ID: 280-132281-1Matrix: SolidDate Collected: 12/18/19 09:30

Date Received: 12/19/19 16:00

Analysis 9095A JDR12/30/19 14:201 TAL DEN481935

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA




Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA




Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA




Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: 191219024-14 Boyd Lake WTP Sludge

Comp

Lab Sample ID: 280-132281-5

Matrix: SolidDate Collected: 12/18/19 09:30Date Received: 12/19/19 16:00


Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Laboratory References:

TAL DEN = Eurofins TestAmerica, Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100


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Login Sample Receipt Checklist

Client: Colorado Analytical Laboratories Inc Job Number: 280-132281-1

SDG Number: 191219024

Login Number: 132281

Question Answer Comment

Creator: Awolaja, Oluwademilade A

List Source: Eurofins TestAmerica, Denver

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact. Not present

N/ASample custody seals, if present, are intact. Not Present

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice. Thermal preservation not required.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

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analytical report 6greeleygov.com/docs/default-source/default...the test results in this report meet...

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