nemc.us final.pdf · the implementation of hplc/post-column techniques for rugged carbamate and...

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2

July 8 – 12, 1991

Table of Contents

Organics ..................................................................................................... 9

Methods for the Determination of Volatile Organic Compounds in Soil Samples ................................ 11

Concentration of Water Soluble Volatile Organic Compounds From Aqueous Samples by Azeotropic Microdistillation ............................................................................................................ 13

Pollution Reduction in the Laboratory Through the Use of Smaller initial Sample Size ........................ 29

Extraction of Phenolic Compounds From Water Samples Using Styrene Initial Sample Size ................... 40

Comparison of Alternative Methods for Analysis for Solid Matrices ............................................... 52

Evaluation of Sample Preparation Methods for Solid Matrices ..................................................... 55

Analysis for Selected Appendix IX Compounds in Environmental Matrices by High Performance Liquid Chromatography/Particle Beam Mass Spectrometry ................................................................. 69

The Implementation of HPLC/Post-Column Techniques for Rugged Carbamate and Glyphosate Analysis .. 83

Determination of Low-Level Explosive Residues in Water by HPLC: Solid Solid-Phase Extraction vs. Salting-Out Solvent Extraction .................................................................................................... 86

Reduction of Azo Dyes to Aromatic Amines for Environmental Monitoring ......................................101

Hazardous Waste Component Identification Using Automated Combined GC/FTIR/MS .......................104

Environmental Applications of Multispectral Analysis ..............................................................117

Sample Preparation Using Supercritical Fluid Extraction Methodology ..........................................119

The Research Status of Supercritical Fluid Extraction for the Analysis of PCBs In Incinerator Ash ..........129

Supercritical Fluid Extraction (SFE) of Total Petroleum Hydrocarbons (TPHs) With Analysis By Infrared Spectroscopy ..............................................................................................................141

Application of Supercritical Fluid Extraction of Dioxins/Furans From Soil and “PUF” ........................150

The Application of Supercritical Fluid Chromatography to the Analysis of Herbicides and Pesticides in TCLP Extracts ....................................................................................................................152

Problem Solving in the Organic Extractions Laboratory: Herbicides .............................................166

Infrared Microsampling for the Qualitative Analysis of Organics Extracted from Soil Samples ..............180

A Performance Comparison Study of Different Types of Devices for Solid Phase Extraction .................182

Standard Reference Spectra for MS/MS Quality Assurance Performance Evaluation, and Proficiency Testing: X[rf]Q Tandern Mass Spectrometers ........................................................................184

Improved Techniques for Formaldehyde Analysis by HPLC Using Automated Sample Preparation and Diode Array Detection ...........................................................................................................196

An Interlaboratory Comparison Study of Supercritical Fluid Extraction for Environmental Samples ........211

An Analytical Manual for Petroleum Products in the Environment ...............................................214

Evaluation of Liquid/Solid Extraction for the Analysis of Organochlorine Pesticides and PCBs in Typical Ground and Surface Water Matrices ...................................................................................216

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July 8 – 12, 1991 Table of Contents cont.

Improving the Analysis of Semi-Volatile Pollutants .................................................................230

Electrospray Combined with ion Trap Mass Spectrometry for Environmental Monitoring .....................239

Recent Advances in the Use of Supercritical Fluid Extraction for Environmental Applications ..............242

Using Supercritical Fluid Extraction to Separate Diesel From Soil Matrices .....................................244

Creative Review of “Tentatively Identified Compound” Data Using the Retention Index ....................256

High Efficiency GPC Cleanup of Environmental Samples- Column Optimization ...............................272

Efficient Aqueous Extraction Using an Emulsion Phase Contractor ...............................................283

SFE Practical Applications for Environmental and Industrial Samples ...........................................291

Inorganics ................................................................................................ 293

Microwave Sample Preparation Methods for Environmental Analysis ............................................295

Comparison of Procedures for TCLP Extract Digestion; Conventional vs. Microwave ..........................298

Sample Decomposition in Closed Vessels with a Pressure Controlled Microwave Oven .......................309

State-of-the-Art of Microwave Digestion Methods for Environmental Analysis .................................311

The Application of X-Ray Fluorescence Spectroscopy for Rapid Hazardous Waste Classification and Screening ...................................................................................................................317

Semi-Quantitative Determination of the Inorganic Constituents in Specific and Non-Specific Categorical Solid Waste Using EDXRF ................................................................................................329

Identifying Sources of Environmental Contamination through Laser Sampling ICP-Mass Spectrometry ....332

ICP/MS Analysis of Toxic Characteristic Leaching Procedure (TCLP) Extract: Advantages and Disadvantages .............................................................................................................347

Chromium VI: An Overview of Its Relevant Environmental Occurrence, Analytical Methods of Quantitation, and Report on Recent Ion Chromatography Methods Development and Validation Activities ................362

Rapid High Performance Microwave Digestion .......................................................................365

The Performance of a Low Cost ICP-MS for the Routine Analysis of Environmental Samples ................367

Robotics for Automated Digestion of Environmental Samples .....................................................370

Application of Laser Sampling ICP-Mass Spectrometry to Environmental Analysis .............................372

Regulatory Compliance ............................................................................... 374

Status of Developing Land Disposal Restrictions for Superfund Soils .............................................376

Certification Protocol for Meeting Organic Treatment Standards for Incineration Ash .......................393

Factors Affecting the Admissibility and Weight of Environmental Data as Evidence ..........................406

Review of Groundwater Monitoring Requirements at RCRA Sites .................................................408

The Paperless Environmental Laboratory: A Plan for Realization.................................................420

Data Management Issues in the Hazardous Waste Industry ........................................................422

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July 8 – 12, 1991 Table of Contents cont.

Air/Groundwater ....................................................................................... 437

New Directions in RCRA Ground-Water Monitoring Regulations ...................................................439

De-Mystifying the Problem of Filtered Vs. Unfiltered Samples ....................................................455

Determination of Target Organics In Air Using Long Path Spectroscopy .........................................471

Measurement of Toxic Organic Compounds in Landfill Gas Samples Using Cryogenic Trapping and Full Scan .........................................................................................................................473

The Determination of the Heat of Combustion and Water Content of Incinerator Feeds Using Near Infrared Spectroscopy ..............................................................................................................475

Source Sampling and Analysis Guidance: A Methods Directory ....................................................487

A Field Investigation of Groundwater Monitoring Well Purging Techniques .....................................496

Analysis of Polychlorinated Biphenyls in Water and Stack Emissions by High Resolution Gas Chromatography/High Resolution Mass Spectrometry ..............................................................517

Continuous Analysis of VOCs in Air Using a New, Phenyl-Methyl Silicone Stationary Phase for High-Resolution Capillary GC ..................................................................................................533

General .................................................................................................. 545

Developing a Uniform Approach for Complying with EPA Methods ...............................................547

Performing TCLP Analyses to Get Meaningful Data..................................................................559

Total Cyanide By Photolysis .............................................................................................562

Ammonia and Total Kjeldahl Nitrogen Determinations Using Flow Injection Analysis with Gas Diffusion ....................................................................................................................564

An Objective Criterion for Terminating Permeability Tests .......................................................580

Sampling and Analysis Plans to Evaluate the Performance of Lead-Based Paint Abatement .................594

Further Evaluation of the Cage Modification to the TCLP ..........................................................606

Comparative Study of EPA TCLP And California W.E.T. for Metals in Different Matrices .....................608

Author Index ........................................................................................... 625

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Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

474

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

475

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

476

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

477

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

478

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

479

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

480

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

481

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

482

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

483

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

484

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

485

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

486

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

487

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

488

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

489

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

490

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

491

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

492

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

493

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

494

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

495

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

496

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

497

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

498

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

499

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

500

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

501

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

502

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

503

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

504

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

505

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

506

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

507

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

508

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

509

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

510

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

511

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

512

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

513

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

514

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

515

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

516

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

517

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

518

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

519

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

520

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

521

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

522

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

523

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

524

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

525

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

526

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

527

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

528

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

529

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

530

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

531

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

532

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

533

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

534

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

535

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

536

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

537

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

538

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

539

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

540

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

541

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

542

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

543

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

544

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

545

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

546

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

547

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

548

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

549

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

550

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

551

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

552

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

553

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

554

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

555

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

556

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

557

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

558

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

559

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

560

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

561

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

562

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

563

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

564

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

565

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

566

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

567

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

568

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

569

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

570

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

571

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

572

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

573

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

574

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

575

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

576

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

577

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

578

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

579

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

580

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

581

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

582

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

583

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

584

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

585

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

586

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

587

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

588

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

589

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

590

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

591

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

592

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

593

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

594

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

595

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

596

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

597

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

598

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

599

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

600

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

601

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

602

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

603

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

604

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

605

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

606

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

607

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

608

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

609

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

610

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

611

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

612

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

613

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

614

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

615

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

616

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

617

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

618

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

619

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

620

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

621

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

622

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

623

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

624

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2 July 8-12, 1991

Index

Alverson, Erik. ............................................... 166

Amick, E. Neal ............................................... 182

Amin, Jakal .................................................. 517

Anderson, Denise R ......................................... 216

Ashraf-Khorassani, M........................................ 242

Atwood, Rita A .............................................. 475

Austiff, Gerald ............................................... 422

Baker, Robert D .............................................. 86

Balas, C ....................................................... 370

Barone, Gary ................................................. 230

Bath, Raymond J ............................................ 471

Baughman, Kim W ........................................... 487

Beckert, W.F ............................................ 55, 119

Bellar, Thomas A ............................................. 11

Bencivengo, Dante J ......................................... 29

Benedicto, J .................................................. 55

Berges, Jack A ............................................... 182

Betowski, Leon D ............................................ 101

Blair, Peter D ................................................ 367

Bloemen, Henk J.Th ........................................ 533

Broadhead, Mark ............................................ 332

Brown, James R ............................................. 439

Brown, Richard D ............................................ 455

Bruce, Mark L ........................................... 13, 141

Bubnis, Bernard ............................................. 564

Buote, Bill .................................................... 295

Buxton, Bruce ................................................ 594

Bychowski, John T. ......................................... 216

Cahill, Marty ................................................. 422

Calvi, J. Phillip .............................................. 564

Carter, Jim ................................................... 196

Colby, Bruce N. ............................................... 29

Coons, J.T .................................................... 608

Cornell, Jeffery L ............................................ 69

Cotter, Richard .............................................. 272

Craig, Carl A ................................................. 244

Cramer, Randy ............................................... 594

Cunningham, Jennifer ...................................... 244

Denoyer, E.R ................................................. 372

Dewalt, Gary ................................................. 594

Dodhiwala, N .................................................. 55

Doeffinger, John ............................................ 166

Dolbow, Kyle ................................................. 559

Dong, Michael W .............................................. 83

Dooper, Rene P.M ........................................... 533

Duba, George A .............................................. 420

Eckel, William P ............................................. 256

Edelman, Dan................................................ 347

Eichelberger, James W ....................................... 11

Elbert, Arnold J ............................................. 475

Fallick, Gary J. .............................................. 272

Fennell, Kat ................................................. 329

Ferko, M.M ................................................... 214

Fitzgerald, Sean ............................................. 166

Foster, Russell ............................................... 272

Fredeen, Kenneth J................................... 332, 372

Freeman, Harold S .......................................... 101

Fuller, M.P ................................................... 180

Genicola, F .................................................. 214

Gianella, Jim ................................................ 166

Goergen, Michael G ......................................... 347

Goodby, Brian ............................................... 196

Greenlaw, Pamela D ........................................ 471

Grillo, A ...................................................... 370

Gutierrez, jenner ........................................... 562

Hagen, Donald F ........................................ 40, 216

Hecht, Charles R ...................................... 129, 152

Hoffman, H.T ................................................ 214

Howe, Ted G................................................. 329

Hoyt, Steven D .............................................. 473

Hsu, Jong-Pyng .............................................. 150

Hsu, W.N ..................................................... 101

Iskander, M.S ................................................ 608

Jackson, Merrill D ........................................... 487

James, Ruby H .............................................. 487

Jassie, Lois ................................................... 295

Johnson, Ann E .............................................. 439

Johnson, Larry D ............................................ 487

Johnson, Teresa S ........................................... 393

Jones, Tammy L ............................................. 211

Karman, Hani S .............................................. 517

Keever, Jeffrey T ........................................... 101

Kelly, Kevin P ................................................ 283

Kettisch, P ................................................... 309

Kingston, H.M ............................................... 295

Klinger, Kristine ............................................. 166

Knapp, G ..................................................... 309

Knapp, Joan O’Neill ........................................ 376

Kobus, Matthew A ..................................... 129, 152

Kolopanis, John W .......................................... 393

Kopera, A.J .................................................. 214

Krecisz, John ................................................ 422

Kuo, Kenneth C.............................................. 283

Lee, Y. Joyce ................................................ 182

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

625

Lee, Richard P .......................................... 13, 141

Leibrand, Roger J ........................................... 104

Levy, J.M ..................................................... 242

Lim, Benjamin S ............................................. 594

Lin, Hung-Yu ................................................. 239

Lobring, Larry B ............................................. 362

Lopez-Avila, Viorica ................................... 55, 101

Lordo, Bob ................................................... 594

Loring, Deborah ............................................. 547

Lott, Chris .................................................... 166

Lowry, Jeffery L .............................................. 69

Luka, Kerri G ................................................. 406

Maltby, Van .................................................. 496

Marcus, Mark F......................................... 152, 317

Markell, Craig G ........................................ 40, 216

Marti, Edwin A ............................................... 517

Martinez, Richard I .......................................... 184

McGuire, John M ............................................. 117

McHugh, James .............................................. 594

McKee, T.M................................................... 298

Meyers, Mark S ............................................... 580

Mignon, Paul K ............................................... 291

Milanes, J...................................................... 55

Miller, Gregory P ............................................ 150

Miller, M.W ................................................... 214

Moses, Michael ............................................... 365

Mosesman, Neil. ............................................. 230

Murshak, Issiah .............................................. 347

Murshak, Violetta F ......................................... 347

Myer, Leslie J.D ............................................. 291

Myer, Vernon B .............................................. 439

O’Donnell, Anne D. ......................................... 216

Olbrot, Roger M ............................................. 329

Pan, Joseph C ................................................ 150

Panholzer, F ................................................. 309

Parr, Jerry.................................................... 547

Petersen, Jim ................................................ 295

Pickering, Michael V. ........................................ 83

Pleva, M.A .................................................... 295

Pospisil, Peter A ........................... 129, 152, 317, 475

Prashar, Suman .............................................. 244

Price, Jody ................................................... 559

Rettberg, Thomas M ........................................ 367

Richter, Bruce E ............................................. 244

Robertson, Gary L ........................................... 182

Roettger, Michael G ........................................ 347

Rossell, A.C .................................................. 242

Rothman, Nancy ............................................. 547

Rubin, Ron ................................................... 365

Rust, Steve ................................................... 594

Ryan, James F ................................................ 52

Ryan, Phillip W ............................................... 29

Rynaski, Amy ................................................. 244

Schalk, A ..................................................... 309

Schlaeger, Larry ............................................. 196

Schofield, William R ........................................ 393

Schrier, Loren C ............................................. 283

Schwemberger, John ....................................... 594

Seeley, R. Craig ............................................. 367

Settle, F.A ................................................... 295

Shah, Nilesh ........................................... 317, 475

Sivia, G.S ..................................................... 608

Sleevi, Peggy ................................................ 547

Smith, Deborah .............................................. 166

Spafford, Ralph B ........................................... 487

Spear, Richard D ............................................ 471

Stanton, Larue .............................................. 166

Stephens, Marvin W ..................................... 13, 141

Stelz, William G ............................................. 408

Tatro, Mark E ................................................ 311

Taylor, Chandler ............................................ 317

Tehrani, Joe ................................................. 291

Thomas, R.J ................................................. 372

Troast, Richard. ............................................. 376

Unwin, Jay P ................................................. 496

Van Kley, Harold ............................................ 317

Vargo, Christine ............................................. 230

Vasavada, Smita ............................................ 196

Verma, V.L ................................................... 298

Villalobos, Kevin ............................................ 150

Voice, Thomas C .............................................. 52

Vonk, Nico ................................................... 533

Voyksner, Robert D ................................... 101, 239

Walter, P ..................................................... 295

Weesner, F.J ................................................ 180

Weichert, Bradley A .......................................... 86

Wellman, Richard L ......................................... 272

Weston, Alan F .............................................. 517

Wetzel, David L ............................................. 475

White, Paul .................................................. 606

Winslow, Michael G ........................................... 86

Wittwer, Teresa. ............................................ 166

Worthington, Jeffrey C............................... 406, 420

Yagley, Timothy J ........................................... 517

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

626

Seventh Annual Waste Testing and Quality Assurance Symposium Vol. 2, Washington D.C, July 8-12, 1991

627