figure 1 – average aliphatic carbon chemical shifts

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CCPNmr Analysis solid-state MAS NMR tutorial figures 1

Figure 1 – Average aliphatic carbon chemical shifts

CCPNmr Analysis solid-state MAS NMR tutorial figures 2

Figure 2 – The glycerol labelling pattern (Averages)

Blue: labelled in the 1,3-13C glycerol sampleRed: labelled in the 2-13C glycerol sample

CCPNmr Analysis solid-state MAS NMR tutorial figures 3

Figure 3 – The glycerol labelling pattern (Isotopomers)

Blue: labelled in the 1,3-13C glycerol sampleRed: labelled in the 2-13C glycerol sample

CCPNmr Analysis solid-state MAS NMR tutorial figures 4

Figure 4 – Spectrum Types

PDSD

CCPNmr Analysis solid-state MAS NMR tutorial figures 5

NCACX

NCOCX

CCPNmr Analysis solid-state MAS NMR tutorial figures 6

Figure 5 – Threonine motifs in the chicken -spectrin SH3 domain

Blue: labelled in the 1,3-13C glycerol sampleRed: labelled in the 2-13C glycerol sample

CCPNmr Analysis solid-state MAS NMR tutorial figures 7

Figure 6 (a) – Peak clusters in a PDSD of uniformly labelled SH3

Figure 6 (b) – Peak clusters in a PDSD of 1,3-13C glycerol labelled SH3

CCPNmr Analysis solid-state MAS NMR tutorial figures 8

Figure 6 (c) – Peak clusters in a PDSD of 2-13C glycerol labelled SH3

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