appendix g sub-area 3.1.11-3.1.15-coa
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Appendix GSub-Area 3.1.11- 3.1.15- COA
GEL LABORATORIES LLC 204D Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: December 4, 2015
Company : MJW Corporation Address: 15 Hazelwood Drive
Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Losey Project: Soil Radioisotopes
......................................... ·-··-····-····· ...... . Client Sample ID: 3.1.11.E. l
Sample lD: 385070002
Matrix: Soil Collect Date: 21-0CT~ 15 13:35
Receive Date: 05-NOV-15
Collector: Client
Moisture: 22.8'%
Parameter Result Uncertainty
Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moi~ture 22 8
Racl Gamma Spec Analysis Gammaspec, Gamma, Solid Actimum-227
"Dry Weight Corrected"
A11t1mo11y- l 25 Cesium-137 Colw.lt-60 Europium-154· Prota~Lin:tum-23 l
Radmm-226 Radium-228
ll 0 l67 +/-0.254 u 0.053 l ..-/.().104
ll u u
0 984 +l-0 0988 -0.0236
0.l45 0.476 0946
l.23
+l-0 0349 +/-0.JJI +/-0.571 +/-0 149 +f-0.325
Tin-126 U! 000 +/.() 126
Rad Gas Flow Proportional Counting
GFPC, Gross A!B. solid "Dry Weight CotTected" Alpha \3.S .. 1 .. 3 32 lkta 21 0 ·+2 81
}'~e .f.~11.l:J~i.~~ .. :P!.epJ-:1.~~~~~~.·v~r~ .P.".f.f(ll_11~~~: ................. . Melhod Descriptfon oiy· s·c;i1 rrer... ...... .. .. .. .. · ... or;·sc;1rr·icil cir:.~1~,;;:o:A:-02 i .. · .. · T.~.e .f.o.1.19"".i.n!?..0n.alr.ti.c~! M.~Uto?s_ ."\:~r~ ~e~f.o.rt1l~~'. ... _ M~tho.g ...... ... .. .. . . ...... .J=?!':~~r.iptjqn .. .. .. .. . .. . . .. . . . ..
/ISTM D 2216 (Modified)
2 DOE HASL 300. 4.523fGa-O1-R
3 Ef'A 900.0ISW846 93!01SM 71 IOB Modified
Notes:
Project: MJW(OO! 15
Client ID: MJWCOOI
MDC RL Units
percent CXCl 11110'15 1319 1521842
(J 482 pC1/g RXF2 \2/03/15 0846 1522383 2 0 llJ7 pC1lg
ll 0738 0100 pCrlg 0060 pCi!g () 255 pCi!g 0 840 pCilg 0123 pCi!g 0 26(> pCi/g 0.135 pCi/g
J 46 4.00 p('1/g KXB2 12i02/15 1112 1525757 3
3.25 10.U pCi/g
·······-··-··· ······-· Analyst Date cxC:;i· .. · .... · ·-i'iiioiis
Time Prep Batch .. i3f9 ... ··-·i52i 842'" ............ - ·- ·······-··-··-
. ........ ,. .. . . .. . . . .. .AiJ.?..LY~LC9-.lillT!f.ltl_tS. ... _ .
Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma}.
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com
Certificate of Analysis
Company: Address:
MJW Corporation 15 Hazelwood Orive Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Lose}
Project: Soil Radioisotopes
Client Sample ID: 3. l.11.E.1 Sample ID: 385070002 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV- l 5 Collector: Client. Moisture: 22.8%
Parameter
Gravimetric Solids 1IST:'vl D 22 l 6 % llois1ure "As Received"
Moi~turc 22 8
Rad Gamma Spc~ Allalysis Gammaspec, Gamma. Solid "Di:v Weigl1t Cor1·ected"
Actmrnm-227 U 0.167 +/-0 254
Antimony-125 U 0.0531 +/-Q.104
Ilisnmth-212 Bismuth-214 Cesmm-137 Cobalt-60
. Europium-154
Lead-212 Lcad-214 Potassium-40 Prota.ctinium-231 Radium-226
Radium-228 Thallium-208
u Ul
UT
1.53 0 946
0. 984 -0.0236
0 00
I 29
I 23 16 5 ouo
().~46
I 23
0364
Tin-126 UI o.oo Rad Gas Flow Proportional Counting
GFPC. Gross AB. solid uD1:1' Weighi Corrected'' Alpllil 13.8 Beta
The following Prep Methods were performed ~1~tl;~d·- . . ...... ·oc;~~·iptii;;:; ... · ............................. .
D1y Soil Prep Dry Soil Prep GL-RAD-A-02 \
T~c. fol.lowi11g_~lt~.1~:t.i~~l. ~l~th.ll~~-·'V.e.rc.P~l'.f.l>':".•~e~ :.\'let hod Description
ASTM 02216 (Modified)
2 DOE HASL 300, 4.52JiGa-O\-R
+/-0.832
+(-0 149 +/-0.0988 +l-0 0349 +/-0.13\
. <-/-0. \29 +/-0. \91
+/-!.34
+1-0 572
+/-0.149 +1-0 325
+/-0_0786
+/•O 126
+/-3 32
+/-U\
J EPA 900 OiSWS46 9310/SM 71 IOB Modified
Surrogatefrracer Recovery Test
Report Date; December 17, 2015
Project: Client ID:
MJWCOOl 15 MJ\\/COOI
MDC Le TPL' RL Date Time Batch Mtd. ..... -···-·-·· ... ·-· -- - ·--- .. ···-·· ......... -· ..... .
p~rccnt CXCI 111!0/15 1319 \521842
0.41>2 0 228 +/-0.266 pC1lg RXF2 l2i03115 0846 1522383 2 () !97 00925 +J-0 107 pC1/g
0 628 {) 279 +1-0.847 pC1/g
iJ. 123 (}057 +/.0.168 pCilg 0 0738. 0.0343 +1-0.127 () 100 pC1lg
0.060 00261 +1-0.0J65 pCi/g
0 255 0 l \7 +/-0 147 pCilg ()I 12 () 0531 +/-(} 165 pCilg
0 139 O Of>53 +/-0.216 pC1lg
(1455 (l 189 4·/-1 9<i pC1/g
0 840 0.394 '1·/-0 582 pC11g
l) 123 0 057 +l-0.168 pCilg
0 266 () 122 +f-iJ.381 pCr!g
0 0624 0 0288 +/-0 0&43 pCi!g l) 135 0064 +/-0.128 pC1/g
3.46 1.51 +l-4:B 400 pCi!g KXB2 12102/15 l l 12 1525757 3
3 2.5 1.54 +/-4.09 10 0 pCilg
········· .... '' .... .. ·--·-····· .. -····· . Analyst Date Time Prep Batch
······· ........ ···- ...... , ..... CXC! I tl!O/l.5 \319 !521842
.... ···-· .. ···-····· ············ ...
..... -······ .. . ...........
Batel! ID R~cover)'% Acceptable'.Limils
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.geLcom
Company: Address:
Contact:
MJW Corporation 1.5 1-fazelwood Drive Suite I 12 Buffalo, New York 14228
Ms. Laurie Losey
Project: Soil Radioisoto:pc~
Client Sample 10: 3.1.11.E. l Sample ID: 385070002
Certificate of Anal,ysis
·Report Date: December 17, 2015
Project: MJWCOOl 15 Client ID: MJWCOOl
Parameter ....... -.... _ ..... .9.u.1tli.rii:r._ ···- .. ~~s.u.it ... ~;n~c;.J:tj!Jn.~ ....... :VIDC' Le ..... _JP_L ... ~.L.. _ l'ni~s DI' Anal}'s; Dat_c !i.l_lle .ll.~~4?~ ... ~~td. Surrogi1ti!ffracer Reco,•ery Test Batch lD l<cco\·cry% Acceptable Limits
Nutes: TPU and Counting Uncertainty are calculated at t11e 95% confidence level ( 1.96-sigma}.
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Certificate of Analysis
Company: Address:
Contact:
MJW Corporation 15 l!azelwood Drive Suite 112 Buffalo, New York 14228
Ms. Laurie Losey
Project: So.ii Radioisotopes
Client Sample ID; 3.1.l l.E.1 Sample JD: 3&5070002 Matrix: Soil Collect Date: 21-0CT- I 5 Receive Date: 05-NOV-!5 Collector: Client Moisture: 22.8%
.l'a.r.~.rr_i.eter_ . . . .......... 9~.'.'!i_fic~~-- Res11I~ ...... r.o.c.cr.!ai.~.t~· ......... i\'IDC Le
Gravimetric Solids ASTM D 22 J 6 ·% A-Jois111re "As Received"
Moisture 22. 8
Rad Gamma Spcc Analysis Gammaspec, Gamma, Sa/id "D1:;· Weigfu Corrected''
Actinrnm-227 U 0.167 +/-0.254 Antimony-125 U 0.0531 +/-0 104 Bismuth-212 I.SJ +/-0.832
B15mulh-214 0 946 +/-0.149 0!$1Um-!J7 0.984 +/-0 0988 Cobalt-60 U -0.0236 +/-0.0349
Europium-154 l)I 000 +/-0131 Lead-212 1 Z9 -t-/-0 129 Lcad-214 1 2J +/-0 191
Potassium-40 Protactinium-231 Rildium-226 R~dium-228
Thall ium-208
Tm-126
!JI
U!
Rad Gas Fiuw Proportional Counting
16 5 (] 00
0.946 1 23
0.364
000
GFPC Gross A.B, solid "D1:J' Weight.Corrected" Alpha 13.8 Beta 21.0
I.h..e. foll.~~~ng P.i:ep !\_:f~t~1~~s- n:~re pcrfo_r~~~- ...... . Met bod Description
DI)· Soil Prep Dr;.· Soil Prep GL-RAD-A-021
+!-I 34
+/-0.572
+l-0 149 +/-0.315
+/-0 0786 +/-0 126
+/-3.32 +/-2 81
The following Analytical Methods were performed ~i~ii;~;i · ·· ··- ···--o~;;~.··ipii~~ · · · ·-- ··· · ·--· ···· ·· ·· ··· · · ·
ASTM D 2216 (Modified)
DOE I IASL 300. 4 S.2 3/Ga-01-R
3 EPA 9000'SW846 9310/SM 71 IOB Modified
Surrogate/Tr~lccr Rceo~·ery Test
0.48~
O.l97 0628. 0 123
0.0738 0 060
0.255 0. 112 0.139 () 455
!1840 0123 0 266
00624 0.135
3.2:5
\) 228
0:0925 0 279 0057
00343 00261 0l17
0 0531 1).0653
0 189 0.394
0 057 () 122
0 02&8
ow~4
1.51 1 54
Analrst .. ···-· -··-··-··-·
CXCI
Project: Client ID:
TPt:
Report Date: Dcccmber·l7, 2015
MJWCOOl 15 MJWCODI
........... -···
~/-0.266
+/-D.107
+/.() 847
+/-0.168 +/-0.127
+/.() 0365
+/-0 147 +/·0.166 +1-0216
+/-1.96
+f-0 582 +1-0 108 •/-0.381
+/-1) 0843
+/-0 128
+/-4 33 +/-4 09
pcrccm
pCi!g pCl/g
pCilg
pC1tg
0 100 pCi/g
pClfg
pC1/g pCi/g
pCilg pCi/g
pCi/g pCi!g. pC1/g pC1ig pC1lg
4 00 pCiig
HJ 0 pC1/g
Date Time
l 1110/15 1319
CXCI 1 l/lllll5 1319 1521842
RXF2 12103115 (l84ri· 1522383 2
KXB2 12102115 1112 1525757 3
Prep Batch
1521842
Batch ID Rt>eovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 1422&
Contact: Ms. Laurie Losey
Project: Soi! Radioisotopes
Client Sample ID: 3.1.11.E. I Sample ID: 385070002
P:i 1:n.TI1 etc r .. . . . . .. _ . .. ____ 9.IJ _;i_li_li~.r- _ -· .. _ .~es~_l_t Surrogatcfl'raccr Recovery Test
Certificate. of Analysis
Report Date: December 17. 2015
Project: MJWCOO I 15 Client ID: MJWCODI
.. l'n~~rla_ifll.Y ....... _i\I~~~ ...... Le ........... 1~!.'!' ......... R.-.J,. .. l!nit~ DF .A.n:1Iy_s~ ... _.))i1ti;. T.i.llle B_atcl1 Mtd.
Batch ID Rccorcry% Acceptable Limils , ..... ·- ...... --·-··-· -· . ·-- . . ... . . . .. . ... . . ... .. . . .. .. .. .. . . .. .... -·· .......... ,_ ...... ······-·· ..... ·--· ....... ·- ··-··-·· ............ -.................... .
Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma).
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Certificate of Analysis
Company: Address:
MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact Ms. Laurie Losey
Project: Soi! Radioisotopes
Client Sample ID: 3. l .1 I .E.2 Sample ID: 389296007 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.&%
-~~~a~1.e~~r. .............. 9u11)_i~~r .. Re_s!1_1t_ .... _ l)!cert.~h1f\: ......... J\:1.DC Le
Gravimetric Solids AST:\.! D 22 I 6 % Moiswre "As Recei•·ed"
Moisture 22.8
Rad Gamma Spec Analysis Gamma with fngrowrft "D1:i· Weight C'on·ectc:d"
Aotimurn-127 U -0.00461 Antimony-125 B1smutl1-2 I 2 Bi~muth-214
Cesium-137 Cobah-60 Europi111n-154 Lcad-212 · Lead-214 Porassium-40
Prornctinmm-231 Radmm-226 Radium-228 Timll mrn-208 Tin-126
lJ
u u
LI!
lll
-01)71)9
1 07 1.18 I 35
ll.00937 O.CJS62
I 25
I 17 15 4 000 I 18 1.23
0.424
0 00
+/.()JOU
+/-0.134 +/-0 710 ... l-0 2UO ... /.!J.136
+/-0 0501 +/-0.145 +/-0 134 +/-0 174 +/-1.72
+l-0 763 +/-0200 +/-0.388
+l-0 0832 +/.!l.0899
Gammaspec. Gamma. Sa/id ''Dry Weii?ht Correc1ed'' Ac1mrnm·227 l! 0. 127 +/-0 443 Antimony-125 lJ -0.0984 ·t-/-0 l6n llismuth-212 lJ 0 37\ +/.() 956 llismulh-214 IJ \!18 +/-0 235 Ce~ium-137 144 +1-0.183 Cobalt-60 U -0 0486 +/-0.0489 Europium-154 U -0.0346 +/-0. l 7.J. Lead-2 !2 I 41 <-/-0 181 Lead-214 0.988 •/-0.2;i0 Pota>sium-40 Protactinium-23 I Radmm-226 Radmm-228 'rballium-20& Tin-126 \J
Rad Gas Flow Propo11ional Counting
14 7 0.00
0.918 1 78
0 316 0 0695
GFPC. Grass A;B, solid "D1:1' We/gJ11 Corrected" Alpha 12.4 BelD 23.l
+/-2 43 +l-l 16
+/-0.235 +/-0 417 +l-0.121 +/-0.156
-t-f-3 64 +l-3 .J.4
0 5.60 0.232
I CIS ll 157
0 0821 0 ()994
0 3()1
0.113 0 171 0.931 (1.960
0 263 0 107 0472
I) 07t4
0.037! 0 043--1
(l 133 () 053
00798 0 404
0446 !) 157 0.0714 0266
0.0755 0.112
0805 019!
1 93 U.220 (1.115
00725 0.349
0 163 0.221
l 42 I 20
0220 () 537 0 11:5 0 233
393 418
0.116 (J 0342
0.0537
0 375 0.131
0 866
0.0972 ll 051.}3 ()0239
u 141 0.0759 ()JOO (} 585 11543
() 0972 0.'..:36 [)051
ll lll.
I 67 1.99
Project: Client TD:
Report Date:
MJWC00115 MJWCOOl
l'cbrual)· I 0, 2016
.. n.c ..... _RL. Y.11its DF .. A_1111lys.t. _Uat_c Frn.c.J3a_t~l1 .. :\ltd •
+1-0.300 +/-0 138 t-l-ll 718 +/-0.223 +/.() 174
+/.O 0503 ·+1.0 150 "-f-0216
+f-0 208 +/-2 20
-t-/.fJ.787 +/-0.223 +1-0.433
+/-0.0906 .. /-0.0937
+/-0.447 +/-0.172
+l-0 971 +/-0.246 +/-0.216
+/-0.0537 +/-0.175 +/-0.21(1 ·'1-0.2(13
+/-2.74 +/-1.20
"'-l·0.246 -rf-0 469
+/-0 123 .,./-0.157
+/-4 37 +1-4 78
0 \00
0.100
perccnL
pC1/g pC1/g pC1/g pCitg pC1/g pC1ig pC1!g pci;g pC1/g pCi/g pC"tlg pC1.lg pCi/g pCr/g pCilg
p('1!g pCi/g pC1/g pC1/g pCilg pC1!g pCifg pCi/g pCi/g pC1/g pC1tg pC1/g pCilg pC1/g pCtlg
4 Oil pC1/g lOll pCi/g
CXC! 01114116 120S 1537312
RXF2 02i05/I& 0744 1537546
RXF2 01/l8/16 1004 1537545
KXB2 01126116 1 !50 1539462 4
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address:
MJW Technical Services 15 Hazelwood Drh•c Suite !12 Buffalo, New York l4228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample l D: 3 .1.11.E.2 Sample JD: 389296007
Parameter
~rhc_f.ollo~\:i~g_Pre_p ~!~!~'.ld.~_\\:ei-e.11.crfor.mcd -· -·· ..... Method Dc~criplion
Dry Soll Prep Dry Soil Prep GL-R.AD-A-021
Jl1c JO..l!.O..'l\'.i_l})J_r\'.'a.lyti_c~.1.'\'.lc_t~.n.~s.~\:C.re P£'.'.f()~Tl_l~.~ ..... '.\lcthml Description ............................................. I ASTM D 2216 (Modified)
2 3
4
DOE l·IASL 300, 4 5 2 3!Ga-O I ·R
DOE HASL 300, 4 5 2.3/Ga-01-R
EPA 'JOO OiSW846 9310/SM 71 IOB Modifkd
Surrogateffraccr Recover)' Test
Notes:
Certificate of Analysis
Report Date: Fehrual)' I 0, 20 l 6
Project: l'vUWCOO I LS Client ID: MJWCOO l
······ ........ . . . !\IDC i,c ..... TP..l.'. ......... ~.L ... _\n_its ... 9.Y... :'.\naly_s1 ...... l>!1t~ T_ime .. IJ.atc~. ~·ltll_.
... ·······-·· ........ ··············-·· ..... . ................. . Analyst Date Time Prep Batch
CXCI 01114116 1208 1537312
Batch IIJ Recovery% Acceptable Limils
TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Certificate of Analysis Report Date: December 4, 2015
Company: Address:
Contact: Project:
MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228 .Ms. Laurie Losey Soil Radioisotopes
.......... ··-·-··-·-----·····-- ·-·-·. . . .... -··- ....... ·--· .. . -·· -· - .... ·-· ............ . Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture:
3. L.12.E.1 385070003 Soil 21-0CT-15 10:25 05-NOV-15 Client 22.6%
Parameter Qualifier Result Uncertainty MDC .............. --·-· .......... ·-·· ..... .... . ... ··-···· .. . ............ .
Gravimetric Solids ASTM D 2216 % Moisture ''As Received'' Moisture 22 6
Rad Gamma Spec Analysis .Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 U iJ 0126 +/-0 297 Antimony-125 lJ -0107 +/-0.111 Ccs1um-l37 Cobalt-60 Europitim-154 Protuctinium-231 Radium-226 Rad1um-228
u .u
LI
Tm-126 . lll
Rad Gas Flow Proportional Counting
!OS -0 0284
0 0371 0.666
I 06 141 0.00
GFPC', Gross A/B, solid "D!Y Weight Corrected" Alpha l6 3 Bm M4
+1-0 120 +l-0 [1415
+1-0.134 +/-0.642 +/-0.187 +!-0 282 +J-0 133
+/-3 'JS +/-3.40
T~~ foU.?~!11~ .~~-~P. .~1.~t~~d~ .\Ve.re perf.~r.rn_ed:_ ....... .
0 53R 0.189
O.On6 0072 0251 0.997 0 145 0259 0.157
3.95
"01
RL
0 lOO
400 100
Project: Client ID:
Units
percent
pC1lg pC1!g pCi/g pC1/g pC1/g pCilg pC1/g pC1/g pC1/g
pCi!g pC1lg.
MJWCOOJ 15 MJWCOO!
CXCI 11110/15 1319 1521842
RXF2 !2i03/l5 0846 1522383
KXB2 12102115 1112 1525757
Method Description Analyst Date Time Prep Batch or:;:·.sotfiir.eP _ ..... -· ····- .. . .. ····b"ry· S-Oii"Prep-·nL:RAD~~.(-t)2'1 · .... . ·· ···cxc1 · ·· ···· · ····· frfioTis - · · ·f3·1··i ... 1.5}t"842" ..... ·-·. ···-·· -·-· ..
.. The. .f.ol!o\'>' l.~¥-~~.1.a.l)~ic~l .. 1\1.~t~~~-s.v.-.e.r~y~rr.~~lll.e.d: .............................. . J'y1~th~9 .. -···· .. ... . .. . .. .. , .. J;?_e_~cript.(CJ.n .... . ... . ................... . I ASTM D 2216 (Modtficd} 2 DOF. HASL 300, 4 5 2.3/Ga-Ol-R
3 · EPA 900.0iSW846 9JIOISM 71 lOB Modified
Notes:· Counting Uncertainty is calculated at the 95% confidence level ( l.96-sigma).
2
3
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gef.com
Company: Address:
Contact:
MJ\V Corporation 15 Hazelwood Drin! Suite 112 Buffalo. New York 14228
Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.l.12.E.1 Samp[e ID: 385070003 Matrix: Soil Collect Date: 2 l-OCT-15 Receive Date: OS·NOV-15 Collector: Client Moist11re: 22.6%
. . .... -··· ········ .....
Certificate of Analysis
.. ........................ ... .....
Project: Client ID:
Rcpo11 Oate: December 17, 2015
MJWCOOl 15 MJWCOOl
Parameter . . . ...... ... . Q.u~~-ifi~1:. Result J:n.cl!r:tainty ... )\.1D( Le ... Et: ..... RL .... ~'ni!S_. P..F.. :~11.~l~·st ___ [)JjtC !im.~ _B_a!~h .. ~l.t~.
Gravimetric Solids ASTM D 2216 % .\.foi:slm'e "As Rec<?ived"
Moisture 22 6 percent CXCJ 1 l/10/1.5 Bl l) 1521842
Rad Gamma Spec Anal)'Sis Gammaspec, Gamma, Solid "D1:v 11-"<!iglll Corr<?Cll!d"
Act!mum-227 ll 0.0126 +1-0297 {) 538 0.256 +/-0 297 pC1/g R..'i:F2 12103/\ 5 0846 1522383 2
Antimony-125 u -0 IU7 +/-0 111 0 189 0 0889 +/-0 \21 pCt/g
Bismlllh-212 UI 000 +/-0 968 1 27 () 598 +/.J 17 pC1!g
Bismuth-214 I 06 +1-0.187 () 145 0.0678 +/-0 208 pC1/g
Ccsiwn-137 1.05 +/-0 120 0.0736 110342 +/-0.151 O.IOO pCi/g
Coball-60 u -0 0284 .. ,.() 0415 0()72 (1.0321 -.-/-0.0435 pCi!g
Europium-154 u 0.0371 +i-0 134 0.251 0.115 +l-0.135 pC1!g
l.ead-212 !..35 H-0 140 0 l \7 (I 0559 +/-0.175 pC1/g
L~ad-214 14(} +/.O 182 0 329 0.161 +/-0.212 pCJ/g
Polassmm-40 \8 3 +/-1.45 0.h80 li.3()2 +/-2 IJ pCi/g
Protuctimum-231 Ul 0.00 +/-0.642 0 997 0474 +/-0 ()59 pCifg
Radrnm-226 1.06 +/-0 187 0 145 lJ.0678 +i-0 .. 208 pC1lg
Radium-228 1.41 +/.Q 282 ll.259 0.119 +/-0.319 pC1tg
Thalliurn-208 0.407 ... /.().07\ () 0677 (Ul3!.5 +/-O.ll791 pCi/g
Tm-126 Ul 0.00 ..-/-0.133 0 1.57 00756 t/.(J 135 pC1lg
Rad Gas Flow Propol'tional Counting GFPC. Gross A B, solid "DrJ' Weight Corrected''
Alpha 16 3 +1.3 98 3.95 169 +1-511 4.00 pC1/g. KXB2 12i02/15 1112 1525757 3
Beta 26 4 +1-3 40 4 01 I 'JI +l-5.01 100 pCilg
·1:~c_f,o]!o,\~i1_1g_P_r:f.'.P._!\I~~~~~-8 w~r~ __ per.ro_rm.ed.. ....... -· . !\-Ictlrnd Description Analyst Date Time Prep Balch
OO>•M•••• "'"''
Dry Soil Prep Dry Soil Prep GJ.-RAD-A-021 CXCl l \ll0/15 1319 15218~2
T_h_e._follcnying_r.'\n_al~:t\c~.1.'.\Ie.th_l)~S-~~.r.'.!Jll!rf.nrm~d :Viet bod Description
ASTM [)2216(Mod1fi~)
2 DOE HASL 300. 4.5 2 3.iGa-01-R
3 El'A 900UISW846 9310JSM 71 JOB l\fod1fied
Su rrogatcffracer Recu"·ery Test Balch ID Recovery% Acceptable Limits
, . '
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14.22&
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3. !.12.E.l Sample TD: 385070003
Surrogateffracer Recovery Test
Notes:
Certificate of Analysis
Report Date: December 17. 2015 ·
Project: MJWCOOl 15 ·Client ID: MJWCOOI
Batch ID Recovery% Acceptable Limits
TPU and Counting Uncertainty are calculated at the 95% confidence level ( l .96-sigma}.
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Certificate of Analysis
Company; Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York !4228
Contact Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample TD: 3. LI 2.E. ! Sample ID: 385070003 Matrix: So fl Collect Date: 21-0CT-15 Receive Date: 05-NOY-15 Collector: Client Moisture: 22.6%
Parameter
Gravimetric Solids ASTJf D 2216 % Moisture "As Rrtcdved"
Moisture 22.6
Rm.I Gamma Spec Analysis . Gammaspec. Gamma. Solid "Dry Weight Corrected"
Actinium-227 !J 0 0!26 +/.O 297
Aniimony-125 U -0 I 07 "'-/·O 111 Bismuth-212 UI 0.00 ·+/-0.968
Bisnrnth-214 Cesium-137 Cobalt-60 Europmm-154 Lead-212 l.ead-214 POUIS~lllm-40
Protactmium-231 Radium-226 Radium-228 -Thallium-208 · lm-126
u u
Ul
Lil
Ratl Gas Flow Proportiunol Counting
1.06 I OS
-0 0284 0 0371
1.35 I 40 18 3 ll.00
l.06 141
0407 o.on
GFPC. Gross A·B. solid "Dry Weight Correc/ed" Alp\la 16 3 B~ ~A
+/-ll.187 +/.(l 120
+/-0 0415
+/-0.134 +/-0.140 +f-0 182
+/-1 45 +/-0642
+/-0. 187 +(.() 282
+/-[) 071 +/-0 133
+/-3.98 +-/-3.40
J'h~f()l_~~~v,i,1~1; !'.r~P ~-i,c_t~_o_~S. ~v,e.~e..P..e~.fn_r.~1~.d ...... . l\-tcthod Description
Dry Soil Pr~p DJ}' Soil Prep GL-RAD·A-021
I~.e. .~IJIJ.0.1~'.ill~.t'\'!:ll)'tic!,ll ~c!.h.t_l~S '''.c.rc __ p_crf()J'.111.e.d. .... Method Dc~cription
ASTM D 2216 l Mod1ticd)
2 DOE HASL 300, 4 S2JiGn-01-R
3 EPA 900.0fSW846 9310/SM 7l 10B Modified
Surrogatefl"raccr Recovery Test
Project: Client rD:
Repoct Date: December l 7, 2015
MJWCOOl 15 MJWCOOJ
M.!?~~- ..... Le ..... TJ>~' .... _RL .. l1nits DF Anjjlyst .. _D_a~~-I!'-1.!~ .. B_:t_!~l.!.. ~~!t~ ..
percent CXCl 11110115 1319 1521842
0 538 0 256 +1-0 297 pCi/g RJff2 12103115 0846 1522383 2
0 189 0 088'> +l-0 l2i pC11g I 27 0598 +1-1.17 pC'i!g
0 145 0 0678 +/-0 208 pCifg 0.0736 0.0342 ··1-0. 151 0.100 pCilg
0.072 0 0321 +f.().0435 pCllg
0251 0.115 +l-0 135 pCt!g IJ! l7 OOWJ +/-0. 173 pCi/g
0.329 0.161 +/-0 212 pCi!g 0680 l) 302 +/-2 13 pCi!g 0997 0.474 +/-0 659 pC1/g () 145 () 0(>78 +/-0 208 pCilg 0.259 () 119 +/-0 319 pCi/g
0.0577 (I 0315 +l-0Jl791 pCi/g
0 157 0 0756 +/-0. 135 pCilg
·' 95 169 +-1-5. l I .i. 00 pCi/g KXB2 12102115 1112 1525757 3
4.01 1.91 +l-5 0 I !0.0 pCl/g
!)ate Tinic Prep Batel!
CXCl 11/10115 1319 1521842
Balch ID Recovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.get.com
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact Ms. Laurie Losey
Project: So.ii Radioisotopes
Client Sample ID: 3.1.12.E.1 Sample lD: 385070003
Certificate of Analysis
. . . .. . .. . . . . .. ··-· -.................. ··-·" -··. --··· .. . ... . .. . . ..... ~. ... . . . . ..... . ., . . .. . . . . . - ·-·. - .. -·· ·-· ··-· ............... -........ ···- .
Report Date: December 17. 2015
Project: MJWCOOl 15 Client ID: MJWCOOJ
. ~a.ralll~!.e~ .... ... . . ........ _9.l!a!if!c.i: _ ···-· l~c_s~_ll __ . J ·n~cr~aint~: .. . _i'r1J:)<;::_ . .. . ~c. . . _._F'.~' -· . _. _ -~~ ___ _l~n~ts. . _ I:>.F. .. :~.~'.l_lyst. ___ 1)at_c __ !_i_~£- _B~f..c~. :\~_t_d.·.
Surrogatcffraccr Recovery Test Batch ID Recovery% Acceptable Limits
Notes: TPU and Counting Uncertainty are calculated at t~e 95% confidence level ( ! .96-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 • (843) 556-8171 - www.gel.com
Company: Address:
MJW Technical Services 15 Hazel\•ood Drive Suite 11'2 · Buffalo. New York 14228
Contact: Ms. Lnurie Losey
Project: Soil Radioisotopes
Client Sample JD: 3. l.12.E.2 Sample ID: 389296008 Matrix: Soil Collect Date: 21~ocT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.7%
Parameter .... Qu.~1_li.~C..r. Result ..... . . .. - ......... ······-·· .. - .
Gra\·imetric Solids ASTM D 2216 % Moisture "As Received"
Moisture 221
R:id Gamma Spec Analysis Gamma wirh /11growth "Dry We(r;ht Correctl!d"
Actmium-227 L' .Q 0241
Antimony-125 u -0 0245 Bismuth-212 lll 0.00
Bismuth-214 I 17
Cesn•m-137 I 4J
Coball-60 lJ -0.0119
Europium-154 L' -0.0941 Lcad-212 l 32 Lead-214 \.15
Potassium-40 .16.3
Protactimum-231 u 0214
Radium-226 1 11 Radium-228 t .27
Thall iuin-208 0.371
Tin-126 u 0 U343
...
Certificate of Analysis
t'_11 c.c.rt.:1.i.n.ty ..... !\IDC Le . ................. -···
+/-0 308 0.549 0260 +/-0.114 {) 203 U.095
+/-0.809 135 0.637
+/-0 153 0 127 0 OSR4
+/-0 117 0.0674 0 031 +!-0 039 () 0668 0.0293
+/-0 131) {) 222 0.()998
+/-0. l 32 0.110 0.0518 +/-0.2IO 0 324 {1158
+/-1.34 () 641 0 2!l0 +f-0.606 1.02 0.482 +I-() 153 () 127 00584 +1-0 300 0 261 O ll'J
+/-0 0751 0(174 0.03.:15
+J-0 159 0.194 ()0936
Tl'li
+/-0 JOS +/-0 114
.;./.1 31
+/-0.181 +/-0 164
+/-0.0394 +/-0 137 +/-0 169 +1-0230
+/-1 95 +/-0615 +/.{l 181 +l-0 362
+/-0.0&12 +/-0 160
Report Date: February 10, 2016
Pmject: Client ID:
MJWCOOI 15 MJ\VCOOl
.......... ·-·······. RL l'nits ................
percent C'XC1 01114116 1208 1537312
pCi/g RXF2 021()511() 0745 153754.6 2 pC1lg pC1lg pCi.'g
u 100 pCilg pC1lg
pCi/g pC1lg pCtlg pC1/g pCilg pC1lg pCi/g
pCiJg pC1/g
Gammaspec. Gamma. Solid ''Dry Weighc Con·ecrl!d". Acunium-227 u ·O 203 +1-0.260 0°16[ 0 214 +/-0.278 pCiig RXF2 01118116 11:40 1537545 3
Antmiony-125 u ()0615 +/-0.116 0223 1).11)3 +/.() 11~ pC1/g
B1smu1h-212 Ul (l.00 +/-0.843 146 ().676 +1-0 997 pCi/g
Bismulh-214 1.00 f-l-0 174 0.147 '()l)n68 +/-0 193 pCi/g
Cesium-137 I 35 +/.() 141 1)0947 0 0435 +1-U.177 0 JI}() pCtlg
Cobalt-60 u -0 0423 +1-00438 0070 0.0289 t/-0.0479 p('i/g
Europmm-154 u O.JO! +/-0 143 0.300 0.134 +i-IJ 150 pCi/g
l.eod-212 1.28 +f-0.131 O. Hl8 () 0508 +/-0.217 pC1/g
l.eud-214 1.21 ol-/-0 182 0 355 () !72 +/.t) 216 pCilg
Potassiuin-40 16 5 +/-] 65 (! 750 0315 ol-i-2.20 pC!/g
Prolactinium-23 l Ul 000 +/-U.805 {) 936 fl 435 +/-0816 pCi!g
Radmm-226 I 00 +/-0.174 0.147 011668 +/-0.193 pCilg
Radmm-228 142 +/-U 2CJ4 0208 00874 +/-0 368 pC'i/g
Thalhum-208 0.466 +/-0 0933 fJ.0706 0 031& +1-0.!0l pCtfg
Tin-\26 Ul 000 ··1-0.0929 0.106 0 0503 +/-ll.0949 pCi/g
Rad Gas Flow Proportional Counting GFPC. Gross A:B. solid "Dr.Y JJ.'eighi Con·ected"
Alpha 13.2 ..-J-.3.11 3.89 1.65 <·/-4 51 4.UO pCi/g KXB2 01 i26116 I J 56 1539462 4
Beta 26 2 +/-3 18 287 1 33 +f-5 03 10 {) pCilg
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com
Certificate of·Analysis
C'ompany; Address:
MJW Technical Services IS Hw.clwood Drive Suite 112 Buffalo. New York t-1228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.l.12.E.2 Sample ID: 389296008
Report Date: fcbruary I 0, 2016
Project: MJWCOOl 15 Client ID: MJWCOO I
_I_'ar~111~_e_t_~.r ....... ___ ···-. ·-· _.Qu_:ili_li«:r_ ···- .. ~c~_u!.t ....... lJn.~cr1:1~11t.- ...... Mf)C' ....... L~..... . .... T.f>L. -· _ .. ~!,.. Y.n.i.ts_ ... l?F _ ,~nnl~:.~.t.. .IJ.~~e '(imc __ B_~tc_ll .... ~·!t~,
'f.he __ follnwi!ll:l J>rcp ~~ct.~~tls ~H~r.e _ _pe_r_f!Jf.!'.ICl~ .... -· ..... ·········-·· ..... . :'vi et hod Description Anal~·st . ·-·· ............ ,_._ .. ... . .. ..... ... ... ............ .. . -·· '• .... ... . . . . ........ ·- ........... - ... -. ······-Dry Sml Prep Dry Soil Prep OL-RAD-A-(l2l CXC l
T.!.1.~. f.ollo~vi11g i:':.n~ly_ti_c111. ~1.E!i~_O.d..s.Yl'el_'~J_le~ftJ.r:•n.:e.~ .............. . Method Description
2
3
.\
ASTM D 2216 (Modified)
DOElIASL 300. 4 5.2 3/Ga-01-R
DOE llASL 300. 4 5.2JiQa,{IJ-R
EPA 900.0ISW846 9310/SM 711 OB.Modified .
Surmgnteffracer Recovery Test
Notes:
D:ite Time Prep Batch ... - ................... _ ................ -··- .................... . ()l/14/16 l208 [537312
Batch ID Recovery% Acceptable Limils
TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Reporl Date: December4, 2015
MJW Corporation Company; Address; 15 Hazelwood Drive
Suite 112
Contact: Buffalo, New York 14228 Ms. Laurie Losey
Project: ··-···· .. -·--····-· ........ .
Client Sample ID: Sample TD:
~.?ii r.za~i()_i_~ot°.p~s. 3.l.13.R.1 3&5070004
Matrix: Collect Date: Receive Date: Collector: Moisture:
Soil 21-0CT-15 10:55 05-NOV-15 Client 20.5%
Parameter ........... __ ...... Qu_~l_ifle.r. ...... ~~-t_i_I_t_ .. l!ncertainty Gravimetric Solids ASTM D 2216 % Moisture "As Received" ;\lo1 sture 20 5
Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Con-ected" Actmium-227 U 0 121 ""/-0.266 Antlmony-125 Cesium-137 Col>alt-60 Europmm-154 Protactinium-231 Radium-226 Radmrn-228
u
u u u
Tin-126 U .Rad Gas Flow Proportional Counting
-0.0425 0 966
0.0291 0.0314 a 90s 0.964
0 679 0 112
Of PC, Gross A/B, solid "Dry Weight Corrected" Alplla 8. \7 B~ IU
:n~e. fol_lo~~i-~~ .. i;>r~r. lv_let~~-~.S._\~~1~e _pe_rfo1111e.d_:
+/-0 111 +/-0.126
+/.O 0422 +/-0.136 . +1-0.859
+/-0 208 +l-0 385 +/-0 124
+1-2 26
+/-2.09
Method Description Df)·SOii r·rcp· ,·· .... . ·- .... -- . "Ill)· 'sOif Prep··oL=R.ftj).A'-021' . ... , ...
_Th.~.~?~ l_~l\vi~t;. f\_nal_y_ti_ca_!_ ~e_t~?~S. ~~'.:. P..~.r~°.rin.~.~'. . Me_llt9.~ ... .. . . . . _ ........... pe~criptic;i,ri.__ . .. .. .
ASTM D 2216 (Modified) DOE HASL 300, 4 5 2 3/Ga-01-R EPA 900 OISW846 93 IO/SM 71 JOB Modified
MDC
0 537 (1.201
0.107 0 0935 o.273 ()%8 0.146 0.302 (l \J5
2.68 2.47
RL
0.100
40()
!OJ)
Project: Client ID:
Units
percent
pCi/g
pC1/g pC'l/g pC1lg pC1/g pC1/g pCi!g pCi/g pC!/g
MJWCOOll5 MJWCOOI
C'XCI 11/10115 1319 1521342
RXF2 12i03!15 0&47 15223g3
KXB2. 12i02/l5 1114 1525757
Analyst Date Time Prep Batch ... CXCT ... ·- .. ··1t.iit}.ij5·· ....... ····-i3fl~···-······152'i84i ... ·-······· ...... , ....... ..
2
J
.. .............. -... . ................ ., .......... -............................. . . A.i1!llyst~mmni;:r.1t.~ ..... ..
Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96·sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com
Certificate of Analysis
Company: Address:
MJW Corporation 15 1-lazclwood Dri\'c Suite 112 Buffalo, New York !4228
Contact: Ms. Laurie Lose,;'
Project: Soil Radioisotopes
C licnt Sample lD: 3 .1.13 .R. ! Sample ID: 385070004 Matrix: Soi! Collect Date: 21-0CT·l5 Receive Date: 05-NOV-15 Collector; Client Moisture: 20.5%
P11rametcr
G1·1ivimctric Solids ASTJf D 2216 % Moistzmr "As Received"
Moisture 20.5
Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight C~orrected"
Actmium-227 lJ 0.121 +/-0266
Antm1011y- i 25 l) -0.0425 +f-0.1 l I 13ismulh-212 l.86 +1-0.689
Bi~muth-214 0.964 +/-U.208' Cesium-137 0.966 +/-0.126 Cobalt-60 U (l 0291 +t-0 0422
Europium-154 U 0.()314 +/-O. l36 Lcad-2 ll · 1 04 +/.Q 16 l Lead-214 0.786 -t-1-0 218
PoUl5s1um-40 Protactinium-231 Radrnm-226 Radmm-22&
Thallmm-208
Ul 109 0.00
0.9M ll.679 0.385
Tin-126 Ul 0 00
Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "D1y 1-Veight Corrected"
Alplia 8 17 Beta 16 3
!_11.~..f~!!<:l'vin.g J.'rep M.etl1i:i~~-'~e.r:e .. pc~~o.rn.1c.d. Method Description
Ory Soil Prep 0[)· Soil l'r"P GL-RAD-A-021
".f~~.e .f<>.1.lo~~i!lg ,\_11~ly!l~~l .. ~l~t.~o.~s- "'.(!l'C perf()r.!.11_e~ Method Description
ASTM 022l6(Modified)
DOE llAS1, JOO. 4.5.2 3/Ga-Ol-R
+J-1 55
+1-0 859 +l-D.208
+/-0385
+1-0.077 +!-0 124
+/-2.26
+f-2.09
2
3 EPA 900_0ISW846 93IOISM 71 lOB Modified
Surro1!:ale/Tracer Recovery Test
MD("... Le
0.537 0 251 0201 0.0921
1.07 0 47g 0.146 0.0658 (1107 0 0493
0.0935 (}0404
0.273 0 119
0.137 0 {)647 0.!59 110736 0 407 0 140 0.968 0.449 0.146 0 0558
0 302 0 134 0 0737 00332
(l 135 00638
2 6g I l'l
2-47 I 18
Analyst
CXC!
Repml Date: December l 7, 2015
Project: Client ID:
MJ\VCOOl !5 MJWCOO!
Jl1.ll ....... _R,1~ ... X_ni.ts ..... DF A!?a)y~~ ... f.>al~ !J.~~ .!l.a.tch Mid.
p;;rcent . ('XCI 111101\5 1319 1521842
+/-IJ272 pCi/g R..XF2 12/03115 0847 15223K3 2
+/-0.113 pCrlg +/-0.713. pCi/g
+/-0-224 pC11g +/-U.149 0 100 pCilg
+/-0 0442 pCl!g
+J-() 137 pCi/g +/-0.182 pCl!g +/-0 228 pC1lg +/-I.Bl pCifg
+/-0 383 pCi!g ·1-/-1)224 pCi/g
+l·O 396 pC1/g
+/-0 0841 pC1!g +/.() 125 pCi!g
+/-2.78 4 00 pC1/g KXB2 12!02/15 I I 14 1525757 3
+1-3 23 10.0 pC1/g
Date Time Prep Batch
I l/!0115 1319 1521842
Batch 10 H.ecovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address:
MJ\V Corporation l5 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.1.13.R.1 Sample JD: 385070004
Certificate of Anal;ysis
Report Date: December 17. 2015
Project: MJWCOOI15 Client ID: MJWCOOJ
J>ar_a.n1_c_t~.r. .... _ . . .... . Qllal!ficr. .. _ _l~e~-~t. _ V11~ertiii11ty MDC Le ..... __ .. IPY.. -· ..... }~~ ..... ~!.~.~t.!' .. _ I)_~-- ~-~~~l.Y-.s.t .... !?.a.t_e_ !}.~~l'. .. !l~.~~h. .... :\1.td'..
Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits
Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite J 12 Bufla!o. New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.1.13.R. l Sample ID: 385070004 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 20.5%
Certificate of Analysis
Project: Client rD:
...... ... ....
Report Date: December 17, 2015
M1WC00115 MJWCOOI
.. ....... - ··- .. ···-···· .... --··- ... - . -P~r:i.~c~e~ . .... .. ·- _ .. _ ... .9.~a!i_fle_~···· .. Res_u_l_I_. ___ I_l).c_cr.tain,tv Ml.>.C: .. 1.c . ... _. ___ Tl'V .... RL l"nits . D.l' .. ~\na,lyst .... _l)n,!_~ __ l_'im..~. !3!1~c-~ .. ~~~· Grnvi1i1ctric Solids
ASTM D 2216 % Moiswre ·~·1s Received" Moisture 2l>.5
Rad Gamma Spec Analysis Gamma~7Jec, Gamma, Solid "Dry Weigh! Correcti!d"
Actmium-227 u 0.121 Antirnony-125 u -0.0425 Bismuth-212 1.86 Bismuth-214 0.964 Ccsium-137 0.966 Cobalt-60 lJ 00291
Europmm-154 u 00314
Lcad-212 1 04 Lcnd-214 0786 Pota5~ium-4() 109
!'mtactiniurn-231 .Ul 0()0
Radium-226 0.964-
Radium-228 0.679 Th.allium-208 0.385 Tm-126 lJl 0.UO
Rnd Gas Flow Proportional Counting GFPC', Gl'oss A. B .. mlid "DrJ' Weigln Corrected"
Alpha S.17 Beta 16 3
+/-0.266 +/-0 111 +/-0 68'J +/-0.208 +/-0.12.6·
+1-0 0422 +/-[).136
+l-0 161 +l-0 218
+/-I 55
+/-0 859 +/.CJ.208 +/-0.38'5 +1-0.077 +/-0.124
-i-/-226
+1·2.09
:r.Jtl.! .. ~o.!!C!.'!:i~t; J.'rc_p .~1el~(_l_d~-~~r,e __ pcrfo_r.~.C..~ ................. _ l\!lethod Descriplioo
[)ry Soil Pr!!p Diy Soil Prep GL-RAD·A-021
T~.C-~l)_H~_why~ r\n_~_lytiC.jll :VI~t.l~t1.~s __ ,~ere !'l.!1'.f.oi::1~cd _ :Vlcthod Description -· I
2
3
ASTM D2216 (Modified)
DOE HASL 300, 45.2.3/G<i-O1-R
EPA 900.0ISW846 93!0/SM 7l IOB Modified
Su .. rogateffracer Recovery Test
(I.537
0.201
I 07
0.146 0 !07 0093~
IJ.273 0.137 0.159 0407 0.968
0.146 0 302
0 {1737 0 l35
2 68
2.47
ll251 0.0921 0479
0.0658 ()0493 (}0404
0.119 0 (1647
0 0736
0.140 0449
0.0658 () 134
0 0332 () 0638
I 19 l !R
Analyst
CXCI
+1.0 272
+!-0 113 +/-0 713 +/-0 224
+/-0.149 +/-0.0442
+/-0 137 +r-0.182 +f-ll 228
+/-I 81 +/.I) 8R3 +/-0 224 +/-0 396
+/-0 0841 +1-tl 125
+/-2 78 +/-3.23
perce1tl
pCi./g pCi/g pC1!g pCi/g
0.100 pC1lg pCi/g pCi/g pCi!g. pCifg pCi/g pCilg pCi/g pC1lg pCi!g pC1lg
4.00 pCi/g 10 0 pC1/g
Date Time
l l/10!!5 1319
CXCI 11/10!15 1319 1521842
RXF2 1210311.5 0847 1522383 2
KXB2 12/02115 l l 14 1525757 3
Prep Batch
1521842
Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address;
Contact Project:
MJ W Corporation 15 Hnzclwood Drive Suite 112 Buffalo, New York 14228
Ms. Laurie Losey
Soil Radioisotopes
Client Sample ID: 3.1.13.R. I Sample ID: 385070004
Surrogalerfracer Recovery Test
Notes:
Certificate of Analysis
TPU and Counting Uncertainty are calculated at the 95'l-'o confidence level (l.96-sigma).
Report Date: December 17, 2015
Project: MJWCOOJ 15 Client ID: MJWCOOI
Bakh ID Recovery% Acceptable Umils
GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843} 556-8171 - www.gel.com
Certificate of Analysis
Company: Address:
MJW Technical Services 15 Hazel\\ood Drive Suite 112 Buffo!o, Ne·w York 14228
Contact: Ms. Laurie Losey
Project Soil Radioisotopes
Client Sample ID: 3.1.13.R.2 Sample JD: 389296009 Matrix: Soil Collect Date: 2l~OCT-l5 Receive Date: 14-JAN-16
. Collector: Client Moisture: 22.4%
Parameter .. 9!1~.1.i_lie~.. .. Rcs_u~t- ... J)~ccl'_I~ in_ty_ ...... i\1DC
Gravimetric Solids ASTM D .:?216 % !vloisture "As Received"
Moisture 22 4
Rad Gammn Spec Analysis Gamma with Ingrowth "Dry Weight Corrected"
Actmium-227 IJ 0172 Antimony-125 l! -IJ.000515 Bi~muth-2 l 2 1.52
l31~muth-2 I 4 0.785
Cesium-137 0.991
C'oball-60 lJ -0022 Europium-! 54 lJ 00246 Lend-212 1 JO
Lcad-214 0 998
Potassium-40 12.0
Protaclmium-231 UI 0.00 Radium-226 () 785 Radmm-22_8 Ul 0 00
Thnllmm-208 02%
Tm-126 u 0.0406
+J-0 331 +/-0 119 +/-0 645
+/-0 179 +1-0 123
+1-0 os ts +/-0 128 +/-0 140
+J-0 204 ... 1-1.1>3
+f-0 91)3 +/-() 179 +f-0 328
+/-0 074 +/.() 114
Gammaspec. Gamma. Solid "D1y Weight Corrected" Actinium-227 u () l l3 +/-0.345
Antmiony-125 lJ -O.ll00289 +1-0 143
Bismulh-212 UI 0.00 +1-1.21
Bismulh-214 0.618 +1-0 184 Ccsium-137 1.10 +l-0 142
Cobalt-60 UI 000 +f-00285
Europium-154 u -<Hl409 +/-0.139
Lcad-212 0 986 +/-0.148
Lcad-214 0 994 +/-0.280
Potassium-40 11.8 +l-1.65 Protactmium-23 l UI noo +/-0.622
Radium-226 0 618 +/-0.184
Radmm-218 Ill +/-(] 281
Thalltum-208 0.326 +!-0 HJ4 Tm-126 UI 0.00 +/-0 l'l2
Rad Gas Flow Proportional Counting Gr"PC. Gross .-1 B. solid "D1:i· Weigh1 Correc:ti!d"
Alpha 11 9 +/-3.8!
Beta 21 <) +/-2.90
U63l 0.216 0.792 () 171
0.0733 0.0944 0.236 () 137 0 173 0.917
I 05
0 l7l I) 650
(l.()756 0 213
11658 0264
I 65 0 170
0.0823 0.0&45
0258 0 l3R
0 376 0 818
l. tO u 170 0271 <l.084 {) 263
399 2.5~
Le
ll.297 +/-0.342
0.0987 +/-0.l t9 0.339 .. 1-0.666
0 0785 +/-0 193
0.0325 +l-0.153
0.0404 ~1-0 0527
0.0998 +/-0.129 00642 +1-0 173 (l 080.J +l-0 223
0.392 +/-193 0.485 +/-0922
0 0785 +/-() 193
0 307 +/-0 539
O U34 +/-0 0786 0. !02 +/-0 116
0 31<1 +/-0 349 0.123 +/-0.143 () 763 +l-1 42 (J.077 +1-0.191
00367 +1-0.168 0 0354 +/-0 0348 () 111 +/-[} 140
O.llM8 +/.JJ l 67 ll 182 +f-0 290
0 342 +/-I 95 0.510 .,./-0.63&
01177 +/-ll.\91 0.117 +/-0 315 O.fl3S ... 1-0.107 ll.126 +/-0·193
I 65 -4·/-4.44 l 16 +l-4.31
Project: Client JD:
Report Date:
MJWCOOl 15 MJ\VCOO I
February IO, 2016
percent CXCl 01114116 1208 1537312
pC1/g RXF2 02i05/l6 0747 1537546 2
pC1/g. pC'ilg pCi/g;
0.100 pCi!g. pC-1/g. pC11g pCi/g pC'i/g pC1lg
pCi/g pC1lg. pCilg pCi/g pCi!g
pCiig RXF2 01118/16 I 12\ 1537545 pCi/g
pC1/g pC'ilg
O.IUO pC1/g pCilg pCiig pC1lg pC1!g pCi.'g pCi/g. pC1lg pCi/g pCilg. pC1lg
40() pCi.lg KXB2 Ol/26116 !152 1539462 4 10.0 pCilg
GEL LA BORA TORIES LLC 2040 Savage Road Charteston SC 29407 -(843) 556-8171 -www.gel.com
Certificate of Analysis
Company: Address:
MJW Technical Services 15 Ilazelwuod Drive Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: J.1.l 3.R.2 Sample ID: 389296009
....... -··· ·-·-···-··· --··· .. ...... . .. . .. . . . .............. ···-·-·-- ··-···-····· ...... ······ l'ar~m~_1:e.~-. .......... Qtrnli_ffor.. .. _ ~.esul~ ..... l!!lm~J1.i11ty_ . . ~me::.
The .f ~H°.\\'.i_rtg_ f_r_c.J.l .~1.c!.~O_<~ .~".~.r~. P.«::r.f.o.rm_e4. . . .. .. . .. .... :\fotho<l Description
·····- ·····-·· .. -- .. ··-· ······ ........... ····-····--
Le
Analyst Date
Report Date: February !O. 2016
Project: MJWCOO ! !5 Client ID: MJWCOO I
Time Prep Batch
Dry Soil Prep Dry Soil PrepGL-RAD-A-021 CXCI 0 l/l4f16 . 1208 1537312
1:bc .. fo.~Jo_\fi_ng_1\n_a!Y,ti~a~~lC!~()~~ \~'.C.~ pe.r_fol_'Jl1Cd ............ ___ .. Method Description
1
3
4
ASTM D 2216 (!vh1dified)
DOE HASL 300..4.5 2.3/Ga-01-R
DOE HASL 300. 4 5 2.3/Ga-01-R
EPA 900 OfSW846 9310/SM 71 IOB Modified
Surrog:itcrrrncer Recovery Test
Notes: TPV and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Batch ID Reco-n~ry% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-B171-www.gel.com
Ce.rtificate of Analysis Report Date: December 4, 2015
Company: MJW Corporation Address: 15 Hazelwood Drive
Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Losey Project: Soil Radioisolopes
.................. . ..................... Client Sample JD: 3.l.l4.R.J Sample 10: 385070005 Matrix: Soil Collect Date: 21-0CT-15 10:20 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3'%
Paramct~r ......... _ ....... _ . 9ua!ifier . _ -~~-s~:l_t. _U11certaJn:t>-• Gravimetric Solids ASTM D 2216 % Moisture "As Received'' Moisture 18 3
Rad Gamma Spm:: Analysis Gammaspe~. Gamma, Solid "Dry Weight Corrected" Achnrui:n-227 U -0 143 +/-0.26& ll.nt1inon}·-125 U -0 126 +/.lJ 10 I Ces[um-137 I 3(! +/-0 128 Cob~lt-6U lJ -0 0090 I +/-0 0442 Europium-154 U 0 00656 . +/-0 118 Protactmium-231 UI 0 00 +J-0.71 R Radtum-226 0.770 +/-U 161 Radiurn-228 O.\l8S +1-0.281 · Tm-12& U! 000 +/-0.0927
Rad Gas Flow Proportional Counting GFPC. Gross A/B, solid "Dry Weight Corrected". Alpha 9 96 +1-3 08 Bel~ 21) 0 +/-2 46
The _t?.Il~.~in~_.Pr.e.P. ... M!?tlJ..CJ.~~-~~re .. e~r[o_rrne~.: ........ _ .......... . Method Description ofi sii·irri~ii · ·· ··· ·· ·· ·· · -··· · · · ··or; ·siii1 1•~.;·r c;c:::R.:i\o:,;,.:i:ii-i · ··
····-··· Project: Client ID:
MJWCOOl 15 lVUWCOOI
IvIDC RL
(J 482 0 173 0 oss
0.0833 0 232 0 81 I 0 124 02~4
()0936
3 99 306
lJ lllO
4ll0 100
p~rcont
pC1!g pCi/g pC.lg pCi/g pCiig pC1/g pC1rg pC1lg pCi!g
pC1/g p('1/g
CXCI 11/J0/15 1319 1521842
RXF2 l 2i03/l .5 0&47 1522383
KXB2 12/02115 I\ 14 1525757
.... . . . . . ·-·· ··- ... -··-····-·-···- --·· ···- ........ . Analyst Date Time Prep Batch · ·c·xcr - ········ - ·iifi011:s· 1319 ·fsii-842········- -····
.T..~-~-'..?_l!.o.v.ving J\.n.a_IXti_~_a! ivlet'.1(}~s -\~~r~ pe_rform_ed_:. .. .... ... .. ... . ... ...... .... .. ... . ........... ··- .... ... ... .. . . . . . .... . .. _ ..... ···········-· ..... . Mt:t.hq~ ... _ .. .. .......... ·- P.c.~~rl.P_tio!, __ ....... . _____ . -··· ... . . . . .. ·-·- .... -·- ... . . . -···-·· b.l.l!!:IY_~t c;::0111!1.1~m.~. I ASTM D 22 \6 (Modified) 2 DOE HASL 300. 4 5.23/Ga-Ol-R
3 EPA 900.0/SWll.\6 93 IOiSM 71 IOB Modified
Notes: Counting Uncertainty is calculated at the 95% confidence fevel ( 1.96-sigma).
2
3
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Bu!Tulo, New York l4228
Contact: Ms. Laurie Losey
Project: Sot! Radioisotopes
Client Sample ID: 3. ! .14.R. l Sample ID: 385070005 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3%
Parameter ........ _.9~1.l_lifi.e'.. ...... -~~sult Cnccrta.int)' ·- ..... ~!D~
Griwimetric Solids ASTM D 22!6 % ivloisture "As Receil'ed"
Moisture
Had Gamma Spec Analysis
18.3
Gammaspec. Gamma, Solid "D1y Weight Con·ected" Actinium-227 U -0.143 +/.(l 268 Annmony-125 ll -0.126 +1-0 101 l3i~mu~1-212 !Jl 0.00 +1-0 555
Bismulh-214 0 770 +f-0.16! Cesium- 137 I 36 +f-0, 128
Cobillt-60 u -0.00901 +1-0.0442
Europium-154 ll 0.00656 +l-0. 11 S Lcad-212 1.07 +/-0.112
Lead-214 0817 +/-ll.194
Potnssium-40 11 5 +/-! 34
Protactmmm-231 Radium-226
Radium-228 111alhum-208 Tm-126
lll
Ul
Rad Gas Flow Proportional Counting
0()()
0.770
0 988
0277
0.00
GFPC Gross ;[:B, solid "Dry 1-Veight Corrected" Alph<i 9 96
Bern 20.u
:r~~.!~l_h1_\l:!~g.P._r~p-~l_e_t~'?-~~ _\\:er,cpi;1:rori,n_c~!._ .. _. -· Method Dcscriplion
+/-0.71 B +/-0.161 +/-(l.281
+/.II 0893 +i-0 0927
+/-3.08 +/-2.46
.................. .... ........ "··- ·········--. ..... ... . . ... ····- ...... ., __ .. Ory Soil Prep Dry Soil l'tep GL-RAD-A-OJ I
The following Analytical :\fothods were performl'd -~~th~ii ··· · ·· ··· ·· .n~~~-~ip.iian· · .... ·· ····· - -·· · --
2
3
ASTM 02216 (Modified)
DOE I IASL 300, 4.5.2 3iGa-01-R
EPA. 900.0!SW846 93 IOiSM 71 lOB Modified
Surrogatefl'raccr Recovery Test
0.482
0.173
1 14 () \24
0.0S.5 0.USJJ
0 232
0 IUI 0 137 () 7~13 {) 811 ().124
0244 0.0735 0()936
3.9\l
306
0 228
0.0796 0 523 () 056
0 0392
0.0364
0 10:?. 0.0478 0 0639 (IJl9 O.J"I& 0.056 0 108
0.0338 () 0449
1 so 147
Analyst
CXCl
+1-0 277 +1-0 117 +/-0.613 +l-0.173 +/-0.172
+/-0.04·14
<-1-0 118 +/-0.173 +l-0 207
+/-! 74 +l-0149
+/-0 173 +/.() 3 lfl
-t/-0.0924
+/-0.094&
+1-370 +/.) 86
Date
Report Date: December 17, 2015
Project: Client ID:
MJWC'00115 MJWCOOI
percent CXCI
pC'i/g RXF2
pCLig pCllg pCi/g
010(1 pCi/g pCi/g pCi/g pC1/g pCLlg pC!/g. pCi/g pC1/g
pC1/g pC1/g pC1/g
l\110115 1319 1521842
.12103115 0847 1522383 2
4.00 pC1/g KXB2 12102115 1114 1525757 3
!O.O pC1lg
Time Prcf1 Batch
11110.115 1319 1521842
Ilatcb ID Recovery% Acceptable Umits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Company: Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
M~. Laurie Losey
Project: Soil Radioisotopes
Client Sample fD: 3. !.[ 4.R.I Sample ID: 385Q_70005
Surrogatcffnu:er Reco\·ery Test
Notes:
Certificate of Analysis
TPU and Counting Uncertainty are calculated at the 95%1 confidence level ( 1.96-sigma}.
Report Date: December 17, 2015
Project: MJWCOO l 15 Client ID: MJWC001
Batcb lD Recovery% Acceptable Limils
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com.
Certificate of Analysis
Company: Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes .
ClientSampleID: 3.I.14.R.l Sample ID: 385070005 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3%
.~ar:im.~t~r .................. _q~~lif.i:~.r.. . .~csult . l!ti~-~.r.ta.i•\.tv.... .. i\:IJ>~.
Gravimetric Solids ASTJf D 2216 % Moisture ".-fs Recefred"
Moisture 183
Rad Gamma Spec Analysis Gammaspec. Ganmw. Sofid "D1:v Weight Corrected"
Actinium-22 7 ll -0.143 +/-0.268 0 482
Antimolly-12:5 u -0.126 +l-0 IOI 0 173
Bismuth-212 UI 000 +l-0.555 1.14
Bismuth-214 0770 +/-0.161 0 124
Cesium-137 1.36 +/-0 128 0.08:5
Cobalt-60 u -0.00901 +/-0.0442 0 !1833
Europium-154 lJ 0.00656 +/-0.118 0.232
Lcad-212. 1.07 +/-0I12 0.101
Lcad-214 0.817 +/-0.194 0.137
Pub~siurn-40 11 5 +/-134 0 743
Protactmium-231 U! 0.00 +/-0 718 0 811
Radium-226 0 770 +/-0 161 () 124
Radium-228 () 988 ·1'/-0281 0.244
Thalhum-208 0 277 +/.(] 0893 0:0735
·['in-J2C1 l!I O.ClO +/-0 0927 0 093t\
Rad Gas Flow Proportional Counting GFPC Gross A.'B, solid "Dry if'eight Corrected"
Alpha \l.96 +/-3.08 3 99
Beta 20.0 +/-246 3.06
'fhc followil1g Prep Melhods were performed :Vi~th~d ______ ....... "·u·e~c~ii;ii~~ ....... -...... ... ..... · .. ·
Dry Soil Prep Dry Soil Prep GL-RAD-A-02 l
!~.I! r~.1.101~~~g .. \na,l)'~_ic:t~ ~e~h.o~s .w~~i: p~rr~.r~1c.d .. ' Method Description
ASTM]) 2216 {Modified)
2 DOE HASL 300, 4.5.2.3/Ga:ot-R
3 EPA 90U.0/SW846 9310/SM 71 IOB Modified
Surrngatcffracer .Recovery Test
Project: Client TD:
Report Dale: December 17. 2015
MJWCOOJ !5 MJWCOOI
·-····· . .Le.. .... .. . :rrt.! __ ........ l!-L. .... l:n.i!S. .. l!f. :.\11.:ilyst. _ ,J):it.~_!i~.c .. B.atch --~ltd.
() 228 (J 0796
0 523
0056 00392 0 0364 0 \02
0 0478 0 0639
OJ\9
OJ78
0.056 0 108
() 0338 0 0449
1.80 147
Analyst
CXC!
+1-0 277
+1-0.117 +1-0 613 +/-0. 173 +1-0 172
+1-0.0444 +/-0.118
+/-O.l7J +/-0 207
+r-1 74 +/-0 749
*/-0 173 +/-0.310
+/-0.0924
+l-0 0948
+/-170 +/-3 86
Dute
1 )/10115
percent CXCI 1 tll0/15 1319 1521842
pCiig RXF2 12/03/15 0847 1522383 2 pCrJg pCi/g pC1!g
0 !00 pC1/g pC1/g pCi!g pCi/g: pCifg
pCi!g pCt!g pCi!g pCi/g: pC1/g pCilg
4 00 pCilg KXB2 12102115 1114 1525757 3 10.0 pCi/g
Time Prep Batch
1319 1521842
Batch ID Rcconry% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Company: Address:
MJW Corporation 15 Hazelwood Drive Sui1e 112 Bu!Talo. New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample TD: 3. l. l 4.R.1 Sample ID: 385070005
Certificate of Analysis
Report Date: December 17. 2015
Project: MJWCOO 115 Client ID: MJWCOO I
_ l'a~'.'!11~.t~.r. ... ···-.. .. . .. . . . guaH!icr. · Result Snccrt:iinty :\-JDC Le TPC RL Uuit~ OF Analvst Date Time Batch Mttl. ...... ·--····-· ····-- ·- ······--· ··---····-- ······-··· ....... - .. ·-·-···· ........ -· ........... ~-· ....... ~ ....... -·· ... -·· ....... . Surrogateffracer Recovery Test Batch JD RcCnl'cry% Acceptable Limits
Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com
Certificate of Analysis
Company; Address:
MJW Technical Service~ l5 Hazelwood Drive Suite 112 Buffalo, New Yorl< 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.1.14.R.2 Sample ID: 389296010 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 19.4%
Paraniet~r... ...... .. . . . .. qu_a_li~cr ..... ~e.sul! .... r11.i!~r~:Ji!!ll'
Gravinietric Solids ASTM D 2216 % Jfoisture "As Recefred"
Moisture 19.4
Rad Gamma S1icc Analysis Gamma wit/: lngrowrh ''Dry Weigfll Corr~c:ted"
Actmium-227 u -0 172 . +/-0 211
Antimony-125 LT ll 0178 ·r/-0.0897
Aismulh-212 UJ 0 00 +/-0.621
Bismuth-214 O.S69 +/-0.144
Cesium-137 1 27 +/-Q.0964
Cobalt-60 u () 110241 +/-0 030
Europium-154 u .() ()386 +f-0.0904
Le~d-212 0.794 +/-0.!04
Lead-214 0.915 +/-0 142
Potassmm-40 11.9 +1-1 17
Protactmium-231 u 0.342 +l-0 443 Radium-226 0869 .,./-0.144 Radium-228 1.02 +l-0 11!0
·niallium-208 0203 +l-0 Oo5l Tin-126 lJ I 000 +/-0 lJ84
Gammaspec. Gamma. Solid "Dry Weight Correcred" Actinium-227 ll -0(}627 +/-0 280
Antimony-125 lJ -00142 +/-0 117
Bismuth-212 1.77 f /.(1 7()0
Bismuth-214 0144 +/-U 173
Ccsium-137 137 +/-0 141
Cobalt-60 ll ll.0227 -t-/·ll 0403
Europium-154 u -00087 +/-0 139
l.ead-212 () 942 +l-0 158
Le~d-214 0 764 +l-0 187
Potassiwn-40 II 4 +/-] 41,
Prolactinium-23 I U! ()00 +/-0.706
Radmm-226 (1.744 +/-0 173
Radmm-228 0.952 +/-0 265
Thilllimn-208 0.100 +/-0.079
Tin-126 UI 000 +/.() 0993
Rad Gas Flow Proportional Counting GFPC Gross A:B. solid "Dry Weigh/ C'on·ected"
Alpha 9 16 +/.J 18 Bela 19 6 ..-/-2 47
. . MQ~ -----· -'~«:'.
(I 3(J5 0 174 0.160 IJ.1)759 0 063 0.305 0.104 () 0486
O.U564 00263 0 0568 0.0254 0.160 00719
0 0986 0.0475 () 234 0114 ll.428 0185 () 775 0.370
0 1Cl4 00486 0 172 0.0779
0 0563 ().0264 () 126 0061
0.518 0.242 0.213 00982 () 864 0.379 0 129 0.0576
0.0746 0.0335 0 OBS6 0.038! 0269 0.118 (j_m 0.0574 0 148 0 0681 0.591 0234 0 953 0.443
0129 (1.0576
\1258 0.112 0 0639 0.0285 0.175 () 0841
3 99 I 75 2.2t/ 1.06
Project: Client lD:
.TPr
Report Date:
MJ\VCOOl 15 MJWCOOl
February lO, 2016
········- .. ······ ..... . ~!,: ..... l'.uits. . _DF_ An:1lys~ .. _ D:i.te .. Tim_e_ B,a~~~----~·1. td:
perccnl CXCI 01114116 120g 15373!2
+/.(l.226 pC,/g RXF2 ()2I05fl6 0842 1537546 2 +1-0 0901 pC1lg
+/.l) 643 pCi/g +/.():161 pCilg +/-!l.140 0 100 pCilg +/.() (}30 pC!lg
+/-0.0921 pC1/g +/.{) 121 pC1/g +/.() 159 pCi/g +/·l.60 pC'ilg
+1-Q 475· pCilg +i-0 161 pCi/g +/-0.228 pCl/g
+/-00672 pC'ilg +/.{) 0858 pC'ilg
+/-0.282 pC1fg RXF2 Ol/181115 112·1 1537.545 3 +/-0 117 pC1/g +t-0 781 pC1/g +/.() 184 pC1/g +i-0.180 0 100 pC1lg
+/.(I 0417 pCi/g +1-ll 140 pCifg +/-1) 179 pCi!& +/-0.198. pCilg +I-I 77 pC!lg
+/-ll 720 pC1/g +/-fl 184 pCi.lg +/-0 302 pCilg
+/.() 0&01 pC1lg +/.() 112 pC1'g
+/-3.62 4 00 pCi/g. KX02 ()1126/t(i 1155 1539462 4 +/-3 70 100 pC1/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8.171 -www.gel.com
Company: Address:
Contact:
MJ\1.' Technical Services 15 Hazelwood Drive Suite ll2 Buffalo, New York !4228
Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.1.14.R.2 Sample ID: 389296010
Certificate of Analysis
Report Date: February !O, 2016
Project: MJWCOOl 15 Client ID: MJWCOO I
.P.~.r~.~e.tc.r .......... -. - . -- - g~~l~.fie.i:._ -··. __ l_~~s11_•1 ..... -r ~.~~f_tain~y. !.l.11~ .folln~Jng_ P!,t:.P. .~'!Cthl)d_S. \~e~I: .r.crfor.m.ctl .. :\fothlld Description
Dry Soil Prep Dry Soil Prep GL-RAD·A-021
'f.hcJoll~w.i11g. Ana..fY.t.i.cal M.cthutls.~\'.c.i.-11·ptrfo~·nied ... :Vkilwd Description
2
3 4
ASTM D2216(Motli!lcd)
oot HASL 300. •l.5 2 3/Ga-01-R
DOE HASL 300, 4.5 2.3iGa-01-R
EPA 900 OISW846 931 OISM 71 lOB Modified
Surrogakffracer Recovery Test
Notes:
Analyst
CXCI
Date Time Prep B:itch ······-- .... __ .. -·-·· ··- ... . .... 01114/lf> 1208 1537312
Balch lD Rcccwcr)'% Acceptable Limits
TPU and Counting Unce11ainly are calculated at the 95% confidence level ( J. 96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
Certificate of AnaJysis Report Date: December 4, 2015
Company: MJW Corporation Address: 15 Hazelwood Drive
Suite 112 Buffalo, New York t4228
Contact: Ms. Laurie Losey Project: Soil Radioisotopes
... . .. . -· ... ·········-········· .. . .. . ... -·········· ·-·· ...... Client Sample ID: 3.1.15.R.l Sample ID: 3&5070006 Matrix: Soil Collect Date: 21-0CT-15 14:40 Receive Date: OS~NOV-15
Collector: Cl.ient Moisture: 21.9%
Parameter Qualifier
Gravimetric Solids ASTM D 2216 % Moisture "As Received"
Europlllm-154 · Protactinium-23 I Radium-226 Radium-228
u
u u
UI
Tin-126 U
Rad Gas Flow Proportional Counting
21.9
0. 121 I 28
00155 0 00314
0,00
0932 01)06
0.0586
GFPC, Gross A/B. solid "Dry Weight Corrected" ~pha 13 I Beta 21 7
+/-0.151 +/-0.914 +/-0.230 +J-0 363 +J-0. 189
+1-3 19 +1-2.71
!!1.e.:f?.l.lo~·i~~-~.r~pJvfeth(JdS -""~E~ p~_rf.or.1n_e<l.: .... . ............... .. Method Description o~: ·s·oj1 rrcp···· · ·· .. , ... · · ····-·· -··nr}~son--·Prep ·01~-RAD~)\-Oz"f · · ··· ··-· · ·
~he ~?l_l_C?.:~i_n?. A11~l:yti~_a.l __ fl.J~t.h?.d_5..Y'c.reye.r.f.?.li1.1ed:_ ... ~-~-t!.~C?Q . . .. .. . _ J?~sc.r.ip\i.QJ1...... ... . . . ..... .
ASTM D 2216 (Modifi~d)
2 DOE HASL 300, 4 5 2.3iGa-Ol-R
3 EPA 9000ISW846 9310/SM 71 IOB Modified
MDC RL
0.605 0.246
00961 0 100 "(I 099&
0 291 1 23
0.190 0.340 0 238
3 76 4 00
3 36 10.0
........ ···-···
Project: Client !D:
percent
pCi!g pCi/g pC1/g pC1!g pCrlg pC1/g pC1fg pCilg pCi!g
pCi!g pCiig
MJWCOOI !5 MJWCOOl
CXCI 11/1011:5 1319 1521842
RXF2 12iOJ/15 1303 1522383
KXB2 12i02/l5 1116 !525757
Analyst Dale Time Prep Batch · · .. c:,·xci ........... · 1"iith1i5- ····· ..... ·1:119·· · ..... 15:.frs4i .... ·- ..... · -
. ............... A!J.a.1.Yst C (}llJAl~!ltS.
Notes: Counting Uncertainty is calculated at'the 95% confidence level ( 1.96-sigma).
2
3
Company: Address:
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
MJW Corporation 15 Hazelwood Drive Suite l !2
Certificate of Analysis
Buffalo, New York 14228 Report Date: December 17. 2015
Contact: Ms. Laurie Losey
Project: Soil RadioisoLopes
Client Sample ID: 3.1.15.R.I Sample ID: 385070006 Matrix: Soil Colfect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9%
.P.~E~!11_et~r . . .. ·- . .. -· .. .9~~1.i~er ..... ~c_s!t_l_l_ .. -· (11c4:!.l'.lll..i~ .. lv
Gra\'imetric Solids ASTM D 2116 % !idoiswre "As Received"
Moisture 21 9
Rad Gamnia Spec Analysis Gammaspec, Gamma. Solid "D1j· Weight Corn~cled"
Actmium-227. U -0 178 +-1-0 348
Anumony-l 25 UI 0 00 +/-0.202
Bismuth-212 UI 0.00 +/-1 ll B1smuth·214 (J.932 +/-0 230
Cesium-137 I 28 +/·ll 158
Cobalt-60 U 0 0155 +/-0.0487
Europmm-I 54 U 0 00314 +/-0 151
Lead-212 1 10 +/-0.154
lead-214 1.16 +/-0.224
Potassium-40 15.0 +/-1.69
l'rolactm1um-23 l
Radium-226
Rmlium-228
Thallium-208
l1l (I{){)
!l.932
0 906
0 295
Tin-126 U 0 058(i
Rae.I Gas Flow PrQporticmal Counting GFPC. Gross AB. solid "Dry lf'eight Corrected'.'
Alpha 13.1
Beta 21 7
+/-0.914
+/-0 230
+i-0 363
+/.() 0794 +!-0 189
+/-3 19
+/-2.71
Th..I! ~oll.~wi1_1g_!'.r_ep ~lctho,~s.'\'l'..Z:c .. pcrfor111.~~- ...................... . Method Description
Dry Soil Prep Dty Soil Prep GL·RAD-A-021
MDC
0 ()05
0246 I 55
(J 190
00961
\J.0998 () 29\ n 144 0.17]
IJ 731
1.23 0.190
0 340
0 0849
() 238
3.76
3 36
........... .....
~r_!J_e fol_l?.'Yi'!~ An_~ly_l_ic~~ J_\'~j!t~IJdS '.".e.~e r.i:r~'or~.e~ .................... _ ....... . Method Description .... J
2
3
ASTM D 2116 (Modtricd)
bOE HASL 300. 4.5.2.3/Ga-O\-R
EPA 900 OiSW846 9310iSM 71 IOB Modified
Le
t\283
0.114
071!! 1)(1877
0.043R 0.0431
0.127 00681
00798
() 297 ll.574
U.O!S77 0.152
00385 0 114
l.70
1.62
..... Analyst
CXCI
Project: Client ID:
MJWCOOl 15 MJWCOOJ
percent CXCI
+/-0.358 pC1/g RXF2 +/-0.210 pCi/g
+1-125 pC1/g
+/-0 243 pCi/g
.,./-0.192 0 !00 pC1/g +/.(! 0492 pCt/g
+/-0.151 pC1/g +/-0.181 pC1lg +1·0245 pC1/g
+/-2.12 pC1tg +/-0.')72 pC1/g
+/-0.243 pCt!g +/.() 387 pCilg
+l-0 ()834 pCtlg
+l-0.190 pCi/g
+/-4 06 400 pCi/g KXB2 +/-404 10.0 pCi/g
....... -.............. , ..... . .... , ...... __ , .. Date Time Prep Batch ... ·····- .. -·- -·- _ .. . ..... .......... ,_ ......... 11/10!15 1319 1521842
\ 1110!\5 1319 1521842
12i03!15 1303 1522383
12i02115 1116 1525757
............. _, ..... . ... •'
....... ·- .............. - ·- .
2
3
Su nogateffraccr Recovery Tcsl Batch lD RccO\'crr% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - 1Nwv1.gel.com
Company: Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228
Ms. Laurie Losey
Project; Soil Radioisotopes
Client Sample ID: 3.1. 15.R. r Sample ID: 385070006
··-·········-······--····-··--··· ....... ················-·····-Pnr.am.~~~r ........................ Q.u_a~if1cr ...... !lesull Surrogutcffracer Recovery Test
Notes:
Certificate of Analysis
Report Date: l)ecember 17. 2015
Project: MJWCOOI15 Client ID: .MJWCOO I
_l)1m.~a.i.nt~:. . .. ~ID<;. .... .Ice ........ __ . WL ......... __ Rf: __ X1_1i_t_~ __ ~F ;\11a~ys_~ .... Da~e. Ti.l?.e -~:ttc_l1 __ !VI.t~.-. Batch ID Recovery% Acceptable Limits
TPU and Counting Uncertainty are calculated at 1he 95% confidence level ( 1.96-sigirta).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com
Company: Address:
MJW Corporation l 5 Huzeh,·ood Drive Suite 112 Bu/Talo. New York 14228
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample ID: 3.1.15.R. I Sample 10: 385070006 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9%
Paran1eter
Grnvimetric Soliils A STM D 2216 % Mois111re "As Recefred"
Mornture 21 9
Rad Gamma Spec Analysis
Certificate of Analysis
l'ncerlaintv MlJC Le ..................
Gammaspec, Gamma. Solid "Dry Weight ('orrecl;~d''
Report Date: December 17. 2015
Project: MJWCOOl 15 Client ID: MJWCOO!
percent CXC"l 11/Hl/15 1319 !521842
i\ctimum-227 U -0 178 +/-0 34S . 0 605 0.283 +/.0.358 pC1/g RXF2 12103115 1303 1522383 2
i\ntimony-125 UI 0.00 +1-ll 202 Blsmuth-2!2 lll () 00 +/-1 l l
Basnrnth-214
Ccsiurn-13 7 Cabalt-60 Europium-l 54
Lcad-212 Lcad-214 Pota.~ium-40
Protactimum-231 Radmm-226
Radmm-228.
Thallium-208
u u
Lil
Tin-126 ll
Rad Gns l'low Proportional Counting
0.932 l 28
0 0155
0.003 \4 1.10.
1.16 IS.0
000
0.932
0.906
0.195 0.05&6
c;FPC, Gross A/B. solid "D1:1' Weig/if Corrected"· Alpha 13.1
Bela 21 7
+/-0.230 +J-0 l5S
+/-0 0487 +l-0 15! +/-0 154
+/-0 224
+J-1 69 +/-0914 +/-0.230 <·/-0.363
.,./-0.(l794 +!-0 189
+/-3 l9 +/-2.71
0.246
155
0 190 00961
00998 () 291 0 144 [) 173
0 731 123
0.190
0340 O.OS49 023~
3 76 3 36
lJ11'...~l!l.~c.1wi11g r,rep :vl_e~h.~.~~.ll·~i:eJi.ci:-1:0.".1.11~.~ .......... '··· " ................ . :\1ctt1od Descri11tion
Dry Soil Prep Dry Sad Prep GL-RAD-A-021
!_li_e.~(111()"'.i.~.g .'\n.?!Y.tii:.a..1. ~.l~~~Y.~S.. 'v.er.e J>_er.f.oi_:11:1e~ . ~lcthod Description
ASTM D 2216 (Modifo:d)
2 DOE HASL 300. 4 5 2. 3/Gn-0 l -R
3 EPA 9GO.O/SW846 93 JO!SM 71 IOB Modified
Surrogatefl'racer Recovery Test
0.114 +/-0 210 pCi/g
0 71S +/-! 2~ pC1/g 0 0877 +/-0.243 pC1lg
0 0438 +/-0 192 0.100 pC1/g
0.0431 +/.!) 0492 pC1/g
0.127 +1-0.1 s l pC1/g
00681 +J-0 lSI pCr/g 00798 +(-0 245 pC1/g
() 297 +l-2 12 pCi/g 0 . .574 +f-0.'>72 pCi.lg
0.0877 +f-0.243 pC1/g
0 152 +/-0.387 pC1/g
0 03S5 +/-0.0834 pCi!g () 114 +/-0•190 pCilg
1.70 +/-4.06 4.00 p('rlg KXB2 12i02fl5 1116 1525757 3
l 62 +1-4.04 100 pCi/g
Analyst Date Time Prell Batch ...• . ....... ··············-·-· ···-······ ........................ .
CXCl 11110115 1319 1521842
Batch 10 Recovery% Acceptuble Limits
GEL LAB.ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 • w.vw.gel.com
Company: Address:
Contact: Project:
MJW Corporation 15 Hazelwood Drh·c Suile 112 Buffalo, New York 14228
Ms. Laurie Losey
Soil Radioisotopes
Client Sample ID: 3.1.15.R. I Sample ID: 385070006
Notes:
Certificate of Analysis
Reporl Date: December 17.2015
Project: MJWCOOl 15 Client ID: MJWCOOI
. ~·\: ....... __ Tl'.L. ···--. }_~!,. . .. _l~_11_it~ .. -~F. An:i_ly~t ... J?.a.~e. :r_-~1.ne__ -~:J~.<:l_i_ .. ~ltd,=. Batch H) Reco\·ery% Acceptable Limits
TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigrna).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8'\71 - www.gel.com
Company: Address:·
MJW Technical Ser.-ices 15 Ha:telwood Drive Suite 112 Buffalo, New York 1422.8
Contact: Ms. Laurie Losey
Project: Soil Radioisotopes
Client Sample m: 3. !.15.R.2 Sample ID: 389296011 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.1%
. ~~rarn_et~r. _ ····-·· .. _ ... _ q1~.~li.fi.c.r. Gravimetric Solids
,-lSTJf D 2216 % Moi.~ture "As Received" M(nsturc 22.1
Rad Gamma Spec An;1lysis Gwnma with lngrowlh "Dry Weight Corrected"
A~tmium-227 u -0.053 Anlimony-125 ll 00738
Bismuth-212 2.07
Bismuth-214 0.833
Cesium-137 1.72
Cob.alt-60 lJ O.U252
Europmm-154 u -U.024 Lead-212 1.18 Lcad-214 I 2(!
Po1ass1um-40 15 3
Prota~lmmm-231 UI 0.00
Radium-226 0 &33 Radmm-228 I 14
Tlmllium-208 0 J87
Tm-126 Lil 0.00
Certificate of Analysis
.Il~.t:.
+/-1) 283 lJ 489 0 231 +1-0 284
+/-0.121 0.231 () ]()9 +/-0.126
+/-0.966 0 966 0.435 +t-0.985
+lo 116 () 143 0.0655 -~/-U 189 +/-0 140 009[) 00411> +1-<i 196
+/-0.0471 0 0908 00396 +1-0 0485
+/-0.150 0.244 0.!06 +/-0.150
-r/-0 129 0.118 O.ll563 +f-0 162 ... ,.() 185 0.33& 0 164 +1-ll 212
+/-1 71 IJ 730 () 308 +l-2 16
+/-0996 () 9117 0427 +/-1.09
+/-() \7() 0 143 0.0655 +/-() 189 +/.() 287 0282 0.126 +f-0 318
+/-0.080 0.0742 0.034 +/-0.0862
-1-0l12 () 124 () 0595 +/.O.l 14
Gammaspec, Gamma. Solid "Dry Weight Corrected" Actmium-227 lJ -00408 +/-0 357 () 663 0.310 +1-0 353 Ant11110ny-125 u 0.0275 +/-0.152 0 281 0 !3lJ +/-0 152
Bismulh-212 Ul 0.00 "-/-0.857 I 67 0773 +/-I 16
Bismulh-214 o s2g +/-01% O.lbO OlJ7\7 +/-0.210
Cesium-137 1.68 +/.().183 .() 1()8 [I 0493 +l-0 23~
Cobalt-60 u 0 00658 +/-0.055! 0.111 00479 +f-0 0552
r::uroprnm-154 v 0.0103 +/-0.135 0.275 0 117 +/-0.135
Lead-212 120 +/.().151 (I 147 0.069\ '+/-0. \85
Lead-214 0 944 <·/-0.267 0204 0.[)948 +/-0 279
Potass i um-40 13 3 +l-1.65 () 617 () 234 +1-2.!JI)
Protacumum-23.\ lJI 0.00 +/-0 8&8 1.54 0727 +-1-1.0(>
Radium-226 0.818 +/-0.196 O.lfiO 0.0717 +/-0.2!0
·Radmm-228 I U7 +/-0 376 {) 377 () 168 +/-0 405
Timllmm-208 0.301 +/.()0966 0 0881 0.(139R +/-0.100
Tm-126 UI 000 +/-0 188 ().2iJ2 U U91i ... /-0.189
Rad Gas Flow Proportional Counting GFPC. Grass A:S. solid "Dry JVeight Con·ected"
Alpha 18 s ·•·l-4 07 3.95 1.72. +/-5 49
Beta 23 7 +/-2 89 282 I 31 +1-4 5(>
Rep.or! Dute: Pcqruary I 0, 2016
Project: Client ID:
MJWC'OOl 15 MJWCOOI
percent CXCl 01114116 1208 1537312
pC1!g RXF2 02105116 0842 1537546 2
pCi/g
pC1/g
pCi/g
0.100 pCi/g
pC!lg pCi/g pCi/g pC!lg pC'1/g pCi/g
pC1/g pCilg
pCilg
pCi/g
pC1!g RXF2 01/18!16 1122 1537.545 3 pC1!g pCi!g pC1/g
0.100 pCi!g
pCi/g pC!lg pCt/g pC1lg pC1ig p('t1£. pCt/g
pCiJg pC1/g pC1/g
4.(1() pC1/g KXB2 Ol/26116 1152 1539462 4
100 pCi/g
Company:. Address:
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
MJW Technical Scrvkcs 15 Hazelwood Drive Suite 112
Certificate of Analysis
Buffalo. New York 14228 Report Date: February 10. 2016
Contact: Ms. Laurie Losey
Project: Soil Rndioisotop(!s
Client Sample ID: 3.1.15.R.2 Sample ID: 389296011
Parameter
The.fo.ll~."'}.ng_f.'r.cJ!.~1.e.~ho<!~~-e.i:~.J!l:~fl)_r~ne~. Method Description -·. . ... Dry Soil Prep
Cncert~intv
Th.c. r.011~,'t.i.ng ,\~a..1yti~<:1l_i\-f.e.1110..d.~ ~\·.e.re. p~rf1n::n1.e~ ... :\·le thud Description
4
.ASTM D 2216 I Modifa:d)
DOE HASL300.4.5 2.3/Ga-01-R
DOI:: HASL 300. 4 5 2 3/Ga-01-R
EPA 900.0iSW846 93 !Q.1SM 71 I013 Modified
Surrogatcffracer Recovery Test
Notes:
Project: MJWC'OO ll5 Client JD: MJWCOOl
Le TPl'
Time
C'XC' I Ol/14116 1208
Prep Batch
1537312
Dnte Time B:itch Mtd. ···-····· . . ........ .
Batch ID Recovery% Acceptable Limits
TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) .556-8171 -www.gel.com
Certificate of Analysis Rep011 Date: December 4, 2015
Company: Address:
Contact: Project:
................. ·-··· Client Sample ID: Sample ID: Matrix:
Collect Date: Receive Date:
Collector:
Moisture:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 1422& Ms. Laurie Losey Soil Radioisotopes
..... ·-···········".' 3.1.16.R.I 385070007 Soil 21-0CT-15 14:10 05-NOV-15 Client
18.1%
Result Uncertainty MDC .... -··· ··- .. -· ....
Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mmsturc 18.!
Rad Gamma Spec.Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 U -0 0964 +i-0 260 Antimony-125 U -0.0282 -t/-0 112 Ccsium-137 I 75 +/-0 161 Cobalt-60 ll 0.0436 +/-0.0414
Europium- 154 Protaclinmn1·23 I Radiwn-226 R.adiw11-228
u lJ
Tm·126 U
Rad Gas Flow Proportional Counting
-0 0232 0 306 0 682 0.716
() 0837
GFPC. Gross AfB, solid "Dry Weight Corrce<ted" Alpha· 14- 7 Beta 21-7
+1-0 114 -t-/-0558 +1-0167 +1-0.295 +1·0 143
+1-3 55 +/-2.59
0 494 0206
00756 00968
n.19! 1.12
0 139 0.279
0 193
3.9S 2.91
ll 100
4.00 100
Pmject Client JD:
percent
pC1/g pCi/J;? pCi/g pCi!g pC1/g: pCilg pCi/g
pC1/g pC1rg
Ih.~ fo.l!()~V.i.n~ .P:~~P ~',~et.~?~s_ ~_ere_r.erforin~d.:_ ···--· __ . .. . . _ -· ....... _ . . . . . . .. ·- _ .. _
·-······ MJWCOOll5 ;...-uwcoo1
CXCl l l/10115 \319 1521842
RXF2 12/03/1; 1303 I 522383
KXB2 12!02il5 1116 1525757
Method Description Analyst Date Time or;;·s-c;,Trre.i» .... ····-· · · ·· .. · ···5iY·s1i11 fiiei> dC:R'AB~;\:-02t · - ·- ·····- · ···· ····· · ··· ·· -·txc1· -· · ... · · -fihohs· - · f:fr9 · · Prep Batch 1521842
. Th~. f~l~()~Y.i~¥_~~-~Ixti~a:1_ ~~~?.ds_\v.er-~ P.~~o.r1ned_: ........................ .. _rv1~~h.P.~. _ .... . .. ········- .... _ _pe~c:r~.P.tion... .... ....... .. .. ..... . . . . .................... _ .. . . .... .. . -· .. .A.!1-~h'1>.t(Qf.\lll)_~n.~s .. _
ASTM D 22!6 (Modified)
2 DOE HASL 300. 4.5.2 3/Ga-Ol-R
3 EPA 900 0 1SW846 9310/SM 71 IOB Modified
Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).
2
3
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