290 south wagner road organic analysis ann arbor … · 14'-15' tm ann arbor technical...
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Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 79.1Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-15.2'-6.0'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 64.6Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg 0.80 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-113'-14'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 84.6Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-118'-19'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 81.5Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-24'-5'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 81.2Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-210.7'-11.7'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 84.5Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-214'-15'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 73.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <3.3 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg <3.3 3.3Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <3.3 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg <3.3 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <3.3 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <3.3 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.Elevated reporting limit due to matrix interference for 8270C analysis.
B-36.5'-7.5'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: -Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg - 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg - 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg - 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg - 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg - 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg - 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg - 0.33
CommentsResults expressed on a wet weight basis.8260B analysis performed by TriMatrix Labs."-" indicates sample not received for analysis.
B-314'-15'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 87.5Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-318'-19'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 57.8Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 8.4 0.5Chlorobenzene (108-90-7) 8260B mg/kg 4.7 0.5Hexachlorobutadiene (87-68-3) 8270C mg/kg 65 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg <3.3 3.3Tetrachloroethene (127-18-4) 8260B mg/kg 4.0 0.51,2-Dichlorobenzene (95-50-1) 8270C mg/kg 89 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg 110 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg 18 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg 5.0 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-48'-9'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 81.6Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 4.9 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-412'-13'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 53.6Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 27 1Chlorobenzene (108-90-7) 8260B mg/kg 160 1Hexachlorobutadiene (87-68-3) 8270C mg/kg 18 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg <3.3 3.3Tetrachloroethene (127-18-4) 8260B mg/kg 10 11,2-Dichlorobenzene (95-50-1) 8270C mg/kg 160 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg 150 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg 7.1 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <3.3 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-59'-10'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 76.6Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 3.2 0.05Chlorobenzene (108-90-7) 8260B mg/kg 2.0 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg 0.81 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg 1.3 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-514'-15'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 57.3Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 79 5Chlorobenzene (108-90-7) 8260B mg/kg 950 5Hexachlorobutadiene (87-68-3) 8270C mg/kg 120 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg 5.0 3.3Tetrachloroethene (127-18-4) 8260B mg/kg 75 51,2-Dichlorobenzene (95-50-1) 8270C mg/kg 390 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg 310 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg 11 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <3.3 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-68'-9'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 69.4Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 1.4 0.05Chlorobenzene (108-90-7) 8260B mg/kg 6.4 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg 1.8 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg 3.2 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-614'-15'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 56.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 0.2 0.1Chlorobenzene (108-90-7) 8260B mg/kg 12 0.1Hexachlorobutadiene (87-68-3) 8270C mg/kg 22 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg <3.3 3.3Tetrachloroethene (127-18-4) 8260B mg/kg 0.6 0.11,2-Dichlorobenzene (95-50-1) 8270C mg/kg 22 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg 18 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <3.3 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <3.3 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-79'-10'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 93.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 0.16 0.05Chlorobenzene (108-90-7) 8260B mg/kg 4.1 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg 0.41 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg 0.63 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.
B-714'-15'
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 65.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg 0.10 0.05Chlorobenzene (108-90-7) 8260B mg/kg 8.4 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg 6.7 3.3Hexachlorobenzene (118-74-1) 8270C mg/kg <3.3 3.3Tetrachloroethene (127-18-4) 8260B mg/kg 0.77 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg 18 3.31,3-Dichlorobenzene (541-73-1) 8270C mg/kg <3.3 3.31,4-Dichlorobenzene (106-46-7) 8270C mg/kg 14 3.31,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <3.3 3.31,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <3.3 3.3
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.na - indicates not applicable.
Duplicatena
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/12/07 Percent Total Solids: 100.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.na - indicates not applicable.
Field Blankna
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Organic AnalysisData Summary Sheet
For: Mr. Steve Lucas ATS Project: Reach D PCAP #D052-TRPDow Chemical Report Date: 3/25/20071078 Building ATS SRF: 0315071Midland, MI 48667
Sample Identification:Sample Depth:
Sample Date: 3/13/07 Percent Total Solids: 100.0Laboratory Receipt Date: 3/15/07Sample Matrix: Sediment
Parameter (CAS #) Method Units ResultReporting
LimitBenzene (71-43-2) 8260B mg/kg <0.05 0.05Chlorobenzene (108-90-7) 8260B mg/kg <0.05 0.05Hexachlorobutadiene (87-68-3) 8270C mg/kg <0.33 0.33Hexachlorobenzene (118-74-1) 8270C mg/kg <0.33 0.33Tetrachloroethene (127-18-4) 8260B mg/kg <0.05 0.051,2-Dichlorobenzene (95-50-1) 8270C mg/kg <0.33 0.331,3-Dichlorobenzene (541-73-1) 8270C mg/kg <0.33 0.331,4-Dichlorobenzene (106-46-7) 8270C mg/kg <0.33 0.331,2,4-Trichlorobenzene (120-82-1) 8270C mg/kg <0.33 0.331,2,4,5-Tetrachlorobenzene (95-94-3) 8270C mg/kg <0.33 0.33
CommentsResults expressed on a dry weight basis.8260B analysis performed by TriMatrix Labs.na - indicates not applicable.
Field Blankna
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: 702785 ATS Project: Reach D PCAP #D052-TRP
Parameter: Volatiles (USEPA 8260B) Report Date:
Results of QA Samples run concurrently with project samples
Spike and/or QC Check Samples
Sample
#D052-TRPLaboratory Control Sample 3/19/07
Benzene <0.05 mg/kg 2.0 mg/kg 2.1 mg/kg 104.5Chlorobenzene <0.05 mg/kg 2.0 mg/kg 2.2 mg/kg 108.01,1-Dichloroethene <0.05 mg/kg 2.0 mg/kg 2.0 mg/kg 101.0Toluene <0.05 mg/kg 2.0 mg/kg 2.1 mg/kg 103.5Trichloroethene <0.05 mg/kg 2.0 mg/kg 1.8 mg/kg 89.5
#D052-TRPLaboratory Control Sample 3/20/07
Benzene <0.05 mg/kg 2.0 mg/kg 2.1 mg/kg 105.0Chlorobenzene <0.05 mg/kg 2.0 mg/kg 2.1 mg/kg 104.51,1-Dichloroethene <0.05 mg/kg 2.0 mg/kg 2.0 mg/kg 99.5Toluene <0.05 mg/kg 2.0 mg/kg 2.1 mg/kg 103.5Trichloroethene <0.05 mg/kg 2.0 mg/kg 1.9 mg/kg 92.5
Comments: Control Limits:Results expressed on a dry weight basis. Benzene (70 - 130)(1) Calculations were performed prior to rounding. Chlorobenzene (70 - 130)(2) na = not applicable, inappropriate spike levels. 1,1-Dichloroethene (70 - 130)(3) nc = not calculated. Toluene (70 - 130)(*) asterisk = outside standard control limits. Trichloroethene (70 - 130)(**) double asterisk = outside optimal spike levels.
Known Concentration
Spiked Concentration
Analyzed Concentration
Percent Recovery
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: 702785 ATS Project: Reach D PCAP #D052-TRP
Parameter: Volatiles (USEPA 8260B) Report Date:
Results of QA Samples run concurrently with project samples
Spike and/or QC Check Samples
Sample
#D052-TRPB-1 5.2'-6.0' 3/12/07 Matrix Spike
Benzene <0.05 mg/kg 2.5 mg/kg 2.7 mg/kg 106.8Chlorobenzene <0.05 mg/kg 2.5 mg/kg 2.7 mg/kg 108.71,1-Dichloroethene <0.05 mg/kg 2.5 mg/kg 2.8 mg/kg 111.6Toluene <0.05 mg/kg 2.5 mg/kg 2.6 mg/kg 103.2Trichloroethene <0.05 mg/kg 2.5 mg/kg 2.4 mg/kg 94.0
#D052-TRPB-1 5.2'-6.0' 3/12/07 Matrix Spike Duplicate
Benzene <0.05 mg/kg 2.5 mg/kg 2.6 mg/kg 105.6Chlorobenzene <0.05 mg/kg 2.5 mg/kg 2.7 mg/kg 106.01,1-Dichloroethene <0.05 mg/kg 2.5 mg/kg 2.8 mg/kg 112.8Toluene <0.05 mg/kg 2.5 mg/kg 2.6 mg/kg 102.8Trichloroethene <0.05 mg/kg 2.5 mg/kg 2.3 mg/kg 93.6
Comments: Control Limits:Results expressed on a dry weight basis. Benzene (70 - 130)(1) Calculations were performed prior to rounding. Chlorobenzene (70 - 130)(2) na = not applicable, inappropriate spike levels. 1,1-Dichloroethene (70 - 130)(3) nc = not calculated. Toluene (70 - 130)(*) asterisk = outside standard control limits. Trichloroethene (70 - 130)(**) double asterisk = outside optimal spike levels.
Known Concentration
Spiked Concentration
Analyzed Concentration
Percent Recovery
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: 702785 ATS Project: Reach D PCAP #D052-TRP
Parameter: Volatiles (USEPA 8260B) Report Date:
Results of QA Samples run concurrently with project samples
Replicate Analysis
Sample
#D052-TRPB-1 5.2'-6.0' 3/12/07 Matrix Spike Benzene 2.7 mg/kg 2.6 mg/kg 2.7 mg/kg 1.1
Chlorobenzene 2.7 mg/kg 2.7 mg/kg 2.7 mg/kg 2.51,1-Dichloroethene 2.8 mg/kg 2.8 mg/kg 2.8 mg/kg 1.1Toluene 2.6 mg/kg 2.6 mg/kg 2.6 mg/kg 0.4Trichloroethene 2.4 mg/kg 2.3 mg/kg 2.3 mg/kg 0.4
Comments: Control Limits:Results expressed on a dry weight basis. Relative Range < or = 35%.(1) Calculations were performed prior to rounding.(3) nc = not calculated.(*) asterisk = outside standard control limits.
Replicate 1 Replicate 2 MeanRelative Range
(percent)
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: 702785 ATS Project: Reach D PCAP #D052-TRP
Parameter: Volatiles (USEPA 8260B) Report Date:
Results of QA Samples run concurrently with project samples
Blank Analysis
Sample Analyzed Concentration QC Decision
#D052-TRPMethod Blank 3/19/07 Less than detectable for all analytes Acceptable Method Blank 3/20/07 Less than detectable for all analytes Acceptable
Comments:
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: 702785 ATS Project: Reach D PCAP #D052-TRP
Parameter: Volatiles (USEPA 8260B) Report Date:
Results of QA Samples run concurrently with project samples
Surrogate Recovery
Sample
#D052-TRPMethod Blank 3/19/07 Method Blank 3/20/07 Laboratory Control Sample 3/19/07 Laboratory Control Sample 3/20/07 B-1 5.2'-6.0' 3/12/07 Spike B-1 5.2'-6.0' 3/12/07 Spike Duplicate B-1 5.2'-6.0' 3/12/07 B-1 13'-14' 3/12/07 B-1 18'-19' 3/12/07 B-2 4'-5' 3/12/07 *B-2 10.7'-11.7' 3/12/07 *B-2 14'-15' 3/12/07 *B-3 6.5'-7.5' 3/12/07 *B-3 14'-15' 3/12/07 *B-3 18'-19' 3/12/07 *B-4 8'-9' 3/13/07 B-4 12'-13' 3/13/07 *B-5 9'-10' 3/13/07 B-5 14'-15' 3/13/07 B-6 8'-9' 3/13/07 B-6 14'-15' 3/13/07 *B-7 9'-10' 3/13/07 B-7 14'-15' 3/13/07 *Duplicate 3/13/07 Field Blank 3/12/07 Field Blank 3/13/07 *
Comments: Control Limits:(1) Calculations were performed prior to rounding. (86 - 118)
(3) nc = not calculated. TOL = Toluene-d8 (88 - 110)(*) asterisk = outside standard control limits. BFB = Bromofluorobenzene (86 - 115)
TOL BFB DBFM
99 90 101100 89 9999 96 101
101 94 10298 96 9798 97 9699 89 88
100 89 8899 90 8899 91 85
100 92 8499 89 8599 91 8499 91 8499 89 8498 93 9296 88 8199 92 9499 93 8498 90 9699 92 80
8899 90 82
85
99 91 8798 89 88
3/25/07
DBFM = Dibromofluoromethane
98 98
100 92
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: QC0RG0316071-D ATS Project: Reach D PCAP #D052-TRP
Parameter: Semivolatiles (USEPA 8270C) Report Date:
Results of QA Samples run concurrently with project samples
Spike and/or QC Check Samples
Sample
#D052-TRPLaboratory Fortified Blank 3/16/07
Hexachlorobutadiene <0.33 mg/kg 4.0 mg/kg 3.4 mg/kg 84.0Hexachlorobenzene <0.33 mg/kg 4.0 mg/kg 3.8 mg/kg 94.31,2-Dichlorobenzene <0.33 mg/kg 4.0 mg/kg 3.4 mg/kg 84.81,3-Dichlorobenzene <0.33 mg/kg 4.0 mg/kg 3.6 mg/kg 90.81,4-Dichlorobenzene <0.33 mg/kg 4.0 mg/kg 3.5 mg/kg 87.01,2,4-Trichlorobenzene <0.33 mg/kg 4.0 mg/kg 3.6 mg/kg 89.81,2,4,5-Tetrachlorobenzene <0.33 mg/kg 4.0 mg/kg 6.8 mg/kg 171.0 *
Comments: Control Limits:Results expressed on a dry weight basis. Hexachlorobutadiene (50 - 130)(1) Calculations were performed prior to rounding. Hexachlorobenzene (50 - 130)(2) na = not applicable, inappropriate spike levels. 1,2-Dichlorobenzene (50 - 130)(3) nc = not calculated. 1,3-Dichlorobenzene (50 - 130)(*) asterisk = outside standard control limits. 1,4-Dichlorobenzene (50 - 130)(**) double asterisk = outside optimal spike levels. 1,2,4-Trichlorobenzene (50 - 130)
1,2,4,5-Tetrachlorobenzene (50 - 130)
Known Concentration
Spiked Concentration
Analyzed Concentration
Percent Recovery
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: QC0RG0316071-D ATS Project: Reach D PCAP #D052-TRP
Parameter: Semivolatiles (USEPA 8270C) Report Date:
Results of QA Samples run concurrently with project samples
Spike and/or QC Check Samples
Sample
#D052-TRPB-2 14'-15' 3/12/07 Matrix Spike
Hexachlorobutadiene <0.33 mg/kg 4.2 mg/kg 3.6 mg/kg 84.6Hexachlorobenzene <0.33 mg/kg 4.2 mg/kg 2.8 mg/kg 65.91,2-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.1 mg/kg 73.91,3-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.2 mg/kg 76.11,4-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.1 mg/kg 73.21,2,4-Trichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.7 mg/kg 86.71,2,4,5-Tetrachlorobenzene <0.33 mg/kg 4.2 mg/kg 3.8 mg/kg 90.0
#D052-TRPB-2 14'-15' 3/12/07 Matrix Spike Duplicate
Hexachlorobutadiene <0.33 mg/kg 4.2 mg/kg 4.1 mg/kg 95.8Hexachlorobenzene <0.33 mg/kg 4.2 mg/kg 4.2 mg/kg 99.81,2-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.3 mg/kg 77.41,3-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.3 mg/kg 76.71,4-Dichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.3 mg/kg 77.11,2,4-Trichlorobenzene <0.33 mg/kg 4.2 mg/kg 3.8 mg/kg 90.61,2,4,5-Tetrachlorobenzene <0.33 mg/kg 4.2 mg/kg 3.0 mg/kg 69.8
Comments: Control Limits:Results expressed on a dry weight basis. Hexachlorobutadiene (50 - 130)(1) Calculations were performed prior to rounding. Hexachlorobenzene (50 - 130)(2) na = not applicable, inappropriate spike levels. 1,2-Dichlorobenzene (50 - 130)(3) nc = not calculated. 1,3-Dichlorobenzene (50 - 130)(*) asterisk = outside standard control limits. 1,4-Dichlorobenzene (50 - 130)(**) double asterisk = outside optimal spike levels. 1,2,4-Trichlorobenzene (50 - 130)
1,2,4,5-Tetrachlorobenzene (50 - 130)
3/25/07
Known Concentration
Spiked Concentration
Analyzed Concentration
Percent Recovery
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: QC0RG0316071-D ATS Project: Reach D PCAP #D052-TRP
Parameter: Semivolatiles (USEPA 8270C) Report Date:
Results of QA Samples run concurrently with project samples
Replicate Analysis
Sample
#D052-TRPB-2 14'-15' 3/12/07 Matrix Spike Hexachlorobutadiene 3.6 mg/kg 4.1 mg/kg 3.8 mg/kg 12.6
Hexachlorobenzene 2.8 mg/kg 4.2 mg/kg 3.5 mg/kg 41.0 *1,2-Dichlorobenzene 3.1 mg/kg 3.3 mg/kg 3.2 mg/kg 4.71,3-Dichlorobenzene 3.2 mg/kg 3.3 mg/kg 3.2 mg/kg 0.91,4-Dichlorobenzene 3.1 mg/kg 3.3 mg/kg 3.2 mg/kg 5.31,2,4-Trichlorobenzene 3.7 mg/kg 3.8 mg/kg 3.8 mg/kg 4.51,2,4,5-Tetrachlorobenzene 3.8 mg/kg 3.0 mg/kg 3.4 mg/kg 25.1
Comments: Control Limits:Results expressed on a dry weight basis. Relative Range < or = 35%.(1) Calculations were performed prior to rounding.(3) nc = not calculated.(*) asterisk = outside standard control limits.
Replicate 1 Replicate 2 MeanRelative Range
(percent)
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: QC0RG0316071-D ATS Project: Reach D PCAP #D052-TRP
Parameter: Semivolatiles (USEPA 8270C) Report Date:
Results of QA Samples run concurrently with project samples
Blank Analysis
Sample Analyzed Concentration QC Decision
#D052-TRPLaboratory Reagent Blank 3/16/07 Less than detectable for all analytes Acceptable
Comments:
3/25/07
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
Quality AssuranceData Summary
QC Batch Number: QC0RG0316071-D ATS Project: Reach D PCAP #D052-TRP
Parameter: Semivolatiles (USEPA 8270C) Report Date:
Results of QA Samples run concurrently with project samples
Surrogate Recovery
Sample
Laboratory Reagent Blank 3/16/07 Laboratory Fortified Blank 3/16/07 B-2 14'-15' 3/12/07 Matrix Spike B-2 14'-15' 3/12/07 Matrix Spike Duplicate B-1 5.2'-6.0' 3/12/07 B-1 13'-14' 3/12/07 B-1 18'-19' 3/12/07 B-2 4'-5' 3/12/07 B-2 10.7'-11.7' 3/12/07 B-2 14'-15' 3/12/07 B-3 6.5'-7.5' 3/12/07 B-3 18'-19' 3/12/07 B-4 8'-9' 3/13/07 B-4 12'-13' 3/13/07 B-5 9'-10' 3/13/07 B-5 14'-15' 3/13/07 B-6 8'-9' 3/13/07 B-6 14'-15' 3/13/07 B-7 9'-10' 3/13/07 B-7 14'-15' 3/13/07 Duplicate 3/13/07 Field Blank 3/12/07 Field Blank 3/13/07
Comments: Control Limits:(1) Calculations were performed prior to rounding. (50-150)(3) nc = not calculated. FBP = 2-Fluorobiphenyl (50-150)(*) asterisk = outside standard control limits.
87.8 91.8 91.8 101.4
74.5 94.4 77.3 86.7
59.7 78.9 67.4 79.5
78.2 89.4 88.1 85.5
75.2 82.6 84.2 81.8
74.9 87.8 98.7 102.3
72.2 82.9 86.7 86.1
72.6 81.2 74.2 84.6
71.2 85.7 81.6 89.8
79.0 90.9 70.0 82.5
83.6 94.2 79.6 86.5
NBZ FBP
86.5 99.2
3/25/07
NBZ = D5-Nitrobenze
TM
ANN ARBOR TECHNICAL SERVICES, INC.
290 South Wagner RoadAnn Arbor, Michigan 48103Tel. 734/995-0995 Fax. 734/995-3731Michigan Laboratory ID: 9604Wisconsin Laboratory ID: 998321720
\\D052-TRP.07\Reach D\Reach D VOC SVOC Report March 07.xls rev. 3/25/07
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