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0001
AMO ENVIRONMENTAL DECISIONS
AUXIER & ASSOCIATES, INC.
West Lake Storm Water
ST AND ARD LEVEL IV REPORT OF ANALYSIS
WORK ORDER #18-06097-OR
July 24, 2018
EBERLINE ANALYTICAL/OAK RIDGE LABO RA TORY OAK RIDGE, TN
0002
TABLE OF CONTENTS
SECTION DESCRIPTION PAGE
I Chain of Custody& pH Check 0004
II Sample Acknowledgement 0012
III Case Narrative 0015
IV Analytical Results Summary 0019
V Analytical Standards 0022
VI Quality Control Sample Results Summary 0050
VII Laboratory Technician's Notes 0061
VIII Analytical Data (Isotopic Uranium) 0088
IX Analytical Data (Isotopic Thorium) 0130
X Analytical Data (Radium-226) 0169
XI Analytical Data (Radium-228) 0203
XII Barium-133 Analytical Tracer Data 0219
XIII Analytical Data (Gross Alpha/Beta) 0248
Last Page 0267
0003
STANDARD OPERATING PROCEDURE
Sample Receiving
Eberline Services - Oak Ridge Laboratory
LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
MP-001, Rev. 19 Effective. 2111118
Page 14 of 15
Eberline Services Work Order # __ 1_8_-_0_6_0_9_7 _____ _ The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial Initials Date Initials Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Client in Possession of Data El
Invoiced by Laboratory
Technical/Clerical Corrections, Signatures Needed, Problems, Etc Date/Initials
Date package approved by:
Laboratory Manager Date
Copy No Radiochemistry Services
0005
Chain of Custody Record N~
Project Name: West '_c ke Stormwater Project Number:
Send Report To: Paul i~osasco / EMSI Sampler (Print Name):~;;"'
Address: Sampler (Print Name): Jl1dr;,e rJpJ/ly,, Shipment Method: FedEx
Airbill Number: /f 2s ;25])5' 9 Ut Phone: Laboratory Receiving:
Fax:
Eberline Services 601 Scarboro Road Oak Ridge, TN 37830 (865) 481-0683 Phone O (865) 483-4621 Fax
2JEBERLINE ~ SERVICES
PagELf__ot_f_
18-06097 REC'D JUN 2 1 2018
Purchase Order·~·----------
. Sample- Sample .... Sample .. -Number of I Comments, Special Lab Sample ID Field Sarn~:le ID Date Time Matrix Containers Instructions, etc. (to be completed by lab)
l,{ - / - (JfY1 / D,,-...:1-f~II 001 D I S / DOO fA t.Ars ;2. I
Note: Level 4 reoc.'-'-;r..,,_t _._,fo""'r....,s""a!.!..!..!.1=-"-'=1--'--"'""""--'"""'"'"-""-"'=~'-'-=,,....,_ Level 2 report required (combine
__ ;___ __ --+---'---+--'---'----+---=------+---+--'-+---+-..:i----+---+-+----+---+----'--+--
Relinquished by: (Signatur3) Date: Time: Sample Custodian Remarks (Completed By Laboratory): tc~ ,' r& r t?-cv ONQC Level I Turnaround I Sample Receipt ·:- -~ ' ,i¼Tinquished by: (Signature,) Time:
;,!/ /"' f J,l/'HTJJ'1'.'TI O 9 Ii) r 3) ~eceivedaiy: (Signafifre) Date: Time:
Total # Containers Received? ~.,.,
Level I D Routine D COC Seals Present? Leve! !I D 24 Hour D COG Seals Intact? Level Ill D 1 Week D Received Containers Intact? Other D Other ___
Temperature?
0006
EBERLINE
Oak Ridge Laboratory
Internal Chain of Custody
Comments
SAMPLE IS DISSOLVED
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep Prep ~ Relinquished by Sample Storage Rough Prep Prep Gmi;ations
Received by Sample Storage Rough Prep Prep Separations
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/"~
Received by fiimple Storag,:,) Rough Prep Prep Separations
~. / .. ____,, Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix i
Sample Fraction
04
Count Room
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18-06097 7/11/2018
UUISO - Level 4 Water
i
HP 210 / 270 Storage Detector Activity : Location
30 RRl.4
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0007
. ~EBER~~'~:;~ · Oak Ridge Laboratory
Internal Chain of Custody
Comments
SAMPLE IS DISSOLVED
Location (circle one
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep Prep ~rations "
Relinquished by Sample Storage Rough Prep Prep ~aration;r
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by s;i~~
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Relinquished by Sample Storage Rough Prep Prep Separations
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Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
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~ Count Room
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'
18-06097 7/11/2018
ThlSO - Level 4 Water
HP 210 / 270 Storage Detector Activity , Location
30 RRl.4
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Printed: 6/21/2018 12:55 PM
0008
EBERLINE ~3EHVl(.::e:_s
Oak Ridge Laboratory
Internal Chain of Custody
Comments
SAMPLE IS DISSOLVED
Location circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep ~a~ions
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by ele~orag;) Rough Prep Prep Separations
--~ Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
Count Room
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:
I
i
Ra226 ~ Level 4 Water
HP 210 / 270 Storage Detector Activity Location
30 RR1.4
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tB 115'5' ·+\ct ,~y 13~
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Printed; 6/21/2018 12:55 PM
0009
( . EBERLINE -~ ,c;EPYICE!::,
·· Oak Ridge Laboratory
Internal Chain of Custody
Comments
SAMPLE IS DISSOLVED
Location (circle one
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep Se~s
Relinquished by Sample Storage Rough Prep Prep s_wefrafions ..__
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep ~ans
Relinquished by Sample Storage Rough Prep Prep S~ns
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
Count Room
Count Room
Count Room
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i
!
18-06097 7/11/2018
Ra228 - Level 4 Water
HP 210 / 270 Storage Detector Activity ; Location
30 RRl.4
Date
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Printed: 6/21/2018 12:55 PM
0010
. . ~EBER~~.i~:~ · Oak Ridge Laboratory
Internal Chain of Custody
Comments
SAMPLE IS DISSOLVED
Location (circle one)
Received by ~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by e Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room
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18-06097 7/11/2018
GaGbT ThSr - Level 4 Water
: I
I HP 210 / 270 Storage : . Detector Activity i Location
j 30 RRl.4
i I
I
Initials Date
A ...... cteiOJ\! Lf fl :J:4 v. ·1-)0; ;l Uh 1{ {,~ \ ~\ l <--i6<
v ~1,/11/t 9) oq fj ~
I
I
Printed: 6/21/2018 12:55 PM
0011
Printed: 6/21/2018 12:07 PM
~ Sample Receiving Report EBER~~~~,~ (Volumes, pH, & CPM)
FR ClientID # Btls Comments Matrix 01 LCS 0 WA
02 BLANK 0 WA
03 DUP 0 WA
04 OU-1-007 Outfall 007 DIS 2 WA Container Number DH Oria
1 7 2 7
Received by: ___ t ___ ·-_l b __ L,L,_·_·~---,-"'· 1--,.. ____ _
Page 1 of 1
Internal Work Order
Storage RRl.4
RRl.4
RRl.4
RR1.4 DH Final
7 7
..
18-06097 Received By
RSPENCER
Rec Vol Ttl CPM Max
7.52 30 Volume Ill CPM
3.7600 26 3.7600 30
MP-001, Rev 5 Effective: 11 /22/02
0013
Client Name Contract/PO Project Type Date Received Required Turnaround Days .. . ... AMO Environmental Decisions WESTLAKE Environmental 06/21/2018 28 18-06097
Project Name Client WO Sample Disp Lab Deadline Internal Deadline I .• •
WESTLAKE WL STORMWATER w 07/11/2018 07/18/2018 07/19/2018 f- <D a:, 0 0
Internal ID Client ID .0 N N U) U) , ~ Sample Date Matrix Storage ('.) N N
"' "' "' .c :5 ('.) 0:: 0:: f-- ::J
01 LCS 06/21/18 WA RRl.4 X X X X X 5
02 BLANK 06/21/18 WA RRl.4 X X X X X 5
03 DUP 06/21/18 WA RRl.4 X X X X X 5
04 OU-1-007 Outfall 007 DIS 06/20/18 10:00 WA RRl.4 X X X X X 5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Totals Per Analysis (non QA samples) 1 1 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Invoice West Lake Landfill OU-1 Resp Report Data Paul Rosasco. P E
~ AMO Environmental Dec1s1ons Eng. Management Support. Inc
Oak Ridge Laboratory PO Box 410 7220 W Jefferson Ave. Suite 406
601 Scarboro Rd. Oanboro. PA 18916 Lakewood. CO 80235 EBER~INE Oak Ridge, TN 37830 ~ERV ICES
Voice 215-230-8282 Voice 303-940-3426
Sample Log In Report Voice: (865) 481-0683 Fax 215-230-8283 Fax
Fax: (865) 483-4621 Contact Marsha Joseph
Voice 865-675-3669
Fax 865-675-3677
Printed 6/2112018 12 55 PM
0014
STANDARD OPERATING PROCEDURE
Sample Receiving
Eberline Services - Oak Ridge Laboratory
SAMPLE RECEIPT CHECKLIST MP-001-2
WORKORDER#_1_8_-_Q_6_O_9_7 __
MP-001, Rev. 19 Effective. 2/11/18
Page 13 of 15
SAMPLE MATRIX/MATRICES: (CIRCLE ONE OR BOTH)
~ NON-AQUEOUS
(CIRCLE EITHER YES, NO, ORN/A)
WERE SAMPLES·
Received in good condition? cry·") N
If aqueous, properly preserved (~) N N/A
WERE CHAIN OF CUSTODY SEALS:
Present on outside of package? C /''J", y) N
Unbroken on outside of package? C y:) ~----- N
Present on samples? ( TI N
( V '0 Unbroken on samples?
y \ N -/ -·
Was chain of custody present upon sample receipt? ( y ') N ~
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: _____________________________ _
SIGNATURE: --~£__·~· ·~(_C_>c...v~"'~· (::_::...> ✓-'~------· --- DATE: __ lQ--=--+-'-(;;u..-<-+-l ...... l_[_' _· --
Copy No. ___ _ Radiochemistry Services
0016
BERLINE
EBS-OR-44023
July 23, 2018
Paul Rosasco
SERVICES
Engineering Management Suppmt, Inc. 7220 W. Jefferson Ave., Suite 406 Lakewood, CO 8023 5
SAMPLE RECEIPT
CASE NARRATIVE Work Order# 18-06097-OR
EBERLINE ANALYTICAL CORPORATION
601 SCARBOFlO F~OAD
OAK RIDGE. TEf'-lNESSEE 37850
PHONE (865) 481-0663
FAX (865) !~83-·L,621
This work order contains one water sample received 06/21/2018. Sample was analyzed as dissolved for Isotopic Uranium, Isotopic Thorium, Radium-226/228 and Gross Alpha/Beta.
CLIENT ID
OU- 1-007 Outfall 007 DIS
ANALYTICAL METHODS
LAB ID
18-06097-04
Isotopic Uranium was analyzed using EPA Method 908.0 Modified. Isotopic Thorium was analyzed using EPA Method 907.0 Modified. Radium-226 was analyzed using EPA Method 903.0 Modified. Radium-
228 was analyzed using EPA Method 904.0. Gross Alpha/Beta was performed using EPA Method 900.0
Modified.
ANALYTICAL RESULTS
Combined Standard Unce1tainty is repo1ted at I-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this repmt are sample-specific.
MDA measurements are dete1mined based on factors and conditions including instrument settings, aliquot size and matrix type.
SPECIAL CIRCUMSTANCES
Samples were filtered through 0.45 µm media to dissociate the suspended fraction from the dissolved
fraction. After filtration, samples were preserved with nitric acid to a pH of <2.0. Results for this work order are all from the dissolved fraction.
Page 1 of 3
0017
ANALYTICAL RES UL TS CONTINUED
ISOTOPIC URANIUM
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Sample demonstrated acceptable results for all Uranium analyses. Total Uranium results were calculated
by mass conversion of Isotopic Uranium activity. Chemical recovery was acceptable for all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for
the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an acceptable
percent recovery.
ISOTOPIC THORIUM
Sample was prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy using energy specific regions of interest for Thorium-230 and Thorium-232. Chemical recovery was
determined by the use of a Thorium-229 tracer. Activity of the Thorium-229 tracer was determined by
alpha spectroscopy using an energy specific region of interest.
Sample demonstrated acceptable results for all Thorium-230 and Thorium-232 analyses. Chemical
recovery was acceptable for all samples. The Thorium-230 and Thorium-232 method blank demonstrated
acceptable results. Results for the Thorium-232 duplicate demonstrated a high relative percent difference;
however, normalized difference is within acceptable limits for the analytical technique. Results for
Thorium-230 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Thorium-230 and Thorium-232 laboratory control sample demonstrated an acceptable
percent recovery.
RADIUM-226
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. This was followed by precipitations of Radium/Barium Sulfate. Precipitates were dissolved in alkaline EDTA. Radium was selectively precipitated and then mounted on micro-porous filter media. Sample was counted by alpha spectroscopy using an energy specific region of interest for Radium-226. Inherent self-absorption from elemental Barium was corrected for in the final result. Chemical recovery was calculated by the use of a Barium-133 tracer, which was determined by HPGe gamma spectroscopy.
Sample demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated an acceptable result. Results for the
Radium-226 duplicate demonstrated a high relative percent difference; however, normalized difference is
within acceptable limits for the analytical technique. Results for the Radium-226 laboratory control
sample demonstrated an acceptable percent recovery.
Page 2 of 3
0018
c--------
ANALYTICAL RESULTS CONTINUED
RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium-
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were then
counted on a gas prop011ional counter. Chemical recovery was determined by the use of a Barium-133
tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Sample demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated an acceptable result. Results for the
Radium-228 duplicate demonstrated a high relative percent difference; however, normalized difference is
within acceptable limits for the analytical technique. Results for the Radium-228 laboratory control
sample demonstrated an acceptable percent recovery.
GROSS ALPHA & BETA
Sample was prepared by evaporation of a representative volumetric aliquot acidified with HNO3.
Reduced sample was then transferred to a steel planchet for final evaporation to dryness and flaming.
Sample was then counted on a gas proportional counter. Results were corrected as required for inherent
self-absorption based on residual mass present.
Sample demonstrated acceptable results for all Gross Alpha and Beta analyses. Due to the high Total
Dissolved Solids content within the sample, method detection limits are slightly high. The Gross Alpha
and Beta method blank demonstrated acceptable results. Results for the Gross Alpha and Beta duplicate
demonstrated a high relative percent difference; however, normalized difference is within acceptable
limits for the analytical technique. Results for the Gross Alpha and Beta laboratory control sample
demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I ce11ify that this data repo11 is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
M.R.McD~ll I Laboratory Manager 1
i Date: 7/23/2018
l'bcrlinc /\nalylical wunts and encourages your feedback regarding our performance providing radiounalylical services. Pkasc
visi1 http://eberlincanalytical.com/ to provide us wilh feedback on our services.
Page 3 of3
0020
Printed: 7/23/2018 9:07 AM
Eberline Analytical Final Report of Analysis
Lab ID
18-06097-01
18-06097-01
18-06097-02
18-06097-03
18-06097-04
18-06097-01
Sample Type
LCS
LCS
MBL
LCS
18-06097-01 LCS
18-06097-02 MBL
18-06097 -03
18-06097-04
18·06097-01
18-06097 •01
18-06097-02
18-06097 •03
18-06097 -04
LCS
LCS
MBL
LCS
KNOWN
SPIKE
BLANK
Client ID
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
KNOWN
SPIKE
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
KNOWN
SPIKE
BLANK
OU·1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
18-06097-01
18-06097-01
18-06097-02
········----···-·•--s-••··-KNOWN
SPIKE
18-06097-03
18-06097-04
18-06097-01
18-06097-01
18-06097-02
18-06097-03
18-06097-04
18-06097-01
18-06097-01
18-06097-02
18-06097-03
18-06097-04
LCS
MBL
LCS
LCS
MBL
DUP
DO
LCS
LCS
MBL
DUP
DO
BLANK ................. -•-············
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
KNOWN
SPIKE
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
KNOWN
SPIKE
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
Report To:
Paul Rosasco, P.E.
Eng: ManagE!n:1~11! ~l_lP.PC>_!t,_ Inc ... 7220 W. Jefferson AvE!., ... ~llite .. 406 Lakewood, CO 80235
Sample Date
06/21 /18 00:00
06/21/1800 00
06/21/18 00:00
06/20/18 10:00
06/20/18 10:00
06/21/18 00:00
06/21/18 00:00
06/21/18 00:00
06/20/18 10:00
06/20/18 10:00
06/21118 00:00
06/20/18 10:00
06/20/18 10:00
06/21/18 00:00
06/21/18 00:00
Receipt Analysis Batch Date Date ID
6/21/2018 7/11/2018 18-06097
6/21/2018 7/11/2018 18-06097
6/21/2018 7/11/2018 18-06097
6/21/2018 7/11/2018 18-06097
6/21/2018 7/11/2018 . 18-06097
Analyte
Gross Alpha
Gross Alpha
6/21/2018 7/11/2018 18-06097 Gross Beta
6/21/2018 7/11/2018 18-06097 Gross Beta
6/21/2018 7/11/2018 18-06097 Gross Beta ,~,~~•~•-- ~•----v~~m,_
6/21/2018 7/11/2018 18-06097 Gross Beta - __ ,,-,, ,.__,,.,_ ,,,,,,, ___ ...,,.,._~_,~,m 6/21/2018
6/21/2018 7/9/2018
6/21/2018 7/9/2018 18-06097 Radium-226
6/21/2018 7/9/2018 18-06097 Radium-226 ······-··-·----········· .--1 ....
6/21/2018 7/10/2018 18-06097 Radium-228 •• o~~~w ~-•~mmw, """
6/21/2018 7/10/2018 . 18-06097 .Radium-228 +-· 06/21/18 00:00 6/21/2018 7/10/2018 18-06097 Radium-228
06/20/18 10:00 6/21/2018 7/10/2018 · 18-06097 Radium-228
06/20/18 10:00 6/21/2018 7/10/2018 18-06097 Radium-228
06/21/18 00:00
06/21 /18 00:00
06/21/18 00:00
06/20/18 10:00
06/20/18 10:00
06/21/18 00:00
06/21/18 00:00
06/21/18 00:00
06/20/18 10:00
06/20/18 10:00
6/21/2018 7/10/2018 18-06097 Thorium-230
6/21/2018 7/10/2018 18-06097 Thorium-230
6/21/2018 7/10/2018 18-06097 Thorium-230
6/21/2018 7/10/2018 18-06097 Thorium-230
6/21/2018 7/10/2018 18-06097 Thorium-230
6/21/2018 7/10/2018 18-06097 Thorium-232
6/21/2018 7/10/2018 18-06097 Thorium-232
6/21/2018 7/10/2018 18-06097 Thorium-232
6/21/2018 7/10/2018 18-06097 Thorium-232
6/21/2018 7/10/2018 18-06097 Thorium-232
SDG:
P_rojec_t: Analysis Category·
Sample Matrix:
Method
EPA 900.0 Modified
EPA 900.0 Modified
Work Order Details·
18-06097 WESTLAKE ENVIRONMENTAL WA
Result cu CSU
2.71 E+02
2.97E+02
1.16E+01
3.77E+00 3.26E+01
MDA
2.39E-01
Page 1 of 2
CV
9.99E-01
Report Units
pCifl
EPA 900.0 Modified 2.77E+02 8.32E+00 --~-s-••··-··-•--'"•····---s-----··········--· ----·········
2.62E+02 2.95E+00 3.63E+01 5.04E-01 1.15E+00 pCi/1
-1.28E-01 2.72E-01 2.73E-01 5.96E-01 1.52E+00 pCi/1 ···············-···········•··························s··-······· EPA 900.0 Modified 2.91 E+00 5.26E+00 5.27E+00 1.08E+01 2.40E+01
EPA 900.0 Modified 1.14E+01 5.14E+00 5.37E+00 9.83E+00 2.29E+01 pCifl
EPA 904.0
EPA 904.0
EPA 904.0
EPA 907.0 Modified
EPA 907.0 Modified
1.37E+00 2.53E+00 2.87E-01 -,~--~- __ , ____ ~-~ ''-----·--·~-
1.05E-01 1.06E-01 3.70E-01 3.46E-02 pCi/1
4.69E-01
7.52E-01
3.09E-01 3.78E-01 4.17E-02
2.14E-01 4.06E·01 3.85E-02
2.09E+00 8.66E-01 8.83E-02
pCi/1
pCi/1
~----,,~---------
pCi/1
pCi/1
pCi/1 4.48E-01 4.27E-01 4.39E-01 8.63E-01 9.19E-02 ······-··-·····-·•············------·--·
8.70E-01 4.99E-01 5.37E-01 9.81 E-01
4.12E-01 4.12E-01 8.71E-01
1.45E-01
1.31E+00 1.55E+00 1.53E-01 '------------ -~---- ,_,,, _____ ,,, ____ ,,,,,,,,,_, __ , ___ _ 6.63E-02 6.66E-02 1.04E-01 9.47E-02 pCifl ·-· --------~~-- ""' "" ,,,, ___ , __ 8.88E-02 9.07E-02 5.26E-02
.. ___ ,,,,_,__ ----~-·-1.73E-01
4.87E+00
1.90E-02
1.08E-01 1.1 0E-01 9.65E-02 9.16E-02 pCi/1
1.75E-01
1.18E+00 1..28E+00 1.44E-01 ---,,~---·-·---- ---
5.37E-02 5.38E-02 8.76E-02
4.38E-02
5.21 E-02
4.38E-02 7.09E-02
5.21E-02 1.07E-01
pCifl
2.00E-02 pCi/1
1.72E-02
9.85E-03
2.64E-02
pCi/1
pCi/1
pCi/1
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value
( EBERLINE ~ -
EBERLINE ANALYTICAL CORPORATION
601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
0021
Printed: 7/23/2018 9:07 AM Page 2 of 2
Report To· Work Order Details:
Eberline Analytical Paul Rosasco, P.E. SDG: 18-06097 ~11JI.:llll-a,_11~g~!l!ent Support, Inc. P,:oLect: WESTLAKE
Final Report of Analysis 7220 W. Jefferso11_Ave,_~llite 406 Anatys_is_~ategory. ENVIRONMENTAL . .. ,_,
Lakewood, CO 80235 Sample Matrix: WA Lab Sample Client Sample Receipt Analysis Batch Report
ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA CV
Units
18-06097-02 MBL BLANK 06/21/18 00:00 6/21/2018 7/10/2018 18-06097 Total Uranium EPA 908.0 Modified 1.90E-01 1.90E-01 3.00E-01 1.54E-02 ug/I ,,_, __
18-06097-03 DUP OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 4.65E-01 4.70E-01 4.46E-01 2.05E-02 ug/I
18-06097-04 DO OU-1-007 Outfall 007 DIS 06/20/18 10:00 2.75E-01 2.94E-01 "--~"'-,,~--, "-' ,,, ________ ,,,. -"'"' '""'"·----
18-06097-01 pCin
""•"'~,,-,,~,,
18-06097-01 LCS SPIKE 06/21/18 00:00 6/21/2018 9.05E-01 7.77E-02 1.47E-02 pCin .--~---- ''" ---~,~--
18-06097-02 MBL BLANK 06/21 /18 00:00 6/21/2018 7/10/2018 7.36E-02 8.90E-02 2.13E-02 pCin
18-06097-03 DUP OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 7/10/2018 1.52E-01 1.32E-01 2.95E-02 p """'"'-·-·-·-·-~-•--· .. e"-''"' ---------,-~•-•<- '""'"-"'-----·--·- .. ---~-~-
18-06097-04 DO OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 7/10/2018 18-06097 1.18E-01 1.19E-01 1.17E-01
18-06097-01 LCS SPIKE 06/21 /18 00:00 6/21/2018 7/10/2018 18-06097 Uranium-235 1.77E-01 1.80E-01 6.68E-02
18-06097-02 MBL BLANK 4.63E-02 1.01E-01 1.49E-02 pCin ,,,,,,,, __ ,,,,, "--·--,,,,
18-06097-03 DUP OU-1-007 Outfall 007 DIS 1.21E-01 1.21E-01 1.56E-01 2.31E-02 --~--------··--~ ··~"'""'" __ ,,,,,,,,,,,,._
18-06097-04 DO OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 7/10/2018 18-06097 Uranium-235 4.02E-02 4.03E-02 8.44E-02 4.92E-03
18-06097-01 LCS KNOWN 06/21/18 00:00 6/21/2018 7/10/2018 18-06097
18-06097-01 LCS SPIKE 06/21/18 00:00 6/21/2018 7/10/2018 18-06097 9.18E-01 -----~--·---- .,,,_,,,,,_ __ "'""•-----~•-•_,,,,,,,,,,_
18-06097-02 MBL BLANK 06/21/18 00:00 6/21/2018 7/10/2018 18-06097 Uranium-238 EPA 908.0 Modified 6.22E-02 6.33E-02 6.35E-02 8.52E-02 1.83E-02 pCin
--·-------- ,,,,, .. --·-------
18-06097-03 DUP OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 1.55E-01 1.56E-01 1.26E-01 -•-•-•-~=•~-vn-•-~•-""'"-,,,,,=• --•-""'"" ---·-·-
__ ,,_, ________
18-06097-04 DO OU-1-007 Outfall 007 DIS 06/20/18 10:00 6/21/2018 9.17E-02 9.21E-02 8.57E-02 1.20E-02 pCi/I
CU:Counting Uncertainty;CSU:Combined Standard Uncertainty (1-sigma);MDA:Minimal Detected Activity;LCS:Laboratory Control Sample; MBL:Blank; DUP:Duplicate; TRG:Normal Sample; DO:Duplicate Original; CV:Critical Value
( . EBERLINE M> ANALYTICAL
EBERLINE ANALYTICAL CORPORATION
601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
0023
..__, ·-·
QA/QC REVIEWED CERTIFICATE OF CALIBRATION L,L-8
Date '7 q(lnitials J![_ ALPHA STANDARD SOLUTION Radionuclide: U-238NAT
Half Life:
Customer:
P.O.No.:
TMA EBERLINE
OR2778
Catalog No.:
(4.468 ± 0.005) x 10~9 years
7338 Reference Date: January 1 1995 12:00 PST.
Source No.: 479-50 Contained Radioactivity: (Total U) 8.016 µ.Ci
Contained Radioactivity: (fotal U) 297 kBq
Description of Solution a. Mass of solution:
b. Chemical form:
65. 2896 g in a 50 ml flame sealed ampoule
Uranyl Nitrate in H20
c. Carrier content: None
d. Density: Approximately I.3202
Radioimpurities
Radioactive Daughters
Refer to attached technical data sheet
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228 Method of Calibration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3.0%
±0,0%
±2,0%
±3,6%
•
g/ml @20°c.
µCi/g.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes•, edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to l!otablish and maintain implicit traceability for a number of nuclidcs,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4. 15).
E=(t(vAu,.A_2 YCONfROL
·· ... ·.·1·· · .. ~. \.•· .. ·:··· .. ·'.···•·:· .. \; ... ·.··.··.··• .. · .. t7J?'. . .
. · .. ·. · .. ·.
: . '-.:.: .. ·-·:.
ISOTOPE PRODUCTS LABORATORIES
3017 N, SAN FERNANDO BLVD.
~ Oet,€r,,1hz{k I f?:2f Date Signed
l ·s. 0 T O P I,
·rROD.UCT.S
l,ABCJRATORIES·:
BURBANK, CALIFORNIA 91504
8]8•843•7000 FAX 818•843•6168
0024
Rev.a; 11101103
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Refere11ce Sta11dards Solutions & Records
EBERLINE SERVICES* OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP 009
CURRENT DATE 7/6/2018 0:00 SOLUTION REFERENCE #....,IP...,L ..... 4_7__,9...,-5,,,,.0,.,...: -----.------, SOLUTION #1-----,U..,....S._--,.,-1
Princi al Radionuclide 234, s, 238u
Radionuclide
Half Life, Years 1 · 4.468E+09j
------1 Certified Activity 8;0}61::+00 µCi Certified Concentration...__ ___ __,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Chemical Composition of Standard Solution I Uranyl nitrate in diluteHNO3. · ·
Half Life, Days l 1,632E+12I
Reference Date!,_ __ 1_/1'--/_19_9_5_0_:0__.o!
97.6400 Weight, Grams 32;$020 Weight, Grams 65.1380 Weight, Grams
8.0160 µCi
Dilution Instructions: Dilution Solvent Used l1MHN03,
Dilute to a volume of! ·· · 1000~00 ·. jmilliliters
Certified Total Activity of! 8.016DjµCi Which Equals 1.780E+07ldpm at the date listed above
This activity concentration is based on the original And after dilution the activity of this solution isl 1. 77955E+04ldpm/m~eforence date listed above. Ail activities am corrected
to the date and time of analysis by the laboratory dai.a processing software.
Expiration Date: I June 26, 2019
Date; 7/6/2018 0:00 --------Date: J i&-J,,c: ----'-1,.......,.,-.~--
0025
Rev.8; 11101/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES ~ OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY Dil.UTJON RECERTIFICATION
MP-009 Solution Reference# JPL479,50
Princi al Radionuclide 234. i35. 238u
Radionuclide of Interest 234• 235
· 238u
Half Life, Years I 4.468E+oel
Parent Solution Cone. 1.7796E+04 dpm/ml
Date 7/6/2018 0:00 Solution # . U-8a
Half Life, Days I 1.632E+12I
Reference Datel._ _ _;....;· 1 .... 11"'°'·11;..,.;e....;.9.;;..5-"'o;a.;;.OO_.!
Chemical Com osition of Standard Solution Uranly Nitrate in 1M HNO3 ·
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
4.0000 ml 7.1182E+04 dpm
1000.00 ml Final Activity Concentration: I 7. 1182E+01 jdpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and tirne of analysis by the laboratory data processing software. ------------------------, Isotopic Distribution as:
U-238 Atom%= 48.239 U-235 Atom % = 2.25 U-234 Atom % ,, 49.501 All values +/- 3.6%
U-238 == 71.182 dpm/ml X 0.48249 = 34.345 dpm/ml U-235 = 71.182 dpm/ml X 0.0225 = 1.602 dpm/ml U-238 = 71.182 dpm/ml X 0.49501 = 35.236 dpm/ml
Isotopic ratios from manufacturer's data sheet ....--....._
9 Expiration Date:f June 26, 2011
Date: 7/6/2018 0:00 _____ ;..._.:..:.;;,_
Date: __ ~--1(-'-'-'+-/__,?.....___
0026
RECORD COPY
Tracer Solution for Environ1nental Analysis & Disequilibrium Studies
Description
Product Description & Measurement Certificate
Principal radionuclide: Daughter Nuclide:
uranium 232 (U-232) Th-228
Product code: UDPl 0050 Batch Number: 92/232/67
Measurement Reference date: 01 March 2000
Accuracy
Radionuclidic Purity
Isotopic Purity
Chemical Composition
Physical Data
Remarks
Approved Signatory
Radioactive concentration U-232 which is equivalent to
6.739E+o3 becquerels per gram of solution 1.821E-01 microcuries per gram of solution
Volume of solution Total activity ofU-232
which is equivalent to
5.035 millilitres 3.61E+o4 becquerels 9. 76E-O 1 microcuries
Method of measurement (see reverse of this certificate) Random uncertainty is:± 0.7% Systematic uncertainty:± 0.5% Overall uncertainty in the radioactive concentration quoted above: ± 1.7% Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages of the activity of the principle radionuclide at the referenc•e date.
Th-228 and daughter activity removed 2 Feb 2000 U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on l/3/00
""he isotopic composition, exprP,Ssed as atom per cent at the reference date .
i'Jot measured
Calculated weight ofU-232, 4.42E-08 grams, as 2M HNO3 solution in a flame sealed glass vial. This Tracer solution has been produced 'carrier free'.
Recommended halflifo of uranium 232: 6.980E+Ol years Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0% Branching ratio for alpha emission: 100% Calculated specific activity of uranium 232: 8.167E+o5 Bq per microgram U-232.
For safety information and notes to ensure correct usage by all persons handling this radior1ctive Tracer solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and approved to ISO 9001.
Project Ref. AE23 l 5
Roger Wiltshi.re
Prepared and characterised .in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps I 0/03/00 AEA Techn,;logy is the trading name of AEA Technology pJc
0027
1(EBER~~"~~ Rev.a; 11/01/03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP009
.----------,CURRENTDATEt--I __ 10~/7~/~20_1_7_0_:0---10I SOLUTION REFERENCE# AENAmersham 92/232/67 I SOLUTION #I U-10 I
Principal Radionuclide 232u I
Half Life, Years
I· 7.200E+01 I Half Life, Days I 2.630E+04I
Radionuclide 232U Reference Date ._I ___ 3/_1_/2_0_00_0:_0_,0 I
Certified Activity 9. 760E-01 µCi Certified Concentration · µCi per gram ....__ ___ ....
Ampoule /Solution Gross~Weight, Grams Empty Ampoule Weight, Grams
Solution Net Weight, Grams Total Activity in Ampoule 0.9760 µCi
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume ofl 1000.00 !milliliters
Certified Total Activity ofl 0.9760lµCi Which Eauals I 2.167E+06ldpm at the date listed above
And after'dilution the activity of this· solution isl 2.167E+03ldp'm/ml This activity concentration is based on the original reference date listed above. All activities are corrected to tl1e date and time of analysis by the laboratory data processing software.
Expiration Date:! October 4, 2018 I
Date: 10/7/2017 0:00
Date:
--------/0 /✓0/,·7
I I
0028
Rev.8; 11/01/03
QUALITY CONTROL PROGRAM . MP-009
Title; Radioactive Reference Standards Solutions & Records
EBERUNE SERVICES - OAK RIDGE LABORATORY · RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Date f--__ 1_0/_7_/2_0_17_0:_00---1
Solution Reference # AEA/Amersham 92/232/67 Solution# U-10a
Principal Radionuclide 3 .u
Radionuclide of Interest 23 U
Half Life, Years
I 7.200E+01 j
Parent Solution Cone. 2.167E+03 dprn/rnl
Chemical Composition of Standard Solution
Half Life, Days
I 2.630E+041
Reference Date~' ___ 3/_1_/2_0_00_0_:_oo~I
Dilution Instructions: Dilution Solvent Used
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
10.0000 ml 2.1670E+04 dpm
1000.00 ml Final Activity Concentration: I 2.1670E+01 jdpm/ml
This activity concentration is based on the original reference date listed above. All activities are · corrected to the date and time of analysis by the laboratory data processing software. ·
Expiration Date:! October 4, 2018
0029
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Radionuclide: Th-232
Half Life: . (1.405 ± 0.006) x 10" 10 years Customer:
P.O.No.:
TMA EBERLINE
VH1632
14-B
Catalog No.: 7232
435-104-2
Reference Date: November 1 1993 12:00 PST.
Source No.: Contained Radioactivity: (Th-232) 0.0933 µCi.
Contained Radioactivity: (Th-232) 3.45 kBg.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
11.9712 g (in a 10 ml flame sealed ampoule)
Th(N03)4 in water
None added
d. Density: Approx. 1.21 g/ml @20°C.
Radioimpurities None detected (other than daughters).
Radioactive Daughters Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208
Radionuclide Concentration
(Th-232) 0.00779
Method of Calibration Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3,0%
±0,0%
±2,0%
±3,6%
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
µCi/g.
2. IPL participates in an NIST measurement assurance program lo establish and maintain implicit traceability for a number of nuclides,
ba.ed on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4. 15).
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000
QUALITY CONTROL
;Vw. ~.1 l 1 'l > Date Signed
0030
Rev.8; 1/10/03
QUALITY CONTROL PROGRAM MP--009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERT/F/CA TION
MP 009
CURRENT DATE 8/16/2017 0:00 SOLUTION REFERENCE #""IP"'""L-4.,..,3....,5....,.:.1,._.04,...:....,.2-· -----. SOLUTION #1-----.=T--h-8...,....;.'--'-'---,-1
Princi al Radionuclide 23 Th, 228Th
Half Life, Years l 1AOSE+tol
Half Life, Days l 5.132E+12!
Reference Date! L.. __ 1 ___ .1_/.1_/1_9_93_· _o:_oo .... l
Ampoule /Solution Gross 18.8415 Weight, Grams Empty Ampoule. ~ ..... 6.9296 Weight, Grams
Solution Net 11.9119 Weight, Grams Total Activity in Ampoule 0.0933 µCi
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used . j1% NitricAcid
Dilute to a volume ofl. -1000.00 . I milliliters
Certified Total Activity ofl 0.0933lµCi Which Eauals 2.071 E+05ldpm at the date listed above
And after dilution the activity of this solution isl 2.071 E+02ldpm/ml This activity concentration is based on the original . . reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data processing software.
Expiration Date: l August 11, 2018
R/1Rl?n17 n-n0
Date: --=gj+-f_,wµ ..... C_,__J--
0031
Rev.8; 1/10/03 Title: Radioactive Reference Standards· Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Solution Reference# IPL 435:::104-2
Princi al Radionuclide 2w&232Th
Radionuclide of Interest · 228 &
232Th
Half Life, Years I 1.4b5E+1ol
Parent Solution Cone. 2.07E+02 · dpm/ml
Chemical Composition of Standard Solution
Date 8/16/2017 0:00 Solution # • ·· · Th,8b
Half Life, Days I 5.132E+12I
Reference Date._l __ 1.;..;1.;../1;.;../1.;...;9...;.9.;.3.;;..0:;.;;.o.;.iol
Dilution Instructions: Dilution Solvent Used l 1 % Nitric Acid
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
· 500,0000 ml 1.0355E+05 dpm
1000.00 ml Final Activity Concentration:! 1.0355E+02jdpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:l August 11, 2018 f
Date: 8/16/2017 0:00
I
0032
RTIFICA TE OF CALIBRA Tl<>ti.t~ 99
\
LPHA ST AND ARD SOLUTION" \Jc' \ ~~t\\t\~,
Radionuclide
Half Life:
Th-230 Customer:
P.O.No.:
~~tit~ \,'?A TMA EBE~~ ~ \t,t \
Catalog No.:
(7 .54 ± 0.03) x 10"4 years
7230 TI4944 \)t\l
Reference Date: November 1 1991 12;00 PST.
Source No.: Contained Radioactivity: 1.036 µCi.
Description of Solution a. Mass of solution:
b, Chemical form:
c. Carrier content:
d. Density:
Radioimpurities
Radioactive Daughters
Radionuclide Concentration
Method of Calibration
5.0042
Th(NO3)4 in O.lN HNO3
None added 1.0016
See attached technical data sheet
See attached technical data sheet
0.207
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
NIST Traceability
±2.0%
±0,5%
±0,2%
±2,7%
grams.
gram/ml @ 20°c.
µCi/gram.
This calibration is implicitly traceable to the National Institute of Standards and Technology. Notes
1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Virginia S. Shirley. 2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of Standard Reference Materials. (As in NRC Regulatory Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES 1800 No. Keystone Street., Burbank, California 91504 818 843 - 7000
0033
Rev.14; 10/10/2012
QUALITY CONTROL PROGRAM MP-009
Tille: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIF/CA TION MP 009
CURRENT DATE 2/10/2018 0:00 SOLUTION REFERENCE #,...IP-L-38-8---11_6 ____ _____, SOLUTION #1---T-h---1---1
Princi al Radionuclide 230Th
Half Life, Years
I 7.540E+04l
Radionuclide 230Thorium Certified Activity 1.036E+00 µCi
Certified Concentration ...__ ___ __,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Chemical Composition of Standard Solution
Half Life, Days
I 2.754E+07I
Reference Date._! __ 1_1_/1_/1_9_9_1 _0_:o__,ol
9.2660 Weight, Grams 4.6218 Weight, Grams 4.6442 Weight, Grams 1.0360 µCi
Dilution Instructions: Dilution Solvent Used
Dilute to a volume of I 1000.00 !milliliters
Certified Total Activity ofi 1.0360jµCi Which Eauals 2.300E+06ldpm at the date listed above
. • • • • . • .----------, This activity concentration is based on the original
And after d1lut1on the act1v1ty of this solution isl 2.300E+03jdpmITTtl-ence date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: I January 10, 2019
Date: 2/10/2018 0:00 -----,----Date: '3 q;
---'-'--+="'-I-'-=;......-
0034
Rev.14; 10/10/2012
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION RECERTIFICATION
MP-009 Date! 2/10/2018 0:001
Solution Reference# IPL 388-116 I Solution #I Th-1 b I
Principal Radionuclide ,.,uTh j
Half Life, Years
I 7.540E+04I
Half Life, Days
I 2.754E+o7\
Radionuclide of Interest ,.,uThorium Reference Date!..._ __ 1_1_/1_/1_9_9_1 _0_:o~ol
Parent Solution Cone. 2.30E+03 dpm/ml
Chemical Composition of Standard Solution
Dilution Instructions:
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
Dilution Solvent Used 10.1N HN03
SECONDARY VOLUMETRIC DILUTION
10.0000 ml 2.2999E+04 dpm
1000.00 ml Final Activity Concentration: I 2.2999E+01 ldpm/ml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.
Expiration Date: l January 10, 2019 !
Date: 2/10/2018 0:00
Date:
-------
2, ,3/1 c;:( I
0035
-~ Isotope Products Laboratories
24937 Avenue Tibbitts Valencia, California 91355
An Eckert & Ziegler Company Tel 661•309•1010 Fax 661•257•8303
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Radionuclide: Half-life: Catalog No.:
Th-229 7340 ± 160 years 7229
Customer: P.O.No.: Reference Date:
EBERLINE SERVICES 00009633 15-Jan-02 12:00 PST
Source No.: 867-54 Contained Radioactivity: (Th-229 only)
1.013 µCi 37.48
Physical Description: A. Mass of solution:
B. Chemical form:
5.0147 gin 5 ml flame-sealed ampoule Th(NO3)4 in 0.1 M HNO3
C. Carrier content: 10µg Th/ml D. Density: 1.0016 g/mL @ 20°c.
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration: 0.2020 µCi/g, 7.474 kBq/g
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in µCi/g was determined using gamma ray spectrometry. Peak energy used for integration: 193 .5 keV Branching ratio used: 0.0441 gammas per decay
Uncertainty of Measurement: A. Type A (random) uncertainty: B. Type B (systematic) uncertainty: C. Uncertainty in aliquot weighing: D. Total uncertainty at the 99% confidence level:
Notes: - See reverse side for leak test(s) performed on this source.
± 0.7 % ± 3.0 % ± 0.0 % ± 3.1 %
7Ji-, 8
kBq
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261. - This solution has a working life of 5 years.
QualityTuntrol Date Signed IPL Ref. No.: 867-54
------------------ ISO 9001 CERTIFIED ------------------Medical Imaging Laboratory Industrial Gauging Laboratory
24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank, California 91504
0036
,: IS: BE .. i,,1,~o!'< I QUALITY CONTROL PROGRAM
MP-008
Rev.a; 1110/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICA T/ON
MP 009
CURRENT DATE 8/16/2017 0:00 SOLUTION REFERENCE #,...IP_L.,....8-67-.• ...,54...,··:-· --.,-,-_.,...-, SOLUTION #1-•· ---:-. ·T-h-.,.1-8-· --
Half Life, Years I i340E+03l
Half Life, Days ! 2.681E+06j
Radionuclide m-rh Certified Activity 1.013E+0O µCi
Reference Date ... l __ 1_/_15_/2_0.,...02_0:_oo .... J
Certified Concentration._ ___ _,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
8.7752 Weight, Grams .. -.. ~,7591 Weight, Grams
5.0161 Weight, Grams 1.0130 µCi
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume of! .· 1000~00. !milliliters
Certified Total Activity ofl 1.0130jµCi Which Equals 2.249E+06jdpm at the date listed above
This activity concentration is based on the original And after dilution the activity of this solution isl 2.249E+D3jdprn/ml reference date listed above. Alf activities are corrected to the date and time of analysis by the laboratory data processing software,
Expiration Date: I August 11, 2018
VP.rifiArl P.. AnnrnvArl Av " ----::,:,-r'!"-------+--½---- n~tA· R/1RI?n11 n-nn
Date:
0037
, f;:;J:3g'.R,L,JNg I QUALITY COMPNnTo9ROL PROGRAM ~ S~RVICC:$ "'\I
Rev. 7; 9/29/99 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Solution Reference # IPL ae7,:,54
Princi al Radionuclide · 229rh ·
Radionuclide of Interest 229rh
Half Life, Years ! 7.340E+03!
Parent Solution Cone. 2.25E+03 dpm/ml
Date 8/16/2017 0:00 Solution# Th~18a ..
Half Life, Days l 2.aa1 E+oaj
Reference Date ... ! __ 1_/1_5_/2_0_02_0:_oo ..... l
Chemical Com osition of Standard Solution
Dilution Instructions:
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
· · · 10:0000 ml 2.2490E+04 dprn
1000:00 ml Final Activity Concentration: I 2.2490E+01 !dpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: I August 11, 2018
Date: __ a_11_6,_12_0 ... 17_0_:.;..oo_
D;,.te:_~-f c./F----,'(3.___· ·.
0038
jl}attonal 1Jnstttute of ~tanbatbs & ~tcbnologp
C!terttf tcate' · 0\
't ,/)., ,~
~· C / · • 1 (1 Standard Reference Material 4251C Barium-133 Radioactivity Standard V ·1-
This Standard Reference Mate.rial (SRM) consists of radioactive barium-133 c~loride, non-radioactive barium
chloride, and hydrochloric acid dissolved in 5 mL of distilled water. The solution is contained in a flame
sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization chambers and
solid-state gamma-ray_spectrometry.systems.
Radiological Hazard
The SRM ampoule contains barium-133 with ·a total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during tlle decay process X-rays and galllI?a rays with energies from 4 to 400 ke V are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiation hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to minimize personnel exposure .. The SRM should be
used only by persons qualified to handle radioactive material. ·
Chemical Hazard
The SRM ampoule c_ontains hydr~chloric acid (HCl) with a concentration of 1 mole per liter of water. The
solution is corrosive and represents a health hazard if it comes in contact with eyes or skin, If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened only by persons qualified to handle both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 °C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule ( or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar~ Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899 October 1994
SRM 4251C, page 1 of 6
Thomas E. Gills, Chief Standard Reference Materials Program
*Notes and references are on pages 5 and 6.
0039
(EBER!;-;~~!', I QUALITY CONTROL PROGRAM
QCP-009
Rev.8; 11/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PH/MARY DILVTION RE'CERTIFICA TION
QCP 009-1
CURRENT DATE 5/5/2018 0:00 SOLUTION REFERENCE #.-N-IS_T_S_R_M_4_2_5_1 C---...... SOLUTION #1----B-a--6-----1
Princi al Radionuclide 133Barium
Half Life, Years
I 1.048E+01 I Radionuclide lJ;jBarium
Certified Activity µCi 1---,---,,-----,--i
Certified Concentration 1.318E+01 µCl per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Chemical Composition of Standard Solution j1 33BaCl2 in 1 M HCI
Half Life, Days I 3.828E+03I
Reference Date~l ___ 9/_1_/1_9_93_0_:o_,ol
9.3081 Weight, Grams 4.2582 Weight, Grams 5.0499 Weight, Grams
66.5577 µCi
Dilution Instructions: Dilution Solvent Used !1M HCI
Dilute to a volume of! 1000.00 I milliliters
Certified Total Activity ofl 66.5577lµCi Which Equals 1.478E+08ldpm at the date listed above
And after dilution the activity of this solution isl 1.478E+05ldpm/ml This ,1ctivity concontrntion is based on the orininal reference date listed above. Al! activiik•s am con-ect,,d to the date and time of analysis by the laboratory tfatrn procnssinfJ softvvaro.,
Expiration Date: I April 26, 2019
0040
Rev.fl; 11/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDAF?Y IJILUTION RECEFITIFICATION
QCP-009-1-A Date I 5/5/18 I Solution #li-----B-a--6-a---i, Solution Reference# NIST SRM4251C
Principal Radionuclide 133sa I
Radionuclide of Interest 1338a
Half Life, Years
I 1.048E+01 I
Parent Solution Cone. 1.48E+05 dpm/ml
Chemical Composition of Standard Solution
I Half Life, Days
I 3.828E+03I
Reference Date._! ___ 9_/_1/_1_99_3_0_:_oo_,I
Dilution Instructions: Dilution Solvent Used l1M HCI
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
25.0000 ml 3.6950E+06 dpm
1000.00 ml Final Activity Concentration: j 3.6950E+03!dpm/ml
This activity concfN,tratlon is based on the ori1:1inal rofornnce date listed above. Al! activitius are corrected to the date an<l l:irne of analysis by the laboratory data procei,sing software.
Expiration Date:! April 26, 2019 I
Date: ___ 5_/5_/_18 __ _
Date: ·Ji\\({ ---+'\ '+\ __ _
0041
CERTIFICATE OF CALIBRATI :r+sAtQC REVIEWED
Radionuclide:
Half Life:
ALPHA STANDARD SOLUTIO ore g, g
Customer:
P'.O.No.:
TMA EBERLINE
VH1888
Catalog No.:
Source No.:
Ra-226
1600 ± 7 years
7226
453-26
Reference Date: February 1 1994
Contained Radioactivity: (Ra-226) 1.001
Contained Radioactivity: (Ra-226) 37.0
12:00 PST.
µCi.
kBq.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
5.1864 g (in a 5 ml Flame Sealed Ampoule)
Ra(NO3)2 in 1 N HNO3
None added
d. Density: L0318 g/ml @20°C.
Radioimpurities None detected(other than daughters)
Radioactive Daughters Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuclide Concentration
(Ra-226) 0.1929
Method of Calibration
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Branching ratio(s) used: 0.0351 gamma rays per decay.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level;
NIST Traceability
±3.4% ±3.1% ±0.2%
±4.6%
µ.Ci/g,
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source,
Notes
1. Nuclear data wen: uiken from "Table of Radioactive Isotopes", editeo by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to establish and mainuiin implicit traceability for a number of nuclides,
based on the blind assaf (and later NIST certification) iifStimdard Reference Materials {As in NRC Reguliltoi:y Guide 4.15).
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000
QUALITY CONTROL
/iA,. '! /99 If Date Signed
0042
;: E El ER!;-;,~!::!,!', I
' QUALITY CONTROL PROGRAM
MP009
Rev.a; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES· OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATEI 9/20/2017 0:001 SOLUTION REFERENCE# IPL453~26 I SOLUTION#! . :Ra~s. I
Principal Radionuclide Half Life, Years Half Life, Da~s 226Radium I I·· .. 1.600E+03I I s.844E+osl
Radionuclide ~0 Radium Reference Date! • 21111994 o:ool
Certified Activity . .1.001E+O0 µCi Certified Concentration µCi per gram
Ampoule /Solution Gross~Weight, Grams Empty Ampoule · Weight, Grams
Solution Net Weight, Grams Total Activity In Ampoule 1.0010 µCi
Chemical Composition of Standard Solution l~Ra(NO3)z in 1 MHNOa • I
Dilution Instructions: Dilution Solvent Used I1M HN03 . I Dilute to a volume ofl · .1000.00 · !milliliters
Certified Total Activity of! 1.0010jµCi Which Equals I 2.222E+06ldpm at the date listed above
And after dilution the activity of this solution isl 2.222E+03ldpm/ml This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software,
Expiration Date: I September 20, 2018 I
~ ( VerCied & Approved By ~- Date: 9/2012017
~~ I \ _/
QC Approval \. ~~ \. ~ Date: 9/20/2017 - I J -
0043
Rev.a; 11/01103 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP009 Date 9/20/2017 0:00 Solution Reference# IPL~453'-2e Solution # .. Ra:..sb
Princi al Radionuclide Half Life, Years 226Radium I · 1.600E+•3j
Half Life, Days I 5.B44E+osl
Radionuclide of Interest· .. 226Radium Reference Date ... I __ 2/_1_/1_9_94_ .. _o:_o_,o I Parent Solution Cone. 2.22E+03. dpm/ml
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
20.0000 ml 4.4440E+04 dpm
.· 1000.00 ml Final Activity Concentration: I 4.4440E+01 jdpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:! __ 2_0._s_e_p-_1_a _ _.
Date: 9/20/2017 0:00 -------Date: 9/20/2017 0:00
-----..;.;,.,,~____,.;.;.....;;...
0044
1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 • U.S.A.
CERTIFICATE OF CALIBRATION Standard Radionuclide
72325-207 1~ . 2/2-, i5 \ lt
Ra-228 5 mL Liquid in Flame Sealed Vial
Phone (404) 352-8677 Fax ( 404) 352-2837
This standard radionuclide source was prepared
gravimetrically from a calibrated master solution. The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
ACTIVITY (dps):
HALF-LIFE:
CALIBRATION DATE:
RELATIIVE EXPANDED UNCERTAINTY (k=2):
Ra-228
4.022 E3
5.75 years
February 10, 2006 12:00 EST
4.0%
Impurities: y-impurities <0.1%
5.10721 grams 0.lM HCl solution with 50 µg/g Ba carrier.
PO NUMBER 00003181, Item 1
SOURCE PREPARED BY: M. Taskaeva, Radiochemist
QA APPROVED:
0045
~EBER""~~!', I
QUALITY CONTROL PROGRAM MP-009
Rev.a; 1/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS
INITIAL DILUTION MP 009
CURRENT DATE! 2/28/2017 0:00! ~----------. --------1 SOLUTION REFERENCE# Analytics 7235-207 SOLUTION #I Ra-12 I Principal Radionuclide
22sRa I Half Life, Years
I 5. 750E+ool
Radionuclide 228Ra Certified Activity 1.087E-01 µCi
Certified Concentration,__ ___ __,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Chemical Composition of Standard Solution
Half Life, Days I 2.100E+03I
Reference Date ... l __ 2_/1_0_/2_0_06_0_:_oo .... l
9.0741 Weight, Grams 3.9858 Weight, Grams 5.0883 Weight, Grams 0.1087 µCi
Dilution Instructions: Dilution Solvent Used I0.5 M HCI
Dilute to a volume ofj 991.00 \Kg
Certified Total Activity ofl 0.1087lµCi Which Equals I 2.413E+05\dpm at the date listed above
And after dilution the activity of this solution isl 2.435E+02ldpm/ml This activity concentration is based 011 the ori9inal rnfernnce dalH listed abovn, A!! 11ctiv!ties arn conedt,d to Hw date and timn of am1lysis by the h1boratory d<1ta processing softwarn ..
Expiration Date:! February 12, 2019 I
Date: 2/12/18
Date:
I I
0046
QA/QC REVIEWED ANALYTICS
CERTIFICATE OF CALIBRATION Standard Radionuclide Source
52094-416
Am-241 10 mL Liquid in Flame Sealed Vial
1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 · U.S.A.
Phone (404) 352-8677 Fax (404) 352-2837
This standard radionuclide source was prepared gravimetrically from a calibrated master liquid radionuclide solution source. The master source was calibrated by liquid scintillation counting.
ANALYTICS maintains traceability to the National Institute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
ACTIVITY (dps):
HALF-LIFE:
CALIBRATION DATE:
TOTAL ERROR:
Am-241
1.975 E+05
432.2 years
March 19, 1996 12:00 EST
3.0%
SYSTEMATIC ERROR: 2.37%
RANDOM ERROR: 0.63%
10.01177 grams of solution lM HCl.
PO NUMBER OR3830, Item 1
SOURCE PREPARED BY: Beverly,
QA APPROVED: M-~
0047
~ 1;;: a _-=:J:;;!. t.,,.tN .e: I QUALITY c~~-00T9ROL PROGRAM
~ SE:RVICES.
Rev.8; 1/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES" OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION (RE-CERT/FICA TION)
Solution Reference # Anal !cs 52094-416
Half Life, Years I 4.322E+o2j
Date 7/29/2017 0:00 Solution# A/B-7 al ha
Half Life, Days I 1.579E+05 I
Radionuclide of Interest 241Am Reference Date!,_ __ 3_/_19_/1_9_9_6_0_:o_,ol
Parent Solution Cone. 1.19E+04 dpm/ml
Chemlcal Composition of Standard Solution
Dilution Instructions:
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
Dilution Solvent Used j1 M HNO3
SECONDARY VOLUMETRIC DILUTION
60.0000 ml 7.1100E+05 dpm
1000.00 ml Final Activity Concentration:! _ 7.11 OOE+02ldpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:! July 29, 2018
0048
l,,.,,o,~ '!t:.. ·\
\~) ~ational 3Jnstitute of ~tanbarbs & mccbnolog!'
ctertif icatt Standard Reference Material 4234A Strontium-90 Radioactivity Standard
This Standard Reference Material (SRM) consists of radioactive strontium-90 chloride, non-radioactive
strontium chloride, non-radioactive yttrium chloride, and hydrochloric acid dissolved in 5 mL of distilled water.
The solution is contained in a flame-sealed NIST borosilicate-glass ampoule. The SRM is intended for the
calibration of beta-particle counting instruments and for the monitoring of radiochemical procedures.
Radiological Hazard
The SRM ampoule contains strontium-90 with a total activity of approximately 13 MBq. Strontium-90 decays
by beta-particle emission to yttrium-90, which also decays by beta-particle emission. None of the beta particles
escape froni the SRM ampoule. The beta particles emitted from strontium-90 and yttrium-90 produce
bremsstrahlung photons with energies up to 2 MeV. Most of these photons escape from the SRM ampoule
and can represent a radiation hazard. Approximate unshielded dose rates at several distances (as of the
reference time) are given in note [a]*. Appropriate shielding and/or distance should be used to minimize
personnel exposure. The SRM should be used only by persons qualified to handle radioactive material.
Chemical Hazard
The SRM ampoule contains hydrochloric acid (HCl) with a concentration of 1 mole per liter of water. The
solution is corrosive and represents a health hazard if it comes in contact with eyes or skin. If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened only by persons qualified to handle both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 °C. The solution in an unopened
ampoule should remain stable and homogeneous until at least March 2005.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through tbe Standard Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899 May 1995 (Text only revised November 1997)
SRM 4234A. page l of 6
Thomas E. Gills, Chief Standard Reference Materials Program
"'Notes and references are on pages 5 and 6.
0049
~ f;; _ _e_f;::RJ.,.._J_hl E I QUALITY c~c~!:oL PROGRAM ~ SER'VICl:::S ~
Rev. 7; 9/29/99 TiHe: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES· OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION (RE-CERT/FICA TIONJ
QCP-009-1-A Date 7/29/2017 0:00 Solution Reference # NIST 4234A Solution # · A/B-7 beta
Princi al Radionuclide 90Strontium ·
Half Life, Years I · 2.878E+01 !
Half Life, Days I 1.051E+04!
Radionuclide of Interest' 80Sr ·· 1 Parent Solution Cone._· · 1,52E+06 .· dpm/ml
Reference Date! ·. · 3/13i19950:oo!
The beta activity of solution reflects the original oostronijum concentration and an equal concentration of OOVttrium.
Chemical Composition of Standard Solution l90SrCl2 in .1 M HCI · I
Dilution Instructions:
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
·· 0'.5000 ml 7.5764E+05 dpm
· 1000;00 ml Final Activity Concentration: I 7 .5764E+02 ! dpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:I July 29, 2018
Date: 07/29/17 _____ ;__,;..;... __ Date: __ ~..,../ 1-+{.._11--
I
0051
Eberline Analytical Analysis Control Chart
• 18-06097
Analyte
U-234
U-238
Analyte
Analyte
U-234
U-238
U-235
Version
Nonnalized Difference
Analysis
UUISO
LCS Measured
86.16%
90.66%
MS Actual %Rec
I I
CSU Measured
14.34%
14.27%
Expected MS Result
I
i
i
I
Duplicate Results
Nonnalized Original I Difference
RPD Result
0.70 30.91 1.88E-01 I
1.69 78.13 1.22E-01
1.63 152.02 1.68E-02
Printed: 7/10/2018 12:23 PM Page 1 of 2
Run Activity Units Aliquot Units __ ___, ____________ Client Name
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncert
Original CSU
1.19E-01
9.21E-02
4.03E-02
I
Uncert.
I Expected
Known
3.60% 7.32E+00 I
3.60% 7.09E+00 [
Matrix Spike
Actual MS Result
Duplicate Result
2.57E-01
2.79E-01
1.23E-01
Actual MS CSU
Duplicate CSU
1.52E-01
1.56E-01
1.21 E-01
Known Error
2.64E-01
2.SSE-01
Sample Result
LCS Relative
Bias
0.86
0.91
AMO Environmental Decisions
Result CSU
6.31E+00 9.0SE-01 I
1 6.43E+00 I 9.18E-01
Sample CSU
Sample Aliquot
Standard ID
U-8a
U-Sa
Standard ID
Standard
ACT(dpm)
3.20E+01
3.10E+01
Standard ACT(dpm)
QC Summary
LCS¾R I
MS¾R I
MSND
OK I
OK ! i
OK I
I
I
Standard Error
3.60E+00
3.60E+00
Standard Error%
I
Standard Added (g}
15.08E-01
I
[ 5.08E-01
Standard Added (g)
RepRPD I Rep ND
NA I OK
NA OK
NA OK
0052
Eberline Analytical Analysis Control Chart
• 0
18-06097
130.00
120.00
110.00
100.00
90.00
80.00
I~-·- Analysis Run
UUISO 1
LCS % Recovery
T - - - _I I I • t I , . --------- l
Activity Unit_s Aliquot Units
pCi
40.00
35.00
30.00
25.00
20.00
15.00
10.00
i
Printed: 7/10/2018 12:23 PM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPD
,--------------
i 70.00 +----------"--------~----------------~
U-234 U-238 5.00
- Lower Error 68.22 72.79
- Upper Error 104.11 108.53
• %R 86.16 90.66
- -LCL 75 75
--Mean 100 100
1- -UCL 125 125
0.00 +-------------~-----------~---------
- LowerError
- UpperError
• RPO
- -CL
U-234 U-238 U-235 ~ 40.32 102.33
I 239.84
21.51 53.94 64.20
30.91 78.13 152.02
35 35 I 35
Normalized Difference
3.50 No Matrix Spike
3.00
2.50
2.00
1.50
1.00
0.50
0.00 LCS ND MSND
-u-2341 0.00
~U-2381 000
0.00
1.69
0.00
0.00
000
0.00
-UCL I 3 3 3
Version
0053
Eberline Analytical Analysis Control Chart
WO
18-06097
Analyte
TH-228
TH-230
TH-232
Analyte
Analyte
TH-228
TH-230
TH-232
Version
Analy,s_is
ThlSO
LCS CSU Measured Measured
119.46% 22.52%
122.48% 23.47%
118.34% 22.29%
Nonna/ized MS Actual Expected Difference %Rec MS Result
Duplicate Results
I Nonna/ized RPD Original
Difference Result
1.35 186.84 5.66E-02
0.33 14.85 1.73E-01
0.29 42.23 1.90E-02
Run Activity Units~ ,:'l_iguot Units
1 pCi I
Laboratory Control Sample
LCS Uncert. Known
Known Result
Expected Expected Error
100.00% 3.60% 4.87E+00 1
1.75E-01 5.82E+00 ..
'
100.00% 2.70% 5.38E+00 i 1.45E-01 6.59E+00
100.00% 3.60% 4.87E+00 ! 1.75E-01 5.76E+00 I
Matrix Spike
Expected Actual Actual Sample Sample
MS Uncert MS Result MS CSU Result CSU
Original Duplicate Duplicate LCS Relative I LCS¾R CSU Result CSU Bias
7.47E-02 1.92E-03 2.69E-02 1.19 OK
1.10E-01 1.49E-01 9.07E-02 1.22 OK
5.21E-02 2.92E-02 4.38E-02 1.18 OK
Printed: 7/10/2018 12:14 PM Page 1 of 2
Client Name
AMO Environmental Decisions
CSU Standard Standard Standard Standard
ID ACT(dpm) Error Added (g) I
1.31E+00 Th-Sb I 1.04E+02 3.60E+00 1.04E-01
1.55E+00 Th-1b 2.35E+01 2.70E+00 5.0BE-01
1.28E+00 Th-Sb 1.04E+02 i 3.60E+00 1.04E-01
I
I Sample Standard
I Standard
I Standard Standard
Aliquot ID ACT(dpm) Error% Added (g)
QC Summary
I I MS¾R I MSND I RepRPD I Rep ND
NA I OK
NA OK
i I NA OK
0054
Eberline Analytical Analysis Control Chart
WO
18-06097 Analysis Run
ThlSO 1
LCS % Recovery i..::,v.uv
r------r------t-120.00
110.00
100.00
- l l 90.00
80.00
--------------- LCL
70.00 TH-228 I TH-230 TH-232
- Lower Error 93.34 I 96.30 92.45
- Upper Error 145.58 I 148.65 144.22
• o/oR 119.46 I 122.48 118.34
- -LCL 75 ' 75 75
--Mean 100 I 100 100
[--UCL 125 125 125
Normalized Difference
3.50 1 --------------------------
3.00 +--------------------------------2.50 -1--------------------------------
2.00 +---------------------------------
1.50 -j----------------------------------
1.00 -1--------------
0.50 +--------------
0.00 LCS ND MS ND
-TH-2281 0.00 1.35 0.00
=rH-230I 0.00 0.33 0.00
- UCL 3 3 3
Version
ActiVi!Y Units
pCi
-+U.UU
35.00
30.00
25.00
20.00
15.00
10.00
I 5.00
I 0.00 .
I - Lower Error
I I
- Upper Error_
• RPD
- -CL
Ali_guot Units
Printed: 7/10/2018 12:14 PM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPD
~--------------1
T I
TH-228 I TH-230 I TH-232
349.09 19.49 I 84.27
24.58 ! 10.22 I 0.20
186.84 I 14.85 i 42.23
35 ! 35 I 35
No Matrix Spike
I I I I I
0055
Eberline Analytical Analysis Control Chart
• 18-06097
Analyte
RA-226
Analyte
Analyte
RA-226
Version
Nonnalized Difference
Analysis
Ra226
LCS Measured
100.62%
MS Actual %Rec
I
CSU Measured
25.16%
Expected MS Result
Duplicate Results
Nonnalized Original
Difference RPD
Result
1.45 115.42 1.02E-01
i
Run Activity Units Aliquot "LJnits
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
Expected MS Uncert
Original CSU
2.14E-01
Uncert. Known
Expected
4.60% I 1.00E+01 I
Matrix Spike
Actual MS Result
Duplicate Result
3.81 E-01
Actual MS CSU
Duplicate CSU
3.09E-01
I
Known Error
4.60E-01
Sample Result
I !
LCS Relative I Bias
1.01 I
Result
1.01 E+01
Sample CSU
LCS¾R
OK
I
I
I
Printed: 7/10/2018 7:19 AM Page 1 of 2
Client Name
AMO Environmental Decisions
CSU
2.53E+00 I
Sample Aliquot
Standard ID
Ra-Sb
Standard ID
Standard
ACT(dpm)
I 4.40E+01
Standard ACT(dpm)
QC Summary
I I
MS¾R MSND
i
I I I
Standard Error
4.60E+00
Standard Error%
RepRPD
NA
I
I
Standard Added (g)
5.0SE-01
Standard Added(g)
Rep ND
OK
0056
Eberline Analytical Analysis Control Chart
WO Analysis Run Activity Units
18-06097 Ra226 1
LCS % Recovery 13000
1 120 00 t
110.00
100.00 •
90.00 I
8000 t I
l 70.00 :
RA-226
Lower Error I 70.86
- Upper Error, 130.38
• %R 100.62
- -LCL 75
--Mean 100
- -UCL 125
Normalized Difference
3.50 ,-----------------------------------
3.00 r---------------------------------2.50 +-------------------------------
2.00 +---------------------------------
1.50 t----------------===----------------
1.00 +--------------
0.50 +--------------
0.00 LCS ND
-RA-226 0.00
- UCL 3
Version
MSND
1.45 0.00
3 3
pCi
--•
40001
35 00
30 00
25 00
20 00
15 00
10 00
5 00
ooo I
Lower Error\
Upper Error I RPD I
- -CL I
Aliguot Units
Printed: 7/10/2018 7:19 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPO
RA-226
178.00
52.85
115.42
35
No Matrix Spike
0057
Eberline Analytical Analysis Control Chart
WO
18-06097
Analyte
RA-228
Analyte
Analyte
RA-228
Version
Analysis Run Activity Units Aliquot Units
Ra228 1 pCi
Laboratory Control Sample
Normalized Difference
LCS Measured
93.82%
MS Actual %Rec
CSU LCS Measured Expected
24.26% I 100.00%
Expected Expected MS Result MS Uncert
Duplicate Results
Normalized RPD
Original Original
Difference Result CSU
2.29 166.75 7.89E-02 4.12E-01
i
Uncert. Known
Expected
5.10% I 9.20E+00
Matrix Spike
Actual MS Result
Duplicate Result
8.70E-01
Actual MS CSU
Duplicate CSU
5.37E-01
I
Known Error
4.69E-01
Sample Result
LCS Relative I Bias
0.94
Result
8.63E+00
Sample CSU
LCS¾R
OK
Printed: 7/11/2018 7:35 AM Page 1 of 2
Client Nam_e ----------1
AMO Environmental Decisions
CSU I I
2.09E+00 I
Sample Aliquot
Standard
ID
Ra-12
Standard ID
Standard ACT(dpm)
I 5.46E+01
Standard ACT(dpm)
QC Summary
MS¾R MSND i
Standard Error
5.10E+00
Standard Error%
RepRPD
NA I
Standard Added (g)
3.75E-01
Standard Added(g)
Rep ND
OK
0058
Eberline Analytical Analysis Control Chart
• A..a~ysis Run
18-06097
130.00
120,00
110.00
100.00
90.00
80.00
70.00 1 I - Lower Error I : - ,_,e.o, I -I • %K
I - -LCL
,--Mean I I- -UCL
Ra228 1
LCS % Recovery
RA-228
64.46
123.18
93.82
75
100
125
Normalized Difference
3.50 ---------------------------------
3.00 +-----------------~---------------2.50 +--------------------------------
2.00 +--------------
1.50 1 ------------
1.00 +--------------
0.50 ,------------:
0.00 , LCS ND MSND
-RA-228I o.oo 2.29 0.00
- UCL 3 3 3
Version
A_ctivit,'_LJnits Aliquot Units
pCi
40 00
35.00
30.00
25.00
20 DO
15.00
10.00
5.00
Printed: 7/11/2018 7:35 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPD
000 +---------------------------------------I RA-228
[--=-_L,ow_er Errori
i l - Upper Error
• RPD --CL
I 250.09 ----i 83.41
I 166.75
35
No Matrix Spike
0059
Eberline Analytical Analysis Control Chart
WO
18-06097
Analyte
GROSS ALPHA_TH
GROSS BETA_SR
Analyte
Analyte
GROSS ALPHA_TH
GROSS BETA_SR
Version
Analysis Run Activity_ Units Aliquot Units
GaGbT ThSr
NonnaJized Difference
LCS Measured
109.59%
94.38%
MS Actual %Rec
CSU Measured
11.00%
13.86%
Expected MS Result
Duplicate Results
i
1 pCi
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncert
Uncert. Known
Known
Expected Error
4.30% 2.71E+02 1.16E+01
3.00% 2.77E+02 8.32E+00
Matrix Spike
Actual I Actual Sample MS Result [ MS CSU Result
I I Normalized Original
I Original Duplicate Duplicate LCS Relative I
RPD Difference Result CSU Result CSU Bias :
i I
2.48E+00 I 3.12E+00 , 7.82E+00 I 1.96 103.70 4.33E+00 1.10
2.21 118.66 i 1.14E+01 I 5.37E+00 I 2.91E+00 I 5.27E+00 I 0.94 I
Result
2.97E+02
2.62E+02
Sample CSU
LCS¾R
OK
OK I
Printed: 7/11/2018 9:52 AM Page 1 of 2
Client Name,___ ___________ -t
AMO Environmental Decisions
CSU
3.26E+01
3.63E+01
Sample Aliquot
Standard ID
A/B-07
A/B-07
Standard ID
Standard ACT (dpm)
5.93E+02
6.08E+02
Standard ACT(dpm)
QC Summary
I
I
MS¾R I MSND I
I
I I
I I
I I
I
Standard Error
4.30E+00
3.00E+00
Standard Error%
RepRPD
NA
NA
I
I
I
Standard Added (g)
1.01E+00
1.01E+00
Standard Added (g)
Rep ND
OK
OK
0060
Eberline Analytical Analysis Control Chart
• 18-06097
130.00
120.00
110.00
100.00
90.00
'
Analysis
GaGbT ThSr
LCS % Recovery
• i
•
Run Activity _!,!_nits Aliquot Units
1 pCi
:::: I 30.00
25.00
20.00 +
15.00
10.00
Printed: 7/11/2018 9:52 AM Page 2 of 2
Client Name
AMO Environmental Decisions
Replicate Sample RPD
=-1' ----------~ ?o.oo +.------G-R_O_S_S_A_L_P_H_A_T_H·-----~------G-R_O_S_S_B_E_T_A_S_R-----~
- 5.00
- Lower Errorj 94.30 i 77.52 ' - Upper Error I 124.89 I 111.24 000 ~. -------------------------------~
GROSS ALPHA TH GROSS BETA SR ~
• ¾R I 109.59 I 94.38 - Lower Error 141.15 162.78
- -LCL I 75 I 75
--Mean I 100 I 100 - Upper Error
I • RPO
66.25 74.55
103.70 118.66
- -UCL I 125 I 125 [--CL 35 35
Normalized Difference 3.50
3.00 No Matrix Spike
2.50
2.00
1.50
1.00
0.50
0 00 LCSND I REP ND ! MSND
- GROSS ALPHA TH 0.00 I 1.96 I 0.00
= GROSS BETA SR 0.00 l 2.21 I 0.00
= 0.00 i 0.00 I 0.00
- UCL 3 I 3 I 3
Version
0063
Printed: 7/6/2018 9:39 AM
~EEIERb~~!;i Work Order Analysis Notes
# Date Dept User
1 07/06/18 09:39 PREP JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridae, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-06097 UUISO
1
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
0064
Printed: 7/9/2018 3:57 PM
4: ~ E El I::: R ~-},J16 ~ Work Order Analysis Notes
# Date Dept User
07 /06/18 09: 39 PREP JHARVEY
2 07 /09/18 15:57 CHEM JDEMELAS
Page 1 of 1
Oak Ridge Laboratory Internal Worl< Order 18-06097 601 Scarboro Rd. -~-· Oak Ridge, TN 37830 Analysis Code UUISO Voice: 865.481.0683 ·-•·"·-~-----·- --· ·-----· www.eberlineservices.com Run Number 1
Notes
AUQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
----·-
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH4I, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in ~10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H2O. Set samples asideJQc.Jsl!J3J:precipitation and filtering. -------~---·~ . ······--·· .,
0065
Printed: 7/10/2018 4:37 AM
~EBER~~!;':lc!;;; Work Order Analysis Notes
# Date Dept User
1 07/06/18 09:39 PREP JHARVEY
2 07 /09/18 15:57 CHEM JDEMELAS
3 07/10/18 04:37 CHEM TSMITH
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-06097 Analysis Code UUISO
---··-····-··----+---------·-··················--11
Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH4I, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in ~1 O ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.
Followed steps 12.1.7 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Uranium)
0066
Eberline Analytical Oak Ridge Laboratory
•=A•-.---~•~''-"'~,~----•••M•o<,•••~ >
. . -~ ~ EBERLINE ~--------------------- -------------- --------SERv1c-Es
Reagents Used in an Analysis
Reagent Reagent
ID Name ""-•"•--w==
017344P Anion Exchange Resin - ---· -· ·--·-·-···"·· ·~···-···-·····,---·······~--·---
019999D02 Hydrochloric Acid ,.
020076S Hydrochloric Acid ,___ ~--·-·-·----~
020137S Hydrochloric Acid , ··--···-··-·-· ·~---~-··'"·
020155S HCI - NH4I ···-•~- --•~N,
020123S HCI - HF """~-·
019999P Hydrochloric Acid -M•- ..
020099S Carbon substrate - ····~····----·--•>••·
020095P Hydrofluoric Acid
019640S Neodymium Carrier ,. ........ -········"········~---·-···- ... -~···
019771P Reagent Alcohol
I 019956P Titanous Chloride 0 M• ••- -•• ••••• •-••••-~• ~ ••-'""-"•W••• •-• ••• ···-····· ··- ·~-····-···
Printed: 7/10/2018 4:40 AM Page 1 of 1
-··
Internal Work Order ~~--~,-
18-06097 Analysis Code Run
UUISO 1 --
Reagent Analyst Date
Concentration ID Recorded
Reagent Grade JDEMELAS 7/9/2018 ··-···--·---
O.SN JDEMELAS 7/9/2018 .. ·-
6.SN JDEMELAS 7/9/2018
SN JDEMELAS 7/9/2018
SN - O.lM JDEMELAS 7/9/2018
6.SN - 0.04N JDEMELAS 7/9/2018
Reagent Grade JDEMELAS 7/9/2018
Solution TSMITH 7/10/2018 ~---··-~-
Reagent Grade TSMITH 7/10/2018
1 mg/ml TSMITH 7/10/2018 -
Reagent Grade TSMITH 7/10/2018
Reagent Grade TSMITH 7/10/2018 -·-----·-· ~•••m
0067
-~ 109
_ ____,,\ c-G_e1~iu11e ~n u~1:±utie-'-A:na1¥>-t> TedJ-~.
~~~~~ '----1---~~~-__. =-+---"--'---"--'--v-+--U_Um ~ -.
1----------------t------
-j-------t-------------~------+--~ ------11-~--~1---·--->;
0069
Printed: 7/6/2018 9:39 AM
~EBERLINE ~ SERVICES
Work Order Analysis Notes
# Date Dept I User !
1 07/06/18 09:39 PREP
I JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridae, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-06097 >---------+-----·------·-~'·---·-
Analysis Code Th ISO 1--------+---------------··~--
Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
0070
Printed: 7/9/2018 3:58 PM Page 1 of 1
~ Oak Ridge Laboratory Internal Work Order 18-06097 601 Scarboro Rd. ~------·--- ··~---·-·-.. ~"¥---····-· -~--··"~-·-·· -~-----·-EBER~~~c~ Oak Ridge, TN 37830 Analysis Code ThlSO
Work Order Analysis Notes Voice: 865.481.0683 ·•-"··-·
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 07/06/18 09:39 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS
2 07/09/18 15:58 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in ~1 O ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinoinn vnl11me to ~15ml. SAi ,s,amnles recioitation and filterina.
0071
Printed: 7/10/2018 4:39 AM Page 1 of 1
~ Oak Ridge Laboratory Internal Work Order 18-06097 601 Scarboro Rd. EBER~~tt~ Oak Ridge, TN 37830 Analysis Code ThlSO Voice: 865.481.0683
Work Order Analysis Notes ------- ~~····· ·-··•~~-- --·~------- ··•-.-.,-----· www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 07/06/18 09:39 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN AND SUBMITTED
SAMPLES TO SEPARATIONS -·
2 07/09/18 15:58 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in ~1 0 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
___ ,_ water, brin~g volume to ~15ml. Set sameles aside for later erecieitation and filterino. ···-·3-·
07/10/18 04:39 CHEM TSMITH Followed steps 12.2.5 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Thorium)
0072
...
Eberline Analytical Oak Ridge Laboratory
'~"~-·---=--•--·-~----,-·
. . ·~ ..
Q_ EBERLINE ~ ----- --------------------------------------- SERv-icEs
Reagents Used in an Analysis .....
Reagent Reagent ID Name .
017344P Anion Exchange Resin Y•~••••-••-• ··• ---- ··--··---,
020137S Hydrochloric Acid r·······
019999P Hydrochloric Acid f· • ee••~s,••••-••-" •
020000P Nitric Acid , ..• .. .... ~-~"'-' . .. ··-·- ···~·-·. --~--,--~--·-·· ---·-····· ------~···--··~.,---.
020146S Nitric Acid f· --· --······---···--------···-·--
020099S Carbon substrate --·····-·~·--·-·
019812S Cerrium Carrier
020095P Hydrofluoric Acid "-·--•-_, .. ,_,,, .. ~~ ------~----·-···--·- ..
019771P Reagent Alcohol ··•··•······ ··••·······•••
Printed: 7/10/2018 4:40 AM Page 1 of 1
Internal Work Order --
18-06097 ---~,_,
Analysis Code Run ..
ThISO 1
Reagent Analyst Date
Concentration ID Recorded
Reagent Grade JDEMELAS 7/9/2018 •<••·-
SN JDEMELAS 7/9/2018
Reagent Grade JDEMELAS 7/9/2018
Reagent Grade JDEMELAS 7/9/2018 -~-·····
SN JDEMELAS 7/9/2018 ·---~-- ---- ---- " .... ----~---···-·---···- ,_ ___
Solution TSMITH 7/10/2018
0.lmg/ml TSMITH 7/10/2018
Reagent Grade TSMITH 7/10/2018 ----
Reagent Grade TSMITH 7/10/2018 ~------
0075
Printed: 7/6/2018 10:00 AM
<(EBER~~~c!;'i Work Order Analysis Notes
# Date Dept User
1 07/06/18 10:00 PREP JHARVEY
Oak Ridge Laboratory 601 Scarboro Rd. Oak RidCle, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-06097 Analysis Code Ra226
1---------+------------- ... Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PREr'IP TO C:,t=PIIPIITIONS
0076
Printed: 7/9/2018 1:49 PM
~EBER !;;,~!;;IC!;;; Work Order Analysis Notes
# Date Dept User
1 07/06/18 10:00 PREP JHARVEY
2 07/09/18 13:49 CHEM JBAILEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-06097 Ra226
1
AUQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS ADDED EDTA TO SAMPLES AND LET SIT. ADDED AMMONIUM SULFATE AND ACETIC ACID TO
SAMPLES. FILTERED ONTO TARED FILTER PAPERS, LET DRY UNDER HEAT LAMP, REWEIGHED,
AND SUBMITTED TO COUNT.
0077
·-
Eberline Analytical Oak Ridge Laboratory
}!Jl;:BERLINE ~ SERVICES
Reagents Used in an Analysis
Reagent Reagent ID Name
019782P Ammonium Hydroxide
019733D05 Ammonium Sulfate
019792D04 Barium Carrier
019767D01 Lead Carrier
019846P Nitric Acid
019210P Acetic Acid
019733D02 Ammonium Sulfate
0199465 EDTA
Reagent
Printed: 7/9/2018 2:36 PM Page 1 of 1
Internal Work Order
18-06097 Analysis Code Run
Ra226 1 Analyst Date
Concentration ID Recorded
Reagent Grade JHARVEY 7/6/2018
200 mg/ml JHARVEY 7/6/2018
1 mg/ml JHARVEY 7/6/2018
166 mg/ml JHARVEY 7/6/2018
Reagent Grade JHARVEY 7/6/2018
Reagent Grade JBAILEY 7/9/2018
200 mg/ml ]BAILEY 7/9/2018
0.25M JBAILEY 7/9/2018
0078
~. 109
-" . 1+~ · · ~J]1_e__C_oufl:l:±1Una lyS,5 . Teel;_. _ ___ u::!:Q ,r l.llim j:&_ __
p.-{ \ k,/ Vv tJ \ ·-.µ; .
----------+---------1----1------+----~--
l
j -------+-----
_,/ '-------l'--------1--------+-----+-------li---------t----·.1
~------~------l-------t-----4-----1-------1----
0080
Printed: 7/6/2018 10:00 AM
4: EBER ~·R~C!'; Work Order Analysis Notes
# Date Dept User
1 07/06/18 10:00 PREP JHARVEY
Oak Ridge Laboratory 601 Scarboro Rd. Oak Ridqe, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-06097 Analysis Code Ra228
---.~----Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
0081
Printed: 7/10/2018 2:37 PM
,:E:BER!ret~c~ Work Order Analysis Notes
I # Date Dept User
1 07/06/18 10:00 PREP JHARVEY
2 07/10/18 14:37 CHEM JBAILEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridge, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-06097 1---·-------+--------·------··-----11
Analysis Code Ra228 -··""•·~---·~·-------·t----------·-·-·'"·············--·······
Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS ADDED FILTER PAPERS FROM COUNT ROOM TO LABELED C-TUBES, FILLED WITH EDTA SOLUTION
AND LET SIT OVERNIGHT. REMOVED FILTER FROM EDTA-ADDED 2MLS YTTRIUM 9MG/ML CARRIER
ADDED 18N NAOH TO SAMPLES AND RECORDED T1. HOT BATHED FOR 15 MIN, CENTRIFUGED AND
DISCARDED SUPERNANT. ADDED 6N HNO3, DI WATER, AND 10N NAOH. HOT BATHED FOR 15 MIN,
CENTRIFUGED AND DISCARDED SUPERNANT. ADDED 1N HNO3, DI WATER, AND AMMONIUM
OXALATE. FILTERED ONTO TARED FILTER PAPERS. LET DRY UNDER HEAT LAMP, REWEIGHED AND
SUBMITTED TO COUNT.
0082
Eberline Analytical Oak Ridge Laboratory
-~ . . Q EBERLINE ~ ·· ········· -·································•···· s·ERv1·c-Es
Reagents Used in an Analysis ---~~ -"~~-·"~
Reagent Reagent ID Name
019782P Ammonium Hydroxide -·
019733D05 Ammonium Sulfate "W•----•
019792D04 Barium Carrier
019767D01 Lead Carrier ---
019846P Nitric Acid , .... 018297D01 Ammonium Oxalate
- -------018971D06 Nitric Acid
019673D02 Nitric Acid
018699D10 Sodium Hydroxide -·---·~-.,
019344D01 Sodium Hydroxide -·--·-·
019519S Yttrium Carrier
-·-·~
Printed: 7/10/2018 2:37 PM Page 1 of 1
Internal Work Order
18-06097 Analysis Code Run
Ra228 1 Reagent Analyst Date
Concentration ID Recorded
Reagent Grade JHARVEY 7/6/2018
200 mg/ml JHARVEY 7/6/2018
1 mg/ml JHARVEY 7/6/2018
166 mg/ml JHARVEY 7/6/2018 ,,.-·,--~·-- ---
Reagent Grade JHARVEY 7/6/2018 -• 'A•-•
5% JBAILEY 7/10/2018
lN ]BAILEY 7/10/2018
6N JBAILEY 7/10/2018 -~--.. -~
l0M JBAILEY 7/10/2018
18M JBAILEY 7/10/2018
9 mg/ml JBAILEY 7/10/2018 ··-
0083
/ ; -A90c, Lr-:}-1 \lO - ' ------- 55 1··
---f'1l~•'I- i~t'~~~Cti<l _c~0 Le ~~Me~~~~ ·T~h,:: · -~i~JoL,~ lioL,c"ct i,,A li· '-1,} .. A.Mo_+-----'-'~ d I,_.., ~_i_ \0-: I ---+-·---m---------1--- .----J-----~----1-- ,:i 1 .. t
',
-~;---~-~-=---=--=--=--=--=--=---· . ___ , __ _,__ ___ ----',________ :: t ---L--·-T ~ 1---------t----,,s; t r , ---J---.. -·- __ _._, .. ,-~,.-, ,1 r ~-i --r---- --:-- f L I --1 -·--------------+--------1---------t------l-----> I
. I --------,~--.. ~I --------;-------+-----t---------+-----4-------.; i
--~---__ .,_ ______ l--------+-----------4---------
-·-~-.. ----.. -·!---------+----~
I -----l--~--·•--------+---------.+- ' --~t-·-·---.. ··J--
:: --·-~·-----··-·--··~ -----·-·------+------->--------->----
' ----t-----·---·1'-------·---·-----··------·-·-~ --------···-··-----'I------·---·----·-~-
- .. ___ ---.. ------1------------------------J------------>---------<----..___
____ __,t--------
. ____ t---------------t------+-----+--------·---~- --------·•- .. -----~·1-------"'
-~~------------------+------------+----------" _______ }·-----------------------4------------1
0085
Printed: 7/10/2018 11:49 AM Page 1 of 1
4: Oak Ridge Laboratory Internal Work Order 18-06097 601 Scarboro Rd. nwm • •, ~'""•••~•m•m ,,, • •
J::::.l::IER.~t~c~ Oak Ridge, TN 37830 Analysis Code GaGbT ThSr Voice: 865.481.0683
Work Order Analysis Notes =--~
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 07/10/18 11:49 PREP JPACHELLA Samples were aliquoted, nitrated and dried. Samples were transferred to tared planchetes, flamed, re-
weighed, and submitted to count room .
(_ " ..,,"J -~ .,.---· ·.-~·· C;;'G
0086
Eberline Analytical Oak Ridge Laboratory
. e: e I;; R ~l~c ~
Reagents Used in an Analysis
Reagent ID
019074D01
019673P ······················-··------
Nitric Acid
Nitric Acid
Reagent Name
3N
Printed: 7/10/2018 1:15 PM Page 1 of 1
Internal Work Order
18-06097 Analysis Code
GaGbT_ThSr Reagent
Concentration Analyst
ID
JPACHELLA
Run
1 Date
Recorded
7/10/2018
Reagent Grade JPACHELLA 7/10/2018
0089
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Work Order 18-06097 Analysis Code l UUISO I
Run 1 Date Received 6/21/2018
Lab Deadline 7/11/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 908.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer U-232
Radiometric Sol# U-10a
Tracer Act (dpm/g) 18.16
Carrier
Carrier Cone (mg/ml)
Internal Sample I Fraction Desc
i
01 LCS
02 MBL
03 DUP
04 DO
~
18-06097 UUISO Run 1
Client ID
LCS
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I
I Login CPM
I 30
!
30
i
Printed: 7/10/2018 4:40 AM Page 1 of 3
I
Sample Sample Date Aliquot
06/21/18 00:00 1.0000E+00
06/21 /18 00:00 1.0000E+00
06/20/18 10:00 1.0000E+00
06/20/18 10:00 1.0000E+00
0090
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal Sample Tracer Fraction Desc Aliquot (g)
01 LCS 1.1051
02 MBL 1.1017
03 DUP 1.0974
04 DO 1.1022
Tracer Total Radiometric Radiometric ACT(dpm) Tracer (pCi) %Rec
20.1 0.00
20.0 0.00
19.9 0.00
20.0 0.00
I
18-06097 UUISO Run 1
Grav Carrier I Grav Filter Added(ml) Tare (g) I
Grav Filter Final (g)
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
' Grav Filter Grav
Net(g) %Rec
i
i
I
Printed: 7/10/2018 4:40 AM Page 2 of 3
I Mean SAF SAF %Rec 1* 2*
0091
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal I Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep I
Date I
Rough Prep ! Prep
By I
Date
I
07 /06/18 07:29
07 /06/18 07:29
07/06/18 07:29
07/06/18 07:29
18-06097 UUISO Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
Sep to Date/Time
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. h Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep tO By
Printed: 711012018 4:40 AM Page 3 of 3
Sep t1 Sep t1
Date/Time By
0092
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1 Printed: 7/10/2018 12:23 PM
Page 1 of 3
~ i::: ::, ~ a:
Cl) 0 b 0 u en -~ -U)
~ ::, ca i::: ::, <(
... -e 0
t: ~ ii <>
i ca C: <( ., .E ;:: ., t3 -~
II) C:
.2
.!!? (.) Q)
Cl ns ....
II C: Q)
E C: 0 ... ·s;: C: w 0 ~ <(
Lab Fraction --01 -----·
02 ------·
I· ~: I
1-~~.
Nuclide Sample
Desc
Client Identification
Activity Units
Results Error Estimate l MDA LCS
Known LCS ¾R
U-234
U-234
LCS
MBL
LCS
BLANK . .. ... . ~:: .. ;::;1 :~:~ .:::~:1 732E•:J:16
U-234 DUP OU-1-007 Outfall 007 DIS pCi/1 2.57E-01 I 1.50E-01 I 1.32E-01
-·--·--------····--1----··--··· ------+··--··-- ·· · I-···-···
U-234 DO OU-1-007 Outfall 007 DIS pCi/1 1.88E-01 I 1.1 SE-01 I 1.17E-01
----l ---------•---··-- - ----- ------·----t--··--~--
--··-····-·l---·---·---1---- ·
LCS Flag
OK
I
RPD Flag
NA
MDA Flag
OK
OK
OK
OK
Blank Flag
OK
--------·-+---··--···-+·--· -+-·--····---··--· +----- ------1-------1----1--· --+-----1--------j -----------l
- ---+---- -----j- I·-···- - ---- ···-·····----··----- ···l··-···---·----·-I··--···-···
·-----··--···t------ t---------·-1-·------j
····-----·-···--·--·-f-··-·-·-1·-·--
---··--···-l·------1----·-· ----i-------- -• ... --•·- 1------·····--·-·+··-·-··--·---· ···I-- ---+-- i -----1 ----+------+------!
1·---·-··-·····-1 ····--··---- ··--··--------+-----1---· ---···---·
0093
Eberline Analytical
Oak Ridge Laboratory
( 11 .. ~o• r:I 01 02
i::
& I 03
Nuclide
U-234
U-234
U-234 ~
04 QI 0 "0 0 en 0 ,!!! -
U-234
i ::, (IJ
::, i:: <(
'-
~ 0 ~
~ ai
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1
, Sample I Sample
I Sample Radiometric Grav Mean
SAF
Desc Date Aliquot % Rec %Rec %Rec
LC$ I 06/21/18 00:00 I 1.00E+00: 117.30 0.00 0.00
MBL I ::::::: :::: I ::::::1 116.21 o.oof o.oo
------···-·------- --------- ·---·---·-
i DUP 84.64 0.00 0.00
... -----+
DO I 06/20/18 10:00 1.ooE+oo[ 11~:3}J o.ool o.oo .. ----··- -----------·----·--------+--- --------~-
-+---------1 --- ----------------------- +------------ ----1--- --·--+-· -··. --~-·- e------ -----!-"'""
----+------- - --(-------------------+------- --------+----- -- ---- +
-+---------1---------------------- ------+-- ----------+- --- --
Printed: 7/10/2018 12:23 PM Page 2 of 3
SeptO
I Sept1
Date/Time Date/Time
1 .. - ---i----- ----- --1 -------------- ----------------- ----"-------- --------f-- ---- - f-------------1------------+---------+----------+---------
C: <( ., .!: .:: 1------j----------------- ------+------------1------ ------------
., .Q
~~ U) C: 0 -------------- -.,._
-- ------r------ -- ---------------1- ------------------1--- ----------------t-------------1--- ----------+----------,
U)
·c::; Q)
1----------1---------------------- - --+-------!-- -------------- ------- ----------- --+---------j--- -------------- ---------1-----
Cl iii
--- -+----- -------1---- ------ ---i--------1----------- --- ---------- 1---- -----f-----------------------"-
-~I C: Q)
E C: 0 ... ·s;: C: w 0 ~ ~
0094
Eberline Analytical
Oak Ridge Laboratory
~ Lab i
Nuclide Fraction I
01 I U-234
§ a:
.g 0 0 .r!,!
1 <ii C: C(
~
0 u, -::::, ::::,
02
03 ---- . -----
04 ---
------ - ---- --·-·-
----·-- ·------·---
--·----
U-234 ------------·--
U-234 --- -----
U-234
-------· ·-- -------- ----
------ ·------- -----····-------· -·--
----
Sample Desc
LCS ---··-~----
MBL --·------
DUP
DO
------
·---------
--·--~-
---~-·---~ ----- --~·----
---
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1
Counting
i Halflife Count I 8kg
Detect Carrier Counts
Date/Time (days) Time i CPM
07/10/18 08:08 A_Spec Alpha_047i 170 ! 4.86 E+02 5.00 E-03 I
------·----··· -------·· -·------. -------------------- -------·-···---- .r-
170-16.64 E+00 07/10/18 08:08 A_Spec Alpha_048i 8.00 E-03
·------------ -- --- --- ----·--- -- " ---- _L l 1-----------~---I
110[1.28 E+01 07/10/18 08:08 A_Spec Alpha_049 7.00 E-03
-- ·---~-- ·-·-------- ·- ·-------- 1
07/10/18 08:08 A_Spec Alpha_050 17011.15 E+01 9.00 E-03
" - -- ----------·------··--
I ---·---····-·"·- - ------·--------- -··- ···-- ---·------------- -···- --·- -1-----
i
---- ---- -1--·---- --------·------ I --- -1 ----·-----·-----
!
·--··----·-----·. - -- ------------·---- --- --I - ---+
~---------- ··--------···-----·--···- -· ----··--·---------------··· ·---·-··-·· -------- - ' -- -!------I
·--------···------- -----··-- ------------ ------·-·---- ··- --·---------~------·--- ----
-----------·- -·····- ---- ·--·---- --···-----·------·- - - --·-----·----·-·-·· --·--·---- - --- --------
---------- ----- .. ------ ·----·--------··- ··-··-----·· t--- ····-·-. - - ---·- -------- - - - --- --- ·--···------- .. ----1·····-· --·-····--
-------- -- - ---------··--------- ----·~ ---··- --!-···- ... ---·------------·-· ··------·- --··---- ·-
1/) C: 0 ~-------- -····
-·--·-------- ----·---·- - --· ---·----··---·~·--···-- -···-··-----·------·----·-
:1!? 0 ·-·----·----··--- -··----- _____ ,. .. ____________ ---·----~· ----··-···--···---- .. ----,·------··· ---------··--· ··- -- ---·-··---···-· --- ·-·--···----·-----I .. --
Q)
Q
ni ----~-~--·--·- -------- ·--- -- ·----···------ ------··-··~ ------ ---·-·· ·--- ···-·- - - . . -- - ·- -- ·-- --- ----------·-· ·----· ----- ·-----·-----·--·-- ·---- _______ _,_ ---------
-i1 C: Q)
0 E C:
- -··---·------· ··----- -- ·--·-- --··-··----· -- ---··-·----·-·- -··-·------ - --· --- --------·------- ·-----·· --- -
0 ---------- t------ ---------· -----·····----··-- ------- ·----··- ------------- -··-·--···--- --·-- ---·--···--·-- -··--------- ···-· --··
I..
"> C: ·- ----~------------·- -· ·----···-·- -- - -- -·--··--····- --- ···-- ---·----·--------- -----·-·--- -·-----·-····
w 0 :ii!
---·----· ------------ --·-----·--· -·------- -----~-·----~-----··-··· ---··------·····-- ---·------------ -----~-·
<(
I
I
Printed: 7/10/2018 12:23 PM Page 3 of 3
Eff
17.4 -·-----
17.6
15.6
13.7
0095
Eberline Analytical Oak Ridge Laboratory
~ -. Lab Nuclide
Fraction
01 U-238
----- ---··--
02 U-238
_ Sample
Desc
LCS -
MBL
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1
Client I Activity . I I LCS Results Error Est,rnate\ MDA
I Identification I Units Known
LCS pCi/1 6.43E+00 7.95E-01 6.18E-02 7.09E+00!
------------·------------ ---- - --··-------~-·
BLANK pCi/1 6.22E-02 6.33E-02 8.52E-02
~ &, ~ ------ --------··-~·-----···· - -··· --- - ·------------- . --------·------------------- ------ -------- ---------·---··--
03 U-238 DUP OU-1-007 Outfall 007 DIS pCi/I 2.79E-01 1.55E-01 1.26E-01
-· -----··-·--·---------- --- -- -------------·-·--·---· --------·----- ----·-·- ---····----·- ------------- - ···--·------
a, 0 'ti 0 0 U) -!!! -
04 U-238 DO OU-1-007 Outfall 007 DIS pCi/1 1.22E-01 9.17E-02 8.57E-02
------- --------- -------- -----·· ··-- ----·--- ····----- -·--·--····--- ---·-·-··-·------
--------· - ---------------- ----- --------- -, __
~ :::, ca C: :::, <(
···----------··-- . ·------------- ---- -···---------···· ·--- -··-----·-··--··-···- I····
-· ----··-----··--·-----------·- - . ---------- -······--·--- ------------· ·- ··-1-----·-------- -- ---- -------------- ---- -----
... ., 'E 0 --- --------------- -----------··- ------------· --------- -·-··---- ·---·· --------------··· ------ -----------~
t: ~ -------·-- -----·-------------- ·-----·--···--
... ________ ., ___________ ------!---------------
oi -~ ~ .. --- !----------- --- -------------
______ I _________ ··----·- -----· ------ ·----····-·--- -- ----- ---------------- -----------
C: <{ ., .s .:: --------·-------- --------------·- ------·--- ----- -- ---·----··-·--···~--~-------· -·-------- _,_ .... -···-- ---------------- -····---·----------·- -----···-
., ~ --~ ------·· t----- ---- -- ----------·-··----- ----------------- ·------- --·-··----- ··--·---- -- - --·· -----·-------- ···- ---·---··----
1/) C:
.2 ------····-···--·-- 1--·· -·- -··--·-----·--- ---~--------. -··---- ·------------------- ------ ·-·--- ----··------ ------- -··-· ----------· ----------·----
1/)
Printed: 7/10/2018 12:23 PM Page 1 of 3
LCS I LCS
I RPO MDA Blank
i %R Flag Flag Flag Flag
90.66 OK OK -------
OK OK ---
NA OK ----------- ----------
OK
·-------
-------
------
-----
·c:; ------------ ------·-------·--·--- ---- •-~--•••-• •••--••-a-••-•-~--••••---•••••--••• •••• -------------. - -- ---- ------- --- ------------------ --------------- -
--------·-·--Cl)
C ca - ----·--- --- ---·-------- ··------------···-···- ---·------· ------- ----- ··-----·······--- ·------ ---- -·--- --· ------·-----
I
i1 C: Cl)
E C:
-------·--J.-..-..-------- --- ----------~------ ··--- -·-·- -------······-- - -·--·----·-·------- ---------·· ------ --·-----·-
0 -----··-- ---- -------- ---·---------- -------- --·-----···--···· --------- ----------- ---·· --· ,--··---- ---·--- ------ ------------- ----------------- --·-
... ·s; C: ----- ·-----------·- '••·- -·· ----------------- ---------·--·---···-~ ·------
w 0 :ii::
--- ------ --·-----·-· -- -- ------ -----------·----·- -- ---·-------
<(
0096
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations Printed: 7/10/2018 12:23 PM Page 2 of 3
~ Lab
Fraction ,I
01 ---·-·----
02
03 - ... -·--
Cl> 0 b 0
Cl) 0
-~ -04
~ ::> Ill
::> C: c:(
~ 0 t: ~ iii " ~ ca C: <( Q)
=e Q) .Q
~~ "' C 0 ·; ·c:; Q)
C cu -~I C Q)
E C 0 .... > C w 0 :i! <(
Work Order: 18-06097-UUISO-1
Nuclide Sample Sample Sample
Desc Date Aliquot
U-238 LCS 06/21/18 00:00 1.00E+00
---------···--- """ ----·-- -·------··--· -------------. --
U-238 MBL 06/21/18 00:00 1.00E+00
U-238 --1 ~,; I 06/20118 '"" --· ---··· ·-- ,. -·--------·-------·-·---··-- -
U-238 DO 06/20/18 10:00
Radiometric
I Grav
%Rec %Rec
117.30 ______________ o.oo [_ ·-·--·
116.21 o.ooi
+ 84.64[ 0.00 ------- -- ---- .... - - l
118.31 0.001 --- - . - r
i '
Mean % Rec
SAF
o.ooj
SeptO Date/Time
o.oo[ . . -+ -----f---·---------------· r----- ..
o.ool
Sept1 Date/Time
... ·····1·· ===r~ --···--··--0.001 I
i ---·- ·-··---···
-~ i --
····'····--·····--····r··------------+-------- -·--···
·1 -·· - ---1--- I
i Ti ---+------1 .
-0 - - - f -~-t-_ -- -_, -r~1--+---l---·--·-1-------+--t -1----+--~ _ -j- - '
I
0097
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1 Printed: 7/10/2018 12:23 PM
Page 3 of 3
~ -C: :l
"'""" a:
<I> 0 'tl 0 0 en ,!!? -~ Ill
:::, C: :::, c:(
,._ <D
'E 0 .,c ,._ ~ .. u
i .. c:: <t ., ~ ., ill -~
ti) C: .2 ti)
(.) Q)
C iu ......
~I C: Q)
E C: 0 ... "> C: w 0 :i: <(
Lab I Fraction
o-i7 02 I
03 -
04
Nuclide
U-238
U-238
U-238
U-238
II Sample
Desc
LCS
MBL
DUP
DO +-------
, ____ _, --- ---------------------!-----------
Counting
Date/Time
07/10/18 08:08
07/10/18 08:08
I Halflife
(days)
------1-------- --------------+-
07/10/18 08:08
Detect [-ca:e,-1
A_Spec I Alpha_047I
A_Spec Alpha_048
-+-
A_Spec I Alpha_049
Count
Time Counts
170/4.98 E+02
170/4.81 E+00
17011.40 E+01
i Bkg
I CPM
r 2.00 E-03
7.00 E-03 ~----
6.00 E-03
--- ------------1------------------- -- 1---------------- ---1-----------------1---------+-------+- -------
07/10/18 08:08 A_Spec I Alpha_050 170/7.49 E+00 3.00 E-03
------------1--------
---+------------·-- --1--------·----. I·-·---- .. ·------~----
I-----' ------------------1----------1---------- --------1--------------1------ --,-------------+------t----------1-----
1-----i------- -----4 ----- --+---------1~-·----~- -·-r
!
Eff
17.4 ---·----
17.6 -----··---~
15.6
13.7
1-----+-------------------i-------~---·····----
1-------1-------- ------------ --------1-- ---1-- ---- -------------1---------------1----------- -I----------------,------- ------J---------1
------------1---------- ---------------+---------- ------ ------1-------------------1---+--- ----1 ------+------I
------, ----------1--- --------1---------------------- - , __ _
----+ ··-------!-- ----------- ·-----··----·------+---- --------.-- 1-------·-·-·-··--·--- -·--!-
r-rr=+---- I I
_ I==-= a-~ a- -------+---- -l-----1 ·-------"'1 ~ --- . ·-------~---- ---· /--
-1- ----------1------
11-----'---- --e---l ------------------------------1------------------I--------------------- --+--
1-----+-- -------+--- !------------------------ ------I ------+------l-------4-----1-------1
-------/----------------- --1 --- --------- -- -----1------------ - - 1-----------1------ ----+-----~,-----
1------,-----------+---1---~------+---------------------1---- ---- ---- ----1----- ----+----
0098
Eberline Analytical
Oak Ridge Laboratory
~ La~ I Nuclide
Fraction [
I 01 U-235
&I
Q> "O 0 u .!!,!
i "' r::: <:(
-~
-11~0_2 +
03
~,,~1 ::, => I 1------·-1--
___ .J_
II) C:
.Q II)
·o Cl)
C
s C: Cl)
E C: 0 ... "> C: w
l-·-·-·-··-1---
U-235 - -··
U-235
U-235
Sample Desc
LCS ·-· ·- -· ·-··--
MBL
DUP
DO ----- ---·--·
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1
Client Activity Results Error Estimate MDA I
Identification Units ii
LCS pCi/1 4.78E-01 1.77E-01 6.68E-02]
--·---···-· ---·-- - ·----- ···- --·---- ··- ----· --····----··. -··+· BLANK i pCi/I 1.57E-02 4.63E-02 1.01 E-01 i
·--·---- I ··----·-----·--- --·--······--·- _J r ····- ····--·· ···--1.21 E-01 1.56E-01 !
OU-1-007 Outfall 007 DIS I pCi/1 1.23E-01 ··~·~ f OU-1-007 Outfall 007 DIS pCi/I 1.68E-02 4.02E-02 8.44E-02
--------·--·--- - - ----~---- -----········ --
-- - ------ ------- --------------·---
LCS LCS
Known %R
I
I
I
I_
Printed: 7/10/2018 12:23 PM Page 1 of 3
I LCS RPD MDA
I Blank
Flag Flag Flag Flag
I I
OK
I I I OK I OK
I I NA i OK
I I OK
J I
-·---!----------- ---------+ ·---- ··~- ---j-------j------+-----+-----+-----+-------j
·--1···-· ·-· .. ···--1 ···--··-
·1-··-·--·· · -·-i·----·--·· ---··· .-----
1---··-··· ------------· . f---·-··-···-···--··+-·-·-·--·-·-·····--1-··--··--·--+-·---·····-j-------j------+-----+------+-------f-------l
0 :E <(
1------+--·---------------+--·-1---- -------- i---- ··-t---
0099
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1 Printed: 7/10/2018 12:23 PM
Page 2 of 3
( Lab ] Nuclide I Sample I Sample
Fraction I Desc Date
01 U-235 I LCS I 06/21/18 00:00
Sample I
Radiometric
Aliquot % Rec
1.00E+00I 117.30
Grav
% Rec
Mean % Rec
0.001 0.00
SAF Sep to
DatefTime Sept1
Date/Time
c:: ::, ct:
GI ,:, 0 u .!!!
i Ill c:: q:
.... -~ u
--·----·--
02 I U-235 I MBL I 06/21/18 00:00 I
~
03 I U-235 I DUP I 06/20/18 10:00
~·---
04 I U-235
QII-en -::,
1.00E+00I 116.21
1.00E+00I 84.64
118.31
0.00/
I 0.001
I ·1
0.001
0.00
o.oo/ ... ---~· ··----·---~i
0.00
---------------- ... [--- -- ------
--------------1--------------1----------+-------------I
::, I I----- --1---- - --- ------+---------1------------ ---- -+------------------ -----+------ -- ··--~--------I
i
1/) C .2 1/)
·c3 Q)
C co .... C Q)
E C e '> C w 0 :E 4:
1--------- ---·----l-··--·-------------t----1--------------+-------------1
--- _______ ,_______ ---+---- -----+-------- -1---------------+
________ , _______ _
------ -------1--------------- ---1------------------------+-----. ------------+--------------------+--
. ------+-- -----------------------+-----------,
----+-------- .. -------------1---
l----1------------ -+------+------------------1----- -------- ---1------ ----------------1- --------------
0100
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations Printed: 7/10/2018 12:23 PM Page 3 of 3
Work Order: 18-06097-UUISO-1
~ Lab I Nuclide
Fraction
01 I U-235
--
02 I U-235 C:
"""'" :::i a: . L_?! __ J ___ U-235
U-235
Sample Desc
LCS
MBL
DUP
Counting
Date/Time
07/10/18 08:08
07/10/18 08:08 -·-------~---··-- ---------l- --·-
07/10/18 08:08
Halflife (days)
-----!-------- +---------
DO 07/10/18 08:08
~I O 11 04
-I -- -
-~ en · ------·--- -1 - -----------1 -----··--·---
(..)
"' ~ Ill C: q;
t: fi
-::> ::>
1/) C 0
.!!? 0 Q)
Cl
Jg C Q)
E C 0 ... ·s; C w 0 :E <(
t----------1··--······ -----··-+-----··-··I-· ·- ···-·-·····--·----··
IL ___ - -
~------- ------1--------- -··------ 1-----·-···. ·---·--·-··-·-··-J-·---·-··
1--------+------·----··-------·------1-··--· ____ , .... --
·+-
Detect Carrier
A_Spec Alpha_047
A_Spec Alpha_048
Count Time
Counts
17012.98 E+01
17019.80 E-01
Bkg CPM
• 1.00 E-03
Eff
17.4
·-·--·-,------, i6.00 E-03 17.6
A_Spec I Alpha_049 170[4.98 E+00 !6.00 E-03 15.6
A_Spec I Alpha_oso 170/ 8.30 E-01 i 1.00 E-03 13.7
- ·-·-· ------+-·· ·----·-·-1-------·-·· ----- - :- . ·--- ·-. ----
. -- ··-·--·-+·-·-··-·-·-+·•·---····---.---·· i-··- - ·--·
. --1· - --·-!- ---+----------!-----. ----+-----,
-~------ ----~1------·-·----f------------·-·------+...........- ____ _,_ _____ _,
""•+--
··I
·+···--·-
0101
Eberline Analytical Oak Ridge Laboratory
~ . "
Lab Fraction
Nuclide
01 Total U
i:: ::, Q:
{; 0 (.)
,!(?
~ 'iij i::
"'(
!I
T-
=> => ..J II-
(fj C: 0
-~ (.) (I)
0 ~ -C: (I)
E C: 0 ... > C: w 0 :ii!: <(
02 Total U
03 Total U
04 Total U
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-UUISO-1
Client Activity I LCS LCS
Identification Units Results Error Estimate MDA
Known %R
LCS ug/I 1.94E+01 2.37E+00 2.1 SE-01 2.11 E+01 91.71
BLANK ug/I 1.92E-01 1.90E-01 3.00E-01 ------·-- ~---------- -----
OU-1-007 Outfall 007 DIS ug/I 8.87E-01 4.65E-01 4.46E-01
OU-1-007 Outfall 007 DIS ug/1 3.71 E-01 2.73E-01 2.94E-01
-------··
---~----------
----··----- ---·-----·-- ---~-----·--
. -- --- ------ -------- -·----- -------- ------------ --
--------- ··-------- . ··-----·--------- --·--------. -------- -~----~--
------~--------- - ... -------·· ···- ·---- ---·-----··--~ -----·-··-------- ----···---------
--·------ ·----·--- --·----·-··--- ------ -··--·····
------
-·---~·--··-·-·-·--·-·-··· ------ ··---- ------~·-------· ·------·-~----
--·---- --·----······-----· --------·
--~-- ·---.. -----·---·-···· - --·---···--·---. --·-· ------·--·-
-·-----·-- -- ·----- ···--------·-·· ----·-··--·-···-- -·--·----~·---·-- -----~----
-·-··· ----·-·-·--· ---··--·· ----------
----··----- ---·--------·····-- ---···-·--------- -·--·-·---··---~ ---------------
··---~---------- -··-·- -------· ------ ------ --·····------··- -·-··----------- ---·------------ -----
Printed: 7/12/2018 2:32 PM Page 1 of 3
LCS I RPD MDA Blank
Flag Flag Flag Flag
OK OK ----
OK INV -- ····-----·---
NA OK -·----·-
OK
--~----- ----·---------
----~-- ··-------
I ! i
-----
·····---·---
---- -------------
----·---- ---·-·-------
-·----·-·-
·--------
--------- ··----·-~--- ---------------- -·-----
--·----·- -----·---··---- - -·--· --- -----
-····-------- --- - ···--·----·--- ----------
-··----·-- - ··-··-----·. -·- - ------··-·-
-·--·------- --·····---- ---- -------
. ··-----·-·--- ----------
-----------
0102
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations Printed: 7/12/2018 2:32 PM Page 2 of 3
Work Order: 18-06097-UUISO-1
(
Lab Fraction
01
Nuclide I Sample Sample
I Sample
I Radiometric
I Oesc Date Aliquot % Rec
Total U LCS 06/21/18 00:00 1.00E+00 117.30 --·---·---- ···--·-·- -------- ------
c: 02 Total U MBL 06/21 /18 00:00 1.00E+00 116.21
& """" 03 --~-------- -------------- - -··----- -·-------
Total U DUP 06/20/18 10:00 1.00E+00 84.64
··-·-···----·-----···------- ···-- -- . __ ., _____ - ... ··--------
.g ::) 04 Total U DO I 06/20/18 10:00 1.00E+00 118.31 ---- --·-----~ -----
8 => -~ ..J j t-q; t-
,._
-e 0 ~
~
'" .,__ ___ _____, _____________ -1--------1---·------------------- ----1 ---- · ---------1-- ----1--
! ., C: "( Q)
~ Q)
i'il -~
rn C 0
.!!l (.) Q)
Cl
1: I ~ ,!!:? Q)
u E C 0 ... ·s: C w 0 :E <(
--- --t-------------1------1------------- ----------····-·--1
l--------·----1--------- ---------1--------
1-----+-------- --1----1-----------·---····
+-------1---- -·-------- --+---
Grav
% Rec
0.00 ...... -- ---·-·-·
0.00
0.00 ----------
0.00
I·---
Mean
''lo Rec
0.00
0.00
SAF
-- I ______ ---·
0.00
Sep to Date/Time
7 I
--i--
····-·-·-··--1------------- --- ··--···-···
---
I
. ------\---· ----·····- -- --1-------·------···-- -·-------·--- - I
.. - -1- -----···· ·-·---- 1- ----------
Sep 11 Date/Time
- -·-
-·-····----~
---·-- - ------------
----~---
---1------------- --1 -1--------- --------1------------
---1--
i-----·-- --- ·---------------------------1 ·· ------- ----
0103
Eberline Analytical Oak Ridge Laboratory
~ .
'
Lab Nuclide
Sample
Fraction Desc
01 Total U LCS
C: ::i a::
{: 0 (.)
,!!l
~ "' C:
'<I;
t 'E 0
~ ~
l "' c:: <,:
"' ~ ., 6l
1: .!!,? u
""""
::::> ::::> ..J II-
VI C: 0 VI (,) Q)
Cl
ctl ..... C: Q)
E C: 0 ... > C: w 0 ~ <(
-----·---
02 ~-
03 -~--------- -
04 ------------····
-------
------------
-· ----~------- ~----- -
Total U MBL ·-~~·
Total U DUP --·--- ·--~
Total U DO ·--
- ·---·-···-·-
. ---·
---.. -·-~--------------
-·
--------·--------·--~ ----
+--·--------···--
----···---·--
--·-··-----··---·--- --···------·
·····------·---- ·-·--··-··---
Preliminary Data Report & Analytical Calculations Printed: 7/12/2018 2:32 PM Page 3 of 3
Work Order: 18-06097-UUISO-1
Counting Halflife Count Counts
Bkg Eff
Date/Time (days) Detect Carrier
Time CPM
07/10118 08:08 A_Spec Alpha_047 170 4.98 E+02 2.00 E-03 17.4
-- ···-·-,.-- ---·· --------- - I-···-· _,, ______ ·--------- ---- ---------· ----- ---·-·-···--- ··------I·. -- ·-·------- -- ------
07/10/18 08:08 A_Spec Alpha_048 170 4.81 E+00 7.00 E-03 17.6
-··-------- - ... ----------- -- - ·---------- ----·--·- ·----···------- - ·----~--------···- --- ----------···----
07110118 08:08 A_Spec Alpha_049 170 1.40 E+01 6.00 E-03 15.6
•·--· ~- ····---- -- ---·------ -- ------------ --·-· ------- -- ---------··----- -------· --------·--- -----·----
07/10118 08:08 A_Spec Alpha_050 170 7.49 E+00 3.00 E-03 13.7
---·--------·------- ·-···-···----- -------···- ------·---- - ..... .. _, .... , . -,·-·-
----- --··------ -- --------··-------- -----···------- . --· , ...... __ ...... -
---------···· ... -----·····-·-1--- '' .... __ , ....... ---- ---- -··· ,-~
--·-----·--- -----------·---- ---·------------ ·-·--· .. ····-· - . ·····-I·------------·-·-----
-------·---~----··-· --- ----- --··-··- - ---·-·-----·----- -·-·-···---- -- . -----· -------··---- ... ,.-... --- -·-
--------------- -------·1-· ·-·····"" ""•--
, ... ···-•-· .. --···
. ·-----·· ------ --·-- - --·-··-- -·--- -· --·-- ••-.--· , .... ,~_ .... _ ....... -
---·-··----- .... ,,,,. --- -- .... .. ··-·----
,_., __ . -------·····--·- -- ·---· --··-··-··--- ....... .... ______ ,,
- ·---------- ---~-----·-·· ... - I··- --·--···-·----- .... ----- . ------- ··---'---· __ _, ---- --·-- -·-···--
- ... ···---- --·------------ --··
- -- ---· --····--- ------·- -------- -------
--··----- ,, ..... - .......... ----- , .. - ·-- ,., .... ... _ .... ..... ,.__,
..... ---------- ---···· ---·-------
_,.,_, ... . -------- ---- --···-· ---- --------- ---····---- -·--·· ----- . --- ------·- ---··-········-----·-- -· - -·
..... "'"""""" . --- -- ·--· ......... ------- ---···· .... --.-· .. ··- ·--'-·
0104
~/cp
Count Room Report Client: AMO Environmental Decisio
18-06097-UUISO-1 (pCi/1) in WA
Tracer ID: U-1 0a
Printed: 7/1012018 4:40 AM Page 1 of 1
Internal Sample Client Sample Sample I Tracer Tracer Radiometric Ii Radiometric ! SAF SAF
Fraction Desc ID Date Aliquot I
Aliquot (g) ACT (dpm) Tracer (pCi) % Rec 1* 2*
01 LCS LCS 06/21/18 00:00 1.0000 1.1051 20.0686 0.00
02 MBL BLANK 06/21/18 00:00 1.0000 1.1017 20.0069 0.00
03 DUP OU-1-007 Outfall 007 DIS 06/20/18 10:00 1.0000 1.0974 19.9288 0.00
04 DO OU-1-007 Outfall 007 DIS 06/20/18 10:00 1.0000 1.1022 ' 20.0160 0.00 [
i
0105
Eberline Analytical Oak Ridge Laboratory
Spike and Tracer Worksheet
Analysis Code Date Technician
UUISO 7/6/2018 7:25 JHARVEY
LCS MS LCSD l MSD 1 LCS MS
lsoto e I So/ # , Activity I Solution 1
1
ApP_r~x Volume Volume
p i dpm/g I Date Addition Used (g) Used (g) Volume I Volume l Known
I Error Added Error
Used(g) Used(g) pCi Estimate pCi Estimate
U-234 / U-8a / 32.0oo/ 7/6/2018/ 0.550 0.5080 7.32/ 0.264 0.00 0.000
U-238 I U-8a I 31.oool 7/6/20181 0.550 0.5080 7 09] 0.255 0.00 0.000
Tracers Balance Printer Tapes
fraction I Isotope So/# Activity Solution Volume Approx Tracer dpmlg Date Used(g) Addition
01 U-232 U-10a 18.160 7/6/2018 1.1051 1.1000
02 U-232 U-10a I 18.160 7/6/2018 1.1017 1.1000
03 U-232 U-10a 18.160 7/6/2018 1.0974 1.1000
04 U-232 U-10a 18.160 7/6/2018 1.1022 1.1000
I
Version 2.0 08/99
Page 1 of 1 Printed: 7/6/2018 7:29 AM
Witness Initials
LCSD -MSD Known i Error Added Error
pCi I Estimate pCi Estimate
0.00 1 0.000 0.00 0.000
0 OOi 0.000 0.00 0.000
LCS
Matrix Spike
0106
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-007 Outfall 007 DIS
04 OU-1-007 Outfall 007 DIS
Comments
Sample
Type
LCS
MBL
DUP
DO
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
UUISO liters 7/11/2018
Muffle Data Dilution Data Aliquot Data
Ratio Post/Pre No of Dils Oil Factor Ratio Aliquot Net Equiv
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO 1.0000E+OO
Techaiciaac ~al\lC,ff atec '.::/-; a
Technician
JHARVEY
MS Aliquot Data
Aliquot Net Equiv
Printed: 7/6/2018 9:39 AM Page 1 of 1
H-3 Solids Only Water Aclcleu H3-D1st-
(ml) Aliq
i
0107
Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167
1806097A-UU Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 U iso
Alpha_047 10006125A 91086 System Bkgd 219035
<not performed>
l.000E+000 7/10/2018 7/10/2018
+/- 0.000E+000 liter 5:51:27 AM 8:08:05 AM
170.0 minutes 170.0 minutes
U232 UU-l0A 1.105 mL 0.2046 +/- 0.0091
Counting Efficiency: 0.1744 +/- 0.0030 on 6/6/2018 1.1730 +/- 0.0558
2:37:41 PM
Chem. Recovery Factor:
Control Certificate Name: NatU U-8A Chem. Recov. of Control: U-238 0.797558 +/- 0.055693
Peak Match Tolerance: 0.150 MeV
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.277 4.734 4.379 4.159
PEAK AREA REPORT
Net Pk Area
697.98 486.15
29.83 497.66
Pk Area Error%
7.43 8.90
36.01 8.79
Ambient Backgnd
1. 02 0.85 0.17 0.34
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
8.4 37.0 3.7
36.9
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.995 0.995 1.000 0.995
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter)
9.06E+000 +/- 7.87E-001 6.31E+000 +!- 7.85E-001 4.78E-001 +/- l.77E-001 6.43E+000 +/- 7.95E-001
1-t-t 1/o/fg
MDA (pCi/liter
8.18E-002 +!- 7.l0E-003 7.77E-002 +/- 6.75E-003 6.68E-002 +/- 5.81E-003 6.18E-002 +!- 5.37E-003
0108
60
55
50
45
40
35 V} .j-J C ::::s 8 30
25
20
15
10
5
0 I
3500 4000
I if
l.orii M.' I ~1.,1 =?.I ]J,1
- [,
11 I
ROI Type: 1
4500
0000216758.CNF
5000 Energy(kev)
I 11
1,1\,1 i'! 11
i lrJ
iii I I
5500
Live Time :10200.000 sec Real Time :10200.400 sec start: 1:3453.S(kev) stop : 1024:6472.?(kev) Acq. start :Tue Jul 10 08:08:05 2018
6000
ROI Type: 3
0109
Channel Data Report 7/10/2018 11:07:54 AM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------1-------1-------1-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 1 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 1
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 1 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 1 0 0 0 0 1 1
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 1 0 0
153: 0 1 1 0 0 0 0 1
161: 1 0 0 0 1 0 1 1
169: 1 0 0 1 0 0 0 0
177: 1 0 1 1 2 0 1 1
185: 2 1 2 2 2 1 0 1
193: 1 1 1 0 1 1 1 0
201: 1 1 0 2 2 1 4 2
209: 5 3 3 2 2 3 2 2
217: 2 3 1 7 7 2 4 6
225: 7 5 7 6 6 13 4 4
233: 10 9 5 16 12 7 8 12
241: 13 14 12 12 20 13 14 14
249: 16 11 13 10 10 10 18 11
257: 11 13 11 10 7 7 7 4
265: 2 1 0 0 0 0 1 0
273: 0 0 0 0 0 1 0 0
281: 0 1 1 1 0 0 0 2
289: 0 0 0 1 0 0 0 0
297: 2 0 1 0 0 0 0 3
305: 1 0 0 0 1 0 1 1
313: 1 2 0 1 0 1 1 0
321: 1 0 3 1 0 0 0 0
329: 1 1 0 1 1 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 1 0 1 0 0
353: 0 0 0 0 0 2 0 1
361: 1 0 0 0 0 1 0 0
0110
Channel Data Report 7/10/2018 11:07:54 AM Page 2
369: 0 1 0 2 0 0 0 2
Sample Title: 01
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 1 0 3 2 1 2 0 3
385: 0 0 3 2 1 1 1 0
393: 3 0 1 2 0 2 1 1
401: 0 0 1 4 4 4 0 1
409: 3 4 3 3 4 2 5 7
417: 3 5 7 10 5 5 11 11
425: 5 10 9 9 14 11 9 6
433: 12 10 15 8 9 15 12 14
441: 13 12 18 14 11 14 12 13
449: 20 6 12 16 14 10 3 8
457: 4 2 0 1 0 1 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 1 0 0 0
481: 0 0 0 0 0 0 1 0
489: 0 0 0 0 0 0 0 1
497: 0 0 0 0 0 1 0 0
505: 0 0 0 0 0 0 1 1
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 1 0 0
529: 1 0 0 1 0 0 0 0
537: 0 0 0 4 1 0 0 1
545: 0 1 0 0 0 0 1 0
553: 2 0 1 1 0 0 1 2
561: 1 3 0 0 1 1 2 1
569: 1 0 2 0 1 1 4 2
577: 3 2 2 5 1 1 2 2
585: 2 2 3 5 2 4 8 5
593: 2 2 5 11 3 3 3 6
601: 7 4 4 8 10 10 10 16
609: 12 14 6 25 16 20 10 17
617: 14 14 13 15 16 12 18 26
625: 13 18 20 20 17 20 26 22
633: 24 19 23 9 20 7 11 5
641: 10 5 2 0 0 1 0 0
649: 0 0 1 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0111
Channel Data Report 7/10/2018 11:07:54 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------1-------1-------1-------I-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 1 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0112
Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167 1806097A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 U iso
Alpha_048 10006125B 83111 System Bkgd 219036
<not performed>
l.000E+000 +!- 0.000E+000 7/10/2018 5:51:27 AM
7/10/2018 8:08:07 AM
170.0 minutes 170.0 minutes
0.0091
liter
Counting Efficiency: Chem. Recovery Factor:
U232 UU-l0A 1.102 mL 0.2045 +/-0.1760 +/-1.1621 +/-
0.0030 on 6/6/2018 0.0554
2:37:42 PM
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.295 4.777 4.368 4.143
0.150 MeV
PEAK AREA REPORT
Net Pk Area
695.62 6.64 0.98 4.81
Pk Area Error%
7.45 84.69
294.85 101.48
Ambient Backgnd
2.38 1. 36 1. 02 1.19
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
39.1 3.0 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
1.000 0.998 0.998 0.988
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter )
9.03E+000 +/- 7.86E-001 8.62E-002 +!- 7.34E-002 l.57E-002 +/- 4.63E-002 6.22E-002 +!- 6.33E-002
l1Gr 1/10/rt
MDA (pCi/liter
1. 06E-001 +!- 9.26E-003 8.90E-002 +/- 7.75E-003 l.0lE-001 +/- 8.78E-003 8.52E-002 +!- 7.41E-003
0113
60
55
50
45
40
35 Vl +-' C: :::::s
8 30
25
20
15
10
5
0 I
3500 4000
!.Ml
4500
ROI Type: 1
0000216759.CNF
I
I_,\ 1:'. I:
5000 Energy(kev)
i h
! 'I
5500
Live Time :10200.000 sec Real Ti me : 10200. 400 sec Start: 1:3443.9(kev) Stop : 1024:6472.3(kev) Acq. Start :Tue Jul 10 08:08:07 2018
6000
ROI Type: 3
0114
Channel Data Report 7/10/2018 11:08:01 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E p 0 R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------1-------1-------1-------I-------I 1 : 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 1 0
201: 0 0 0 1 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 1
249: 0 0 0 1 0 1 0 0
257: 0 0 0 0 0 0 0 0
265: 0 1 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 1 0 0
313: 0 0 0 1 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0115
Channel Data Report 7/10/2018 11:08:01 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channel\------\-------\-------\-------\-------\-------\-------\-------1 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 1 0 1 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 1 0 0
449: 0 1 0 0 0 0 0 0
457: 0 0 0 0 0 2 0 1
465: 0 0 0 0 0 0 1 0
473: 0 0 0 0 0 0 0 0
481: 1 0 0 0 0 0 0 0
489: 0 1 0 0 1 0 0 0
497: 0 1 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 1 0 0 0 0 0 0
521: 0 1 0 1 0 0 1 0
529: 0 0 0 0 1 0 0 0
537: 1 0 0 0 0 0 0 0
545: 0 0 0 0 1 0 1 0
553: 0 1 0 0 1 0 0 1
561: 0 0 1 0 2 3 0 0
569: 0 0 0 2 0 1 3 1
577: 1 0 2 2 1 2 1 0
585: 2 3 1 1 2 2 2 3
593: 1 3 6 3 2 3 3 1
601: 7 4 4 6 6 2 5 6
609: 6 7 9 14 12 12 8 10
617: 6 13 16 11 12 15 13 19
625: 16 14 9 18 11 16 16 18
633: 22 25 23 30 28 27 27 21
641: 24 30 15 14 14 3 5 1
649: 1 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 2 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 1 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0116
Channel Data Report 7/10/2018 11:08:01 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------1-------1-------1-------I-------I-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 1 1 0 1 0 0 1 0
977: 1 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0117
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency: Counting Efficiency: Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 U-234 U-235 U-238
T
Energy (MeV)
5.265 4.722 4.405 4.133
OU-1-007 OUTFALL 007 DIS DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167 1806097A-UU 03 Shelf 2 U iso
Alpha_049 10006121A 49 System Bkgd 219037
<not performed>
1.000E+000 6/20/2018 7/10/2018
+/- 0.000E+000 liter 5:51:27 AM 8:08:01 AM
170.0 minutes 170.0 minutes
U232 UU-l0A 1.097 mL 0.1325 +/- 0.0070 0.1565 +/- 0.0028 on 2/16/2018 12:37:01 PM 0.8464 +/- 0.0471
0.150 MeV
PEAK AREA REPORT
Net Pk Area
448.77 12.81
4.98 13.98
Pk Area Error%
9.29 57.66 97.79 54.61
Ambient Backgnd
3.23 1.19 1. 02 1. 02
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
38.9 3.0 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.990 0.989 0.997 0.981
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter )
9.00E+000 +/- 9.30E-001 2.57E-001 +!- 1.50E-001 l.23E-001 +!- 1.21E-001 2.79E-001 +/- 1.55E-001
/rG
1fo/rs
MDA (pCi/liter
l.83E-001 +!- l.89E-002 l.32E-001 +!- 1.36E-002 1.56E-001 +/- l.61E-002 l.26E-001 +!- 1.30E-002
0118
60
55
50
45
40
35 V)
-I-' C: ~
8 30
25
20
15
10
5
0000216760.CNF
!I ! )I
'' ~
1l ii
7
0 q I I! !I 1! !I'"' •, ,,, . ' I i' ~I l I ' . ! i I I .' ' •. · ·•·"· I· · 1 1 '' ! ! 1 l 500 .. I 1 1
: 1 1 F 1 1 I I I I I 111111 1 I/: I
4000 4500 5000 Energy(kev)
5500
ROI Type: 1
Live Time :10200.000 sec Real Time :10200.300 sec start: 1:3474.l(kev) Stop : 1024: 6513, l(keV) Acq. Start :Tue Jul 10 08:08:01 2018
I I 1 I 1! I ! ! 1 l 6000 6500
ROI Type: 3
0119
Channel Data Report 7/10/2018 11:08:07 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E p 0 R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channel\------l-------l-------1-------1-------1-------I-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 1
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 1
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 1 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 1
177: 0 0 0 0 1 0 0 0
185: 0 0 0 0 0 1 0 1
193: 0 0 0 0 0 0 0 1
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 1 1 0 0 0 0
225: 0 0 0 0 1 1 1 1
233: 0 1 0 0 0 1 1 0
241: 0 1 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 1 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 1 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 1 0 1 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 1 0 0 0 0 0 0
329: 0 0 1 0 0 0 1 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 1 0
361: 0 0 0 0 0 0 0 0
0120
Channel Data Report 7/10/2018 11:08:07 AM Page 2
369: 0 1 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 0 0 0 0 0 0 0 0
385: 1 0 0 0 0 0 0 0
393: 0 0 0 0 1 0 0 0
401: 0 0 0 0 1 0 0 0
409: 0 0 0 0 1 0 1 0
417: 0 0 0 0 0 0 1 1
425: 1 0 0 0 1 0 2 0
433: 0 1 0 0 0 0 0 0
441: 1 1 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 1 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 1 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 1 0 0 0 0 0 0 0
537: 0 0 1 1 0 0 2 1
545: 0 0 1 0 0 2 0 0
553: 1 0 3 0 0 0 1 0
561: 2 1 0 0 1 4 3 2
569: 1 3 4 2 3 4 1 3
577: 2 4 1 1 5 4 4 3
585: 4 4 4 3 4 6 4 9
593: 8 3 7 10 11 13 8 11
601: 11 11 12 5 11 4 13 13
609: 14 15 13 13 14 18 14 14
617: 11 14 17 5 12 12 8 4
625: 4 0 2 0 1 2 1 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0121
Channel Data Report 7/10/2018 11:08:07 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 1 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 1 0
945: 0 0 0 0 0 0 0 0
953: 1 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0122
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency: Counting Efficiency: Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.281 4.742 4.385 4.137
OU-1-007 OUTFALL 007 DIS \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167 1806097A-UU 04 Shelf 2 U iso
Alpha_050 10006121B 50 System Bkgd 219038
<not performed>
l.000E+000 6/20/2018 7/10/2018
+/- 0.000E+000 liter 5:51:27 AM 8:08:03 AM
170.0 minutes 170.0 minutes
U232 UU-l0A 1.102 mL 0.1620 +/- 0.0078 0.1369 +/- 0.0025 on 2/16/2018 12:37:00 PM 1.1831 +/- 0.0612
0.150 MeV
PEAK AREA REPORT
Net Pk Area
551.15 11.47
0.83 7.49
Pk Area Error%
8.36 62.23
239.53 74.41
Ambient Backgnd
0.85 1.53 0.17 0.51
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
29.2 4.4 3.0 3.0
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.997 0.997 1.000 0.984
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/liter)
9.04E+000 +/- 8.58E-001 l.88E-001 +/- 1.18E-001 l.68E-002 +/- 4.02E-002 l.22E-001 +/- 9.17E-002
N, 7/rofrg
MDA (pCi/liter
9.82E-002 +/- 9.33E-003 l.17E-001 +/- l. llE-002 8.44E-002 +/- 8.0lE-003 8.57E-002 +/- 8. 13E- 003
0123
60
55
50
45
40
35 V) ...., C ::::i;
8 30
25
20
15
10
5
0 I
3500
'1
,\ :\/ i1}fj~
4000
ROI Type: 1
= ~ ' ::,
4500
0000216761.CNF
5000 Energy(kev)
~ = ' ::,
5500
Live Time :10200.000 sec Real Time :10200.300 sec Start: 1: 344 7. 7 (kev) Stop : 1024:6482 .6(kev) Acq. Start :Tue Jul 10 08:08:03 2018
6000
ROI Type: 3
0124
Channel Data Report 7/10/2018 11:08:14 AM Page 1
******************************************************* ***** s p E C T R A L D A T A R E p 0 R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 1 0 0 0 0 0 0 0 49: 0 0 0 0 0 0 0 0
57: 1 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0 73: 0 0 0 0 0 0 0 0 81: 0 0 0 0 0 0 0 0 89: 0 0 0 0 0 0 0 0 97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0 113: 0 0 0 0 0 0 0 0 121: 0 0 0 0 0 0 0 0 129: 0 0 0 0 0 0 0 0 137: 0 0 0 0 0 0 0 0 145: 0 0 0 0 0 0 0 0 153: 0 0 0 0 0 0 0 0 161: 0 0 0 0 0 0 0 0 169: 0 0 0 0 0 0 0 0 177: 0 0 0 0 0 0 1 0 185: 0 0 0 0 0 0 0 0 193: 0 1 0 0 0 0 0 1 201: 0 0 0 0 0 0 0 0 209: 0 0 0 0 0 0 0 0 217: 0 1 0 0 0 0 0 0 225: 0 0 0 0 0 0 0 0 233: 0 0 0 0 0 0 0 0 241: 0 0 0 1 0 0 0 1 249: 0 0 1 0 0 0 1 0 257: 1 0 0 0 0 0 0 0 265: 0 0 0 0 0 0 0 0 273: 0 0 0 0 0 0 0 0 281: 0 0 0 0 0 0 0 0 289: 0 0 0 0 0 0 0 0 297: 0 0 0 0 0 0 0 0 305: 0 0 0 0 0 0 0 0 313: 0 0 0 0 1 0 0 0 321: 0 0 0 0 0 0 0 0 329: 0 0 0 0 0 0 0 0 337: 0 0 0 0 0 0 0 0 345: 0 0 0 0 0 0 0 0 353: 0 0 0 0 0 0 0 0 361: 0 1 0 0 0 0 0 1
0125
Channel Data Report 7/10/2018 11:08:14 AM Page 2
369: 0 0 1 0 1 0 0 1
Sample Title: 04
Channell------l-------l-------l-------l-------1-------1-------1-------\ 377: 0 0 0 0 0 0 0 0
385: 1 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 1 0
409: 0 0 0 0 0 0 0 1
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 1 2 0 0
433: 0 0 0 0 0 0 1 0
441: 1 0 0 1 2 0 0 0
449: 0 1 1 0 0 0 0 0
457: 0 1 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 1 0 0 0 0 0
481: 0 0 0 1 0 0 0 0
489: 0 0 1 0 0 0 2 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 1 0
513: 0 0 0 0 0 0 1 0
521: 0 0 0 0 0 0 0 1
529: 0 0 0 0 0 1 0 0
537: 0 0 0 1 1 0 0 0
545: 0 0 0 0 0 0 0 1
553: 0 0 1 0 0 0 1 0
561: 1 0 0 2 0 0 2 1
569: 0 2 1 0 0 1 1 0
577: 2 1 2 4 2 4 0 1
585: 1 2 2 2 2 1 3 3
593: 2 1 6 2 3 5 4 1
601: 4 7 12 6 1 9 12 12
609: 10 7 15 11 8 10 11 15
617: 12 9 15 10 14 10 13 12
625: 12 19 21 17 26 22 19 19
633: 18 17 13 13 10 13 7 1 641: 1 0 1 0 0 0 0 0 649: 0 0 0 0 0 0 0 0 657: 0 0 0 0 0 0 0 0 665: 0 0 0 0 0 1 0 0
673: 0 1 0 0 0 0 0 0 681: 0 0 0 0 0 0 0 0 689: 0 0 0 0 0 0 0 0 697: 0 0 0 0 0 0 0 0 705: 1 0 0 0 0 0 0 0 713: 0 0 0 0 0 0 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 0 0 0 0 0 0 753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0 769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 0 0 0 0 0 793: 0 0 0 0 0 0 0 0
0126
Channel Data Report 7/10/2018 11:08:14 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------j-------1-------1-------1-------j-------l-------l-------l 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 1 0 0 897: 0 0 0 0 0 0 0 0 905: 0 0 0 0 0 0 0 0 913: 0 0 0 0 0 0 0 0 921: 0 0 0 0 0 0 0 0 929: 0 0 0 0 0 0 0 0 937: 0 0 0 0 0 0 0 0 945: 0 0 0 0 0 0 0 0 953: 0 0 0 0 0 0 0 0 961: 0 0 0 0 0 0 0 0 969: 0 0 0 0 0 0 0 0 977: 0 0 0 0 0 0 0 0 985: 0 0 0 0 0 0 0 1 993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0 1009: 0 0 0 0 0 0 0 0 1017: 0 0 0 0 0 0 0 0
0127
Page 1 of 2 7/10/2018 5:36:53 AM
/'") I\ Cl II\ Al\ 11 I\ DV or::::onoT ~It VVIIIIIVlrH \ I I \l-1 \../I\ I
Review Of QA Results - Pulser Check
Date : 7/10/2018 Time : 5:36:53 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 001 2lf ALL Not Done
Alpha 002 2lf ALL Not Done
Alpha 003 2lf ALL Passed 7/10/2018 5:16:04 AM
Alpha 004 2lf ALL Passed 7/10/2018 5:16:05 AM
Alpha 005 2lf ALL Not Done
Alpha 006 2lf ALL Not Done
Alpha 007 2lf ALL Not Done
Alpha 008 2lf ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 2lf ALL Passed 7/10/2018 5:16:06 AM
Alpha 011 2lf ALL Passed 7/10/2018 5:16:07 AM
Alpha 012 2lf ALL Passed 7/10/2018 5:16:08 AM
Alpha 013 2lf ALL Not Done
Alpha 014 2lf ALL Passed 7/10/2018 5:16:09 AM
Alpha 015 2lf ALL Not Done
Alpha 016 2lf ALL Not Done
Alpha 033 Alpha Analystl 00DC Peak Energy Action 7/10/2018 5:16:10 AM
Alpha 034 Alpha AnalystlO0DC ALL Not Done
Alpha 035 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:11 AM
Alpha 036 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:13 AM
Alpha 037 Alpha Analystl00DC ALL Not Done
Alpha 038 Alpha Analystl 00DC ALL Not Done
Alpha 039 Alpha Analystl 00DC PeakFWHM Action 7/10/2018 5:16:14 AM
Alpha 040 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:16 AM
Alpha 041 Alpha Analyst I 00DC ALL Passed 7/10/2018 5:16:17 AM
Alpha 042 Alpha Analyst I 00DC ALL Passed 7/10/2018 5:16:19 AM
Alpha 043 Alpha AnalystlO0DC ALL Not Done
Alpha 044 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:20 AM
Alpha 045 Alpha Analyst I 00DC ALL Passed 7/10/2018 5:16:22 AM
Alpha 046 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:23 AM
Alpha 047 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:25 AM
Alpha 048 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:27 AM
Alpha 049 Alpha AnalystlO0DC ALL Passed 7/10/2018 5:16:28 AM
Alpha 050 Alpha Analyst I 00DC ALL Passed 7/10/2018 5:16:31 AM
Alpha 051 Alpha Analystl00DC ALL Not Done
Alpha 052 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:33 AM
Alpha 053 Alpha Analystl00DC PeakFWHM Action 7/10/2018 5:16:35 AM
Alpha 054 Alpha Analystl00DC ALL Not Done
Alpha 055 Alpha Analystl 00DC ALL Not Done
Alpha 056 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:37 AM
Alpha 057 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:39 AM
Alpha 058 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:41 AM
0128
Page 2 ot 2 Kev1ew ot UA Kesutts - t'ulser 1..;necK 7/10/2018 5:36:53 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha Analyst 1 00DC ALL Passed 7/10/2018 5:16:44 AM
Alpha 060 Alpha Analvstl00DC ALL Passed 7/10/2018 5:16:47 AM
APPROVED BY:
APPROVAL DATE: "])I_O/t8
0129
Library Listing Report 6/12/12 12:17:04 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Uranium
Nuclide Library Description: U-232,-234,-235,-238
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV ( % ) Uncert. (Abs.+-)
U-232 2.174E+009 5302.500* 0.000 99.8000 0.0000
U-234 7.731E+Ol2 4761.500* 0.000 99.8000 0.0000
U-235 2.221E+016 4385.500* 0.000 80.9000 0.0000
U-238 1.410E+Ol7 4184.400* 0.000 100.2300 0.0000
* :=, key line
TOTALS: 4 Nuclides 4 Energy Lines
0131
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Work Order 18-06097
Analysis Code [~·Th ISO.. 7 Run 1
Date Received 6/21/2018
Lab Deadline 7/11/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 907.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer Th-229
Radiometric Sol# Th-18a
Tracer Act (dpmlg) 22.46
Carrier
Carrier Cone (mglml)
Internal Sample I Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
18-06097 ThlSO Run 1
Client ID
LCS
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Login CPM
30
30
Printed: 7/10/2018 4:41 AM Page 1 of 3
Sample Sample Date Aliquot
06/21/18 00:00 1.0000E+00
06/21/18 00:00 1.0000E+00
06/20/18 10:00 1.0000E+00
06/20/18 10:00 1.0000E+00 I
!
0132
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal Sample Tracer
Fraction Desc Aliquot (g)
01 LCS 0.4656
02 MBL 0.2332
03 DUP 0.2319
04 DO 0.2310
Tracer Total Radiometric I Radiometric ACT(dpm) Tracer(pCi) %Rec
10.5 0.00
5.2 0.00
5.2 0.00
5.2 0.00
18-06097 ThlSO Run 1
Grav Carrier I Grav Filter
Added(ml) Tare (g) Grav Filter Final (g)
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I I
I
Grav Filter Grav I
Net (g) ¾Rec I
I
Printed: 7/10/2018 4:41 AM Page 2 of 3
Mean SAF SAF ¾Rec 1* 2*
0133
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Rough Prep Prep
Date By Date
07 /06/18 07:25
07/06/18 07:25
07 /06/18 07:25
07/06/18 07:25
18-06097 ThlSO Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
Sep to Date/Time
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep to By
I
Printed: 7/10/2018 4:41 AM Page 3 of 3
Sep t1 Sep t1 Date/Time By
0134
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 1 of 3
~ ®
C: ::, a::
~ 8 -!!! (I)
~ 111 C: <t
~I
"C""'"
0 u, -.c I-
II) C: 0 ·-.!!! (.) Q)
C ns -C: Q)
E C: 0 .... ·s; C: w 0 ::!!: <(
Lab Fraction
01
I 02
Nuclide
TH-228
TH-228
I. Sample
Desc
LCS
MBL
Client
Identification
LCS
Activity Units
Results ) Error Estimate MDA I LCS LCS
Known %R
pCi/1 s.s2E+ool 1.19E+oo 1.BBE-01 4.B7E+ool 119.46
i ---~ .. ·----+---• .. l ·- ~-------- -··---~··------ ··1-··- -r··--
BLANK pCi/1 4.84E-02I. 6.01 E-02 9.12E-02 ;
LCS Flag
OK
RPD Flag
I
MDA I Flag
OK
OK
Blank Flag
OK
03 TH-228 DUP OU-1-007 Outfall 007 DIS pCi/1 1.92E-03 I 2.69E-02 I 7 .69E-02 NA OK
I I ----1-- ------------+-- ------ .... , .... ••·----+---....... • +·--......... --... ; ..... .
04 TH-228 DO OU-1-007 Outfall 007 DIS pCi/1 5.66E-02I 7.45E-02I 1.19E-01 OK
-----+··-··-·-----+---- , ... ----+-----~-- --+----------t-----;--------
_ ..... ---+·······-····--····-.... __ --+--- ···I
I-·-···· -I··-· ... ••-----+------ I····· -- -- -. - - ----··------l - ·····1··········--·········+-----·+-.. -·--·· .. I······· .. ······-c .. ·····-·--+-----+-----+------1
··-···· ....... --+------ I ·-· , .. ·······-----·-··· .. +···· ... · ······-+··.. . .. ····+··-----+------,--·---+--......... , ··-·····--+------1•----+------,
,-----+--- .. -----+---.. I·· .. •·· ·•· .. ·-+···· ···· ....... ·······1--.... _._ ·-···I
····+·· t-------1·--·· .. ·-··· -+------1- -----,-1----+----+----l-----1
1·-·-····· --+·-···· ...... ------+-- .... ,
1-------j-·--··· -----· - -----4 ·--- -1--·-- .:_ ... : . -- ·--······:- ·- ·- .. + ... ___ •--- t ....... ·········I······--··· ---- ·····+· ....... ·········· ·····-·· .. ···-·····- ... ••·I········· ····· .. +··· .. ······· ... --1---..
_., ___ ,._ .. ----+-- ------+- ···· .. ·I·· ........................ -----·--r-----· .... + .. ······· · ··-l·····--··-····+---.. +·-----1----.... -t------1f---------1----f---------1
+--········· .
r------+-----·- - ------1 ·-----·I·--------
1-.. ··-·····+- .. •· -----1----+-----··•• .. •·····--·· .. ····--··· ----,.---·· ...... + ...
-···-------f----- I·.. ······-1··
: ~~ i I I I I I : I
0135
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 2 of 3
~ Lab Nuclide
Sample Sample
Fraction i Desc Date -----,
01 [ TH-228 LCS 06/21/18 00:00
Sample Radiometric
Aliquot % Rec
1.ooE+oo! 65.13 I
Grav % Rec
0.00
Mean
% Rec
o.ooi
SAF SeptO
Date/Time
Sep t1 Date/Time
&!
a, "ti 0 0 .!!! ~ ca C: q;
C: ~ 0
T"" I I
0 en -~ t-- I 1---···-··+·
1/) C: 0 1/)
·o Q)
C
Jg C: Q)
E C: 0 ... ·s: C: w 0 :ii: <(
-·---- -·-- -------- ·--/
TH-228 MBL 06/21/18 00:00
··-- --------~-·~
TH-228 I DUP I 06/20/18 10:00 -- --------- -------·---· ·---· ·-
TH-228 DO 06/20/18 10:00
-- -·-- --- -+-- -------1-----·
·-----1---
1.00E+00 107.62 0.00
······-·-·····-···I··-·······--···-·---
1.ooE+oo! 114.43 0.00
.. / .
1.ooE+ooi 92.94 0.00
f·-···
0.00i i
-T o.oo,
I o.ool
I
I l
------·-·----~-·-----f~···--····- ------------ - --1-----···--
···--·-1---1----------+-- ·· -·-·-1- ··· -··-··-····--·····--+··-· ~~--t=----t--------+-------1
--·-·----+-·--· 1------- ----+---·····-- ----·-·----··-------1---·----------------~------t-------------1
----+----1-···--··-·······-·-·--···--·--··- 1-·-··-----·-·f--···-- -·-·····-·-I·····--·-·-·-······· I·····--·-····-
-··--··-···· ·······-+-··-···--· .. --f-··· . -· -··-+···--·-·
- -+--··--·I-···-···
+-·-··-·!----- -·----+--
0136
Eberline Analytical Oak Ridge Laboratory
~ Lab Nuclide I Sample I
Fraction Desc
01 TH-228 LCS I
02 TH-228 MBL I C: :::, -c-0:: 03 I TH-228 I DUP I
--~-
0 I I _ 04 _J__ TH-228 ___ _L_ DO _j
Cl> "0 0
(.)
~ I 1-------·-~---•...J----.-.!!!
~ .c Ill C: ... I 1---------l--- ------ ------------,---ci:
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1
Counting
I Halflife
Date/Time (days) Detect Carrier Count I Counts I
Bkg
Time CPM
07 /10/18 08:04 ' '
110)2.27 E+02 I 1.00 E-02 A_Spec / Alpha_003'
07/10/18 08:04
07/10/18 08:04
i I I------
I ' A_Spec !Alpha:-0_04! 170 I 3.64 E+00 18.00 E-03
A_Spec IA1pha_o10I 110.02j1.5o E-01 15.00 E-03
-I '------.--
07/10/18 08:04 A_Spec Alpha_o11f 170.02j3.79 E+oo_J1.30 E-02
.. --- . --,-. -- --------- .
I
Printed: 7/10/2018 12:14 PM Page 3 of 3
Eff
15.9
18.5
18.4
19.5
-------1--------------)----------------.+-------t-----
---1---------
---------1--
---+---- -~------j------1
1/) C: 0 I 1---------- -1------
1/)
·o Q)
C (ti -~I C: Q)
E C:
- ... ---1 ----- ---------------
. . . . .. I · --------------- ---------------
!
0 ... ·s: C: w 0 ::!!: <(
0137
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 1 of 3
~ Lab
Fraction
01
Nuclide ! Sample Client Activity
\ Desc Identification Units
TH-230 LCS LCS pCi/I
Results I Error Estimate
6.59E+00/ 1.31E+00
MDA LCS
Known LCS %R
1.53E-01 / 5.38E+00I 122.48
LCS Flag
OK
RPO Flag
MDA Blank
Flag Flag
OK
C: ::i T""' 0::
Cl)
"l::J 0 0 (..) en .!!!
~ -ca .c C: I-"(
-.... ., ~ 0 t: ~ .; .g ~ "' C: <( ., :§ .... ., il:l --~
II)
C: 0 II)
·c:; Cl> C
--- -~---- ---·--·---- ----·-
02 TH-230 MBL BLANK
03 TH-230 I DUP I OU-1-007 Outfall 007 DIS
-
04 TH-230 DO OU-1-007 Outfall 007 DIS
---- ""--·-···- --·------- ----···
--·----·-·----- . -··---------· ---·- --------·-
--·---- ·-·---- ------·-------···-···------···-·--·-----·----
--------- - -----
1------1--·-·-----·- ---·--··--+---·-···--1·--··-·-·---
pCi/I
pCi/I
pCi/I
----+---------- -
5.27E-021 6.63E-02 1.04E-01,
i
OK I OK -1----
l 1.49E-01 I 8.SSE-02
1.73E-01 I 1.0SE-01
5.26E-02j
----··i --9.65E-02/ ___ ._···t----+---+------+
NA OK -OK
_!
I
i-+----t-17-- --------1 - -I
·-r-·---·-1 I
-1------·····---~~~~·~-~ l ~=L ~ I I I I I
-·---·r----;----------------- ··----+--
----~-----~----------·····-•-- . -+·· ------1- -----+--
----+----1---·---·----·-·-·--------------·--·-----·----.i.-- ·-1--··-·-··--------+--·---- ·--+--·-·-·- ·-
co I L--··- - ·--,.----1------;---- •',----·--- -----·-----) - ----J------···-----··-· --/---··---
-~I C: Cl> E C: 0 I.,
> C: w ------1--·-· -----+-------! --------- -····--··-~·---+----- -+----------·+---------•-------+------+-----+-----+-----+-----I
0 :ii: <t
0138
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 2 of 3
,: Lab Fraction
Nuclide
01 TH-230
Sample Desc
LCS
Sample Date
06/21/18 00:00
Sample Aliquot
1.00E+00
Radiometric Grav Mean SAF
SeptO Sept1
%Rec % Rec % Rec Date!Tirne Date/Time
65.13 0.00: 0.00
C: ::, a::
Cl> ,::i 0 0 .!/.! ~ a, C: q;
~ 1:! 0 ~ ~
l .. C: "I: Cl> .s .:: ., ~
j
---~-----------------J--------1----·- -·---- . --------·· ----·-
02 TH-230 MBL 06/21/18 00:00 1.00E+00I 107.621 o.ool 0.00
~
--- -----~-1----·-
03 TH-230 DUP 06/20/18 10:00 1.00E+00I 114.43I 0.001 0.00 I
-·----·---- I ·--·--· )-
04 I TH-230 DO 06/20/18 10:00 1.00E+00I 92.94I 0.001 0.00
0 en -..c I- I I ·-- ·· - !-··
11'1 C: 0
.!!? (.) Q)
C
Jg C: Q)
E C: 0 ... '> C: w 0 :E <(
------·· -1----------.---···-~--t-- -------+-------·-------l-------------1
--+-----· ·--·· ····-··-·--·· ···t·-······-----····-- · ····-·· ·· f··---···-······- ······-·I·---····
······-····- ..... J..•-·-······- ····---·--------1··--·-··-·1-·--·-······· ·-··· ·--·· -··--·--1--·-···-·····--····+···
----·
•··---···-···--1-·- --/.------····---·l~------·-------1------ . +--·········· ·-·--···· ···-+----·----+----------+--·-------------1
·-f---
1----··•-•i-••-···-·--------t----1-···-···-···--·--·- ---+------ , ____ ····---···· ---······1 ··-········-·····------·-1·····---···-··-····· f--------+--------------1-----------1
1-----,-.-------------l---+---~~-·-·--···· . ----1--- ··-+-
0139
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations Printed: 7/10/2018 12:14 PM
Page 3 of 3 Work Order: 18-06097-ThlSO-1
~ 11 "' Fraction
~H1 c: I 02 ::, ~
a:: I • • 03 -
Nuclide : Sample I ~SC
TH-230 LCS I
TH-230 i MBL I TH-230
r-ou;-J.
04 TH-230 DO
Counting DatefTime
07/10/18 08:04
07/10/18 08:04
07/10/18 08:04 -------··--·-------
07/10/18 08:04
Halflife (days)
--~--
Detect
A_Spec
A_Spec
A_Spec
A_Spec
~' 0 I - - . -- , ___ ·---------- ···--t-···---···----· . I-···
u U) ,!!! ~ -ii .c:
I-
1--··-·--•-··---- ····--1-·······- -···l-····-·-····- ··-----+-- ···--··-····· +-
l-----+----------------+---------1----
1-----J··-···-· ----· +-··-· +······-· - --~----- -->-------- --)---
,, _____ ,.. _______ ··f-··--1-···---·-··--·-···· --r---------j·········-··
1----+------ 1---····-1··--·····-······-·· · ----+---- ···+
l--·--·1------- f·--···--1-··-···-·- -··- ·--···---t---- ·····-····I·····-···-
Carrier Count I Counts 8kg
Time CPM Eff
Alpha_003 170 2.57 E+02 5.00 E-03 15.9
----
Alpha_004 170 3.96 E+00 1.20 E-02 18.5
---··· --·+ . Alpha_010 170.02 1.18 E+01 i1.oo E-03 18.4
I -·
Alpha_011 170.02 1.18 E+01 !1.00 E-03 19.5
+·--·-··-·--l .. ··--····+----···-·--·······~-······-· -----1
- ______ ..J ______ _,
·-·· +·--··-·--1 --1---- ··-'- ·······--··---1 -------1
···-l-·····-·····---·I· ---+----· -·, I
1--····-·+·--··· ------j ···-··· ·1---····-· .. ···-1·····-····--· +··-- -·-1-·--··--t------+------1
1/) C 0 1----······-····--· +---- ··-·-+·-·······-···-·-·I-·-··· ········--·····-1·-······-·+-·-··-·---+------+------1
.!!? 0 a,
----•l--•··--1--·· · -·-····-·····-·--··1-·--·--·------·· ···· I··· ····1·· ····---·-f-····-···-···'------C--- ---t-----1
C ca IL .. +-····--1··-·-···---··--· · -·· ---1----···---·····-I····-·· · ······--·····1-----j
.... ~I C
a, E C
1------<-·--------1--··--·11------ ----·-!---·--·----· ···I-···--·· ..
0 ... > C w 0 ~
1----•-l-••· ----+ -····-·· -----<----- +----·--
<(
0140
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 1 of 3
;: Lab Fraction
01
Nuclide I Sample Client I Activity
Desc Identification I Units
TH-232 ~LCS LCS pCi/1
Results I Error Estimate, MDA LCS
Known
LCS
%R
5.76E+00[ 1.18E+001 1.44E-01[ 4.87E+00I 118.34 I
LCS Flag
OK
RPO Flag
MDA Flag
OK
Blank Flag
c:: :::i ll::
a, ,:, 0 0 .!!,!
i 111 c:: ct
... ~
---·-
02 T"'"
I I 03
----- -------------·---·-·- - ----- ----~---
TH-232 MBL BLANK pCi/I -- --·-·-------- -··---·----
TH-232 I DUP I OU-1-007 Outfall 007 DIS pCi/I -·--
3.73E-021 --;_;;;.02\ 8.76E~; l
2.s2E-02l_4_.3_sE_-o~J __ 1~oiE:o~--- i------+----~---
04 0
TH-232 I DO I OU-1-007 Outfall 007 DIS pCi/I 1.90E-02 s.21 E-02! 1.07E-01 I --+--·-----·-------,- -- ------·--------·1 ----- ---+----t----J,
I
u, -.I:. 1-- I 1----- ---·
- -,---·-·-----··---····+-----1----- ----+------ - -----!-·---·---- -1---
···-- -- -------t---------- ----·---\-----~---- ···----j---·- I
··----·/---
-----
1------ ----+------ ----+--- 1---- -----··--·-------·----- ···----• -··----···---
(/) C: 0 I 1--- ---+-- --
.~ (.) Cl)
C
.5 C:
-----
------------ -·----··--- ----·-····-- -------·
-----·- ---- ----+·--- -·---·-··-·---1 ·····--···-- --------1-----~-·---------+----
-----+-----
-OK OK
-·7---
NA I OK
OK
Cl)
E ---·- --1------···-···-·---·-r----~----- --·----r--------1------t--------,f------1-----1------1
C: 0 ... '> C: w 0 ~ <(
----·--1 ----------·------+--- -!---------- ·--------,------
0141
C: ::3 a:
.g 0 u
Eberline Analytical Oak Ridge Laboratory
~ ~ ~
Lab Fraction
01
02
03
04
Nuclide
TH-232 ·---
TH-232
TH-232
TH-232
I Sample
! Desc
LCS
MBL ------
DUP
-----·- -··· ---·--
DO
0 en -------~---··-----~- --------- ..
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1
Sample Sample Radiometric Grav I Mean I SAF Date Aliquot % Rec % Rec I % Rec I
06/21/18 00:00 1.00E+00 65.13 0.00 0.00
------ --f-.-.-------·- -
06/21/18 00:00 1.00E+00 107.62 0.00
--1--=-----~-------·
06/20/18 10:00 1.00E+00 114.43[ 0.00 0.00
-- ------------~- ----~------·----- ----~ - --I
06/20/18 10:00 1.00E+00 92.941 0.00 0.00
-··----·----~--- --------·----- --
,!!! ----- - -- -- ·---- - --- --·· -------------- ~-----~-- !---·---------·- . . --- --·------- ---------·------·- --~----
~ "' C: c:t
~
~
-.c I-
1/) C 0
.!!? c., Q)
C
J9 C Q)
E C 0 ... > C w 0 :E <(
~------·--
-~------·--
---------- - ----------
···--·--
-----·---
------·--·
··-~-- -·-·---
-·-·--····- ---------·--
---·-··---------·-- -·-··-·-··-
---- ---------
--'----··----····-
--·-
·-~-------·-·
·----•-.------~--- ---·-
------
. -- ·-·-- -· ---·----··-··
--·--~------
-··----··-
---- ---· --·--------·---
·----··--- ·-- ------- -----
--·--------
--····-- -··---- ·------··-- ··--·-····--
----·-------- ----------------
·-·---- ----·----- -·
.. -·-···--···---··---------
-------
------- ·-----~-~--··--~---------
··----·----- !-·------------ ----- --
- -- - ----· -·- -- ---· ··------·-·---·---
·------···-··-------
.... ----···---------- . --·--------------------
-----···
i ·--------•-,-- - --,--- ·-----·-·------··· - ----- -·----- ------------ ·-------~---
--···------···~ --·-----··--·-··- - -- ······-- ------- --·-- ----··--- ···------·----···-- ---···-----·-
---·-·--------- ----------------- ----- ·- ----- ------·-···--- --··---------
------------··~·····------- --------··-·-----··--···-·- 1---,---------·-----·•-I---
---------· ------------- --·-·-- ----.----
·----- I---·-··--------
~---~-- ·---- ·------·-- .. -·- - -·-· ··----------~----~--
-------···----·-- -···--·~-·---- ------~---
: I
I i
Printed: 7/10/2018 12:14 PM Page 2 of 3
Sep tO Sep 11 Date/Time Date/Time
-~
I ! - -------------
-·-----·-··--~---·-
--------
------ I
--------
0142
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-ThlSO-1 Printed: 7/10/2018 12:14 PM
Page 3 of 3
( Lab i Nuclide I Sample I Counting
Fraction I Desc Dateffime
01 I TH-232 I LCS I 07/10/18 08:04
Halflife (days)
Detect Carrier
A_Spec I Alpha_003
Count Time
Counts 8kg CPM
170)2.25 E+02 [4.00 E-03
-+-- ---- - -! -i
Eff
15.9
C: :::i ll::
G> 1:l 0 0 .!/? ~ Ill C: C(
~
~
~
0 en -.c I-
U) C 0
.!!1 0 Cl)
C
Jg C Cl)
E C 0 ... ·s; C w 0 :E <(
·----\-.
02 I TH-232 I MBL I 07/10/18 08:04 A_Spec Alpha_004 170\ 2.81 E+00 [7.00 E-03 18.5
-----1--··--·-----·---·---r·-·--~-----··-r-----·-·-11----···- --",-----1------'
03 TH-232 I DUP I 07/10/18 08:04
-
04 TH-232 ! DO I 07/10/18 08:04
170.02 [ 2.32 E+00 \ 4.00 E-03
·----+----+I ;
110.02/1.3~ E+oo koo E-02
A_Spec
A_Spec
Alpha_010
Alpha_011
18.4
19.5
--···-----····
1----- i
--f-
----+-----1 i .. I
---+--· .. ---.. , ... _ .... +---·----+---
. --··· r-------·- -----· --·-·-+·-----·-- _ __, ___ ___, ·--·-··--·--------+------1--------1
1----,---- .. --·--+-.. --1--· .. -
1--.. --- -------.. ---1 --+------+-.. - · .... -•,
---.. ----... -1 .. -·
-~---------+-··· --------+
... --.. ------l--·------1----------+ ... - ... ---·----.... - - .. I .. - .. ---. - ........ -1------------+ .. -- ·------+ ...... __ ........ -+
------,---~.--------------~--~-------- --··· ..... -,------+-- ·-+-----
0143
>.\ '17
Count Room Report Client: AMO Environmental Decisio
Internal Sample Client I
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-007 Outfall 007 DIS
04 DO OU-1-007 Outfall 007 DIS
I
18-06097-ThlSO-1 (pCi/1) in WA Tracer ID: Th-18a
Sample I Sample Tracer
Date Aliquot Aliquot (g)
06/21/18 00:00 1.0000 0.4656
06/21/18 00:00 1.0000 0.2332
06/20/18 10:00 1.0000 0.2319
06/20/18 10:00 1.0000 0.2310
Tracer ACT(dpm)
10.4574
5.2377
5.2085
5.1883
I Radiometric Tracer (pCi)
I
Printed: 7/10/2018 4:41 AM Page 1 of 1
I Radiometric SAF SAF . %Rec 1* 2* I
0.00 I
I
0.00
0.00
0.00
0144
Eberline Analytical
Oak Ridge Laboratory
Isotope So/# Activity dpm/g
Th-228 Th-8b 103.560
Th-230 Th-1b 23.520
Th-232 Th-8b 103.560
fraction I Isotope Sol#
01 Th-229 Th-18a
02 Th-229 Th-18a
03 Th-229 Th-18a
04 Th-229 Th-18a
Version 2.0 08/99
Solution I Approx Date I Addition
7/6/2018/ 0.100
11612018 I 0.500
7/6/20181 0.100
Tracers Activity I Solution dpmlg / Date
22.4601 7/6/2018
22.460 7/6/2018
22.460 7/6/2018
22.460 7/6/2018
i I I
Spike and Tracer Worksheet
Analysis Code Date
ThlSO 7/6/2018 7:19
LCS MS LCSD MSD LCS
Volume Volume Volume Volume Known I
Technician
JHARVEY
MS Error Added I Error
Page 1 of 1
Printed: 7/6/2018 7:25 AM
Witness Initials
--
Leso· -----
""""lVISD Known I Error Added Error
Used(g) Used(g) Used(g) Used(g) I
pCi i Estimate pCi I Estimate pCi ; Estimate pCi I Estimate I
0.1044 4.81I 0.175 o.ool 0.000 o oo/ 0.000 0.00 I
0.000
0.5078 o.ool I
5.38] 0.145 0.000 0 001 0.000 0.00 0.000
0.1044 4.81I 0.175 I
0.00! I
0.000 o.oo[ 0.000 0.00 0.000 - - -
Balance Printer Tapes
Volume Approx Tracer LCS Used(g) Addition
0.4656 0.2200
0.2332 0.2200
0.2319 0.2200
0.2310 0.2200
Matrix Spike
I
0145
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-007 Outfall 007 DIS
04 OU-1-007 Outfall 007 DIS
Comments
Sample
Type
LCS
MBL
DUP
DO
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
ThlSO liters 7/11/2018
Muffle Data Dilution Data Aliquot Data
Ratio Post/Pre No of Dils Oil Factor Ratio Aliquot Net Equiv
i 1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
Teohoiciao ~~~Date ~£12
Technician
JHARVEY
MS Aliquot Data
Aliquot Net Equiv
Printed: 7/6/2018 9:38 AM Page 1 of 1
H-3 Solids Only WaterAaaea N:ruIsr
(ml) Aliq
0146
Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167
1806097A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 Th iso
Alpha_003
3 System Bkgd 219019
<not performed>
1.000E+000 +!- 0.000E+000 7/10/2018 5:43:45 7/10/2018 8:04:56
170.0 minutes 170.0 minutes
Th229 S TH-18A 0.466 rnL 0.1036 +/- 0.0083
AM AM
liter
Counting Efficiency: 0.1591 +/- 0.0028 on 2/16/2018 0.6513 +/- 0.0536
3:44:29 PM
Chern. Recovery Factor:
Control Certificate Name: NatTh Th-8 Chern. Recov. of Control: TH-232 1.183360 +/- 0.128602
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.830 5.384 4.874 4.626 3.955
0.175 MeV
PEAK AREA REPORT
Net Pk Area
6 .13 227.30 184 .13 257.15 225.32
Pk Area Error%
92.21 13. 06 14.53 12.25 13. 08
Ambient Backgnd
1. 87 1. 70 1. 87 0.85 0.68
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 9.2 6.2 4.4 4.6
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.998 0.999 1.000 0.989 0.991
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter)
1.61E-001 +/- 1.50E-001 5.82E+000 +/- 1.19E+000 4.73E+000 +!- 7.45E-001 6.59E+000 +!- l.31E+000 5.76E+000 +/- 1.18E+000
~ 1/rrfrs
MDA (pCi/liter
1. 99E-001 +!- 3.13E-002 1.88E-001 +/- 2. 96E- 002 1.95E-001 +/- 3.07E-002 1.53E-001 +!- 2.42E-002 1.44E-001 +!- 2.27E-002
0147
Vl .µ C ~
60
55
50
45
40
35
0000216763.CNF
Live Time :10200.000 sec Real Time :10200.000 sec Start: 1:3496.6(kev) Stop : 1024:6544.G(kev) Acq. start :Tue Jul 10 08:04:56 2018
8 30
25
20
15
10
5
0 ITT" w I Mm 1m1 1111 1 1 1 , " . M 1 11 'I ! 1M! ! M!IW]OHM!r-l!jf', , , ·· .. "·. ' 1
: j 11 / 111' j I 1 , ii'. , ·•··1,wl''' ,1 • l 3 500 \! "' ·· ,Jii: i!, , 1 rnimmw:1 rn 1 1 ·. 1~ 1 1111 AMijflli.' , 1, . . . 1 I II ,MH!1! ! Mlj)lill Ml I I ~
4000
ROI Type: 1
4500 5000 Energy(kev)
5500 6000 6500
ROI Type: 3
0148
Channel Data Report 7/10/2018 10:59:26 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200
Elapsed Real Time: 10200
Channel\------l-------1-------1-------1-------I-------I-------I-------I
1 : 10200 10200 0 0 0 1 0 0
9 : 0 0 0 0 0 0 0 0
17: 1 0 0 0 0 0 1 0
25: 0 0 0 1 0 0 0 0
33: 0 0 1 0 0 0 0 0
41: 0 0 1 0 0 1 0 0
49: 1 0 0 0 1 0 1 1
57: 0 0 0 0 0 0 0 0
65: 0 0 0 1 0 0 0 0
73: 2 0 2 2 1 2 0 0
81: 0 1 1 1 1 0 0 2
89: 1 2 0 3 2 1 1 1
97: 2 3 3 2 1 0 0 3
105: 0 0 2 2 1 1 1 1
113: 3 4 2 0 2 4 3 2
121: 1 3 3 2 1 6 2 2
129: 4 2 5 4 8 3 2 5
137: 4 3 1 5 3 8 6 5
145: 5 5 4 4 7 4 5 3
153: 3 5 4 5 5 8 2 1
161: 3 5 7 7 9 2 11 5
169: 3 6 8 3 6 3 7 2
177: 1 0 1 0 0 0 0 0
185: 0 0 1 0 0 1 0 0
193: 0 0 0 0 0 1 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 1 0
217: 1 0 0 0 0 0 0 0
225: 0 0 0 1 0 0 0 0
233: 0 0 0 0 0 0 1 0
241: 1 0 0 0 0 1 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 1 0 0 0 0
265: 0 0 0 0 0 0 1 0
273: 0 0 1 1 0 0 1 0
281: 0 0 0 1 1 0 1 1
289: 0 1 2 1 1 0 1 0
297: 0 0 1 1 1 0 1 0
305: 0 0 1 0 0 0 0 1
313: 0 2 0 0 1 0 0 2
321: 1 1 1 2 0 0 1 0
329: 3 2 3 3 1 0 2 1
337: 1 0 1 2 2 1 2 2
345: 1 2 1 0 1 3 2 3
353: 2 0 3 4 1 4 2 2
361: 5 1 5 4 3 6 2 5
0149
Channel Data Report 7/10/2018 10:59:26 AM Page 2
369: 2 8 5 6 4 5 7 3
Sample Title: 01
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 4 11 3 4 5 5 6 7
385: 5 3 4 8 5 3 6 2
393: 8 8 3 8 4 6 6 9
401: 7 4 2 0 1 1 0 0
409: 3 1 2 0 0 1 3 2
417: 0 0 2 2 3 0 2 1
425: 1 0 0 1 0 1 0 3
433: 4 3 4 1 4 3 1 6
441: 3 4 7 1 4 3 0 5
449: 3 4 5 1 3 0 1 2
457: 4 3 2 1 0 1 2 5
465: 1 2 3 0 3 1 0 0
473: 1 2 3 3 0 0 0 1
481: 1 1 3 2 1 2 1 1
489: 3 2 0 0 1 1 1 1
497: 0 0 0 2 2 2 0 1
505: 1 1 0 1 0 1 2 0
513: 1 1 2 1 2 0 2 2
521: 0 0 1 0 0 2 1 2
529: 0 0 0 0 0 1 1 0
537: 1 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 1 1 0 1 1 1 2
561: 4 1 0 3 0 0 0 2
569: 1 0 3 1 2 1 0 4
577: 0 2 2 0 2 2 2 0
585: 1 0 1 1 1 2 1 4
593: 0 2 3 2 1 3 2 3
601: 0 6 1 6 4 2 0 1
609: 6 2 5 4 4 2 5 6
617: 5 7 6 3 8 5 7 4
625: 4 0 2 4 9 5 2 5
633: 11 7 6 3 4 4 9 4
641: 7 7 10 9 10 10 10 3
649: 4 8 2 3 1 1 3 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 1 0 0 0 1
673: 0 0 0 0 0 0 0 0
681: 1 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 2 0 0 0
705: 2 0 0 0 0 0 1 1
713: 0 0 1 0 0 1 1 0
721: 0 0 2 0 0 1 0 2
729: 2 1 1 1 2 1 0 0
737: 0 0 2 1 0 0 1 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 1 0
769: 0 0 0 1 0 0 0 0
777: 0 1 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 1 0 0 0 0 0 0 0
0150
Channel Data Report 7/10/2018 10:59:26 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------l-------l-------l-------1-------1-------1-------\ 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 1
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 1 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 1 0 0 0 0
881: 0 0 0 0 0 0 1 0
889: 0 0 1 0 1 0 0 0
897: 1 0 0 0 1 0 0 1
905: 0 0 0 0 0 1 0 0
913: 0 0 0 1 0 0 0 0
921: 0 0 1 0 1 0 0 0
929: 1 2 1 0 2 1 1 0
937: 0 2 2 0 2 0 0 3
945: 0 1 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 1
961: 0 0 2 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 1 0 0
0151
Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167
1806097A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 Th iso
Alpha_004
4 System Bkgd 219020
<not performed>
l.000E+000 7/10/2018 7/10/2018
170.0
+/- 0.000E+000 liter 5:43:45 AM 8:04:57 AM
minutes 170.0 minutes
Th229 S TH-18A 0.233 mL 0.1994 +/- 0.0162
Counting Efficiency: 0.1853 +/- 0.0032 on 2/16/2018 1.0762 +/- 0.0895
3:44:30 PM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.806 5.295 4.880 4.673 3.991
0.175 MeV
PEAK AREA REPORT
Net Pk Area
3.15 3.64
177.49 3. 96 2.81
Pk Area Error%
126.67 123.16
14.74 124.69 142.99
Ambient Backgnd
0.85 1. 36 0.51 2.04 1.19
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
2.9 2.9 9.3 2.9 2.9
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.990 0.944 1.000 1.000 1.000
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
4.29E-002 +/- 5.48E-002 4.84E-002 +/- 6.0lE-002 2.37E+000 +/- 3.78E-001 5.27E-002 +/- 6.63E-002 3.73E-002 +/- 5.37E-002
~ 1/ro/r5
MDA (pCi/liter
8.16E-002 +!- l.30E-002 9.12E-002 +!- l.45E-002 7.0lE-002 +!- l.12E-002 1. 04E- 001 +/- l.65E-002 8.76E-002 +/- l.40E-002
0152
Vl +-' C ~
60
55
50
45
40
35
8 30
25
20
15
10
5
0000216738.CNF
,;,~ 11 :i: i< I-
Live Time :10200.000 sec Real Time :10200.000 sec start: 1: 3488. l(kev) stop : 1024:6492.S(kev) Acq. Start :Tue Jul 10 08:04:57 2018
11 I I " I I ! ·' I 1· I 'I"' I '!"'' 'ii ''I ,,,, ' ! \ ' I I ' I ! ! l
0 ,· ,I I I• ''I•' ;1, I· ,,; I •\'I I ,'.I '. ' ' I ' I I, I I 11
3500 4000 4500 5000 5500 6000 6500 Energy(kev)
ROI Type: 1 ROI Type: 3
0153
Channel Data Report 7/10/2018 10:59:33 AM Page 1
******************************************************* ***** s p E C T R A L DAT A R E p 0 R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 10200 10200 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 1 0 0 0
153: 0 0 0 0 0 0 0 0
161: 1 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 1 1 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 1 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0154
Channel Data Report 7/10/2018 10:59:33 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channelj------l-------l-------l-------l-------1-------1-------1-------\ 377: 0 1 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 1 0 0 0 0 0 0
401: 0 0 1 0 0 0 0 0
409: 0 0 0 1 0 0 0 0
417: 0 0 1 1 0 0 0 1
425: 1 0 0 0 0 1 0 1
433: 0 0 0 0 0 1 1 2
441: 2 2 1 1 2 1 4 0
449: 3 4 1 4 3 1 2 3
457: 2 2 3 3 6 1 7 8
465: 6 3 4 1 2 1 5 1
473: 4 0 5 3 2 2 1 0
481: 1 0 1 1 0 2 3 2
489: 1 4 1 3 3 4 0 2
497: 2 2 2 1 2 1 0 2
505: 2 1 2 0 1 0 1 1
513: 0 0 1 1 2 0 0 1
521: 2 0 0 2 0 0 0 1
529: 2 0 2 0 0 0 0 0
537: 0 0 0 0 1 0 1 0
545: 0 0 0 0 0 0 0 0
553: 1 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 1 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 1 0 0 0 0 0
609: 0 0 0 0 1 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 1 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 1 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 1 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 1 0 0 0 0
793: 0 1 0 0 0 0 0 0
0155
Channel Data Report 7/10/2018 10:59:33 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 1 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 1 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 1 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0156
Sample Description: Spectrum File: Batch Identification:
OU-1-007 OUTFALL 007 DIS DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167
1806097A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
03 Shelf 2 Th iso
Alpha_0l0
10 System Bkgd 219021
<not performed>
l.000E+000 6/20/2018 7/10/2018
170.0
+/- 0.000E+000 liter 5:43:45 AM 8:04:53 AM
minutes 170.0 minutes
Th229 S TH-18A 0.232 mL 0.2106 +/- 0.0168
Counting Efficiency: 0.1841 +/- 0.0032 on 2/16/2018 1.1443 +/- 0.0933
3:44:30 PM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.934 5.438 4.882 4.656 3.965
0.175 MeV
PEAK AREA REPORT
Net Pk Area
0.32 0.15
186.49 11. 83
2.32
Pk Area Error%
647.08 1398. 6
14.38 57.46
149.13
Ambient Backgnd
0.68 0.85 0.51 0.17 0.68
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
2.9 2.9 5.1 2.9 2.9
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.964 0.992 1.000 0.999 0.995
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter)
4 .13E- 003 +!- 2.68E-002 1. 92E-003 +/- 2.69E-002 2.36E+000 +/- 3.68E-001 1. 49E-001 +!- 8.88E-002 2.92E-002 +!- 4.38E-002
M 1/1oft
MDA (pCi/liter
7.29E-002 +!- l.14E-002 7.69E-002 +/- l.20E-002 6.63E-002 +/- l.04E-002 5.26E-002 +!- 8.21E-003 7.09E-002 +!- 1.llE-002
0157
V)
-1-' C ~
45
35
8 30
25
20
15
10
5
0000216739.CNF
0 11 ' , II
4000
ROI Type: 1
4500 5000 Energy(kev)
5500
Live Time :10201.000 sec Real Time :10201.000 sec start: 1:3509.l(kev) Stop : 1024: 6494. 5 (keV) Acq. Start :Tue Jul 10 08:04:53 2018
6000
ROI Type: 3
6500
0158
Channel Data Report 7/10/2018 10:59:40 AM Page 1
*******************************************************
***** s p E C T R A L DAT A R E p 0 R T *****
*******************************************************
Sample Title: 03
Elapsed Live time: 10201 Elapsed Real Time: 10201
Channell------l-------l-------1-------1-------1-------I-------I-------I 1: 10201 10201 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 1 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 1 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 1 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 1
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 1 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 1 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 1 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0159
Channel Data Report 7/10/2018 10:59:40 AM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------l-------1-------1-------1-------\
377: 0 0 0 1 0 0 0 0
385: 0 1 1 0 0 0 1 0
393: 0 0 1 0 1 0 0 0
401: 0 1 0 0 0 0 0 1
409: 0 0 1 0 0 2 0 0
417: 0 0 1 1 0 1 0 0
425: 0 1 0 0 1 1 0 0
433: 2 3 3 0 0 2 1 1
441: 2 2 3 1 1 5 2 6
449: 3 0 5 5 3 3 4 0
457: 5 5 3 1 3 2 2 3
465: 5 1 0 4 3 2 1 2
473: 2 2 1 3 4 2 6 1
481: 0 1 4 3 2 1 2 4
489: 0 2 3 0 3 1 4 1
497: 1 0 0 1 0 0 0 0
505: 0 1 2 1 2 3 1 0
513: 1 2 2 0 2 0 0 0
521: 1 0 0 1 0 0 1 1
529: 0 1 1 0 1 0 0 0
537: 0 0 1 2 1 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 1 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 1 0 0
665: 0 0 0 0 0 0 0 1
673: 0 0 0 0 0 0 1 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 1 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 1 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0160
Channel Data Report 7/10/2018 10:59:40 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channel\------l-------l-------l-------l-------1-------1-------1-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 1
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 1 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 1 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 1 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0161
Sample Description: Spectrum File: Batch Identification:
OU-1-007 OUTFALL 007 DIS \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002167
1806097A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
04 Shelf 2 Th iso
Alpha_0ll
11 System Bkgd 219022
<not performed>
l.000E+000 6/20/2018 7/10/2018
170.0
+/- 0.000E+000 liter 5:43:45 AM 8:04:55 AM
minutes 170.0 minutes
0.0155
Counting Efficiency:
Th229 S TH-18A 0.231 mL 0.1812 +/-0.1950 +/-0.9294 +/-
0.0034 on 2/16/2018 0.0809
3:44:30 PM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.869 5.285 4.883 4.616 3.930
0.175 MeV
PEAK AREA REPORT
Net Pk Area
2.47 3.79
159.81 11.81
1. 30
Pk Area Error%
163.79 130.59
15.57 60.30
273.47
Ambient Backgnd
1. 53 2.21 1.19 1.19 1.70
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
2.6 2.6 5.5 2.6 2.6
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.998 0.933 0.999 0.984 0.977
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/liter )
3.71E-002 +/- 6.llE-002 5.66E-002 +!- 7.45E-002 2.35E+000 +!- 3.92E-001 l.73E-001 +/- l.08E-001 l.90E-002 +/- 5.21E-002
1ro1(t,
MDA (pCi/liter
l.07E-001 +!- 1. 78E-002 l.19E-001 +!- 1. 99E-002 9.68E-002 +!- 1. 62E-002 9.65E-002 +!- 1.61E-002 l.07E-001 +/- l.80E-002
0162
V)
+-' C: :::::i
60
55
50
45
40
35
8 30
25
20
15
10
5
0000216740.CNF
I I
0 ,I ,, '"
4000
ROI Type: 1
' 4500 5000
Energy(kev) 5500
Live Time :10201.000 sec Real Time :10201.000 sec Start: 1:3638.?(kev) Stop : 1024:6325.9(keV) Acq. Start :Tue Jul 10 08:04:55 2018
6000
ROI Type: 3
0163
Channel Data Report 7/10/2018 10:59:48 AM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10201 Elapsed Real Time: 10201
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 10201 10201 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 1 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 1 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 1
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 1 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 1 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 1 0
313: 0 0 0 0 0 0 0 1
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 1 0 1 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 1 0 0
0164
Channel Data Report 7/10/2018 10:59:48 AM Page 2
369: 0 0 1 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 1 0 1
393: 0 0 0 0 0 0 1 1
401: 0 3 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 1
417: 0 0 0 0 1 0 0 0
425: 0 1 0 0 0 0 2 0
433: 1 1 0 1 2 1 1 1
441: 1 3 0 0 3 4 4 2
449: 1 1 1 0 2 1 0 8
457: 7 2 4 7 4 2 1 1
465: 1 6 1 3 2 1 5 1
473: 1 1 3 3 1 3 2 0
481: 3 2 3 0 1 0 2 2
489: 0 1 1 0 0 0 2 1
497: 1 0 0 1 1 0 0 1
505: 0 1 3 1 1 2 0 1
513: 1 0 0 0 2 2 0 0
521: 2 1 1 0 1 0 1 1
529: 1 1 1 1 2 0 1 1
537: 1 0 1 1 0 1 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 1 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 1 0 0 0 0
585: 0 0 0 1 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 1 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 1 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 1 1 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 1 0 0 0 0 0 0 0
785: 0 0 0 1 0 0 0 1
793: 0 0 0 0 0 0 0 0
0165
Channel Data Report 7/10/2018 10:59:48 AM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channel\------\-------\-------\-------\-------\-------\-------\-------1 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 1 0 0 0 0 0 0
913: 0 0 1 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 1 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 1
1001: 0 0 1 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0166
Page 1 of 2 7/10/2018 5:36:53 AM
ex-Al r'\ l\ Cl II\ 111\ 111\ DV DCDnDT ~n \JVIVIIVlr\l \ I I \'-I ~,\I
Review Of QA Results - Pulser Check
Date : 7/10/2018 Time : 5:36:53 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 001 2lf ALL Not Done
Alpha 002 2lf ALL Not Done
Alpha 003 2lf ALL Passed 7/10/2018 5:16:04 AM
Alpha 004 2lf ALL Passed 7/10/2018 5:16:05 AM
Alpha 005 2lf ALL Not Done
Alpha 006 2lf ALL Not Done
Alpha 007 2lf ALL Not Done
Alpha 008 2lf ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 2lf ALL Passed 7/10/2018 5:16:06 AM
Alpha 011 2lf ALL Passed 7/10/2018 5:16:07 AM
Alpha 012 2lf ALL Passed 7/10/2018 5:16:08 AM
Alpha 013 2lf ALL Not Done
Alpha 014 2lf ALL Passed 7/10/2018 5:16:09 AM
Alpha 015 2lf ALL Not Done
Alpha 016 2lf ALL Not Done
Alpha 033 Alpha Analystl00DC Peak Energy Action 7/10/2018 5:16:10 AM
Alpha 034 Alpha Analystl00DC ALL Not Done
Alpha 035 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:11 AM
Alpha 036 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:13 AM
Alpha 037 Alpha Analystl 00DC ALL Not Done
Alpha 038 Alpha Analyst 1 00DC ALL Not Done
Alpha 039 Alpha Analystl00DC PeakFWHM Action 7/10/2018 5:16:14 AM
Alpha 040 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:16 AM
Alpha 041 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:17 AM
Alpha 042 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:19 AM
Alpha 043 Alpha Analystl00DC ALL Not Done
Alpha 044 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:20 AM
Alpha 045 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:22 AM
Alpha 046 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:23 AM
Alpha 047 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:25 AM
Alpha 048 Alpha Analyst 1 00DC ALL Passed 7/10/2018 5:16:27 AM
Alpha 049 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:28 AM
Alpha 050 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:31 AM
Alpha 051 Alpha Analystl00DC ALL Not Done
Alpha 052 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:33 AM
Alpha 053 Alpha Analystl00DC PeakFWHM Action 7/10/2018 5:16:35 AM
Alpha 054 Alpha Analyst! 00DC ALL Not Done
Alpha 055 Alpha Analystl00DC ALL Not Done
Alpha 056 Alpha AnalystlO0DC ALL Passed 7/10/2018 5:16:37 AM
Alpha 057 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:39 AM
Alpha 058 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:41 AM
0167
Page 2 of 2 Kev1ew OT UA KeSUltS - t-'UISer GnecK
7/10/2018 5:36:53 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha Analystl00DC ALL Passed 7/10/2018 5:16:44 AM
Alpha 060 Alpha Analystl 00DC ALL Passed 7/10/2018 5:16:47 AM
APPROVED BY:
APPROVAL DATE: ·+/lo/t8
0168
Library Listing Report 6/12/12 12:16:29 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Thorium
Nuclide Library Description: Th-227,-228,-229,-230,-232
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV ( % ) Uncert. (Abs.+-)
TH-227 6.873E+008 5850.000* 0.000 97.5000 0.0000
TH-228 6.034E+007 5400.000* 0.000 99.9400 0.0000
TH-229 2.487E+Oll 4872.000* 0.000 99.5200 0.0000
TH-230 2.379E+012 4672.000* 0.000 99.8200 0.0000
TH-232 4.434E+017 3997.000* 0.000 100.0000 0.0000
* = key line
TOTALS: 5 Nuclides 5 Energy Lines
0170
Eberline Services Oak Ridge Laboratory Analysis Sheet
Work Order
Analysis Code
Run
Date Received
Lab Deadline
18-06097
Ra226 I 1
6/21/2018
7/11/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 903.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer Ba-133
Radiometric Sol# Ba-6a
Tracer Act (dpm/g) 480.67
Carrier
Carrier Cone (mg/ml)
Internal Sample I Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
!
18-06097 Ra226 Run 1
Client ID
LCS
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Login CPM
30
30
Printed: 7/9/2018 2:36 PM Page 1 of 3
Sample i Sample
Date I
Aliquot
06/21/18 00:00 1.0000E+00
06/21/18 00:00 1.0000E+00
06/20/18 10:00 1.0000E+00
06/20/18 10:00 1.0000E+00
i
I I
0171
Eberline Services Oak Ridge Laboratory Analysis Sheet
Internal Sample Tracer Fraction Desc Aliquot (g)
01 LCS 2.2121
02 MBL 2.2067
03 DUP 2.2113
04 DO 2.2115
Tracer Total ACT(dpm)
1063.3
1060.7
1062.9
1063.0
Radiometric Radiometric Tracer (pCi) %Rec
655.0 136.75
658.0 137.72
584.0 121.98
621.0 129.69
18-06097 Ra226 Run 1
Grav Carrier Grav Filter Added(ml) Tare (g)
0.0208
0.0210
0.0212
0.0215
Grav Filter Final (g)
0.0308
0.0315
0.0288
0.0292
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Grav Filter Grav
I Net(g) %Rec
0.0100
0.0105
0.0076
0.0077
Printed: 71912018 2:36 PM Page 2 of 3
Mean SAF SAF
%Rec 1* 2*
110.00 3.00" 1.00
110.00 3.00" 1.00
110.00 2.66 1.00
110.00 2.69 1.00
0172
Eberline Services Oak Ridge Laboratory Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Date
Rough Prep Prep By Date
07/06/18 07:18
07/06/18 07:18
07/06/18 07:18
07/06/18 07:18
18-06097 Ra226 Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
Sep to Date/Time
07 /09/18 12:48
07/09/18 12:48
07/09/18 12:48
07 /09/18 12:48
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep to
I By
JBAILEY
JBAILEY
JBAILEY
JBAILEY
Printed: 71912018 2:36 PM Page 3 of 3
Sep t1 Sep t1 Date/Time By
0173
Eberline Analytical
Oak Ridge Laboratory
~ ®
C: ::i a::
i 0 0 ,!!! ~ 'iij C: ct
-~
~
(D N N ca a::
ti) C: .2 .!!? (.) Q)
C cu -C: Q)
E C: 0 ... ·s; C: w 0 :ii: <(
Lab Nuclide Fraction
01 RA-226
-----
02 RA-226
03 RA-226
--------·
04 RA-226
~--·--------·
--
-·----
-·--··--·
Sample Desc
LCS
MBL -----·-
DUP r·---·
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-Ra226-1
Client Activity
I Results I Error Estimate MDA Identification Units i
I
LCS pCi/I 1.01E+01 j 1.37E+00 2.87E-01 !
--·· "---•-··---- - -----·-· .. T
BLANK pCi/I -6.23E-02 1 1.0SE-01 3.70E-01
----- " -·-· - ---·---·---··-----· --
OU-1-007 Outfall 007 DIS pCi/I 3.81E-01 2.99E-01 3.78E-01
----· - -------
OU-1-007 Outfall 007 DIS pCi/I 1.02E-01 2.13E-01 4.0SE-01
··--------- - --------··-·--
---------· --·- . ---- -- -------
------- ----------------- ---·------ ------····-~---- ---~--- -
---·-------.. r
' -·--·-··----···
·-----· ----
--------~-
·-·--···---~-
---~·-· --
-----
-
LCS LCS
Known %R
1.00E+01 100.62 ,
'
i I
Printed: 7/10/2018 7:19 AM Page 1 of 3
LCS RPD MDA
I Blank
Flag Flag Flag Flag
OK OK
OK OK
NA OK
OK
0174
C:
&!
~ 0 0 .!!,!
~ iii C: ct
II
Eberline Analytical
Oak Ridge Laboratory
~
(0 N N ca a::
1/) C: .Q .!!! (.) Cl)
C C'a ...... C: Cl)
E C: 0 ... > C: w 0 :E <(
Lab Fraction
01 -------~-
02
03
04
----
----
---··
Nuclide
RA-226 ------
RA-226
RA-226
RA-226 --·----···---·· - -------~-
---------·-·-
---------
---------··----
r----------------··
---------~-
--------·------------
---~-----
·-
Sample Desc
LCS
MBL
DUP
DO -------
-----
---·-----
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-Ra226-1
Sample I Sample Radiometric Grav
I Mean
Date I Aliquot %Rec % Rec %Rec
06/21/18 00:00 1.ooE+ooi 100.00 0.00 110.001
- ---- ---
06/21/18 00:00 1.ooE+ooi 100.00 0.00 i
110.001 i
"---7---···---· i.
06/20/18 10:00 1.ooE+ooi 100.00 0.00 110.00!
·+ L-
06/20/18 10:00 1.00E+00! 100.00 0.00 110.00
··r-·· i I ····1 I
--=-=l--------- ~----
··- ---- --------
-----·-- ·-· -------~--·-------.
-···-- ···--·- ·---···---~--
I .
---··---·-
-----·--------
-------- ·-----
---·--
SAF I i I
I I
Printed: 7/10/2018 7: 19 AM Page 2 of 3
Sep to I
Sep t1
Date/Time Date/Time
7/9/2018 12:48 ·------ -···----
7/9/2018 12:48 ··---------- -
7/9/2018 12:48 ----- -------
7/9/2018 12:48
----·--·--
-------
0175
Eberline Analytical Oak Ridge Laboratory
~ ~
§ a:: """"
GI (0 "O 0 N 0 .!!! N £ ns cu a:: c:: ct
... ~ 0 -l: ~ oi u
i .. C: <( ., .s 1:: ., fil -~
fl) C 0 'iii ·c:; Q)
C ta -!I C Q)
E C 0 ... ·s; C w 0 :E <(
Lab
I Nuclide Fraction
01 RA-226
02 RA-226
03 RA-226
04 RA-226
--
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-Ra226-1
Sample Counting Halflife Detect i Carrier Count
Desc Date/Time (days) I Time Counts
LCS 07/09/18 14:44 A_Spec [Alpha_047 170 2.21 E+02 i
~--.. ·--- "·----- -
MBL 07/09/18 14:44 A_Spec Alpha_048 170 -1.38 E+00
-------- .. ----
DUP 07/09/18 14:44 A_Spec Alpha_049 170 8.45 E+00
----·-~---- _.. ________
DO 07/09/18 14:44 A_Spec Alpha_oso 170 1.96 E+00
__ ,. __ ' ...
- ··---------- --~- --·-·--· --------------
------·----·-
--------
---···------· -·--
·-----·-·- -----
---~-- -----------
-~----- . -----------~--··--
·--~----·
·--- -··--··---·---
------
·-------
Bkg CPM
6.00 E-03
1.40 E-02
1.50 E-02
1.20 E-02
Printed: 7/10/2018 7:19 AM Page 3 of 3
Eff
17.4
17.6
15.6
13.7
0176
Count Room Report Client: AMO Environmental Decisio
Internal Sample I
Client Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-007 Outfall 007 DIS
04 DO OU-1-007 Outfall 007 DIS
18-06097-Ra226-1 (pCi/I) in WA Tracer ID: Ba-6a
Sample Sample
I Tracer
Date Aliquot Aliquot (g)
06/21/18 00:00 1.0000 2.2121
06/21/18 00:00 1.0000 2.2067
06/20/18 10:00 1.0000 2.2113
06/20/18 10:00 1.0000 2.2115
Tracer Radiometric ACT(dpm) Tracer (pCi)
1063.2901 655.0000 I
1060.6945 658.0000
1062.9056 584.0000
1063.0017 621.0000
Printed: 7/9/2018 2:36 PM Page 1 of 1
Radiometric SAF SAF ¾Rec 1· 2·
136.75 3.00A 1.00
137.72 3.00A 1.00
121.98 2.66 1.00
129.69 2.69 1.00
I
0177
Eberline Analytical
Oak Ridge Laboratory
LCS & Matrix Spikes
Isotope So/#
Ra-226 Ra-Sb
fraction I Isotope
01 Ba-133
02 Ba-133
03 Ba-133
04 Ba-133
Version 2.0 08/99
Activity dpm/g
43.970
So/#
Ba-6a
Ba-6a
Ba-6a
Ba-6a
Solution Date
7/6/2018
Tracers Activity dpmlg
480.670
480.670
480.670
480.670
Approx Addition
0.500
Solution Date
7/6/2018
7/6/2018
7/6/2018
7/6/2018
Spike and Tracer Worksheet
Analysis Code
Ra226 LCS
Volume Used (g)
0.5054
Volume Used (g)
2.2121
2.2067
2.2113
2.2115
MS Volume Used(g)
Approx Addition
2.1100
2.1100
2.1100
2.1100
Date
7/6/2018 7:01
LCSD Volume Used(g)
MSD Volume Used (g)
Technician
JHARVEY
LCS MS Known
pCi
10.01
Tracer
Error Estimate
0.460
Added pCi
0.00
Error Estimate
0.000
Balance Printer Tapes
Page 1 of 1
Printed: 7/6/2018 7:18 AM
Witness Initials
MSD Known i Error Added Error
pCi Estimate pCi Estimate
o.ool 0.000 0.00 0.000
LCS
Matrix Spike
0178
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-007 Outfall 007 DIS
04 OU-1-007 Outfall 007 DIS
Comments
Sample
Type
LCS
MBL
DUP
DO
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
Ra226 liters 7/11/2018
Muffle Data Dilution Data Aliquot Data
Ratio Post/Pre Noof Dils Dil Factor Ratio Aliquot Net Equiv
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
Technician d-~e~oare '-4-, m
Technician
JHARVEY
MS Aliquot Data
Aliquot Net Equiv
Printed: 7/6/2018 9:36 AM Page 1 of 1
H-3 Solids Only wa tefA<Rlecr-1 3u1st-
(ml) , Aliq
0179
Eberline Analytical - Oak Ridge Version 1.1 10/2015
Work Order
TRetec AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 DUP
04 OU-1-007 Outfall 007 DIS
/""\.
Technician: t;,'1,-f'l o/ '(jl I \
Sample
Type
LCS MBL
DUP DO
Gravimetric Worksheet
Analysis Code
Ra226
Carrier Data
Gravimetric Carrier
Filter Data Carrier Added Filter Tare Filter Final
(ml) (g) (g)
0.0208 0.0308
0.0210 0.0315 0.0212 0.0288 0.0215 0.0292
..,....1 (\
,1 'JI 1v Date: _1_/ __ I _/.J..LL_
Carrier Cone (mg/ml)
Filter Net (g)
0.0100 0.0105
0.0076
0.0077
Printed: 7/9/2018 1 :45 PM Page 1 of 1
Technician
JBAILEY
Gravimetric %
Recovery
0180
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
SPIKE \\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00002166 1806097A-RA 01 Shelf 2 Ra
Alpha_047 10006125A 91086 System Bkgd 219035
<not performed>
l.000E+000 +/- 0.000E+000 liter 3.000E+000 7/9/2018 7/9/2018
Generic Div. Factor: 2:09:31 PM 2:44:04 PM
170.0 minutes 170.0 minutes
1.0000 +/- 0.0000 0.1744 +/- 0.0030 on 6/6/2018 0.1744 +/- 0.0030
l.000E+000
2:37:41 PM
Control Certificate Name: Ra226 Ra-Sb Chem. Recov. of Control: RA-226 0.335357 +/- 0.025425 Peak Match Tolerance: 0.350 MeV
Nuclide
RA-224 RA-226
Nuclide
RA-224 RA-226
Energy (MeV)
Id Conf.
5.471 4.585
PEAK AREA REPORT
Net Pk Area
5.47 220.98
Pk Area Error%
96. 55 13. 22
Ambient Backgnd
1. 53 1. 02
NUCLIDE ANALYSIS RESULTS
Energy (keV)
Activity (pCi/liter )
0.942 0.949
5685.50* 4785.00*
2.62E-001 +/- 2.53E-001 l.0lE+00l +/- l.37E+000
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
MDA
3.0 4.4
(pCi/liter
3.41E-001 +/- l.lSE-002 2.87E-001 +/- 9.72E-003
0181
60
55
50
45
40
35 Vl .j-J s::: ::::s
8 30
25
20
15
10
5
0 I
3500
ROI Type: 1
I
4000 4500
0000216682.CNF
5000 Energy(kev)
Live Time 10200.000 sec Rea 1 Time 10200 .100 sec start: 1 3453.S(kev) stop : 1024 6472. 7(kev) Acq. start Mon Jul 09 14:44:04 2018
5500 6000
0182
Channel Data Report 7/9/2018 5:38:47 PM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1: 2 0 2 1 1 1 1 0
9: 0 3 0 1 1 0 0 2
17: 1 2 0 1 1 1 1 0
25: 0 0 1 0 2 2 0 0
33: 0 1 1 1 1 2 3 1
41: 4 1 0 1 2 0 1 1
49: 1 2 1 1 1 0 1 0
57: 0 2 2 1 1 1 2 0
65: 0 0 4 1 1 1 3 1
73: 1 0 4 0 2 2 2 0
81: 2 1 2 2 1 0 1 0
89: 1 2 2 0 2 0 3 0
97: 1 2 2 2 3 1 1 2
105: 1 1 2 1 1 1 1 0
113: 1 0 1 1 1 2 2 3
121: 0 2 2 1 2 3 1 4
129: 1 2 1 1 2 2 2 2
137: 3 0 2 1 3 2 2 4
145: 0 0 0 4 1 0 1 0
153: 1 2 1 3 1 1 2 1
161: 0 2 0 2 0 2 1 1
169: 1 0 3 3 1 2 0 2
177: 0 0 0 0 2 2 0 1
185: 2 2 0 1 0 1 1 0
193: 2 1 5 0 1 2 2 1
201: 2 1 1 0 4 2 1 3
209: 1 2 2 2 2 2 1 0
217: 0 1 3 2 1 0 1 0
225: 3 1 2 1 1 1 3 1
233: 3 3 4 1 2 0 2 1
241: 0 2 1 0 2 1 1 4
249: 0 4 1 3 4 0 3 2
257: 3 3 2 0 4 1 0 2
265: 3 2 2 3 1 1 3 2
273: 3 0 5 0 1 1 0 1
281: 0 0 1 3 1 2 1 2
289: 4 3 1 0 4 0 1 0
297: 0 3 2 1 1 1 0 1
305: 1 0 1 2 2 2 2 1
313: 0 2 1 2 3 2 2 1
321: 2 2 4 2 2 0 0 1
329: 0 1 2 2 0 3 2 3
337: 4 0 0 1 2 2 1 2
345: 0 2 3 0 0 3 0 1
353: 3 3 1 0 1 3 2 3
361: 1 1 4 2 3 2 1 0
0183
Channel Data Report 7/9/2018 5:38:47 PM Page 2
369: 0 2 4 2 1 0 1 1
Sample Title: 01
Channell------l-------l-------l-------l-------1-------1-------1-------\ 377: 0 1 3 2 1 3 0 0
385: 2 3 0 1 0 1 0 1
393: 0 1 1 1 4 0 0 1
401: 0 2 2 1 1 0 0 3
409: 3 2 6 2 1 3 1 5
417: 1 1 2 3 0 1 2 0
425: 1 3 3 2 1 1 1 1
433: 3 1 4 2 1 2 4 0
441: 3 2 3 1 1 1 0 3
449: 0 0 1 0 1 2 1 0
457: 1 0 1 0 1 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 1 0 0 0 0 0 0
489: 0 0 0 1 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 1 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 1
529: 0 0 1 0 0 0 0 0
537: 0 1 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 1 0 0 0 0 0
569: 0 0 0 0 0 1 1 0
577: 1 0 0 0 0 0 0 0
585: 1 0 0 0 0 0 0 2
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 1 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 1
633: 0 0 0 1 0 0 0 0
641: 1 0 0 0 0 0 0 0
649: 0 1 0 0 0 0 0 0
657: 0 1 0 1 0 0 1 0
665: 0 0 0 1 0 0 0 0
673: 0 0 0 0 0 0 0 1
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 1 0
729: 0 0 0 0 0 0 0 1
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 1 1 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 1 0 1
785: 0 0 0 0 0 0 0 1
793: 0 0 0 0 0 0 1 0
0184
Channel Data Report 7/9/2018 5:38:47 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------1-------1-------1-------I-------I-------I-------I 809: 0 0 1 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 1 0 1
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 1 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 1 0 0
0185
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.531 4.779
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002166
1806097A-RA 02 Shelf 2 Ra
Alpha_048 10006125B 83111 System Bkgd 219036
<not performed>
1.000E+000 +/- 0.000E+000 liter 3.000E+000 7/9/2018 7/9/2018
Generic Div. Factor: 2:09:31 PM 2:44:05 PM
170.0 minutes 170.0 minutes
1.0000 +/- 0.0000
1.000E+000
0.1760 +/- 0.0030 on 6/6/2018 0.1760 +/- 0.0030
2:37:42 PM
0.350 MeV
PEAK AREA REPORT
Net Pk Area
-2.89 -1.38
Pk Area Error%-
82.82 168.33
Ambient Backgnd
2.89 2.38
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
0.0 3.0
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter )
MDA (pCi/liter
RA-224 RA-226
0. 969 1.000
5685.50* -1.37E-001 +/- 1.14E-001 4785.00* -6.23E-002 +/- 1.05E-001
4.16E-001 +/- 1.41E-002 3.70E-001 +/- 1.25E-002
0186
60
55
50
45
40
35 V)
+-' C:
8 30
25
20
15
10
5
0 I I
3500 4000 4500
ROI Type: 1
0000216683.CNF
<D
~
5000 Energy(kev)
5500
Live Time :10200.000 sec Real Time :10200.100 sec start: l:3443.9(kev) Stop : 1024: 6472 .3(keV) Acq. start :Mon Jul 09 14:44:05 2018
6000
0187
Channel Data Report 7/9/2018 5:38:54 PM Page 1
******************************************************* ***** s p E C T RA L DAT A R E P O R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------l-------1-------1-------1 1 : 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0 233: 0 0 0 0 0 0 0 0 241: 0 0 0 0 0 0 0 0 249: 0 0 0 0 0 0 0 0 257: 0 0 0 0 0 0 0 0 265: 0 0 0 0 0 0 0 0 273: 0 0 0 0 0 0 0 0 281: 0 0 0 0 0 0 0 0 289: 0 0 0 0 0 0 0 0 297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0 321: 0 0 0 0 0 0 0 0 329: 0 0 0 0 0 0 0 0 337: 0 0 0 0 0 0 0 0 345: 0 0 0 0 0 0 0 0 353: 0 0 0 0 0 0 0 0 361: 0 0 0 0 0 0 0 0
0188
Channel Data Report 7/9/2018 5:38:54 PM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 1 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0 569: 0 0 0 0 0 0 0 0 577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0 601: 0 0 0 0 0 0 0 0 609: 0 0 0 0 0 0 0 0 617: 0 0 0 0 0 0 0 0 625: 0 0 0 0 0 0 0 0 633: 0 0 0 0 0 0 0 0 641: 0 0 0 0 0 0 0 0 649: 0 0 0 0 0 0 0 0 657: 0 0 0 0 0 0 0 0 665: 0 0 0 0 0 0 0 0 673: 0 0 0 0 0 0 0 0 681: 0 0 0 0 0 0 0 0 689: 0 0 0 0 0 0 0 0 697: 0 0 0 0 0 0 0 0 705: 0 0 0 0 0 0 0 0 713: 0 0 0 0 0 0 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 0 0 0 0 0 0 753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0 769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 0 0 0 0 0 793: 0 0 0 0 0 0 0 0
0189
Channel Data Report 7/9/2018 5:38:54 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------1-------1-------1-------I-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 1 0 0 0 0 0
969: 1 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0190
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.580 4.575
OU-1-007 OUTFALL 007 DIS DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002166 1806097A-RA 03 Shelf 2 Ra
Alpha_049 10006121A 49 System Bkgd 219037
<not performed>
1.000E+000 2.660E+000 6/20/2018 7/9/2018
170.0
+/- 0.000E+000 liter Generic Div. Factor:
2: 09: 31 PM 2:44:00 PM
minutes 170.0 minutes
1.0000 +/- 0.0000
1.000E+000
0.1565 +/- 0.0028 on 2/16/2018 12:37:01 PM 0.1565 +/- 0.0028
0.350 MeV
PEAK AREA REPORT
Net Pk Area
-5.29 8.45
Pk Area Error%
53.30 78.43
Ambient Backgnd
6.29 2.55
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter )
MDA (pCi/liter
RA-224 RA-226
0.986 0.944
5685.50* -2.52E-001 +/- 1.35E-001 4785.00* 3.81E-001 +/- 2.99E-001
5.54E-001 +/- 1.95E-002 3.78E-001 +/- l.33E-002
0191
55
50
45
40
35 V'I -I-' C:
8 30
25
20
15
10
5
0 3500
ROI Type: 1
4000
0000216684.CNF
i1 .'l :\I i_ Ii ,\'
4500 5000 Energy(kev)
5500
""' ~ ~ ;l;
Live Time :10200.000 sec Real Time :10200.100 sec Start: 1: 3474. l(kev) Stop : 1024: 6513. l(kev) Acq. Start :Mon Jul 09 14:44:00 2018
6000 6500
0192
Channel Data Report 7/9/2018 5:39:01 PM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------l-------l-------1-------1-------1-------I 1 : 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 1 0 0
233: 0 0 0 0 0 0 0 0 241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 1
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 1 0 0
313: 0 0 0 0 0 0 0 0
321: 0 1 0 1 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 1
345: 1 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0193
Channel Data Report 7/9/2018 5:39:01 PM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 1 1 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 1 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 1
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 0 0 0
433: 0 0 0 0 0 0 1 0
441: 1 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 1 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0 521: 0 0 0 0 0 0 0 0 529: 0 0 0 0 0 0 0 0 537: 0 0 0 0 0 0 0 0 545: 0 0 0 0 0 0 0 0 553: 0 0 0 0 0 0 0 0 561: 0 0 0 0 0 0 0 0 569: 0 0 0 0 0 0 0 0 577: 0 0 0 0 0 0 0 0 585: 0 0 0 0 0 0 0 0 593: 1 0 1 0 0 0 0 0 601: 0 0 0 0 0 0 0 0 609: 0 0 0 0 0 0 0 0 617: 0 0 0 0 0 0 0 0 625: 0 0 0 0 0 0 0 0 633: 0 1 0 0 0 0 0 0 641: 0 0 0 0 0 0 0 0 649: 0 0 0 0 0 0 0 0 657: 0 0 0 0 0 0 0 0 665: 0 0 0 0 0 0 0 0 673: 0 0 0 0 0 0 0 0 681: 0 0 0 0 0 0 0 0 689: 0 0 0 0 0 0 0 0 697: 0 0 0 0 0 0 0 0 705: 0 0 0 0 0 1 0 0 713: 0 0 0 0 0 0 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 0 0 0 0 0 0 753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 1
769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 0 0 0 0 0 793: 0 0 0 0 0 0 0 0
0194
Channel Data Report 7/9/2018 5:39:01 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------l-------1-------1-------1-------\ 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 1 0 0
953: 1 0 0 0 0 1 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0195
Sample Description: Spectrum File: Batch Identification: Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Generic Mult. Factor: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Chem. Recovery Factor: Counting Efficiency: Effective Efficiency:
Peak Match Tolerance:
Nuclide
RA-224 RA-226
Energy (MeV)
5.426 4.624
OU-1-007 OUTFALL 007 DIS \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002166 1806097A-RA 04 Shelf 2 Ra
Alpha_050 10006121B 50 System Bkgd 219038
<not performed>
l.000E+000 +/- 0.000E+000 liter 2.690E+000 6/20/2018 7/9/2018
Generic Div. Factor: 2: 09: 31 PM 2:44:02 PM
170.0 minutes 170.0 minutes
1.0000 +/- 0.0000
l.000E+000
0.1369 +/- 0.0025 on 2/16/2018 12:37:00 PM 0.1369 +/- 0.0025
0.350 MeV
PEAK AREA REPORT
Net Pk Area
-1. 21 1. 96
Pk Area Error%
189.99 208.49
Ambient Backgnd
2.21 2.04
NUCLIDE ANALYSIS RESULTS
Reagent Backgnd
0.00E+000 0.00E+000
FWHM (keV)
3.0 3.0
Nuclide Id
Conf. Energy (keV)
Activity (pCi/liter)
MDA (pCi/liter
RA-224 RA-226
0.916 0. 967
5685.50* -6.67E-002 +/- l.27E-001 4785.00* l.02E-001 +/- 2.13E-001
4.41E-001 +/- l.57E-002 4.06E-001 +/- l.44E-002
0196
60
55
50
45
40
35 V) .j-J C ::::l
8 30
25
20
15
10
5
0 I
3500
ROI Type: 1
I
4000 4500
0000216685.CNF
5000 Energy(kev)
.._,.
' ~
5500
Live Time :10200.000 sec Rea 1 Ti me : 10200 .100 sec start: 1: 3447. 7(kev) stop : 1024:6482.G(kev) Acq. start :Mon Jul 09 14:44:02 2018
6000
0197
Channel Data Report 7/9/2018 5:39:07 PM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 0 0 0 1 0 0 0 0 9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0 25: 0 0 0 0 0 0 0 0 33: 0 0 0 0 0 0 0 0 41: 0 0 0 0 0 0 0 0 49: 0 0 0 0 0 0 0 0 57: 0 0 0 0 0 0 0 0 65: 0 0 0 0 0 0 0 0 73: 0 0 0 0 0 0 0 0 81: 0 0 0 0 0 0 0 0 89: 0 0 0 0 0 0 0 0 97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0 113: 0 0 0 0 1 0 1 0 121: 0 0 0 0 0 0 0 0 129: 0 0 0 0 0 0 0 0 137: 0 0 0 0 0 0 0 0 145: 0 0 0 0 0 0 0 0 153: 0 0 0 0 0 0 0 0 161: 0 0 0 0 0 1 0 0 169: 0 0 0 0 0 0 0 0 177: 0 0 0 0 0 0 0 0 185: 0 0 0 0 0 0 0 0 193: 0 0 0 0 1 0 0 0 201: 0 1 0 0 0 0 0 0 209: 0 0 0 0 0 0 0 0 217: 0 0 0 0 0 0 0 0 225: 0 0 0 0 0 0 0 0 233: 0 0 0 0 0 0 0 0 241: 0 0 0 0 0 0 0 0 249: 0 0 0 0 0 0 0 0 257: 0 0 0 0 0 0 0 0 265: 0 0 0 0 0 0 0 0 273: 0 0 0 0 0 0 0 0 281: 0 0 0 0 0 0 0 0 289: 0 0 0 0 0 0 0 0 297: 0 0 0 0 0 0 0 0 305: 0 0 0 0 0 0 0 0 313: 0 0 0 0 0 0 0 0 321: 0 0 0 0 0 0 0 0 329: 0 0 0 0 0 0 0 0 337: 0 0 0 0 0 0 0 0 345: 0 0 0 0 0 0 0 0 353: 0 0 1 0 0 0 0 0 361: 0 0 0 0 0 0 0 0
0198
Channel Data Report 7/9/2018 5:39:07 PM Page 2
369: 0 0 1 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------l-------1-------1-------1-------\ 377: 0 0 0 0 0 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 1 0 0 0 0
433: 0 0 0 1 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 0 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 1 0 0 0 0 0
625: 0 0 0 1 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 1 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0199
Channel Data Report 7/9/2018 5:39:07 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0 865: 0 0 0 0 1 0 0 0 873: 0 0 0 0 0 0 0 0 881: 0 0 0 0 0 0 0 0 889: 0 0 0 0 0 0 0 0 897: 0 0 0 0 0 0 0 0 905: 0 0 0 0 0 0 0 0 913: 0 0 0 0 0 0 0 0 921: 0 0 0 0 0 0 0 0 929: 0 0 0 0 0 0 0 0 937: 0 0 0 0 0 0 0 0 945: 0 0 0 0 0 0 0 0 953: 0 0 0 0 0 0 0 0 961: 0 0 0 0 0 0 1 0 969: 0 0 0 0 0 0 0 0 977: 0 0 0 0 0 0 0 0 985: 0 0 0 0 0 0 0 0 993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0 1009: 0 0 0 0 0 0 0 0 1017: 0 0 0 0 0 0 0 0
0200
i--age I m L.
7/9/2018 5:33:38 AM
I I nA ,~I II\Al\!1ARV Rt=PnRT """""',;;,,. --~"1,lt,,U>I.I llil ll, II II ll-111 -II 'Iii II
Review Of QA Results - Pulser Check
Date : 7/9/2018 Time : 5:33:38 AM
CHAMBER DEVICE PARAMETER FLAG DATE Alpha 001 21f ALL Not Done Alpha 002 21f ALL Not Done Alpha 003 21f ALL Passed 7/9/2018 5:20:39 AM Alpha 004 21f ALL Passed 7/9/2018 5:20:39 AM Alpha 005 2lf ALL Not Done Alpha 006 21f ALL Not Done Alpha 007 21f ALL Not Done Alpha 008 21f ALL Not Done Alpha 009 21f ALL Not Done Alpha 010 21f ALL Passed 7/9/2018 5 :20:40 AM Alpha 011 2lf ALL Passed 7/9/2018 5:20:41 AM Alpha 012 21f ALL Passed 7/9/2018 5:20:42 AM Alpha 013 2lf ALL Not Done Alpha 014 2lf ALL Passed 7/9/2018 5:20:43 AM Alpha 015 2lf ALL Not Done Alpha 016 21f ALL Not Done Alpha 033 Alpha Analyst! 00DC Peak Energy Action 7/9/2018 5:20:44 AM Alpha 034 Alpha Analyst! 00DC ALL Not Done Alpha 035 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:20:46 AM Alpha 036 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:20:47 AM Alpha 037 Alpha Analyst 1 00DC ALL Not Done Alpha 038 Alpha Analyst 100 DC ALL Not Done Alpha 039 Alpha Analystl00DC PeakFWHM Action 7/9/2018 5:20:49 AM Alpha 040 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:20:50 AM Alpha 041 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:20:52 AM Alpha 042 Alpha Analystl00DC ALL Passed 7/9/2018 5:20:53 AM Alpha 043 Alpha Analystl00DC ALL Not Done Alpha 044 Alpha Analystl00DC ALL Passed 7/9/2018 5:20:55 AM Alpha 045 Alpha Analyst 100 DC ALL Passed 7/9/2018 5:20:56 AM Alpha 046 Alpha Analystl00DC ALL Passed 7/9/2018 5:20:58 AM Alpha 047 Alpha Analyst 100 DC ALL Passed 7/9/2018 5:21:00 AM Alpha 048 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:21:01 AM Alpha 049 Alpha Analystl00DC ALL Passed 7/9/2018 5:21:03 AM Alpha 050 Alpha Analystl00DC ALL Passed 7/9/2018 5:21:05 AM Alpha 051 Alpha Analyst! 00DC ALL Not Done Alpha 052 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:21:07 AM Alpha 053 Alpha Analyst! 00DC PeakFWHM Action 7/9/2018 5:21:09 AM Alpha 054 Alpha Analyst 1 00DC ALL Not Done Alpha 055 Alpha Analyst 1 00DC ALL Not Done Alpha 056 Alpha Analystl00DC ALL Passed 7/9/2018 5:21:10 AM Alpha 057 Alpha Analyst! 00DC ALL Passed 7/9/2018 5:21:13 AM Alpha 058 Alpha Analyst 1 00DC ALL Passed 7/9/2018 5:21:15 AM
0201
1-'age L OT L Kev1ew ot UA Kesults - 1-'u1ser l;necK
7/9/2018 5:33:38 AM
CHAMBER DEVICE PARAMETER FLAG DATE Alpha 059 Alpha Analystl 00DC ALL Passed 7/9/2018 5:21:17 AM
Alpha 060 Alpha Analystl 00DC ALL Passed 7/9/2018 5:21:20 AM
APPROVED BY:
APPROVAL DATE: ·119 I \b
0202
Library Listing Report 6/12/12 12:16:17 PM Page l
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Radium
Nuclide Library Description: Ra-226, Po-218, Rn-222
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV (%) Uncert. (Abs.+-)
PO-218 5.049E+010 6003.000* 0.000 99.9800 0.0000
RN-222 5.049E+010 5490.000* 0.000 99.9200 0.0000
RA-226 5.049E+0l0 4785.000* 0.000 100.0000 0.0000
* = key line
TOTALS: 3 Nuclides 3 Energy Lines
0204
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Work Order 18-06097
Analysis Code I Ra228 I Run 1
Date Received I 6/21/2018
Lab Deadline I 7/11/2018
Client I AMO Environmental Decisions
Project I WESTLAKE
Report Level I 4
Activity Units I pCi
Aliquot Units
Matrix WA
Method EPA 904.0
Instrument Type Alpha/Beta GPC
Radiometric Tracer Ba-133
Radiometric Sol# Ba-Ga
Tracer Act (dpm/g) 480.32
Carrier Yttrium
Carrier Cone (mg/ml) 31.1
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
18-06097 Ra228 Run 1
Client ID
LCS
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Login I CPM
30
30
Printed: 7/10/2018 2:37 PM Page 1 of 3
Sample Sample Date Aliquot
06/21 /18 00:00 1.0000E+00
06/21/18 00:00 1.0000E+00
06/20/18 10:00 1.0000E+00
06/20/18 10:00 1.0000E+00
0205
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal Sample Tracer
Fraction Desc Aliquot (g)
01 LCS 2.2121
02 MBL 2.2067
03 DUP 2.2113
04 DO 2.2115
Tracer Total ACT(dpm)
1062.5
1059.9
1062.1
1062.2
Radiometric Radiometric
Tracer(pCi) %Rec
655.0 136.85
658.0 137.82
584.0 122.06
621.0 129.79
18-06097 Ra228 Run 1
Grav Carrier Grav Filter
Added(ml) Tare (g)
2.000 0.0859
2.000 0.0862
2.100 0.0860
2.000 0.0862
I Grav Filter
Final (g)
0.1480
0.1470
0.1509
0.1467
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Grav Filter I Grav Net(g) %Rec
0.0621 99.84
0.0608 97.75
0.0649 99.37
0.0605 97.27
Printed: 711012018 2:37 PM Page 2 of 3
Mean SAF SAF %Rec 1* 2*
109.82 1.00 1.00
107.52 1.00 1.00
109.31 1.00 1.00
106.99 1.00 1.00
0206
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Date
Rough Prep Prep I By Date
07/10/18 12:40
07/10/18 12:40
07 /10/18 12:40 I
I 01110118 12:40 i
18-06097 Ra228 Run 1
Prep By
JBAILEY
JBAILEY
JBAILEY
JBAILEY
Sep to Date/Time
07/09/18 12:48
07/09/18 12:48
07/09/18 12:48
07/09/18 12:48
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. " Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep to By
JBAILEY
JBAILEY
JBAILEY
JBAILEY
I
Printed: 7/10/2018 2:37 PM Page 3 of 3
Sep t1 Sep t1 Date/Time By
07/10/18 12:59 JBAILEY
07/10/18 12:59 JBAILEY
07/10/18 12:59 JBAILEY
07/10/18 12:59 JBAILEY
0207
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-Ra228-1 Printed: 7/11/2018 7:35 AM
Page 1 of 3
~ Lab
Fraction
01
T
Nuclide I Sample I Client Activity Results I Error Estimate i MDA
LCS
I LCS LCS
I RPO MDA
I Blank
Desc Identification Units Known %R Flag Flag Flag Flag
RA-228 LCS LCS pCi/1 8.63E+00 7.52E-01 I 8.66E-01 9.20E+ool 93.82 OK OK I
c:: ::i a::
GI "0 0 u .!!!
i <a c:: q:
'l:
~
~---··
02 or- -·------·
03 ------------
04 00 N N I 1---- --1 -
C'G 0::
1/) C: .2 1/) ·c:; Q)
0 ca -C: Q)
E C: e ·s;:
11 ----
--------1-----
--··---~-- ----·- --------·-----·
RA-228 MBL BLANK
-------· ____ ,. ___ --~-----
RA-228 DUP OU-1-007 Outfall 007 DIS
--------- --·-------··
RA-228 DO OU-1-007 Outfall 007 DIS
··----- --~---- ---------------
- ----+------1- ------·
.. --- -------+-------1--------------------
- --------- -4--------1--------- --------------------
I --- --- - ----- -1 -- -- ---7 pCi/1 4.48E-01 __ 4.2~~-01 ~ 8.63E-01 OK OK
pCi/1 8.70E-01 4.99E-01 9.81 E-01 ! NA OK
-----·---- -··--···-- - ····-- -···+ -· ··-·-------···----I
pCi/1 7 .89E-02 4.12E-01 8. 71 E-01 ( I
OK
- - --·- - -----· ---
.. -- +--------1 - -- . ___ J _ ----~- -- ___ i
I I
- -:--------- -------- +--
--1-------
-+-----------+--~--+---+----- -1--i---------,
I
I I
--------- ... ·--·-····---!-· --- - -
- ----····--r----··--
------------e---------1---------- ------------ ---- -+------------ -- --+---- ··-------------1--------+------+--------t------+------+------+------r-------l
C: w ----- -1----- ----------- ----+
I I
0 ::i: <(
0208
Eberline Analytical Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-Ra228-1 Printed: 7/11/2018 7:35 AM
Page 2 of 3
~ ~
C: ::, a::
{: 0 u .!2 ~ iii C: c:(
1:
5
T"'"
00 N N ca 0::
1/) C: .Q .!!? u Q)
C
s C: Q)
E C: 0 ... ·;; C: w 0 :E <(
Lab I r I Sample I Sample I Sample I Radiometric Grav ·1 Mean ·1 S F [ Sep to [ Sep 11
Fraction Nuc ide Desc Date Aliquot % Rec % Rec % Rec ! A / DatefTime · DatefTime
I I I 01 I RA-228 I LCS I 06/21/18 00:00 1.00E+00 136.851 99.841 109.82 1.00/ 7/9/2018 12:48/ 7/10/2018 12:59
i f ' I
02 I RA-228 MBL I 06121118 00:00 1.ooE+oo . ~;;_~;I 97.151 . . 101.52! 1.001 11912018 12:48[ 111012018 12:59
___ 03 ______ RA-228 DUP 06/20/18_1~:~~-t-~~OE~~Or--~ :9.3~1···· 109.31[ 1.00[ 7/9/201812:48[ 7/10/201812:59
04 RA-228 DO 06/20/18 10:00 1.00E+00 129.791 97.27 106.99[ 1.00[ 7/9/2018 12:481 7/10/2018 12:59
--- ------·-----·"·------ ··-- -- ___ ., ·- -----· ·---·----- --------· ---~ -- -
I ·-1-··-------·1·- --·- ----1 I
.... -------1 .. --------· .. -r __ ....... _____ ... 1 ............. ___ --t· ·------1.. _..,__ ______ _J I
.. -1--- ..... ___ l·-- .... ··--·-t··-- ·--····---··----- .... f·· --i--- ···----··---+-·- ... _......, · ----- -·--f-l
_I ,_ I
----1-.... -• ----- .. ,+--·------....
--+--......... _,____ ............ ·"·i--"----+- ---+---
-~--------------l·-·--·--- ·--·--.. --f-··--.. --,-· ... ... -·-··--·-·--·-··"-J-...
-----+-- ··-+· ...... 1. · ........ ,_ __ .......... · +--..--- ··---·"-1-----· ---; -------- t-------------1
··-- ............. f-· .. ··· .. •-.. •-·--i--f----· .. ---.-t·-----------1-----------I
----t--· ----1--
. - ---• .. --• .. ---+--- ---1--.. •-"
1-----·--t·--···"·-·----·--+----1·-.. --,---·--· .. --.... - •-.. ·--·!--·"
0209
Eberline Analytical
Oak Ridge Laboratory
( I I Lab Fraction
01
Nuclide
RA-228
----
02 i:::
RA-228
~ ::i
a: 11 03 --- -. ·----- -·---- ~---·
RA-228
__ 04 RA-228 Q) 00 "0 0 N u .!!1 N i ca Ill 0:: i::: q;
Preliminary Data Report & Analytical Calculations Printed: 7/11/2018 7:35 AM Page 3 of 3
Work Order: 18-06097-Ra228-1
: Sample I Counting Halflife
' Desc OatefTime (days) Detect
LCS 07/10/18 15:01 LB4110A
------·-·-- ·-----------····------
MBL 07/10/18 15:01 LB4110A
i -·· -------- ---------·- --------··-· ----
I DUP 07/10/18 15:01 LB4110A
DO I 07/10/18 15:01 LB4110A
--·--·f---····---·-1-- ------------------------1-----··.
·-----·---. ··--------
. -+-·------- ---1---------- --- --
Carrier Count I Time 1
Counts Bkg CPM
Eff
j
I :: -I . :::i C3 120
C4 120
1---- ----
---)------
856/ 1.21 0.4667
199 i 1 _333333333 0.4578
-+ 30~1 -
1.9 0.4699
17711.416666667[ 0.4692 I -T·-··
i -----··-------1----------1
-~-·"·--- ·-·--·----)--·-- ----,------
+---------r------i--------~--------+---
1-------- --1----- -----···- -----····-----1----------
t: ~ u
II)
C: 0 II)
(.) Q)
C ni -C: Q)
E C: 0 I-
> C: w 0 ~ <{
- ·---+-··---·-·---, --·----------- -------------1----- -- - -· -1-----------~1-----·- -- 1--- ---------!--
---------/--- ·----+---·-·-- +---------- -- 1--·····-- ·-··-·/---
---+-----·-· -· ---+--- --------+-------!
------- ;-------·--1----------- ----------i-------------- .. -+-· --------- ··-+----- ----4---------1----
_. ___________ _
0210
Count Room Report Client: AMO Environmental Decisio
Internal Sample Client
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-007 Outfall 007 DIS
04 DO OU-1-007 Outfall 007 DIS
18-06097-Ra228-1 (pCi/I) in WA Tracer ID: Ba-Ga
Sample Sample Tracer
Date Aliquot Aliquot(g)
06/21/18 00:00 1.0000 2.2121
06/21/18 00:00 1.0000 2.2067
06/20/18 10:00 1.0000 2.2113
06/20/18 10:00 1.0000 2.2115
Tracer Radiometric ACT(dpm) Tracer (pCi)
1062.5159 655.0000
1059.9221 658.0000
1062.1316 584.0000
1062.2277 621.0000
Printed: 7/10/2018 2:37 PM Page 1 of 1
Radiometric SAF SAF %Rec 1• 2•
136.85 1.00 1.00
137.82 1.00 1.00
122.06 1.00 1.00
129.79 1.00 1.00
0211
Eberline Analytical Oak Ridge Laboratory
LCS & Matrix Spikes
Isotope Sol# Activity Solution dpmlg Date
Ra-228 Ra-12 54.550 7/10/2018
Tracers
fraction Isotope Sol# Activity dpmlg
01 Ba-133 Ba-6a 480.320
02 Ba-133 Ba-6a 480.320
03 Ba-133 Ba-6a 480.320
04 Ba-133 Ba-Sa 480.320
Version 2.0 08/99
Approx Addition
0.370
Solution Date
7/10/2018
7/10/2018
7/10/2018
7/10/2018
Spike and Tracer Worksheet
Analysis Code Date Technician
Ra228 7/10/2018 12:40 JBAILEY
LCS MS LCSD MSD LCS MS Volume Volume Volume Volume Known Error Added Error
Used(g) Used(g) Used{g) Used(g) pCi Estimate pCi Estimate
0.3745 9.20 0.469 0.00 0.000
Balance Printer Tapes
Volume Approx Tracer Used (g) Addition
2.2121 2.1100
2.2067 2.1100
2.2113 2.1100
2.2115 2.1100
Page 1 of 1 Printed: 7/10/2018 12:40 PM
Technician Initials Witness Initials
16 LCSD MSD
Known Error Added Error
pCi Estimate pCi Estimate
0.00 0.000 0.00 0.000
LCS
Matrix Spike
0212
Lab
Eberline Analytical
Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-007 Outfall 007 DIS
04 OU-1-007 Outfall 007 DIS
Comments
Sample
Type LCS
MBL
DUP
DO
Aliquot Worksheet
Analysis Code Rµt Units Lab Deadline
Ra228 liters 7/11/2018
Muffle Data Dilution Data Aliquot Data
Ratio Post/Pre Noof Dils Oil Factor Ratio Aliquot Net Equiv
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
Technician: =d~ o-Wtj Dare ':I&: a
Technician
JHARVEY
MS Aliquot Data
Aliquot Net Equiv
Printed: 7/6/2018 9:36 AM Page 1 of 1
H-3 Solids Only vvater ruiaoo-~A:ruIst-
(ml) Aliq
0213
Eberline Analytical - Oak Ridge Version 1.1 10/2015 Gravimetric Worksheet
Work Order -
1s-oso91 I 1
Work Order Analysis
Code
Gravimetric Carrier
Ra228 Yttrium
TRetec AMO Environmental Decisions Sample Carrier Data Filter Data
Carrier Added Filter Tare Filter Final
Fraction Client ID Type (ml) (g) (g)
01 LCS LCS 2.0000 0.0859 0.1480
02 BLANK MBL 2.0000 0.0862 0.1470
03 DUP DUP 2.1000 0.0860 0.1509
04 OU-1-007 Outfall 007 DIS DO 2.0000 0.0862 0.1467
/\ I -~' . . '
Technician: , .I ~/1/'
(~ 0
'-'°' l ~ 1
Date: _:z__J _)_£_! -1tL_
Carrier Cone
(mg/ml)
31.1000
Filter Net (g)
0.0621 0.0608 0.0649 0.0605
Printed: 7/10/20182:31 PM Page 1 of 1
Technician
JBAILEY
Gravimetric %
Recovery
99.84 97.75 99.37 97.27
0214
Detector ID Sample ID Alpha Beta Count Time Voltage TOD ~ \'.'-i C1 1806097-01 20 856 120 1410 7/10/2018 3:01:24 PM
\~~ 4
C2 1806097-02 10 199 120 1410 7/10/2018 3:01:25 PM
C3 1806097-03 13 307 120 1410 7/10/2018 3:01 :25 PM
C4 1806097-04 12 177 120 1410 7/10/2018 3:01:25 PM
0215
Eberline Analytical Oak Ridge Labo·atory
Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
! LB4110A - B3
LB4110A - B4
LB4110A - Cl
• LB4110A - C2
• LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
• LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta Calibration Date
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
Alpha 11/2/2017
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
7/10/2018 1.33E-01
7/10/2018 5.00E-02
7/10/2018 1.83E-01
7/10/2018 5.00E-02
7/10/2018 1.17E-01
7/10/2018 5.00E-02
7/10/2018 1.67E-02
7/10/2018 6.67E-02
7/10/2018 1.S0E-01
7/10/2018 3.33E-02
7/10/2018 3.33E-02
7/10/2018 5.00E-02
7/10/2018 5.00E-02
7/10/2018 2.00E-01
7/10/2018 2.33E-01
7/10/2018 1.00E-01
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
7/10/2018 6.67E-02
7/10/2018 0.00E+00
7/10/2018 1.00E-01
7/10/2018 3.33E-02
7/10/2018 1.33E-01
7/10/2018 1.S0E-01
7/10/2018 8.33E-02
7/10/2018 3.33E-02
I
PFW LCL
p -4.47E-02
p I -5.83E-02
p -3.30E-02
p -2.93E-02
p -3.93E-02
p -1.32E-02
p -6.0lE-02
p -3.72E-02
p -2.54E-02
p -3.87E-02
p -5.53E-02
p -3.35E-02
p -3.17E-02
p -l.97E-02
p -4.46E-02
p -2.32E-02
p -4.29E-02
p -3.09E-02
p -8.81E-02
p -4.SSE-02
p -3.0lE-02
p -3.30E-02
p -4.14E-02
p -2.38E-02
p -4.87E-02
p -4.75E-02
p -4.94E-02
p -3.17E-02
Mean
8.87E-02
9.57E-02
9.88E-02
8.48E-02
1.l0E-01
1.13E-01
8.0lE-02
7.99E-02
8.68E-02
6.04E-02
6.92E-02
7.86E-02
1.34E-01
1.20E-01
1.04E-01
1.44E-01
1.lOE-01
6.37E-02
9.llE-02
7.04E-02
6.71E-02
4.64E-02
5.42E-02
6.91E-02
5.68E-02
7.47E-02
8.17E-02
7.70E-02
(Q \ Printed: 7/10/2018 6:44 AM --71 "0(63
Page 1 of 1 -r-
UCL
2.22E-01
2.S0E-01
2.30E-01
1.99E-01
2.59E-01
2.40E-01
2.20E-01
l.97E-01
1.99E-01
1.59E-01
1.94E-01
1.91E-01
3.00E-01
2.59E-01
2.52E-01
3.12E-01
2.62E-01
1.58E-01
2.70E-01
1.86E-01
1.64E-01
1.26E-01
1.S0E-01
1.62E-01
1.62E-01
1.97E-01
2.13E-01
1.86E-01
0216
Eberline Analytiec I Oak Ridge Labore tory
Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - 01
_B4110A - 02
_B4110A - 03
_B4110A - 04
LB4110A - El
LB4110A - E2
_B4110A - E3
_B4110A - E4
_B4110A - Fl
_B4110A - F2
_B4110A - F3
_B4110A - F4
!_B4110A - Gl
LB4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta Calibration Date
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
7/10/2018 1.S0E+00
7/10/2018 1.48E+00
7/10/2018 1.30E+00
7/10/2018 1.33E+00
7/10/2018 1.48E+00
7/10/2018 1.65E+00
7/10/2018 1.07E+00
7/10/2018 1.45E+00
7/10/2018 1.20E+00 .
7/10/2018 1.33E+00
7/10/2018 1.90E+00 .,
7/10/2018 1.42E+00,
7/10/2018 1.45E+00
7/10/2018 1.72E+00
7/10/2018 1.48E+00
7/10/2018 1.72E+00
3/23/2018 3.33E-02
3/23/2018 1.67E-02
3/23/2018 6.67E-02
3/23/2018 0.00E+00
7/10/2018 1.43E+00
7/10/2018 7.S0E-01
7/10/2018 6.13E+00
7/10/2018 1.12E+00
7/10/2018 1.80E+00
7/10/2018 2.38E+00
7/10/2018 1.77E+00
7/10/2018 1.88E+00
PFW LCL
p 9.02E-01
p 9.79E-01
p 1.04E+00
p 9.48E-01
p 1.08E+00
p 6.16E-01
p 9.0lE-01
p 7.lSE-01
p 8.28E-01
p 7.00E-01
p 9.35E-01
p 7.89E-01
p 8.40E-01
p -4.53E-01
p 8.14E-01
p I 9.28E-01
p 7.66E-01
p 5.45E-01
p 4.98E-01
p 5.67E-01
p 9.21E-01
p 4.87E-01
F -2.lSE-01
p i
6.77E-01
p 8.44E-01
f 1.27E+00
p 9.16E-01
p 6.SSE-01
Mean
1.36E+00
1.S0E+00
1.53E+00
1.40E+00
1.56E+00
1.SlE+00
1.37E+00
1.39E+00
1.25E+00
1.21E+00
1.83E+00
1.22E+00
1.32E+00
1.66E+00
1.27E+00
1.43E+00
1.32E+00
9.58E-01
1.20E+00
1.04E+00
1.39E+00
8.71E-01
1.31E+00
1.16E+00
1.31E+00
1.75E+00
1.43E+00
1.37E+00
Printed: 7/10/2018 6:44 AM Page 1 of 1
UCL
1.82E+00
2.02E+00
2.0lE+00
1.85E+00
2.03E+00
2.41E+00
1.84E+00
2.07E+00
1.67E+00
1.73E+00
2.72E+00
1.65E+00
1.80E+00
3.77E+00
1.73E+00
1.93E+00
1.88E+00
1.37E+00
1.91E+00
1.S0E+00
1.87E+00
1.25E+00
2.84E+00 ,
1.65E+00
1.78E+00
2.23E+00
1.94E+00
2.09E+00
\LQ '1-\\d\ ~
0217
Eberline Analytical Oak Ridge Latoratory
Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - B1
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB411 )A - Gl
LB411)A - G2
LB411JA - G3
LB4110A - G4
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
GPC Detector Report (ALL Efficiencies)
Count Date Eff
7/10/2018 0.2304
7/10/2018 0.2108
7/10/2018 0.2159
7/10/2018 0.2055
7/10/2018 0.2185
7/10/2018 0.1988
7/10/2018 0.2398
7/10/2018 0.2138
7/10/2018 0.2086
7/10/2018 0.2150
7/10/2018 0.2403
7/10/2018 0.2116
7/10/2018 0.2178
7/10/2018 0.2475
7/10/2018 0.2497
7/10/2018 0.1912
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
7/10/2018 0.2180
7/10/2018 0.1825
7/10/2018 0.2406
7/10/2018 0.2091
7/10/2018 0.1993
7/10/2018 0.2018
7/10/2018 0.2216
7/10/2018 0.1980
PFW LCL
p 0.2156
p 0.2006
F 0.1853
F 0.2114
p 0.2028
p 0.1824
I p 0.2169
p 0.2061
I p 0.1961
p -0.1433
p 0.2299
p 0.1993
! p 0.2109
p 0.2355
p 0.2378 . p 0.1824
F 0.1687 I F 0.1518
F 0.1547
F 0.1747
p 0.1478
p 0.1776
p 0.2311
p 0.2020
p 0.1904
p 0.1941
p 0.2154
p 0.1915
,<? Printed: 7/10/2018 6:44 AM ~y§
Page 1 of 1.'1-,\\o{\
Mean UCL
0.2257 0.2357 !
0.2111 0.2215
0.1999 0.2144
0.2267 0.2421
0.2227 0.2425 I
0.2009 0.2194
0.2344 0.2519
0.2215 0.2370
0.2077 0.2194
0.2268 0.5968 I 0.2425 0.2551 I 0.2149 0.2305
0.2219 0.2329
0.2517 0.2679
0.2500 0.2623
0.1955 0.2086 I
0.2258 0.2830
0.2051 0.2584
0.2075 0.2603
0.2355 0.2963
0.2130 0.2782
0.1846 0.1915
0.2382 0.2453
0.2110 0.2200
0.1991 0.2078
0.2025 0.2109
0.2249 0.2345
0.1997 0.2079
0218
Eberline Analy:ical Oak Ridge Laboratory
Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB411JA - C2
LB411JA - C3
LB411JA - C4
LB411JA - D1
LB411JA - D2
LB411JA - D3
LB4110A - D4
LB411JA-El
LB411JA - E2
LB411 )A - E3
LB411 1)A - E4
LB411 )A - Fl
LB411 1)A - F2
LB4110A - F3
LB4111)A - F4
LB4110A - Gl
LB4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta Calibration Date
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
GPC Detector Report (ALL Efficiencies)
Count Date Eff
7/10/2018 0.5450
7/10/2018 0.4636
7/10/2018 0.5365
7/10/2018 0.4867
7/10/2018 0.5324
7/10/2018 0.4951
7/10/2018 0.5872
7/10/2018 0.5289
7/10/2018 0.4767
7/10/2018 0.5179
7/10/2018 0.5931
7/10/2018 0.5184
7/10/2018 0.6478
7/10/2018 0.6343
7/10/2018 0.6415
7/10/2018 0.4983
3/23/2018 0.0436
3/23/2018 0.0428
3/23/2018 0.0551
3/23/2018 0.0569
7/10/2018 0.5352
7/10/2018 0.4595
7/10/2018 0.6095"
7/10/2018 0.5234
7/10/2018 0.4589
7/10/2018 0.4885
7/10/2018 0.5459
7/10/2018 0.4826
PFW
p
p
F
F
p
p
p
p
p
p
p
p
p
p
p
p
F
F
F
f
p
p
p
p
p
p
p
p
Printed: 7/10/2018 6:44 AM t---?@. Page 1 of 11,--\\o(\D
LCL Mean UCL
0.5123 0.5366 0.5608
0.4285 0.4632 0.4980
0.4423 0.4784 0.5144
0.5060 0.5417 0.5774
0.4983 0.5385 0.5786
0.4604 0.4995 0.5385
0.5433 0.5817 0.6201
0.5062 0.5442 0.5822
0.4451 0.4808 0.5165
0.4954 0.5192 0.5431
0.5690 0.5995 0.6300
0.4857 0.5257 0.5658
0.6207 0.6409 0.6610
0.6032 0.6440 0.6848
0.6135 0.6418 0.6701
0.4763 0.5026 0.5289
0.4162 0.5409 0.6655
0.3730 0.4913 0.6097
0.3852 0.4994 0.6137
0.4534 0.5890 0.7247
0.3672 0.5284 0.6896
0.4417 0.4610 0.4802
0.5949 0.6144 0.6339
0.5177 0.5344 0.5510
0.4393 0.4583 0.4773
0.4753 0.4874 0.4996
0.5234 0.5438 0.5642
0.4687 0.4870 0.5053
0220
7/9/2018 2:14:35PM
~pex-Gamma Analysis Report for 1806097-01
SPIKE
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator Detector Name
Geometry Live Time Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1806097-01 : SPIKE : RA RECOVERY
: 1.000E+00 units
: Countroom
: 7/9/2018 1:56:33PM
: 7/9/2018 1 :59:23PM
: BAFIL
: Administrator
: GE3 : BAFIL : 900.0 seconds
: 902.2 seconds
: 0.25 %
: 2.50 : 1 - 4096 : 9 - 4096 : 1.000 keV
: 2/17/2018 : 11/9/2014
: 68074
PEAK ANALYSIS REPORT
Peak Analysis Performed on 7/9/2018 2:14:28PM
Peak
No.
Peak Analysis From Channel
Peak Analysis To Channel 4096
Energy (keV)
ROI start
ROI end
Peak Centroid
Net Peak Area
Net Area Uncertainty
Page 1 of6
Continuum Counts
FWHM (keV)
0221
7/9/2018 2:14:35PM Page 2 of6
Analysis Report for 1806097-01
M m M m M
M m
M m
M m
M
m M m M
SPIKE
Peak Energy ROI
No. (keV) start
1 20.23 15 -2 31. 26 15 -3 52.13 44 -4 62.28 44 -5 81.13 75 -6 112.71 104 -7 141.18 132 -8 159.32 154 -9 276.48 267 -
10 285.82 267 -11 303.55 294 -12 333.77 328 -13 337.94 328 -14 355.96 349 -15 366.92 362 -16 386.36 374 -17 391.80 374 -18 416.55 407 -19 436.82 432 -20 455.90 451 -21 468.01 4 60 -22 511.07 504 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area Continuum
end Centroid Area Uncertainty Counts
40 20.67 2.88E+02 53.00 3.84E+02
40 31.70 7.85E+03 138.07 5.46E+02
69 52.55 4.24E+0l 73.03 6.24E+02
69 62.70 7.44E+02 79 .11 8.74E+02
97 81.53 1.52E+03 75.13 1.89E+02
119 113.09 3.77E+02 72. 35 5 .11E+02
152 141.54 1.00E+02 71.15 5.18E+02
166 159.67 5.18E+0l 45.78 2. 96E+02
288 276.76 1.77E+02 49.99 1.83E+02
288 286.09 2.43E+0l 16.45 4.09E+0l
311 303.81 1.80E+02 55.68 2.18E+02
342 334.01 1.21E+02 33.17 6.69E+0l
342 338.17 3.llE+0l 27.40 4.67E+0l
362 356.19 6.70E+02 58.09 7.72E+0l
374 367.14 2.24E+0l 24.17 5.72E+0l
395 386.56 6.18E+02 55.24 9.78E+0l
395 392.00 1.89E+0l 28.00 2.69E+0l
428 416.73 1.10E+02 36.03 6.60E+0l
442 437.00 l.25E+02 25.03 1.78E+0l
459 456.06 9.00E+00 10.99 1.20E+0l
475 468.17 5.12E+0l 16.85 7.69E+00
516 511.20 2.32E+0l 12.09 5.65E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 20.23 2 31.26 3 52.13 4 62.28 5 81.13 6 112. 71 7 141.18
: 7/9/2018 2:14:28PM
: \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000066391.CNF
Original Orig. Area Ambient Backgr. Subtracted
Area Uncertainty Background Uncert. Area
2.88E+02 53.00 7.20E+0l 4.82E-01 2.16E+02
7.85E+03 138.07 7.85E+03
4.24E+0l 73.03 4.24E+0l
7.44E+02 79.11 7.44E+02
1.52E+03 75.13 1.52E+03
3.77E+02 72.35 2.15E+0l 5.28E-01 3.56E+02
1.00E+02 71.15 1.00E+02
FWHM (keV)
4.25 6.57 8.86 6.27 2.37 2.17 4. 96 2.95 8.38 3.73 1. 65 5.23 4.84 1. 87 1. 39 5.30 5.27 4.30 1. 99 1. 47 1. 75 1. 60
Subtracted Uncert.
5.30E+0l 1.38E+02 7.30E+0l 7.91E+0l 7. 51E+0l 7.23E+0l 7. llE+0l
0222
7/9/2018 2:14:35PM Page 3 of 6
Analysis Report for 1806097-01
SPIKE
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
8 159.32 5.18E+0l 45.78 5.18E+0l 4.58E+0l
M 9 276.48 1.77E+02 49.99 1.77E+02 5.00E+0l
m 10 285.82 2.43E+0l 16.45 2.43E+0l 1.65E+0l
11 303.55 1.80E+02 55.68 1.80E+02 5.57E+0l
M 12 333.77 1.21E+02 33.17 1.21E+02 3.32E+0l
m 13 337.94 3.llE+0l 27.40 3.llE+0l 2.74E+0l
14 355. 96 6.70E+02 58.09 6.70E+02 5.81E+0l
15 366.92 2.24E+0l 24.17 2.24E+0l 2.42E+01
M 16 386.36 6.18E+02 55.24 6.18E+02 5.52E+01
m 17 391.80 1.89E+0l 28.00 1.89E+0l 2.80E+0l
18 416.55 l.10E+02 36.03 1.10E+02 3.60E+0l
19 436.82 l.25E+02 25.03 1.25E+02 2.50E+0l
20 455.90 9.00E+00 10.99 9.00E+00 1.l0E+0l
21 468.01 5.12E+0l 16.85 5.12E+0l 1.69E+0l
22 511.07 2.32E+0l 12.09 1.39E+0l 1.31E+00 9.23E+00 1.22E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/units) Uncertainty
SN-113 0. 96 255.12 1. 93 391.69 * 61.90 1.44E+0l 2.14E+0l
BA-133 0.97 30.80 * 97.60 6.73E+00 l.18E-01
302.84 * 17.80 7.84E+02 3.69E+02
356.01 * 60.00 6.55E+02 8.76E+0l
0223
Analysis Report for 1806097-01
SPIKE
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
7/9/2018 2:14:35PM
INTERFERENCE CORRECTED REPORT
? = X =
Nuclide Name
SN-113 BA-133
Nuclide Id
Confidence
0. 964 0.973
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
1.44E+Ol 6.73E+OO
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
2.14E+Ol 1.18E-01
Page 4 of 6
Comments
0224
Analysis Report for 1806097-01
M
M
m M
M
m M
m
M
SPIKE
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
1 20.23
3 52 .13
4 62.28
5 81.13
6 112. 71
7 141.18
8 159.32
9 276.48
10 285.82
12 333.77
13 337.94
15 366.92
16 386.36
18 416.55
19 436.82
20 455.90
21 468.01
22 511.07
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
7/9/2018 2:14:35PM
UNIDENTIFIED PEAKS
: 7/9/2018 2:14:28PM
: 1 : 4096
Peak Size (CPS)
2.40231E-01
4. 71317E-02
8.26408E-01
1.68641E+00
3.95497E-01
1. lllllE-01
5.75278E-02
1. 96732E-01
2. 69646E-02
1.34854E-0l
3.45494E-02
2.48911E-02
6.86279E-0l
l.22222E-01
1.39026E-01
1.00000E-02
5.68384E-02 ,
1.02514E-02
Peak CPS(%) Uncertainty
12.26
86.08
5.32 2.48
10.16
35.57
44.21
14.12
33.90
13. 66
44.06
53.95
4.47
16.38
10.00
61.05
16.47
65.92
NUCLIDE MDA REPORT
Peak Type
Sum
Sum
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Page 5 of6
Tolerance Nuclide
0225
7/9/2018 2:14:35PM Page 6 of 6
Analysis Report for 1806097-01
SPIKE
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/units) (pCilunits) (pCi/units) (pCilunits)
FE-55 5.89 24.50 4.06E-09 4.06E-09 -9.89E-11 1.95E-09
CO-57 122.06 85.51 8.08E+0l 8.08E+01 -l.17E+02 3.95E+0l
136.48 10.60 6.19E+02 2.llE+0l 3.00E+02
NI-59 6.92 29.80 3.18E-08 3.18E-08 -7.38E-10 1.53E-08
MO-93 16.59 52.90 7.53E-04 7.53E-04 -1.llE-05 3.68E-04
18.60 10.00 1.53E-02 2.34E-03 7.49E-03
NB-93M 16.57 9.43 4.18E-03 4.18E-03 -6.16E-05 2.04E-03
CD-109 88.03 3. 72 1.16E+03 1.16E+03 7.43E+03 5.70E+02
+ SN-113 255.12 1. 93 2.60E+03 5.26E+0l -2.25E+03 1.24E+03
391.69 * 61.90 5.26E+0l 1.44E+0l 2.53E+0l
SN-119M 23.87 16.10 1.74E-01 1.74E-01 -l.61E-02 8.63E-02
25.10 22.70 1.98E-01 2.47E+00 9.82E-02
I-125 35.49 6.49 9.54E+00 9.54E+00 -2.82E+00 4. 72E+00
I-129 29.78 57.00 3.08E-01 3.08E-01 3.84E+00 1.53E-01
33.60 13.20 3.19E+00 -9.41E-01 1.58E+00
39.58 7.52 1.70E+0l -5.08E+00 8.43E+00
+ BA-133 30.80 * 97.60 1.28E-01 1.28E-01 6.73E+00 6.31E-02
302.84 * 17.80 3.61E+02 7.84E+02 1.75E+02
356.01 * 60.00 4.49E+0l 6.55E+02 2.llE+0l
CE-139 165.85 80.35 9.19E+0l 9.19E+0l -2.26E+00 4.44E+0l
CE-144 133.54 10.80 5.72E+02 5. 72E+02 7.30E+0l 2.77E+02
HG-203 279.19 77.30 7.62E+0l 7.62E+0l 7.66E+0l 3.66E+0l
PB-210 46.50 4.25 3.79E+0l 3.79E+01 -2.45E+0l 1.86E+0l
PA-231 9.28 42.00 1.16E-06 l.16E-06 -2.24E-08 5.62E-07
10 .11 20.20 7.52E-06 -1.31E-07 3.66E-06
283.67 1. 60 3.59E+03 -1.12E+0l 1.73E+03
302.67 2.30 2. 72E+03 6.36E+03 1.32E+03
TH-231 25.64 14.70 3.65E-01 3.65E-01 4.54E+00 1.81E-01
84.21 6.40 5.78E+02 3.63E+03 2.85E+02
PA-234M 9.89 89.00 1.18E-06 l.18E-06 -2.28E-08 5.73E-07
21.72 64.90 1.84E-02 -3.63E-05 9.13E-03
37.93 23.75 4.09E+00 -1.21E+00 2.03E+00
131.42 20.40 2.83E+02 -1.71E+02 1.37E+02
TH-234 63.29 3.80 2.34E+02 2.34E+02 -5.10E+02 1.15E+02
NP-237 29.37 14.00 1.13E+00 1.13E+00 1.41E+0l 5.59E-01
86.50 12.60 3.22E+02 2.04E+03 1.59E+02
U-237 97.08 16.30 1.78E+02 1.31E+02 -1.28E+0l 8.63E+0l
101.07 26.30 1.31E+02 -8.92E+00 6.39E+0l
114.00 12.30 4.99E+02 -2.79E+02 2.44E+02
208.01 22.00 3.48E+02 -1.53E+02 1.68E+02
AM-241 59.54 35.90 1.86E+0l 1.86E+0l 8.0lE+0l 9. llE+00
AM-243 74.67 66.00 3.72E+0l 3.72E+0l -6.05E+0l 1.84E+0l
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0226
105
104
= = ..... ' <(
~ lQ3__J rd u V)
O'l 0
,--I
V)
+-' C :::s 0 u
102
101
100
= = ..... ' ~
500 1000
-ROI Type: 1
1500
0000068074.CNF
2000 channel
2500
Live Time :900.000 sec Real Time :902.240 sec Start: 1: O.S(kev) stop : 4096:4097.3(kev) Acq. start :Mon Jul 09 13:59:23 2018
3000
-ROI Type: 2
3500 4000
0227
7/9/2018 2:31:02PM
pex-Gamma Analysis Report for 1806097-02
BLANK
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure Operator Detector Name
Geometry Live Time Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1806097-02 : BLANK : RA RECOVERY
: 1.000E+00 units
: Countroom
: 7/9/2018 1 :56:42PM
: 7/9/2018 2:15:51PM
: BAFIL : Administrator
: GE3 : BAFIL : 900.0 seconds
: 902.3 seconds
: 0.26 %
: 2.50
: 1 - 4096 : 9 - 4096 : 1.000 keV
: 2/17/2018
: 11/9/2014
: 68077
PEAK ANAL YS/S REPORT
Peak Analysis Performed on 7/9/2018 2:30:56PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI start
ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Page I of6
Continuum Counts
FWHM (keV)
0228
7/9/2018 2:31:02PM Page 2 of6
Analysis Report for 1806097-02
M m M m m m
M m
M m
M m
m
m
M
m
BLANK
Peak Energy ROI
No. (keV) start
1 20.19 15 -2 31. 2 9 15 -3 54.08 4 6 -4 61.86 46 -5 66.36 4 6 -6 81.15 46 -7 112.67 102 -8 276.57 271 -9 286.38 271 -
10 304.68 297 -11 334.76 328 -12 356.20 34 7 -13 386.49 378 -14 417.01 406 -15 436.98 433 -16 445.31 443 -17 468.54 4 62 -18 509.57 503 -19 567.65 562 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area Continuum
end Centroid Area Uncertainty Counts
40 20.63 2.07E+02 54.22 4.SSE+02
40 31.73 7.74E+03 138.58 6. 21E+02
88 54.50 2.04E+02 65.86 4.74E+02
88 62.27 3.97E+02 50.32 2.12E+02
88 66.77 2.18E+02 47.24 2.1SE+02
88 81. 55 1.46E+03 75.55 2.26E+02
120 113. OS 3.23E+02 83.38 6.85E+02
290 276.84 6.66E+Ol 37.52 l.36E+02
290 286.64 1.96E+Ol 25.16 6.17E+Ol
322 304.94 2.01E+02 70. 27 2.08E+02
345 335.00 1.60E+02 44.01 l.21E+02
367 356.42 6.7SE+02 66.37 1.35E+02
396 386.69 4.86E+02 57.84 l.14E+02
428 417.20 1.0SE+02 38.75 7.87E+Ol
443 437.16 l.37E+02 26.70 2.20E+Ol
449 445.48 6.23E+OO 8.99 9.SSE+OO
474 468.69 4.27E+Ol 15.04 6.54E+OO
514 509.70 1.99E+Ol 11. 31 6.26E+OO
573 567.75 1.20E+Ol 6.93 O.OOE+OO
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 20.19 2 31.29 3 54.08 4 61.86 5 66.36 6 81.15 7 112. 67 8 276.57 9 286.38
10 304.68
: 7/9/2018 2:30:56PM
: \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000066391.CNF
Original Orig. Area Ambient Backgr. Subtracted
Area Uncertainty Background Uncert. Area
2.07E+02 54.22 7.20E+Ol 4.82E-01 1.3SE+02
7.74E+03 138.58 7.74E+03
2.04E+02 65.86 2.04E+02
3.97E+02 50.32 3.97E+02
2.18E+02 47.24 2.18E+02
1.46E+03 75.55 1.46E+03
3.23E+02 83.38 2.lSE+Ol S.28E-01 3.01E+02
6.66E+Ol 37.52 6.66E+Ol
1. 96E+Ol 25.16 1.96E+Ol
2.01E+02 70.27 2.01E+02
FWHM (keV)
4. 27 6.57 8.70 2.43 2.41 2.37 2 .11 4.69 4.44 2.02 1. 49 1. 95 4.10 4.38 2.48 2 .11 2 .13 2.51 6,74
Subtracted Uncert.
S.42E+Ol l.39E+02 6.59E+Ol 5.03E+Ol 4. 72E+01 7.SSE+Ol 8.34E+Ol 3.75E+Ol 2.52E+Ol 7.03E+Ol
0229
7/9/2018 2:31:02PM Page 3 of6
Analysis Report for 1806097-02
BLANK
Peak Energy Original
No. (keV) Area
11 334.76 1.60E+02 12 356.20 6.75E+02 13 386.49 4.86E+02 14 417.01 l.05E+02 15 436.98 1.37E+02 16 445.31 6.23E+00 17 468.54 4.27E+0l 18 509.57 1.99E+0l 19 567.65 1.20E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
Orig. Area Uncertainty
44.01 66.37 57.84 38.75 26.70
8.99 15.04 11. 31
6.93
Ambient Background
Backgr. Subtracted Uncert. Area
1.60E+02 6.75E+02 4.86E+02 1.05E+02 1.37E+02 6.23E+00 4.27E+0l 1.99E+0l 1.20E+0l
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy
Name Confidence (keV)
BA-133 0. 96 30.80 302.84 356.01
• = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
*
*
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
Yield(%)
97.60 17.80 60.00
Activity
(pCi/units)
6.68E+00
6.58E+02
Activity
Uncertainty
1. 20E-01
9.31E+01
Subtracted Uncert.
4.40E+0l 6.64E+01 5.78E+0l 3.88E+0l 2.67E+0l 8.99E+00 1.50E+0l 1.13E+0l 6.93E+00
0230
7/9/2018 2:31:02PM
Analysis Report for 1806097-02
BLANK
INTERFERENCE CORRECTED REPORT
? = X = @ =
Nuclide Name
BA-133
Nuclide Id
Confidence
0.968
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
6.68E+OO
nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
1.20E-01
Page 4 of 6
Comments
0231
Analysis Report for 1806097-02
M
M
m
m
m
M
m
BLANK
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
1 20.19
3 54.08
4 61.86
5 66.36
6 81.15
7 112. 67
8 276.57
9 286.38
10 304.68
11 334.76
13 386.49
14 417.01
15 436.98
16 445.31
17 468.54
18 509.57
19 567.65
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
7/9/2018 2:31 :02PM
UNIDENTIFIED PEAKS
: 7/9/2018 2:30:56PM
: 1 : 4096
Peak Size (CPS)
1.50472E-01
2.27214E-01
4.41649E-01
2.41795E-01
1. 6212 lE+00
3.34525E-01
7.40426E-02
2.17270E-02
2.23308E-01
1.78195E-01
5.40040E-01
1.16296E-01
1.52222E-01
6.91919E-03
4.74758E-02
2.20773E-02
1.33333E-02
Peak CPS(%) Uncertainty
20.02
16.10 6.33
10.85 2.59
13. 85
28.15 64.35
17.48
13. 72 5.95
18.51 9.75
72 .15 17.60
28.47
28.87
NUCLIDE MDA REPORT
Peak Type
Sum
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Page 5 of6
Tolerance Nuclide
0232
7/9/2018 2:31:02PM Page 6 of6
Analysis Report for 1806097-02
BLANK
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/units) (pCilunits) (pCi/units) (pCi/units)
FE-55 5.89 24.50 4.00E-09 4.00E-09 -8. 98E-11 1.93E-09
CO-57 122.06 85.51 7.92E+0l 7.92E+0l -5.28E+0l 3.87E+0l
136.48 10.60 5. 96E+02 2.74E+02 2.89E+02
NI-59 6.92 29.80 3.13E-08 3.13E-08 -6.70E-10 1.51E-08
MO-93 16.59 52.90 7.42E-04 7.42E-04 -1.0lE-05 3.62E-04
18.60 10.00 1.48E-02 1.58E-03 7.28E-03
NB-93M 16.57 9.43 4.llE-03 4. llE-03 -5.59E-05 2.0lE-03
CD-109 88.03 3. 72 l.16E+03 l.16E+03 -2.62E+03 5.69E+02
SN-113 255.12 1. 93 2.89E+03 8.03E+0l 8.20E+02 1.38E+03
391.69 61.90 8.03E+0l -5.45E+00 3.91E+0l
SN-119M 23.87 16.10 1.73E-01 1.73E-01 -9.93E-03 8.56E-02
25.10 22.70 1.96E-01 2.43E+00 9.72E-02
I-125 35.49 6.49 9.44E+00 9.44E+00 -6.93E+00 4.68E+00
I-129 29.78 57.00 3.05E-01 3.05E-01 3.70E+00 1.51E-01
33.60 13.20 3.16E+00 -2.31E+00 1.57E+00
39.58 7.52 l.69E+0l -1.25E+0l 8.37E+00
+ BA-133 30.80 * 97.60 1.38E-01 1.38E-01 6.68E+00 6.78E-02
302.84 17.80 3.58E+02 -1.36E+0l 1.73E+02
356.01 * 60.00 6.88E+0l 6.58E+02 3.31E+0l
CE-139 165.85 80.35 9.46E+0l 9.46E+0l 1.57E+0l 4.58E+0l
CE-144 133.54 10.80 5.44E+02 5.44E+02 -5.34E+0l 2.64E+02
HG-203 279.19 77. 30 7.80E+0l 7.80E+0l 1.31E+02 3.75E+0l
PB-210 46.50 4.25 3.83E+0l 3.83E+0l -6.02E+0l 1.88E+0l
PA-231 9.28 42.00 1.15E-06 1.15E-06 -2.03E-08 5.58E-07
10 .11 20.20 7.36E-06 -l.19E-07 3.58E-06
283.67 1. 60 3.64E+03 -3.78E+0l 1.75E+03
302.67 2.30 2.77E+03 -1.05E+02 1.34E+03
TH-231 25.64 14.70 3.61E-01 3.61E-01 4.47E+00 1.79E-01
84.21 6.40 5.73E+02 -8.95E+02 2.82E+02
PA-234M 9.89 89.00 1.17E-06 1.17E-06 -2.07E-08 5.68E-07
21.72 64.90 1.81E-02 -2.68E-04 8.97E-03
37.93 23.75 4.05E+00 -2.98E+00 2.00E+00
131.42 20.40 2.75E+02 -5.26E+02 1.33E+02
TH-234 63.29 3.80 2.38E+02 2.38E+02 -4.75E+02 1.17E+02
NP-237 29. 37 14.00 1.12E+00 1.12E+00 1.35E+0l 5.53E-01
86.50 12.60 3.20E+02 -6.51E+02 1.58E+02
U-237 97.08 16.30 1.78E+02 1.32E+02 -1.06E+03 8.66E+0l
101.07 26.30 1.32E+02 2.56E+0l 6.40E+0l
114.00 12.30 4.94E+02 -7.81E+0l 2.42E+02
208.01 22.00 3.50E+02 5.70E-01 1.69E+02
AM-241 59.54 35.90 1.90E+0l 1.90E+0l 8.04E+0l 9.33E+00
AM-243 74.67 66.00 3.77E+0l 3.77E+0l 1.39E+02 1.86E+01
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0233
lQS
lQ4
= = 7 <(
~ lQLLl ro u Vl
O'l 0 .-
1 Vl +-' C: :::l 0 u
102
101
100
...... ' ;;!;
500 1000
-ROI Type: 1
1500
0000068077 .CNF
2000 channel
2500
Live Time :900.000 sec Real Time :902.330 sec Start: 1: 0.S(keV) Stop : 4096:4097.3(kev) Acq. Start :Mon Jul 09 14:15:51 2018
3000
-ROI Type: 2
3500 4000
0234
7/9/2018 2:15:16PM
pex-Gamma Analysis Report for 1806097-03
OU-1-007 OUTFALL 007 DIS
GAMMA SPECTRUM ANAL YS/S
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator Detector Name
Geometry Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1806097-03 : OU-1-007 OUTFALL 007 DIS
: RA RECOVERY
: 1.000E+00 units
: Countroom
: 7/9/2018 1:57:01PM
: 7/9/2018 1:59:31PM
: BAFIL : Administrator
: GE4 : BAFIL
: 900.0 seconds
: 936.7 seconds
: 3.91 %
: 2.50 : 1 - 4096 : 15 - 4096
: 1.000 keV
: 2/24/2018
: 11/9/2014
: 68075
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 7/9/2018 2:15:10PM
Peak No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI start
ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Page 1 of6
Continuum Counts
FWHM (keV)
0235
7/9/2018 2:15:16PM Page 2 of6
Analysis Report for 1806097-03
M m
M m M
m m
M
m m
M
m
OU-1-007 OUTFALL 007 DIS
Peak Energy ROI
No. (keV) start
1 30.94 24 -2 35.28 24 -3 52.66 4 7 -4 61.64 57 -5 66.64 64 -6 81.17 75 -7 112. 57 106 -8 122.80 120 -9 142.29 138 -
10 149.40 14 6 -11 276.45 272 -12 302.95 297 -13 306.95 297 -14 330.70 329 -15 333.81 329 -16 337.70 32 9 -17 356.12 34 9 -18 384.41 380 -19 387.04 380 -20 390.66 380 -21 430.04 427 -22 436.85 432 -23 468.36 4 64 -24 509.54 504 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI end
39 39 56 64 69 86
118 124 145 151 279 311 311 341 341 341 360 397 397 397 432 439 472 512
Peak Net Peak Net Area Continuum
Centroid Area Uncertainty Counts
30.00 2.06E+03 98.61 2.17E+02
34.34 4.92E+02 72.99 1.62E+02
51.74 5.05E+0l 48.04 3.03E+02
60.73 1.04E+02 58.92 5.11E+02
65.73 7.59E+0l 41. 40 2.64E+02
80.27 8.78E+02 77.69 3.08E+02
111.69 2.19E+02 65.06 3.91E+02
121.93 1.92E+0l 21.08 7.76E+0l
141.44 3.33E+0l 28.77 1.15E+02
148.56 l.85E+0l 23.94 1.01E+02
275.70 5.88E+0l 24.41 6.04E+0l
302.23 1.18E+02 27.20 4.94E+0l
306.23 1.95E+0l 21.52 3.70E+0l
330.00 1.25E+0l 8.43 9.89E+00
333.11 5.88E+0l 23.07 4.06E+0l
337.00 2.48E+0l 20.37 5.47E+0l
355.44 3. 72E+02 46.52 8.53E+0l
383.75 7.92E+0l 27. 47 5.06E+0l
386.39 9.20E+0l 28.97 3.l0E+0l
390.01 2.51E+0l 32.75 3.80E+0l
429.42 6.60E+00 7.62 6.80E+00
436.24 6.00E+0l 16.97 8.00E+00
467.78 1.64E+0l 10.98 7.20E+00
508.99 1.0lE+0l 9.82 7.86E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 7/9/2018 2:15:10PM
Env. Background File : \\0 R-GAMMA 1 \ApexRoot\Countroom\Data\0000066684 .CNF
Peak Energy Original Orig. Area Ambient Backgr. Subtracted
No. (keV) Area Uncertainty Background Uncert. Area
1 30.94 2.06E+03 98.61 2.06E+03
2 35.28 4.92E+02 72.99 4.92E+02
3 52.66 5.05E+0l 48.04 5.05E+0l
4 61.64 1.04E+02 58.92 1.04E+02
5 66.64 7.59E+0l 41.40 7.59E+0l
FWHM (keV)
2.29 2.40 1. 96 1. 7 2 1. 97 2.34 2.20 2.62 2. 96 1. 62 1. 50 2.53 2.28 2.32 2.55 2.32 2.09 2.98 1. 98 3.79 1. 76 2.08 5.01 1. 62
Subtracted Uncert.
9.86E+0l 7.30E+0l 4.80E+0l 5.89E+0l 4.14E+0l
0236
7/9/2018 2:15:16PM Page 3 of 6
Analysis Report for 1806097-03
OU-1-007 OUTFALL 007 DIS
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
6 81.17 8.78E+02 77.69 8.78E+02 7.77E+0l
7 112.57 2.19E+02 65.06 2.19E+02 6.51E+0l
8 122.80 1.92E+0l 21.08 1.92E+0l 2. llE+0l
9 142.29 3.33E+0l 28.77 3.33E+0l 2.88E+0l
10 149.40 1.85E+0l 23.94 0.00E+00 0.00E+00 1.85E+0l 2.39E+0l
11 276.45 5.88E+0l 24.41 5.88E+0l 2.44E+0l
M 12 302.95 1.18E+02 27.20 1.18E+02 2. 72E+0l
m 13 306.95 1.95E+0l 21.52 1.95E+0l 2.15E+0l
M 14 330.70 1.25E+0l 8.43 1.25E+0l 8.43E+00
m 15 333.81 5.88E+0l 23.07 5.88E+0l 2.31E+0l
m 16 337.70 2.48E+0l 20.37 2.48E+0l 2.04E+0l
17 356.12 3. 72E+02 46.52 3.72E+02 4.65E+0l
M 18 384.41 7.92E+0l 27.47 7.92E+0l 2.75E+0l
m 19 387.04 9.20E+0l 28.97 9.20E+0l 2.90E+0l
m 20 390.66 2.51E+0l 32.75 2.51E+0l 3.28E+0l
21 430.04 6.60E+00 7. 62 6.60E+00 7.62E+00
22 436.85 6.00E+0l 16.97 6.00E+0l 1.70E+0l
23 468.36 1.64E+0l 10.98 1.64E+0l 1.l0E+0l
24 509.54 1.0lE+0l 9.82 1.0lE+0l 9.82E+00
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
NUCLIDE /DENTJFICAT/ON REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/units) Uncertainty
CO-57 0.75 122.06 * 85.51 9.39E+00 1.04E+0l
136.48 10.60
I-125 0.99 35.49 * 6.49 4.39E+02 6.61E+0l
BA-133 0.99 30.80 * 97.60 9.30E+0l 4.80E+00
302.84 * 17.80 5.83E+02 2.24E+02
356.01 * 60.00 5.84E+02 l.06E+02
PA-231 0.99 9.28 42.00 10 .11 20.20
283.67 1.60 302.67 * 2.30 4.52E+03 1.74E+03
0237
Analysis Report for 1806097-03
OU-1-007 OUTFALL 007 DIS
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
7/9/2018 2:15:16PM
INTERFERENCE CORRECTED REPORT
? = X =
Nuclide Name
CO-57 I-125 BA-133 PA-231
Nuclide Id
Confidence
0.758 0.993 0.997 0.997
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
9.39E+00 4.39E+02 9.41E+0l 3.79E+03
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
l.04E+0l 6.61E+0l 4.79E+00 l.74E+03
Page 4 of6
Comments
0238
7/9/2018 2:15:16PM
Analysis Report for 1806097-03
m M
m m M
m m
OU-1-007 OUTFALL 007 DIS
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
3 52.66
4 61.64
5 66.64
6 81.17
7 112. 57
9 142.29
10 149.40
11 276.45
13 306.95
14 330.70
15 333.81
16 337.70
18 384.41
19 387.04
20 390.66
21 430.04
22 436.85
23 468.36
24 509.54
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
UNIDENTIFIED PEAKS
: 7/9/2018 2:15:10PM
: 1 : 4096
Peak Size (CPS)
5.60616E-02
1.15995E-01
8.42842E-02
9.75564E-01
2.42841E-01
3.70086E-02
2.05395E-02
6.53308E-02
2 .1 7021E-02
1.39126E-02
6. 53501E-02
2.75285E-02
8.79544E-02
1.02252E-01
2. 79411E-02
7.33333E-03
6.66667E-02
1.82222E-02
1. 11905E-02
Peak CPS(%)
Uncertainty
47.61 28.22 27.29
4.42 14.88 43.20 64.75 20.76 55.08 33.65 19.61 41.11 17.35 15.74 65.12 57.70 14.14 33.47 48.77
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Peak Type
Sum Sum
Sum
Sum
Sum
Sum
Page 5 of6
Tolerance Nuclide
0239
7/9/2018 2:15:16PM Page 6 of6
Analysis Report for 1806097-03
OU-1-007 OUTFALL 007 DIS
Nuclide Energy Yield(%) Line MDA NuclideMDA Activity Dec. Level
Name (keV) (pCi/units) (pCi/units) (pCilunits) (pCilunits)
FE-55 5.89 24.50 5.43E-03 5.43E-03 0.00E+00 0.00E+00
+ CO-57 122.06 * 85.51 1.67E+0l 1.67E+0l 9.39E+00 7.71E+00
136.48 10.60 1.99E+02 6.87E+0l 9.34E+0l
NI-59 6.92 29.80 7.53E-03 7.53E-03 0.00E+00 0.00E+00
MO-93 16.59 52.90 1.04E+00 1.04E+00 2.81E-0l 4.92E-01
18.60 10.00 9.70E+00 2.15E+0l 4.66E+00
NB-93M 16.57 9.43 5.79E+00 5.79E+00 1.57E+00 2.75E+00
CD-109 88.03 3. 72 3.24E+02 3.24E+02 -1. 22E+02 1.52E+02
SN-113 255.12 1. 93 1. 2 9E+03 7.17E+0l 4.26E+02 5.92E+02
391.69 61.90 7.17E+0l 1.56E+0l 3.37E+0l
SN-ll 9M 23.87 16.10 1.02E+0l 7.78E+00 7.69E+00 4.91E+00
25.10 22.70 7.78E+00 2.00E-01 3.72E+00
+ I-125 35.49 * 6.49 9.79E+0l 9.79E+0l 4.39E+02 4.77E+0l
I-129 29.78 57.00 1.56E+0l 1.56E+0l 1.18E+02 7. 72E+00
33.60 13.20 8.42E+0l 5.89E+02 4.16E+0l
39.58 7.52 5.42E+0l -1.02E+0l 2.58E+0l
+ BA-133 30.80 * 97.60 5.02E+00 5.02E+00 9.30E+0l 2.45E+00
302.84 * 17.80 2.39E+02 5.83E+02 1.13E+02
356.01 * 60.00 7.13E+0l 5.84E+02 3.35E+0l
CE-139 165.85 80.35 3.29E+0l 3.29E+0l -4.05E+00 1.55E+0l
CE-144 133.54 10.80 1.95E+02 1.95E+02 l.17E+02 9.17E+0l
HG-203 279.19 77. 30 4.79E+0l 4.79E+0l -1.09E+00 2.25E+0l
PB-210 46.50 4.25 1.08E+02 1.08E+02 -7.61E+00 5.l0E+0l
+ PA-231 9.28 42.00 1.32E-02 1.32E-02 0.00E+00 0.00E+00
10 .11 20.20 3.53E-02 0.00E+00 0.00E+00
283.67 1. 60 1.60E+03 6.07E+02 7.29E+02
302.67 * 2.30 1.85E+03 4.52E+03 8.72E+02
TH-231 25.64 14.70 1.49E+0l 1.49E+0l -2.56E+00 7.19E+00
84.21 6.40 5.34E+02 2.45E+03 2.61E+02
PA-234M 9.89 89.00 7.52E-03 7.52E-03 0.00E+00 0.00E+00
21. 72 64.90 2.24E+00 3.39E+00 1.08E+00
37.93 23. 7 5 2.94E+0l 8.80E+0l l.43E+0l
131.42 20.40 9.80E+0l 4.48E+00 4.60E+0l
TH-234 63.29 3.80 4.18E+02 4.18E+02 8.18E+02 2.03E+02
NP-237 29.37 14.00 6.05E+0l 6.05E+0l 4.93E+02 2.99E+0l
86.50 12.60 9.92E+0l 8.52E+00 4.67E+0l
U-237 97.08 16.30 9.06E+0l 6.36E+0l -4.62E+0l 4. 27E+0l
101.07 26.30 6.36E+0l 2.14E+0l 3.0lE+0l
114.00 12.30 2.63E+02 6.13E+02 1.28E+02
208.01 22.00 1.24E+02 -1.56E+0l 5.76E+0l
AM-241 59.54 35.90 3.60E+0l 3.60E+0l 6.49E+0l 1.74E+0l
AM-243 74.67 66.00 1.63E+0l 1.63E+0l -3.26E-01 7.72E+00
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0240
105
104
~ 103 ro u V)
O"> 0 ,
I V)
+-' C: :::s 0 u
102
0000068075.CNF Live Time :900.000 sec Real Time :936.660 sec Start: 1: 2. O(kev) Stop : 4096:4091.G(kev) Acq. Start :Mon Jul 09 13:59:31 2018
100 U® Pl I \@ 1 ) a I H Ml I I Ip t II m 1 111 rnunnv !YU DO Ill IW ~IJ I I IHI II JI) Ill II It\ l I I \I I I I
500 1000
-ROI Type: 1
1500 2000 channel
2500 3000
-ROI Type: 2
3500 4000
0241
7/9/2018 2:31:41PM
pex-Gamma Analysis Report for 1806097-04
OU-1-007 OUTFALL 007 DIS
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1806097-04
: OU-1-007 OUTFALL 007 DIS
: RA RECOVERY
: 1.000E+00 units
: Countroom
: 7/9/2018 1:57:16PM
: 7/9/2018 2: 15:58PM
: BAFIL
: Administrator
: GE4
: BAFIL
: 900.0 seconds
: 934.1 seconds
: 3.65 %
: 2.50
: 1 - 4096
: 15 - 4096
: 1.000 keV
: 2/24/2018
: 11/9/2014
: 68078
PEAK ANAL YS/S REPORT
Peak Analysis Performed on : 7/9/2018 2:31:34PM
Peak
No.
Peak Analysis From Channel
Peak Analysis To Channel
Energy (keV)
ROI start
ROI end
: 1 : 4096
Peak Centroid
Net Peak Area
Net Area Uncertainty
Page 1 of6
Continuum Counts
FWHM (keV)
0242
7/9/2018 2:31:41PM Page 2 of6
Analysis Report for 1806097-04
M m
M m
M m m M m
M
m
M
m
OU-1-007 OUTFALL 007 DIS
Peak Energy ROI
No. (keV) start
1 30.95 24 -2 35.14 24 -3 52.20 4 7 -4 61.77 56 -5 66.08 56 -6 81. 24 7 5 -7 112. 2 9 10 6 -8 159.62 155 -9 225.48 219 -
10 276.77 272 -11 303.37 2 97 -12 335.09 328 -13 356.05 34 9 -14 376.09 372 -15 384.47 380 -16 387.22 380 -17 391.75 380 -18 414.96 40 9 -19 418.12 409 -20 437.16 432 -21 467.82 4 65 -22 471.82 4 65 -23 511.83 505 -24 583.78 579 -25 759.44 7 55 -26 1238.97 1235 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI end
39 39 55 74 74 86
117 163 228 281 309 340 360 378 396 396 396 424 424 442 478 478 517 587 762
1242
Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts
30.01 2.20E+03 103.43 2.47E+02
34.21 5.10E+02 76.01 2.01E+02
51. 27 5.43E+0l 42.06 2.39E+02
60.86 2.30E+02 46.47 2.08E+02
65.17 1.16E+02 42.51 2.19E+02
80.34 9.42E+02 77.10 2.60E+02
111.42 2.34E+02 59.40 3.24E+02
158.78 4.l0E+0l 35.74 1. 72E+02
224.69 3.21E+0l 32.22 1.30E+02
276.02 7.0lE+0l 25.02 4.79E+0l
302.64 1.45E+02 34.54 7.47E+0l
334.39 9.07E+0l 29.33 5.86E+0l
355.37 3.96E+02 43.91 4.64E+0l
375.42 1.27E+0l 10.43 1.06E+0l
383.82 1.31E+02 31.30 1.l0E+0l
386.57 1.15E+02 28.46 4.16E+00
391.10 3.98E+0l 29.46 3.28E+00
414.33 2.26E+0l 18.37 3.03E+0l
417.50 2.06E+0l 16.29 1.98E+0l
436.55 7.50E+0l 17.32 0.00E+00
467.24 1.97E+0l 6.93 6.55E-0l
471.24 9.22E+00 10.77 4.76E+00
511.29 3.l0E+0l 13. 35 6.00E+00
583.30 2.00E+0l 8.94 0.00E+00
759.13 8.00E+00 5.66 0.00E+00
1239.14 7.00E+00 5.29 0.00E+00
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 30.95 2 35.14 3 52.20
: 7/9/2018 2:31:34PM
: \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000066684. CNF
Original Orig. Area Ambient Backgr. Subtracted
Area Uncertainty Background Uncert. Area
2.20E+03 103.43 2.20E+03
5.10E+02 76.01 5.10E+02
5.43E+0l 42.06 5.43E+0l
FWHM (keV)
2.26 2.20 2.20 2.18 2.39 2.21 2.42 4.85 4.77 2.19 2.52 2.31 2.28 4.58 3.24 1. 98 4.58 2.86 2.34 3.06 2.63 2. 63 2.33 2.70 1.16 1. 92
Subtracted Uncert.
1.03E+02 7.60E+0l 4.21E+0l
0243
7/9/2018 2:31 :41PM Page 3 of6
Analysis Report for 1806097-04
OU-1-007 OUTFALL 007 DIS
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
M 4 61.77 2.30E+02 46.47 2.30E+02 4.65E+0l
m 5 66.08 1.16E+02 42.51 1.16E+02 4.25E+0l
6 81. 24 9.42E+02 77.10 9.42E+02 7.71E+0l
7 112.29 2.34E+02 59.40 2.34E+02 5.94E+0l
8 159.62 4.l0E+0l 35.74 4.l0E+0l 3.57E+01
9 225.48 3.21E+0l 32.22 3.21E+0l 3.22E+0l
10 276.77 7.0lE+0l 25.02 7.0lE+0l 2.50E+0l
11 303.37 1.45E+02 34.54 1.45E+02 3.45E+0l
12 335.09 9.07E+0l 29.33 9.07E+0l 2.93E+0l
13 356.05 3. 96E+02 43.91 3. 96E+02 4.39E+0l
14 376.09 l.27E+0l 10.43 l.27E+0l 1.04E+0l
M 15 384.47 1.31E+02 31.30 l.31E+02 3.13E+0l
m 16 387.22 1.15E+02 28.46 l.15E+02 2.85E+0l
m 17 391.75 3.98E+0l 29.46 3.98E+0l 2.95E+0l
M 18 414.96 2.26E+0l 18.37 2.26E+0l 1.84E+0l
m 19 418.12 2.06E+0l 16.29 2.06E+0l 1.63E+0l
20 437.16 7.50E+0l 17.32 7.50E+0l 1.73E+0l
M 21 467.82 1.97E+0l 6.93 1.97E+0l 6.93E+00
m 22 471.82 9.22E+00 10.77 9.22E+00 1.08E+0l
23 511.83 3.l0E+0l 13. 35 1.27E+0l 1. 4 lE+00 1.83E+0l 1.34E+0l
24 583.78 2.00E+0l 8.94 3.74E+00 l.22E+00 1.63E+0l 9.03E+00
25 759.44 8.00E+00 5.66 8.00E+00 5.66E+00
26 1238.97 7.00E+00 5.29 7.00E+00 5.29E+00
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/units) Uncertainty
SN-113 0.94 255.12 1. 93 391.69 * 61.90 6.26E+0l 4.71E+0l
I-125 0.98 35.49 * 6.49 4.52E+02 6.83E+0l
BA-133 0.99 30.80 * 97.60 9.96E+0l 5.05E+00
302.84 * 17.80 7. 13E+02 2.77E+02
356.01 * 60.00 6.21E+02 1.06E+02
0244
Analysis Report for 1806097-04
OU-1-007 OUTFALL 007 DIS
Nuclide Id Energy
Name Confidence (keV)
PA-231 0.99 9.28 10 .11
283.67 302.67
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
*
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
7/9/2018 2:31:41PM Page 4 of 6
Yield(%) Activity Activity
(pCi/units) Uncertainty
42.00 20.20 1. 60 2.30 5.52E+03 2.15E+03
INTERFERENCE CORRECTED REPORT
Nuclide Name
SN-113 I-125 BA-133 PA-231
Nuclide Id
Confidence
0.946 0.981 0.993 0.995
? = nuclide is part of an undetermined solution
X = nuclide rejected by the interference analysis
Wt mean Activity
(pCi/units)
6.26E+0l 4.52E+02 1.01E+02 4.74E+03
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Comments Activity
Uncertainty
4.71E+0l 6.83E+0l 5.04E+00 2.15E+03
0245
7/9/2018 2:31:41PM
Analysis Report for 1806097-04
M
m
M
m M
m
M
m
OU-1-007 OUTFALL 007 DIS
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
3 52.20
4 61.77
5 66.08
6 81.24
7 112.29
8 159.62
9 225.48
10 276.77
12 335.09
14 376.09
15 384.47
16 387.22
18 414.96
19 418.12
20 437.16
21 467.82
22 471.82
23 511.83
24 583.78
25 759.44
26 1238.97
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
UNIDENTIFIED PEAKS
: 7/9/2018 2:31 :34PM
: 1 : 4096
Peak Size (CPS)
6. 03161E-02
2.55640E-01
1.29421E-01
1.04675E+00
2.60000E-01
4.55818E-02
3. 564 72E-02
7.78605E-02
1.00759E-01
1.41049E-02
1.46046E-01
1.27384E-01
2.51648E-02
2.28952E-02
8.33333E-02
2.19202E-02
1.02399E-02
2.03082E-02
1.80656E-02
8.88889E-03
7.77778E-03
Peak CPS(%) Uncertainty
38.74 10.10 18.25
4.09
12.69 43.56 50.21 17.85 16.17 41.07
11.91
12.41 40.56 39.54
11. 55 17.56
58.43 36.73 27.76
35.36 37.80
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\WSRC.NLB
Peak Type
Sum Sum
Sum
Sum
Page 5 of6
Tolerance Nuclide
0246
7/9/2018 2:31:41PM Page 6 of6
Analysis Report for 1806097-04
OU-1-007 OUTFALL 007 DIS
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/units) (pCi/units) (pCi/units) (pCi/units)
FE-55 5.89 24.50 5.43E-03 5.43E-03 0.00E+00 0.00E+00
CO-57 122.06 85.51 2.18E+0l 2.18E+0l -7.87E+00 1.02E+0l
136.48 10.60 1.87E+02 -1.23E+02 8.75E+0l
NI-59 6.92 29.80 7.53E-03 7.53E-03 0.00E+00 0.00E+00
MO-93 16.59 52.90 9.54E-01 9.54E-01 8.62E-02 4.51E-01
18.60 10.00 9.32E+00 2.00E+0l 4.48E+00
NB-93M 16.57 9.43 5.33E+00 5.33E+00 4.82E-01 2.52E+00
CD-109 88.03 3.72 3.60E+02 3.60E+02 -1.06E+02 1.70E+02
+ SN-113 255.12 1. 93 1.21E+03 3.61E+0l -4.85E+02 5.51E+02
391.69 * 61.90 3.61E+0l 6.26E+0l 1.59E+0l
SN-119M 23.87 16.10 1.08E+0l 8.41E+00 6.04E+00 5.18E+00
25.10 22.70 8.41E+00 -2.44E+00 4.04E+00
+ I-125 35.49 * 6.49 1.04E+02 1.04E+02 4.52E+02 5.09E+0l
I-129 29.78 57.00 1.64E+0l 1.64E+0l 1.29E+02 8.13E+00
33.60 13.20 8.85E+0l 6.74E+02 4.37E+0l
39.58 7.52 5.78E+0l 5.27E+00 2.76E+0l
+ BA-133 30.80 * 97.60 5.37E+00 5.37E+00 9. 96E+0l 2.62E+00
302.84 * 17.80 2.14E+02 7.13E+02 l.00E+02
356.01 * 60.00 7.16E+0l 6.21E+02 3.37E+0l
CE-139 165.85 80.35 2.83E+0l 2.83E+0l -1.33E+00 1.32E+0l
CE-144 133.54 10.80 1. 96E+02 1. 96E+02 6.34E+0l 9.22E+0l
HG-203 279.19 77.30 4.73E+0l 4.73E+0l 5.36E+0l 2.22E+0l
PB-210 46.50 4.25 l.21E+02 1.21E+02 1.92E+0l 5.72E+0l
+ PA-231 9.28 42.00 1.32E-02 1.32E-02 0.00E+00 0.00E+00
10 .11 20.20 3.53E-02 0.00E+00 0.00E+00
283.67 1. 60 1.24E+03 9.33E+0l 5.51E+02
302.67 * 2.30 1.66E+03 5.52E+03 7.77E+02
TH-231 25.64 14.70 1.62E+0l 1.62E+0l -4.0lE+00 7.83E+00
84.21 6.40 5.43E+02 2.56E+03 2.66E+02
PA-234M 9.89 89.00 7.52E-03 7.52E-03 0.00E+00 0.00E+00
21. 72 64.90 2.24E+00 2.92E+00 1.08E+00
37.93 23.75 3.08E+0l 9.05E+0l 1.50E+0l
131.42 20.40 1.03E+02 2.49E+0l 4.85E+0l
TH-234 63.29 3.80 4.20E+02 4.20E+02 8.54E+02 2.04E+02
NP-237 29.37 14.00 6.38E+0l 6.38E+0l 5.57E+02 3.15E+0l
86.50 12.60 l.06E+02 8.04E+00 5.03E+0l
U-237 97.08 16.30 8.88E+0l 5.99E+0l -4.58E+0l 4.18E+0l
101.07 26.30 5.99E+0l -1.12E+00 2.82E+0l
114.00 12.30 2.62E+02 5.95E+02 1. 27E+02
208.01 22.00 1. 27E+02 -4.73E+0l 5.95E+0l
AM-241 59.54 35.90 3.61E+0l 3.61E+0l 6.79E+0l 1.75E+0l
AM-243 74.67 66.00 1.83E+0l 1.83E+0l -1.21E+02 8.69E+00
+ = Nuclide identified during the nuclide identification • = Energy line found in the spectrum
> = MDA value not calculated @ = Half-life too short to be able to perform the decay correction
0247
lQS
104
= =
~ 103 .I ro u V}
0-, 0
r--1
V}
+-' s::::: :=s 0 u
102
101
= = 7 ~ _, = -,c
= = _, ' ~
100 ll"PI IN I I I •-,
500 1000
-ROI Type: 1
1500
0000068078.CNF
2000 channel
2500
Live Time :900.000 sec Real Time :934.050 sec Start: 1: 2.0(kev) Stop : 4096:4091.6(kev) Acq. Start :Mon Jul 09 14:15:58 2018
3000
-ROI Type: 2
3500 4000
0249
Eberline Services
Oak Ridge Laboratory
Analysis Sheet
Work Order 18-06097
Analysis Code [ . GaGbT_ThSr
Run 1 Date Received 6/21/2018
Lab Deadline 7/11/2018
Client I AMO Environmental Decisions
Project WESTLAKE
Report Level 4
Activity Units pCi
Aliquot Units
Matrix WA
Method EPA 900.0 Modified
Instrument Type Alpha/Beta GPC
Radiometric Tracer
Radiometric Sol#
Tracer Act (dpm/g)
Carrier
Carrier Cone (mg/ml)
Internal Sample
Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
18-06097 GaGbT_ThSr
Run 1
Client ID
LCS
BLANK
OU-1-007 Outfall 007 DIS
OU-1-007 Outfall 007 DIS
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. h Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I I Login CPM
30
30
Printed: 7/10/20181:15 PM
Page 1 of 3
I Sample
I Sample
Date Aliquot
06/21 /18 00:00 1.0000E+00
06/21/18 00:00 1.0000E+00
06/20/18 10:00 7.0000E-02
06/20/18 10:00 7.0000E-02
I
0250
Eberline Services Oak Ridge Laboratory
Analysis Sheet
Internal Sample Tracer
Fraction Desc A/iquot(g)
01 LCS
02 MBL
03 DUP
04 DO
I I I
I I
Tracer Total ACT(dpm)
I
I I !
I
I
I
Radiometric Radiometric
Tracer (pCi) %Rec
0.00
0.00
0.00
0.00
18-06097 GaGbT_ThSr
Run 1
Grav Carrier Grav Filter
Added(ml) Tare(g)
7.7589
7.7589
7.7668
7.7539
I
Grav Filter Final (g)
7.7590
7.7590
7.8039
7.7879
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Grav Filter Grav Net(g) %Rec
0.0001
0.0001
0.0371
0.0340
I i !
I
I
i I I
I
i I
I I I
I
Printed: 7/1012018 1:15 PM Page 2 of 3
Mean SAF SAF
%Rec 1* 2*
1.00 1.00
1.00 1.00
1.00 1.00
1.00 1.00
I
0251
Eberline Services Oak Ridge Laboratory
Analysis Sheet
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
Rough Prep Rough Prep
Date By Prep Date
07/10/1811 :47
07/10/1811 :47
07/10/18 11 :47
07/10/1811:47
I
I
'
l
I :
18-06097 GaGbT_ThSr
Run 1
I Prep By
I
JPACHELLA
JPACHELLA
JPACHELLA
JPACHELLA
i
Sep tO Date/Time
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I Sep tO
I By i
I
I
!
I
'
I I
Printed: 7/10/20181:15 PM Page 3 of 3
Sept1 Sep t1
Date/Time By
I
i
I i
0252
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-GaGbT-1 Printed: 7/11/2018 9:51 AM
Page 1 of 3
~ . ., Lab
Fraction
01
02
Nuclide i Sample i Oesc
GROSS ALPHA LCS
Client Identification
LCS
Activity Units
pCi/1
Results [_Error Estimate I MDA I
2.97E+02 I 3. 77E+00 2.39E-01 [
LCS LCS I
LCS
I RPD
Known ¾R Flag Flag MDA Blank
Flag Flag
2.71E+02 109.59 I OK OK
C: ::3 ct
~ 0 (.)
.!!! ~ ca C: ,:(
i t: ~
l "' C: <C Cl)
.E: .:: Cl)
nl
t: .!!! u
oir-
1-.c C) ca
C)
ti) C .Q .!!? 0 Q)
C
s C Q)
E C 0 ... ·s: C w 0 :ii: <(
GROSS ALPHA MBL BLANK pCi/1
1---+------··+·. ------l-·---·-
03 GROSS ALPHA I DUP OU-1-007 Outfall 007 DIS pCi/1
·--1--·· ____________ __, ___ ----
04 GROSS ALPHA DO I OU-1-007 Outfall 007 DIS pCi/1
I --1-----------+- - ·- ---1--·-------·· ------------+---
------+-------------! -------1---------
1------+------------+-~-·----I~-- ------------ -------+·----··-··
--···----
--- ·----r---- +----------'---·--·--
1.29E-02 1.36E-01 3.14E-01 I OK OK ----
7.82E+00 4.24E+00 7.21E+00 NA INV ··-----1----·---~- ~--
2.48E+00I 3.10E+00 6.27E+00 INV
.. --·-+---
---1
I------+---------+---·--+-- -------------··--1---·-·--- -- --, ---- · -----··-----,-·--------------1-----·-·-----+---- --·----- '-----------+---+-----------1-----+------J
- --------···--+--·---- ··--------!-·------------;-------+--- i
1------+------------+-----I- ·--·· +------- ·--- -·-----l·---- ---·---- --·· --·--7------+------+------+------+------1
1-----+--------------, --+---- -------- 1---- --- - +----
1-------------------------,--.--•··--·· ----------+-------------t-----------1
-----------l-------t-··- . i J
1-----+--------- --l----t----------------t------- ·-----1-·--
I o---------+-------r--------1- --- -------1--------------1----+-------+-------+----+
1--------+--------+--------t--------------j-------+-----+-----r-----r----+-------+----1----------+----------1---
0253
Eberline Analytical
Oak Ridge Laboratory
~ Lab Nuclide I Sample
Fraction Desc
01 GROSS ALPHA LCS ------
02 GROSS ALPHA MBL
--··-
03 I GROSS ALPHA DUP
--- -·--- ----------;.....-----
I-04 GROSS ALPHA DO
--·- --- --------- -----~
..0 (!) --·~------
a:s (!) .•. --- -----··-----~- ~---
----- - ·-- - -·--- ---- -----··--------·-- ---··-.... .g ._ 0 -·-- c-···-
~
~ .; -~ ~ .. ----------·----------~ C: <{ .. :§ .... .. ijj -~ ------------ -- ----------··· ----------
(/)
C: .2 (/)
·o --------··· --·----·-- ------------~-- --···---
Cl) C
.5 -----··--··--- ------------------------·-· -----
~I C: Cl)
E C:
·--·--------------- ----
0 ---·- ------- i---------... ·s;: C: w
---------------f--·
0 ::!!: <(
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-GaGbT-1
Sample Sample Radiometric Grav Mean I SAF
Date Aliquot %Rec %Rec % Rec I
06/21/18 00:00 1.00E+00 0.00 0.00 o.oo' 1.00
- ---"-·---------··---- -------- ------ --·--------··---- -----.-·-- -----~--
06/21/18 00:00 1.00E+00 0.00 o.oo: 0.00 1.00
-----·- . -- --·•--,----- - --
06/20/18 10:00 i 7.00E-02 0.00 o.ooi 0.00 1.59 -- -- -----
06/20/18 10:00 I
7.00E-02 0.00 0.00 0.00 1.51
---------~----------- --·· -- ···-- --- -----·---
I --------
·•--I·-
·--- ----.--- . ----·--· ----------- ,-----·- --··----- -- ----- - ·----·---- -·
-------- --------------·· ···-- ····-·-··-·-··-····------·- !--------
--····-----------------------·--·-- ------·-----· --- - - . ----- ----·-·-·· f----------
-----------··---- ----------·---
·------- -·~------- -· ---- ··-- .. --------
·----------·--· --···---··-----------·--
--·---- -- --·-- - - - ---···-- ------·---···------- -- ... -····---·--·--
------ -·------------ -·------------·--··-- --·----·--·---
------ --- ---- ------------ ---•-.------·-----------. ---···--···- ____ ,, _____ , _______ --------
-·------·---- -- -------- --------------------------- ---- ----- -·-··---· ···--- - --·-----------·
---------------- --- --------------~- ,_ ________
----··-··--··-- ------ -------------+--~---·---·----
- ------------··- --·------
----------
I
I
SeptO
Printed: 7/11/2018 9:51 AM Page 2 of 3
Sep 11
DatefTime Date/Time
. -----------
---··---------
i ----··--·
! ·-
i I
I !
0254
Eberline Analytical Oak Ridge Laboratory
~ ' Ji
j Sample Lab Nuclide Fraction Desc
01 GROSS ALPHA I LCS I
c:: :J It
.g 0 (.)
.!!! ~ iij c:: q;
....
~ t: ~ j ~ .. C: "( Q)
.!:: 'i:: ., i'd
i: ,!!! u
~
....
.c (!) cu (!)
(/) C: 0
.!!? 0 Q)
C
~ C: Q)
E C: 0 ... ·s; C: w 0 :E <(
02
03
04
------
I ··~··--~·-···T··
GROSS ALPHA I MBL ·-- -
i
GROSS ALPHA I DUP I
-1 ·-
GROSS ALPHA +o~ --------
·------·-
··------
----·---·-
···--------- -------·
-------
--- -·-
--------
-
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-GaGbT-1
I
I Counting I Halflile Carrier Count
I Detect Counts
Date/Time (days) i Time
07/11/18 07:32 LB4110A D1 120 23786 __ ,, ________
·---· -- ·---
07/11/18 07:32 LB4110A D2 120 15
--·- --··- --·----. ·-·- -·-· ---------------
07/11/18 07:32 LB4110A D3 120 44
---------- ·--------··--·-----·- ------·· --- ··----------i----··
07/11/18 07:32 LB4110A D4 120 21
----···------- --··- -----------------· - ----
- .. --------------·----- --·--·--- ·---~-------- -
--------·- ___ ., -~
-·---- --·- ----·- - ----·-------- ··---- -· -- ----------------
·---
-----·- ···----------
-~-·-------- ------·-·------ . --·-·---------- -
-----· ----·----_____ ,, __
------·· ·----·-----· ----···-· --·--·-·----. --- --·---·-------
-------------- ----~---- . ·-----------
----------·------------- ---------·--- -----
------- --------- -·---------
-----~--·-- -· ~---------- ·--- f------·
·---··----· -·-
---···--------- ------ -~-----------··-·
··>---·-···
I Bkg
I CPM
0.066666667 1
0.1166666671
Printed: 7/11/2018 9:51 AM Page 3 of 3
Elf
0.3007 ··-···---~--
0.2912 ______ J_ I
0.1333333331 0.3054
0.1 0.2944
i I
I
I
I i
I
0255
Eberline Analytical
Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 GROSS BETA
§ a::
{: 0 0 ,!! ~ cii c:: <t
1: .!!! 0
""'"
1-jl (!) ca (!)
1/) C 0 1/)
·c:; Q)
a .! C Q)
E C 0 ... ·s: C w 0 :E <(
I
02 GROSS BETA -- ·-- ----··--·--·----
03 GROSS BETA
04 GROSS BETA
--- ,, -- ·----------
··--·------
----------
--·
I Sample Desc
LCS
MBL ----~
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-GaGbT-1
Client Activity LCS Results Error Estimate MDA
Identification '
Units Known
LCS pCi/I 2.62E+02 2.95E+00 I 5.04E-01 i 2.77E+02
------··-··---·-· -
BLANK pCi/I -1.28E-01 2.72E-01 5.96E-01 \
--~- ------- .. -------------i ·,~···
OU-1-007 Outfall 007 DIS pCi/1 2.91E+00 5.26E+00 1.08E+01 I .. -- --· -------
~983E~01• OU-1-007 Outfall 007 DIS pCi/I 1.14E+01 5.14E+00
i---- --~-------
---------------·------------ - ---·· , ____ ··---·-----~
·- ------ -- ---------- --------- ------- ------------ -·---
----~--··----·--- ----- -·----
.. -~-----
I --·---·-
--···
------ ···-~·-·
------ --·----·------·--. -···-·---··
·- -~--·-----
-- --- "·-~·----·--
-----··---
LCS I %R I
94.38
Printed: 7/11/2018 9:52 AM Page 1 of 3
LCS I RPD MDA Blank
I Flag Flag Flag Flag
OK OK
OK OK
NA INV --'----------
INV
0256
Eberline Analytical
Oak Ridge Laboratory
Preliminary Data Report & Analytical Calculations Printed: 7/11/2018 9:52 AM Page 2 of 3
Work Order: 18-06097-GaGbT-1
~ ---,-
Lab
I Nuclide I Sample Sample Sample Radiometric Grav
I Mean
I SAF I Sep to I Sep 11
Fraction Desc Date Aliquot % Rec % Rec % Rec Date/Time I Datemme
01 I GROSS BETA I LCS 06/21/18 00:00 1.00E+00 0.00 o.oo\ ____ 0.00 1.00 -------- ----····-- -· ---· - ----
~
---
.g I-0 .c 0
02 t GROSS BETA MBL 06~111800~0 -1 1.00••1 - o.oo 0.00 0.00 1.00
1-- -- ---- - -- -- -- -- ·--------·------ ---·--. -- ----
03 GROSS BETA DUP 0612011810:00 __ J 1.ooE-02 _______ o.oo 0.00 0.00 1.08
-·-·----- ~----------- - ----[--------------- ------· -------
04 GROSS BETA DO 06/20/18 10:00 I 7.00E-02 0.00 o.oo[ 0.00 1.07
,!!! (!) _; Ill cu i::: q: (!)
-- ---------1---
- ---l------··--t
.... a,
t! 0 t: ~
i f--------1---- I
I i
.; -~ ~ ., C: <I;
1--------1---- --- -- ----------+--------!------ - ---------------------+ - ----1---·- - -----+- -----+--+-- 7 --------ti __ _
a, .s .::: a,
nl -~ ------l-----------------------1---------1--------------- ___ ___, _________ --------1---- ----------
1/) C: 0
.!? 0 Q)
•------------,----- -----------------+- ----1-----
Q
J9
~I C: Q)
E C: 0 ---,------!----- -----1--- ----1------- -------------+
... -----+- ----------+-----+-----------+---------------1
·s: C: w 0 :E <(
0257
Eberline Analytical
Oak Ridge Laboratory
( Lab Nuclide
Sample
Fraction Desc
01 GROSS BETA I LCS
C: ::s a:
.g 0 0 ,!!! ~ "iii C: q:
-~
"'"""
1-.c (!) ns (!)
II) C: 0 II)
·o Q)
C
.f:! C: Q)
E C: 0 ... ·s; C: w 0 ~ <(
----------- -----···· - ..
02 GROSS BETA MBL
·------··- - ·-···
03 GROSS BETA DUP ----~------
04 GROSS BETA DO _L............ __________ -··---- :-----·---~
--------- -~---~- ----- .. - -- -
··---- 4-------··---
----
--4••·---
- ---·----·- ··--- ·-------
-·-·--·----·- ·-------- _____ ., ___
·--------- -------·-··-
--------·------·--·-- -----··----
·--··· ------·---
--·----- -·- --
-·---- ------------------ -- ---- -----·-
-------- ------···
---------
··---
Preliminary Data Report & Analytical Calculations
Work Order: 18-06097-GaGbT-1
Counting I Halflife Detect I Carrier Count
Counts 8kg
Date/Time l (days) I Time CPM
07/11/18 07:32 LB4110A D1 12oi 41871 1.1
--~· -· ---!-07/11/18 07:32 LB4110A D2 1201 161 1.483333333
' -------·-- ------ ---·-·------·-------- ---------------
07/11/18 07:32 LB4110A D3 1201 2191 1.55
------·---·-----· - ------·--- - /--- ---------·--- ----·-· ---------·----- -------------
07/11/18 07:32 LB4110A D4 120 297 i 1.666666667
--------~-----------~------- ----· ... , ... ---··------· --------- ---···
-·---------·----- - --- ·-·-----·-!-------- ----- -----·-
-~----- ··--·------ ·------·-- ------ ·------·---. -----··-- -·--- -----
I --------- ·--···--·----- ----· -·-----·------- -------- ----·----- -----·
---------·~·-·-··- ·---- . -··-------·
---------- -·------------- ·- - ·-·----·-·· ----·---- -···-···--·- ------~- --------·-- --'·-·
--·---····-···----· ---·---- --····-·-----·-----·--- ··----------
----~---- ----· . ., ___________
------ ----------- --·-·-----· ··----·---- - ·----·---- ····--·-----··-- -- -
----·-·--·-------·--- --·--·-·------- ·------·---------··· -----···--·-
---·-·- -----····-- - ----------·---·-·---·- ··-·-··-------------- - -------------···-
--------. ·······-·- -- --···------- ·-------·-----
-- -__________ _. ___ -----··'"-----
-·---- ----- --·------ ---------
---- ···------------------- ---· ·-f------ --·----'----
-------- --- --~---·---- ··-
I
Printed: 7 /11/2018 9 52 AM Page 3 of 3
Eff A to B, Cor
0.5104 297.844565
0.4979 1.341666667
0.4343 1.732086667
0.4889 2.475
0258
Count Room Report Client: AMO Environmental Decisio
Internal Sample Client
Fraction Desc ID
01 LCS LCS
02 MBL BLANK
03 DUP OU-1-007 Outfall 007 DIS
04 DO OU-1-007 Outfall 007 DIS '
I !
I i
I i ! I I :
I I I i I
I I I
I
I I
18-06097-GaGbT _ ThSr-1 (pCi/I) in WA Tracer ID:
Sample Sample Tracer Tracer
Date Aliquot Aliquot (g) ACT(dpm)
06/21/18 00:00 1.0000
06/21/18 00:00 1.0000
06/20/18 10:00 0.0700
06/20/18 10:00 0.0700
'
'
I
I
I
I
I
Radiometric Tracer (pCi)
Printed: 7/10/2018 1 :15 PM Page 1 of 1
Radiometric SAF SAF %Rec 1* 2*
0.00 1.00 1.00
0.00 1.00 1.00
0.00 1.00 1.00
0.00 1.00 1.00
I
I
0259
Eberline Services Oak Ridge Laboratory
Internal Work Order Run I 18-06097 1
LCS & Matrix Spikes I Isotope Sol# '
, ............ J Solution Approx
dpmlg Date Addition
Am-241 NB-07 i 593.400 7/10120181 0.800
SrY-90 NB-07 607.930 711012018i 0.900 --- ·--
Tracers
fraction ! Isotope Sol# Activity Solution dpmlg Date
--r---
Version 2.0 08/99
Spike and Tracer Worksheet
Analysis Code
GaGbT ThSr LCS MS
Volume Volume Used (g) Used(g)
1.0133
1.0133
Volume Approx Used(g) Addition
Date
7/10/2018 11:47
LCSD Volume Used(g)
MSO Volume Used(g)
Technician
JPACHELLA
LCS MS
Known pCi
270.85
277.48
Tracer
Error Estimate
11.647
8.325
Added pCi
0.00
0.00·
Error Estimate
0.000
0.000 --+------- -----·-----
Balance Printer Tapes
o.oo:
0.00
Page 1 of 1 Printed: 71101201811:47 AM
Error Estimate
0.000
0.000
LCS
Witness Initials
MSO Added
pCi
o.oo'
0.00,
Error Estimate
0.000
0.000
Matrix Spike
0260
Lab
Eberline Analytical Oak Ridge Laboratory
AMO Environmental Decisions
Fraction Client ID
01 LCS
02 BLANK
03 OU-1-007 Outfall 007 DIS
04 OU-1-007 Outfall 007 DIS
Comments
Sample
Type
LCS MBL
DUP DO
Aliquot Worksheet
Analysis Code I Rpt Units lab Deadline
GaGbT _ ThSr I liters 7/11/2018
Muffle Data Dilution Data Aliquot Data
Ratio Post/Pre No of Dils Dil Factor Ratio Aliquot Net Equiv
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
7.0000E-02 7.0000E-02
7.0000E-02 7.0000E-02
I
'
Technician: /vie ......, r 'c Date: __ 11_:::_1~
Technician
MHIGHTOWER
MS Aliquot Data
Printed: 7/10/2018 7:44 AM Page 1 of 1
H-3 Solids Only Water Added H3 Dist
Aliquot Net Equiv (ml) Aliq
0261
Eberline Services - Oak Ridge Version 1.0 9/1999 Gravimetric Worksheet
Work Order •
1s-oso91 I 1
Work Order Analysis
Code Gravimetric
Carrier
GaGbT ThSr
TRetec AMO Environmental Decisions Sample Carrier Data Filter Data Carrier Added Filter Tare Filter Final
Fraction Client ID Type (ml) (g) (g)
01 LCS LCS 7.7589 7.7590
02 BLANK MBL 7.7589 7.7590
03 DUP DUP 7.7668 7.8039
04 OU-1-007 Outfall 007 DIS DO 7.7539 7.7879
Technician: craJU Date:~ /(7',/ ~
Carrier Cone {mg/ml)
Filter Net (g)
0.0001 0.0001 0.0371 0.0340
Printed: 7/10/2018 11 :44 AM Page 1 of 1
Technician
JPACHELLA
Gravimetric %
·Recovery
0262
Eberline Services - Oak Ridge Version 1.0 9/1999 TDS / TSS Worksheet
Work Order I Run I
1s-oso91 I 1
Analysis Code
GaGbT_ThSr
TRetec AMO Environmental Decisions Filter Data Aliquot Filter Tare Filter Final
Fraction Client ID ml (g) (g)
04 OU-1-007 Outfall 007 DIS 5.0000 7.7913 7.7978
Technician: /t Date: _2_;~ ( tl
Filter Net (g)
0.0065
Technician
Printed: 7/10/2018 6:45 AM Page 1 of 1
MHIGHTOWER
TDS/TSS Maximum Aliq
(mg/L) (ml)
1300.0000 76.92
0263
Detector ID Sample ID Alpha Beta Count Time Voltage TOD
D1 1806097-01 23786 41871 120 1410 7/11/2018 7:32:07 AM -~p D2 1806097-02 15 161 120 1410 7/11/2018 7:32:07 AM I I' c~ D3 1806097-03 44 219 120 1410 7/11/2018 7:32:08 AM :}I\ io D4 1806097-04 21 297 120 1410 7/11/2018 7:32:08 AM
0264
Eberline Analyticc I Oak Ridge Laborctory
[ Detector
~ LB4110A - Al LB4110A - A2
LB4110A - A3
f LB4110A - A4 LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
_B4110A - Cl
_B4110A - C2
_B4110A - C3
_B4110A - C4 ,_ _B4110A - D1
_B4110A - D2
_B4110A - D3
i_B4110A - D4
_B4110A - El
_B4110A - E2
_B4110A - E3
'_B4110A - E4
_B4110A - Fl
'_B4110A - F2
1-B4110A - F3
LB4110A - F4 -LB4110A - Gl
LB4110A - G2 -LB4110A - G3 -LB4110A - G4
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM i i
7/11/2018 1.17E-01
7/11/2018 1.33E-01
7/11/2018 1.17E-01
7/11/2018 2.S0E-01
7/11/2018 1.00E-01
7/11/2018 1.17E-01
7/11/2018 1.33E-01
7/11/2018 1.17E-01
7/11/2018 6.67E-02 I 7/11/2018 1.00E-01 I 7/11/2018 6.67E-02
7/11/2018 l.67E-02
7/11/2018 6.67E-02 ·
7/11/2018 l.17E-01.
7/11/2018 l.33E-01 ,
7/11/2018 1.00E-01 "
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
3/23/2018 0.00E+00
7/11/2018 3.33E-02
7/11/2018 3.33E-02
7/11/2018 1.67E-02
7/11/2018 5.00E-02
7/11/2018 1.67E-02
7/11/2018 1.17E-01
7/11/2018 6.67E-02
7/11/2018 6.67E-02
PFW LCL Mean
p -4.43E-02 8.89E-02
p -5.78E-02 9.59E-02 p , -3.26E-02 9.89E-02
p -3.23E-02 8.56E-02
p -3.90E-02 1.lOE-01
p -1.29E-02 1.13E-01
p -5.98E-02 8.03E-02
p -3.69E-02 8.0lE-02
p -2.53E-02 8.67E-02
p -3.85E-02 6.06E-02
p -5.S0E-02 6.92E-02
p -3.41E-02 7.82E-02
p -3.21E-02 1.34E-01
p -1.94E-02 1.20E-01
p -4.41E-02 1.04E-01
p i -2.32E-02 1.44E-01
p -4.29E-02 1.lOE-01
p -3.09E-02 6.37E-02
p -8.81E-02 9.llE-02
p ! -4.SSE-02 7.04E-02
p -3.04E-02 6.67E-02
p -3.27E-02 4.63E-02
p -4.19E-02 5.37E-02
p -2.36E-02 6.89E-02
p -4.89E-02 5.66E-02
p -4.72E-02 7.49E-02
p -4.92E-02 8.16E-02
p -3.lSE-02 7.69E-02
Printed: 7/11/2018 7:16 AM Page 1 of 1
UCL
2.22E-01
2.S0E-01
2.30E-01
2.04E-01 ' I 2.59E-01
2.40E-01
2.20E-01
1.97E-01
1.99E-01
1.60E-01
1.93E-01
1.91E-01
2.99E-01
2.59E-01
2.52E-01
3.12E-01
2.62E-01
1.58E-01 I
2.70E-01
1.86E-01
1.64E-01
1.25E-01 I 1.49E-01
1.61E-01
1.62E-01
1.97E-01
2.12E-01
1.85E-01 I
G? ·:-+/t l ft9J
0265
Eberline Analytiec,I Oak Ridge Laborntory
r Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
i LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
:_B4110A - D2
_B4110A - D3
_B4110A - D4
LB4110A - El -LB4110A - E2
~
,_B4110A - E3 -_B4110A - E4
LB4110A - Fl -_B4110A - F2 ~
_B4110A - F3
_B4110A - F4
LB4110A - Gl
I_B4110A - G2
LB4110A - G3
LB4110A - G4
Alpha/Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Beta
Calibration Date
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
GPC Detector Report (ALL Backgrounds)
Count Date Bkg CPM
7/11/2018 1.22E+00
7/11/2018 1.37E+00
7/11/2018 1.45E+00
7/11/2018 1.68E+00
7/11/2018 1.22E+00
7/11/2018 1.37E+00
7/11/2018 1.33E+00
7/11/2018 1.63E+00
7/11/2018 1.02E+00
7/11/2018 1.30E+00
7/11/2018 2.lSE+00
7/11/2018 1.28E+00
7/11/2018 1.lOE+00
7/11/2018 1.48E+00
7/11/2018 1.SSE+00 ·
7/11/2018 1.67E+00 ,,
3/23/2018 3.33E-02
3/23/2018 1.67E-02
3/23/2018 6.67E-02
3/23/2018 0.00E+00
7/11/2018 1.23E+00
7/11/2018 1.02E+00
7/11/2018 8.S0E-01
7/11/2018 1.53E+00
7/11/2018 1.75E+00
7/11/2018 2.42E+00
7/11/2018 1.88E+00
7/11/2018 1.33E+00
PFW LCL
p 9.0lE-01
p 9.79E-01
p 1.04E+00
p 9.47E-01
p 1.07E+00
p I 6.17E-01
p 9.02E-01
p I 7.17E-01
p 8.26E-01
p 7.02E-01
F 9.37E-01
p 7.90E-01
p 8.38E-01
p -4.49E-01
p 8.13E-01
p 9.28E-01
p 7.66E-01
i p 5.45E-01
p 4.98E-01
p 5.67E-01
p 9.19E-01
p 4.89E-01
p -2.20E-01
p 6.73E-01
p 8.41E-01
F 1.26E+00
p 9.12E-01
p 6.56E-01
Mean
1.36E+00
1.S0E+00
1.53E+00
1.40E+00
1.SSE+00
1.SlE+00
1.37E+00
1.39E+00
1.25E+00
1.21E+00
1.83E+00
1.22E+00
1.32E+00
1.66E+00
1.27E+00
1.43E+00
1.32E+00
9.58E-01
1.20E+00
1.04E+00
1.39E+00
8. 73E-01
1.30E+00
1.17E+00
1.31E+00
1.75E+00
1.43E+00
1.37E+00
Printed: 7/11/2018 7:16 AM Page 1 of 1
UCL
1.82E+00
2.02E+00
2.0lE+00
1.85E+00
2.04E+00
2.41E+00
1.84E+00
2.07E+00
1.67E+00
1.73E+00
2.72E+00
1.65E+00
1.80E+00
3.76E+00
1.73E+00
1.93E+00
1.88E+00
1.37E+00
1.91E+00
1.S0E+00
1.86E+00
1.26E+00
2.83E+00
1.66E+00
1.79E+00
2.25E+00
1.95E+00
2.09E+00
f;? -:i--r,, nf3
0266
Eberline Analyt cal Oak Ridge Laboratory
Detector
LB4110A - Al
LB4110A - A2
LB4110A - A3
LB4110A - A4
LB4110A - Bl
LB4110A - B2
LB4110A - B3
LB4110A - B4
LB4110A - Cl
LB4110A - C2
LB4110A - C3
LB4110A - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A - F3
LB4110A - F4
LB411CA - Gl
LB411CA - G2
LB411CA - G3
LB411CA - G4
Alpha/Beta
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Alpha
Calibration Date
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
11/2/2017
GPC Detector Report (ALL Efficiencies)
Count Date Eff
7/11/2018 0.2275
7/11/2018 0.2161
7/11/2018 0.2016
7/11/2018 0.2221
7/11/2018 0.2202
7/11/2018 0.1946
7/11/2018 0.2337
7/11/2018 0.2164
7/11/2018 0.2047
7/11/2018 0.2180
7/11/2018 0.2411
7/11/2018 0.2130
7/11/2018 0.2250
7/11/2018 0.2523
7/11/2018 0.2477
7/11/2018 0.1939
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
3/23/2018 0.0000
7/11/2018 0.2178
7/11/2018 0.1823
7/11/2018 0.2377
7/11/2018 0.2057
7/11/2018 0.1998
7/11/2018 0.2059
7/11/2018 0.2279
7/11/2018 0.1952
PFW LCL
p 0.2156
p 0.2006
p 0.1853
p 0.2114
p 0.2028
p 0.1824
p 0.2169
p 0.2060
p 0.1961
p -0.1424
p 0.2299
p 0.1993
p 0.2109
p 0.2355
p 0.2378
p 0.1824
F 0.1687
F 0.1518
F 0.1547
F 0.1747
p 0.1483
p 0.1776
p 0.2312
p 0.2019
p 0.1904
p 0.1941
p 0.2154
p 0.1914
Printed:
Mean
0.2257
0.2111
0.1999
0.2267
0.2226
0.2009
0.2344
0.2215
0.2077
0.2267
0.2425
0.2149
0.2219
0.2517
0.2500
0.1955
0.2258
0.2051
0.2075
0.2355
0.2131
0.1845
0.2382
0.2109
0.1991
0.2025
0.2250
0.1997
7/11/2018 7:16 AM ~Y/ rL Page 1 of 1 •1,-/() jc:7
UCL
0.2357
0.2216
0.2144
0.2421
0.2425
0.2193
0.2518
0.2369
0.2193
0.5958
0.2551
0.2304
0.2329
0.2679
0.2622
0.2086
0.2830
0.2584
0.2603
0.2963
0.2779
0.1915
0.2452
0.2200
0.2078
0.2109 I
0.2345
0.2079
0267
Eberline Analytical Oak Ridge Laboratory
Detector
LB4110A - Al
LB411(,A - A2
LB411CA - A3
LB411CA - A4
LB411CA - Bl
LB411CA - B2
LB411CA - B3
LB411CA - B4
LB411CA - Cl
LB411CA - C2
LB411CA - C3
LB411CA - C4
LB4110A - D1
LB4110A - D2
LB4110A - D3
LB4110A. - D4
LB4110A - El
LB4110A - E2
LB4110A - E3
LB4110A - E4
LB4110A - Fl
LB4110A - F2
LB4110A. - F3
LB4110A. - F4
LB4110A - Gl
LB4110A - G2
LB4110/\ - G3
LB4110i'\ - G4
Alpha/Beta Calibration Date
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
Beta 11/2/2017
GPC Detector Report (ALL Efficiencies)
Count Date Eff
7/11/2018 0.5488
7/11/2018 0.4709
7/11/2018 0.4783
7/11/2018 0.5486
7/11/2018 0.5288
7/11/2018 0.4978
7/11/2018 0.5971
7/11/2018 0.5322
7/11/2018 0.4772
7/11/2018 0.5198
7/11/2018 0.6054
7/11/2018 0.5120
7/11/2018 0.6424
7/11/2018 0.6435
7/11/2018 0.6387
7/11/2018 0.5044
3/23/2018 0.0436
3/23/2018 0.0428
3/23/2018 0.0551
3/23/2018 0.0569
7/11/2018 0.5376
7/11/2018 0.4733
7/11/2018 0.6204
7/11/2018 0.5353
7/11/2018 0.4446
7/11/2018 0.4920
7/11/2018 0.5425
7/11/2018 0.4838
PFW
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
p
F
F
F
F p
p
p
p
p
p
p
p
Printed: 7/11/2018 7:16 AM l? Page 1 of 1-::j- /\ \ /\ ~
LCL Mean UCL
0.5123 0.5366 0.5609
0.4286 0.4633 0.4980
0.4424 0.4784 0.5143
0.5061 0.5417 0.5774
0.4983 0.5384 0.5785
0.4605 0.4994 0.5384
0.5434 0.5818 0.6202
0.5062 0.5441 0.5821
0.4452 0.4808 0.5164
0.4955 0.5192 0.5430
0.5691 0.5995 0.6300
0.4857 0.5257 0.5657
0.6208 0.6409 0.6610
0.6033 0.6440 0.6847
0.6135 0.6418 0.6700
0.4764 0.5026 0.5288
0.4162 0.5409 0.6655
0.3730 0.4913 0.6097
0.3852 0.4994 0.6137
0.4534 0.5890 0.7247
0.3683 0.5285 0.6886
0.4416 0.4611 0.4806
0.5950 0.6145 0.6339
0.5178 0.5344 0.5509
0.4391 0.4582 0.4773
0.4753 0.4875 0.4996
0.5234 0.5438 0.5642
0.4688 0.4870 0.5053