air sparge system upgrade and monitoring well …

75
Antea USA, Inc. AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL INSTALLATION REPORT Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, Washington Ecology VCP No. NW2684 Antea ® Group Project No. I42603142 August 9, 2016 Prepared for: Platinum Energy 30343 Canwood Street, Suite 200 Agoura Hills, CA 91301 Prepared by: Antea®Group 4006 148 th Avenue NE Redmond, WA 98052 800 477 7411

Upload: others

Post on 04-Dec-2021

7 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Antea USA, Inc.

AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL INSTALLATION REPORT

Former Platinum Energy Station No. 2603142

2841 South 188th Street, SeaTac, Washington

Ecology VCP No. NW2684

Antea®Group Project No. I42603142 August 9, 2016

Prepared for: Platinum Energy 30343 Canwood Street, Suite 200 Agoura Hills, CA 91301

Prepared by: Antea®Group 4006 148th Avenue NE Redmond, WA 98052 800 477 7411

Page 2: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page i

www.anteagroup.com

TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY ...................................................................................................................................... 1

2.0 CONSTRUCTION IMPLEMENTATION ................................................................................................................. 2

2.1 Pre-Construction Meeting ............................................................................................................................ 2

2.2 Well Installation ........................................................................................................................................... 2

2.3 Mobilization and Construction Facilities ...................................................................................................... 3

3.0 REMEDIATION SYSTEM EXPANSION ................................................................................................................. 4

3.1 Layout of System Components .................................................................................................................... 4

3.2 Trenching and Surface Restoration .............................................................................................................. 4

3.3 Remediation System Equipment .................................................................................................................. 5

4.0 CONSTRUCTION COMPLETION AND SYSTEM STARTUP ................................................................................... 5

5.0 SPARGE WELL RE-DRILLING .............................................................................................................................. 5

6.0 CONCLUSION AND RECOMMENDATIONS ........................................................................................................ 6

7.0 REMARKS .......................................................................................................................................................... 8

Table

Table 1 Summary of Soil Analytical Results

Figures

Figure 1 Cover

Figure 2 Legend

Figure 3 Site Map with Installed Air Sparge Trench Layout

Figure 4 System Compound and Trench Layout Details

Figure 5 Air Sparge Well Details

Figure 6 Air Sparge Piping and Instrumentation Diagram

Appendices

Appendix A Boring Logs

Appendix B Laboratory Analytical Report

Appendix C Waste Manifest

Page 3: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

www.anteagroup.com

Air Sparge System Upgrade and Monitoring

Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Ecology VCP No.: NW2684

Antea®Group (Antea Group) has prepared this report to summarize remediation system and well installation

activities performed at the former Platinum Energy Station No. 2603142 located at 2841 South 188th Street in

SeaTac, King County, Washington (hereinafter referred to as “the Property”). In June 2014, five air sparge (AS)

wells (AS-2, 3, 4, and 5) and one soil vapor extraction (SVE) well, HSVE-1, were installed and connected in order to

expand the influence and increase effectiveness of the current air sparging and soil vapor extraction (AS/SVE)

remediation system. Additionally, monitoring well MW-22 was installed to monitor groundwater conditions

downgradient of the existing monitoring well network. Groundwater monitoring and AS/SVE system testing

performed in 2015 showed that the remediation system upgrades were not performing effectively in the northeast

portion of the Property because the thin perched water-bearing zone was not being influenced. Therefore, air

sparge wells AS-2, AS-3, and AS-4 were re-drilled as wells AS-2A, AS-3A, and AS-4A, respectively, in September

2015 in order to place the well screen at a shallower depth, thus improving remediation efficacy.

1.0 EXECUTIVE SUMMARY

Antea Group provided remediation system design services, project management, oversight and quality assurance

during the design and construction of five new AS wells (AS-2 through AS-6), one horizontal SVE well (HSVE-1) and

retrofitting to the existing SVE/AS system. The existing system was installed by a previous site owner and did not

successfully remediate the Property to the point of obtaining a “No Further Action” status. The five new AS wells

were installed near monitoring wells MW-7 and MW-13 in order to further remediate soil and groundwater

hydrocarbon impacts in these areas. Cascade Drilling, Inc. (Cascade) of Woodinville, Washington was contracted to

perform drilling and well installation activities. IO Environmental & Infrastructure, Inc. (IO) of Redmond,

Washington was contracted to perform trenching activities, installation of new lateral AS lines, installation of a

new HSVE well, and to make the necessary equipment, well, and electrical connections. The new AS wells and the

new HSVE well were connected to existing remediation equipment already sized for the planned demand. The

work took place in June and July of 2014.

Additionally, Antea Group directed the installation of one groundwater monitoring well, MW-22, in the southwest

portion of the Property in order to monitor groundwater conditions downgradient of the existing monitoring well

network. The work took place concurrently with the AS well drilling that occurred in June 2014. Monitoring well

Page 4: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 2

www.anteagroup.com

MW-22 was drilled to 19.5 feet below ground surface (bgs) and was screened from 4.5 to 19.5 feet bgs. Soil

samples were collected at depths of 5, 10, and 15 feet bgs for laboratory analysis. Concentrations of petroleum

hydrocarbons were not detected above the respective Washington State Department of Ecology (Ecology) Model

Toxics Control Act (MTCA) Method A cleanup levels and laboratory method reporting limits (MRLs).

Operation of the retrofitted AS/SVE system was initiated in February 2015. Adequate air flow was observed within

wells AS-5 and AS-6; however, testing indicated that wells AS-2, AS-3, and AS-4 were likely screened within less

permeable soils beneath the perched water bearing zone which was preventing acceptable air flow at optimum air

injection pressures. Antea Group and Holocene Drilling Inc. (Holocene) of Puyallup, Washington mobilized to the

Property in September 2015 to install new air sparge wells adjacent to wells AS-2, AS-3, and AS-4. The screens of

the new wells AS-2A, AS-3A, and AS-4A were installed at shallower depths in order to better influence the perched

water unit.. The re-drilled wells were installed with 2-foot screens set from 13 to 15 feet bgs (AS-2A and AS-3A)

and from 13.5 to 15.5 feet bgs (AS-4A) with one foot sumps set below the screen. Antea Group disconnected the

AS conveyance piping at wells AS-2, AS-3, and AS-4 and re-connected the piping to the new AS wells. Additionally,

wells AS-2 through AS-4 were abandoned in place by Holocene according to the requirements of Ecology’s Water

Well Construction Act (1971) Chapter 18.104 RCW (WAC 173-160-460).

2.0 CONSTRUCTION IMPLEMENTATION

2.1 Pre-Construction Meeting

On March 5, 2014, an on-site pre-construction meeting was attended by representatives of IO and Antea Group.

Issues discussed during the meeting included the project objectives, plans and specifications, contract timing,

health and safety issues, lines of communication, roles and responsibilities, and work days and hours.

2.2 Well Installation

On June 23 and 24, 2014, Antea Group personnel directed Cascade in the installation of monitoring well MW-22

and air sparge wells AS-2 through AS-6. The wells were installed using an 8.25-inch diameter hollow stem auger

drill rig. Monitoring well MW-22 was installed to a total depth of 19.5 feet bgs and completed with 15 feet of

0.010-inch slotted screen from 4.5 feet bgs to 19.5 feet bgs. A sand filter pack was placed from 3 feet bgs to 19.5

feet bgs. The well was completed with a 1.5 foot seal of hydrated bentonite chips, 1.5 feet of concrete and a flush

mounted well monument. Soil samples were collected at depths of 5, 10, and 15 feet bgs and submitted to ALS

Environmental (ALS) of Everett, Washington for quantitative chemical analysis of total petroleum hydrocarbons as

gasoline (TPH-G), total petroleum hydrocarbons as diesel (TPH-D), total petroleum hydrocarbons as oil (TPH-O),

and for benzene, toluene, ethylbenzene, and total xylenes (BTEX). Laboratory analysis indicated that the

concentration of each analyte in each sample was below the respective MTCA Method A cleanup levels and MRLs.

Page 5: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 3

www.anteagroup.com

Air sparge wells AS-2 through AS-6 were each installed to a total depth of 25 feet bgs and completed with two feet

of 0.010-inch slotted screen from 21 feet to 23 feet bgs. An additional 2-foot sump was installed at the bottom of

the screened interval of each AS well to collect any silt or sediment that may enter the well and avoid fouling the

screen. A sand pack was placed from 19 to 25 feet bgs and followed by a bentonite seal from 4 feet bgs to 19 feet

bgs. The wells were temporarily completed with sand from 6 inches bgs to 4 feet bgs and a 6-inch concrete patch

to allow for the wells to be later connected to the air sparge lines. Soil samples were collected at 5, 10, 15, 20, and

25 feet bgs from each boring location and submitted to ALS for quantitative chemical analysis of TPH-G, TPH-D,

TPH-O, and BTEX constituents. Concentrations of TPH-G were detected above the MTCA Method A cleanup level

in the 15 feet bgs sample in well AS-2, the 5 and 10 feet bgs samples of well AS-3, and the 5 and 10 feet bgs

samples of well AS-4 at concentrations ranging from 88 milligrams per kilogram (mg/kg) to 1,000 mg/kg. All

remaining analytes were not detected above the respective MTCA Method A cleanup levels and/or laboratory

MRLs. A summary of soil analytical results is present in Table 1. The laboratory analytical report is included in

Appendix B.

The soils observed during the installation of wells MW-22 and AS-2 through AS-6 consisted of sandy silts, sandy

gravelly silts, silty sands, clayey gravelly sands, and silty gravelly sands, which is consistent with soils that were

observed in previous subsurface investigations. The thickest silt layer was discovered in the northeast corner of

the Property at approximately 20 feet bgs.

Soil cuttings generated during drilling activities were placed in 55-gallon drums and stored within the remediation

system compound until they were picked up by Philips Service Coloration (PSC) on October 3, 2014 and

transported to Burlington Environmental in Kent, Washington for disposal. Waste manifest documentation is

included in Appendix B.

2.3 Mobilization and Construction Facilities

On July 21, 2014, IO and Antea Group began equipment mobilization activities and general preparations.

Arrangements for storage of materials, equipment, and site security were made with Platinum Energy. The

southwest portion of the Property adjacent to the remediation equipment compound was used for storage of the

steel plates for the duration of the project. Additional equipment was kept in the subcontractors’ trailer and

removed from the Property at the end of each work day. Subcontractors mobilized equipment used for excavating

and trenching, plumbing, concrete removal, soil disposal transport, concrete finish work, asphalt placement, and

equipment placement. Antea Group representatives were continually on-site from the time field activities were

initiated through completion of subgrade construction activities, equipment placement, and resurfacing work.

Page 6: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 4

www.anteagroup.com

3.0 REMEDIATION SYSTEM EXPANSION

3.1 Layout of System Components

Antea Group notified the State of Washington One Call Service and contracted with a private utility locating

company prior to any intrusive work at the Property. On July 21, 2014, representatives of Antea Group and IO

established locations of trenching layouts at the Property. The location of the trenches were adjusted based on

utility locates, relevant site conditions, and Property owner concerns.

3.2 Trenching and Surface Restoration

IO began trenching activities by laying out trenches as per the plans and adjustments decided in the field, as

described above. The new addition to the remediation system layout is included in Figure 3. Excavation work was

initiated at the Property on July 21, 2014 and all surface restoration work was completed by July 28, 2014.

Micro-trenching techniques were used for installation of the AS lines in order to minimize waste, impact on the

surrounding area, and the chance of encountering subsurface obstructions. Trenching activities began at the

equipment compound and proceeded towards the wells to avoid problems of encountering obstacles which would

require a change in layout. The asphalt was saw cut at a width of 6 inches and removed by hand. Soil was then

cleared to 10 inches bgs using a vacuum truck. Asphalt cutting was performed by Evergreen Concrete Cutting, Inc.

and soil removal was completed by Marine Vacuum Services, Inc. (Mar-Vac).

Once the trench was cleared, the single, two-inch diameter schedule 80 SVE line and the five one-inch diameter

schedule 80 PVC air sparge lines were placed within the trench. Well HSVE-1 was installed in the northeast portion

of the Property in the trench connecting to well AS-3 and was constructed from a 6-foot run of 0.010-inch slotted

2-inch diameter schedule 80 PVC. The HSVE piping extends back to the SVE system and was connected to the

existing moisture separator. A 14-gauge locating wire was set above the piping near the center of the trench. The

locating wire runs the entire distance of the trench and was brought up to surface at the equipment compound.

The air sparge lines were connected to the air sparge wells with a 2-inch to 1-inch reducing PVC tee. Once

connections to the wells were complete, pressure testing of the lines was performed. Packers were temporarily

installed in each AS well casing at the tee and compressed air was introduced into the lines. A compressor was

used to fill each line until a pressure of 30 pounds per square inch (PSI) was reached. The pressure was maintained

for thirty minutes at each well to pass the test. Upon completion of the pressure test, the lines were covered by

controlled density fill (CDF) to approximately 3 inches bgs. The surface was restored with sanded asphalt to match

the existing surface. Surface restoration activities were completed by AC Paving Northwest, Inc.

Asphalt spoils that were generated on July 21, 2014 were temporarily placed on visqueen sheeting and covered

overnight. The asphalt was collected the following day by Mar-Vac. Minimal waste was generated during the

Page 7: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 5

www.anteagroup.com

micro-trenching process and all excavation work was performed using a Mar-Vac vacuum truck. This allowed for

all soil to be contained within the vacuum truck and no drums or stockpiles of soil were left on-site.

3.3 Remediation System Equipment

The expanded AS system receives air from a rotary claw compressor capable of discharging 30 standard cubic feet

per minute (scfm) of air at 28 psi. On November 18 and 19, 2014, the AS manifold was installed along the southern

fence of the remediation compound. The manifold connects the air compressor to new air sparge wells AS-2

through AS-6 and also existing sparge well AS-1. Each leg includes an isolation valve, flow meter, and pressure

gauge. Figures 3 through 6 include site plans, trench details with cross-sections and piping elevations, a system

enclosure layout diagram, and a piping and instrumentation diagram.

4.0 CONSTRUCTION COMPLETION AND SYSTEM STARTUP

The air sparge system was turned on December 14, 2014. Upon startup, the air sparge lines held pressure at 15 psi

and flow readings were zero on the sparge manifold after an initial rush of air. It was concluded that the existing

air sparge blower was not strong enough to push air down the air sparge wells. Flow was present at the well

monuments after removing the caps. Antea Group began troubleshooting the system on February 5, 2015. Antea

Group personnel rented a gas-powered air compressor capable of 150 psi. The compressor was connected to the

air sparge manifold in place of the existing compressor. At pressures of 50 to 65 psi, sparge wells AS-2 and AS-3

could hold flow. At a pressure rating of 75 psi, flow entered well AS-4.

Based on these results, Antea Group recognized that the three air sparge wells in the northeast corner of the

Property (AS-2 through AS-4) had likely been screened in dense glacial till that underlies the perched water bearing

zone where hydrocarbon impacts have been identified. The glacial till is common in the region and is relatively

impermeable even though it resembles a more permeable soil when disturbed and crumbled during drilling.

Thus, the injected air was not able to exit the well screens at an acceptable pressure and flow, and would not be

likely to reach the perched water unit as intended to increase dissolved oxygen levels. After considering other

blowers or methods of increasing air pressure, Antea Group decided that the most effective solution would be to

re-drill the three wells. The air sparge compressor ran in the months during the testing and well re-drilling,

supplying air to wells AS-1, AS-5, and AS-6 but not to the wells located in the northeast corner (AS-2 through AS-4).

5.0 SPARGE WELL RE-DRILLING

On September 30, 2015, Antea Group directed the installation of three new air sparge wells at the northeast

corner of the Property. The wells were labeled AS-2A, AS-3A, and AS-4A, and were drilled just upstream of air

sparge wells AS-2, AS-3, and AS-4, respectively, so that the new wells could be plumed into the existing air sparge

Page 8: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 6

www.anteagroup.com

system piping during drilling. Utility locates were performed on the morning of September 30, and the boreholes

were vacuum/air knife cleared to 5 feet bgs, which also exposed the one inch air sparge lines. The lines were cut

and capped upstream of the old wells.

Well AS-4A is screened from 13.5 feet to 15.5 feet bgs. Wells AS-2A and AS-3A are screened from 13 feet to 15

feet bgs. These screens are significantly shallower than the old air sparge wells in order to avoid penetrating too

far into the glacial till that was identified and was likely preventing sparge flow from leaving the well casing of wells

AS-2 through AS-4. The 0.010-inch slotted screens are still deep enough to be underwater for the majority of the

year. A sand pack extends a foot below and above the new air sparge well screens. The wells were the completed

with bentonite chips to 1.5 feet bgs, followed by sand, concrete, and a flush well monument. The wells were

plumbed into the existing air sparge piping, utilizing 2-inch to 1-inch tees to connect the pipe runs to the sparge

wells. Well HSVE-1, also in the northeast corner of the Property, was not disturbed during the sparge well re-

drilling. Original sparge wells AS-2 through AS-4 were abandoned in place by Holocene according to the

requirements of Ecology’s Water Well Construction Act (1971) Chapter 18.104 RCW (WAC 173-160-460).

At the conclusion of the drilling on October 2, 2015, the new air sparge wells were tested for flow using the air

sparge system compressor. Flow was present at sparge wells AS-2A and AS-3A, but not at AS-4A. It is possible that

some bentonite may have clogged the AS-4A well screen since the well was slightly overdrilled and backfilled with

some bentonite. A separate electrical oil-free compressor was installed in the equipment compound on October

16, 2015 to supply flow separately to well AS-4A at a slightly higher pressure of 30 psi. Antea Group installed a

timer on this compressor and as of December 31, 2015, the compressor is set to run for two 1.5-hour cycles in the

morning and evening to limit motor wear.

6.0 CONCLUSION AND RECOMMENDATIONS

Between June 2014 and October 2015, Antea Group upgraded the Property’s AS/SVE system to improve

remediation efficiency. Results of the initial upgrade confirmed that additional modifications including the re-

drilling of three of the new air sparge wells and adding a separate compressor for well AS-4A were warranted to

achieve remediation effectiveness in the northeast portion of the Property. The expanded system has been

consistently operating since these adjustments were made. The system has been optimized by Antea Group to

promote air flow in areas of the Property which contain petroleum hydrocarbon impacted groundwater. Monthly

system monitoring and quarterly groundwater monitoring events confirm that system operation is effective.

A preliminary review of the data collected during the first quarter groundwater monitoring event of 2016 indicates

that the last two monitoring wells (MW-7 and MW-17) at the Property that had been remaining above the MTCA

Method A cleanup levels are now in compliance. Antea Group will continue to operate the AS/SVE system until

groundwater levels at the Property consistently meet the MTCA Method A cleanup levels. Once a practical

Page 9: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142 August 9, 2016 Page 7

www.anteagroup.com

remediation endpoint is achieved, Antea Group will shut down the system. One year (four consecutive quarters)

of groundwater compliance monitoring will be performed and a “No Further Action” status will be requested from

Ecology.

Page 10: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 11: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142

www.anteagroup.com

Antea USA, Inc.

Table

Table 1 Summary of Soil Analytical Results

Page 12: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

TABLE 1

SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS

Former Platinum Energy Facility No. 26031422841 S 188th St

SeaTac, Washington

Sample IDSample

Date

Depth BGS

(feet)

Gasoline

Range

(mg/kg)

Diesel

Range

(mg/kg)

Oil

Range

(mg/kg)

Benzene

(mg/kg)

Toluene

(mg/kg)

Ethyl-

benzene

(mg/kg)

Total

Xylenes

(mg/kg)

MW-22-5 6/23/2014 5 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20MW-22-10 6/23/2014 10 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20MW-22-15 6/23/2014 15 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-2-5 6/23/2014 5 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-2-10 6/23/2014 10 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-2-15 6/23/2014 15 88 <25 <50 <0.60 <1.0 <1.0 <4.0AS-2-20 6/23/2014 20 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-2-25 6/23/2014 25 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-3-5 6/23/2014 5 1000 420 <50 <0.030 0.14 2.9 6.6AS-3-10 6/23/2014 10 200 <25 <50 <0.30 <0.50 <0.50 <2.0AS-3-15 6/23/2014 15 13 <25 <50 <0.030 <0.050 <0.050 <0.20AS-3-20 6/23/2014 20 5.8 <25 <50 <0.030 <0.050 <0.050 <0.20AS-3-25 6/23/2014 25 3.8 <25 <50 <0.030 <0.050 <0.050 <0.20AS-4-5 6/23/2014 5 330 30 <50 <0.030 <0.050 <0.050 0.40AS-4-10 6/24/2014 10 110 <25 <50 <0.60 <1.0 <1.0 <4.0AS-4-15 6/24/2014 15 3.6 <25 <50 <0.030 <0.050 <0.050 <0.20AS-4-20 6/24/2014 20 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-4-25 6/24/2014 25 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-5-5 6/23/2014 5 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-5-10 6/24/2014 10 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-5-15 6/24/2014 15 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-5-20 6/24/2014 20 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-5-25 6/24/2014 25 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-6-5 6/23/2014 5 <3.0 <25 72 <0.030 <0.050 <0.050 <0.20AS-6-10 6/24/2014 10 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-6-15 6/24/2014 15 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-6-20 6/24/2014 20 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20AS-6-25 6/24/2014 25 <3.0 <25 <50 <0.030 <0.050 <0.050 <0.20MTCA Method A Cleanup Levels: 100/30

a 2,000 2,000 0.03 7 6 9

NOTES:

All concentrations are in milligrams per kilogram (mg/kg). < = Less than the stated laboratory reporting limit.Gasoline range = Gasoline range hydrocarbons by Ecology Method NWTPH-GxDiesel range = Diesel range hydrocarbons by Ecology Method NWTPH-Dx with silica gel cleanupOil range = Oil range hydrocarbons by Ecology Method NWTPH-Dx with silica gel cleanupBTEX = Aromatic compounds by EPA Method 8260Bold indicates exceedance above the MTCA Method A cleanup level.

is present.

a MTCA Method A Cleanup levels for TPH-g are 100 mg/kg when no Benzene is present and 30 mg/kg when Benzene

Analysis

Page 1

Page 13: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142

www.anteagroup.com

Antea USA, Inc.

Figures

Figure 1 Cover

Figure 2 Legend

Figure 3 Site Map with Installed Air Sparge Trench Layout

Figure 4 System Compound and Trench Layout Details

Figure 5 Air Sparge Well Details

Figure 6 Air Sparge Piping and Instrumentation Diagram

Page 14: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 15: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 16: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 17: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 18: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 19: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 20: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142

www.anteagroup.com

Antea USA, Inc.

Appendix A

Boring Logs

Page 21: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23/2014

BORING DEPTH: 19.5'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 4.5' – 19.5' (0.010)SAND PACK: 3' – 19.5' (2x12)

Co

ncre

teB

en

ton

ite

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

ML

Surface = Asphalt.Air knife/vac to 5' bgs.

Sandy SILT: brown; 80% silt; 15% fine to coarse sand; trace gravel; no odor.

San

d

-

-

-

WELL/BORING: MW – 22

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty SAND: brown; 25% silt; 65% medium sand; 10% fine to coarse subrounded gravel; no odor.

SM Silty Gravelly SAND: brown; 30% silt; 40% medium sand; 30% coarse subrounded gravel; no odor.

DRY 0.0 -

DRY 0.0 2850/6"

DMP 0.2 1450/6"

Cobbles @ 19.5'No Recovery

Unique Ecology Well ID: BHL 528

Page 22: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23/2014

BORING DEPTH: 25'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Concrete

Be

nto

nit

e

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

SP SAND: brown; 100% medium sand; no odor.

San

d

-

-

-

WELL/BORING: AS – 2

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Gravelly Sandy SILT: brownish gray; 40% silt; 35% fine to medium sand; 25% fine to coarse gravel; no odor.

SM Silty SAND: gray; 30% silt; 65% fine to medium sand; trace medium to coarse gravel; odor.

DRY 0.0 -

DRY 7.9 131416

DRY 86.0 50/6"

Silty SAND: gray; 40% silt; 55% sand; trace medium to coarse gravel; no odor.

Unique Ecology Well ID: BHL 529

DRY 8.5 50/6" SM

San

d

Page 23: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23/2014

DESCRIPTION/LOGGED BY: Eric Sanchez

San

d

-

-

-

WELL/BORING: AS – 2

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty SAND: gray; 40% silt; 55% sand; trace medium to coarse gravel; no odor.

DMP 9.2 50/4"

Unique Ecology Well ID: BHL 529

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

43

44

BORING DEPTH: 25'

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Page 24: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Be

nto

nit

eS

an

dS

an

d

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23/2014

BORING DEPTH: 25'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Concrete

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

ML

Surface = Asphalt.Air knife/vac to 5' bgs.

Sandy SILT: gray; 80% silt; 15% fine to coarse sand; trace fine gravel; odor.

-

-

-

WELL/BORING: AS – 3

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

ML Sandy SILT: brown; 60% silt; 35% fine to medium sand; trace fine to medium gravel; odor.

SM Silty Gravelly SAND: gray; 25% silt; 45% fine to medium sand; 30% fine to medium subrounded gravel; odor.

DRY 3,022 -

MST 59.4 50/2"

DRY 17.4 50/6"

Same as above.

Unique Ecology Well ID: BHL 530

MST 9.9 50/6" SM

Page 25: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23/2014

DESCRIPTION/LOGGED BY: Eric Sanchez

San

d

-

-

-

WELL/BORING: AS – 3

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty Gravelly SAND: gray; 25% silt; 45% fine to medium sand; 30% fine to medium subrounded gravel; odor.

DRY 15.0 50/3"

Unique Ecology Well ID: BHL 530

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

43

44

BORING DEPTH: 25'

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Page 26: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Be

nto

nit

eS

an

dS

an

d

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

BORING DEPTH: 25'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Concrete

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

ML

Surface = Asphalt.Air knife/vac to 5' bgs.

Sandy Gravelly SILT: brownish gray; 75% silt; 10% fine to medium sand; 15% fine to coarse gravel; trace cobbles; odor.

-

-

-

WELL/BORING: AS – 4

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty SAND: gray; 20% silt; 75% fine to coarse sand; trace fine gravel; odor.

SM Silty Gravelly SAND: light brown; 35% silt; 50% fine to coarse sand; 15% fine gravel; no odor.

DRY 856.1 -

MST 1,354 152527

DRY 4.8 50/6"

Sandy Gravelly SILT: gray; 55% silt; 30% fine to medium sand; 15% fine to coarse gravel; no odor.

Unique Ecology Well ID: BHL 531

DRY 0.3 50/6" ML

Page 27: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

DESCRIPTION/LOGGED BY: Eric Sanchez

San

d

-

-

-

WELL/BORING: AS – 4

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty Gravelly SAND: gray; 30% silt; 50% sand; 20% gravel; no odor.

WET 3.0 50/6"

Unique Ecology Well ID: BHL 531

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

43

44

BORING DEPTH: 25'

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Page 28: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Be

nto

nit

eS

an

dS

an

d

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

BORING DEPTH: 25'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Concrete

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

ML

Surface = Asphalt.Air knife/vac to 5' bgs.

Sandy Gravelly SILT: brown; 50% silt; 30% fine to medium sand; 20% fine to medium subrounded gravel; no odor.

-

-

-

WELL/BORING: AS – 5

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty Gravelly SAND: brown; 30% silt; 45% fine to medium sand; 25% medium to coarse subrounded gravel; no door.

SM Silty Gravelly SAND: gray; 30% silt; 50% fine to coarse sand; 20% fine to coarse subrounded gravel; slight odor.

DRY 0.0 -

DRY 0.0 122031

WET 1.6 50/6"

Clayey Gravelly SAND: grayish brown; 30% clay; 45% fine to coarse sand; 25% fine to coarse gravel; no odor.

Unique Ecology Well ID: BHL 532

WET 0.0 50/6" SC

Page 29: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

DESCRIPTION/LOGGED BY: Eric Sanchez

San

d

-

-

-

WELL/BORING: AS – 5

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SC Clayey Gravelly SAND: grayish brown; 30% clay; 45% fine to coarse sand; 25% fine to coarse gravel; no odor.

WET 0.0 50/6"

Unique Ecology Well ID: BHL 532

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

43

44

BORING DEPTH: 25'

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Page 30: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Be

nto

nit

eS

an

dS

an

d

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

BORING DEPTH: 25'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Concrete

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

SM

Surface = Asphalt.Air knife/vac to 5' bgs.

Silty Gravelly SAND: brown; 30% silt; 40% fine to coarse sand; 30% fine to coarse gravel; cobbles in borehole; no odor.

-

-

-

WELL/BORING: AS – 6

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Silty Gravelly SAND: brown; 10% silt; 70% fine to medium sand; 20% fine to medium gravel; no odor.

SC Clayey SAND: gray; 30% clay; 70% medium to coarse sand; no odor.

DRY 1.0 -

MST 0.0 2350/6"

WET 0.8 50/6"

Same as Above.

Unique Ecology Well ID: BHL 533

WET 0.5 64/4" SC

Page 31: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Cascade Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 6/23-24/2014

DESCRIPTION/LOGGED BY: Eric Sanchez

San

d

-

-

-

WELL/BORING: AS – 6

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SC Clayey Gravelly SAND: gray; 30% clay; 40% fine to coarse sand; 30% fine to coarse gravel; no odor.

WET 1.1 65/6"

Unique Ecology Well ID: BHL 533

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

43

44

BORING DEPTH: 25'

WELL SCREEN: 21' – 23' (0.010)SAND PACK: 19' – 25' (2x12)

Page 32: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Holocene Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 9/30-10/2/2015

BORING DEPTH: 16.5'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 13-15' (0.020)SAND PACK: 12.5-16.5' (10x20)

Co

ncre

teB

en

ton

ite

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

SM

Surface = Asphalt 4"Air knife/vac to 5' bgs.

Silty Gravelly SAND: brown; 20% silt; 75% fine to medium sand; 5% fine to medium gravel.

San

d

-

-

-

WELL/BORING: AS-2A

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Same as Above: gray @11'; slight odor.

SM Silty Gravelly SAND: gray; 10% silt; 85% fine to medium sand; 5% fine to medium gravel; slight odor.

MST 9.3 649

MST

7.2

101218

MST8.9

3.850/4"

Unique Ecology Well ID: BJX 712

SM Same as Above.MST373

1750/5"

SM Silty SAND: gray; 15% silt; 80% fine sand; trace fine gravel; loose; odor.

MST177

41829

Page 33: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Holocene Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 9/30-10/1/2015

BORING DEPTH: 16.5'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 13-15' (0.020)SAND PACK: 12.5-16.5' (10x20)

Co

ncre

teB

en

ton

ite

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

SM

Surface = Asphalt 4"Air knife/vac to 5' bgs.

Silty Gravelly SAND: brown; 15% silt; 75% fine sand; 10% fine to medium gravel; loose.

San

d

-

-

-

WELL/BORING: AS-3A

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

No Recovery.

MST 5.3 61615

- - 50/6"

Unique Ecology Well ID: BJX 711

SM Silty Gravelly SAND: gray; 20% silt; 70% fine sand; 10% fine to medium gravel; odor.

MST 39.4 2850/3"

SM Silty SAND: gray; 20% silt; 75% fine to medium sand; trace medium gravel; dense; odor.

MST 2,085 163338

Page 34: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

WELL/BORINGCOMPLETION FI

RS

T

STA

BIL

IZE

D

MO

ISTU

RE

DE

NS

ITY

BLO

WS

/ 6"

PID

(ppm

)

DE

PTH

(FE

ET)

RE

CO

VER

Y

SAM

PLE

INTE

RV

AL

GR

AP

HIC

SURVEY DATE:

DTW:US

CS

S

YM

BO

L CASING ELEVATION

STATE: WADRILLER: Holocene Drilling, Inc.

SAMPLING METHOD: SPT DRILLING METHOD: HSA

BORING DIAMETER: 8.25"

WELL CASING: SCH 40 PVC 2"

INSTALLATION DATE: 9/30-10/1/2015

BORING DEPTH: 20.5'

DESCRIPTION/LOGGED BY: Eric Sanchez

WELL SCREEN: 13.5-15.5' (0.020)SAND PACK: 12.5-16' (10x20)

Co

ncre

teB

en

ton

ite

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

22

SM

Surface = Asphalt 4"Air knife/vac to 5' bgs.

Silty Gravelly SAND: gray; 10% silt; 80% sand; 10% fine to medium gravel.

-

-

-

WELL/BORING: AS-4A

PROJECT: I42603142CLIENT: ELTLOCATION: 2841 South 188th StreetCITY: SeaTac

SM Same as Above: increasing silt; odor.

MST 11.7 71014

MST 1,221 173440

Unique Ecology Well ID: BJX 710

SM Same as Above: very dense.MST20.7

3350/4"

SM Silty Gravelly SAND: gray; 20% silt; 70% sand; 10% fine gravel dense; odor. 1" medium sand lens @12'; wet.

MST 3,300 183750

San

d

SM Silty Gravelly SAND: brown; 15% silt; 75% fine to medium sand; 10% fine gravel.

MST3.8

4150/2"

SM Same as Above.DRY2.0

4150/3"

SM Same as Above.- - 4350/4"

SM Same as Above: increasing density. DRY 3.8 50/6"

Page 35: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142

www.anteagroup.com

Antea USA, Inc.

Appendix B

Laboratory Analytical Report

Page 36: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Mr. Joe Rounds

Antea Group

4006 - 148th Ave NE

Redmond, WA 98052

Dear Mr. Rounds,

On June 25th, 29 samples were received by our laboratory and assigned our laboratory project

number EV14060165. The project was identified as your 2603142. The sample identification and

requested analyses are outlined on the attached chain of custody record.

No abnormalities or nonconformances were observed during the analyses of the project samples.

Please do not hesitate to call me if you have any questions or if I can be of further assistance.

Sincerely,

ALS Laboratory Group

Rick Bagan

Laboratory Director

July 2, 2014

Page 1

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 37: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID MW-22-5

COLLECTION DATE: 6/23/2014 9:15:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-01

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC13.0 0.74 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/27/2014 DLC10.030 0.0060 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/27/2014 DLC10.050 0.0049 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.050 0.0056 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.20 0.015 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 9.3 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC1140 0.426 06/27XXXXXXXXX109 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/27/2014 DLC1140 0.426 06/27XXXXXXXXX109 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.93 06/30XXXXXXXXX111 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 2

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 38: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID MW-22-10

COLLECTION DATE: 6/23/2014 9:50:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-02

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC13.0 0.51 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/27/2014 DLC10.030 0.0041 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/27/2014 DLC10.050 0.0033 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.050 0.0039 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.20 0.010 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

06/30/2014 EBS125 8.5 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC1140 0.294 06/27XXXXXXXXX107 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/27/2014 DLC1140 0.294 06/27XXXXXXXXX110 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.61 06/30XXXXXXXXX98.4 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 3

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 39: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID MW-22-15

COLLECTION DATE: 6/23/2014 10:00:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-03

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC13.0 0.56 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/27/2014 DLC10.030 0.0045 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/27/2014 DLC10.050 0.0037 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.050 0.0042 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

06/30/2014 EBS125 8.9 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC1140 0.321 06/27XXXXXXXXX96.1 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/27/2014 DLC1140 0.321 06/27XXXXXXXXX94.6 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.78 06/30XXXXXXXXX92.5 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 4

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 40: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-2-5

COLLECTION DATE: 6/23/2014 10:15:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-04

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC13.0 0.70 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/27/2014 DLC10.030 0.0056 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/27/2014 DLC10.050 0.0046 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.050 0.0053 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.20 0.014 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

06/30/2014 EBS125 8.8 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC1140 0.403 06/27XXXXXXXXX101 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/27/2014 DLC1140 0.403 06/27XXXXXXXXX95.4 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.73 06/30XXXXXXXXX121 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 5

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 41: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-2-10

COLLECTION DATE: 6/23/2014 11:20:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-05

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC13.0 0.53 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/27/2014 DLC10.030 0.0042 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/27/2014 DLC10.050 0.0034 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.050 0.0040 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/27/2014 DLC10.20 0.010 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

06/30/2014 EBS125 9.2 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 DLC1140 0.301 06/27XXXXXXXXX110 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/27/2014 DLC1140 0.301 06/27XXXXXXXXX104 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.88 06/30XXXXXXXXX115 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 6

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 42: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-2-15

COLLECTION DATE: 6/23/2014 11:25:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-06

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC2060 12 20 06/27XXXX88 MG/KGTPH-Volatile Range NWTPH-GX XXX60XXXXX XXXXX

06/30/2014 DLC200.60 0.096 U20U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.60XXXXX XXXXX

06/30/2014 DLC201.0 0.079 U20U 06/27XXXX MG/KGToluene EPA-8021 XXX1.0XXXXX XXXXX

06/30/2014 DLC201.0 0.091 U20U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX1.0XXXXX XXXXX

06/30/2014 DLC204.0 0.24 U20U 06/27XXXX MG/KGXylenes EPA-8021 XXX4.0XXXXX XXXXX

06/30/2014 EBS125 8.7 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC20140 GS20.345ND- GS2 06/27XXXXXXXXX84.9 GS2TFT 20X Dilution NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/30/2014 DLC20140 GS20.345ND- GS2 06/27XXXXXXXXX102 GS2TFT 20X Dilution EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.69 06/30XXXXXXXXX106 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

GS2 - Surrogate outside of control limits due to dilution. U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 7

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 43: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-2-20

COLLECTION DATE: 6/23/2014 11:30:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-07

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC13.0 0.55 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/30/2014 DLC10.030 0.0044 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/30/2014 DLC10.050 0.0036 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/30/2014 DLC10.050 0.0042 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/30/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

06/30/2014 EBS125 8.3 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

06/30/2014 EBS150 16 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC1140 0.315 06/27XXXXXXXXX91.3 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/30/2014 DLC1140 0.315 06/27XXXXXXXXX92.2 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

06/30/2014 EBS1134 3.53 06/30XXXXXXXXX100 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 8

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 44: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-2-25

COLLECTION DATE: 6/23/2014 11:35:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-08

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.58 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0046 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0038 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0044 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 9.1 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.332 06/27XXXXXXXXX102 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.332 06/27XXXXXXXXX106 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.85 06/30XXXXXXXXX113 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 9

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 45: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-3-5

COLLECTION DATE: 6/23/2014 11:35:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-09

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC100300 73 100 06/27XXXX1000 MG/KGTPH-Volatile Range NWTPH-GX XXX300XXXXX XXXXX

06/28/2014 DLC10.030 0.0058 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0047 1 06/27XXXX0.14 MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0055 1 06/27XXXX2.9 MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.014 1 06/27XXXX6.6 MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 10 1 06/30XXXX420 MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 20 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC100140 GS20.416ND- GS2 06/27XXXXXXXXX160 GS2TFT 100X Dilution NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.416 06/27XXXXXXXXX102 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 4.36 06/30XXXXXXXXX79.5 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

GS2 - Surrogate outside of control limits due to dilution. U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline and weathered diesel 1.

Page 10

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 46: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-3-10

COLLECTION DATE: 6/23/2014 1:15:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-10

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC1030 5.7 10 06/27XXXX200 MG/KGTPH-Volatile Range NWTPH-GX XXX30XXXXX XXXXX

06/30/2014 DLC100.30 0.046 U10U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.30XXXXX XXXXX

06/30/2014 DLC100.50 0.037 U10U 06/27XXXX MG/KGToluene EPA-8021 XXX0.50XXXXX XXXXX

06/30/2014 DLC100.50 0.043 U10U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.50XXXXX XXXXX

06/30/2014 DLC102.0 0.11 U10U 06/27XXXX MG/KGXylenes EPA-8021 XXX2.0XXXXX XXXXX

07/01/2014 EBS125 8.7 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC10140 GS20.325ND- GS2 06/27XXXXXXXXX77.0 GS2TFT 10X Dilution NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/30/2014 DLC10140 GS20.325ND- GS2 06/27XXXXXXXXX92.9 GS2TFT 10X Dilution EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.71 06/30XXXXXXXXX119 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit. GS2 - Surrogate outside of control limits due to dilution.

Page 11

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 47: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-3-15

COLLECTION DATE: 6/23/2014 1:35:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-11

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.51 1 06/27XXXX13 MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0041 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0033 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0038 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.010 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 9.1 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.290 06/27XXXXXXXXX112 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.290 06/27XXXXXXXXX114 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.85 06/30XXXXXXXXX99.8 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 12

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 48: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-3-20

COLLECTION DATE: 6/23/2014 1:40:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-12

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.56 1 06/27XXXX5.8 MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0045 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0036 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0042 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 8.3 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 16 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.318 06/27XXXXXXXXX101 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.318 06/27XXXXXXXXX103 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.53 06/30XXXXXXXXX103 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 13

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 49: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-3-25

COLLECTION DATE: 6/23/2014 1:45:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-13

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.55 1 06/27XXXX3.8 MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0044 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0036 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0041 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 8.9 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.313 06/27XXXXXXXXX124 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.313 06/27XXXXXXXXX126 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.76 06/30XXXXXXXXX85.8 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 14

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 50: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-4-5

COLLECTION DATE: 6/23/2014 12:00:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-14

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC1030 8.0 10 06/27XXXX330 MG/KGTPH-Volatile Range NWTPH-GX XXX30XXXXX XXXXX

06/28/2014 DLC10.030 0.0064 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0052 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0060 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.016 1 06/27XXXX0.40 MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 9.1 1 06/30XXXX30 MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/30/2014 DLC10140 GS20.455ND- GS2 06/27XXXXXXXXX77.1 GS2TFT 10X Dilution NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.455 06/27XXXXXXXXX89.8 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.85 06/30XXXXXXXXX85.4 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

GS2 - Surrogate outside of control limits due to dilution. U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains weathered diesel 1.

Page 15

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 51: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-4-10

COLLECTION DATE: 6/24/2014 9:10:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-15

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC2060 11 20 06/27XXXX110 MG/KGTPH-Volatile Range NWTPH-GX XXX60XXXXX XXXXX

06/28/2014 DLC200.60 0.089 U20U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.60XXXXX XXXXX

06/28/2014 DLC201.0 0.072 U20U 06/27XXXX MG/KGToluene EPA-8021 XXX1.0XXXXX XXXXX

06/28/2014 DLC201.0 0.084 U20U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX1.0XXXXX XXXXX

06/28/2014 DLC204.0 0.22 U20U 06/27XXXX MG/KGXylenes EPA-8021 XXX4.0XXXXX XXXXX

07/01/2014 EBS125 9.4 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC20140 GS20.317ND- GS2 06/27XXXXXXXXX65.5 GS2TFT 20X Dilution NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC20140 GS20.317ND- GS2 06/27XXXXXXXXX35.0 GS2TFT 20X Dilution EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.98 06/30XXXXXXXXX89.0 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

GS2 - Surrogate outside of control limits due to dilution. U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 16

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 52: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-4-15

COLLECTION DATE: 6/24/2014 9:15:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-16

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.65 1 06/27XXXX3.6 MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0052 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0042 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0049 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.013 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 8.8 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.372 06/27XXXXXXXXX101 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.372 06/27XXXXXXXXX101 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.74 06/30XXXXXXXXX93.2 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains highly weathered gasoline.

Page 17

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 53: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-4-20

COLLECTION DATE: 6/24/2014 9:20:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-17

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.59 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0047 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0038 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0044 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.012 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 9.0 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.336 06/27XXXXXXXXX117 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.336 06/27XXXXXXXXX120 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.83 06/30XXXXXXXXX93.7 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 18

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 54: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-4-25

COLLECTION DATE: 6/24/2014 9:25:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-18

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.53 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0043 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0035 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0040 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.010 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/01/2014 EBS125 8.6 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/01/2014 EBS150 17 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.305 06/27XXXXXXXXX92.6 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.305 06/27XXXXXXXXX95.4 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/01/2014 EBS1134 3.62 06/30XXXXXXXXX95.6 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 19

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 55: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-5-5

COLLECTION DATE: 6/23/2014 1:55:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-19

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.76 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0061 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0050 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0058 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.015 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 9.4 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 18 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.437 06/27XXXXXXXXX106 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.437 06/27XXXXXXXXX107 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.97 06/30XXXXXXXXX91.0 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 20

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 56: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-5-10

COLLECTION DATE: 6/24/2014 11:35:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-20

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC13.0 0.54 U1U 06/27XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

06/28/2014 DLC10.030 0.0044 U1U 06/27XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

06/28/2014 DLC10.050 0.0035 U1U 06/27XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.050 0.0041 U1U 06/27XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

06/28/2014 DLC10.20 0.011 U1U 06/27XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 7.8 U1U 06/30XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 15 U1U 06/30XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/28/2014 DLC1140 0.311 06/27XXXXXXXXX104 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

06/28/2014 DLC1140 0.311 06/27XXXXXXXXX103 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.32 06/30XXXXXXXXX85.6 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 21

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 57: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-5-15

COLLECTION DATE: 6/24/2014 11:40:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-21

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.62 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0050 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0041 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0047 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.012 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 8.3 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 16 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.357 07/01XXXXXXXXX104 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.357 07/01XXXXXXXXX105 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.53 06/26XXXXXXXXX92.3 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 22

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 58: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-5-20

COLLECTION DATE: 6/24/2014 11:45:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-22

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.61 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0049 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0040 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0046 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.012 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 9.4 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 18 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.348 07/01XXXXXXXXX104 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.348 07/01XXXXXXXXX104 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.99 06/26XXXXXXXXX96.7 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 23

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 59: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-5-25

COLLECTION DATE: 6/24/2014 11:50:00 AM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-23

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.63 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0050 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0041 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0047 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.012 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 8.8 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 17 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.358 07/01XXXXXXXXX108 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.358 07/01XXXXXXXXX102 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.71 06/26XXXXXXXXX86.5 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 24

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 60: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-6-5

COLLECTION DATE: 6/23/2014 3:20:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-24

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.65 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0052 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0042 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0049 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.013 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 8.9 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 17 1 06/26XXXX72 MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.370 07/01XXXXXXXXX126 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.370 07/01XXXXXXXXX121 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.76 06/26XXXXXXXXX88.4 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains lube oil.

Page 25

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 61: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-6-10

COLLECTION DATE: 6/24/2014 1:40:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-25

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.54 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0043 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0035 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0040 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.011 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 9.0 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 17 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.306 07/01XXXXXXXXX113 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.306 07/01XXXXXXXXX110 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.80 06/26XXXXXXXXX82.1 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 26

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 62: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-6-15

COLLECTION DATE: 6/24/2014 1:45:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-26

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.63 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0050 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0041 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0047 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.012 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 8.3 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 16 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.359 07/01XXXXXXXXX98.6 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.359 07/01XXXXXXXXX97.1 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.53 06/26XXXXXXXXX89.4 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 27

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 63: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-6-20

COLLECTION DATE: 6/24/2014 1:50:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-27

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.68 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0054 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0044 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0051 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.013 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 7.8 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 15 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.388 07/01XXXXXXXXX112 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.388 07/01XXXXXXXXX112 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.30 06/26XXXXXXXXX85.9 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 28

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 64: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID AS-6-25

COLLECTION DATE: 6/24/2014 1:55:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-28

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC13.0 0.80 U1U 07/01XXXX MG/KGTPH-Volatile Range NWTPH-GX XXX3.0XXXXX XXXXX

07/01/2014 DLC10.030 0.0064 U1U 07/01XXXX MG/KGBenzene EPA-8021 XXX0.030XXXXX XXXXX

07/01/2014 DLC10.050 0.0052 U1U 07/01XXXX MG/KGToluene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.050 0.0061 U1U 07/01XXXX MG/KGEthylbenzene EPA-8021 XXX0.050XXXXX XXXXX

07/01/2014 DLC10.20 0.016 U1U 07/01XXXX MG/KGXylenes EPA-8021 XXX0.20XXXXX XXXXX

07/02/2014 EBS125 7.8 U1U 06/26XXXX MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25XXXXX XXXXX

07/02/2014 EBS150 15 U1U 06/26XXXX MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50XXXXX XXXXX

MIN RPDSURROGATE

SPIKE

ADDEDLIMITS

XXXXX XXXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX07/01/2014 DLC1140 0.460 07/01XXXXXXXXX102 TFT NWTPH-GX XXX60XXXXX XXXXXXXXXX

07/01/2014 DLC1140 0.460 07/01XXXXXXXXX102 TFT EPA-8021 XXX60XXXXX XXXXXXXXXX

07/02/2014 EBS1134 3.32 06/26XXXXXXXXX84.6 C25 NWTPH-DX w/ SGA XXX58XXXXX XXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 29

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 65: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 2603142

CLIENT SAMPLE ID Soil-Comp-1

COLLECTION DATE: 6/24/2014 2:00:00 PM

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

EV14060165

ALS SAMPLE#: EV14060165-29

DATE: 7/2/2014

DATA RESULTS

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds DATE RECEIVED: 06/25/2014

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION

FACTORUNITS

LIMITSXXXXX XXXX

REPORTING

LIMITSRESULTSMETHOD

ANALYSIS

DATE

ANALYSIS

BYQUALXXXXX

PR

DAX06/27/2014 RAL10.020 0.0041 U1U 06/27XXXX MG/KGMercury EPA-7471 XXX0.020XXXXX XXXXX

06/26/2014 RAL51.0 0.83 5 06/26XXXX3.7 MG/KGArsenic EPA-6020 XXX1.0XXXXX XXXXX

06/26/2014 RAL50.50 0.16 5 06/26XXXX140 MG/KGBarium EPA-6020 XXX0.50XXXXX XXXXX

06/26/2014 RAL50.50 0.26 U5U 06/26XXXX MG/KGCadmium EPA-6020 XXX0.50XXXXX XXXXX

06/26/2014 RAL50.50 0.42 5 06/26XXXX30 MG/KGChromium EPA-6020 XXX0.50XXXXX XXXXX

06/26/2014 RAL50.50 0.27 5 06/26XXXX5.7 MG/KGLead EPA-6020 XXX0.50XXXXX XXXXX

06/26/2014 RAL55.0 3.6 U5U 06/26XXXX MG/KGSelenium EPA-6020 XXX5.0XXXXX XXXXX

06/26/2014 RAL50.50 0.26 U5U 06/26XXXX MG/KGSilver EPA-6020 XXX0.50XXXXX XXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 30

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 66: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

LABORATORY BLANK RESULTS

CLIENT PROJECT: 2603142

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

ALS SDG#: EV14060165

DATE: 7/2/2014

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds

MB-062714S - Batch 83713 - Soil by NWTPH-GX

METHOD

ANALYSIS DATE

ANALYSIS BYANALYTE

DE

T

OR

G RSLTYPXX

RL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

TPH-Volatile Range 06/28/2014 DLC TRN YXXX3.0 1.5 MG/KG3.0 1 UU XXXXX XXXXX XXXXNWTPH-GX

U - Analyte analyzed for but not detected at level above reporting limit.

MBG-070114S - Batch 83692 - Soil by NWTPH-GX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

TPH-Volatile Range 07/01/2014 DLC TRN YXXX3.0 1.5 MG/KG3.0 1 UU XXXXX XXXXX XXXXNWTPH-GX

U - Analyte analyzed for but not detected at level above reporting limit.

MB-062714S - Batch 83713 - Soil by EPA-8021

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

Benzene 06/28/2014 DLC TRN YXXX0.030 0.018 MG/KG0.030 1 UU XXXXX XXXXX XXXXEPA-8021

Toluene 06/28/2014 DLC TRN YXXX0.050 0.020 MG/KG0.050 1 UU XXXXX XXXXX XXXXEPA-8021

Ethylbenzene 06/28/2014 DLC TRN YXXX0.050 0.016 MG/KG0.050 1 UU XXXXX XXXXX XXXXEPA-8021

Xylenes 06/28/2014 DLC TRN YXXX0.20 0.053 MG/KG0.20 1 UU XXXXX XXXXX XXXXEPA-8021

U - Analyte analyzed for but not detected at level above reporting limit.

MB-070114S - Batch 83692 - Soil by EPA-8021

METHOD

ANALYSIS DATE

ANALYSIS BYANALYTE

DE

T

OR

G RSLTYPXX

RL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

Benzene 07/01/2014 DLC TRN YXXX0.030 0.018 MG/KG0.030 1 UU XXXXX XXXXX XXXXEPA-8021

Toluene 07/01/2014 DLC TRN YXXX0.050 0.020 MG/KG0.050 1 UU XXXXX XXXXX XXXXEPA-8021

Ethylbenzene 07/01/2014 DLC TRN YXXX0.050 0.016 MG/KG0.050 1 UU XXXXX XXXXX XXXXEPA-8021

Xylenes 07/01/2014 DLC TRN YXXX0.20 0.053 MG/KG0.20 1 UU XXXXX XXXXX XXXXEPA-8021

U - Analyte analyzed for but not detected at level above reporting limit.

MB-062614S2 - Batch 83605 - Soil by NWTPH-DX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

TPH-Diesel Range 06/26/2014 DLC TRN YXXX25 12 MG/KG25 1 UU XXXXX XXXXX XXXXNWTPH-DX

TPH-Oil Range 06/26/2014 DLC TRN YXXX50 23 MG/KG50 1 UU XXXXX XXXXX XXXXNWTPH-DX

U - Analyte analyzed for but not detected at level above reporting limit.

MB-063014S - Batch 83687 - Soil by NWTPH-DX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

TPH-Diesel Range 06/30/2014 EBS TRN YXXX25 12 MG/KG25 1 UU XXXXX XXXXX XXXXNWTPH-DX

Page 31

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 67: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

LABORATORY BLANK RESULTS

CLIENT PROJECT: 2603142

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

ALS SDG#: EV14060165

DATE: 7/2/2014

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds

MB-063014S - Batch 83687 - Soil by NWTPH-DXTPH-Oil Range 06/30/2014 EBS TRN YXXX50 23 MG/KG50 1 UU XXXXX XXXXX XXXXNWTPH-DX

U - Analyte analyzed for but not detected at level above reporting limit.

MBLK-6272014 - Batch R236475 - Soil by EPA-7471

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

Mercury 06/27/2014 RAL TRN NXXX0.020 0.0041 MG/KG0.020 1 UU XXXXX XXXXX XXXXEPA-7471

U - Analyte analyzed for but not detected at level above reporting limit.

MB-062614S - Batch 83497 - Soil by EPA-6020

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG RSL

TYPXXRL PQL QUAL

DILUTION

FACTOR UNITS

LIMITSXXXXX XXXXX XXXXLIMITS

REPORTING

RESULTS

Arsenic 06/26/2014 RAL TRN NXXX0.20 0.15 MG/KG0.20 1 UU XXXXX XXXXX XXXXEPA-6020

Barium 06/26/2014 RAL TRN NXXX0.10 0.028 MG/KG0.10 1 UU XXXXX XXXXX XXXXEPA-6020

Cadmium 06/26/2014 RAL TRN NXXX0.10 0.045 MG/KG0.10 1 UU XXXXX XXXXX XXXXEPA-6020

Chromium 06/26/2014 RAL TRY NXXX0.10 0.074 MG/KG0.10 1XXXXX XXXXX XXXX1.6 EPA-6020

Lead 06/26/2014 RAL TRN NXXX0.10 0.047 MG/KG0.10 1 UU XXXXX XXXXX XXXXEPA-6020

Selenium 06/26/2014 RAL TRN NXXX1.0 0.64 MG/KG1.0 1 UU XXXXX XXXXX XXXXEPA-6020

Silver 06/26/2014 RAL TRN NXXX0.10 0.046 MG/KG0.10 1 UU XXXXX XXXXX XXXXEPA-6020

U - Analyte analyzed for but not detected at level above reporting limit.

Page 32

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 68: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

LABORATORY CONTROL SAMPLE RESULTS

CLIENT PROJECT: 2603142

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

ALS SDG#: EV14060165

DATE: 7/2/2014

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds

XXXLABORATORY CONTROL SAMPLE RESULTS

83692 - Soil by NWTPH-GXALS Test Batch ID:

METHOD

ANALYSIS DATERPD

ANALYSIS BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DE

T

OR

GRSLT TYPE

RPRT RS

XXREPORTINTPH-Volatile Range - BS 0.493.0 07/01/2014 DLC1 66.5 122.725.0 SC YesY Y98.9 XXXREPORTING REPORTINGNWTPH-GX

TPH-Volatile Range - BSD 0.49 1.53.0 07/01/2014 DLC1 66.5 122.725.0 SC YesY Y2101 9.14 XXXREPORTING REPORTINGNWTPH-GX

83713 - Soil by NWTPH-GXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE ADDED%REC

LIMITS DET

ORGRSLT TYPE

RPRT RS

XXREPORTINTPH-Volatile Range - BS 0.493.0 06/28/2014 DLC1 66.5 122.725.0 SC YesY Y91.8 XXXREPORTING REPORTINGNWTPH-GX

TPH-Volatile Range - BSD 0.49 1.53.0 06/28/2014 DLC1 66.5 122.725.0 SC YesY Y293.5 9.14 XXXREPORTING REPORTINGNWTPH-GX

83692 - Soil by EPA-8021ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DET

ORGRSLT TYPE

RPRT RS

XXREPORTINBenzene - BS 0.00610.030 07/01/2014 DLC1 67.7 1241.00 SC YesY Y92.2 XXXREPORTING REPORTINGEPA-8021

Benzene - BSD 0.0061 0.0180.030 07/01/2014 DLC1 67.7 1241.00 SC YesY Y294.3 8.5 XXXREPORTING REPORTINGEPA-8021

Toluene - BS 0.00670.050 07/01/2014 DLC1 71 1231.00 SC YesY Y96.0 XXXREPORTING REPORTINGEPA-8021

Toluene - BSD 0.0067 0.0200.050 07/01/2014 DLC1 71 1231.00 SC YesY Y297.6 9.7 XXXREPORTING REPORTINGEPA-8021

Ethylbenzene - BS 0.00530.050 07/01/2014 DLC1 69.8 1171.00 SC YesY Y93.4 XXXREPORTING REPORTINGEPA-8021

Ethylbenzene - BSD 0.0053 0.0160.050 07/01/2014 DLC1 69.8 1171.00 SC YesY Y295.0 10 XXXREPORTING REPORTINGEPA-8021

Xylenes - BS 0.0180.20 07/01/2014 DLC1 70 1193.00 SC YesY Y94.5 XXXREPORTING REPORTINGEPA-8021

Xylenes - BSD 0.018 0.0530.20 07/01/2014 DLC1 70 1193.00 SC YesY Y296.1 10 XXXREPORTING REPORTINGEPA-8021

83713 - Soil by EPA-8021ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DET

ORGRSLT TYPE

RPRT RS

XXREPORTINBenzene - BS 0.00610.030 06/28/2014 DLC1 67.7 1241.00 SC YesY Y88.9 XXXREPORTING REPORTINGEPA-8021

Benzene - BSD 0.0061 0.0180.030 06/28/2014 DLC1 67.7 1241.00 SC YesY Y290.6 8.5 XXXREPORTING REPORTINGEPA-8021

Toluene - BS 0.00670.050 06/28/2014 DLC1 71 1231.00 SC YesY Y94.8 XXXREPORTING REPORTINGEPA-8021

Toluene - BSD 0.0067 0.0200.050 06/28/2014 DLC1 71 1231.00 SC YesY Y296.8 9.7 XXXREPORTING REPORTINGEPA-8021

Ethylbenzene - BS 0.00530.050 06/28/2014 DLC1 69.8 1171.00 SC YesY Y94.5 XXXREPORTING REPORTINGEPA-8021

Ethylbenzene - BSD 0.0053 0.0160.050 06/28/2014 DLC1 69.8 1171.00 SC YesY Y296.7 10 XXXREPORTING REPORTINGEPA-8021

Xylenes - BS 0.0180.20 06/28/2014 DLC1 70 1193.00 SC YesY Y94.5 XXXREPORTING REPORTINGEPA-8021

Xylenes - BSD 0.018 0.0530.20 06/28/2014 DLC1 70 1193.00 SC YesY Y296.7 10 XXXREPORTING REPORTINGEPA-8021

83605 - Soil by NWTPH-DXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DET

ORGRSLT

TYPE

RP

RT RS

XXREPORTINTPH-Diesel Range - BS 3.925 06/26/2014 DLC1 76.2 112125 SC YesY Y94.7 XXXREPORTING REPORTINGNWTPH-DX

TPH-Diesel Range - BSD 3.9 1225 06/26/2014 DLC1 76.2 112125 SC YesY Y498.5 12 XXXREPORTING REPORTINGNWTPH-DX

Page 33

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 69: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

CERTIFICATE OF ANALYSIS

LABORATORY CONTROL SAMPLE RESULTS

CLIENT PROJECT: 2603142

CLIENT: Antea Group4006 - 148th Ave NERedmond, WA 98052

ALS SDG#: EV14060165

DATE: 7/2/2014

WDOE ACCREDITATION: C601

CLIENT CONTACT: Joe Rounds

XXXLABORATORY CONTROL SAMPLE RESULTS

83687 - Soil by NWTPH-DXALS Test Batch ID:

METHOD

ANALYSIS DATERPD

ANALYSIS BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DE

T

OR

GRSLT TYPE

RPRT RS

XXREPORTINTPH-Diesel Range - BS 3.925 07/01/2014 EBS1 76.2 112125 SC YesY Y109 XXXREPORTING REPORTINGNWTPH-DX

TPH-Diesel Range - BSD 3.9 1225 07/01/2014 EBS1 76.2 112125 SC YesY Y3112 12 XXXREPORTING REPORTINGNWTPH-DX

R236475 - Soil by EPA-7471ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITS DET

ORGRSLT TYPE

RPRT RS

XXREPORTINMercury - BS 0.00140.020 06/27/2014 RAL1 81.8 1170.250 SC YesY N94.0 XXXREPORTING REPORTINGEPA-7471

Mercury - BSD 0.0014 0.00410.020 06/27/2014 RAL1 81.8 1170.250 SC YesY N598.8 8.84 XXXREPORTING REPORTINGEPA-7471

83497 - Soil by EPA-6020ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS

BYMIN MAX RPDSPIKED COMPOUND QUAL

SPIKE ADDED%REC

LIMITS DET

ORGRSLT TYPE

RPRT RS

XXREPORTINArsenic - BS 0.0490.20 06/26/2014 RAL1 80 1205.00 SC YesY N98.9 XXXREPORTING REPORTINGEPA-6020

Arsenic - BSD 0.049 0.150.20 06/26/2014 RAL1 80 1205.00 SC YesY N199.5 8.91 XXXREPORTING REPORTINGEPA-6020

Barium - BS 0.00900.10 06/26/2014 RAL1 80 1205.00 SC YesY N104 XXXREPORTING REPORTINGEPA-6020

Barium - BSD 0.0090 0.0280.10 06/26/2014 RAL1 80 1205.00 SC YesY N1103 10 XXXREPORTING REPORTINGEPA-6020

Cadmium - BS 0.0150.10 06/26/2014 RAL1 80 1205.00 SC YesY N102 XXXREPORTING REPORTINGEPA-6020

Cadmium - BSD 0.015 0.0450.10 06/26/2014 RAL1 80 1205.00 SC YesY N1103 9.2 XXXREPORTING REPORTINGEPA-6020

Chromium - BS 0.0250.10 06/26/2014 RAL1 80 1205.00 SC YesY N140 XXXREPORTING REPORTINGEPA-6020

Chromium - BSD 0.025 0.0740.10 06/26/2014 RAL1 80 1205.00 SC YesY N2137 9.6 XXXREPORTING REPORTINGEPA-6020

Lead - BS 0.0160.10 06/26/2014 RAL1 80 1205.00 SC YesY N103 XXXREPORTING REPORTINGEPA-6020

Lead - BSD 0.016 0.0470.10 06/26/2014 RAL1 80 1205.00 SC YesY N1104 9.36 XXXREPORTING REPORTINGEPA-6020

Selenium - BS 0.211.0 06/26/2014 RAL1 80 1205.00 SC YesY N99.2 XXXREPORTING REPORTINGEPA-6020

Selenium - BSD 0.21 0.641.0 06/26/2014 RAL1 80 1205.00 SC YesY N099.5 10.7 XXXREPORTING REPORTINGEPA-6020

Silver - BS 0.0150.10 06/26/2014 RAL1 80 1205.00 SC YesY N109 XXXREPORTING REPORTINGEPA-6020

Silver - BSD 0.015 0.0460.10 06/26/2014 RAL1 80 1205.00 SC YesY N1108 8.71 XXXREPORTING REPORTINGEPA-6020

APPROVED BY:

Laboratory Director

APPROVED BY

Page 34

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626

ALS Laboratory Group A Campbell Brothers Limited Company

Page 70: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 71: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 72: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 73: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …

Air Sparge System Upgrade and Monitoring Well Installation Report Former Platinum Energy Station No. 2603142 2841 South 188th Street, SeaTac, WA 98188 Antea Group Project No. I42603142

www.anteagroup.com

Antea USA, Inc.

Appendix C

Waste Manifests

Page 74: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …
Page 75: AIR SPARGE SYSTEM UPGRADE AND MONITORING WELL …