additional materials available on the hei … appendix i... · additional materials available on...
TRANSCRIPT
ADDITIONAL MATERIALS AVAILABLE ON THE HEI WEB SITE
Research Report 184
Advanced Collaborative Emissions Study (ACES): Lifetime Cancer and Non-Cancer Assessment in Rats Exposed to New-Technology Diesel
Exhaust
Part 1. Assessment of Carcinogenicity and Biologic Responses in Rats after Lifetime Inhalation of New-Technology Diesel Exhaust in the ACES Bioassay
Appendix I.
Characterization of Exposure Atmospheres in the ACES Bioassay
McDonald et al.
Additional Materials I.D. Fuel and Oil Analyses
Additional Materials may appear in a different order from that in the original Investigators’ Report, and
some remnants of their original names may be apparent.
Additional Materials I.D was originally Appendices B and C.
The HEI Exposure Characterization Panel reviewed the draft of this appendix but not the final version. This appendix did not undergo the HEI scientific editing and production process but was proofread for spelling and
grammar only.
Correspondence may be addressed to Dr. Jacob D. McDonald, Lovelace Respiratory Research Institute, 2425
Ridgecrest Dr., SE, Albuquerque, NM 87108; e-mail: [email protected].
Although this document was produced with partial funding by the United States Department of Energy (DOE), under the terms of Contract/Award Number DE-AC26-05NT42429, and certain motor vehicle and engine
manufacturers, the opinion expressed herein are those of the authors and do not necessarily reflect the views of the DOE or motor vehicle and engine manufacturers.
© 2015 Health Effects Institute, 101 Federal Street, Suite 500, Boston, MA 02110-1817
Michael Clearwater
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/11/10
LOVEMC
V7000244A
Description :Sample ID: 19FEB10-F409-111, Diesel Fuel
JLMAMSP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 02/19/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7000244
Oil Type : Diesel Fuel (GN_130)Serial#: 1802741 09744
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 757 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 369 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 388 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 483 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 571 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 648 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 660 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.0 % vol.Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % WtCetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25.2 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.8 % vol
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
69
Michael Clearwater
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/11/10
LOVEMC
V7000244A
Description :Sample ID: 19FEB10-F409-111, Diesel Fuel
JLMAMSP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 02/19/10
Lovelace Respiratory Research Institute
Herguth ID :
Oil Type : Diesel Fuel (GN_130)Serial#: 1802741 09744
Unit Type : Diesel Fuel (GN_DF001)
Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 mg/kg
Michael Clearwater
REVISED REPORT supersedes lab # V7000244 and includes sulfur by D3120 result.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
70
Michael Clearwater
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/11/10
LOVEMC
V7000244A
Description :Sample ID: 19FEB10-F409-111, Diesel Fuel
JLMAMSP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 02/19/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7000244
Oil Type : Diesel Fuel (GN_130)Serial#: 1802741 09744
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 757 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 369 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 388 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 483 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 571 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 648 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 660 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.0 % vol.Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % WtCetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25.2 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.8 % vol
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
71
Michael Clearwater
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/11/10
LOVEMC
V7000244A
Description :Sample ID: 19FEB10-F409-111, Diesel Fuel
JLMAMSP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 02/19/10
Lovelace Respiratory Research Institute
Herguth ID :
Oil Type : Diesel Fuel (GN_130)Serial#: 1802741 09744
Unit Type : Diesel Fuel (GN_DF001)
Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 mg/kg
Michael Clearwater
REVISED REPORT supersedes lab # V7000244 and includes sulfur by D3120 result.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
72
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/26/10
LOVEMC
V7000633
Description :Serial# F409-111-14APR10, Clear Diesel
JLMDEMP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 04/14/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7000633
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 754 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 343 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 381 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 413 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 504 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 639 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 680 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 689 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.0 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.1 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.8 % volSulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % Wt
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
73
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/26/10
LOVEMC
V7000633
Description :Serial# F409-111-14APR10, Clear Diesel
JLMDEMP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 04/14/10
Lovelace Respiratory Research Institute
Herguth ID :
Tom Holmes
Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
74
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/30/10
LOVEMC
V7000633A
Description :Serial# F409-111-14APR10, Clear Diesel
JLMDEMP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 04/14/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7000633
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 754 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 343 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 381 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 413 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 504 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 639 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 680 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 689 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.0 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.1 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.8 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 ppm
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
75
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/30/10
LOVEMC
V7000633A
Description :Serial# F409-111-14APR10, Clear Diesel
JLMDEMP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 04/14/10
Lovelace Respiratory Research Institute
Herguth ID :
Tom Holmes
REVISED REPORT supersedes lab # V7000633 and includes updated sulfur test.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
76
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
06/22/10
LOVEMC
V7001241
Description :Sample ID: FY09-111-08JUN10-Fuel, Chevron #2 Clear Diesel
JK101621P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 06/08/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7001241
Oil Type : Diesel Fuel (GN_130)Label States: Total Engine Hours: 2586
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 760 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 380 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 396 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 411 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 424 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 448 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 473 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 496 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 522 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 550 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 583 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 604 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 629 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 668 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 676 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.2 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.6 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26.5 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.4 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 3 ppm
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
77
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
06/22/10
LOVEMC
V7001241
Description :Sample ID: FY09-111-08JUN10-Fuel, Chevron #2 Clear Diesel
JK101621P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 06/08/10
Lovelace Respiratory Research Institute
Herguth ID :
Label States: Total Engine Hours: 2586
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
78
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
08/16/10
LOVEMC
V7001845
Description :Sample ID: FY09-111-30JUL10-Fuel, Chevron #2 Clear Diesel
JK101657P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 07/29/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7001845
Oil Type : Diesel Fuel (GN_130)Project# FY09-111 ACES, Acct/Org/Project: JLMEPR
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 761 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 380 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 420 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 460 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 486 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 510 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 534 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 560 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 609 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 632 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 671 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 676 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.8 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 36.5 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.6 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.2 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.2 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 ppm
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
79
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
08/16/10
LOVEMC
V7001845
Description :Sample ID: FY09-111-30JUL10-Fuel, Chevron #2 Clear Diesel
JK101657P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 07/29/10
Lovelace Respiratory Research Institute
Herguth ID :
Project# FY09-111 ACES, Acct/Org/Project: JLMEPR
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
80
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
10/14/10
LOVEMC
V7002326
Description :Sample ID: FY09-111-01OCT10, Chevron #2 Clear Diesel Fuel
FY09-111 ACESP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 10/01/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7002326
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 762 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 379 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 411 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 468 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 492 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 518 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 550 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 588 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 611 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 641 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . DNR Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 686 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95.8 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 48.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.3 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33.6 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65.3 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 ppm
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
81
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
10/14/10
LOVEMC
V7002326
Description :Sample ID: FY09-111-01OCT10, Chevron #2 Clear Diesel Fuel
FY09-111 ACESP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 10/01/10
Lovelace Respiratory Research Institute
Herguth ID :
Tom Holmes
Result does not meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Distillation at 90% exceeds maximum (640°F). Testing could not be completed due to sample condition.Value(s) have been rechecked and verified.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
82
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/09/10
LOVEMC
V7003059
Description :Sample: FY09-111-24nov10-fuel, Chevon #2 Clear Diesel Fuel
FY09-111 ACESP.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/24/10
Lovelace Respiratory Research Institute
Herguth ID : LABV7003059
Oil Type : Diesel Fuel (GN_130)Label States: Total Engine Hours: 4505
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 765 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 367 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 381 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 395 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 406 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 429 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 454 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 479 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 507 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 537 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 570 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 615 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 654 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 660 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 47.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.7 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27.1 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0.9 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.0 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 4 ppm
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
83
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/09/10
LOVEMC
V7003059
Description :Sample: FY09-111-24nov10-fuel, Chevon #2 Clear Diesel Fuel
FY09-111 ACESP.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/24/10
Lovelace Respiratory Research Institute
Herguth ID :
Label States: Total Engine Hours: 4505
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
84
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
01/28/11
LOVEMC
V7003451
Description :Sample ID: FY09-111-17Jan11-Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/17/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7003451
Oil Type : Diesel Fuel (GN_130)
Total Engine Hours: 5082, Paperwork States: Sample Description: Chevron #2 Clear Diesel Fuel,Project/PO#: FY09-111 ACES
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 764 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 331 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 361 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 375 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 399 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 471 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 500 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 566 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 586 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 646 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 659 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.5 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 46.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.4 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.7 % vol
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
85
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
01/28/11
LOVEMC
V7003451
Description :Sample ID: FY09-111-17Jan11-Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/17/11
Lovelace Respiratory Research Institute
Herguth ID :
Oil Type : Diesel Fuel (GN_130)
Total Engine Hours: 5082, Paperwork States: Sample Description: Chevron #2 Clear Diesel Fuel,Project/PO#: FY09-111 ACES
Unit Type : Diesel Fuel (GN_DF001)
Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % Wt
Tom Holmes
Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
86
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
02/10/11
LOVEMC
V7003451A
Description :Sample ID: FY09-111-17Jan11-Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/17/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7003451
Oil Type : Diesel Fuel (GN_130)
Total Engine Hours: 5082, Paperwork States: Sample Description: Chevron #2 Clear Diesel Fuel,Project/PO#: FY09-111 ACES
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 764 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 331 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 361 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 375 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 399 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 471 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 500 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 566 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 586 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 646 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 659 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.5 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 46.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.4 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.7 % vol
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
87
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
02/10/11
LOVEMC
V7003451A
Description :Sample ID: FY09-111-17Jan11-Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/17/11
Lovelace Respiratory Research Institute
Herguth ID :
Oil Type : Diesel Fuel (GN_130)
Total Engine Hours: 5082, Paperwork States: Sample Description: Chevron #2 Clear Diesel Fuel,Project/PO#: FY09-111 ACES
Unit Type : Diesel Fuel (GN_DF001)
Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 ppm
Tom Holmes
REVISED REPORT supersedes lab # V7003451 and includes updated sulfur result.Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
88
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
Tom Holmes Quotation No. 204887 (LOVEMC) Lovelace Respiratory Research Institute Quotation Date: February 1, 2011 2425 Ridgecrest Drive, SE Albuquerque, NM 87108 Email: [email protected] Phone: (505) 348-9600 Fax: (505) 348-4980
QUOTATION
Item Qty Description/Analysis Methodology Fee Extend ________________________________________________________________________________
1 1 Fuels 353.85 353.85 Volume of sample required: 631 ml
Distillation of Petroleum Product (FUELS) ASTM D86 Cetane Index (Calculation Only) (FUELS) ASTM D976 Gravity, API (Hydrometer Method) (FUELS) ASTM D287 *Hydrocarbon Types by Fluorescent (FUELS) ASTM D1319 Sulfur by Microcoul. (FUELS) ASTM D3120 Turnaround time is 7-10 working day(s) from receipt of sample.
QUOTATION TOTAL 353.85 each
*Test are subcontracted to another facility and should be completed between 7-10 working days
Thank you for the opportunity to provide you with the above quotation for your samples. The above quotation is based on your requested scope of work and/or our recommended analytical methods for your sample type. However, prices are subject to change based on the actual sample type as determined upon receipt. Reference oils are required for baseline data.
Our standard turn around time is four (4) working days. Rush charges are double above prices for 48-hour turn around and triple for 24-hour. Any analysis that is subcontracted to another facility (lab) will be processed within 7-10 working days depending on the test. Samples arriving in large batches may have longer turn around times based on testing and oil types. This quotation is valid for 90 days. Please refer to quotation number when submitting samples. All ASTM methods will be performed at the latest published revision.
Reports can be transmitted via email upon completion at no additional charge. We also have Internet access-iLAMP available for an additional $300/ year that will allow you to retrieve your data, view and print reports, set up units and route list, print labels, etc. Please contact Customer Service to order iLAMP.
A credit application or payment is required with all new accounts. Please fax one to 707-554-0109. Credit will be extended based on the reference verification. The sample turn around time may be longer based on credit reference responses.
Laboratory Pricing Policy
1. Hours of Operation And Normal Availability Regular laboratory hours are 8:00 AM to 5:00 PM Monday through Friday. For condition monitoring analyses, our normal turnaround is 48 hours (two working days). For all other analyses, our normal turnaround is 96 hours (four working days). Any analysis that is subcontracted to another facility
ACES: Phase 3B: Characterization of Exposure Atmospheres
89
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
(lab) will be processed within 7-10 working days depending on the test. Please note there may be delays in turn around times based on account setup and credit references.
2. Minimum Invoice Charges, Rush Analyses and Overtime Rates A minimum fee of $25.00 may be charged for any analysis invoice. For Condition Monitoring analyses, "RUSH" samples results are available within 24 hours (or less) and are charged at three times the normal analyses rate. For other analyses there are two "RUSH" provisions for work performed during our regular laboratory hours: a) 48 hour (2 working day) analysis time is charged at twice the normal analysis fee. b) 24 hour (one working day) turnaround, or less, is charged at three times the normal analysis fee. There are some analyses that cannot be completed in less than 24 hours; however, they can be moved ahead of the scheduled samples waiting for that analysis. These analyses will be charged at the 24 hour rush rate. Laboratory work performed during other hours, including Saturday, Sunday or recognized Holidays may be charged at triple our normal analyses rates, an hourly rate with a four (4) hour minimum charge, or $1,500, whichever is greater. Nuclear Quality Assured (10 CFR 50 Appendix B) or radioactive samples analyzed during periods other than normal hours will be charged a minimum of $2,500.
3. Quality Assurance Program And Surveillance Analyses performed under the Safety Related Part 21 Program are charged at 1.35 times the applicable fee. Surveillance of work performed at Herguth Laboratories, Inc. by client representatives may be charged at three times the applicable fee. All ASTM methods are performed at the latest published revision.
4. Radioactive Materials Analyses on radioactive samples will be assessed a surcharge of 1.5 times the analysis fee or a fee of $125 per sample (Condition Monitoring Rads), as specifically quoted to the customer. Radioactive lubricant samples are properly disposed of by Herguth provided the sample meets our disposal criteria. This service is not applicable for non-liquid lubricant samples, which must be returned to the client.
5. Sample Pick-Up And Delivery Sample pick-up and delivery during normal working hours may be charged at a minimum of $25 within a 25 mile radius. The fee will be $50 within a radius of 50 miles. Sample pick-up during non-working hours may be charged a minimum of $100 plus expenses. This applies to the nine (9) San Francisco Bay Area counties. Special arrangements must be made for custody transfers and pick-ups outside of this area.
6. Sample Retention and Disposal Samples will be held for a minimum of 30 days. Long term retention services are available by special request. Non-hydrocarbon samples, "unknown" samples, and samples containing elements or constituents which cannot be accommodated by our normal waste streams will either be returned, or if requested, disposed of properly. Handling and disposal surcharges may be assessed. Samples can be returned to the client if requested.
Terms, Conditions, and Limitations
All services rendered by Herguth Laboratories, Inc. are undertaken, and all rates are based upon the following terms:
(a) Neither Herguth Laboratories, Inc., nor any of its employees, agents or sub-contractors shall be liable for any loss or damage arising out of Herguth Laboratories, Inc.'s. performance or non-performance, whether by way of negligence or breach of contract, or otherwise, in any amount greater than twice the amount billed to the customer for the work leading to the claim of the customer. Said remedy shall be the sole and exclusive remedy against Herguth Laboratories, Inc. arising out of its work.
ACES: Phase 3B: Characterization of Exposure Atmospheres
90
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
(b) All claims must be in writing within forty-five (45) days after delivery of the Herguth Laboratories, Inc. report regarding said work, or such claim shall be deemed as irrevocably waived.
(c) Herguth Laboratories, Inc. reports are submitted in writing and are for our customers only. Our customers are considered to be only those entities being billed for our services. Acquisition of a Herguth Laboratories, Inc. report by other than our customer does not constitute a representation of Herguth Laboratories, Inc. as to the accuracy of the contents thereof.
(d) In no event shall Herguth Laboratories, Inc., its employees, agents or sub-contractors be responsible for consequential or special damages of any kind or in any amount.
(e) No deviation from the terms set forth herein shall bind Herguth Laboratories, Inc. unless explicitly agreed upon and accepted contractually, or unless explicitly expressed in writing and signed by a Corporate Officer of Herguth Laboratories, Inc.
(f) Depending on specific customer requirements and/or changes in operations, Herguth Laboratories, Inc. reserves the right to change the pricing and availability of analyses as published in price list(s).
(g) All ASTM methods are performed at the latest published revision.
Should you have any questions regarding this quote, please contact myself at 800-645-5227 ext. 3012. We look forward to working with you on this and future projects. Please refer to this quotation number when submitting samples.
Please visit our website for additional services and capabilities www.herguth.com.
_______________________________________ Linda Perry Sales & Marketing
ACES: Phase 3B: Characterization of Exposure Atmospheres
91
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/28/11
LOVEMC
V7004199
Description :Sample: FY09-111-15mar11-fuel, Chevron #2 Clear Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 03/15/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7004199
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 755 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 337 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 366 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 382 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 394 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 405 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 505 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 535 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 570 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 615 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 651 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 664 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.1 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 47.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.6 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27.9 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.1 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 5 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
92
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
03/28/11
LOVEMC
V7004199
Description :Sample: FY09-111-15mar11-fuel, Chevron #2 Clear Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 03/15/11
Lovelace Respiratory Research Institute
Herguth ID :
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
93
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
05/20/11
LOVEMC
V7004725
Description :Sample ID: FY09-111-10may-11fuel, Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 05/10/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7004725
Oil Type : Diesel Fuel (GN_130)Chevron #2 Clear Diesel Fuel, Label States: Total Engine Hours: 6351
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 758 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 342 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 377 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 393 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 409 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 424 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 451 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 479 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 504 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 556 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 585 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 603 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 626 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 661 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 671 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.1 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 47.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 35.9 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29.7 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.6 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68.7 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
94
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
05/20/11
LOVEMC
V7004725
Description :Sample ID: FY09-111-10may-11fuel, Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 05/10/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7004725
Chevron #2 Clear Diesel Fuel, Label States: Total Engine Hours: 6351
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
95
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
07/21/11
LOVEMC
V7005385
Description :Sample ID: FY09-111-07Jul11-Fuel, Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 07/07/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7005385
Oil Type : Diesel Fuel (GN_130)Chevron #2 Clear Diesel Fuel
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 760 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 353 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 383 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 401 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 416 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 428 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 454 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 480 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 506 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 532 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 560 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 591 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 635 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 674 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 680 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.0 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 50.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.9 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67.1 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 10 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
96
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
07/21/11
LOVEMC
V7005385
Description :Sample ID: FY09-111-07Jul11-Fuel, Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 07/07/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7005385
Chevron #2 Clear Diesel Fuel
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
97
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
09/21/11
LOVEMC
V7006238
Description :Sample: FY09-111-06SEP11-Fuel, Chevron #2 Clear Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 09/06/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7006238
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 761 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 339 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 369 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 382 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 396 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 406 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 430 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 455 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 482 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 540 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 572 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 591 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 615 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 654 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 656 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.7 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 48.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.9 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26.5 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.2 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 10 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
98
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
09/21/11
LOVEMC
V7006238
Description :Sample: FY09-111-06SEP11-Fuel, Chevron #2 Clear Diesel Fuel
JK110737P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 09/06/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7006238
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed, noting visibledebris was present in sample.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
99
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
11/22/11
LOVEMC
V7006931
Description :FY09-111-07NOV11-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/07/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7006931
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 762 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 358 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 382 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 403 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 447 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 469 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 489 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 508 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 555 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 571 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 592 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 624 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 642 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.2 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 39.3 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20.7 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.8 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76.5 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 7 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
100
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
11/22/11
LOVEMC
V7006931
Description :FY09-111-07NOV11-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/07/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7006931
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
101
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/29/11
LOVEMC
V7007282
Description :FY09-111-13DEC11-FUEL, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 12/13/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7007282
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 762 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 343 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 373 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 387 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 413 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 437 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 460 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 482 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 505 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 529 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 577 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 600 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 632 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 650 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98.0 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.8 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24.7 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.6 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71.7 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 4 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
102
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/29/11
LOVEMC
V7007282
Description :FY09-111-13DEC11-FUEL, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 12/13/11
Lovelace Respiratory Research Institute
Herguth ID : LABV7007282
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
103
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
02/13/12
LOVEMC
V7007704
Description :FY09-111-30JAN2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/31/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7007704
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 764 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 326 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 370 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 385 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 400 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 411 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 435 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 484 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 511 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 540 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 573 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 592 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 647 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 664 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.5 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 47.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32.3 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.8 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63.9 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 4 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
104
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
02/13/12
LOVEMC
V7007704
Description :FY09-111-30JAN2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 01/31/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7007704
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
105
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/12/12
LOVEMC
V7008264
Description :Sample ID: FY09-111-29MAR2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 03/29/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7008264
Oil Type : Diesel Fuel (GN_130)Label States: Total Engine Hours: 3312
Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 765 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 334 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 370 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 399 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 484 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 510 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 568 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 585 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 605 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 632 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 654 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 48.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.8 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27.9 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.0 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 6 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
106
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
04/12/12
LOVEMC
V7008264
Description :Sample ID: FY09-111-29MAR2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 03/29/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7008264
Label States: Total Engine Hours: 3312
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
107
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
06/15/12
LOVEMC
V7008917
Description :Sample ID: FY09-111-29MAY2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 05/29/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7008917
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 758 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 348 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 447 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 467 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 486 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 507 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 528 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 553 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 567 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 585 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 633 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98.3 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 52.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 40.0 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21.2 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4.8 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.0 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 6 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
108
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
06/15/12
LOVEMC
V7008917
Description :Sample ID: FY09-111-29MAY2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 05/29/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7008917
Tom Holmes
Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Mindy L. Villalba, Project Managercc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
109
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
08/23/12
LOVEMC
V7010055
Description :Sample ID: FY09-111-02Aug2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 08/02/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7010055
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 758 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 377 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 390 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 405 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 417 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 440 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 466 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 490 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 518 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 549 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 584 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 606 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 632 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 670 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 685 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.4 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 48.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.1 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67.7 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 7 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
110
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
08/23/12
LOVEMC
V7010055
Description :Sample ID: FY09-111-02Aug2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 08/02/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7010055
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
111
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
10/11/12
LOVEMC
V7010749
Description :Sample ID: FY09-111-25Sep2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 09/25/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7010749
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001) UnitTime : 1262
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 757 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 357 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 394 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 408 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 479 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 499 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 520 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 541 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 568 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 583 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 602 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 629 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 648 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98.1 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 53.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 39.7 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20.8 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76.1 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 5 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
112
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
10/11/12
LOVEMC
V7010749
Description :Sample ID: FY09-111-25Sep2012, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 09/25/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7010749
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
113
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/05/12
LOVEMC
V7011835
Description :FY09-111-14NOV2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/27/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7011835
Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 763 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 335 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 378 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 395 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 408 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 421 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 469 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 491 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 513 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 537 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 564 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 581 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 601 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 631 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 654 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98.4 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.9 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45.9 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44.1 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
115
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/05/12
LOVEMC
V7011835
Description :FY09-111-14NOV2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/27/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7011835
Tom Holmes
Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed. Noting,Aromatic level exceeds the maximum of 35 % vol. and Cetane Index is > 40.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
116
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/19/12
LOVEMC
V7011835A
Description :FY09-111-14NOV2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 1
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/27/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7011835
Oil Type : Diesel Fuel (GN_130)
Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 763 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 335 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 378 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 395 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 408 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 421 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 469 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 491 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 513 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 537 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 564 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 581 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 601 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 631 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 654 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98.4 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.9 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24.5 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.9 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.6 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 mg/kg
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
117
Tom Holmes
2425 Ridgecrest Drive, SEAlbuquerque NM 87108
12/19/12
LOVEMC
V7011835A
Description :FY09-111-14NOV2012-Fuel, Chevron #2 Clear Diesel Fuel
JK120015P.O. Number :
Test Performed Proc-Rev Result
Page 2
Client Code :
Certificate of AnalysisLab Number
Sample Date : 11/27/12
Lovelace Respiratory Research Institute
Herguth ID : LABV7011835
Tom Holmes
REVISED REPORT supersedes lab # V7011835 and includes updated D1319 results.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.
Respectfully Submitted,Herguth Laboratories, Inc.
Bobby R Licu, Senior Evaluatorcc:
101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com
These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.
erlabcs.frx Rev. 04/20/11ISO 9001:2008 and ISO/IEC 17025:2005 Certified
ACES: Phase 3B: Characterization of Exposure Atmospheres
118
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
Tom Holmes Quotation No. 204505 (LOVEMC) Lovelace Respiratory Research Institute Quotation Date: July 29, 2010 2425 Ridgecrest Drive, SE Albuquerque, NM 87108 Email: [email protected] Phone: (505) 348-9600 Fax: (505) 348-4980 QUOTATION Item Qty Description/Analysis Methodology Fee Extend ________________________________________________________________________________ 1 1 Diesel Engine Oils 21.63 21.63 Volume of sample required: 100 ml Viscosity Measurements (SBD1) ASTM D445 Neutralization Number (SBD1) HL-1118 FTIR Nicolet (SBD1) HL-1140 Metals by ICP AES (SBD1) HL-1158 Turnaround time is 2 working day(s) from receipt of sample. QUOTATION TOTAL 21.63 ea Thank you for the opportunity to provide you with the above quotation for your samples. The above quotation is based on your requested scope of work and/or our recommended analytical methods for your sample type and package pricing. Tests selected on a one-on-one basis and not tested as a package may be subject to price adjustments. Prices are also subject to change based on the actual sample type as determined upon receipt. Reference oils are required for baseline information. Our standard turn around time is two (2) working days. Rush analysis is triple for a 24 hour turn around time. Any analysis that is subcontracted to another facility (lab) will be processed within 7-10 working days depending on the test. Samples received in larger batches may have a longer turn around time depending on sample type and tests requested. This quotation is valid for 90 days. Please refer to this quotation number when submitting samples. Sampling kits will be included in this program. Kits include a bottle, label, ID Form, and mailer. Sampling pumps and tubing will be charged at list price. Postage paid labels are also available for an additional fee. Please visit our website to view a current list of supplies Reports can be transmitted via email upon completion at no additional charge. We also have Internet access-iLAMP available for an additional $300/ year that will allow you to retrieve your data, view and print reports, set up units and route list, print labels, etc. Please contact Customer Service to order iLAMP. A credit application or payment is required with all new accounts. Please fax one to 707-554-0109. Credit will be extended based on the reference verification. The sample turn around time may be longer based on credit reference responses. Laboratory Pricing Policy 1. Hours of Operation And Normal Availability Regular laboratory hours are 8:00 AM to 5:00 PM Monday through Friday. For condition monitoring analyses, our normal turnaround is 48 hours (two working days). For all other analyses, our normal turnaround is 96 hours (four working days). Any analysis that is subcontracted to another facility
ACES: Phase 3B: Characterization of Exposure Atmospheres
120
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
(lab) will be processed within 7-10 working days depending on the test. Please note there may be delays in turn around times based on account setup and credit references. 2. Minimum Invoice Charges, Rush Analyses and Overtime Rates A minimum fee of $25.00 may be charged for any analysis invoice. For Condition Monitoring analyses, "RUSH" samples results are available within 24 hours (or less) and are charged at three times the normal analyses rate. For other analyses there are two "RUSH" provisions for work performed during our regular laboratory hours: a) 48 hour (2 working day) analysis time is charged at twice the normal analysis fee. b) 24 hour (one working day) turnaround, or less, is charged at three times the normal analysis fee. There are some analyses that cannot be completed in less than 24 hours; however, they can be moved ahead of the scheduled samples waiting for that analysis. These analyses will be charged at the 24 hour rush rate. Laboratory work performed during other hours, including Saturday, Sunday or recognized Holidays may be charged at triple our normal analyses rates, an hourly rate with a four (4) hour minimum charge, or $1,500, whichever is greater. Nuclear Quality Assured (10 CFR 50 Appendix B) or radioactive samples analyzed during periods other than normal hours will be charged a minimum of $2,500. 3. Quality Assurance Program And Surveillance Analyses performed under the Safety Related Part 21 Program are charged at 1.35 times the applicable fee. Surveillance of work performed at Herguth Laboratories, Inc. by client representatives may be charged at three times the applicable fee. All ASTM methods are performed at the latest published revision. 4. Radioactive Materials Analyses on radioactive samples will be assessed a surcharge of 1.5 times the analysis fee or a fee of $125 per sample (Condition Monitoring Rads), as specifically quoted to the customer. Radioactive lubricant samples are properly disposed of by Herguth provided the sample meets our disposal criteria. This service is not applicable for non-liquid lubricant samples, which must be returned to the client. 5. Sample Pick-Up And Delivery Sample pick-up and delivery during normal working hours may be charged at a minimum of $25 within a 25 mile radius. The fee will be $50 within a radius of 50 miles. Sample pick-up during non-working hours may be charged a minimum of $100 plus expenses. This applies to the nine (9) San Francisco Bay Area counties. Special arrangements must be made for custody transfers and pick-ups outside of this area. 6. Sample Retention and Disposal Samples will be held for a minimum of 30 days. Long term retention services are available by special request. Non-hydrocarbon samples, "unknown" samples, and samples containing elements or constituents which cannot be accommodated by our normal waste streams will either be returned, or if requested, disposed of properly. Handling and disposal surcharges may be assessed. Samples can be returned to the client if requested. Terms, Conditions, and Limitations All services rendered by Herguth Laboratories, Inc. are undertaken, and all rates are based upon the following terms: (a) Neither Herguth Laboratories, Inc., nor any of its employees, agents or sub-contractors shall be liable for any loss or damage arising out of Herguth Laboratories, Inc.'s. performance or non-performance, whether by way of negligence or breach of contract, or otherwise, in any amount greater than twice the amount billed to the customer for the work leading to the claim of the customer. Said remedy shall be the sole and exclusive remedy against Herguth Laboratories, Inc. arising out of its work.
ACES: Phase 3B: Characterization of Exposure Atmospheres
121
101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109
www.herguth.com
(b) All claims must be in writing within forty-five (45) days after delivery of the Herguth Laboratories, Inc. report regarding said work, or such claim shall be deemed as irrevocably waived. (c) Herguth Laboratories, Inc. reports are submitted in writing and are for our customers only. Our customers are considered to be only those entities being billed for our services. Acquisition of a Herguth Laboratories, Inc. report by other than our customer does not constitute a representation of Herguth Laboratories, Inc. as to the accuracy of the contents thereof. (d) In no event shall Herguth Laboratories, Inc., its employees, agents or sub-contractors be responsible for consequential or special damages of any kind or in any amount. (e) No deviation from the terms set forth herein shall bind Herguth Laboratories, Inc. unless explicitly agreed upon and accepted contractually, or unless explicitly expressed in writing and signed by a Corporate Officer of Herguth Laboratories, Inc. (f) Depending on specific customer requirements and/or changes in operations, Herguth Laboratories, Inc. reserves the right to change the pricing and availability of analyses as published in price list(s). (g) All ASTM methods are performed at the latest published revision. Should you have any questions regarding this quote, please contact myself at 800-645-5227 ext. 3012. We look forward to working with you on this and future projects. Please refer to this quotation number when submitting samples. Please visit our website for additional services and capabilities www.herguth.com.
________________________________________ Linda Perry Sales & Marketing
ACES: Phase 3B: Characterization of Exposure Atmospheres
122
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K101
657
Lab
Num
ber :
V10
5661
9
08/1
2/10
Page
1
14:0
9:28
NO
RM
AL:
Sam
ple
data
is s
atis
fact
ory.
No
actio
n is
requ
ired
at th
is ti
me.
Plea
se p
rovi
de e
quip
men
t mak
e an
d m
odel
. Add
ition
al s
ampl
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nee
ded
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esta
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nd.
Res
ampl
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hal
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mal
inte
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nd a
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fere
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sam
ple
for a
naly
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Mar
k th
esa
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nd in
dica
te th
e FU
LL N
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and
GR
ADE
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bric
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Tom
Hol
mes
Love
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Res
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stitu
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25 R
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Dat
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inim
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natio
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datio
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0 D
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Und
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War
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Typ
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Typ
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War
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Ove
r Max
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t Tim
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Tim
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Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
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wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
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tion
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Fuel
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l % V
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mAl
umin
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ium
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Cop
per p
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ad p
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n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
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alci
um p
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agne
sium
ppm
Bariu
m p
pmM
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denu
m p
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ium
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12.0
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sed
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Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
123
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : K
U09
-111
Lab
Num
ber :
V10
6106
6
08/2
8/10
Page
1
09:3
0:02
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
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hig
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leas
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ake
and
mod
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ll na
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grad
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lubr
ican
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serv
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in o
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r(s).
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r pro
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npr
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brok
en ri
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ve id
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oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
08/1
9/10
08/2
4/10
08/2
5/10
08/2
8/10
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
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ngin
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* =
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** =
exc
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Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
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ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0610
6608
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10
Com
para
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Gra
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lysi
s
Silic
on
Lead
Cop
per
Chr
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m
Alum
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datio
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Vis
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Pho
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348
-960
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resu
lts a
re s
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itted
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suan
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erm
s, C
ondi
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and
Lim
itatio
ns a
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abor
ator
y P
ricin
g P
olic
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o re
spon
sibi
lity
or li
abili
ty is
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umed
for t
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anne
r in
whi
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ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
124
Oil
Type
: Ap
pear
s to
be
SAE
40
P.O
. : S
G10
0350
Lab
Num
ber :
V10
6628
2
09/2
0/10
Page
1
18:2
4:43
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
09/0
9/10
09/1
2/10
09/1
3/10
09/2
0/10
Ship
ped
:R
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ved:
Prin
ted:
Sam
pled
:
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t Typ
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ID: F
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exc
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Ala
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mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
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guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
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ertif
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Lab
Num
ber
Sam
ple
Dat
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inim
umM
axim
umV1
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10
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para
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m
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datio
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er F
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umin
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ium
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timon
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um p
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Lov
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rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
125
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : F
Y09-
111
ACES
Lab
Num
ber :
V10
7249
1
12/0
7/10
Page
1
08:5
1:20
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.S
oot c
onte
nt is
hig
h. O
ther
test
resu
lts a
re a
ccep
tabl
e. D
rain
oil
and
chan
ge fi
lter(s
). A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
se p
rovi
deeq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
09/3
0/10
10/0
6/10
10/0
7/10
10/1
1/10
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
30SE
P10-
OIL
- FY
09-1
11-3
0SEP
10-O
IL, D
iese
l Eng
ine *
= ex
ceed
s C
autio
n lim
it
**
= e
xcee
ds A
larm
lim
it
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0724
9109
/30/
10
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Oil
Tim
e (H
R)
Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
ot %
wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
lfina
tion
Abs/
Fuel
% V
olG
lyco
l % V
olM
etal
sIro
n pp
mAl
umin
um p
pmC
hrom
ium
ppm
Cop
per p
pmLe
ad p
pmTi
n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
pmC
alci
um p
pmM
agne
sium
ppm
Bariu
m p
pmM
olyb
denu
m p
pmPo
tass
ium
ppm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 76 7 4 32 8 4 44.
5 20
5063 0
15.5
35.
62__
____
____
**3.
3 15<0
.10 25
<2.0
<0.1
0__
____
____ 46 3 1 1 1 1 <1
<0.1 <1 5 3 3
1325
1060
2567 8 <1 3 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: N
uno
H. M
orei
ra, E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
126
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : F
Y09-
111
ACES
Lab
Num
ber :
V10
7757
7
11/0
1/10
Page
1
16:1
0:19
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
10/2
5/10
10/2
5/10
10/2
8/10
11/0
1/10
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
25O
CT1
0-O
IL -
FY09
-111
-25O
CT1
0-O
IL, D
iese
l Eng
ine * =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0775
7710
/25/
10
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Oil
Tim
e (H
R)
Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
ot %
wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
lfina
tion
Abs/
Fuel
% V
olG
lyco
l % V
olM
etal
sIro
n pp
mAl
umin
um p
pmC
hrom
ium
ppm
Cop
per p
pmLe
ad p
pmTi
n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
pmC
alci
um p
pmM
agne
sium
ppm
Bariu
m p
pmM
olyb
denu
m p
pmPo
tass
ium
ppm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 74 4 4 7 4 4 44.
5 20
4136 0
15.5
14.
56__
____
____
**3.
5 14<0
.10 21
<2.0
<0.1
0__
____
____ 33 2 1 1 1 <1 <1
<0.1 <1 2 <2 1
919
815
1826 5 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
127
Oil
Type
: SA
E 15
W-4
0 (G
N_0
45)
P.
O. :
FY0
9-11
1 AC
ES
Lab
Num
ber :
V10
8488
7
12/0
6/10
Page
1
18:2
2:03
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
11/1
5/10
12/0
1/10
12/0
2/10
12/0
6/10
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
15N
OV1
0-E
- FY0
9-11
1-15
NO
V10,
Die
sel E
ngin
e
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0848
8711
/15/
10
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Oil
Tim
e (H
R)
Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
ot %
wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
lfina
tion
Abs/
Fuel
% V
olG
lyco
l % V
olM
etal
sIro
n pp
mAl
umin
um p
pmC
hrom
ium
ppm
Cop
per p
pmLe
ad p
pmTi
n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
pmC
alci
um p
pmM
agne
sium
ppm
Bariu
m p
pmM
olyb
denu
m p
pmPo
tass
ium
ppm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 93 7 4 26 15 4 43.
1 20
0 015
.07
4.83
____
____
__**
3.2 14
<0.1
0 22<2
.0<0
.10
____
____
__ 35 2 1 1 1 1 <1<0
.1 <1 3 <2 394
096
220
92 8 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 06/
21/2
010
ACES: Phase 3B: Characterization of Exposure Atmospheres
128
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : F
Y09-
111
ACES
Lab
Num
ber :
V10
8658
0
12/1
6/10
Page
1
17:3
3:16
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties.
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
12/0
6/10
12/1
3/10
12/1
4/10
12/1
6/10
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
10D
EC10
-OIL
- FY
09-1
11--1
0DEC
10-D
iese
l Eng
ine
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0865
8012
/06/
10
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Oil
Tim
e (H
R)
Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
ot %
wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
lfina
tion
Abs/
Fuel
% V
olG
lyco
l % V
olM
etal
sIro
n pp
mAl
umin
um p
pmC
hrom
ium
ppm
Cop
per p
pmLe
ad p
pmTi
n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
pmC
alci
um p
pmM
agne
sium
ppm
Bariu
m p
pmM
olyb
denu
m p
pmPo
tass
ium
ppm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 66 4 4 7 4 4 44.
5 20
4627 0
15.0
95.
32__
____
____
**3.
2 11<0
.10 16
<2.0
<0.1
0__
____
____ 34 1 1 1 1 <1 <1
<0.1 <1 2 <2 <1 920
865
2016 10 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
129
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V10
8977
1
01/1
0/11
Page
1
15:5
2:38
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
01/0
3/11
01/0
5/11
01/0
6/11
01/1
0/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
03JA
N11
-OIL
- FY
09-1
11-0
3JA
N11
-OIL
, Die
sel E
ngin
e * =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0897
7101
/03/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Oil
Tim
e (H
R)
Vis
@ 1
00 D
eg C
TBN
mg
KO
H/g
FTIR So
ot %
wt.
Oxi
datio
n Ab
s/cm
Wat
er F
TIR
% V
olSu
lfina
tion
Abs/
Fuel
% V
olG
lyco
l % V
olM
etal
sIro
n pp
mAl
umin
um p
pmC
hrom
ium
ppm
Cop
per p
pmLe
ad p
pmTi
n pp
mN
icke
l ppm
Silv
er p
pmAn
timon
y pp
mSi
licon
ppm
Sodi
um p
pmBo
ron
ppm
Zinc
ppm
Phos
phor
us p
pmC
alci
um p
pmM
agne
sium
ppm
Bariu
m p
pmM
olyb
denu
m p
pmPo
tass
ium
ppm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 65 4 4 7 4 4 44.
5 20
4877 0
15.1
73.
63__
____
____
**3.
3 14<0
.10 23
<2.0
<0.1
0__
____
____ 34 1 1 1 1 1 <1
<0.1 <1 6 10 <1
1100 871
2117 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 06/
21/2
010
ACES: Phase 3B: Characterization of Exposure Atmospheres
130
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V10
9363
5
02/0
2/11
Page
1
14:1
3:01
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
01/2
4/11
01/2
7/11
01/2
8/11
02/0
2/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
24JA
N11
-OIL
- FY
09-1
11-2
4JA
N11
-OIL
, Die
sel E
ngin
e * =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0936
3501
/24/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 64 4 4 7 4 4 44.
5 20
5146 0
15.1
910
.10
____
____
__**
3.4 11
<0.1
0 25<2
.0<0
.10
____
____
__ 35 2 1 1 1 1 <1<0
.1 1 2 3 <1 983
812
2017 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
131
Oil
Type
: SA
E 15
W-4
0 (G
N_0
45)
P.
O. :
JK1
1073
7
Lab
Num
ber :
V10
9912
7
03/0
1/11
Page
1
15:2
8:59
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.S
oot c
onte
nt is
hig
h. O
ther
test
resu
lts a
re a
ccep
tabl
e. D
rain
oil
and
chan
ge fi
lter(s
). A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
se p
rovi
deeq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
02/2
2/11
02/2
4/11
02/2
5/11
03/0
1/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
22FE
B11
-OIL
- FY
09-1
11-2
2FEB
11-O
IL, D
iese
l Eng
ine *
= ex
ceed
s C
autio
n lim
it
**
= e
xcee
ds A
larm
lim
it
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
0991
2702
/22/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 89 7 4 24 15 4 43.
1 20
5437 0
15.3
43.
92__
____
____
**3.
8 13<0
.10 19
<2.0
<0.1
0__
____
____ 35 2 1 1 1 1 <1
<0.1 <1 3 5 <1
1010 902
1723 7 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: N
uno
H. M
orei
ra, E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
132
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
0264
5
03/2
1/11
Page
1
13:3
1:46
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
03/1
4/11
03/1
6/11
03/1
7/11
03/2
1/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
14M
AR
11-O
IL -
FY09
-111
-14M
AR
11-O
IL, D
iese
l Eng
ine
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1026
4503
/14/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 62 4 4 7 4 4 44.
5 20
5693 0
15.0
25.
07__
____
____
**3.
4 11<0
.10 24
<2.0
<0.1
0__
____
____ 34 2 1 1 2 <1 <1
<0.1 <1 2 2 <1
1064 931
2182 5 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
133
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
0627
4
04/1
2/11
Page
1
17:4
1:32
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.S
oot c
onte
nt is
hig
h. O
ther
test
resu
lts a
re a
ccep
tabl
e. D
rain
oil
and
chan
ge fi
lter(s
). A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
se p
rovi
deeq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
04/0
1/11
04/0
7/11
04/0
8/11
04/1
2/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
05A
PR11
-OIL
- FY
09-1
11-0
5APR
11-O
IL, D
iese
l Eng
ine * =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1062
7404
/01/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 60 4 4 7 4 4 44.
5 20
5950 0
15.2
84.
15__
____
____
**3.
3 12<0
.10 15
<2.0
<0.1
0__
____
____ 35 2 1 1 1 1 <1
<0.1 <1 2 <2 <1 987
899
2103 7 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: N
uno
H. M
orei
ra, E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
6/21
/201
0
ACES: Phase 3B: Characterization of Exposure Atmospheres
134
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
0934
4
05/0
2/11
Page
1
13:3
6:18
This
is a
bas
elin
e re
fere
nce
sam
ple.
Res
ult(s
) app
ear a
ccep
tabl
e, n
otin
g th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
unav
aila
ble.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
04/2
6/11
04/2
7/11
04/2
8/11
05/0
2/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : N
ew O
il (G
N_N
O00
1)
ID: F
Y09-
111-
26A
PR11
-NEW
- N
ew M
otor
Oil:
FY0
9-11
1-26
APR
11-O
S222
049C
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1093
4404
/26/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Alum
inumIro
n
Oxi
datio
n
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 6 4 4 7 4 4 44.
5 20
0 015
.93
8.43
____
____
__<0
.1 3<0
.10 <2
<2.0
<0.1
0__
____
____ 2 1 <1 <1 <1 <1 <1
<0.1 <1 3 16 1
1339
1161
2558 8 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 06/
21/2
010
ACES: Phase 3B: Characterization of Exposure Atmospheres
135
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
0934
5
05/0
2/11
Page
1
13:3
6:20
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. T
he T
otal
Bas
e N
umbe
r (re
serv
e al
kalin
ity) i
s ap
proa
chin
g m
inim
umac
cept
able
leve
l. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Addi
tiona
l sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
sepr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
04/2
6/11
04/2
7/11
04/2
8/11
05/0
2/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
ID: F
Y09-
111-
26A
PR11
-OIL
- FY
09-1
11-2
6APR
11-O
IL, D
iese
l Eng
ine * =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1093
4504
/26/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20
6191 0
15.3
4*4
.52
____
____
__**
3.3 15
<0.1
0 19<2
.0<0
.10
____
____
__ 31 2 1 1 1 <1 <1<0
.1 <1 2 <2 <110
24 894
2082 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 06/
21/2
010
ACES: Phase 3B: Characterization of Exposure Atmospheres
136
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
1273
9
05/2
4/11
Page
1
17:0
9:56
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.S
oot c
onte
nt is
hig
h. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for p
rope
r com
bust
ion
prop
ertie
s(e
xhau
st b
ack
pres
sure
, ope
ratin
g te
mpe
ratu
res,
wor
n/br
oken
ring
s, e
xces
sive
idlin
g, h
ung
valv
es,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
.R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
05/1
8/11
05/1
9/11
05/2
0/11
05/2
4/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
18M
AY1
1-O
IL -
FY09
-111
-18M
AR
11-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1127
3905
/18/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 58 4 4 7 4 4 44.
5 20
6438 0
15.2
44.
37__
____
____
**3.
1 14<0
.10 19
<2.0
<0.1
0__
____
____ 21 1 1 1 1 <1 <1
<0.1 <1 1 5 <1 827
705
1622 4 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
137
Oil
Type
: SA
E 15
W-4
0 (G
N_0
45)
P.
O. :
JK1
1073
7
Lab
Num
ber :
V11
1619
3
06/2
1/11
Page
1
09:0
8:18
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
06/0
9/11
06/1
3/11
06/1
4/11
06/2
1/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
09JU
N11
-OIL
- FY
09-1
11-0
9JU
N11
-OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1161
9306
/09/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 89 7 4 24 15 4 43.
1 20 50 50
6694 0
15.2
05.
37__
____
____
**3.
3 16<0
.10 19
<2.0
<0.1
0__
____
____ 30 2 1 1 2 <1 <1
<0.1 <1 2 2 <1
1119
1045
2332 11 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
138
Oil
Type
: SA
E 15
W-4
0 (G
N_0
45)
P.
O. :
JK1
1073
7
Lab
Num
ber :
V11
2080
4
07/1
4/11
Page
1
15:0
3:16
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.Th
e To
tal B
ase
Num
ber (
rese
rve
alka
linity
) is
appr
oach
ing
min
imum
acc
epta
ble
leve
l. S
oot c
onte
ntis
hig
h. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for p
rope
r com
bust
ion
prop
ertie
s (e
xhau
st b
ack
pres
sure
, ope
ratin
g te
mpe
ratu
res,
wor
n/br
oken
ring
s, e
xces
sive
idlin
g, h
ung
valv
es, i
mpr
oper
fuel
setti
ngs,
air
inta
ke re
stric
tions
). A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
atha
lf no
rmal
inte
rval
. Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
07/0
4/11
07/1
1/11
07/1
2/11
07/1
4/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
04JU
L11-
OIL
- FY
09-1
11-0
4JU
L11-
OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1208
0407
/04/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 89 7 4 24 15 4 43.
1 20 50 50
6966 0
15.2
9*3
.75
____
____
__**
3.4 5
<0.1
0 8<2
.0<0
.10
____
____
__ 33 2 1 1 2 <1 <1<0
.1 <1 2 <2 113
1210
2925
72 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
139
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
3289
9
10/0
4/11
Page
1
13:0
2:17
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
07/2
1/11
09/2
9/11
09/3
0/11
10/0
4/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
21JU
L11-
OIL
- FY
09-1
11-2
1Jul
11-O
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1328
9907
/21/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 60 4 4 7 4 4 44.
5 20 50 50
7191 0
15.2
65.
65__
____
____
**3.
2 6<0
.10 13
<2.0
<0.1
0__
____
____ 28 2 1 1 1 <1 <1
<0.1 <1 2 3 1
1108
1001
2235 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
140
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
2561
8
08/1
8/11
Page
1
13:0
2:11
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. F
TIR
indi
cate
s oi
l is
sulfi
nate
d. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for
prop
er c
ombu
stio
n pr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exce
ssiv
e id
ling,
hun
g va
lves
, im
prop
er fu
el s
ettin
gs, a
ir in
take
rest
rictio
ns).
Add
ition
al s
ampl
e is
need
ed to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
08/1
4/11
08/1
5/11
08/1
6/11
08/1
8/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
14A
UG
11-O
IL -
FY09
-111
-14a
ug11
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1256
1808
/14/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 61 4 4 7 4 4 44.
5 20 50 50
7445 0
15.2
15.
45__
____
____
**3.
5 15<0
.10
*30
<2.0
<0.1
0__
____
____ 34 2 1 2 2 <1 <1
<0.1 <1 2 5 <1
1236
1115
2497 10 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
141
Oil
Type
: SA
E 15
W-4
0 (G
N_0
45)
P.
O. :
JK1
1073
7
Lab
Num
ber :
V11
2968
2
09/1
5/11
Page
1
16:1
9:59
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
09/0
7/11
09/1
2/11
09/1
3/11
09/1
5/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
07SE
P11-
OIL
- FY
09-1
11-0
7SEP
11-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1296
8209
/07/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 39 4 4 7 4 4 44.
5 20 50 50
0 015
.04
5.43
____
____
__*3
.0 7<0
.10 13
<2.0
<0.1
0__
____
____ 31 2 1 1 2 1 <1
<0.1 <1 2 3 3
1322
1122
2557 9 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
142
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
3289
8
10/0
4/11
Page
1
13:0
2:14
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. G
lyco
l and
sod
ium
indi
cate
coo
lant
inhi
bito
rs; c
heck
for s
ourc
e. D
rain
oil
and
chan
ge fi
lter(
s).
Che
ck fo
r pro
per c
ombu
stio
n pr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hun
g va
lves
, im
prop
er fu
el s
ettin
gs, a
ir in
take
rest
rictio
ns).
Mon
itor c
oolin
g sy
stem
for l
evel
cha
nges
and
/or a
dditi
ons.
Res
ampl
e at
hal
f nor
mal
inte
rval
.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
09/2
6/11
09/2
9/11
09/3
0/11
10/0
4/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
26SE
P11-
OIL
- FY
09-1
11-2
6Sep
11-O
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1328
9809
/26/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Gly
col
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 60 4 4 7 4 4 44.
5 20 50 50
7937 0
14.9
05.
53__
____
____
**3.
2 7<0
.10 14
<2.0
**0.
42__
____
____ 33 2 1 1 2 <1 <1
<0.1 1 5
**15
0 12 969
875
1982 8 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
143
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
3770
0
11/0
1/11
Page
1
17:0
5:20
NO
RM
AL:
Sam
ple
data
is s
atis
fact
ory.
No
actio
n is
requ
ired
at th
is ti
me.
Addi
tiona
l sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
sepr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
10/2
0/11
10/2
7/11
10/2
8/11
11/0
1/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
20O
CT1
1-O
IL -
FY09
-111
-20O
CT1
1-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1377
0010
/20/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
02.
0016
.80
3.0 30
0.20 30 5.0
0.20 99 16 4 36 50 4 43.
1 20
1487 0
15.4
45.
11__
____
____ 2.6 7
<0.1
0 14<2
.0<0
.10
____
____
__ 46 2 1 2 1 1 <1<0
.1 <1 5 4 111
5010
6323
92 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
144
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
4020
5
11/1
5/11
Page
1
12:5
7:03
NO
RM
AL:
Sam
ple
data
is s
atis
fact
ory.
No
actio
n is
requ
ired
at th
is ti
me.
Plea
se p
rovi
de e
quip
men
t mak
e an
d m
odel
as
wel
l as
the
full
nam
e an
d gr
ade
of th
e lu
bric
ant i
nse
rvic
e. A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
11/0
9/11
11/1
0/11
11/1
1/11
11/1
5/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
09N
OV1
1-O
IL -
FY09
-111
-09N
OV1
1-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1402
0511
/09/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
1697 0
15.2
35.
32__
____
____ 2.3 6
<0.1
0 12<2
.0<0
.10
____
____
__ 40 2 1 1 2 1 <1<0
.1 <1 3 3 <113
0111
0024
76 6 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
145
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
4304
1
12/0
6/11
Page
1
12:5
0:52
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
12/0
1/11
12/0
1/11
12/0
2/11
12/0
6/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
01D
EC11
-OIL
- FY
09-1
11-0
1dec
11-o
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1430
4112
/01/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Silv
erTin
Lead
Cop
per
Chr
omiu
m
Alu
min
umIron
Sulfi
natio
n
Oxi
datio
n
Soot
Typi
cal
War
ning
O
ver
Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
1949 0
15.4
54.
67__
____
____
*2.6 6
<0.1
0 13<2
.0<0
.10
____
____
__ 40 2 1 1 1 1 <1 0.1 <1 3 2 1
1115
1017
2253 6 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
146
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
4304
1
12/0
6/11
Page
1
12:5
0:52
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
12/0
1/11
12/0
1/11
12/0
2/11
12/0
6/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
01D
EC11
-OIL
- FY
09-1
11-0
1dec
11-o
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1430
4112
/01/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Silv
erTin
Lead
Cop
per
Chr
omiu
m
Alu
min
umIron
Sulfi
natio
n
Oxi
datio
n
Soot
Typi
cal
War
ning
O
ver
Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
1949 0
15.4
54.
67__
____
____
*2.6 6
<0.1
0 13<2
.0<0
.10
____
____
__ 40 2 1 1 1 1 <1 0.1 <1 3 2 1
1115
1017
2253 6 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
147
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K-11
0737
Lab
Num
ber :
V11
4593
8
12/2
7/11
Page
1
15:5
2:45
NO
RM
AL:
Sam
ple
data
is s
atis
fact
ory.
No
actio
n is
requ
ired
at th
is ti
me.
Plea
se p
rovi
de e
quip
men
t mak
e an
d m
odel
as
wel
l as
the
full
nam
e an
d gr
ade
of th
e lu
bric
ant i
nse
rvic
e. A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
12/1
9/11
12/2
0/11
12/2
1/11
12/2
7/11
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
19D
EC11
-OIL
- FY
09-1
11-1
9dec
11-o
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1459
3812
/19/
11
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
2181 0
15.2
95.
84__
____
____ 2.4 6
<0.1
0 13<2
.0<0
.10
____
____
__ 45 3 1 1 1 1 <1<0
.1 1 6 4 <115
0312
7428
79 7 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
148
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
4954
3
01/1
8/12
Page
1
17:2
4:11
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
half
norm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
01/1
6/12
01/1
6/12
01/1
7/12
01/1
8/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
16JA
N12
-OIL
- FY
09-1
11-1
6JA
N20
12-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1495
4301
/16/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
2411 0
15.2
56.
58__
____
____
*2.8 10
<0.1
0 16<2
.0<0
.10
____
____
__ 38 2 1 2 1 1 <1<0
.1 <1 2 4 589
785
619
82 11 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
149
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
5278
0
02/1
3/12
Page
1
15:0
8:49
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
02/0
6/12
02/0
7/12
02/0
8/12
02/1
3/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
06FE
B12
-OIL
- FY
09-1
11-0
6FEB
2012
-OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1527
8002
/06/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 59 4 4 7 4 4 44.
5 20 50 50
2683 0
15.5
34.
94__
____
____
*2.9 7
<0.1
0 15<2
.0<0
.10
____
____
__ 37 2 1 1 1 1 <1<0
.1 <1 2 3 <111
05 923
2190 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
150
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
5713
6
03/0
9/12
Page
1
15:5
3:55
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. F
TIR
indi
cate
s oi
l is
sulfi
nate
d. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for
prop
er c
ombu
stio
n pr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exce
ssiv
e id
ling,
hun
g va
lves
, im
prop
er fu
el s
ettin
gs, a
ir in
take
rest
rictio
ns).
Add
ition
al s
ampl
e is
need
ed to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
03/0
6/12
03/0
6/12
03/0
7/12
03/0
9/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
01M
AR
12-O
IL -
FY09
-111
-01M
ar12
-Oil,
Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1571
3603
/06/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
on
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@ 1
00 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 5.0
0.20 58 4 4 7 4 4 44.
5 20 50 50
2998 0
15.4
94.
18__
____
____
**3.
3 18<0
.10
*26
<2.0
<0.1
0__
____
____ 39 2 1 1 1 <1 <1
<0.1 <1 2 <2 1
955
815
1950 5 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
151
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
5900
0
03/2
3/12
Page
1
16:2
4:25
NO
RM
AL:
Sam
ple
data
is s
atis
fact
ory.
No
actio
n is
requ
ired
at th
is ti
me.
Plea
se p
rovi
de e
quip
men
t mak
e an
d m
odel
as
wel
l as
the
full
nam
e an
d gr
ade
of th
e lu
bric
ant i
nse
rvic
e. A
dditi
onal
sam
ple
is n
eede
d to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
03/2
0/12
03/2
0/12
03/2
1/12
03/2
3/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
19M
AR
12-O
IL -
FY09
-111
-19M
AR
12-O
IL, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1590
0003
/20/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 58 4 4 7 4 4 44.
5 20 50 50
3189 0
14.7
66.
22__
____
____ 2.2 6
<0.1
0 12<2
.0<0
.10
____
____
__ 22 2 1 1 1 1 <1<0
.1 <1 3 2 197
987
921
23 6 <1 27 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
152
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
6193
5
04/1
6/12
Page
1
12:5
1:09
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Oth
er te
st re
sults
are
acc
epta
ble.
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
04/1
0/12
04/1
1/12
04/1
2/12
04/1
6/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
10A
PR20
12-O
- FY
09-1
11-1
0apr
2012
-oil,
Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1619
3504
/10/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Silv
er
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 59 4 4 7 4 4 44.
5 20 50 50
0 015
.03
4.83
____
____
__*2
.7 7<0
.10 14
<2.0
<0.1
0__
____
____ 27 2 1 1 1 <1 <1 0.1 1 2 2 <1 941
822
1877 4 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
153
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
6193
5
04/1
6/12
Page
1
12:5
1:09
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Oth
er te
st re
sults
are
acc
epta
ble.
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
04/1
0/12
04/1
1/12
04/1
2/12
04/1
6/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
10A
PR20
12-O
- FY
09-1
11-1
0apr
2012
-oil,
Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1619
3504
/10/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Silv
er
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.0
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 59 4 4 7 4 4 44.
5 20 50 50
0 015
.03
4.83
____
____
__*2
.7 7<0
.10 14
<2.0
<0.1
0__
____
____ 27 2 1 1 1 <1 <1 0.1 1 2 2 <1 941
822
1877 4 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
154
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
6516
0
05/0
9/12
Page
1
13:5
1:52
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.S
oot c
onte
nt is
hig
h. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for p
rope
r com
bust
ion
prop
ertie
s (e
xhau
stba
ck p
ress
ure,
ope
ratin
g te
mpe
ratu
res,
wor
n/br
oken
ring
s, e
xces
sive
idlin
g, h
ung
valv
es, i
mpr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
llna
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
05/0
3/12
05/0
6/12
05/0
7/12
05/0
9/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
03M
AY1
2-O
IL -
FY09
-111
-03M
AY2
012
OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1651
6005
/03/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
02.
0016
.80
3.0 30
0.20 30 2.5
0.20 99 16 4 36 50 4 43.
1 20
3910 0
15.1
34.
94__
____
____
*2.9 7
<0.1
0 16<2
.0<0
.10
____
____
__ 31 2 1 1 1 1 <1<0
.1 <1 3 2 111
51 983
2404 5 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: A
aron
D. L
arso
n, E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
155
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
7360
1
07/1
0/12
Page
1
17:2
2:05
AB
NO
RM
AL:
Abn
orm
al te
st re
sults
are
pre
sent
.So
ot c
onte
nt is
hig
h. C
hrom
ium
may
indi
cate
ring
wea
r. T
in is
an
indi
cato
r of b
earin
g/bu
shin
gal
loys
, bra
ss a
nd/o
r sol
der.
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
. Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
sw
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
07/0
2/12
07/0
8/12
07/0
9/12
07/1
0/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
02JU
L201
2 - F
Y09-
111-
02ju
l201
2-oi
l
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1736
0107
/02/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Vis
@10
0 D
eg C
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
02.
0016
.80
3.0 30
0.20 30 2.5
0.20 99 16 4 36 50 4 43.
1 20
274 0
14.8
75.
09__
____
____
*3.0 15
<0.1
0 20<2
.0<0
.10
____
____
__ 72 2**
7 4 3**
6 <1<0
.1 <1 10 16 114
9311
5829
39 10 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: N
uno
H. M
orei
ra, Q
AM
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
156
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
7793
9
08/0
9/12
Page
1
14:2
5:23
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.To
m H
olm
esLo
vela
ce R
espi
rato
ry R
esea
rch
Inst
itute
2425
Rid
gecr
est D
rive,
SE
Alb
uque
rque
, NM
871
08
07/3
0/12
08/0
6/12
08/0
7/12
08/0
9/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
30JU
L12-
OI -
FY0
9-11
1-30
JUL2
012
OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1779
3907
/30/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 67 4 4 6 4 4 44.
5 20 50 50
540 0
14.4
44.
55__
____
____
*2.9 8
<0.1
0 19<2
.0<0
.10
____
____
__ 44 2 3 2 2 3 <1<0
.1 <1 4 5 111
96 979
2255 6 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
157
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
8005
6
08/2
7/12
Page
1
18:1
2:18
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Dra
in o
il an
d ch
ange
filte
r(s).
Che
ck fo
r pro
per c
ombu
stio
npr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exc
essi
ve id
ling,
hung
val
ves,
impr
oper
fuel
set
tings
, air
inta
ke re
stric
tions
). R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
08/2
1/12
08/2
2/12
08/2
3/12
08/2
7/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
21A
UG
2012
- FY
09-1
11-2
1aug
2012
-oil
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1800
5608
/21/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 67 4 4 6 4 4 44.
5 20 50 50
780 0
14.7
84.
81__
____
____
**3.
1 17<0
.10 25
<2.0
<0.1
0__
____
____ 42 2 2 1 2 2 <1
<0.1 <1 4 5 1
1248
1056
2543 8 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
158
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
8363
4
09/2
0/12
Page
1
13:3
3:52
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
dium
may
indi
cate
coo
lant
inhi
bito
rs; c
heck
for s
ourc
e. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for
prop
er c
ombu
stio
n pr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exce
ssiv
e id
ling,
hun
g va
lves
, im
prop
er fu
el s
ettin
gs, a
ir in
take
rest
rictio
ns).
Add
ition
al s
ampl
e is
need
ed to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Plea
se p
rovi
de e
quip
men
t mak
ean
d m
odel
as
wel
l as
the
full
nam
e an
d gr
ade
of th
e lu
bric
ant i
n se
rvic
e.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
09/1
1/12
09/1
7/12
09/1
8/12
09/2
0/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
11SE
P201
2 - F
Y09-
111-
11se
p201
2-oi
l, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1836
3409
/11/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 67 4 4 6 4 4 44.
5 20 50 50
1069 0
15.0
15.
02__
____
____
**3.
6 16<0
.10 23
<2.0
<0.1
0__
____
____ 42 2 2 2 1 2 <1
<0.1 <1 3 5 2
1222
1059
2291 61 <1 3 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
159
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K110
737
Lab
Num
ber :
V11
9041
8
11/0
2/12
Page
1
11:0
1:43
MO
NIT
OR
: D
ata
for m
achi
ne a
nd/o
r flu
id c
ondi
tion
shou
ld b
e no
ted
and
mon
itore
d.So
ot c
onte
nt is
hig
h. P
leas
e pr
ovid
e eq
uipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
half
norm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
10/2
2/12
10/2
9/12
10/3
0/12
11/0
2/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
22O
CT2
012
- FY0
9-11
1-22
oct2
012-
oil,
Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1904
1810
/22/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
on
Nic
kel
Tin
Lead
Cop
per
Chr
omiu
m
Alu
min
umIron
Sulfi
natio
n
Oxi
datio
n
Soot
Typi
cal
War
ning
O
ver
Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 66 4 4 6 4 4 44.
5 20 50 50
1625 0
14.4
34.
67__
____
____
*2.8 10
<0.1
0 16<2
.0<0
.10
____
____
__ 29 2 1 1 1 2 1<0
.1 <1 3 4 211
9910
0822
96 7 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
160
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
8675
2
10/0
9/12
Page
1
12:1
8:10
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. F
TIR
indi
cate
s oi
l is
sulfi
nate
d. D
rain
oil
and
chan
ge fi
lter(s
). C
heck
for p
rope
rco
mbu
stio
n pr
oper
ties
(exh
aust
bac
k pr
essu
re, o
pera
ting
tem
pera
ture
s, w
orn/
brok
en ri
ngs,
exce
ssiv
e id
ling,
hun
g va
lves
, im
prop
er fu
el s
ettin
gs, a
ir in
take
rest
rictio
ns).
Add
ition
al s
ampl
e is
need
ed to
hel
p es
tabl
ish
trend
. R
esam
ple
at h
alf n
orm
al in
terv
al.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
10/0
3/12
10/0
4/12
10/0
5/12
10/0
9/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
03O
CT1
2-O
IL -
FY09
-111
-03O
CT2
012-
OIL
, Die
sel E
ngin
e
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1867
5210
/03/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 67 4 4 6 4 4 44.
5 20 50 50
1376 0
14.9
55.
08__
____
____
**3.
7 19<0
.10
**33
<2.0
<0.1
0__
____
____ 40 2 2 2 1 2 <1
<0.1 1 2 2 1
1155 995
2407 7 <1 1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: B
obby
R L
icu,
Sen
ior E
valu
ator
- F
or q
uest
ions
abo
ut th
is re
port
, ple
ase
call
888-
437-
4884
.er
labg
t1.fr
x R
ev. 0
5/19
/11
ACES: Phase 3B: Characterization of Exposure Atmospheres
161
Oil
Type
: SA
E 40
(GN
_032
)
P.O
. : J
K120
015
Lab
Num
ber :
V11
9270
3
11/1
6/12
Page
1
10:4
6:39
AB
NO
RM
AL:
Abn
orm
al re
sults
for f
luid
are
pre
sent
. E
quip
men
t app
ears
sat
isfa
ctor
y.So
ot c
onte
nt is
hig
h. L
evel
s m
ay b
e du
e to
oil
serv
ice
time
(not
pro
vide
d).
Dra
in o
il an
d ch
ange
filte
r(s).
Add
ition
al s
ampl
e is
nee
ded
to h
elp
esta
blis
h tre
nd.
Res
ampl
e at
hal
f nor
mal
inte
rval
.Pl
ease
pro
vide
equ
ipm
ent m
ake
and
mod
el a
s w
ell a
s th
e fu
ll na
me
and
grad
e of
the
lubr
ican
t in
serv
ice.
Tom
Hol
mes
Love
lace
Res
pira
tory
Res
earc
h In
stitu
te24
25 R
idge
cres
t Driv
e, S
E
Alb
uque
rque
, NM
871
08
11/1
2/12
11/1
3/12
11/1
4/12
11/1
6/12
Ship
ped
:R
ecei
ved:
Prin
ted:
Sam
pled
:
Uni
t Typ
e : E
ngin
e, D
iese
l (G
N_D
E001
)
* =
exce
eds
Cau
tion
limit
** =
exc
eeds
Ala
rm li
mit
101
Cor
pora
te P
lace
, Val
lejo
, CA
9459
0w
ww
.her
guth
.com
ISO
900
1:20
08 a
nd IS
O/IE
C 1
7025
:200
5 C
ertif
ied
ID: F
Y09-
111-
12N
OV1
2-O
IL -
FY09
-111
-12N
ov20
12-O
il, D
iese
l Eng
ine
Lab
Num
ber
Sam
ple
Dat
eM
inim
umM
axim
umV1
1927
0311
/12/
12
Com
para
tive
Gra
phic
Ana
lysi
s
Sodi
um
Silic
onTin
Lead
Cop
per
Chr
omiu
m
Alum
inumIro
n
Sulfi
natio
n
Oxi
datio
n
Soot
TBN
Und
er M
in
War
ning
Typ
ical
Typ
ical
War
ning
Ove
r Max
Uni
t Tim
e (H
R)
Flui
d Ti
me
(HR
)Vi
s @
100
Deg
CTB
N m
g K
OH
/gFT
IR Soot
% w
t.O
xida
tion
Abs/
cmW
ater
FTI
R %
Vol
Sulfi
natio
n Ab
s/Fu
el %
Vol
Gly
col %
Vol
Met
als
Iron
ppm
Alum
inum
ppm
Chr
omiu
m p
pmC
oppe
r ppm
Lead
ppm
Tin
ppm
Nic
kel p
pmSi
lver
ppm
Antim
ony
ppm
Silic
on p
pmSo
dium
ppm
Boro
n pp
mZi
nc p
pmPh
osph
orus
ppm
Cal
cium
ppm
Mag
nesi
um p
pmBa
rium
ppm
Mol
ybde
num
ppm
Pota
ssiu
m p
pm
12.5
03.
0016
.80
3.0 30
0.20 30 2.5
0.20 66 4 4 6 4 4 44.
5 20 50 50
1889 0
14.4
04.
83__
____
____
*3.0 11
<0.1
0 18<2
.0<0
.10
____
____
__ 26 2 1 1 1 1 <1<0
.1 <1 2 4 <111
85 923
2264 6 <1 <1 <3
Cod
e :L
OVE
MC
Lov
elac
e R
espi
rato
ry R
esea
rch
Inst
itute
Pho
ne :(
505)
348
-960
0 F
ax :(
505)
348
-498
0Th
ese
resu
lts a
re s
ubm
itted
pur
suan
t to
our c
urre
nt T
erm
s, C
ondi
tions
and
Lim
itatio
ns a
nd L
abor
ator
y P
ricin
g P
olic
y. N
o re
spon
sibi
lity
or li
abili
ty is
ass
umed
for t
he m
anne
r in
whi
ch th
ese
resu
lts a
re u
sed
or in
terp
rete
d.
Eval
uate
d B
y: D
avid
F. F
ryck
i, C
LS -
For
que
stio
ns a
bout
this
repo
rt, p
leas
e ca
ll 88
8-43
7-48
84.
erla
bgt1
.frx
Rev
. 05/
19/1
1
ACES: Phase 3B: Characterization of Exposure Atmospheres
162