AAnalyst 600AAnalyst 600

ES HwangES Hwang

Inorganic Product SpecialistInorganic Product Specialist

PerkinElmer KoreaPerkinElmer Korea

AAnalyst 600…AAnalyst 600…

FeaturesFeatures• Dedicated THGA furnaceDedicated THGA furnace• High sensitivity segmented High sensitivity segmented

solid-state photodiode solid-state photodiode detectordetector

• Simultaneous measurement Simultaneous measurement of sample and reference of sample and reference beamsbeams

• Transversely heated graphite Transversely heated graphite furnace furnace

• Longitudinal Zeeman effect Longitudinal Zeeman effect background correction background correction

BenefitsBenefits THGA furnace reduces THGA furnace reduces

interferences in difficult matricesinterferences in difficult matrices Exceptional analytical performance Exceptional analytical performance

and detection limitsand detection limits Highest Long-term StabilityHighest Long-term Stability Minimized interferences and Minimized interferences and

memory effectsmemory effects Shorter analysis time (fast furnace Shorter analysis time (fast furnace

programs)programs) Best possible background Best possible background

correction with no light losscorrection with no light loss

… … the best dedicated THGA furnace systemthe best dedicated THGA furnace system

AAnalyst 600 AAnalyst 600 AA SpectrometersAA Spectrometers

AAnalyst 600 AAnalyst 600 Revolutionary Optical SystemRevolutionary Optical System

AAnalyst 600 AAnalyst 600 Unique FeaturesUnique Features

First AA spectrometerFirst AA spectrometer • Integrated furnaceIntegrated furnace

Zeeman-THGA graphite furnaceZeeman-THGA graphite furnace

AAnalyst 600 AAnalyst 600 Unique FeaturesUnique Features

First AA spectrometerFirst AA spectrometer• 8-8-lamp holderlamp holder

Automatic lamp selection and adjustment Automatic lamp selection and adjustment • Built-in power suppliesBuilt-in power supplies

Hollow cathode lampsHollow cathode lamps Electrodeless discharge lamps Electrodeless discharge lamps

AAnalyst 600AAnalyst 600Highly Versatile Furnace AutosamplerHighly Versatile Furnace Autosampler

User Benefits:User Benefits: Automatic generation Automatic generation

of reference solutionsof reference solutions Automatic multiple Automatic multiple

injectionsinjections Automatic dilutionAutomatic dilution Automatic injection Automatic injection

into a preheated tube into a preheated tube Variable pipetting Variable pipetting

speedspeed Ease-of-operationEase-of-operation

AAnalyst 600 AAnalyst 600 Revolutionary Optical SystemRevolutionary Optical System

Real time double beam system Real time double beam system

High sensitivity segmented solid-state photodiode High sensitivity segmented solid-state photodiode detectordetector• User Benefits:User Benefits:

Exceptional analytical performanceExceptional analytical performance Highest Long-term StabilityHighest Long-term Stability

AAnalyst 600 AAnalyst 600 Customized Solid-State DetectorCustomized Solid-State Detector

Highest quantum efficiency Integrated low noise CMOS

charge amplifier array Exceptional signal-to-noise ratio

AAnalyst 600 AAnalyst 600 Quantum Efficiency of DetectorsQuantum Efficiency of Detectors

photomultiplier

solid state detector

AAnalyst 600 AAnalyst 600 Furnace (THGA) Instrument Detection LimitsFurnace (THGA) Instrument Detection Limits

THGA Instrument detection limits (IDL) / pgTHGA Instrument detection limits (IDL) / pg

ElementElement PMT PMT PhotodiodePhotodiode

AsAs 9 9 66

CrCr 1.5 1.5 0.40.4

CuCu 5 5 44

MnMn 2 2 1.51.5

PbPb 3 3 3 3

TlTl 7.5 7.5 77

AAnalyst 600 AAnalyst 600 Automatic Lamp SelectorAutomatic Lamp Selector

8-Lamp holder Built-in power

supplies for hollow cathode and electrodeless discharge lamps

Automatic alignment, element, wavelength and slit selection

AAnalyst 600 AAnalyst 600 Unique Overall ConceptionUnique Overall Conception

Total system control Total system control via via AA WinLab32 software for AA WinLab32 software for highest versatility and simplest operating highest versatility and simplest operating convenienceconvenience• Atomizer controlAtomizer control• Lamp and lamp current controlLamp and lamp current control• THGA controlTHGA control• Accessory controlAccessory control

AAnalyst 600 AAnalyst 600 Unique Software ConceptionUnique Software Conception

Automatic system setup from stored user’s methodsAutomatic system setup from stored user’s methods• Direct from Direct from WorkspaceWorkspace

MethodMethod Sample informationSample information Individual screen design, window selection Individual screen design, window selection etcetc..

• User Benefits:User Benefits: Analytical reliability Analytical reliability Ease-of-operationEase-of-operation Time-savingTime-saving

Bringing a new level of productivity to high-performance AA

WinLab32 for AAWinLab32 for AA

AA WinLab32 - Features and BenefitsAA WinLab32 - Features and Benefits

Improve productivityImprove productivity• Data Reprocessing *Data Reprocessing *• WinLab32 Offline *WinLab32 Offline *• Priority samples *Priority samples *• Append to Analysis List *Append to Analysis List *• Edit CalibrationEdit Calibration• Recall CalibrationRecall Calibration• Furnace Method Development wizard *Furnace Method Development wizard *

Improve ease of use and reduce trainingImprove ease of use and reduce training• Tool tips (available in 6 languages) *Tool tips (available in 6 languages) *• Wizards *Wizards *• Analysis List *Analysis List *• AS-93 parameters integrated *AS-93 parameters integrated *

* New features not present in 16-bit AA WinLab

AA WinLab32 - Features and BenefitsAA WinLab32 - Features and Benefits

Reduce training and supportReduce training and support• Common look and feel with WinLab32 for ICP-OESCommon look and feel with WinLab32 for ICP-OES• CD Document PackCD Document Pack

Improve stability and data accessibilityImprove stability and data accessibility• Access database *Access database *

Method and data securityMethod and data security• Password protection *Password protection *• Multiple user levels *Multiple user levels *• Data check sums to detect changes *Data check sums to detect changes *• 21 CFR Part 11 Compliant21 CFR Part 11 Compliant

* New features not present in 16-bit AA WinLab

WinLab32 for AA WorkspaceWinLab32 for AA Workspace

Toolbar

Automated Analysis

Results

Status Monitor

Common look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform training

Calibration

Data ReprocessingData Reprocessing

Recalculation of analytical data Recalculation of analytical data • Correct SIF errorsCorrect SIF errors• Change calibration functionChange calibration function• Delete replicate(s)Delete replicate(s)

Performed using the raw dataPerformed using the raw data Samples can be reprocessed in any sequenceSamples can be reprocessed in any sequence Original data are preservedOriginal data are preserved Analytical log can be printedAnalytical log can be printed Reprocessed data are identified Reprocessed data are identified

Data ReprocessingData Reprocessing

Select samples in the order you want them

reprocessed.

Status display

Change sample information in these

columns

Furnace Method Development WizardFurnace Method Development Wizard

Define FurnaceSteps to cycleTemperatures

Define SolutionsTo Analyze

Analyze Solutions and Display Results

Align Autosampler Tip WizardAlign Autosampler Tip Wizard

Auto dilution by systemAuto dilution by system

Priority SamplePriority Sample

Samples can be added without interrupting current analyses

Exporting Data to LABWORKSExporting Data to LABWORKS

Export data to LABWORKS

WinLab32 Enhanced Security OptionWinLab32 Enhanced Security Option

Enhancement to WinLab32 for AA (Enhancement to WinLab32 for AA (andand ICP) ICP) Significant set of new featuresSignificant set of new features

• Audit trailsAudit trails• File versioningFile versioning

Enable compliance with new regulationsEnable compliance with new regulations• 21 CFR Part 11 - Pharmaceutical21 CFR Part 11 - Pharmaceutical• 40 CFR Part 3 - Environmental (proposed)40 CFR Part 3 - Environmental (proposed)• OthersOthers

Primarily for highly regulated laboratoriesPrimarily for highly regulated laboratories• Users actions are restrictedUsers actions are restricted• Increased storage space requirementsIncreased storage space requirements• Additional information entry requirementsAdditional information entry requirements• Requires more system housekeepingRequires more system housekeeping

AAnalyst 600 AAnalyst 600 Total Range Graphite Furnace AATotal Range Graphite Furnace AA

THGA-type furnace with Zeeman-effect background THGA-type furnace with Zeeman-effect background correctioncorrection

User Benefits:User Benefits: Selection of the best system for individual Selection of the best system for individual

requirements and budgetsrequirements and budgets High performance, near interference-free trace High performance, near interference-free trace

analysis with STPF conceptanalysis with STPF concept

AAnalyst 600AAnalyst 600Integrated THGA Furnace SystemIntegrated THGA Furnace System

AAnalyst 600AAnalyst 600Zeeman THGA FurnaceZeeman THGA Furnace

Transversely heated graphite furnace Transversely heated graphite furnace

Longitudinal Zeeman effect background correction Longitudinal Zeeman effect background correction

User Benefits:User Benefits: Exceptional detection limitsExceptional detection limits Minimized interferences and memory effectsMinimized interferences and memory effects Best possible background correctionBest possible background correction Mimimum sample preparation timeMimimum sample preparation time Shorter analysis time (fast furnace programs)Shorter analysis time (fast furnace programs)

AAnalyst 600 AAnalyst 600 Integrated THGA SystemIntegrated THGA System

THGA Concept: more THGA Concept: more than 2500 systems in than 2500 systems in use use

Longitudinal Zeeman-Longitudinal Zeeman-Effect: highly resolved Effect: highly resolved background background compensation without compensation without light losslight loss

DC furnace power DC furnace power supplysupply

Closest approach Closest approach to the "ideal system" to the "ideal system"

AAnalyst 600 AAnalyst 600 Integrated THGA SystemIntegrated THGA System

0.000

0.025

0.050

0.075

0.100

0.125

0 1 2 3 4 5 6 7 8

Time / s

Ab

sorb

ance

AA-BG

BG

Atomic and background signals

for Ba, 20uL, 25 ug/L

AAnalyst 600AAnalyst 600 Zeeman Zeeman versus versus DD2 2 Background CorrectionBackground Correction

Background correction independent of wavelengthBackground correction independent of wavelength

True double-beam with only one optical pathTrue double-beam with only one optical path

Baseline noise at least 2x lowerBaseline noise at least 2x lower

Optical resolution Optical resolution is 100x better is 100x better

Char. mass typically 10 and 20 % poorer than with DChar. mass typically 10 and 20 % poorer than with D22 (the (the

mm00 for the worst case, Cu, is 50% poorer) for the worst case, Cu, is 50% poorer)

Zeeman-effect background correction gives superior Zeeman-effect background correction gives superior detection limits in real samplesdetection limits in real samples

AAnalyst 600 AAnalyst 600 Highly Versatile Furnace AutosamplerHighly Versatile Furnace Autosampler

High-capacity, interchangeable sample traysHigh-capacity, interchangeable sample trays88 88 or 146 sample positionsor 146 sample positions

Full AA WinLab32 control including multi-taskingFull AA WinLab32 control including multi-tasking

User Benefits:User Benefits: Automatic generation of reference solutionsAutomatic generation of reference solutions Automatic multiple injectionsAutomatic multiple injections Automatic dilutionAutomatic dilution Automatic injection into a preheated tube Automatic injection into a preheated tube Variable pipetting speedVariable pipetting speed Ease-of-operationEase-of-operation

AAnalyst 600AAnalyst 600Flow Injection - Furnace CouplingFlow Injection - Furnace Coupling

Optional accessory for coupling FI-MHS with furnace Optional accessory for coupling FI-MHS with furnace AAAA

Software controlled automatic operationSoftware controlled automatic operation

User Benefits:User Benefits: Detection limits in range of ng/LDetection limits in range of ng/L Time-savings by automatic on-line operationTime-savings by automatic on-line operation Less interferences since matrix components are Less interferences since matrix components are

removed in the FI systemremoved in the FI system

AAnalyst 600 AAnalyst 600 Automatic Slurry SamplingAutomatic Slurry Sampling

Optional ultrasonic probe integrated in the Optional ultrasonic probe integrated in the autosampler autosampler

Automatic introduction of solid samples as slurriesAutomatic introduction of solid samples as slurries

Full software controlFull software control

User Benefits:User Benefits: Reduced sample preparation and analysis timeReduced sample preparation and analysis time Reduced potential for contaminationReduced potential for contamination Easy operationEasy operation

What else can PerkinElmer offer?What else can PerkinElmer offer?

Sample Preparation SolutionsSample Preparation Solutions• Multiwave 3000 Multiwave 3000 • High Pressure Asher (HPA)High Pressure Asher (HPA)

Flow Injection Technology (FIAS)Flow Injection Technology (FIAS)• For sample pre-treatmentFor sample pre-treatment• Hydride generationHydride generation

Stand-alone Mercury systems (FIMS)Stand-alone Mercury systems (FIMS) Sample Introduction SystemsSample Introduction Systems

• AutodilutorsAutodilutors• Laser Ablation systemsLaser Ablation systems

World class service and supportWorld class service and support

Inorganic sample preparation….Inorganic sample preparation….

Multiwave 3000Multiwave 3000• Reduced digestion timesReduced digestion times• Superior digestion qualitySuperior digestion quality• Time-saving Time-saving • Easy operationEasy operation• Maximum safetyMaximum safety

High Pressure AsherHigh Pressure Asher• Complete sample Complete sample

mineralizationmineralization• Minimum organic residueMinimum organic residue• No elemental lossesNo elemental losses• No contaminationNo contamination

……a clear solution for sample preparation !a clear solution for sample preparation !

Multiwave 3000Multiwave 3000

HPA systemHPA system

FIAS – Flow Injection SystemsFIAS – Flow Injection Systems

2 2 ModelsModels• FIAS 100 (1 valve, 1 pump)FIAS 100 (1 valve, 1 pump)• FIAS 400 (1 valve, 2 pumps)FIAS 400 (1 valve, 2 pumps)

Automated sampling for Automated sampling for Flame AAFlame AA• DilutionDilution• Add reagents or modifiersAdd reagents or modifiers• Matrix removalMatrix removal• PreconcentrationPreconcentration

Improved sample handlingImproved sample handling• Small sample volumesSmall sample volumes• High solids samplesHigh solids samples

Hydride generationHydride generation• Determination of As, Se, Te, Determination of As, Se, Te,

Be, Sb, SnBe, Sb, Sn

FIAS 100 systemFIAS 100 system

FIAS 400 systemFIAS 400 system

Flow Injection Mercury SystemsFlow Injection Mercury Systems

FIMS 400FIMS 400• Determines Mercury via Determines Mercury via

Cold Vapor AA (CVAA)Cold Vapor AA (CVAA)

• Small footprintSmall footprint

• Fully automatedFully automated

• Easy to operateEasy to operate

• Stand alone systemStand alone system

• Cost effectiveCost effective

• Now with WinLab32 for AA Now with WinLab32 for AA softwaresoftware

AAnalyst 600 AAnalyst 600 ConclusionsConclusions

Not just another AA!Not just another AA!

No compromises!No compromises!

Easiest, simplest AA furnace Easiest, simplest AA furnace

Full automationFull automation

Full range of accessoriesFull range of accessories

Power of AA WinLab32 softwarePower of AA WinLab32 software

Ultimate in performanceUltimate in performance

The AA instrument to take you beyond 2000...The AA instrument to take you beyond 2000...