5-2012jpn105deg-yabe
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Determination of moistureDetermination of moisturecontentcontent
in Japanin Japan
Routine reference methodRoutine reference method
JapaneseStandard
JPN (105 JPN (105˚C)˚C)
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1. Appication1. Appication
!.!. De"nition #. Apparatus#. Apparatus
$.$. Procedure 5.5. Cacuation and e%pression of
resuts
&. R&. Re'ision
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1.Appication1.Appication
his method is appied to
padd*+ ,ro-n rice+ -hite rice+-heat + ,are*+ naed ,are*+ ,uc-heat + so*,ean and ,eans in form
of /rain
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!. De"nition!. De"nition
oss in mass+ e%pressed as aoss in mass+ e%pressed as apercenta/e+ under/one ,* the productpercenta/e+ under/one ,* the product
under the conditions speci"ed in thisunder the conditions speci"ed in thisstandardstandard
oisture content is e%pressed as aoisture content is e%pressed as apercenta/epercenta/e
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#. Apparatus#. Apparatus
1) Ana*tica ,aance1) Ana*tica ,aance
!) 2rindin/ mi!) 2rindin/ mi
#) eta dish#) eta dish$) 3'en$) 3'en
5) Desiccator5) Desiccator
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#. Apparatus41#. Apparatus41
1) Ana*tica1) Ana*tica,aance,aance
Capa,e ofCapa,e of-ei/hin/ to an-ei/hin/ to an
accurac* of accurac* of
0.1m/0.1m/
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#. Apparatus4!#. Apparatus4!
!)!) 2rindin/ mi2rindin/ mi
not a,sor,not a,sor,
moisture+ eas* tomoisture+ eas* tocean+cean+
-ithout heat+-ithout heat+ti/htness to air+ti/htness to air+
at !0at !0˚C˚C and &06and &06R.7.R.7.
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#. Apparatus4##. Apparatus4#
#)#) eta disheta dish
Non4corrodi,e+Non4corrodi,e+
ti/ht4"ttin/+ti/ht4"ttin/+ AuminumAuminum
container+container+
a diameter ofa diameter of 5050~~ &0 mm&0 mm andandhei/ht ofhei/ht of !5 mm!5 mm
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#. Apparatus4$#. Apparatus4$
$)$) 3'en3'en Constant andConstant and
sta,esta,e forfor 5hr at5hr at
10&.510&.5˚C˚C 1.01.0˚C˚C++andand correspond tocorrespond to
the a,orator*the a,orator*conditioncondition
at !0at !0˚C˚C andand&06 R7.&06 R7.
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#. Apparatus45#. Apparatus45
5)5) DesiccatorDesiccator
Containin/ anContainin/ an
e8ecti'ee8ecti'edesiccantdesiccant
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$. Procedure41$. Procedure41
he resut is the arithmetic he resut is the arithmeticmean of t-o separatemean of t-o separatedeterminations of thedeterminations of themoisture contents -hichmoisture contents -hichmeet themeet the repeata,iit*repeata,iit*re9uirementre9uirement++
sha not e%ceedsha not e%ceed 0.16.0.16.Round the resut toRound the resut to one pacesone paces
of decimas.of decimas.
1)1) :ei/h empt* dishes to the:ei/h empt* dishes to the
nearestnearest 0.1m/0.1m/
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$. Procedure4!$. Procedure4!
!)!) est portion est portion;n case of sampes to;n case of sampes to,e /round+ pro'ide a,e /round+ pro'ide atest portiontest portion si/ht*si/ht*
/reater than 5//reater than 5/,efore /rindin/+ and,efore /rindin/+ and-ei/h a the /rind.-ei/h a the /rind.
:ei/h the test:ei/h the testportions afterportions after/rindin/ to the/rindin/ to thenearestnearest 0.1m/0.1m/..
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$. Procedure4#$. Procedure4#
#)#) Dr*in/ Dr*in/ Pace the open dishesPace the open dishes
containin/ the testcontainin/ the testportions to/ether -ithportions to/ether -ith
the ids in the o'enthe ids in the o'enand ea'e forand ea'e for5hr5min5hr5min from thefrom themoment -henmoment -hen
the o'en temperaturethe o'en temperature
is re/ained tois re/ained to 10&.510&.5˚C˚C 1.01.0 ゚゚ ˚C˚C..
Do not open the o'enDo not open the o'endoor durin/ dr*in/.door durin/ dr*in/.
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$. Procedure4$$. Procedure4$
$)$) :ei/hin/ :ei/hin/ :hen the:hen the
dishes ha'edishes ha'e
cooed to thecooed to thea,orator*a,orator*temperature+temperature+-ei/h them to-ei/h them to
the nearestthe nearest0.1m/.0.1m/.
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55. Cacuation and e%pression. Cacuation and e%pressionof resuts of resuts
he moisture content+ he moisture content+ mm%%+ e%pressed as+ e%pressed aspercenta/e ,* mass is /i'en ,* the foo-in/percenta/e ,* mass is /i'en ,* the foo-in/e9uations.e9uations.
mm%% --00)?1006)?1006
-here-here --00 andand --11 are the -ei/hts+ in /rams+ ofare the -ei/hts+ in /rams+ ofthe test portion and the dried test portion+the test portion and the dried test portion+
respecti'e*.respecti'e*.
he resut is the arithmetic mean of t-o he resut is the arithmetic mean of t-omeasurements 'aues -hich meet themeasurements 'aues -hich meet therepeata,iit* re9uirement+0.16.repeata,iit* re9uirement+0.16. Round theRound the05/15/16 15
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&.Re'ision&.Re'ision
105105 ˚C˚C.. method ismethod isa8ected ,* thea8ected ,* the
en'ironmentaen'ironmentacondition.condition.
(temperature and(temperature and
humidit*)humidit*)
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Rice Con'ersion ta,eRice Con'ersion ta,e
Needed to countNeeded to countthethemeasurementmeasurement
resuts to theresuts to thereferencereferencecondition ofcondition of!0!0˚C˚C and &0and &0%%
R.7.R.7.
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Thank You for your attention!