* 0007a 1a ; volatile organics analysis data sheet · 2020. 11. 30. · id epa sample no. pesticide...

* 0007A1A ;VOLATILE ORGANICS ANALYSIS DATA SHEET

: ITW-iBab Name: IT PITTSBURGH Contract:

Lab' Code: TTPA _ Case No.: 03_485 SAS 'to . : 3DG Me.: " " =

Matrix: : soil/water} SOIL.,.. Lab Sar.ple ID: ITW-13

Sair.pie wt/vcl: 5.2 (g/r.L) G Lab Filv ID:

Level: (low/r.ed) LpW_ Date Deceived:

% Moisture: not dec. 26 Dat-j Analysed:

Column: 'pack/cap) PACK Dilution Factor: 1.:

CONCENTRATION UNITS:CAS NO. COMPOUND 'ug/L or ug/Kg: UG/KG ;

!

; 74-37-3 —— ——— --Chioromethane_______________\ 13 ;u! 74-33-9-- — -----Bro-r.ome thane_______________: 13 'U! 75-01-4————————Vinyl Chloride_____________' 13 U; 75-00-3————————Chloroethane_______________1 13 -U I; 75-09-2-------—Methylene .Chloride__________', 6 !3J-! 67-64-1 ———————— Acetone____________________1 13 : U .i 75-15-0 ————— — Carbon Disulfide___________; 6 'rJ! 75-35-4 ——————— 1,1-Dichlorcethane_________; 6; 75-34-3 ——————— 1,1-Dichloroethane_________1 6 '•'; 540-59-0- — ——— 1,2-Dichloroethene (total)__; 5! 57-56-3----- — --Chloroform_________________; 5 "\ 107-0(5-2 —————— -1,2-Dichioroethar.e_________; 6: 78-33-3 — ————— 2-Butanone___________:____! 15! 71-55-6------- — 1,1,1-Trichloroethane_______: 5i 56-23-5 ——————Carbon Tetrachlorida_______! 5! 103-05-4——————Vinyl Acetate______________! 13! 75-27-4--——----Bromodichloromethane_______\ 6I 73-37-5 — — - — --1, 2-Dichloropropane________; 6! 10061-01-5 —— -—cis-1, 3-Dichloropropene_____; 6! 79-01-6 —— ————Trichloroethene___________: 61 124-48-1——————Dibromochloronsethane_______! 6! 79-00-5———————1,1, 2-Trichloroethane_______' 6i 71-43-2———————Benzene__________________! 6 . U! 10061-02-6————Trans-1, 3-Dichloropropene___' 6 '• Ui 110-75-8 ——————— 2-CHLOROETHYLVINYLETHER_____! at-W-! 75-25-2————————Bromoforn__________________' 6 'J! 108-10-1 —————— 4-Methyl-2-Pentanone_______! 13! 591-78-6 —————— 2-Hexanone________________! 13! 127-18-4- — ———Tetrachloroethene__________'. 6 ;u! 79-34-5———————1,1,2,2-Tetrachloroethar.e___' 6 :u! 103-38-3 ———— ——Toluene___________________! 6 ;*J! 108-90-7 —— -----Chlorobenzen-s_____________'•. 6 'U! 1CO-41-4 ————— -Ethylbenzene______________! 5! 100-42-5 —————— Styrene___________________! 6! 1320-20-7—.-———Total Xylenes______________', 5i 107-02-3——————ACROLEIN_________________;

FORM I VGA

ftR382B60

! 107-13-1———————ACRYLONITRILE_______________: 4$ -5-

FORM I VOA

AR30286I

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: IT PITTSBURGH _____ -Contract:ITW-.,,0 0217[

Jode: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 005

Matrix: (soil/water) SOIL Lab Sample ID: Q00209002

Sample wt/vol: 30.0 (g/mL) G__ Lab File ID: _______

Level: (low/med) LOW Date Received: 02/17/90

% Moisture: not dec. 25 dec. ___ Date Extracted: 02/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 02/24/90

GPC Cleanup: (Y/N) Y_ pH: 4.4 Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

319-84-6 ——————— alpha-BHC_________319-85-7———————beta-BHC__________319-86-8——————delta-BHC________58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9————————4 , 4 ' -DDE__________72-20-8———————Endrin__________33213-65-9————Endosulfan II_____72-54-8 ——————— 4 , 4 ' -ODD_________1031-07-8—————Endosulfan sulfate_50-29-3———————4 , 4 ' -DDT_________72-43-5———————Methoxychlor__53494-70-5————Endrin ketone_5103-71-9—————alpha-Chlordane.5103-74-2—————gamma-Chlordane.8001-35-2—————Toxaphene_____12674-11-2—————Aroclor-1016___11104-28-2————Aroclor-1221__11141-16-5————Aroclor-1232__53469-21-9————Aroclor-1242__12672-29-6—————Aroclor-1248___11097-69-1————Aroclor-1254__11096-82-5————Aroclor-1260__

21 |U21 iU21 iU21 !U21 !U21 iU21 !U21 !U43 iU43 !U43 !U43 !U43 !U43 !U43 iU

210 iU43 iU

210 !U210 !U430 iU210 iU210 !U210 !U210 !U210 |U430 iU430 !U

FORM I PEST 1/87 Rev,

IB3028S2

0003, EPA - CLP

r.imo: I'ASJ^ITTSBUPQH __ . ___ . __ . Con IT- -a- 1 : ^Tr":F3TCNE

-i.c '-.3C il/wr.tsr) ; =GIL

el ' lo;«/ iT̂ d ) '. L3W__

or,ca-!tr9.t io.~i LJni';= (ug'L ;r m g - k g dry -alight); i^G, KG

ICAS Mo.

i 7429-90-517445-38-2! 7440-39-3| r?4./40~-4" ~7i 7440-43-9i 7̂ 40-70-E! 7440-47-3! 7-440-48-41 7440-50-817439-39-6174-39-92-117439-95-41 7439-96-517439-97-6I 7440-02-01 74-40-09-71 7440-EE-4! 7440-E3-5! 7440-E8-01 744O-6E-EI 7̂ 40-66-61 _;&.1 ]•££1 1«ni» •

1 Analyte

1 Aluminum! Ar sen i c1 Sari urn1 Bervl 1 i urni CadmiumI Calcium1 ChromiumI Cobalti Copper1 IronI Lead1 Magnesiumi Manganese1 Mercury1 Nickel! Potassium1 Si Iver1 SodiumIThallium1 VanadiumIZinc1111

! Corcentration

1 264001 0.531 54.71 2 . 0! 0 . 53! 194I 9,91 E3..41 43.61 46EOO1 9.5i 79SO1 418: 0.13i ii.i! 985i i .a! 76.6i 0 . 53i 144! 78.4i1!1

1 r" i r> 'MI1 '—* » 0; it i

! ' i !1 ! IP 1I'J! WN IF !1 ! IP :! ! IP !! U 1 N i P i1 S i ! P :! I IP 11 I IP 11 ! IP 1I I - P I1 I 3M IF :I I I P ii ! IP 1i u i : cv iI I I P i131 E ;P 1IB! IP '1 B 1 IP!IL'I W IF 11 i E IP 1I I I P 1I ! I I! I 1 iI I 1 11 ! 1 I

Color Before: BROWN___ Clari ny Before: _____ Textures!

Color After: BROWN___ Clarity After: _____ Artifacts

Comments:

FORM I - IN

AR302863

* 0013A1A E?A SAMPLE JfC .

VOLATILE ORGANICS ANALYSIS DATA SHEET

,ab Name: IT PITTSBURGH .. Contract:

Lab Code: ITPA___ Case No.: Q34_86 SAS Mo.: __ _ ._ SDG No.: O C 5 _ _

Matrix: (soil/water) SOIL . .. Lab Sample ID: ITW-1C

Sample wt/vol: ._5.Q. (g/iaL) G.._ _ Lab File ID: 2Q7C222D

Level: (low/^ed) LOW_ Date Received: C2/l"/9:

% Moisture: not dec. _ _2_5 __ Date Analyzed: 02/22/90

Column: (pack/cap) PACK_ Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3———————Chlorome thane__________74-33-9-----—--Broir.oir.e thane___________75-01-4———————Vinyl Chloride_________75-00-3————————Chloroe thane____________75-09-2————————Methylene Chloride_______67-64-1-——-—--Acetone________________75-15-0————————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene______75-34-3———--—1,1-Dichloroethane______540-59-0 —————— 1, 2-Dichloroethene (total67-66-3----—---Chloroform_____________107-06-2 —————— 1, 2-Dichloroethane______78-93-3 ——— ———— 2-Butanone_____________71-55-6 ——————— 1,1,1-Trichloroethane___56-23-5- ——— ———Carbon Tetrachloride______108-05-4——————Vinyl Acetate___________75-27-4-—————-Bromodichloromethane____78-87-5———————1, 2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene79-01-6———————Trichloroethene________124-48-1——————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroe thane71-43-2———————Benzene_______________10061-02-6————Trans-1,3-Dichloropropene110-75-8;———————2-CHLOROETHYLVINYLETHER75-25-2———————Bromoform___________________108-10-1——————4-Methyl-2-Pentanone____591-73-6———————2-Hexanone_____________127-18-4—-———Tetrachloroethene_______79-34-5———————1,1,2, 2-Tetrachloroethane.108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________

13 ;u13 !U13 !U13 !U5 !BJ

15 '7 !U7"7

77 !U7 ;u

35 '7 U7

13 'U7 ' U7 ,U7 !U7 :u7 :u7 !U77 :u

7 :*;13 !U13 ;'J7 ;u7 !U7 i'J7 ! U7 !U7 !U7 !U1330-20-7—,———-Total Xylenes____________

107-02-8——————ACROLEIN_________________! 4$ •**• U• 1

FORM I VOA —————————— ——̂ j._, ?^_^

! 107-13-1———————ACRYLONITRILE

FORM I VOA

A8302865

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: IT PITTSBURGH__________ Contract:ITW-1C

La*. Jode: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 005


Sample wt/vol: 30.0 (g/mL) G__ Lab File ID: ________



Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 02/24/90



319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8———————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide959-98-8——————Endosulfan I_____~m60-57-1———————Dieldrin________72-55-9 ———————— 4 , 4 ' -DDE__________72-20-8———————Endrin__________33213-65-9—————Endosulfan II____72-54-8————————4 , 4 ' -DDD_________1031-07-8—————Endosulfan sulfate50-29-3 ——————— 4 , 4 ' -DDT_________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9 —————— alpha-Chlordane__5103-74-2—————gamma-Chlordane__8001-35-2—————Toxaphene_______12674-11-2————Aroclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232_____53469-21-9————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5————Aroclor-1260_____

22 !U22 !U22 |U22 !U22 1U22 1U22 !U22 iU43 !U43 iU43 iU43 iU43 iU43 !U43 iU

220 !U43 iU

220 iU220 iU430 !U220 !U220 !U220 !U220 !U220 !U430 !U430 iU


AR302866

•J.S. EPA - CLP

INORGANIC -'iM.'.-Lv'SES 3ATA SHEET

i JTW1CLab N'.-sme: ITA3_PITTSEUR8H_.._._._.„_.. Cc/ntr-.CT;: ^ I REST :'M Iij 7429-_9o-5I 7440-3S-21 7440-39-3174^0-41-7j 7440-43-91 744O-70-Si 7440-47-31 7440-48-41 744O-5O-817439-8̂ -617439-92-1! 7439-95-41 7439-96-517439-97-61 7440-05-0j 7440-09-7! 744O-22-41 7440-S3-51 7440-28-017440-62-2I 744O-66-61 5̂fti •̂ r̂'.'i lintl ̂ ^

ii Aluminumi Arsenic1 Bariumi Bervl 1 ium1 Cadmium! Ca 1 c i urni Chromium! Cobalt! Cooper1 IronILeadI Magnesium1 Manganesei Mercury(Nickel1 PotassiumISilver1 Sodium1 Thai 1 ium1 VanadiumIZinc«__11L

ssooo0 . 5365.13.60 . 5395.385 . 040 . 318.0

6330O4.4

1 1 20014900.1119.96231.8

90,50.53157156

1i !U! IM

I |i

1 U 1 NBl

1i

1 1!

1 1 SN1

! iUl

Bl EIB IBlIUI W! E11i11

1 iIP 1IF !IP 1IP !IP 1IP !IP 1IP !IP iIP !I F 1IP 1IP i! C V iIP 1IP 1IP 1IP 1IF 1IP iiP 1| |1 11 i1 1

Color Before: BROWN___ Clarity Before: _____ Texture:7" i

Color After: BROWN___ Clarity Afte>-: _____ Artifacts: YES.

Comments:ARTIFACTS: STONES ____•____ ______________..__..._

FORM I - IN7.'SB

ftR3028S7

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

i ITW2ALab Name: IT PITTSBURGH ________ Contract: _____ j

Lab Code: ITPA Case No.: 03486 SAS No.: _____ SDG No.: 025

Matrix: (soil/water) SOIL Lab Sample ID: ITW2A

Sample wt/vol: 5.1 (g/mL) G__ Lab File ID: 2010315D


% Moisture: not dec. 24 Date Analyzed: 03/15/90

Column: (pack/cap) PACK Dilution Factor: 1.00


i 74-87-3 ———74-83-9 ———75-01-4 ———75-00-3 ———"7*?— no— o— — — —67-64-1 ———75-15-0 ———75-35-4 ———75-34-3 ———540-59-0 ——67-66-3 ———107-06-2 ——

71-55-6 ———C£ t ̂ C —

108-05-4 ——75-27-4 ———*TQ_OT C___

10061-01-5-/ y \j i-"»o ""«"«"-••

J.4&4I %O K _ 1KTZ»_

108-10-1 ——S5Q1 — TQ — C—^—

127-18-4 ——79-34-5 ———

100-41-4 ——100-42-5 ——1330-20-7—J.U / U « O

——— Chlorome thane——— Bromome thane———— Vinvl Chloride——— Chloroethane——— Methvlene Chloride——— Acetone——— Carbon Disulfide——— 1 . 1-Dichloroethene——— 1 , 1-Dichloroethane——— 1,2-Dichloroethene (total) __——— Chloroform——— 1 , 2-Dichloroethane——— 2-Butanone——— 1 , 1 . l-Trichloro« thane——— Carbon Tetrachloride———— Vinvl Acetate——— Bromodichloromethane———— 1 . 2-Dichloropropane——— cis-1 . 3-Dichloroorooene———— Trichloroethene „.——— Dibromochloromethane- ——— 1 . 1 . 2-Trichloroethane5 ——— Benzene——— Trana-1 , 3-Dichloropropene———— 2-CHLOROETHYLVINYLETHER

——— 4-M«thyl-2-Pentanone

—— • — Tetrachloroethene——— 1 ,1,2, 2-Tetrachloroe thane ___——— Toluene——— Chlorobenzene———— Ethvlbenzene——— Stvrene———— Total Xvlenes

ACKVJJjBiiW

X J1313j. j

X J

61366

a. J

6666D

«O613

1 13' Co

66666664

!!U1 IT1 U1 TT1 U!UI w «f1 Ou!U!Ui Ui Ui U!UiU!Ui Ui U!Ui Ui Ui U1 TTi U!U:u:u!U!U!U!U!U!U!UIU!Ui

0004/f107-13-1——————ACRYLONITRILE______________i 64 !U !

FORM I VOA 1/87 Rev.

IE3028S9

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

jab Name: IT PITTSBURGH__________ Contract:ITW2A

Lab Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 02J5_



Level: (low/med) LOW Date Received: 03/13790

% Moisture: not dec. 24 dec. ___ Date Extracted: 03/1_5/_9J3


GPC Cleanup: (Y/N) Y_ pH: ____ Dilution Factor: 1.0


111-44-4 ——qe;_K7 a ___ _y 3 Of oK£1 T\-\ ————f •» .L t >j .L106-46-7 ——100-51-6 ——95-50-1 ———QK A o T

108-60-1 ——106-44-5 ——621-64-7 ——C7 — 7O — 1 — — —

17 O ;? Q J~7 Q _ C Q 1

Q Q_*T C_C _-I rt c £T Q

65-85-0 ———111 — Q1 —1 ———

120-82-Btffc91-20-3-**106-47-MB87-68-3-***59-50-7 ———91-57-6 ———77-47-4 ———{JO — DC — *5— — — —QK_QC_4 —————& •** ^ W *•

^ X 3 O / """" — ̂

88-74-4 ———131-11-3 ——ona QC a—£ A£ Of"\ O

———— Phenol——— bis (2-Chloroethvl) Ether———— 2-Chlorophenol——— 1 . 3-Dichlorobenzene——— 1,4-Dichlorobenzene——— Benzyl Alcohol——— 1 , 2-Dichlorobenzene—— 2-Methvlohenol

——— bis (2-Chloroisopropyl) Ether———— 4-Methvlohenol——— N-Nitroso-Di-n-Propylamine __———— Hexachloroe thane———— Nitrobenzene———— Isoohorone——— 2-Nitrochenol——— 2 . 4-Dimethvlphenol——— Benzoic Acid——— bis (2-Chloroethoxy) Me thane __——— 2 . 4-Dichlorophenolp ——— 1 . 2 , 4-Tr ichlorobenzene———— Naohthalenet ——— 4-Chloroaniline' ——— Hcxachlorobutadiene———— 4-Chloro-3-Methylphenol——— 2-Methvlnaphthalene—— - — Hexachlorocyclopentadiene ___——— 2 . 4 , 6-Trichlorophenol——— 2 , 4 , 5-Trichlorophenol

——— 2-Nitroaniline——— Dimethyl Phthalate———— Acenaphthylene———— 2 , 6-Dinitrotoluene

!i 870

O / U

0 / Uo / vo / U •o / Uo / VJo / UO / wO / VJo / Uo / Uo / Uo / Uo / Uo / wOO wo / vyo / U870870870870o / UO / U

i H7n• O / wO / VJ

4200o / U4200o / U1 "^nX J wO / U

I

!UiUi UI Ui U!U!Ui U!Ui UI Ui Ui Ui U1 U!U!Ji Ui U!U!UiU!Ui Ui U1 TTi Ui Ui Ui U!Ui U1 TI vJi UIi

FORM I SV-1 1/37 Rev.

&R3G287Q

r\vj

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________

Name: IT PITTSBURGH__________ Contract:ITW2A

Lab Code: ITPA Case No.: 034_86_ SAS No.: _..___ SDG No.: 025






GPC Cleanup: (Y/N) Y_ pH: ____ Dilution Factor: l.._g


y .7 u y

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ___

I ITW2ALab Name: IT PITTSBURGH_________ Contract: ________ !______

I Coda: ITPA Ca»« No.: 03486 SAS No.: _____ SDG No.: 025


Sample wt/vo'l: 30.0 (g/mL) G__ Lab File ID: _______


% Moisture: not dec. 25 dec. _ Date Extracted: 03/23/90




319-85-7 ———11 O_QC_fi____

58-89-9 —— —76-44-8 -----309-00-2 — —1024-57-3——959-98-8 — —60-57-1 -----72-55-9 ————

1^O1 1_£R_O__

72—54—8————"1031-07-8 ——

72-43-5 ——— -53494-70-5—5103-71-9 ——5103-74-2——8001-35-2 ——12674-11-2—11104-28-2—11141-16-5-̂53469-21-9-H12672-29-f-«11097-69-1—11096-82-5—

1

• ——— aloha-BHC• ——— beta-BHC- ——— delta-BHC

• ——— Aldrin

. —— Endosulfan I

. —— Dieldrin

. ——— 4. 4 '-DDE• ——— Endrin• —— Endosulfan II „ .,• —— 4 . 4 ' -DDD

• ——— 4 . 4 ' -DDT. ——— Methoxychlor. „„ n ,• ——— Endrin ketone..,,' ——— alpha-Chlordane _.._ , ..... —— cruuM-Chlordane— — Toxaphene• ——— Aroelor-1016q̂ -- Aroclor-1221•fc-Aroelor-1232K̂̂ JLroclor-12 4 2

—— — Aroelor-1254— —— Aroclor-1260 ...

21 |U21 |U21 IU21 IU21 |U21 |U21 IU21 IU43 IU43 iU43 IU43 IU43 IU43 !U43 IU210 IU43 IU210 IU210 IU430 IU210 IU210 !U210 IU210 IU210 IU430 IU430 IUf 1


AR3Q2872

U.S. EPA - CLP

i r- mn/Kc '.if/ we.i-;h!r) : rii'/K.C

004

CA5 No .

7420 -9G -574 40 -33 -27440-39-37440--''! 1 -77440-43-97440-70-2744O-47--3744O-48--47440-50-37439 -Ŝ -6743'? -92-17439-95-47439-96-57439-97-67440-02-07440-09-77440-22-47440-23-57440-26-07440-62-2744O-6d-6

. ~.£•&&---X.'.:'-

. «*•;,- =

1

i An. -a Ly feei!

! Alum inum] Arnenic-', Rcsriumi 3er-y .1 1 iurn1 Cadm Li.im! Ca.lc''um_,,! Chromii im!Coba.U- _„! Copper! Iron,. _____! i .ead! Magnesium! Manganese! MercuryiNickel! Potassium[Silver! Sodium! Thallium! Vanadium!Zinc• ,.„«,,„;fef̂'y**?®-

Coric;ent:r,!ib iiv>ri

1.09HO..._„.„ _ __s.a

203.....___..n.29

n . 5.?____ 15700

35.68.269.0

_ .. ... _. __ i 5 "5 on271

_________ 43403560 . S339.8

_________ .1470O,SO2450. 5343. 4397

//

C

--

RU..

B

—

UBU

,-.

O

N

M

p" __p.p.,C'V

Co .lor Before: BRQMJP^' " . :> ̂Clarity Before: _____. Texture: MfOTUr"

Color Aftert BROWN___ Clarity Afber: _____ Artifact:;: YK-?;. _

Comments:ROOTS_&_STONES_____________________________________________________.__.

FORM I - IN

IR302873

0009ft1A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET _____________iI ITW2B

Lab Name: IT PITTSBURGH__________ Contract: _________ I______


Matrix: (soil/water) SOIL Lab Sample ID: ITW2B

Sample wt/vol: 5.1 . (g/mL) G__ Lab File ID: 2Q60315D





74-87-3 ———74-83-9 ———75-01-4 ———75-00-3 ———75-09-2 ———67-64-1 ———75-15-0 ———75-35-4 ———75-34-3 ———540-59-0 ——67-66-3 ———1 n*7— nc— o— — —

71-55-6 —— -56-23-5 ———108-05-4 ——75-27-4 ———*7 O _OT_R____

10061-01-5-79-01-6 ———124-48-1 ——79-00-5*--71-43-flflp»10061-̂ H-no-79iMpf~rr_-im_fSF~_/ O— 3D— 44W1>——108-10-1 ——

1 "JT — I 9_4___

79-34-5 ———1UO OO — J— — —

100-41-4 ——100-42-5 ——1330-20-7—

——— Chlorome thane——— Bromome thane——— Vinyl Chloride——— Chloroethane——— Methylene Chloride——— Acetone——— Carbon Disulfide——— 1,1-Dichloroethene——— 1 . 1-Dichloroethane——— 1 , 2-Dichloroethene (total) __——— Chloroform——— 1 . 2-rDichloroe thane———— 2-Butanon«——— 1 . 1 , 1-Trichloroe thane——— Carbon Tetrachloride———— Vinyl Acetate——— Bromodichloromethane——— 1 . 2-Dichloroorooane——— ci»-l . 3-Dichlorooropene——— Trichloroethene——— Dibronochlorome thane

- —— Benzene- ——— Tran»-l , 3-Dichloropropene———— 2-CHLOROBTHYLVINYLETHER .• ——— Bromoform——— 4-Methyl-2-Pentanone

—— : — Tetrachloroethene——— 1 ,1,2, 2-Tetr achloroe thane ___——— Toluene——— Chlorobenzene——— Ethylbenzene——— Stvrene——— Total Xvlenes

l^«t»rtT 9TMT

11ij.1111

495

55

1JL

11

5555522511

) U1 555555554

!!U!U!U!UIB TBvJI!Ui U!UIUi UIUi U!UIU!Ui Ui UiUiUIU!U!UIU!Ui U!UIUIU1 TI1 U

IU!UIU!UIUIU!


ftR-302871*

107-13-1———————ACRYLONITRILE_______________| 54

«-.' V

FORM I VOX 1/87 Rev.

IB3G287S

0019AIB EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____________iii ITW2B

Lab Name: IT PITTSBURGH__________ Contract: _________ j_______

Lab Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 025








1 rt Q Q C O

111-44-4-AC C «7 O

541-73-1-106-46-7-100-51-6-95-50-1—QK—A O 1

i ns— fin— 1 -J . U O O U A106-44-5-621-64-7-fi*7 — TO — 1 — -QQ— QC 1 _•7 Q — RO 1 _Q Q— "7 R — C _

105-67-9-65-85-0—111-91-1-

120-82-U91-20-3-4106-47-d87-68-3«3CO C A ^

91-57-6—TT 4 T A

95-95-4—O O ^ A A88-74-4 —131-11-3-

O U O ^ V I *

- ————— Phenol- ————— bis (2-Chloroethyl) Ether• ————— 2-Chlorophenol• ————— 1 , 3-Dichlorobenzene• ————— 1 . 4-Dichlorobenzene• ————— Benzyl Alcohol• ————— 1 , 2-Dichlorobenzene. ————— 2-Methylohenol• ————— bis (2-Chloroisopropyl) Ether _• ————— 4-Methylohenol• ————— N-Nitroso-Di-n-Propylamine __• ————— Hexachloroe thane• ————— Nitrobenzene• ————— Isophorone• ————— 2-Nitrophenol• ————— 2 , 4-Dimethylphenol• ————— Benzoic Acid• ————— bis ( 2-Chloroe thoxy ) Methane __————— 2 . 4-DichlorophenolWff ——— 1 . 2 . 4-Tr ichlorobenzene•r- ——— NaphthaleneWjr ——— 4-ChloroanilineSS- ——— Hexachlorobutadiene————— 4-Chloro-3-Methylphenol————— 2-M«thylnaphthalene——— -^-Hexachlorocyclopentadiene ___————— 2 , 4 . 6-Trichlorophenol————— 2 , 4 , 5-Trichlorophenol————— 2-Chloronaphthalene————— 2-Nitroaniline————— Dimethyl Phthalate————— Acenaphthylene————— 2 , 6-Dinitrotoluene

730730730730730-7307307307307307307307307307307303600730730730730730730730730

i 73073036007303600730730

i 730!

IUIUIUIUIUIU!U!U!UIU!UIUIUIU!UIUIUIUIUIU!U!UIUIU!UIU!U!UIUIUIU!UIUi

FORM I SV-1 1/87 Rev.

AB302876

0020A1C EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

! ITW2BLab Name: IT PITTSBURGH_________ Contract: j_____





% Moisture: not dec. 10 dec. J__ Date Extracted: 03/15/90




!i yy \>;3 & — — —i Q •a_-j

PBSTICIDB ORGANICS ANALYSIS DATA SHEETBPA SAMPLIfc HCKrj A

V Jcb/f

! ITW2BLab Name: IT PITTSBURGH _________ Contract: _______ \

I Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 025




% Moisture: not dec. 10, dec. _ Date Extracted: 03/23/90


GPC Cleanup: {Y/N) Y_ pH: 5.2 Dilution Factor: 1.00


eo_oa_a_____

309-00-2 ———1 rt9̂ «.S"7 — ̂— «..

60-57-1 -----72-55-9 ————•a^oi ̂ _£R_a__/• wfll Q— •«•••1031-07-8 ——50-29-3 ——— -72-43-5 — ——53494-70-5—5103-71-9——5103-74-2——8001-35-2——12674-11-2—11104-28-2—11141-16-5—53469-21-9—12672-29-6—11097-69-1—

A T wkl* « B tJ/*

W M 4- M _ Q 13 f*

_ j^l ^m ntvs*

• ——— oamna-BHC (Lindane)• ——— Heotachlor• ——— Aldrin• —— Heotachlor eooxide• —— Endosulfan I• ——— Dieldrin

f % UUa• —— Endrin• ——— Endosulfan II _.„• ——— 4. 4 '-ODD• —— Endosulfan sulfate- ——— 4.4'-DDT• ——— Methoxvchlor• ——— Endrin ketone• ——— alpha-Chlordane. ——— aaaaa-Chlordane. ——— Toxaohene .— —— Aroclor-1016-ffer-Aroclor-1221i«fe-Aroelor-1232•̂ Xraelor-1242•»-- Aroelor-1248— - — Aroclor-1254

11096-82-5 ————— Aroelor-1260

18181818181818183636363636363618036180180360180180180180180360360i

! !!U !!U !fU t!U !!U 1IU !!l>' !!U!U!U!U!U!UiU!UIU!UiU!U!U!UIU!U!U!U!UIU1 1

FORM I PEST 1/87 Rev

IR302878

U.-5. EPA - CLP 005

1 --PA t-.ArVi :'- MI i.INORGANIC ANAI Y'>£'̂ HA PA OHf-;r;; r

II

! ITW2BiNl.ini'-r: r. fAS ..PITTSBURGH ___ ______ i. >..,.;.,;. K. !•; : K LRF'j I'l'iN!-:. _ ; _

, jj-i I'.iiijr-. I fPA __ _Case No. : i i>^/i .?•(••. SA'.'. \i.~i . : _ ;':.(>C, Mo. r Ov?.

-i^l:,-- i «•, i" •-.'•' L j /w.-^vrr) : SOLI, . i ...

eve., f i. '•'.•; /med ) : I ("'UI___ Onte Reef* I v--c< : '"r ."'./,

Cor ic'?-rihrn 1. 1 on Unit.'-, (uo/l or ins/ko dr-y w^i-jht-j- MG/

11

CA'3 Mo. i Anr-a 1. yt:e

74>i9-9Q -5 ! A Li.un I m.iin._7a/iO • 33-2 ! Arsen ic744H -J9-3 !BarNi.urn74 40-- 41 -7 I Beryllium744H -'i-3- -^ ! Cadmium7440-7O- 2 iCalciLim7440-47-. 5 ! Chromium7440--4P, -/i iCoba.lt7440-50-8 iCopoer-7439--PO-6 ! Iron7439-92-1 iLead74o\'-95-4 ! Magnesium7439-96-5 ! Manganese7439-97-6 1 Mercury7440-G2-0 ! Nickel7440-09-7 ! Potassium744O--22-4 ! Silver7440-23-5 ! Sodium7440-28-0 ! Thallium7440-62-2 ! Vanadium744O-66-6 SZinc

ii ,i

- . .I--.--:

«fe—— }

Concent;r;-it: Ion

._. _______ 21.9Q1 . .14. 5

0.2213.337. 74. 70 . 4 37.324902.466. 46. 3

0.11O.3662.70,6547. 30.443.94.7

/

o

."3U

8

U

8

UBUBUB

Q

W

**

N*

E*NN*E

3E*

M

f'_FPPPPPPPPFPPCVPPPPFPP

Color Before: BROfc&tK- -.''.:' Clarity Before:, .__£,

0011,41A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET _____________I! ITW2C

Lab Name: IT PITTSBURGH_________ Contract: ________ j______


Matrix: (soil/water) SOIL Lab Sample ID: ITW2C




Column: (pack/cap) PACK Dilution Factor: l.Q_____


74-83-9 ——75-01-4 ——75-00-3 ——75-09-2 ——67-64-1 ——75-15-0 ——75-35-4 ——75-34-3 ——540-59-0—67-66-3 ——

•71 KB C.

56-23-5 ——108-05-4—75-27-4 ——/ O O / 3

10061-01-579-01-6 ——

79-00-5̂ 3171-43-2JB10061-OM110-75-V

108-10-1—cai *ro_e127-18-4—79-34-5 ——AwO OO J

100-41-4—100-42-5—1330-20-7-107-02-8—

———— Chlorome thane———— Bromome thane———— Vinyl Chloride———— Chloroe thane———— Methvlene Chloride———— Acetone———— Carbon Disulfide———— 1 . 1-Dichloroethene———— 1 . 1-Dichloroe thane———— 1 , 2-Dichloroethene ( total ) __———— Chloroform———— 1 . 2-Dichloroethane———— 2-Butanone———— 1 , 1 . 1-Trichloroe thane———— Carbon Tetrachloride———— Vinvl Acetate———— Bromodichlorome thane———— 1 . 2-Dichloroprooane———— cis-1 . 3-DichloroDrooene .———— Trichloroethene- ——— Dibromochloromethane— — —— 1 . 1 . 2-Tr ichloroethaneA*. —— Benzenei£ ——— Tran»-l , 3-Dichloropropene ___*- ——— 2-CHLOROETHYLVINYLETHER- ——— Bromoform————— 4-M«thyl-2-Pentanone

—— " — Tetrachloroethene———— 1 ,1,2, 2-Tetrachloroethane ___———— Toluene———— Chlorobenzene———— Ethylbenzene „., „-. ——— Stvrene———— Total Xvlenes————— ACROLEIN

12J.4»

X*

1*

«u66

Ltt

126

6666

. 246121 5

i 12CO66666660

! !!U |IU!U !!U !IB *t 1BJ I! !!U I!Ui Ui Ui U!U!J!UIUi UIUiU!U!U!U!U!U!U!U!UIUIU!UIU!UIUIUIUIU1 Tt1 U

1


SB30288Q

107-13-1———————ACRYLONITRILE______________! 60 !U


ft830288l

0021/jIB EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________

Lab Name: IT PITTSBURGH_________ Contract:ITW2C


Matrix: (soil/water) SOIL Lab Sample ID: ITW2C_







! 108-95-2——————Phenol______________! 111-44-4——————bis (2-Chloroethyl) EtherI 95-57-8———————2-Chlorophenol_______~541-73-1——————1, 3-Dichlorobenzene.106-46-7——————1, 4-Dichlorobenzene

I iQO-51-6——————Benzyl Alcohol.95-50-1———————1, 2-Dichlorobenzene________95-48-7———————2-Methylphenol____________108-60-1——————bis (2-Chloroisopropyl)Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1———————Isophorone_______________88-7 5-5———————2-Ni trophenol_____________105-67-9——————2,4-Dimethylphenol________65-85-0———————Benzoic Acid______________111-91-1——————bia(2-Chloroethoxy) Me thane__120-83-2——————2,4-Dichlorophenol_________120-82-lJJi^———1,2,4-Trichlorobenzene_____

•———Naphtha 1 ene.106-47-^gJp*———4-Chloroaniline________87-68-3—;—————Hexachlorobutadiene_____59-50-7———————4-Chloro-3-Methylphenol91-57-6———————2-Methylnaphthalene_____77-47-4—————-—Hexachlorocyclopentadiene.88-06-2———————2,4,6-Trichlorophenol___95-95-4———————2,4,5-Trichlorophenol91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Nitroaniline_________

I 131-11-3——————Dimethyl Phthalate.i 208-96-8——————Acenaphthylene___I 606-20-2——————2,6-Dinitrotoluene

800 1U800 IU800 IU800 !U800' |U800 |U800 |U800 iU800 |U800 |U800 |U800 iU800 IU800 |U800 |U800 |U3900 iU800 |U800 |U800 iU800 |U800 iU800 |U800 IU800 !U800 IU800 IU3900 IU800 IU3900 IU800 IU800 |U800 |U

FORM I SV-1 1/87 Rev,

AR302882

1C EPA SAMPSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___

! ITW2CLab Name: IT PITTSBURGH_______ Contract: !









!i a i — "}o_ o__ — — —1 C1 O O C

! 100-02-7 ———! 132-64-9 ———i 121-14-2 ———1 O A C.C. O

! 7005-72-3 ——

i 100-01-6 ———! 534-52-1 ———j 86-30-6 ————! 101-55-3 ———! 118-74-1 ———1 O T — O C R «

! 85-01-8 ————1 1 1 A •! *> *7

| O* / % 4

\ 206-44-0 ——— •', 129-00-0|M-1 85-68-7-jBp-! 91-94-l-«p-1 " f g" ^ Ĵ T̂! SO DO — J " "•""

! 117-81-7 ——— •1 117-84-0 ——— •1 A w w 77 &\ O/IT — rt Q _Q — ___.

! 50-32-8 ———— •! 193-39-5— — •| .b & W «J J W\ 53-70-3 ————i i n

PESTICIDE ORGANICS ANALYSIS DATA SHEETBPA SAMPLEO@P7/1

" {"

I ITW2CLab Naae: IT PITTSBURGH _________ Contract: I

L Cod«: ITPA Case No. : 03486 SAS No. : ______ SDG No. : 025



Level: (low/raed) LOW Date Received: 03/13/90

% Moisture: not dec. 17. dec. _ Date Extracted: 03/23/90




319-84-6 —— -11 o_a £_•?..___319-86-8 —— -

76-44-8 ——— -309-00-2 —— -1024-57-3——959-98-8 —— -60-57-1 ——— -72-55-9 ——— -72-20-8 ——— -^131 ?_CC.O«>

/ m 94 O

1031-07-8——50-29-3 ——— -72-43-5 ——— -53494-70-5—5103-71-9——5103-74-2——8001-35-2——12674-11-2—11104-2S-2—11141-16-5—53469-21-9-112672-29-6—

- ——— alpha-BHC• ——— beta-BHC. ——— delta-BHC• ——— aaasta-BHC (Lindane)• ——— Heotachlor „ ,„.,• ——— Aldrin——— Heotachlor eooxide. —— Endosulfan I. ——— Dieldrin• ——— 4. 4 '-DDE

- ——— Endosulfan II. ——— 4 . 4 • -DDD

• ——— 4.4'-DDT• ——— Methoxychlor _ _ ..,- ——— Bndrin ketone,,, _.,.., ,,,. ——— aloha-Chlordane— — -gaaM-Chlordane., ——— Toxaphene ,._ „—— "Aroelor-lOie.... ....„,., .,..,.«lB

CLP 006I ~>>.A '"AiT; " ''••' •. "™

INORGANIC ANAI.Y'-FV OA f A "•••••:'.'• V _ '

: ITWICi\i."*m~ : L TAG .PITTSBURGH.______.„_.._ C- . s , ! , - . , , \. • : l r'JiT, 1'ONH ,

: . !b iVu-i--; i ;..-~A. . CaVv: .l&'&* !

(;onr,.-fi-i1:r.st ion i C

6920 !3.51

46 . 7 ! R_..___. ___ a, =.a IB..._,......,__ Q.431U

1 56 ! B____ . __ _17. 71 _

16.3!23 . 2 I20600 !8.2!311 !R.501 !

n . 1 1 ! uS.9IB52218

0. 72 !U41. SIR0.47! U41. 3!.31.3!

1 1 . i n I , M •i

/ .... _..___ / i

Q

_______

**

N*

3E*NN*E

UEA

n

pFo

p_.ppp _pppC.T

PPcvppPpFPP

„ ...... '

Color Before: BROSajfe'" A-; "*•-.; -.:• Clarity Before: ____ Texture: f i iAH":-c_«n«̂ 5«-» -.,_*» ——————" "?*••

"oLor After: GR'AY " Clarity After: _____ Artifacts: YL''3

Comments:STONES___________________________

FORM I - IN

ftR30288S

1A ' EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

ITW3Aab Name: IT PITTSBURGH _________ Contract: ________

Lab Code : ITPA Case No . : 03486 SAS No . : _____ SDG No . : 010


Sample wt/vol: 4.9 (g/mL) G__ Lab File ID: 2020226N





-I 74-87-3———————Chloromethane74-83-9——.————Broroomethane__;_________ i75-01-4'——————Vinyl Chloride___________S75-00-3———————Chloroe thane_____________I75-09-2———————Methylene Chloride________i67-64-1———————Acetone_________________!75-15-0———————Carbon Disulfide__________!75-35-4———————1,1-Dichloroethene________!75-34-3———————1,1-Dichloroethane_________I540-59-0——————1,2-Dichloroethene (total)__I67-66-3———————Chloroform_______________!107-06-2 —————— 1 , 2-Dichloroethane ________ i78-93-3 ——————— 2-Butanone _______________ i71-55-6 ——————— 1 , 1 , 1-Trichloroethane ______ !56-23-5 —————— Carbon Tetrachloride ______ I108-05-4 —————— Vinyl Acetate _____________ i75-27-4 ——————— Bromodichloromethane _______ !78-87-5 ——————— 1 , 2-Dichloropropane ________ !10061-01-5 ———— cis-1 , 3-Dichloropropene ____ I79-01-6 ——————— Trichloroethene ___________ i124-48-1 —————— Dibromochlorome thane _______ !79-00-5 ——————— 1 , 1 , 2-Trichloroethane ______ i71-43-2-—?- ————— Benzene _________________ i

Trans-1 , 3-Dichloropropene ___ i110-75-8**; ————— 2-CHLOROETHYLVINYLETHER _____ i75-25-2 ——————— Bromoform ________________ i108-10-1 —————— 4-M« thy 1-2- Pent anone _______ I591-78-6 —————— 2-Hexanone ______________ !

! 127-18-4——————Tetrachloroethene_________!i 79-34-5——————1,1,2,2-Tetrachloroethane___!! 108-88-3——————Toluene__________________II 108-90-7——————Chlorobenzene_____________!I 100-41-4—————Ethylbenzene____________!I 100-42-5——————Styrene_________________!! 1330-20-7—-———Total Xylenes_____________II 107-02-8———————ACROLEIN__________________II___________________________________!___

FORM I VOXAB302886

! 107-13-1——————ACRYLONITRILB

FORM I VOX 1/87 RevftR3Q2887

00 4AIB EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______

i.ab Name: IT PITTSBURGH__________ Contract:ITW-3A


Matrix: (soil/water) SOIL Lab Sample ID: ITW-3A







i i108-95-2——————Phenol____________________i 850 1U111-44-4——————bis (2-Chloroethyl) Ether_____I 850 !U95-57-8———————2-Chlorophenol____________! 850 !U541-73-1——————1,3-Dichlorobenzene________! 850 !U106-46-7——————1,4-Dichlorobenzene________! 850 !U100-51-6——————Benzyl Alcohol____________! 850 !U95-50-1———————1,2-Dichlorobenzene________! 850 !U

850 !U850 !U850 !U850 !U850 !U850 !U850 !U850 !U850 !U660 !J850 1U850 !U850 !U850 !U850 1U850 1U850 !U850 !U850 !U850 !U

4100 !U850 !U

4100 !U850 !U850 !U850 !U

95-48-7———————2-Methylphenol___________108-60-1——————bis (2-Chloroisopropyl) Ether.106-44-5——————4-Methylphenol__________\621-64-7——————N-Nitroso-Di-n-Propylamine_67-72-1———————Hexachloroethane_________98-95-3———————Nitrobenzene____________78-59-1———————Isophorone______________88-75-5———————2-Nitrophenol___________105-67-9——————2,4-Dimethylphenol_______65-85-0———————Benzoic Acid____________111-91-1——————bis (2-Chloroethoxy) Methane_120-83-2——————2, 4-Dichlorophenol________120-82-lr—————1 • 2,4-Trichlorobenzene____91-20-3———————Naphthalene_____________106-47-a-—————4-Chloroaniline__________87-68-3———————Hexachlorobutadiene______59-50-7———————4-Chloro-3-Methylphenol___91-57-6———————2-Methylnaphthalene______77-47-4——————Hexachlorocyclopentadiene_88-06-2———————2,4,6-Trichlorophenol_____95-95-4———————2,4,5-Trichlorophenol_____91-58-7———————2-Chloronaphthalene______88-74-4———————2-Nitroaniline___________131-11-3——————Dimethyl Phthalate.208-96-8——————Acenaphthylene-___606-20-2——————2,6-Dinitrotoluene

FORM I SV-1 1/87 Rev,88302888

1C EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________

Lab Name: IT PITTSBURGH _______ Contract:ITW-3A

Lab Code: ITPA Case No.: 03486 SAS No.: _____ SDG No.: 02l_

Matrix: (soil/water) SOIL Lab Sample ID: ITW-3A

Sample wt/vol: 30.1 (g/mL) G___ Lab File ID: 5030327D






99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene___________51-28-5———————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran____________121-14-2——————2 , 4-Dinitrotoluene_______84-66-2———————Diethylphthalate________7005-72-3——————4-Chlorophenyl-phenylather.86-73-7——————Fluorene ___________]100-01-6——————4-Nitroaniline_________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6———————N-Nitrosodiphenylamine (1).101-55-3——————4-Bromophenyl-phenylether__118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene____________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluor anthene____________129-00-0——————Pyrene________________85-68-7——•————Butylbenzylphthalate_____91-94-1——-———3,3' -Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene_______________117-81-7——————bis(2-Ethylhexyl)Phthalate.117-84-0——————Di-n-Octyl Phthalate_____205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo (k) Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5——————Indeno(1,2, 3-cd) Pyrene___53-70-3———————Dibenz (a, h) Anthracene____191-24-2——————Benzo (g,h,i) Pe-rylene_____

4100 |U850 |U

4100 |U4100 |U850 |U850 !U850 !U850 IU850 !U

4100 !U4100 !U850 IU850 |U850 1U280 !BJ850 !U850 |U850 !U850 |U850 IU850 !U

1700 !U850 iU850 1U200 ! J850 !U850 iU850 |U850 |U850 |U850 |U850 |U

(1) - Cannot be separated from Diphenylamine

FORM i sv-2 &R3028891/87 Rev

ID EPA SAMPLEPESTICIDE ORGANICS ANALYSIS DATA SHEET _______

Lab Name: IT PITTSBURGH__________ • Contract:ITW3A

Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 010








319-84-6——————alpha-BHC_________319-85-7——————beta-BHC_________319-86-8——————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9———————4 , 4 ' -DDE_________72-20-8———————Endrin__________33213-65-9————Endosulfan II_____72-54-8 ——————— 4 , 4 ' -DDD_________1031-07-8—————Endosulfan sulfate50-29-3 ——————— 4, 4 ' -DOT_________72-43-5——————M«thoxychlor__53494-70-5————Endrin katone__5103-71-9—————alph«-Chlordane.5103-74-2—————gamma-Chlordane.8001-35-2—————Toxaphene_____12674-11-2————Aroclor-1016__11104-28-2—,——Aroclor-1221__11141-16-5————Aroclor-1232__53469-21-9—————Aroclor-1242__12672-29-6————Aroclor-1248__11097-69-1————Aroclor-1254__11096-82-5————Aroclor-1260__

s1

20 !U20 !U20 !U20 |U :!20 !U20 |U20 !U20 !U39 iU39 !U39 !U39 IU39 !U39 !U39 iU

200 !U39 IU200 !U200 |U390 !U200 !U200 !U200 iU200 !U200. IU390 !U390 !U


SR30289G

U.S. ERA - CLP

INCRE6NIC ANAL'-'PES DATA SHEE""

Lab M..vr.-= T TASi_PITTSBURGH_...__._....„..., Contract; i __ _.__..._. __ .

Lab Cod3- i!r~'A .... _ ._-.Ca.

ooogfr1A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET ____

! ITW3Buab Name: IT PITTSBURGH__________ Contract: _____ i______

Lab Code:, ITPA Case No.: 03486 SAS No.: ______ SDG No.: 010


Sample wt/vol: 5.1 (g/mL) G__ Lab File ID: 2Q10227D





74-87-3———————Chlorome thane__________74-83-9———————Bromome thane___________75-01-4———————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroe thane______540-59-0——————1, 2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroe thane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroe thane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane^,_____10061-01-5————cia-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——————Dibromochlorome thane____79-00-5-——————1,1,2-Trichloroethane____71-43-2--—————Benzene_______________10061-02-6-————Trmna-1,3-Dichloropropene110-75-8———————2-CHLOROETHYLVINYLETHER__7 5-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroe thane.108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——r———Styrene1330-20-7—————Total Xylenes

I 107-02-8———————ACROLEIN____

12 |U12 IU12 IU12 |U6 IB6 IBJ6 IU6 |U6 IU6 iU6 iU6 |U

10 IJ6 IU6 IU

12 iU6 IU6 !U6 !U6 |U6 IU6 1U6 IU6 |U

!U6 IU

12 IU12 |U6 IU6 IU6 IU3 IJ2 IJ6 IU8

!U

FORM I VOX 1/87 RevSR3Q2892

ooioA107-13-1——————ACRYLONITRILE______________! £o -** !U

FORM I VOA 1/87 RevHH302893

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______ ^j,

! ITW3B !Lab Name: IT PITTSBURGH ____ Contract: _____ ! . !

L Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 010






GPC Cleanup: (Y/N) N_ pH: 6.0 Dilution Factor: 1.00


319-84-6——————alpha-BHC_________319-85-7——————beta-BHC_________319-86-8——————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide959-98-8——————Endosulfan I_____60-57-1———————Disldrin________72-55-9———————4 , 4 ' -DDE_________72-20-8——————Endrin_________33213-65-9————Endosulfan II____72-54-8 ———————— 4 , 4 ' -ODD_________1031-07-8—————Endosulfan sulfate50-29-3————————4 , 4 ' -DDT_________|72-43-5———————M«thoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————alph*-Chlordane__5103-74-2—————ganuna-Chlordan*__8001-35-2——-——Tox*ph«ne_______12674-11-2————Aroclor-1016_____11104-28-2—————Aroclor-1221_____11141-16-5————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6————Aroclor-1248_____11097-69-1————Aroclor-1254____11096-82-5————Aroclor-1260_____

9.6IU9.6!U9.6IU9.61U9.6!U9.6!U9.6!U9.6!U

19 iU19 !U19 !U19 !U19 !U19 !U19 !U96 iU19 !U96 !U96 !U190 !U96 !U96 !U96 !U96 !U96 !U190 !U190 !U

FORM I PEST 1/87 Rev.

AR30289**

0005U.S. EPA - :;L;~

INGR3A ̂ n --M^_Y3ES D^TA SHEETi

1b Narp^; :TAS_P ITTSBl!RGH__._.__. _ ...._... -c .- 1~ -r r- , F '• 1'̂ r J|-iE .. : ... _ _ .

Lab 7, c c:--,; TT--a__. Cssa Nc . ; O.V'---~

oouA1A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET _____________I! ITW3C

Name: IT PITTSBURGH__________ Contract: _________ !_______

Lab Code: ITPA__ Case No.: 03486 SAS No.: ______ SDG No.: 010





Column: (pack/cap) PACK Dilution Factor: 1.0_____


74-87-3 ——————— Chloromethane __________74-83-9 ——————— Bromome thane ___________75-01-4 ——————— Vinyl Chloride __________75-00-3 ——————— Chloroe thane ___________75-09-2 ——————— Methylene Chloride ______67-64-1 ——————— Acetone _______________75-15-0 ——————— Carbon Disulfide ________75-35-4 ——————— 1 , 1-Dichloroethene ______75-34-3 ——————— 1 , 1-Dichloroethane ______540-59-0 —————— 1 , 2-Dichloroethene ( total )67-66-3 ——————— Chloroform _____________107-06-2 —————— 1 , 2-Dichloroethane ______78-93-3 ——————— 2-Butanone _____________71-55-6 ——————— 1 , 1 , 1-Trichloroethane ____56-23-5 ——————— Carbon Tetrachloride _____108-05-4 —————— Vinyl Acetate __________75-27-4 ——————— Bromodichloromethane _____78-87-5 ——————— 1 , 2-Dichloropropane _____10061-01-5 ———— cis-1 , 3-Dichloropropene __79-01-6 —————— Trichloroethene ________124-48-1 —————— Dibromochlorome thane ____79-00-5—— ———— 1 , 1 , 2-Trichloroe thane ___71-43-2-- • ————— Benzene ______________10061-02-6- ———— Trans-1 , 3-Dichloropropene110-75-8 ——————— 2-CHLOROETHYLVINYLETHER __75-25-2 ——————— Bromoform108-10-1 —————— 4-Methyl-2-Pentanone591-78-6 —————— 2-Hexanone127-18-4 —————— Tetrachloroethene79-34-5 ——————— 1 ,1,2, 2-Tetrachloroethane108-88-3 —————— Toluene108-90-7 —————— Chlorobenzene100-41-4 —————— Ethylbenzene100-42-5 —————— Styrene1330-20-7— ——— Total Xylenes107-02-8 ——————— ACROLEIN

13 IU13 1U13 IU13 IU !5 !BJ7 iBJ:6 !U6 !U6 iU6 iU6 !U6 IU11 ! J6 !U6 IU

13 IU6 IU6 IU6 IU6 IU6 IU6 !U6 IU6 iU

!U|U|UIUIUIUIU

FORM I VOA&H3Q2896

! 107-13-1———————ACRYLONITRILE.


$8302897

ID EPA SAMPLPESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: IT PITTSBURGH__________ Contract:ITW3C



Sample wt/vol: 30.1 (g/ir.L) G__ Lab File ID: _________


% Moisture: not dec. 24 dec. _ Date Extracted: 03/03/90




319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8——————delta-BHC_________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9———————4, 4 ' -DDE_________72-20-8———————Endrin__________33213-65-9————Endosulfan II_____72-54-8 ——————— 4 , 4 ' -ODD_________1031-07-8—————Endosulfan sulfata50-29-3———————4, 4 ' -DOT_________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————alpha-Chlordanc___5103-74-2—————gamma-Chlordane___8001-35-2—————Toxaph«ne________12674-11-2————Aroclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5————Xroclor-1232_____53469-21-9————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5————Aroclor-1260_______

21 !U21 1U21 !U21 |U21 !U21 !U21 !U21 !U42 !U42 !U42 !U42 !U42 !U42 !U42 !U210 !U42 iU210 !U210 iU420 !U210 iU210 !U210 !U210 iU210 !U420 !U420 !U


HR302898

0006'J-3. EPA - C:.,P

i £P£ BA:1F"_E ••-••:•..INORGANIC ANALYSES DA "A SHEET

[

i ITW3CL-?H i'i-.T.-?? TTAS_PITTSBURGH.

s1. i as: _.£ 1

Cor.-~s*itv •- 1 ion Ur:.ts 'ug/L. or T-'j/vg

!

i CA3 Wo .1; 7^59— =?o-3i7:...40-?S--21 74 -'+0-3 9 -317,440-^-1-7I 7440-43-9i7/,.̂ 0--70-e1 7

1A EPA SAMPLE/ NO .VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: IT PITTSBURGH__________ Contract:ITW4A1

Lab Code: ITPA Case No.: 034.86.. SAS No.: _____ SDG No.: 002

Matrix: (soil/water) SOIL Lab Sample ID: ITW4A1

Sample wt/vol: ,._.i«J. (g/mL) G.. Lab File ID: 20.50221D

Level: (low/med) LOW Date Received: 02/15/90.

% Moisture: not dec. _2_2 Date Analyzed: 02/21/90

Column: (pack/cap) PACK Dilution Factor: 1̂ 00


74-87-3———————Chloromethane__________74-83-9———————Bromome thane____________75-01-4———————Vinyl Chloride__________75-00-3———————Chloroe thane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3 ——————— 1,1-Dichloroethane_______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform_____________107-06-2——————1, 2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————Trans-1,3-Dichloropropene_110-75-8———————2-CHLOROETHYLVINYLETHER__75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone_______591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene___________________108-90-7——————Chlorobenzene_______________100-41-4——————Ethylbenzene__________100-42-5——————Styrene_______________________1330-20-7—————Total Xylenes__________107-02-8———————ACROLEIN_____________

13 !13 iU13 IU13 IU6 IBJ

14 I7 |U7 !U7 |U7 IU2 IJ7 IU

13 IU77 |U

13 IU7 |U7 IU7 IU7 |U7 IU7 IU7 |U7 |U

IU7 IU

13 IU13 !U7 IU7 IU1 IJ1 IJ7 IU7 |U3 IBJ

IUi.1FORM I VGA 1/87 Rev.

AR302900

0000 ••' f\107-13-1———————ACRYLONITRILE_______________! feS -t*- ,'U ! ̂ x '


flR30290!

PESTICIDE ORGANICS ANALYSIS DATA SHEET ______________

ITW4AlOOQl5ALab Name: IT PITTSBURGH_________ Contract:

->b Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 002

heitrix: (soil/water) SOIL Lab Sample ID: Q00207001

Sample wt/yol: 30.1 (g/mL) G__ Lab File ID: ________






319-84-6——————alpha-BHC________319-85-7———————beta-BHC__________319-86-8——————delta-BHC________58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxid«_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9———————4 , 4 ' -DDE_________72-20-8———————Endrin__________33213-65-9————Endosulfan II____72-54-8 ——————— 4 , 4 ' -ODD_________1031-07-8—————Endosulfan sulfate50-29-3 ——————— 4, 4 ' -DDT_________I72-43-5———————Methoxychlor_____53494-70-5————Endrin k«ton«____5103-71-9—————alpha-Chlordan«___5103-74-2—————gamma-Chlordane___8001-35-2—————Toxaphene________12674-11-2————Aroclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232_____53469-21-9————Aroclor-1242_____12672-29-6————Aroclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5————Aroclor-1260_____

20 !U20 !U20 !U20 iU20 !U20 !U20 !U20 !U39 !U39 !U39 !U39 iU39 !U39 !U39 !U200 !U39 !U

200 !U200 !U390 !U200 !U200 iU200 !U200 iU200 !U390 !U390 !U

FORM I PEST 1/87 R

SR302902

6000'1U.S. EFA - CLP1 EFA SAMPLE NG,

INORGANIC ANALYSES DATA SHEET ____„___..__.„.._i! ITW4A1

Lab Na.-r.e: ITAS_PITTSBUR.GH____.____._„ Co r>t ;-. Uf CT. i U

! Copperi Iron(LeadIMaanesiumf Manganese! Mercury(Nickel! Potassiumi S i 1 ver1 Sod ium1 Thai 1 iumi Vanadium.tZincr~Jr1

/L or mg/-.:g dry

i i! Co ncentrat i on i Ci !1 3430 !! _ 0 . 74 i B!.._. _ ... __ . E4.7JB1 0 . 69 1 E!_.._.. ___ _ 0.50 IDi 764 i 3I 13.3!! 3.4'Bi 21.01

1330011 25.911 380 ! 3! 150!1 0.12IU1 4. SIBi aeiiBi 0 . 74 1 U! 43.7! B1 0 . £5 1 U1 18.51I 53.1)!- -r !i_ 2. i-1 ' 1

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Color Before: 'BROWN___ Clarity Before: _____ Texture: MEDIUM

Color After: BROWN___ Clarity After: _____ Artifacts: YES._...

Comments:ARTIFACTS:_GRASS, ..STONES___________________________________________

FORM I - IN«•? •/ •

HR302903

00009A1A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET ______________I1

! ITW-4A2Lab Name: IT PITTSBURGH__________ Contract: _________ !______


Matrix: (soil/water) SOIL Lab Sample ID: ITW-4A2

Sample wt/vol: 4.9 (g/mL) G_._ Lab File ID: 2060220D


% Moisture: not dec. 19 Date Analyzed: P_2/.2Q/90_



74-87-3———————Chlorome thane.74-83-9———————Bromome thane75-01-4———————Vinyl Chloride__________75-00-3———————Chloroe thane___________75-09-2———————Methylene Chloride67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1, 2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroe thane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichlorome thane____78-87-5———————1, 2-Dichloropropane______10061-01-5————cis-1,3-Dichloropropene__79-01-6-——————Trichloroethene_________124-48-1——————Dibromochlororaethane____79-00-5——————1,1,2-Trichloroethane___71-43-2-——————Benzene______________10061-02-6————Trans-1,3-Dichloropropene_110-75-8———————2-CHLOROETHYLVINYLETHER__75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2, 2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8———————ACROLEIN________________

13 |U13 |U13 !U13 !U5 !BJ

13 ',U6 !U6 iU6 |U6 !U6 !U6 !U

13 !U6 !U6 iU

13 iU6 |U6 !U6 !U6 IU6 SU6 |U6 |U6 !U

!U6 1U

13 !U13 !U6 !U6 !U6 !U6 iU6 iU6 !U6 !U

!U

MS

FORM I VOA 1/87 Rev

AR3Q29QI*

OOOIO/'107-13-1———————ACRYLONITRILE_______________i fi -t* !U !

FORM I VOA . 1/87 Rev,

PESTICIDE ORGANICS ANALYSIS DATA SHEET ________

_,...... oooLab Name: IT PITTSBURGH__________ Contract:

*> Code: ITPA Case No.: 03486 SAS No.: ______ SDG No.: 002








319-84-6——————alpha-BHC________319-85-7———————beta-BHC__________319-86-8——————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______[309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9———————4, 4 ' -DDE_________72-20-8———————Endrin__________33213-65-9————Endosulfan II_____72-54-8————————4 , 4 ' -ODD__________1031-07-8—————Endosulfan sulfate_50-29-3———————4, 4 ' -DDT_________72-43-5———————Methoxychlor_____53494-70-5————Endrin keton«____5103-71-9—————alpha-Chlordan«___5103-74-2—————gamma-Chlordane___8001-3 5-2 —————Toxaphene________12674rll-2————Aroclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232_____53469-21-9————Aroclor-1242_____12672-29-6————Aroclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5————Aroclor-1260_____

19 !U19 !U19 JU19 |U19 !U19 |U19 !U19 !U38 !U38 !U38 !U38 iU38 !U38 !U38 !U

190 !U38 |U190 !U190 !U380 !U190 !U190 !U190 !U190 !U190 !U380 !U380 !U

FORM I PEST 1/87 Re

AR3G2906

00005U.S. ERA - CLP

1 EPA 3£-1?L=: ! 50IL_ Lab Sample I'3« l"~U'4 A ?

Lavel < low/med 5 ; L3W _ Oste Received-, vS/ 15 •

% Solids: _34.9

Concentration (Jni:s (ug/L or rug /kg dry weight;? :-1'3/KG

I iIDAS No. 11 !1 7429-90-5 1I744O--33--E i! 744O-39-3 !! 7440-4 1-7 • I| 7440-43-9 11 7440-70-2 i17440-47-3 i; 7440-43-4 1i 7440-50-3 11 7439-89-6 117439-92-1 i'7439-95-4 117439-96-5 117439-97-6 117440-02-0 11 7440-09-7 117440-22-4 117440-23-5 1i 7440-28-0 i!74'4O-62-2 11 7440-66-6̂ 11 --r̂ ' ""'"It| •JJS*-̂ . .̂ *tI '•-;•'/• • :. ; J?1 Jj-££«_ f

Analyse Ii

Aluminum !Arsenic: !Barium 1Bervl 11 urn •'Cadmium 1Calcium 1Chromium !Cobalt !Copoer 1Iron !Lead iMagnesium iManganese 1Mercurv iNickel iPotassium!Silver 1Sodium iThallium 1Vanadium 1Zinc 1S&ir 1

1r-; ii

i !C o P. c e n t r a t i o n 1 C 1

4300 1 11.41 B 1

S3 . E I B !0 . 63 1 B iO . 47 i U !522 IB!16.81 :5.5IB!15, 6 i !

23000 ! !29.1! 1299 I B 1161 1 1

O . 1 1 1 U I5 . 2 i B 1291 !Bi0 . 7 1 1 U 140 . 5 1 B 10 . 23 1 U 121.31 142 . 3 1 1

.... __ . _ „ _l 1r i '' ! 1

1 1

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i iIM 1

IP 1IF 1IP iIP i!P i1 P !1 P 1IP 1IP 1! P !1 F !; P !1 P iiCVIIP 1IP iIP 11 P iIF \i P !IP !1 1i 1• 11 1

Color Before:

Color After:

Comments :ARTIFACTS:

fc . .w

3ROWN Clarity Before: Texture: HI

BROWN ___ Clarity After: _____ Artifacts': Yi

GRASS, STONES ' _ _ _ _ _ _ _ „ _ .

HEDILM

FORM I •- IN

006/4IB EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________.

Lab Name: IT PITTSBURGH__________ Contract:ITW-4A

Lab Code: ITPA Case No.: 03486 SAS No.: ___._ SDG No.: 021__

Matrix: (soil/water) SOIL_ Lab Sample ID: ITW-4A

Sample wt/vol: 30._! (g/mL) G_ _ Lab File ID: 5_p_6Q.3_28ID _ _

Level: (low/med) LOW Date Received: 03/07290

% Moisture: not dec. 13 dec. ___ Date Extracted: 03/15_/_iQ


GPC Cleanup: (Y/N) Y_ pH: _____ Dilution Factor: 1.0_,_.


108-95-2 —————— Phenol_______________111-44-4——————bis (2-Chloroethyl) Ether___95-57-8———————2-Chlorophenol___________541-73-1——————1, 3-Dichlorobenzene______106-46-7——————1, 4-Dichlorobenzene______100-51-6——————Benzyl Alcohol___________95-50-1———————1, 2-Dichlorobenzene_______95-48-7———————2-Methylphenol___________108-60-1——————bis (2-Chloroisopropyl) Ether.106-44-5——————4-Methylphenol________•621-64-7——————N-Nitroso-Di-n-Propylamine_67-72-1———————Hexachloroethane_________98-95-3———————Nitrobenzene____________78-59-1———————Isophorone______________88-75-5———————2-Nitrophenol____________105-67-9——————2,4-Dimethylphenol_______65-85-0———————Benzole Acid_____________111-91-1——————bis(2-Chloroethoxy)Methane_120-83-2——————2, 4-Dichlorophenol________120-82-1=——————1, 2, 4-Trichlorobenzene____91-20-3———————Naphthalene_____________106-47-8——————4-Chloroaniline__________87-68-3———————Hexachlorobutadiene_______59-50-7———————4-Chloro-3-Methylphenol___91-57-6———————2-Methylnaphthalene_______77-47-4———————Hexachlorocyclopentadiene__88-06-2———————2 , 4 , 6-Trichlorophenol_____95-95-4———————2, 4, 5-Trichlorophenol_____91-58-7———————2-Chloronaphthalene_________88-74-4———————2-Nitroaniline___________131-11-3——————Dimethyl Phthalate_______208-96-8——————Acenaphthylene"___________606-20-2——————2, 6-Dinitrotoluene_______

750 !U750 |U750 |U750 !U750 !U750 iU750 |U750 !U750 iU750 |U750 !U750 IU750 IU750 IU750 !U750 |U79 | J

750 |U750 !U750 |U750 IU750 IU750 |U750 IU750 |U750 IU750 IU3700 IU750 IU3700 IU750 IU750 |U750 !U

FORM I SV-1 * :7 RevSB302908

007/f1C EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: IT PITTSBURGH_______ Contract:ITW-4A

Lab Code: ITPA Case No.: 03486_ SAS No.: ___. __ SDG No.: 021

Matrix: (soil/water) SOIL Lab Sainple ID: ITWMA_ .,_

Sample wt/vol: 30.1 (g/mL) G_.__ Lab File ID: 506032JD __


% Moisture: not dec. 13 dec. ___ Date Extracted: 03_/15/9_C




99-09-2 ——————— 3-Nitroaniline__________83-32-9———————Acenaphthene___________51-28-5———————2 , 4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2 —————— 2 , 4-Dinitrotoluene_______84-66-2———————Diethylphthalate_________7005-72-3——————4-Chlorophenyl-phenylether.86-73-7———————Fluor ene________________100-01-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol.86-30-6———————N-Nitrosodiphenylamine (1).101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene____________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluor an thene____________129-00-0*-—————Pyrene________________85-68-7—•—————Butylbenzylphthalate_____91-94-1-——————3,3' -Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene_______________117-81-7——————bis (2-Ethylhexyl) Phthalate.117-84-0——————Di-n-Octyl Phthalate_____205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo (k) Fluoranthene_____50-32-8—————-—Benzo (a) Pyrene__________193-39-5——————Indeno (1,2, 3-cd) Pyrene___53-70-3———————Dibenz (a,h) Anthracene____191-24-2——————Benzo (g,h, i) PeVylene_____

3700 !U750 iU3700 iU3700 !U750 iU750 iU750 !U750 !U750 !U3700 !U3700 !U750 |U750 !U750 iU3700 !U750 !U750 iU750 !U750 !U750 !U750 iU1500 1U750 JU750 !U1100 !100 ! J750 !U750 !U750 !U750 !U750 !U750 !U

(1) - Cannot be separated from Diphenylamine

FORM I SV-2

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ________

Lab Name: IT PITTSBURGH__________ Contract:ITW4B

Lab Code: ITPA Case No.: CJ486 SAS No.: ______ SDG No.: CLQ2

Matrix: (soil/water) SOIL Lab Sample ID: ITW4B ______

Sample wt/vol: 4.9 (g/mL) G__ Lab File ID: 202022ID



Column: (pack/cap) PACK Dilution Factor: 1.00_____


74-87-3———————Chlorome thane___________74-83-9———————Bromome thane___________75-01-4———————Vinyl Chloride__________75-00-3———————Chloroe thane____________75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulf ide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1, 2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate___________75-27-4———————Broraodichloromethane____78-87-5———————1, 2-Dichloropropane_____10061-01-5————cis-l/3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochlorome thane_____79-00-5———————1.1,2-Trichloroe thane____71-43-2—•—————Benzene______________10061-02-6————Trans-1,3-Dichloropropene110-75-8———————2-CHLOROETHYLVINYLETHER__75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8———————ACROLEIN________________

12 |U12 !U12 1U12 !U8 IB

12 !U6 |U6 !U6 1U6 !U6 !U6

12 !U6 !U6 !U

12 1U6 !U6 |U6 !U6 !U6 !U6 !U6 !U6 !U

•»• !U6 |U12 |U12 !U6 !U6 !U9 !6 |U6 iU6 !U4 1BJ

&0-ti- IU

FORM I VOA 1/87 Rev

&R3029IQ

! 107-13-1 ——————— ACRYLONITRILE_______________! Co

FORM I VOA I/87 Rev

RR3029H

PESTICIDE ORGANICS ANALYSIS DATA SHEET ______

ITW4BLab Name: IT PITTSBURGH_________ Contract:



Sample wt/v.ol: 30.0 (g/mL) G__ Lab File ID: ________






319-84-6——————alpha-BHC________319-85-7———————beta-BHC_________319-86-8———————delta-BHC_________58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxid«_959-98-8——————Endosulfan I_____60-57-1——————Dieldrin________72-55-9————————4 , 4 ' -DDE__________72-20-8———————Endrin__________33213-65-9————Endosulfan II____72-54-8———————4 , 4 ' -DDD_________1031-07-8—————Endosulfan sulfate50-29-3———————4, 4 ' -DOT________I72-43-5———————Methoxychlor_____53494-70-5————Endrin k«ton«____5103-71-9—————alph«-Chlordan«___5103-74-2—————ganuna-Chlordane___8001-35-2—————Tox»phen«_______12674-11-2————Aroclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232_____53469-21-9————Aroclor-1242_____12672-29-6————Aroclor-1248_____11097-69-1————Aroclor-1254_____

160 iU160 !U160 !U160 |U160 !U160 iU160 !U160 !U310 iU310 !U310 iU310 iU310 !U310 iU310 iU

1600 !U310 iU

1600 iU1600 !U3100 !U1600 !U1600 !U1600 iU1600 !U1600 iU3100 !U

11096-82-5————Aroclor-1260_______________! 3100 !U

FORM I PEST 1/87 Re

RR3029I2

oooosI EPA 3AMF:!.. I

I.NQRf3AHIC ANALV'rZ? DATA -;HI"ET

JTW46ab ;-3,'ne; iTA.5_PITT3BUF_GH_____..___ Cocti .-irt : F1RESTQNE._ :....._.....__..___.

_ab Cod."? 5 fTPA___ C^se T4c . ; C,:J4R6 13A5 No- ; _ ___ SDG -ic- , : •!'•"

l*trix ''so :. 3/watsr 5 : SOIL... !.. -ib -3a^npls IDs ITW4B.

( Ic-w/Ti^ci) ; L.CW_ ._ Data Racaived? ("'3''. ~

3.:.Ud

00013/'1A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET _________

ITW-4CLab Name: IT PITTSBURGH__________ Contract:

Lab Code: ITPA Case No.: 03486 SAS No.: _.___ SDG No.: 002

Matrix: (soil/water) SOIL Lab Sample ID: ITW-4C__

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: 2Q7Q220D



Column: (pack/cap) PACK Dilution Factor: 1_L.Q____.


74-87-3———————Chlorome thane___________74-83-9———————Bromome thane____________75-01-4———————Vinyl Chloride__________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform_____________107-06-2——————1, 2-Dichloroethane______78-93-3———————2-Butanone______________71-55-6———————1,1,1-Trichloroethane_____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2——————Benzene_________________10061-02-6-———Trans-1,3-Dichloropropene110-75-8———————2-CHLOROETHYLVINYLETHER__75-25-2———————Bromof orm_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroe thane.108-88-3——————Toluene__________________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes____________107-02-8——————ACROLEIN_______________

12 iU12 ]U12 !U12 |U6 IB12 |U6 |U6 !U6 iU6 !U6 IU6 |U

48 IB6 IU6 |U

12 IU6 |U6 |U6 |U6 |U6 |U6 IU6 IU6 IU

AH -4* ! U6 |U

12 |U12 |U6 IU6 |U6 IU6 |U6 IU6 |U6 IU

WO 43- |U

*/Afc,

FORM I VOA 1/87 Re%

ftR3029U

00014 A107-13-1——————ACRYLONITRILE __________! feo 4* ! U

FORM I VOA 1/87 Rev

PESTICIDE ORGANICS ANALYSIS DATA SHEET ________

ooojivLab Name: IT PITTSBURGH_________ Contract:









319-84-6——————alpha-BHC________________! 19 !U319-85-7——————beta-BHC__________________i 19 !U319-86-8——————delta-BHC___________________________! 19 !U58-89-9———————gamma-BBC (Lindane)________! 19 JU76-44-8———————Heptachlor_______________! 19 iU309-00-2——————Aldrin__________________I 19 !U1024-57-3—————Heptachlor epoxide_____________! 19 !U959-98-8——————Endosulfan I_________________! 19 !U60-57-1———————Dieldrin________________! 38 !U72-55-9———————4, 4'-DDE____________________________! 38 !U72-20-8———————Endrin_______________________! 38 |U33213-65-9————Endosulfan II_____________! 38 JU72-54-8———————4,4'-DDD__________________! 38 !U1031-07-8—————Endosulfan sulfate_______________! 38 !U50-29-3———————4, 4'-DOT________________________! 38 !U72-43-5———————Msthoxychlor_____________! 190 !U53494-70-5————Endrin keton«____________I 38 iU5103-71-9—————alpha-Chlordan*______________! 190 !U5103-74-2—————gasuna-Chlordan*__________! 190 !U8001-35-2—————Toxaph«n«________________! 380 iU12674-11-2————Aroclor-1016_____________! 190 !U11104-28-2————Aroclor-1221______________! 190 !U11141-16-5————Aroclor-1232_________________i 190 !U53469-21-9————Aroclor-1242____________________I 190 !U12672-29-6————Aroclor-1248_____________! 190 iU11097-69-1————Aroclor-1254______________! 380 !U11096-82-5————Aroclor-1260______________! 380 !U

FORM I PEST 1/87 Re

8R3Q29I6

00007U.S. EPA - CLP

1INORGANIC Ar? OATA 'SHEET __..„.._ .„.___

I ITW4CLab KUms: I r;-S._PTTTSBURGH____._____ ':•:-r tract: :"TKEcTGN£_.. I ___ _____

LaD Code; rTPA_ âse Nr> . • O3-.-86 EA3 No , J __ _ _ _ SD'3 Nr> , : '.; ;

Matrix : *5o 11/waêr'• :" SQIL._ !.,...?b 3amp 1 e IDs 77W-C

Level ( ! o.'j''ii:ed': : LOW_ De+a Received: .'

/. 3o 1 ids* ..33.5

Concentration Units (ug/L or mg/kg dry weight); MG/KG

f

iCAS No.ij V429-90-51 7440-38-21 7440-39-317440-41-7-| 7440-43-917440-70-21 7̂ 0-47-3-; 74-./40-48-41 744 0-50-8! 7439-89— 6 '1 7439-92-117439-95-4! 7439-96-517439- 97-6| 7440-02-0I 7440-09-7i 7440-22-4i 7440-23-51 744O-28-O1 7440-6E-S1 744Q.-66r-4W1. • • ' '"'̂P«̂ S?̂ •: - .'*'.;

l̂ Ŵ - -•• , £<i-!̂. . -?•*

i i; Analyte 1i i! A 1 urn i num '1 Arsenic i! Barium <\ Beryl 1 ium !i Cadmium 11 Calcium i1 Chromium 11 Cobalt i! Cop per'Iron i1 Lead !1 Magnesium 11 Manganese 11 Mercurv 1INickel 1I Potassium!1 Silver 1(Sodium 11 Thallium 1(Vanadium 1iînc 1infr 'i'£; ' !

I." 1

! 1Co nc en t r a t i o n 1 C 1

! i1 50OO ! 10.47IBI

108! !1.71 !

0 . 43 1 U 1463 1 B 11 . 3 1 U 15 , 3 1 B i6.4) |

1 3400 ! i•3 ., 3 1 !

2140! !3941 !

0 „ 1 1 1 U !2. SIB!4190! 10 . 72 1 U 131.4IBI0 . 24 1 U 11 i . O 1 B I45.81 1

1 J_ Z_ J" " i _ i _ _

! 11 1

I iQ IM i

l • 1IP !

N IF iE IP i

IP !IP !

E IP 1* IP 1

IP .1IP 1: p i

S* IF!E !P 1N IP i

1 CV !;p iIP 1IP 1IP 1

W IF iIP 1

N* 1 P 1; j1 1! ii i

1 i

Color Before:

Color After:

Comments:ARTIFACTS:

|

•BROWN " Clarity Before:

BROWN Claritv After:

STONES

Texture: MED

Artifacts: YES

FORI* I - IN

* 0015/VIA SPA SAMPL'I :rcVOLATILE ORGANICS ANALYSIS DATA SHEET

! ITW5ALab Narr.e: IT PITTSBURGH . Contract: _._ '_______

Lab Code: ITPA__ Case Nc. : Q.3435 5AS Me.: SDG :io. : CC5

Matrix: (soil/water) SOIL Lab Sair.ple ID: ITW5A

Sample wt/vcl: 5 .,0 (g/mL) G . _ Lab File ID: 2060221:!

Level: (low/rr.ed) LOW__ Date Received: C2-'17/90

% Moisture: not dec. 30 . Date Analyzed: 02/22/90

Colu.T.n: (pack/cap) P.AC-L . Dilution Factor: 1 .._T

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG _ Q

74-37-3 — ——74-33-9 ————75-01-4 ————75-00-3 ————

67-64-1 ————•75-15-0 ————75-35-4 ————75-34-3 ————540-59-0 ———

107-06-2 ———

71-55-6 ————c a ^> T c108-05-4 ———75-27-4 ————/ O O / O — — —

10061-01-5 —

79-00-5 ————

110-75-8 ———

108-10-1 ———KQ1 _"7Q_C__ _

79-34-5 ————J . U O O O J1 no Qn_T__— _100-41-4 ———100-42-5 ———1330-20-7 ——107-02-8 ———

-- — Chl or crr.e thane——— Srorr.ome thane——— Vinyl Chloride----Chloroe thane- — -Methylene Chloride----Acetone- —— Carbon Disulfide——— 1 , 1-Di

* 0007a 1a ; volatile organics analysis data sheet · 2020. 11. 30. · id epa sample no. pesticide...

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