subindex (aoac)

74
Subject Index AACC–AOAC methods aflatoxins in corn, Ch 49, p 14 biuret in fertilizers, Ch 2, p 19 β-D-glucan in barley and oats, Ch 32, pp 31–32B niacin and niacinamide in foods, drugs, and feeds, Ch 45, pp 14–15 nutrients in fertilizers, Ch 2, pp 25–26 protein (crude) in animal feed, Ch 4, p 13 riboflavin in foods and vitamin prepara- tions, Ch 45, pp 10–12 Absorbance nomograph relating concentration, ab- sorptivity, and, App C, p 17 (vol 1) Absorption indicator method quaternary ammonium compounds in formulations, Ch 7, p 100 Absorptivity nomograph relating concentration, absor- bance, and, App C, p 17 (vol 1) Acenocoumarol, Ch 19, pp 20–22, 35 Acephate in lettuce, Ch 10, pp 10–11 in soluble powder formulations, Ch 7, pp 97–97A in strawberries, Ch 10, pp 10–11 in technical material, Ch 7, pp 97-97A in tomatoes, Ch 10, pp 10–11 Acetaminophen, Ch 19, pp 7–9, 35 Acetanilid, Ch 18, pp 48, 58; Ch 19, pp 9–10, 35; Ch 20, p 32 Acetic acid in bread, Ch 32, pp 32B–33 in cake, Ch 32, p 36 corn-derived in apple cider vinegar, Ch 37, pp 21A–22 safe handling of, App B, p 3 in seafood, Ch 35, pp 13–14 Acetic anhydride safe handling of, App B, p 3 Acetic serum method water (added) in milk, Ch 33, p 26 Acetone in distilled liquors, Ch 26, pp 14–15 in drugs, Ch 18, p 2 extract in fish meal, Ch 4, p 26 safe handling of, App B, p 5 Acetone extraction method fat in fish meal, Ch 35, p 10 Acetone peroxides in baking premixes, Ch 47, pp 40–41 Acetonitrile safe handling of, App B, p 5 Acetyl value of oils and fats, Ch 41, p 5 2-Acetylamino-5-nitrothiazole in feeds, Ch 5, p 1 Acetylation methods hair preparations, Ch 15, p 9 hydroxyl value of oils and fats, Ch 41, p 6 phenylephrine HCl in drugs, Ch 18, p 22 Acetylcarbromal, Ch 19, pp 13, 35 Acid fuchsin D, Ch 46, p 8 Acid hydrolysis methods amino acids in feeds, Ch 4, pp 4–12 copper-reducing substances in spices, Ch 43, p 3 fat in bread, Ch 32, p 34 fat in eggs, Ch 34, p 2 fat in flour, Ch 32, p 5 fat in macaroni products, Ch 32, p 38 fat in seafood, Ch 35, pp 9–10 filth in baked goods, Ch 16, pp 20–21 filth in corn flour, Ch 16, p 19 phenacetin and phenyl salicylate in drugs, Ch 19, p 11 starch in baking powders, Ch 25, pp 3–4 Acid value of butterfat, Ch 33, p 56F Acid-detergent fiber in feeds, Ch 4, p 28A in feeds and forages, Ch 4, p 20–21 Acid-insoluble residue method soil in frozen spinach, Ch 16, p 35 Acidic drugs, Ch 19, pp 1–2 Acidity in nonalcoholic beverages, Ch 29, p 2 of beer, Ch 27, p 6 of brewing sugars and sirups, Ch 27, p 35 of cheese, Ch 33, p 61 of corn sirups and sugars, Ch 44, p 40 of eggs, Ch 34, pp 6–7 of feeds, Ch 4, p 31 of food dressings, Ch 43, p 8 of fruit products, Ch 37, p 11 of honey, Ch 44, p 31 of milk, Ch 33, p 7 of prepared mustard, Ch 43, p 6 of roasted coffee, Ch 30, p 2 of tragacanth drugs, Ch 20, p 31 of water, Ch 11, pp 2–3 of wines, Ch 28, pp 8–9 see also Fat acidity Acids in beer, Ch 27, p 6 in bread, Ch 32, pp 33–34 in butter, Ch 33, p 57 in canned vegetables, Ch 42, pp 8–9 in color additives, Ch 46, p 25 in cordials and liqueurs, Ch 26, p 21 in cream, Ch 33, p 48 in distilled liquors, Ch 26, p 9 in hops, Ch 27, p 32 in nonalcoholic beverages, Ch 29, p 1 in oils and fats, Ch 41, pp 11–12 safe handling of, App B, pp 2–3 solution strengths, App C, p 3 (vol 1) in vinegars, Ch 43, p 11 see also Fatty acids Aconitine, Ch 18, pp 45, 58; Ch 20, pp 23, 32 Acrylamide disc electrophoresis method identification of fish species, Ch 35, pp 25–26 Acrylonitrile in food, Ch 48, pp 6–7 Adamkiewicz test protein in feeds, Ch 4, p 13 Adipose tissue hexachlorobenzene and mirex residues in, Ch 10, pp 52–53 Adrenocortico steroids, Ch 21, pp 8–14 Adulterants meat and poultry adulteration of meat products, Ch 39, p 22 in processed Florida orange juice, Ch 37, pp 21–22 in spices, Ch 43, pp 4–5 Aerobic plate counts bacteria in chilled, frozen, precooked, or prepared foods, Ch 17, pp 3–4 in dry rehydratable film, Ch 17, pp 10–11 in foods, Ch 17, pp 10–11 microorganisms in dairy products, Ch 17, pp12–13 microorganisms in foods, Ch 17, pp 8–10 pectin gel method, Ch 17, p 10 Aerosol products antiperspirants, Ch 15, pp 4–5 Affinity quantitative determination β-lactam antibiotics in milk, Ch 33, p 38 Aflatoxin B 1 , B 2 in cottonseed products, Ch 49, pp 21–23, 24A–25 in foods and feeds, Ch 49, pp 5–6 in mixed feed, Ch 49, pp 24A–25 in peanuts and peanut products, Ch 49, pp 8–10 Aflatoxin G 1 , G 2 in cottonseed products, Ch 49, pp 21–23 in foods and feeds, Ch 49, pp 5–6 in peanuts and peanut products, Ch 49, pp 8–10 © 1998 AOAC INTERNATIONAL

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  • Subject Index AACCAOAC methods

    aflatoxins in corn, Ch 49, p 14biuret in fertilizers, Ch 2, p 19-D-glucan in barley and oats, Ch 32,

    pp 3132Bniacin and niacinamide in foods, drugs,

    and feeds, Ch 45, pp 1415nutrients in fertilizers, Ch 2, pp 2526 protein (crude) in animal feed, Ch 4,

    p 13riboflavin in foods and vitamin prepara-

    tions, Ch 45, pp 1012Absorbance

    nomograph relating concentration, ab-sorptivity, and, App C, p 17 (vol 1)

    Absorption indicator methodquaternary ammonium compounds in

    formulations, Ch 7, p 100Absorptivity

    nomograph relating concentration, absor-bance, and, App C, p 17 (vol 1)

    Acenocoumarol, Ch 19, pp 2022, 35Acephate

    in lettuce, Ch 10, pp 1011in soluble powder formulations, Ch 7,

    pp 9797Ain strawberries, Ch 10, pp 1011in technical material, Ch 7, pp 97-97Ain tomatoes, Ch 10, pp 1011

    Acetaminophen, Ch 19, pp 79, 35Acetanilid, Ch 18, pp 48, 58; Ch 19,pp 910, 35; Ch 20, p 32Acetic acid

    in bread, Ch 32, pp 32B33in cake, Ch 32, p 36corn-derived in apple cider vinegar,

    Ch 37, pp 21A22safe handling of, App B, p 3in seafood, Ch 35, pp 1314

    Acetic anhydride safe handling of, App B, p 3

    Acetic serum methodwater (added) in milk, Ch 33, p 26

    Acetone in distilled liquors, Ch 26, pp 1415 in drugs, Ch 18, p 2 extract in fish meal, Ch 4, p 26 safe handling of, App B, p 5

    Acetone extraction method fat in fish meal, Ch 35, p 10

    Acetone peroxides in baking premixes, Ch 47, pp 4041

    Acetonitrile safe handling of, App B, p 5

    Acetyl value of oils and fats, Ch 41, p 5

    2-Acetylamino-5-nitrothiazole in feeds, Ch 5, p 1

    Acetylation methods hair preparations, Ch 15, p 9 hydroxyl value of oils and fats, Ch 41,

    p 6phenylephrine HCl in drugs, Ch 18, p 22

    Acetylcarbromal, Ch 19, pp 13, 35Acid fuchsin D, Ch 46, p 8Acid hydrolysis methods

    amino acids in feeds, Ch 4, pp 412copper-reducing substances in spices,

    Ch 43, p 3fat in bread, Ch 32, p 34fat in eggs, Ch 34, p 2fat in flour, Ch 32, p 5fat in macaroni products, Ch 32, p 38fat in seafood, Ch 35, pp 910filth in baked goods, Ch 16, pp 2021filth in corn flour, Ch 16, p 19phenacetin and phenyl salicylate in

    drugs, Ch 19, p 11 starch in baking powders, Ch 25, pp 34

    Acid value of butterfat, Ch 33, p 56F

    Acid-detergent fiber in feeds, Ch 4, p 28Ain feeds and forages, Ch 4, p 2021

    Acid-insoluble residue method soil in frozen spinach, Ch 16, p 35

    Acidic drugs, Ch 19, pp 12Acidity

    in nonalcoholic beverages, Ch 29, p 2of beer, Ch 27, p 6of brewing sugars and sirups, Ch 27, p 35of cheese, Ch 33, p 61of corn sirups and sugars, Ch 44, p 40of eggs, Ch 34, pp 67of feeds, Ch 4, p 31 of food dressings, Ch 43, p 8of fruit products, Ch 37, p 11of honey, Ch 44, p 31of milk, Ch 33, p 7of prepared mustard, Ch 43, p 6of roasted coffee, Ch 30, p 2of tragacanth drugs, Ch 20, p 31 of water, Ch 11, pp 23 of wines, Ch 28, pp 89 see also Fat acidity

    Acids in beer, Ch 27, p 6in bread, Ch 32, pp 3334in butter, Ch 33, p 57in canned vegetables, Ch 42, pp 89in color additives, Ch 46, p 25in cordials and liqueurs, Ch 26, p 21

    in cream, Ch 33, p 48in distilled liquors, Ch 26, p 9in hops, Ch 27, p 32in nonalcoholic beverages, Ch 29, p 1in oils and fats, Ch 41, pp 1112safe handling of, App B, pp 23 solution strengths, App C, p 3 (vol 1) in vinegars, Ch 43, p 11see also Fatty acids

    Aconitine, Ch 18, pp 45, 58; Ch 20,pp 23, 32Acrylamide disc electrophoresis method

    identification of fish species, Ch 35, pp 2526

    Acrylonitrile in food, Ch 48, pp 67

    Adamkiewicz test protein in feeds, Ch 4, p 13

    Adipose tissue hexachlorobenzene and mirex residues

    in, Ch 10, pp 5253Adrenocortico steroids, Ch 21, pp 814 Adulterants

    meat and poultry adulteration of meatproducts, Ch 39, p 22

    in processed Florida orange juice, Ch 37,pp 2122

    in spices, Ch 43, pp 45Aerobic plate counts

    bacteria in chilled, frozen, precooked, orprepared foods, Ch 17, pp 34

    in dry rehydratable film, Ch 17, pp 1011

    in foods, Ch 17, pp 1011microorganisms in dairy products,

    Ch 17, pp1213 microorganisms in foods, Ch 17,

    pp 810pectin gel method, Ch 17, p 10

    Aerosol products antiperspirants, Ch 15, pp 45

    Affinity quantitative determination-lactam antibiotics in milk, Ch 33,

    p 38Aflatoxin B1, B2

    in cottonseed products, Ch 49, pp 2123,24A25

    in foods and feeds, Ch 49, pp 56in mixed feed, Ch 49, pp 24A25in peanuts and peanut products, Ch 49,

    pp 810Aflatoxin G1, G2

    in cottonseed products, Ch 49, pp 2123in foods and feeds, Ch 49, pp 56in peanuts and peanut products, Ch 49,

    pp 810

    1998 AOAC INTERNATIONAL

  • Aflatoxin M1 in cheese, Ch 33, p 62in dairy products, Ch 49, p 30in fluid milk, Ch 49, pp 3435in liver, Ch 49, p 32in milk and cheese, Ch 49, pp 3031 in milk and powdered milk, Ch 33, p 31

    Aflatoxins in cocoa beans, Ch 49, p 12in coconut, copra, and copra meal,

    Ch 49, p 13in corn, Ch 49, p 14in corn, almonds, Brazil nuts, peanuts,

    and pistachio nuts, Ch 49, pp 2424A

    in corn and peanuts, Ch 49, p 6in corn, cottonseed, peanuts, and peanut

    butter, Ch 49, pp 67in cottonseed products, Ch 49, pp 2123in cottonseed products and mixed feed,

    Ch 49, pp 2425in foods and feeds, Ch 49, pp 56 in green coffee, Ch 49, p 27identification of, Ch 49, pp 45, 2830in peanuts and peanut products, Ch 49,

    pp 810in pistachio nuts, Ch 49, p 27in soybeans, Ch 49, p 27sampling of, Ch 49, p 2standards for, Ch 49, pp 34 see also specific aflatoxins

    Agar in meat, Ch 39, pp 1920

    Agar cutterantibiotics in feed, Ch 5, p 34

    Air oven methods moisture in cereal adjuncts, Ch 27, p 29solids and moisture in flour, Ch 32, p 1solids and moisture in macaroni prod-

    ucts, Ch 32, p 38solids in yeast, Ch 27, p 38

    Aklomide in feeds, Ch 5, pp 12

    Alachlorin finished drinking water, Ch 10,

    pp 2630in pesticide formulations, Ch 7, pp 5052

    Alaska King Crab Marketing and Control BoardAOAC method

    drained weight of frozen crabmeat, Ch 35, pp 45

    Alba red, Ch 46, p 8Albumin

    in evaporated milk, Ch 33, p 53in milk, Ch 33, p 16

    Alcohol in almond extract, Ch 36, p 17in anise and nutmeg extracts, Ch 36,

    p 19in beer, Ch 27, p 4

    in cassia, cinnamon, and clove extracts,Ch 36, pp 1819

    in cordials and liqueurs, Ch 26, p 19 in distilled liquors, Ch 26, pp 16 in drugs, Ch 18, p 2 extract of spices, Ch 43, p 2in flavor extracts and toilet preparations,

    Ch 36, p 20in flavors, Ch 36, p 1 in fruit products, Ch 37, p 3in ginger extract, Ch 36, p 19handling of, Ch 49, p 1 in lemon, orange, and lime extracts,

    Ch 36, p 11in nonalcoholic beverages, Ch 29, p 1in peppermint, spearmint, and winter-

    green extracts, Ch 36, p 19percentages by volume in mixtures of

    ethyl alcohol and water, App C,pp 2126 (vol 2)

    percentages by weight in mixtures of ethylalcohol and water, App C, p 27

    precipitate in fruit products, Ch 37, p 9in sirups used in confectionery, Ch 44,

    p 19solution strengths, App C, p 3 (vol 1) in vanilla extract, Ch 36, p 1in vinegars, Ch 43, pp 1112in wines, Ch 28, pp 13see also Ethyl alcohol

    Alcohol method solids in yeast, Ch 27, p 37

    Alcoholic beverages certified reference materials for, App A,

    pp 89 ethyl carbamate in, Ch 28, pp 1414Asee also Beer; Cordials and liqueurs;

    Distilled liquors; Malt beveragesand brewing materials; Wines

    Alcoholic products denaturants in, Ch 8, p 1

    Alcohols (higher) and ethyl acetate in distilled liquors,

    Ch 26, pp 1214Aldehydes

    as acetaldehyde in frozen vegetables, Ch 42, p 12

    in cordials and liqueurs, Ch 26, p 20in distilled liquors, Ch 26, pp 9, 1011in lemon and orange oils, Ch 36,

    pp 1516in lemon, orange, and lime extracts,

    Ch 36, pp 1314in wines, Ch 28, p 11

    Aldicarb in formulations, Ch 7, pp 2223 in grapes and potatoes, Ch 10, pp 3639

    Aldrin in formulations, Ch 7, pp 5253 in water, Ch 10, pp 1317

    multiresidue methods, Ch 10, p 6 Alfalfa leaves

    filth in, Ch 16, pp 3841Alginates

    in chocolate beverages, Ch 29, p 7in chocolate frozen desserts, Ch 33, p 73 in chocolate products, Ch 31, p 16in food dressings, Ch 43, p 10

    Alimentary pastes filth in, Ch 16, p 22

    Alizarin cyanine green F, Ch 46, p 6Alizurol purple, Ch 46, p 9Alizurol purple SS, Ch 46, p 8Alkalies

    safe handling of, App B, pp 34solution strengths, App C, p 3 (vol 1)

    Alkalimeter method carbon dioxide in liming materials,

    Ch 1, pp 23Alkalimetric ammonium molybdophos-phate method

    phosphorus in feeds, Ch 4, p 35Alkalimetric methods

    phosphorus in fertilizers, Ch 2, pp 7, 9,1011

    Alkaline hydrolysis method phenacetin and phenyl salicylate in

    drugs, Ch 19, p 11Alkaline phosphatase activity

    in fluid dairy products, Ch 33, pp 3637Alkaline phosphatase detection methods

    mammalian feces in grain products, Ch 16, pp 5456

    filth in grain products, Ch 16, pp 5456mammalian feces in ground black

    pepper, Ch 16, pp 5657Alkaline phosphatase test

    mammalian feces, Ch 16, p 54Alkalinity

    of ash of cacao products, Ch 31, p 2of ash of dry skim milk, Ch 33, p 56of ash of vinegars, Ch 43, p 11of ash of wines, Ch 28, p 6of water, Ch 11, p 3

    Alkaloid drugs chichona, Ch 20, pp 1618 ephedra, Ch 20, pp 911ergot, Ch 20, pp 1114 ipecac, Ch 20, pp 79 microchemical tests, Ch 18, pp 4447 opiates, Ch 20, pp 16 optical crystallographic properties,

    App C, pp 45 (vol 1)physostigmine, Ch 20, pp 1418 rauwolfia, Ch 20, pp 1823 refractive indices, App C, p 13 (vol 1) titration factors, Ch 20, p 2 tropane, Ch 20, pp 67 xanthine, Ch 18, p 5354; Ch 20, p 7 see also specific drugs

    1998 AOAC INTERNATIONAL

  • Alkaloidsin ephedra, Ch 20, p 9 sabadilla, in pesticide formulations,

    Ch 7, pp 4950 in tobacco, Ch 3, pp 3031

    Alkanolamines norepinephrine in epinephrine prepara-

    tions, Ch 18, pp 2122 phenylalkanolamine salts in elixirs and

    sirups, Ch 18, pp 2526 phenylephrine HCl in drugs, Ch 18,

    pp 2224 phenylpropanolamine HCl in drugs,

    Ch 18, p 25Alkoxyl groups

    microchemical determination, Ch 12, p 13

    Allergenic extracts in drugs, Ch 20, p 31

    Allethrin technical and formulations, Ch 7,

    pp 4142Allobarbital, Ch 18, p 47Allopurinol, Ch 19, pp 3233, 35Allspice

    extract, Ch 36, p 20filth in, Ch 16, pp 3840, 41 foreign matter in, Ch 16, p 39tannin in, Ch 43, p 3

    5-Allyl-5-(2-cyclopenten-1-yl) barbitu-ric acid, Ch 18, p 47Almonds

    aflatoxins in, Ch 49, pp 2424AAlmond extract

    alcohol in, Ch 36, p 17benzaldehyde in, Ch 36, pp 1718benzoic acid in, Ch 36, p 18hydrocyanic acid, Ch 36, p 18nitrobenzene in, Ch 36, p 18

    Aloin, Ch 20, pp 28, 32-Amylase

    in flour, meal, and malted cereals, Ch 32,p 20

    in malt, Ch 27, pp 2829Alphazurine FG, Ch 46, p 6Alternating current spark excitationmethod

    metals in plants, Ch 3, p 3Aluminum

    in baking powders, Ch 25, pp 45in coal fly ash, Ch 9, pp 3134 in deodorants, Ch 15, pp 34 in face powders, Ch 15, p 8 in liming materials, Ch 1, pp 5, 7in plants, Ch 3, pp 23, 45 in soil acidifiers, Ch 2, p 35in solid wastes, Ch 9, pp 3134in waters and wastewaters, Ch 9,

    pp 3444in water, Ch 11, pp 13, 1415

    Aluminum oxide in face powders, Ch 15, p 8 in liming materials, Ch 1, p 5

    Aluminum sulfate soil acidifiers aluminum in, Ch 2, p 35

    Amaranth, Ch 46, pp 12 American Association of Cereal Chem-ists, see AACCAmerican Conference of Governmental Industrial HygienistsAOAC method

    antimony in food, Ch 9, p 9American Oil Chemists Society, seeAOCS American Society of EnologistsAOACmethod

    acidity of wines, Ch 28, p 8American Spice Trade AssociationAOAC method

    piperine in pepper preparations, Ch 43,pp 56

    Ametrynin finished drinking water, Ch 10,

    pp 2630pesticide formulation, Ch 7, pp 4041

    Aminesin color additives, Ch 46, p 13

    Amino acidsin feeds, Ch 4, pp 412 in vitamin preparations, Ch 45, pp 4951

    Aminobarbital, Ch 18, p 47Aminobenzoates

    antipyrene with benzocaine in drugs, Ch 18, pp 2829

    benzocaine in drugs, Ch 18, p 28 butacaine sulfate in drugs, Ch 18,

    pp 2930procainamide HCl in drugs, Ch 18, p 30procaine in drugs, Ch 18, pp 3132

    p-Aminobenzoic acid in feeds, Ch 5, pp 23

    Aminocarb technical and formulations, Ch 7, p 23Aminomethyl phosphate in water,

    Ch 10, pp 5051Aminomethylphosphonic acid

    and glyphosate in environmental water,Ch 10, pp 5051

    2-Amino-5-nitrothiazole in feeds, Ch 5, p 3

    Aminophylline, Ch 19, pp 15, 35Aminopyrine, Ch 18, pp 48, 58; Ch 19, pp 11, 12, 35pAminosalicylic acid, Ch 19, pp 23, 35Amitriptyline, Ch 18, pp 3233, 58Amitrole

    in formulations, Ch 7, p 35Ammonia

    anhydrous, sampling of, Ch 2, p 3in baking powders, Ch 25, p 5in crabmeat, Ch 35, p 6

    safe handling of, App B, p 3 solution strengths, App C, p 3 (vol 1)solutions, sampling of, Ch 2, pp 13 in water, Ch 11, pp 910

    Ammoniacal silver nitrate safe handling of, App B, p 5

    Ammonium, see Quaternary ammoniumcompoundsAmmonium bromide

    in elixir, Ch 18, pp 910Ammonium glycyrrhizinate

    in flavor extracts, Ch 36, pp 2223Ammonium hydroxide

    safe handling of, App B, p 3Ammonium thiocyanates, App A, p 1Amobarbital, Ch 18, pp 47, 58; Ch 19, p 35Amobarbital sodium, Ch 19, p 14Amphetamines

    chemical name, Ch 18, p 58; Ch 22, p 6 enantiomers in bulk drugs, syrups, and

    capsules, Ch 22, pp 12 in drugs, Ch 18, pp 2627 microchemical tests, Ch 18, pp 5253

    Amprolium in feeds, Ch 5, pp 3, 4

    Amyl alcohol in distilled liquors, Ch 26, pp 1314

    Amyl p-dimethylaminobenzoate in suntan preparations, Ch 15, pp 1011

    Amylocaine, Ch 18, pp 45, 58Analgesics/antipyretics

    acetaminophen in drug preparations, Ch 9, pp 79

    acetanilid in drugs, Ch 19, pp 910 aminopyrine in drugs, Ch 19, pp 11, 12 aspirin in drugs, Ch 19, pp 1012with caffeine in drugs, Ch 19, pp 1011 with codeine in drugs, Ch 19, p 9 with morphine in drugs, Ch 19, p 10phenacetin in drugs, Ch 19, pp 1011 with phenobarbital in drugs, Ch 19,

    pp 1112with phenolphthalein in drugs, Ch 19,

    p 12phenyl salicylate in drugs, Ch 19, p 11 quinine in drugs, Ch 19, p 10 salicylamide in drugs, Ch 19, pp 89 sodium salicylate in drugs, Ch 19, p 10

    Anilazine in formulations, Ch 7, p 24

    Aniline safe handling of, App B, p 5

    Animal fats cis- and trans-octadecenoic isomers and

    general fatty acid composition in,Ch 41, pp 2627A

    organochlorine pesticide residues in, Ch 10, pp 12A13

    1998 AOAC INTERNATIONAL

  • in vegetable fats and oils, Ch 41,pp 3536

    Animal feeds, see Feeds Animal tissues

    certified reference materials for, App A,pp 89

    chlortetracycline, oxytetracycline, andtetracycline in edible animal tis-sues, Ch 23, pp 1923

    copper in liver, Ch 14, pp 12 in feeds, identification of, Ch 4,

    pp 3738 see also Drugs and feed additives in ani-

    mal tissuesAnion-exchange methods

    carbohydrates in soluble (instant) coffee,Ch 30, pp 511

    phytate in foods, Ch 32, pp 4243Anions

    in water, Ch 11, pp 2830Anise

    extract, Ch 36, p 19filth in, Ch 16, pp 3840 foreign matter in, Ch 16, p 39

    Annatto filth in, Ch 16, pp 3840, 41 in macaroni products, Ch 32, pp 4041

    Anodic stripping voltammetric methodscadmium and lead in food, Ch 9, pp 45 lead in evaporated milk, Ch 9, p 17

    ANOT in animal tissues, Ch 23, pp 12

    Anthocyanins in fruit juices, Ch 37, p 18

    Antibiotics -lactam in milk, Ch 33, pp 3843optical crystallographic properties, App C,

    pp 56 (vol 1) refractive indices, App C, pp 1314

    (vol 1) see also specific antibiotics

    Antibiotics in feeds bacitracin, Ch 5, pp 3031, 3638 chemical methods for, Ch 5, pp 3033 chlortetracycline, Ch 5, p 31 chlortetracycline HCl, Ch 5, pp 3840 common and chemical names of, Ch 5,

    p 51 erythromycin, Ch 5, pp 4041 griseofulvin, Ch 5, p 32hygromycin, Ch 5, p 41 lasalocid, Ch 5, pp 3233, 4142 lincomycin, Ch 5, p 43 monensin, Ch 5, pp 4345neomycin, Ch 5, pp 4546 novobiocin, Ch 5, p 46 nystatin, Ch 5, pp 4647 oleandomycin, Ch 5, pp 47oxytetracycline, Ch 5, pp 4748 procaine penicillin, Ch 5, p 48

    spectinomycin, Ch 5, pp 4849 streptomycin, Ch 5, p 49tylosin, Ch 4, p 38; Ch 5, p 50

    Anticoagulants, Ch 19, pp 2023Antiemetics, Ch 18, pp 5455Antifungals, Ch 18, p 56Antihistamines

    with aspirin, phenacetin, and caffeine indrugs, Ch 18, pp 2021

    chlorpheniramine maleate in drug tab-lets, Ch 18, pp 1920

    codeine in presence of, Ch 20, pp 12 in dosage forms, Ch 18, pp 1726drug combinations, Ch 18, p 17 hydrocodone in presence of, Ch 20,

    pp 34 meperidine in drugs, Ch 18, pp 1718 mephentermine sulfate in drugs, Ch 18,

    p 18 methapyrilene in expectorants, Ch 18,

    pp 1819optical crystallographic properties,

    App C, p 7 (vol 1) pheniramine maleate in dosage forms,

    Ch 18, pp 2021pyrilamine in cough sirup, Ch 18, p 19 refractive indices, App C, p 14 (vol 1) thonzylamine HCl, Ch 18, p 2021

    Antihypertensives, Ch 18, pp 5758Antimicrobial drugs

    in milk, Ch 33, pp 4345Antimony

    in coal fly ash, Ch 9, pp 3134in food, Ch 9, p 9in solid wastes, Ch 9, pp 3134in wastewaters, Ch 9, pp 3444

    Antioxidants butylated hydroxyanisole and butylated

    hydroxytoluene in cereals, Ch 47,pp 56

    in corn and rice breakfast cereals, Ch 32,p 30

    in food, Ch 47, pp 12in oils and fats, Ch 47, pp 25phenolic in oils, fats, and butter oil,

    Ch 47, pp 24propyl gallate in food, Ch 47, pp 67

    Antiparkinsonian drugs, Ch 18, pp 5657 Antiperspirants

    boric acid in, Ch 15, pp 56 zirconium in, Ch 15, pp 45

    Antipyretics, see Analgesics/antipyreticsAntipyrine, Ch 18, pp 2829, 58Antiseptics

    thymol in, Ch 19, p 7AOACAACC methods

    aflatoxins in corn, Ch 49, p 14biuret in fertilizers, Ch 2, p 19niacin and niacinamide in foods, drugs,

    and feeds, Ch 45, pp 1415

    nutrients in fertilizers, Ch 2, pp 2526 protein (crude) in animal feed, Ch 4,

    p 13riboflavin in foods and vitamin prepara-

    tions, Ch 45, pp 1012AOACAOCS methods

    crude fiber in feeds, Ch 4, pp 2628fatty acids in encapsulated fish oils and

    fish oil methyl and ethyl esters, Ch 49, pp 67

    fatty acids (crude) in oils and fats, Ch 41,pp 1011

    hydrocarbons (saturated) in glycerides,Ch 41, pp 4041

    hydroxyl value of oils and fats, Ch 41, p 6

    1-monoglycerides and monoglycerideconcentrates, Ch 41, pp 4344

    peroxide value of oils and fats, Ch 41, p 9polyunsaturated acids in oils and fats,

    Ch 41, pp 1317trans isomers in margarines and shorten-

    ings, Ch 41, pp 27A27CAOACASBC methods

    aphids in hops, Ch 16, pp 78calcium in beer, Ch 27, pp 1011ethanol in beer, Ch 27, pp 45extract of barley for malting, Ch 27,

    p 21glycerol in beer, Ch 27, p 6moisture in malting barley, Ch 27, p 21N-nitrosodimethylamine in beer, Ch 27,

    pp 1516 specific gravity of beer and wort, Ch 27,

    p 3AOACAmerican Water Works Asso-ciation method

    glyphosate and aminomethylphos-phonic acid in environmentalwater, Ch 10, pp 5051

    AOACASTM methodscadmium and lead in earthenware, Ch 9,

    p 6B cation exchange capacity for peat, Ch 2,

    p 39 extractives from flexible barrier materi-

    als, Ch 48, pp 45lead and cadmium extracted from

    ceramicware, Ch 9, pp 6A6BAOACCIPAC methods

    alachlor in formulations, Ch 7, pp 5152

    aminocarb, technical and pesticide for-mulations, Ch 7, p 23

    anilazine in formulations, Ch 7, p 24 azinphos-methyl in formulations, Ch 7,

    pp 80A81 butachlor in formulations, Ch 7, pp 5859 captan in formulations, Ch 7, pp 5960

    1998 AOAC INTERNATIONAL

  • chloramben in formulations, Ch 7, p 60

    chlordimeform in formulations, Ch 7, pp 6263

    chlorotoluron, chloroxuron, or me-toxuron in formulations, Ch 7,pp 2728

    copper in fungicides, Ch 7, pp 1112 cyanazine in formulations, Ch 7,

    pp 3637cyhexatin technical and formulations,

    Ch 7, pp 9899cypermethrin in pesticide formulations,

    Ch 7, p 42 DDT in formulations, Ch 7, pp 6566deltamethrin in pesticide formulations,

    Ch 7, p 43dicamba-MCPA and dicamba-2,4-D in

    formulations, Ch 7, p 67 dichlobenil in formulations, Ch 7,

    pp 6869 diflubenzuron in formulations, Ch 7,

    pp 7071 diquat in formulations, Ch 7, p 38endosulfan in formulations, Ch 7,

    pp 7172fentin in formulations, Ch 7, p 12fentin in fentinmaneb formulations,

    Ch 7, pp 1213folpet in formulations, Ch 7, pp 7273 formothion in formulations, Ch 7,

    pp 8586 -BHC in technical BHC, formulations,

    and lindane shampoos and lotions,Ch 7, pp 5556

    isofenphos, technical and formulations,Ch 7, pp 8687

    maneb in formulations, Ch 7, pp 1314

    mercury in organic mercurial seed disin-fectants, Ch 7, pp 2021

    methamidophos in formulations, Ch 7,pp 8990

    methiocarb technical and pesticide for-mulations, Ch 7, pp 2930

    metolachlor in formulations, Ch 7, p 76 organochlorine pesticide contamination

    of pesticide formulations, Ch 7, pp 78

    oxydemetonmethyl in pesticide formu-lations, Ch 7, pp 8990

    oxythioquinox in formulations, Ch 7, pp 99100

    perimiphos methyl in formulations, Ch 7, pp 9394

    permethrin in formulations, Ch 7, pp 4344

    phosphamidon in formulations, Ch 7, pp 9495

    propachlor in formulations, Ch 7, pp 7778

    propoxur technical and pesticide formu-lations, Ch 7, p 31

    temephos in formulations, Ch 7, pp 9596

    terbuthylazine in formulations, Ch 7, pp 3940

    tetradifon (technical) in formulations,Ch 7, pp 7879

    thiram in formulations, Ch 7, pp 3233triadimefon technical and pesticide for-

    mulations, Ch 7, pp 3334triazines in formulations, Ch 7,

    pp 4041 AOACCodex-Adopted methods, seeCodex-AdoptedAOAC methods AOACFood Chemicals Codex method

    neutralizing value of sodium aluminumphosphate, Ch 25, pp 23

    AOACIDF methodsListeria monocytogenes in milk and

    dairy products, Ch 17, pp 94D98AOACInternational Fruit Juice Unionmethod

    patulin in apple juice, Ch 49, pp 4344AOACIUPAC methods

    aflatoxin B1 in corn and roasted peanuts,Ch 49, pp 1618

    aflatoxin B1 in cottonseed products andmixed feed, Ch 49, pp 24A25

    aflatoxins in corn, cottonseed, peanuts,and peanut butter, Ch 49, pp 67

    antioxidants in oils and fats, Ch 47, pp 25

    butyric acid in fats containing butterfat,Ch 47, pp 2829

    copper in food, Ch 9, p 10copper, iron, and nickel in edible oils and

    fats, Ch 9, pp 78fatty acids in oils and fats, Ch 41,

    pp 1718fumonisns B1, B2, and B3 in corn, Ch 49,

    pp 4951methyl esters of fatty acids in oils and

    fats, Ch 41, pp 1819patulin in apple juice, Ch 49, pp 4344phenolic antioxidants in oils, fats, and

    butter fats, Ch 47, pp 24tiglycerides in oils and fats, Ch 41,

    p 31AOACOffice International du Cacao etdu Chocolat methods

    alkalinity of ash of cacao products, Ch 31, p 2

    ash of cacao products, Ch 31, pp 56AOCSAOAC methods

    crude fiber in feeds, Ch 4, pp 2628

    fatty acids in encapsulated fish oils andfish oil methyl and ethyl esters, Ch 49, pp 67

    fatty acids (crude) in oils and fats, Ch 41,pp 1011

    hydrocarbons (saturated) in glycerides,Ch 41, pp 4041

    hydroxyl value of oils and fats, Ch 41, p 6

    1-monoglycerides and monoglycerideconcentrates, Ch 41, pp 4344

    peroxide value of oils and fats, Ch 41, p 9

    polyunsaturated acids in oils and fats,Ch 41, pp 1317

    trans isomers in margarines and shorten-ings, Ch 41, pp 27A27C

    APC drugs, Ch 19, pp 1011codeine in, Ch 20, p 3

    Aphids in hops, Ch 16, pp 78

    Apomorphine, Ch 18, pp 45, 58; Ch 20,pp 1, 32Apomorphine HCl, Ch 20, p 2Apple butter

    filth in, Ch 16, p 27mold in, Ch 16, p 61

    Apple chops filth in, Ch 16, p 27

    Apple cider vinegarcorn-derived acetic acid in, Ch 37,

    pp 2324Apple juice

    corn syrup in, Ch 37, pp 1920D-malic acid in , Ch 37, pp 1617L-malic and total malic acid ratio, Ch 37,

    pp 2122patulin in, Ch 49, pp 4244quinic, malic, and citric acids in, Ch 37,

    pp 1314Apples

    azinphos-methyl pesticide residues on,Ch 10, p 39

    captan pesticide residues in, Ch 10, p 41 carbaryl pesticide residues in, Ch 10,

    pp 4243dodine pesticide residues in, Ch 10,

    pp 4546 fluorine on, Ch 9, p 10 glyodin pesticide residues in, Ch 10,

    pp 4950 lead on, Ch 9, p 15 N-methylcarbamate residues on, Ch 10,

    pp 32C33, 3639 naphthyleneacetic acid pesticide resi-

    dues in, Ch 10, pp 5657 nicotine residues in, Ch 10, pp 5758 organochlorine pesticide residues in,

    Ch 10, pp 1718

    1998 AOAC INTERNATIONAL

  • organophosphorus pesticide residues on,Ch 10, pp 2124

    thiram pesticide residues in, Ch 10, pp 60, 78

    Applesauce ethylenethiourea pesticide residues in,

    Ch 10, pp 4849Apricots

    azinphos-methyl pesticide residues on,Ch 10, p 39

    Aprobarbital, Ch 18, pp 47, 58Arabinose

    in sugars and sirups, Ch 44, p 12Arachidonic acid

    in oils and fats, Ch 41, pp 1317Arecoline, Ch 18, pp 45, 58; Ch 20,pp 2, 32Aroclor

    in serum, Ch 10, pp 1921Arprinocid

    in feeds, Ch 5, p 4 in premixes, Ch 5, p 4

    Arsanilic acid in feeds, Ch 5, pp 23, 45

    Arsenic in animal tissues, Ch 23, p 2 in baking powders, Ch 25, p 5 in Bordeaux mixtures, Ch 7, pp 3, 1516 in cacodylate injections, Ch 18, p 5 in calcium arsenate formulations, Ch 7,

    pp 3, 10, 16in coal fly ash, Ch 9, pp 3134in feeds, Ch 5, p 5; Ch 14, p 1 in food, Ch 9, pp 13, 9 in iron methylarsenate, Ch 18, p 5 in iron-arsenic tablets, Ch 18, p 5 in lead arsenate formulations, Ch 9,

    pp 9, 15 in liver tissue, Ch 14, p 1in magnesium arsenate, Ch 7, p 3 in meat, Ch 39, p 5in meat and poultry, Ch 9, p 9 in Paris green pesticides, Ch 7, p 8in pesticide formulations, Ch 7, pp 23,

    810in plants, Ch 3, p 13 in sodium cacodylate, Ch 18, p 5in solid wastes, Ch 9, pp 3134in wastewater, Ch 9, pp 3444 in water, Ch 11, pp 23, 24 in zinc arsenite, Ch 7, pp 1011

    Arsenic oxide in lead arsenate formulations, Ch 7, p 9

    Arsenious oxide in Bordeaux mixtures, Ch 7, p 15 in calcium arsenate formulations, Ch 7,

    p 10 in lead arsenate formulations, Ch 7, p 9 in Paris green pesticide, Ch 7, p 8in pesticide formulations, Ch 7, pp 910

    standard solutions, App A, p 2in zinc arsenite formulations, Ch 7, p 11

    Arsenic trioxide safe handling of, App B, p 6

    Arsenious oxide titration methods chlorine in calcium hypochlorite and

    bleaching powder, Ch 7, p 18 sodium hypochlorite in pesticide formu-

    lations, Ch 7, p 18-Asarone

    in wines, Ch 28, p 15ASBCAOAC methods

    aphids in hops, Ch 16, pp 78calcium in beer, Ch 27, pp 1011ethanol in beer, Ch 27, pp 45extract of barley for malting, Ch 27, p 21glycerol in beer, Ch 27, p 6moisture in malting barley, Ch 27, p 21N-nitrosodimethylamine in beer, Ch 27,

    pp 1516 specific gravity of beer and wort, Ch 27,

    p 3Asbestos

    safe handling of, App B, p 7Ascorbic acid, see Vitamin CAsh

    of baked products, Ch 32, p 36in baking powders, Ch 25, p 5 of beer, Ch 27, p 8Aof bread, Ch 32, p 34of brewing sugars and sirups, Ch 27,

    p 35of butter, Ch 33, p 56Eof cacao products, Ch 31, pp 12, 8of canned vegetables, Ch 42, p 6of cereal adjuncts, Ch 27, p 31of cheese, Ch 33, p 59of confectionery, Ch 44, p 18 of cordials and liqueurs, Ch 26, p 20of corn sirups and sugars, Ch 44, p 40of cream, Ch 44, p 1of distilled liquors, Ch 26, p 6of dried milk, Ch 44, p 18of evaporated milk, Ch 44, p 22of feeds, Ch 4, p 4 of flour, Ch 32, p 2of fruits and fruit products, Ch 37, p 7of grains, Ch 32, p 22of honey, Ch 44, p 21of lemon, orange, and lime extracts,

    Ch 36, p 14of macaroni products, Ch 32, p 38of maple products, Ch 44, p 32of meat extracts and similar products,

    Ch 39, p 23of meat, Ch 39, p 4of milk, Ch 33, p 10in mineral oil-soap emulsions, Ch 7,

    pp 1920of molasses, Ch 44, p 15

    of nonalcoholic beverages, Ch 29, p 1of nuts and nut products, Ch 40, p 2 in peat, Ch 2, p 37 of plants, Ch 3, p 1 of roasted coffee, Ch 30, p 2of seafood, Ch 35, p 6of soybean flour, Ch 32, p 30of spices, Ch 43, p 2of sugars and sirups, Ch 44, p 3of sweetened condensed milk, Ch 33,

    p 54 of tea, Ch 30, pp 1112of vanilla extract, Ch 36, p 6 of vinegars, Ch 43, p 11of wines, Ch 28, p 6

    Aspirin antihistamines in drugs with, Ch 18,

    pp 2021, 58chemical name, Ch 18, p 58; Ch 19,

    p 35microchemical tests, Ch 18, p 49 and phenacetin and caffeine in drugs,

    Ch 19, pp 1011 and phenacetin and phenyl salicylate in

    drugs, Ch 19, p 11 and phenobarbital in drugs, Ch 19,

    pp 1112 and phenolphthalein in tablets, Ch 19,

    p 12ASTMAOAC methods

    cadmium and lead in earthenware, Ch 9,p 6B

    cation exchange capacity for peat, Ch 2,p 39

    extractives from flexible barrier materi-als, Ch 48, pp 45

    ASTMIntersociety CommitteeAOACmethods

    fluoride in plants, Ch 3, pp 1520Atomic absorption spectrophotometricmethods

    aluminum in baking powders, Ch 25, pp 45

    aluminum in soil acidifiers, Ch 2, p 35 arsenic, selenium, and zinc in food,

    Ch 9, pp 23 biuret in fertilizers, Ch 2, pp 1920boric acid in food, Ch 47, p 14cadmium and lead in earthenware, Ch 9,

    p 6Bcadmium in food, Ch 9, pp 910cadmium in water, Ch 11, pp 1517 calcium in fertilizers, Ch 2, pp 2526,

    2728 calcium, magnesium, and phosphorus in

    cheese, Ch 33, pp 5960chromium in water, Ch 11, pp 1517 copper and nickel in tea, Ch 9, pp 89 copper in distilled liquors, Ch 26, pp 67copper in fertilizers, Ch 2, pp 2526, 29

    1998 AOAC INTERNATIONAL

  • copper in fungicides, Ch 7, p 11 copper in liver, Ch 14, pp 12 copper in serum, Ch 14, p 2 copper in water, Ch 11, pp 1517copper, iron, and nickel in edible oils

    and fats, Ch 9, pp 78 dibutyltin dilaurate in feeds, Ch 5, pp 89 iron, copper, and nickel in edible oils

    and fats, Ch 9, pp 78iron in distilled liquors, Ch 26, p 8iron in fertilizers, Ch 2, pp 2526, 29iron in iron chelate concentrates, Ch 2,

    p 30 iron in water, Ch 11, pp 1517 lead and cadmuim extracted from

    ceramicware, Ch 9, pp 6A6Blead in edible oils and fats, Ch 41,

    pp 99Blead in evaporated milk, Ch 9, p 16 lead in fish, Ch 9, p 18 lead in food, Ch 9, p 19 lead in paint, Ch 8, pp 23lead in water, Ch 11, pp 1517 magnesium in fertilizers, Ch 2,

    pp 2526, 30magnesium in water, Ch 11, pp 1517 manganese in fertilizers, Ch 2,

    pp 2526, 31, 32 mercury in mercury-containing drugs,

    Ch 18, pp 1214 mercury in water, Ch 11, pp 1718 mercury (methyl) in seafood, Ch 9,

    pp 2628metals in plants and pet foods, Ch 3, p 3minerals in animal feed, Ch 4, p 31minerals in ready-to-feed milk-based

    formulas and pet foods, Ch 50,p 14

    nickel, copper, iron and, in edible oilsand fats, Ch 9, pp 78

    nickel in tea, Ch 9, p 28 nutrients in fertilizers, Ch 2, pp 2526,

    2932potassium in beer, Ch 27, p 19 potassium in water, Ch 11, pp 1920roxarsone in feeds and premixes, Ch 5,

    pp 2223 silver in water, Ch 11, pp 1517 sodium in beer, Ch 27, p 19sodium in fertilizers, Ch 2, pp 3233 tin in food, Ch 9, pp 2930 zinc in fertilizers, Ch 2, p 33 zinc in food, Ch 9, p 31 zinc in water, Ch 11, pp 1517

    Atomic absorption spectrophotometric-flame photometric methods

    calcium, potassium, and sodium in elec-trolyte replenishers, Ch 18,pp 910

    zinc in serum, Ch 14, pp 23

    Atomic weights, App C, p 2 (vol 1)Atraton

    in finished drinking water, Ch 10, pp 2630

    Atrazines, Ch 7, pp 4041in finished drinking water, Ch 10,

    pp 2630in water, Ch 10, pp 3132B

    Atrazine dealkylatedin water, Ch 10, pp 6164

    Atropine sulfate, Ch 20, p 2Atropine, Ch 18, pp 45, 48; Ch 20,pp 2, 6, 32Automated methods

    acenocoumarol, dicumarol, phenpro-coumon, warfarin potassium, andwarfarin sodium in drugs, Ch 19,pp 2022

    carbon, hydrogen, and nitrogen determi-nation, Ch 12, pp 56

    2,4-D in formulations, Ch 7, p 63 digoxin in drugs, Ch 20, pp 2627 fat in milk, Ch 33, pp 2226fluoride in plants, Ch 3, pp 1520 lysine in nutritional supplements, Ch 45,

    pp 6566methenamine and methenamine mande-

    late in drugs, Ch 18, pp 4142 niacin and niacinamide in cereal prod-

    ucts, Ch 45, pp 1314niacin and niacinamide in foods, drugs,

    and feeds, Ch 45, pp 1415nitrogen in meat, Ch 39, p 7 nitrogen in plants, Ch 3, p 24 phenylephrine HCl in drugs, Ch 18,

    pp 2324phosphorus in fertilizers, Ch 2, pp 79 phosphorus in meat, Ch 39, p 4phosphorus in water, Ch 11, pp 2122 potassium in fertilizers, Ch 2, pp 2223 protein in feeds, Ch 4, p 15protein in grains, Ch 32, pp 2324riboflavin in foods and vitamin prepara-

    tions, Ch 45, pp 1012Azide method

    oxygen (dissolved) in water, Ch 11, p 5Azinphos-methyl

    in formulations, Ch 7, pp 7981 residues on cole-type crops and fruits,

    Ch 10, p 39Babcock methods

    essential oil in flavor extracts and toiletpreparations, Ch 36, p 20

    fat in cream, Ch 33, pp 5052fat in raw milk, Ch 33, pp 1921fat in seafood, Ch 35, p 10

    Baby foodsnitrate in, Ch 50, pp 1112Bacillus anthracis differentiation from

    B. cereus, Ch 17, pp 5455

    Bacillus cereus differentiation from other strains, Ch 17,

    pp 5455 enumeration and confirmation in foods,

    Ch 17, pp 5254Bacillus stearothermophillus

    in sugars, Ch 17, p 44Bacillus stearothermophilus disc methods

    -lactam antibiotics, Ch 23, pp 1819-lactam antibiotics in milk, Ch 23, p 18

    Bacillus subtilis qualitative field disk assay

    -lactam antibiotics in milk, Ch 23, p 18Bacillus thuringiensis

    differentiation from B. cereus, Ch 17,pp 5455

    Bacitracin in feeds, Ch 5, pp 3031, 3638

    BacitracinMD (BMD)in complete feed, microbiological plate

    assay method, Ch 5, pp 3738 Bacon

    N-nitrosamines (volatile) in, Ch 39, pp 911

    N-nitrosopyrrolidine in, Ch 39, pp 1112

    Bacteria in foods and cosmetics, Ch 17, pp 56population of maple sap, Ch 44,

    pp 3637Bacteria count

    in dairy products, Ch 17, pp 12C12Ein milk, Ch 17, pp 12B12Din raw milk, Ch 17, pp 68

    Bacterial colony counts dairy products, Ch 17, pp 12C13

    Bacteriostatic activity of disinfectants, Ch 6, pp 17, 1516of laundry additives, Ch 6, pp 1516

    Bagoong saucelight filth from fish paste and sauce not

    containing spice, Ch 16, p 26Bailey-Andrew methods

    caffeine in roasted coffee, Ch 30, pp 23

    caffeine in tea, Ch 30, pp 1213Baked products

    acetic and propionic acids in cake, Ch 32, p 36

    ash of, Ch 32, p 36extraneous materials in, Ch 16, pp 2022fat in, Ch 32, p 36fat in fig bars and raisin filled crackers,

    Ch 32, p 37fiber (crude) in, Ch 32, p 36filth in, Ch 16, pp 2021 mineral oil in, Ch 32, pp 3536moisture in fig bars and raisin filled

    crackers, Ch 32, pp 3637

    1998 AOAC INTERNATIONAL

  • pH of, Ch 32, p 36protein in, Ch 32, p 36solids in, Ch 32, p 36sterols (as cholesterol) in, Ch 32, p 36sugars in, Ch 32, p 36

    Baking chemicals neutralizing values, Ch 25, p 2preparation of sample, Ch 25, p 1

    Baking powders aluminum in, Ch 25, pp 45carbon dioxide in, Ch 25, pp 12metals and other constituents in, Ch 25,

    p 5 phosphorus in, Ch 25, p 6preparation of sample, Ch 25, p 1 starch in, Ch 25, pp 34tartaric acid in, Ch 25, p 3

    Baking premixes acetone peroxides in, Ch 47, pp 4041

    Barbanin water, Ch 10, pp 6164

    Barbital, Ch 18, pp 47, 49Barbiturates

    in drugs, Ch 18, pp 4750 optical crystallographic properties,

    App C, p 4 (vol 1) refractive indices, App C, pp 1415 (vol 1)

    Barbituric acid condensation method citral in flavor extracts and toilet prepa-

    rations, Ch 36, pp 2021Barium

    in coal fly ash, Ch 9, pp 3134in plants, Ch 3, pp 2, 4 in solid wastes, Ch 9, pp 3134in waters and wastewaters, Ch 9,

    pp 3444in water, Ch 11, pp 1819

    Barium-140 in milk, Ch 13, pp 68

    Barium hydroxide treatment acidity of wines exclusive of SO2,

    Ch 28, p 9Barium sulfate

    in face powders, Ch 15, p 8Barley

    filth in cereals, Ch 16, p 23 -D-glucan in, Ch 32, pp 3132Bfor malting, Ch 27, p 21ochratoxin A in corn and, Ch 49, pp 4041ochratoxins in, Ch 49, pp 3839piperonyl butoxide pesticide residues in,

    Ch 10, p 59 sterigmatocystin in, Ch 49, pp 44A44B

    Bathocuproine method copper in fungicides, Ch 7, pp 1112

    Bay leaves filth in, Ch 16, pp 3840

    Beans hydrocyanic acid in, Ch 49, pp 4849weevils in, Ch 16, p 31

    see also Green beansBean curd

    light filth, Ch 16, p 33Bean paste

    light filth, Ch 16, pp 3132Beef

    adulteration of meat products, Ch 39, p 22

    calcium in mechanically separated meat,Ch 39, p 15

    filth in ground beef or hamburger, Ch 16, pp 2627

    preservatives in ground meat, Ch 47, pp 1011

    virus in, Ch 17, pp 115116 see also Meat and meat products

    Beer acidity of, Ch 27, p 6 acids (volatile), Ch 27, p 6alcohol in, Ch 27, p 4ash of, Ch 27, p 8bitterness of, Ch 27, pp 1415calcium in, Ch 27, pp 1011caloric content, Ch 27, p 6caramel in, Ch 27, p 14carbohydrate content, Ch 27, p 6carbon dioxide in, Ch 27, pp 89 chlorides in, Ch 27, p 13color of, Ch 27, p 1copper in, Ch 27, pp 1112deliverable contents of in bottles and

    cans, Ch 49, pp 4041dextrin, Ch 27, pp 1011diacetyl in, Ch 27, p 10ethanol in, Ch 27, pp 45 extract, Ch 27, p 3 fermentation of, Ch 27, p 5 foam collapse rate, Ch 27, pp 910glycerol in, Ch 27, p 6haze after chilling, Ch 27, p 3iron in, Ch 27, pp 1213nitrogen (free amino) in, Ch 27, p 8N-nitrosodimethylamine in, Ch 27,

    pp 1516pH of, Ch 27, p 6phosphorus in, Ch 27, p 8potassium in, Ch 27, p 19protein in, Ch 27, p 8proteolytic chillproofing enzymes in,

    Ch 27, p 15sample preparation, Ch 27, p 1sodium in, Ch 27, p 19specific gravity, Ch 27, p 4starch (unconverted) in, Ch 27, p 8sugars (reducing), Ch 27, p 7sulfur dioxide in, Ch 27, pp 1314 viscosity, Ch 27, p 3

    Belladonna, Ch 20, p 6Bellier test

    peanut oil in olive, cottonseed, corn, andsoybean oils, Ch 41, p 38

    Bemegride, Ch 18, pp 47, 58Bendiocarb, Ch 7, pp 2425Bendroflumethiazide, Ch 19, pp 27, 35Benedict solution method

    lactose in meat, Ch 39, pp 2021Benfluralin, Ch 7, pp 5758Benomyl, Ch 7, p 25Bentazon, Ch 7, p 36

    in finished drinking water, Ch 10, pp 6772A

    Benzaldehyde in almond extract, Ch 36, pp 1718in cordials and liqueurs, Ch 26, p 21in nonalcoholic beverages, Ch 29, p 2

    Benzene safe handling of, App B, p 5

    Benzene hexachloride in formulations, Ch 7, pp 5657residues, Ch 10, pp 39, 5153

    Benzocaine, Ch 18, pp 2829, 49, 58Benzoic acid

    in almond extract, Ch 36, p 18chemical name, Ch 18, pp 49, 58 in flour, Ch 32, pp 1718in food, Ch 47, pp 710in nonsolid food and beverages, Ch 47,

    p 8in orange juice, Ch 37, pp 2223

    Benzoquinone method hair preparations, Ch 15, p 9

    Benzoyl peroxide bleach in flour, Ch 32, pp 1718

    Benzo[a]pyrene in food, Ch 48, pp 14

    Benzthiazide, Ch 19, pp 2930, 35Benztropine mesylate, Ch 20, pp 67, 32Benzylmorphine, Ch 18, p 45Berberine, Ch 18, pp 45, 58Berlin Institute method

    invert sugar in sugars and sirups, Ch 44,pp 910

    Berry fruits seeds in, Ch 37, p 6

    Berylliumin coal fly ash, Ch 9, pp 3134in solid wastes, Ch 9, pp 3134in wastewater, Ch 9, pp 3444

    BetaDGlucansin barley and oats, Ch 32, pp 3132Bin oat and barley fractions and readyto

    eat cereals, Ch 32, pp 2328Beta particle counting method

    strontium-90 in water, Ch 13, pp 23 Betaine

    in orange juice, Ch 37, p 10

    1998 AOAC INTERNATIONAL

  • Beverages benzoic acid in, Ch 47, p 8quaternary ammonium compounds in,

    Ch 47, pp 2122salicyclic acid in, Ch 47, pp 2324see also Alcoholic beverages; Distilled

    liquors; Malt beverages and brew-ing materials; Nonalcoholic bever-ages and concentrates; andSpecific beverages

    BF method aflatoxins in peanuts and peanut prod-

    ucts, Ch 49, p 10-BHC

    in lettuce, strawberries, and tomatoes,Ch 10, pp 1011

    in water, Ch 10, pp 1317BHC

    in water, Ch 10, pp 1317BHC

    in formulations, Ch 7, pp 5356in water, Ch 10, pp 1317

    BHCin water, Ch 10, pp 1317

    Bicarbonate in water, Ch 11, p 13

    Bifuran in feeds, Ch 5, p 12

    Bioassay methods chick edema factor in oils and fats,

    Ch 41, pp 4142eye irritants in cosmetics, Ch 15, p 3 paralytic shellfish poison, Ch 35, pp 22vitamins and other nutrients, Ch 45,

    pp 5363Biochemical identification kit methods

    E. coli in foods, Ch 17, pp 6364 Enterobacteriaceae in foods, Ch 17,

    pp 6364 Salmonella sp. in foods, Ch 17,

    pp 6264Biochemical oxygen demand

    of water, Ch 11, pp 35Biological samples

    copper in serum, Ch 14, p 2Biphenyl

    in citrus fruits, Ch 10, pp 3940Bismuth

    in drugs, Ch 18, pp 56Bismuthate methods

    manganese in fertilizers, Ch 2, p 32 manganese in water, Ch 11, pp 2324

    Bitartrate method tartaric acid in fruit and fruit products,

    Ch 37, p 11Bithionol

    in feeds, Ch 5, p 6Bitterness

    of beer, Ch 27, pp 1415

    Bitterness units method bitterness of beer, Ch 27, p 14

    Biuret in fertilizers, Ch 2, pp 1920

    Biuret test protein in feeds, Ch 4, p 12

    Blackberries insects in frozen products, Ch 16,

    pp 2728 mold in, Ch 16, pp 6162

    Bleaching powder chlorine in, Ch 7, p 18

    Block digestion method protein (crude) in meat, Ch 39, pp 78

    Bloodcholinesterase in, Ch 14, pp 34

    Blueberries maggots in, Ch 16, p 28

    Bone fertilizers, Ch 2, p 3Borates in food, Ch 47, p 11Bordeaux mixtures

    arsenic in, Ch 7, pp 3, 1516arsenious oxide in, Ch 7, p 15with calcium arsenate, Ch 7,

    pp 3, 45, 16 carbon dioxide in, Ch 7, pp 1516 copper in, Ch 7, pp 4, 1516with lead arsenate, Ch 7, pp 45, 1516 lead in, Ch 7, pp 4, 16 moisture in, Ch 7, pp 14, 15, 16 with Paris green, Ch 7, pp 45, 15 with zinc arsenate, Ch 7, pp 45, 11

    Boric acid in antiperspirants and deodorants,

    Ch 15, pp 56 in face powders, Ch 15, p 8 in food, Ch 47, pp 11, 12, 1314in meat, Ch 47, p 12in water, Ch 11, pp 23, 24

    Boron in caviar, Ch 47, pp 1112 in fertilizers, Ch 2, pp 2627 in plants, Ch 3, pp 24, 13

    Boron trifluoride method fatty acids in oils and fats, Ch 41,

    pp 1718Bovine milk

    multiple sulfonamide residues in, Ch 23,pp 1316

    multiple tetracycline residues in, Ch 33,pp 4347

    sulfamethazine residues in, Ch 23, pp 1113

    Brazil nutsaflatoxins in, Ch 49, pp 2424A

    Breaded fish products fish content, Ch 35, pp 12 fish flesh content in frozen coated fish,

    Ch 35, p 10

    Breading filth in, Ch 16, pp 2122

    Breads acetic and propionic acids in, Ch 32,

    pp 3233acids (volatile) in, Ch 32, pp 3334ash of, Ch 32, p 34calcium in, Ch 32, p 34chloride in ash of, Ch 32, p 34citric acid in, Ch 32, p 34fat and fat number, Ch 32, p 32Bfat in, Ch 32, p 34fiber (crude) in, Ch 32, p 34fiber (total dietary), Ch 45, p 70filth in, Ch 16, pp 2021 iron in, Ch 32, p 34lactose in, Ch 32, p 35pH of, Ch 32, p 35protein in, Ch 32, p 34sample preparation, Ch 32, p 32Asolids (total) in, Ch 32, p 32Bsterols (as cholesterol) in, Ch 32, p 34sugars in, Ch 32, p 35 thiamine in, Ch 45, pp 89vitamins in enriched bread, Ch 32, p 34

    Breakfast cereals extraneous materials in, Ch 16,

    pp 2223 see also Cereal foods

    Brewers grits, Ch 16, p 15Brewers grains, Ch 27, pp 3839Brewing materials, see Malt beveragesand brewing materialsBrillant lake red R, Ch 46, p 7Brilliant blue FCF, Ch 46, pp 12, 4 Brine flotation method

    filth in corn meal, Ch 16, pp 1617Brine saturation method

    filth in sage, Ch 16, pp 4344Broccoli

    filth in canned products, Ch 16, p 34Brodifacoum, Ch 7, p 97Bromacil

    in finished drinking water, Ch 10, pp 2630

    Bromate titration resorcinol in hair lotions, Ch 15, p 9 salicylic acid in hair lotions, Ch 15, p 9

    Bromates in white and whole wheat flour, Ch 32,

    pp 1819Bromides

    in dosage forms, Ch 18, pp 910in water, Ch 11, pp 24, 2830

    Brominated vegetable oils in nonalcoholic beverages, Ch 47,

    pp 4142Bromination methods

    benzocaine in drugs, Ch 18, pp 2829 dinitrophenol in drugs, Ch 19, p 3

    1998 AOAC INTERNATIONAL

  • phenolsulfonates in deodorants, Ch 15,p 7

    phenolsulfonates in drugs, Ch 19, p 6 sterols in macaroni products, Ch 32, p 39 thiouracil in drugs, Ch 19, p 31

    Brominemicrochemical methods, Ch 12, pp 13safe handling of, App B, p 5 in water, Ch 11, p 23

    Bromisovalum, Ch 19, pp 13, 35Bromophenol blue methods

    quaternary ammonium compounds infood and beverages, Ch 47,pp 2122

    quaternary ammonium compounds inmilk, Ch 47, p 19

    Bromoxynil octanoate in formulations, Ch 7, p 58

    Brucine, Ch 18, pp 45, 58Brucine colorimetric method

    nitrogen (nitrate) in water, Ch 11, pp 1011Bufencarb

    in grapes and potatoes, Ch 10, pp 3639Buffer solutions

    for calibration of pH equipment, App A,pp 23

    for colorimetric pH comparisons, App A,p 3

    Buquinolate in feeds, Ch 5, p 6

    Bushel weight malt, Ch 27, p 9

    Butabarbital sodium, Ch 18, pp 47, 58;Ch 19, pp 17, 35Butacaine sulfate, Ch 18, pp 2930, 58Butachlor, Ch 7, pp 5959

    in finished drinking water, Ch 10, pp 2630

    Butalbital, Ch 18, pp 47, 58Butethal, Ch 18, pp 47, 58Butter

    acids (volatile) in, Ch 33, p 57butyric acid in, Ch 33, pp 56G57casein, ash, and salt in, Ch 33,

    pp 56F56Gcritical temperature of dissolution of oil

    from, Ch 33, p 56F examination of fat, Ch 33, p 56Efat in, Ch 33, p 56Efatty acids in, Ch 33, pp 56G56Hfilth in, Ch 16, p 11 moisture in, Ch 33, p 56Emold in, Ch 16, p 65; Ch 33, p 57phosphatase in, Ch 33, p 57preservatives in, Ch 33, p 57salt in, Ch 33, p 56Esample preparation, Ch 33, pp 56D56Esampling, Ch 33, pp 3, 56D

    Butter oil-sitosterol in, Ch 41, pp 3435

    Butterfat acid value of, Ch 33, p 56F color additives in, Ch 33, p 56Flactic acid in, Ch 33, p 56Frefractive index of, Ch 33, p 56Fvegetable fats in, Ch 41, pp 3233

    n-Butyl alcohol in distilled liquors, Ch 26, pp 1213

    Butylate in finished drinking water, Ch 10,

    pp 2630in herbicide formulations, Ch 7,

    pp 3132Butylated hydroxyanisole

    in cereals, Ch 47, pp 56in foods, Ch 47, pp 12in oils and fats, Ch 47, pp 25

    Butylated hydroxytoluene in cereals, Ch 47, pp 56in foods, Ch 47, pp 12 in oils and fats, Ch 47, pp 25

    2-(p-tert-Butylphenoxy)-1-methyl 2-chloroethyl sulfite (aramite) residues,Ch 10, p 40Butyric acid

    in bread, Ch 32, pp 3334in butter, Ch 33, pp 56G57 in fat, Ch 41, pp 1213in fats containing butterfat, Ch 41,

    pp 2829in seafood, Ch 35, pp 1314

    Cabbage N-methylcarbamate residues on, Ch 10,

    pp 32C33nicotine residues in, Ch 10, pp 5758

    Cacao bean and its products aflatoxins in cocoa beans, Ch 49, p 12alginates in chocolate beverages, Ch 29,

    p 7alginates in, Ch 31, p 16alkalinity of insoluble and soluble ash of,

    Ch 31, p 2ash of, Ch 31, pp 12, 8caffeine in, Ch 31, pp 1617chocolate liquor, cacao mass, Ch 31, p 8crude fiber in, Ch 31, p 3fat in, Ch 31, pp 811filth in, Ch 16, pp 67 fructose, glucose, lactose, maltose, and

    sucrose in milk chocolate, Ch 31,p 13

    glucose in, Ch 31, pp 1315lactose in milk chocolate, Ch 31,

    pp 1213milk fat in milk chocolate, Ch 31, p 12moisture in, Ch 31, p 1nitrogen in, Ch 31, p 2pectic acid in, Ch 31, pp 35pH of, Ch 31, p 2

    protein in milk chocolate, Ch 31, p 12

    Salmonella in chocolate, Ch 17, pp 5860, 6971, 9193

    sample preparation, Ch 31, p 1shell in, Ch 31, p 3spiral vessel count of, Ch 31, pp 56starch in, Ch 31, pp 1516 stone cell and group count of, Ch 31,

    pp 68sucrose in, Ch 31, pp 1314threobromine in, Ch 31, pp 1617

    Cacao fat coconut and palm kernel oils in cocoa

    butter and fat from milk chocolate,Ch 31, p 11

    critical temperature for dissolution inacetic acid, Ch 31, p 11

    index of refraction, Ch 31, p 10iodine absorption number, Ch 31, p 10lecithin in, Ch 31, pp 1112melting point, Ch 31, p 10milk fat in milk chocolate, Ch 31, p 11Reichert-Meissl and Polenske values,

    Ch 31, p 10saponifieation number, Ch 31, p 11separation of, Ch 31, p 10silver number for coconut and palm ker-

    nel oils, Ch 31, p 11unsaponifiable matter in cocoa butter,

    Ch 31, p 11Cacodylate injections

    arsenic in, Ch 18, p 5Cadmium

    in coal fly ash, Ch 9, pp 3134in cookware, Ch 9, pp 56in earthenware, Ch 9, pp 66Ain feeds, Ch 5, p 6 in food, Ch 9, pp 9, 15, 910 in foodware, Ch 9, pp 66Aand lead extracted from ceramicware,

    Ch 9, pp 6A6Bin solid wastes, Ch 9, pp 3134in wastewaters, Ch 9, pp 3444 in water, Ch 11, pp 1517

    Cadaverinein canned tuna, Ch 16, pp 27

    Caffeine, Ch 19, p 35; Ch 20, p 32acetanilid in drugs with, Ch 19, pp 910 aminopyrine in drugs with, Ch 19,

    p 11antihistamines in drugs with, Ch 18,

    pp 2021aspirin in drugs with, Ch 19, pp 1011 in cacao products, Ch 31, pp 1617codeine in drugs with, Ch 19, p 9 in green coffee, Ch 30, p 1microchemical tests, Ch 18, p 53 morphine in drugs with, Ch 19, p 10 in nonalcoholic beverages, Ch 29, p 4

    1998 AOAC INTERNATIONAL

  • phenacetin in drugs with, Ch 19, pp 1011phenobarbital in drugs with, Ch 19,

    pp 1112 with potassium bromide in drugs, Ch 18,

    p 8quinine in drugs with, Ch 19, p 10 in roasted coffee, Ch 30, pp 23in tea, Ch 30, pp 1213

    Calciumin baking powders, Ch 25, p 5in beer, Ch 27, pp 1011in bread, Ch 32, p 34in calcium arsenate formulations, Ch 7,

    p 10 in canned vegetables, Ch 42, p 6in coal fly ash, Ch 9, pp 3134in face powders, Ch 15, p 8in feeds, Ch 4, p 32 in fertilizers, Ch 2, pp 2526, 27-28, in flour, Ch 32, p 4in fruits and fruit products, Ch 37, p 8in infant formulas, Ch 50, pp 1416in lime sulfur formulations, Ch 7, p 17 in liming materials, Ch 1, pp 5, 6 in magnesic limestone, Ch 1, pp 12 with magnesium in drugs, Ch 18,

    p 7with magnesium amd phosphorus in

    cheese, Ch 33, pp 5960 in mechanically separated poultry and

    beef, Ch 39, p 15with phosphorus and iron in vitamin

    preparations, Ch 18, p 8with potassium and sodium in electrolyte

    replenishers, Ch 18, pp 910in plants, Ch 3, pp 24, 5 in ready-to-feed milk-based infant for-

    mulas and pet foods, Ch 50,pp 1516

    safe handling of, App B, p 3in salt, Ch 11, p 31in solid waste, Ch 9, pp 3134in water, Ch 11, p 15in waters and wastewaters, Ch 9,

    pp 3444Calcium arsenate

    Bordeaux mixtures with, Ch 7, pp 4, 16 formulations, Ch 7, pp 3, 10

    Calcium bromide, Ch 18, pp 910Calcium carbonate

    in calcium silicate slags, Ch 1, pp 34Calcium cyanide formulations, Ch 7, p 16Calcium cyclamate

    in canned fruit, Ch 47, p 44in nonalcoholic beverages, Ch 47, p 43

    Calcium gluconate, Ch 18, pp 78Calcium hypochlorite

    chlorine in, Ch 7, p 18

    Calcium oxalate precipitate method oxalic acid in canned vegetables, Ch 42,

    pp 89Calcium oxide

    in liming materials, Ch 1, pp 2, 5safe handling of, App B, p 4

    Calcium pantothenate in vitamin preparations, Ch 45, p 40

    Calcium salicylate drugs, Ch 20, p 7 Calcium silicate slags, Ch 1, pp 34

    sulfide sulfur in, Ch 1, p 4 Calculation method

    protein efficiency ratio, Ch 45,pp 5961

    Calomel mercury in, Ch 18, pp 1415 in ointments, Ch 18, p 16

    Caloric content of beer, Ch 27, p 6of wines, Ch 28, p 6

    Cambridge filter pads nicotine on, Ch 3, pp 3132

    Camphor, Ch 20, pp 2728, 32Canadian lead number

    of maple products, Ch 44, p 33Candling procedures

    parasites in fish muscle, Ch 35, pp 2425

    Candy filth in, Ch 16, p 30 Salmonella in, Ch 17, pp 6769

    Cannabinol, Ch 22, pp 4, 6Canned food containers

    microleak detection, Ch 17, pp 42B44Canned foods

    low-acid, commercial sterility, Ch 17,pp 4146

    tin in, Ch 9, pp 2930 see also specific foods and food groups

    Capillary gas chromatographic methodcis- and trans-octadecenoic isomers and

    general fatty acid composition inhydrogenated vegetable oils andanimal fats, Ch 41, pp 2627A

    Capillary tube method melting point of fats and fatty acids,

    Ch 41, p 4Capsicums

    capsaicinoids in, Ch 43, pp 1315filth in, Ch 16, pp 4142 in ginger extract, Ch 36, p 19

    Captan in formulations, Ch 7, pp 5960residues in firm fruits, Ch 10, p 41

    Caramel in beer, Ch 27, p 14in cordials and liqueurs, Ch 26, p 21

    Caraway extract, Ch 36, p 20Caraway seed

    filth in, Ch 16, pp 3840

    foreign matter in, Ch 16, p 39Carbadox

    in feeds, Ch 5, pp 67Carbamate pesticides

    aldicarb, Ch 7, p 22; Ch 10, pp 3639aminocarb, Ch 7, p 23 anilazine, Ch 7, p 24bendiocarb, Ch 7, pp 2425 benomyl, Ch 7, p 25 bufencarb, Ch 10, pp 3639carbanolate, Ch 10, pp 32C33 carbaryl, Ch 10, pp 32C33 carbofuran, Ch 7, pp 2627; Ch 10,

    pp 32C33 dithiocarbamates, Ch 7, p 28Ain finished drinking water, Ch 10,

    pp 3336methiocarb, Ch 7, pp 2930; Ch 10,

    pp 3639 methomyl, Ch 10, pp 3639 N-methylcarbamate, Ch 10,

    pp 3139 oxamyl, Ch 10, pp 3339 pirimicarb, Ch 7, pp 3031 thiocarbamates in herbicide formula-

    tions, Ch 7, pp 3132 thiram, Ch 7, pp 3233triadimefon, Ch 7, pp 3334

    Carbanolate on apples, cabbage, collards, corn ker-

    nels, green beans, kale, and turniptops, Ch 10, pp 32C33

    Carbanthrene blue, Ch 46, p 6Carbaryl

    on apples, cabbage, collards, corn ker-nels, green beans, kale, and turniptops, Ch 10, pp 32C33

    in apples and spinach, Ch 10, pp 4243 in grapes and potatoes, Ch 10, pp 3639

    Carbidopa, Ch 19, pp 1314, 35Carbofuran

    on apples, cabbage, collards, corn ker-nels, green beans, kale, and turniptops, Ch 10, pp 32C33

    in formulations, Ch 7, pp 2627 in grapes and potatoes, Ch 10, pp 3639

    Carbofuran phenolin water, Ch 10, pp 6164

    Carbohydrate content of beer, Ch 27, p 6of soluble (instant) coffee, Ch 30, p 511of fruit juices, Ch 37, pp 1415of wines, Ch 28, p 5

    Carbon in fertilizers, Ch 2, p 28 and hydrogen and nitrogen, microchem-

    ical determination, Ch 12, pp 56 and hydrogen, microchemical determi-

    nation, Ch 12, pp 35

    1998 AOAC INTERNATIONAL

  • Carbon column cleanup method organophosphorus pesticide residues,

    Ch 10, pp 2122Carbon dioxide

    in baking powders, Ch 25, p 1 in beer, Ch 27, p 8A in Bordeaux mixtures, Ch 7, pp 15, 16correction factors for gasometric deter-

    mination of, App C, pp 2930 (vol 2)

    density, App C, p 28 (vol 2) in liming materials, Ch 1, pp 23in self-rising flour, Ch 32, p 5in wines, Ch 28, pp 1113

    Carbon disulfide in fumigant mixtures, Ch 7, pp 2122 safe handling of, App B, p 5

    Carbon disulfide evolutionmethods

    dithiocarbamates in formulations, Ch 7,pp 2829

    maneb in pesticide formulations withfentin acetate or fentin hydroxide,Ch 7, pp 1314

    Carbon ratio mass spectrometric methods corn sirups and sugars in honey, Ch 44,

    pp 2729corn syrup and cane sugar in maple

    syrup, Ch 44, pp 3233corn syrup in apple juice, Ch 37, pp 1920corn syrup in orange juice, Ch 37, p 20

    Carbon stable isotope ratio methodscorn-derived acetic acid in apple cider

    vinegar, Ch 37, pp 21A22Carbon tetrachloride in drugs, Ch 18, p 2 in fumigant mixtures, Ch 7, pp 2122 safe handling of, App B, p 5 in wheat and corn grain, Ch 10, p 32B

    Carbonates in fertilizers, Ch 2, p 28in water, Ch 11, p 13

    Carbophenothion on apples and green beans, Ch 10,

    pp 2122 on apples, carrots, endive, kale, lettuce,

    potatoes, and strawberries, Ch 10,pp 2224

    Carboxinin finished drinking water, Ch 10,

    pp 2630Carbromal, Ch 19, pp 1314, 35Carcinogens

    safe handling of, App B, p 7Cardamon

    filth in, Ch 16, pp 3840, 42 foreign matter in, Ch 16, p 39

    Carius combustion methods bromine, chlorine, or iodine determina-

    tion, Ch 12, pp 13 sulfur determination, Ch 12, pp 1011

    Carmel in wines, Ch 28, p 11

    Carotenes in dried plant materials and mixed feeds,

    Ch 45, pp 56in fresh plant materials and silages,

    Ch 45, pp 45in macaroni products, Ch 32, pp 4041in plants, Ch 3, p 28

    Carotenoids in eggs, Ch 34, p 1in macaroni products, Ch 32, pp 4042

    Carrotsorganophosphorus pesticide residues on,

    Ch 10, pp 2224Casein

    in butter, Ch 33, p 56Ein evaporated milk, Ch 33, p 53in malted milk and chocolate malted

    milk, Ch 33, p 55in milk, Ch 33, pp 1516phosphatase in, Ch 33, p 36Salmonella in, Ch 17, pp 5860

    Casein coagulation method proteolytic chillproofing enzymes,

    Ch 27, p 15Cassia extract

    alcohol in, Ch 36, pp 1819oil in, Ch 36, p 19

    Cat-eye bioassay method, Ch 16, p 7Catalase

    in frozen vegetables, Ch 42, pp 1213Catalytic combustion method

    sulfur determination, Ch 12, p 13Cation exchange capacity

    for peat, Ch 2, p 39Catsup

    benzoic acid in, Ch 47, p 8Caustic value

    liming materials, Ch 1, p 2Caviar

    boron in, Ch 47, pp 1112Cayenne pepper

    ground, capsaicinoids in, Ch 43,pp 1315

    filth in, Ch 16, p 41CB methods

    aflatoxins in cocoa beans, Ch 49, p 12aflatoxins in peanuts and peanut prod-

    ucts, Ch 49, pp 810Celery

    thiram pesticide residues in, Ch 10, p 60Celery leaves

    filth in, Ch 16, pp 3840 Celery seed

    filth in, Ch 16, pp 3840, 42 foreign matter in, Ch 16, p 39

    Cellulose acetate strip methodidentification of fish species, Ch 35,

    pp 27-28

    Cephaeline, Ch 20, pp 79, 32Ceramic fiber filter method

    crude fiber in feeds, Ch 4, pp 2628Cereal adjuncts, brewing materials, Ch 27, pp 2931Cereal foods

    antioxidants in corn and rice breakfastcereals, Ch 32, p 30

    baked products, Ch 32, pp 3537bread, Ch 32, pp 32A35butylated hydroxyanisole and butylated

    hydroxytoluene in, Ch 47, pp 56

    filth in, Ch 16, pp 2223glucose, fructose, sucrose, and maltose

    in presweetened cereals, Ch 32, p 30

    macaroni, egg noodles, and similar prod-ucts, Ch 32, pp 3743

    niacin and niacinamide in, Ch 45, pp 1314

    starch in, Ch 32, p 25wheat flour, Ch 32, pp 12wheat, rye, corn, buckwheat, rice, bar-

    ley, and soybeans and products,Ch 32, pp 2231

    Cereal grains crude protein in oilseeds and, Ch 32,

    pp 2122dietary fiber, Ch 32, pp 56

    Cereal products -D-glucan in cereal products containing

    high levels of glucose, Ch 32-Dglucans in oat and barley fractions

    and readytoeat cereals, Ch 32, pp 2328

    starch (Total), Amyloglucosidase-Amy-lase, Ch 17, p 27

    total soluble and insoluble dietary fiber,Ch 32, pp 79

    Certified reference materials, App A, pp 811Cesium-137

    in foods in -Ray Spectrometric, Ch 13,p 7

    in milk and other foods, Ch 13, pp 68

    Charcoal column chromatographicmethod

    separation of sugars in honey, Ch 44, pp 2224

    Cheese acidity of, Ch 33, p 61aflatoxin M1 in, Ch 33, p 62; Ch 49,

    pp 3031 ash of, Ch 33, p 59calcium, magnesium, and phosphorus,

    Ch 33, pp 5960chloride in, Ch 33, p 61citric acid in, Ch 33, p 65

    1998 AOAC INTERNATIONAL

  • color additives in, Ch 33, p 62dehydroacetic acid in, Ch 47, pp 1415 fat in, Ch 33, pp 6364filth in, Ch 16, pp 1112 gelatin in cottage cheese, Ch 33, p 66gums in soft curd cheese, Ch 33, p 66lactose in process cheese, Ch 33, p 65light filth in, Ch 16, pp 1212Amoisture in, Ch 33, pp 5859nitrate and nitrite in, Ch 33, pp 6263nitrogen in, Ch 33, p 61phosphatase in, Ch 33, pp 6769salt in, Ch 33, p 61sample collection, Ch 33, p 58sample preparation, Ch 33, p 58sampling, Ch 33, pp 34sorbic acid in, Ch 47, pp 2425sorbic acid in cottage cheese, Ch 33,

    p 66tartaric acid in, Ch 33, p 64titanium in, Ch 9, p 30; Ch 33, p 61

    Chelated iron in iron chelate concentrates, Ch 2, p 30

    Chelometric methods liming materials, Ch 1, p 6

    Chemical hazards safe handling of, App B, pp 47

    Chemical oxygen demand of water, Ch 11, pp 67

    Chemical preservatives in foods, Ch 47, pp 737

    Chenopodium oil, Ch 20, p 29Cherries

    azinphos-methyl pesticide residues on,Ch 10, p 39

    maggots in, Ch 16, p 28Chervil

    filth in, Ch 16, pp 3840Chewing gum

    filth in, Ch 16, p 31Chick bioassay

    vitamin D3 in poultry feed supplements,Ch 45, pp 5758

    Chick edema factor in oils and fats, Ch 41, pp 4142

    Chick embryo bioassay toxicity of aflatoxin B1, Ch 49, p 30

    Chicory filth in, Ch 16, p 7 in roasted coffee, Ch 30, p 3

    Chili peppercapsaicinoids in, Ch 43, pp 1315

    Chili powder filth in, Ch 16, p 41

    Chinchona alkaloids, Ch 20, pp 1618Chives

    filth in, Ch 16, pp 3840Chloral hydrate, Ch 19, pp 18, 35Chloramben

    in formulations, Ch 7, p 60

    Chloramine T pesticide formulations,Ch 7, pp 1819Chloramines

    in milk, Ch 33, pp 2829Chloramphenicol

    in milk, Ch 33, pp 4243Chlordane, AG

    alpha and gamma isomers in, Ch 7, p 62

    granular formulations, Ch 7, p 62 heptachlor in, Ch 7, p 62 technical, hexachlorocyclopentadiene

    in, Ch 7, pp 6162 technical, in formulations, Ch 7,

    pp 6061, 62Chlordane

    in water, Ch 10, pp 1317Chlordane

    in water, Ch 10, pp 1317Chlordimeform

    in formulations, Ch 7, pp 6263Chloride

    in ash of bread, Ch 32, p 34in beer, Ch 27, p 13in cheese, Ch 44, p 12in calcium cyanide formulations, Ch 7,

    p 16 in deodorants, Ch 15, p 6 in distilled liquors, Ch 26, pp 89in eggs, Ch 34, p 5in fertilizers, Ch 2, p 28in meat extracts and similar products,

    Ch 39, p 23in milk-based infant formula, Ch 50,

    p 11in plants, Ch 3, p 14 in prepared mustard, Ch 43, p 6in roasted coffee, Ch 30, p 3in tobacco, Ch 3, p 29 in water, Ch 11, pp 1112, 2830 in water-soluble color additives, Ch 46,

    pp 2425 in wines, Ch 28, p 6see also Salt; Sodium chloride

    Chlorinated hydrocarbons in drugs, Ch 18, p 3

    Chlorine as sodium chloride in seafood, Ch 35,

    pp 78 in bleaching powder, Ch 7, p 18 in calcium hypochlorite, Ch 7, p 18 in chloramine T, Ch 7, pp 1819 in disinfectants, Ch 6, p 8 in fat of flour, Ch 32, pp 1617in feeds, Ch 4, pp 3233 in fertilizers, Ch 2, p 28 in fruit products, Ch 37, p 9in meat and meat products, Ch 39, p 4microchemical methods, Ch 12, pp 13 in organohalogen pesticides, Ch 7, p 52

    safe handling of, App B, p 5in sodium hypochlorite, Ch 7, p 18

    Chlorine methods chlordane, technical and formulations,

    Ch 7, pp 6061DDT in formulations, Ch 7, pp 6566 heptachlor in formulations, Ch 7,

    pp 7374Chlorobenzilate

    in formulations, Ch 7, pp 4041in water, Ch 10, pp 1317

    Chlorobutanol in drugs, Ch 18, pp 34chemical name, Ch 18, p 58

    Chloroform in drugs, Ch 18, p 2 safe handling of, App B, p 5 in wheat and corn grain, Ch 10, p 32B

    Chloroform extraction2-isopropyl-4-pentenoyl urea, Ch 19,

    p 18Chloroform-methanol extractionmethod

    fat in foods, Ch 45, pp 6465Chlorogenic acid

    in green coffee, Ch 30, p 1in roasted coffee, Ch 30, p 3

    Chloronebin water, Ch 10, pp 1317

    p-Chlorophenyl phenyl sulfone residues, Ch 10, p 43

    Chlorophyll in plants, Ch 3, pp 2628

    Chloroplatinate methods potassium in fruits and fruit products,

    Ch 37, p 7Chloropropham

    in finished drinking water, Ch 10, pp 2630

    Chloropropylatein formulations, Ch 7, pp 4041

    Chlorothalonilin water, Ch 10, pp 1317

    Chlorothiazide, Ch 19, pp 2730, 35Chlorotoluron, Ch 7, pp 2728Chloroxuron, Ch 7, pp 2728Chlorpheniramine maleate, Ch 18, pp 1921, 58; Ch 20, pp 1011, 32Chlorpropamide, Ch 19, pp 23, 35Chlorpyrifos

    in formulations, Ch 7, p 81 in lettuce, strawberries, and tomatoes,

    Ch 10, pp 1011Chlortetracycline

    in edible animal tissues, Ch 23, pp 1923in feeds, Ch 5, p 31

    Chlortetracycline HCl in feeds, Ch 5, pp 3840

    Chocolate and chocolate productsalginates in frozen desserts, Ch 33, p 73

    1998 AOAC INTERNATIONAL

  • cacao mass of chocolate liqueur, Ch 31,p 8

    casein in chocolate malted milk, Ch 33,p 55

    filth in, Ch 16, pp 67see also Cacao bean and its products;

    Milk chocolateCholecalciferol, see Vitamin DCholesterol

    animal fats in vegetable oils and fats, Ch 41, pp 3536

    in baked products, Ch 32, p 36in bread, Ch 32, p 34in eggs, Ch 34, pp 35in foods, Ch 45, pp 7375in macaroni products, Ch 32,

    pp 3940in multicomponent foods, Ch 45,

    pp 6870Choline, Ch 18, pp 45, 58Cholinesterase

    activity in whole blood, Ch 14, pp 34

    in blood, Ch 14, p 4Cholinesterase inhibition method

    organophosphorus pesticide residues,Ch 10, pp 2426

    Chromatographic methods acetic and protionic acids in bread,

    Ch 32, pp 32B33aspirin, phenacetin, and caffeine in

    drugs, Ch 19, p 10 benzoic and salicylic acids in drugs,

    Ch 19, p 1 codeine in APC drug tablets, Ch 20, p 3codeine with antihistamines in drugs,

    Ch 20, pp 12 ergotamine in drugs, Ch 20, pp 1213 fatty acids (volatile) in seafood, Ch 35,

    pp 1114 fatty acids and butyric acid in butter,

    Ch 33, pp 56G57glucose in honey, Ch 44, p 26 glycerides in shortening, Ch 41, pp 4546ipecac alkaloids in drugs, Ch 20, pp 79isocitric acid in fruits and fruit products,

    Ch 37, p 11morphine in opium and paregoric,

    Ch 20, pp 45 neostigmine in drugs, Ch 20, pp1516 physostigmine salicylate and physostig-

    mine sulfate in drug dosage forms,Ch 20, p 14

    polar components in frying fats, Ch 41,pp 2425

    vanillin, ethyl vanillin, and coumarin invanilla extract, Ch 36, pp 45

    see also Column chromatographic meth-ods; Gas chromatographic meth-

    ods; Liquid chromatographicmethods

    Chromatographic-spectrophotometricmethod, Ch 30, p 3Chromic acid

    safe handling of, App B, p 3Chromium

    in coal fly ash, Ch 9, pp 3134hexavalent in drinking water, ground

    water and industrial effluents, Ch 9, pp 4446

    in solid wastes, Ch 9, pp 3134in wastewaters, Ch 9, pp 3444in water, Ch 11, pp 1517

    Chromotropic acid colorimetric methodmethanol in distilled liquors, Ch 26, p 15

    Cigarette filler glycerol in, Ch 3, p 30menthol in, Ch 3, p 34

    Cinchonidine, Ch 18, pp 45, 58Cinchonine, Ch 18, pp 45, 58Cinchophen, Ch 18, pp 49, 58; Ch 20, pp 24, 32Cinnamon

    alcohol in extracts, Ch 36, pp 1819filth in, Ch 16, pp 3840, 42, oil in extracts, Ch 36, p 19

    CIPACAOAC methods alachlor in formulations, Ch 7, pp 5152 aminocarb, technical and pesticide for-

    mulations, Ch 7, p 23anilazine in formulations, Ch 7, p 24 azinphos-methyl in formulations, Ch 7,

    pp 80A81 butachlor in formulations, Ch 7, pp 5859 captan in formulations, Ch 7, pp 5960 chloramben in formulations, Ch 7, p 60 chlordimeform in formulations, Ch 7,

    pp 6263 chlorotoluron, chloroxuron, or me-

    toxuron in formulations, Ch 7, pp 2728

    copper in fungicides, Ch 7, pp 1112 cyanazine in formulations, Ch 7,

    pp 3536cyhexatin technical and formulations,

    Ch 7, pp 9899cypermethrin in pesticide formulations,

    Ch 7, p 42 DDT in formulations, Ch 7, pp 6566deltamethrin in pesticide formulations,

    Ch 7, p 43dicamba-MCPA and dicamba-2,4-D in

    formulations, Ch 7, p 67 dichlobenil in formulations, Ch 7,

    pp 6869 diflubenzuron in formulations, Ch 7,

    pp 7071 dithianon in technical products and for-

    mulations, Ch 7, pp 2828A

    diquat in formulations, Ch 7, pp 3637 endosulfan in formulations, Ch 7,

    pp 7172fentin in formulations, Ch 7, p 12fentin in fentinmaneb formulations,

    Ch 7, pp 1213folpet in formulations, Ch 7, pp 7273 formothion in formulations, Ch 7,

    pp 8586 -BHC in technical BHC, formulations,

    and lindane shampoos and lotions,Ch 7, pp 5556

    isofenphos, technical and formulations,Ch 7, pp 8687

    maneb in formulations, Ch 7, pp 1314mercury in organic mercurial seed disin-

    fectants, Ch 7, pp 2021 methamidophos in formulations, Ch 7,

    pp 8990 methiocarb technical and pesticide for-

    mulations, Ch 7, pp 2930metolachlor in formulations, Ch 7, p 76 organochlorine pesticide contamination

    of pesticide formulations, Ch 7, pp 78

    oxydemetonmethyl in pesticide formu-lations, Ch 7, pp 8990

    oxythioquinox in formulations, Ch 7, pp 99100

    perimiphos methyl in formulations, Ch 7, pp 9394

    permethrin in pesticide formulations, Ch 7, pp 4344

    phosphamidon in pesticide formula-tions, Ch 7, pp 9495

    propachlor in formulations, Ch 7, pp 7778

    propoxur technical and pesticide formu-lations, Ch 7, p 31

    temephos in formulations, Ch 7,pp 9596

    terbuthylazine in formulations, Ch 7, pp 3940

    tetradifon (technical) in formulations,Ch 7, pp 7879

    thiram in formulations, Ch 7, pp 3233triadimefon technical and pesticide for-

    mulations, Ch 7, pp 3334triazines in formulations, Ch 7, pp 4041

    Citralin flavor extracts and toilet preparations,

    Ch 36, pp 2021in lemon and orange extracts, Ch 36,

    p 14Citric acid

    in bread, Ch 32, p 34in cheese, Ch 33, p 65in cordials and liqueurs, Ch 26, p 21in dried milk, Ch 33, p 56

    1998 AOAC INTERNATIONAL

  • in fruits and fruit products, Ch 37,pp 11, 1314

    in milk, Ch 33, pp 78in nonalcoholic beverages, Ch 29, p 1in wines, Ch 28, p 10

    Citrus fruitbiphenyl pesticide residues in, Ch 10,

    pp 3940filth in canned juices, Ch 16, p 29mold in juices, Ch 16, pp 6263, 65see also Specific fruits

    Citrus Red No. 2, Ch 46, p 5Clams

    shell in canned products, Ch 16, p 25shucked, volume of, Ch 35, p 4

    Clioquinolin creams and ointments, Ch 18, p 35

    Clopidol, Ch 23, pp 24, 18Clostridium botulinum

    and toxins in foods, Ch 17, pp 4648Clostridium nigrificans

    in sugars, Ch 17, p 44Clostridium perfringens

    in foods, Ch 17, pp 4851from shell fish, Ch 17, pp 5152

    Clostridium thermosaccharolyticumin sugars, Ch 17, p 44

    Clovesalcohol in extracts, Ch 36, pp 1819 filth in, Ch 16, pp 3840foreign matter in, Ch 16, p 39oil in extracts, Ch 36, p 19tannin in, Ch 43, p 3

    Coating and grazing substancesin roasted coffee, Ch 30, pp 34

    Coal fly ash metals in, Ch 9, pp 3134

    Cobalaminassays, Ch 45, pp 4144in milk-based formulas, Ch 50,

    pp 1921in vitamin preparations, Ch 45, pp 4445

    Cobaltin coal fly ash, Ch 9, pp 3134in feeds, Ch 4, p 33in fertilizers, Ch 2, p 28in plants, Ch 3, pp 58in solid wastes, Ch 9, pp 3134in wastewaters, Ch 9, pp 3444

    Cocaine, Ch 20, p 32HCl, Ch 20, pp 2, 32; Ch 22, pp 2, 6 microchemical tests, Ch 18, p 45with procaine in drugs, Ch 18, pp 3031titration factors, Ch 20, p 2

    Cocoa-buttercoconut and palm kernel oils in, Ch 31,

    p 11unsaponifiable matter in, Ch 31,

    p 11see Cacao bean and its products

    Coconutaflatoxins in, Ch 49, p 13filth in, Ch 16, p 13Salmonella in, Ch 17, pp 6769shredded, glycerol in, Ch 44, p 3

    Coconut oilin cocoa butter and in fat extracted from

    milk chocolate, Ch 31, p 11silver number for detection of, Ch 31,

    p 11Cod fish

    minced flesh in mixed fillet-minced codblocks, Ch 35, p 5

    Cod liver oilin emulsions, Ch 20, p 28

    Codeinewith acetanilid in drugs, Ch 19, p 9with antihistamines, Ch 20, pp 12in APC drug tablets, Ch 20, p 3with caffeine in drugs, Ch 19, p 9chemical name, Ch 19, p 35microchemical tests, Ch 18, p 45phosphate, Ch 20, p 2with procaine in drugs, Ch 18, pp 3031sulfate, Ch 20, p 2and terpin hydrate in elixirs, Ch 20,

    pp 23titration factors, Ch 20, p 2

    Codex Allmentarius Draft EuropeanRegional Standard for Vinegar-AOACmethod

    solids in vinegar, Ch 43, p 12Codex-AdoptedAOAC Methods

    acid value of butterfat, Ch 33, p 56Facidity (titratable) of fruit products,

    Ch 37, pp 1011acids (volatile) in oils and fats, Ch 41,

    pp 1112acrylonitrile in food, Ch 48, pp 67aflatoxin M1 in dairy products, Ch 49,

    p 30aflatoxin M1 in milk and cheese, Ch 49,

    pp 3031alcohol by volume in distilled liquors,

    Ch 26, pp 23alkaline phosphatase activity, Ch 33,

    pp 3738alpha-tocopherol and alpha-tocopheryl

    acetate in foods and feeds, Ch 45,pp 3034

    arsenic, cadmium, lead, selenium, andzinc in food, Ch 9, pp 13

    arsenic in food, Ch 9, p 9ascorbic acid om vitamin preparations

    and juice, Ch 45, pp 1617ash of animal feed, Ch 4, p 4ash of cacao products, Ch 31, p 8ash of flour, Ch 32, p 2ash of nuts and nut products, Ch 40, p 2ash of spices, Ch 43, pp 1315

    cacao mass (fat-free) of chocolate liquor,Ch 31, p 8

    cadmium and lead in food, Ch 9, pp 45cadmium, chromium, copper, iron, lead,

    magnesium, manganese, silver,Zinc in water, Ch 11, pp 1517

    cadmium in food, Ch 9, pp 910carotene in fresh plant materials and si-

    lages, Ch 45, pp 45chloride in cheese, Ch 33, p 61chloride in water, Ch 11, pp 1112cis, cis-methylene interrupted polyun-

    saturated fatty acids in oils, Ch 41,pp 2526

    citric acid in cheese, Ch 33, p 65cobalamin (vitamin B12 activity) in vita-

    min preparations, Ch 45, pp 4445copper in food, Ch 9, p 10copper, iron, and nickel in edible oils and

    fats, Ch 9, pp 78copper and nickel in tea, Ch 9, pp 89essential oil in emulsion, Ch 36, p 20evaporated milk (unsweetened), Ch 33,

    pp 5354face powders, Ch 15, p 8fat (crude) in nuts and nut products,

    Ch 40, p 1fat (crude) or ether extract in animal

    feed, Ch 4, p 25fat (milk) in milk chocolate, Ch 31, p 11fat acidity grains, Ch 32, p 24fat in cacao products, Ch 31, pp 811fat in cheese, Ch 33, p 63fat in cream, Ch 33, p 49fat in dried milk, Ch 33, p 56fat in flavor, Ch 32, p 5fat in ice cream and frozen desserts,

    Ch 33, p 72fat in milk, Ch 33, p 18fat in whey cheese, Ch 33, p 63fats (vegetable) in butterfat, Ch 41,

    pp 3234fatty acids in oils and fats, Ch 41,

    pp 1718fiber (crude) in animal feed, Ch 4,

    pp 2628fish content of frozen breaded fish prod-

    ucts, Ch 35, pp 12folic acid (pteroylglutamic acid) in vita-

    min preparations, Ch 45, pp 4546freezing point of milk, Ch 33, pp 57fructose, glucose, lactose, maltose, and

    surcrose in milk chocolate, Ch 31,p 13

    grains, Ch 32, p 22hydroxymethylfurfural in honey, Ch 44,

    p 26ice cream and frozen desserts, Ch 33,

    p 72

    1998 AOAC INTERNATIONAL

  • iodide in ready-to-feed milk-based in-fant formula, Ch 50, pp 1213

    iodine in iodized salt, Ch 11, p 31lead in edible oils and fats, Ch 41,

    pp 99Blead in food, Ch 9, pp 1920mercury (methyl) in fish and shellfish,

    Ch 9, pp 2425mercury in fish, Ch 9, p 21mercury in food, Ch 9, pp 2021mercury in water, Ch 11, pp 1718methyl esters of fatty acids in oils and

    fats, Ch 41, pp 1819milk fat in milk chocolate, Ch 31, p 11minced fish flesh in mixed fillet-minced

    cod blocks, Ch 35, p 5moisture in animal feed, Ch 4, p 1moisture in butter, Ch 33, p 33moisture in cacao products, Ch 31, p 1moisture in cheese, Ch 33, p 58moisture in dried fruits, Ch 37, p 4moisture in nuts and nut products, Ch 40,

    p 1moisture (loss of mass on drying) in

    frozen french-fried potatoes,Ch 42, p 14

    mold in tomato products, Ch 16,pp 6364

    net contents of frozen seafoods, Ch 35,p 1

    niacin and niacinamide (nictoinic acidand nicotinamide) in vitaminpreparations, Ch 45, pp 4647

    niacin and niacinamide in drugs, foods,and feeds, Ch 45, pp 1213

    nitrate and nitrite in cheese, Ch 33,pp 6263

    nitrites in cured meat, Ch 39, pp 89nitrogen (total) in fertilizers, Ch 2,

    pp 1314nitrogen (total) in milk, Ch 33, pp 1012nonprotein nitrogen in whole milk,

    Ch 33, pp 1213oil (essential) in fruits and fruit products,

    Ch 37, p 18oil (peanut) in oils and fats, Ch 41, p 37organochlorine and organophosphorus

    pesticide residues, Ch 10, pp 110pantothenic acid in milk-based infant

    formula, Ch 50, pp 2425pantothenic acid in vitamin preparations,

    Ch 45, pp 4748parasites in fish muscle, Ch 35,

    pp 24 -25peroxide value of oils and fats, Ch 41,

    p 9Bphosphatase (residual) in ice cream and

    frozen desserts, Ch 33, p 74phosphorus in milk-based infant for-

    mula, Ch 50, pp 1516

    protein (milk) in milk chocolate, Ch 31,p 12

    protein (total) in flour, Ch 32, pp 1213protein efficiency ratio, Ch 45, pp 5859protein in ice cream and frozen desserts,

    Ch 33, p 72protein nitrogen content of milk, Ch 33,

    p 13refractive index of butterfat, Ch 33,

    p 56Fresidue (acid-insoluble) (soil) in fruits

    and vegetables (frozen), Ch 16,pp 2930

    riboflavin (vitamin B2) in foods and vi-tamin preparations, Ch 45,pp 910

    sampling of dairy products, Ch 33, p 1sodium and potassium in dried milk,

    Ch 33, pp 56A56Bsodium chloride in canned vegetables,

    Ch 42, pp 78solids (total) and moisture in flour,

    Ch 32, p 1solids (total) in canned vegetables,

    Ch 42, p 4solids (total) in cream, Ch 33, p 48solids (total) in milk, Ch 33, p 10solids (soluble) in tomato products,

    Ch 42, pp 56solids in sirups, Ch 44, pp 23sorting corn grits, Ch 27, p 29sprial vessel count of cacao products,

    Ch 31, pp 56stone cell and group count of cacao prod-

    ucts, Ch 31, pp 69sulfites in foods, Ch 47, pp 2931sulfites in foods and beverages, Ch 47,

    pp 3334sulfurous acid (total) in dried fruit,

    Ch 47, p 27sweetened condensed milk, Ch 33,

    pp 5455thiamine (vitamin B1) in foods, Ch 45,

    pp 67tin in canned foods, Ch 9, pp 2930tin in food, Ch 9, p 29total dietary fiber in foods, Ch 45,

    pp 7071total, soluble, and insoluble dietary fiber

    in foods, Ch 32, pp 79trans-vitamin K1 (phylloquinone) in

    ready-to-feed milk-based infantformula, Ch 50, pp 68

    vinegars (1), Ch 43, pp 1315viscosity (apparent consistency) of fruit

    products, Ch 37, p 3vitamin A in margarine, Ch 45, p 1vitamin A in mixed feeds, premixes, and

    foods, Ch 45, pp 14

    vitamin A (retinol) in milk-based infantformula, Ch 50, pp 12

    vitamin A (retinol isomers) in milk andmilk-based infant formula, Ch 50,pp 12

    vitamin B6 (pyridoxine, pyridoxal, pyri-doxamine) in food extracts, Ch 45,pp 5153

    vitamin C (total) in vitamin preparations,Ch 45, pp 1718

    vitamin D in milk, vitamin preparations,and feed concentrates, Ch 45,pp 5357

    vitamin D3 (cholecalciferol) in ready-to-feed milk-based infant formula,Ch 50, pp 56

    vitamin E activity (all-ractocopherol)in milk-based infant formula,Ch 50, pp 45

    water (added) in milk, Ch 33, p 26Aweight per unit volume of packaged ice

    cream, Ch 33, p 74zinc in food, Ch 9, p 31

    Coffeefilth in, Ch 16, p 7

    Coffee (green)aflatoxins in, Ch 49, p 27caffeine in, Ch 30, p 1chlorogenic acid in, Ch 30, p 1coloring matter in, Ch 30, p 1macroscopic examination, Ch 30, p 1ochratoxin A in, Ch 49, pp 3940

    Coffee (roasted)acidity of, Ch 30, p 2ash of, Ch 30, p 2caffeine in, Ch 30, pp 23chicory in, Ch 30, p 3chlorides in, Ch 30, p 3chlorogenic acid in, Ch 30, p 3coating and glazing substances in,

    Ch 30, p 34dextrin in, Ch 30, pp 34fiber (crude) in, Ch 30, p 4gelatin in, Ch 30, pp 34glucose (commercial) in, Ch 30,

    pp 34macroscopic examination, Ch 30, p 2moisture in, Ch 30, pp 45petroleum ether extract of, Ch 30, p 4sample preparation, Ch 30, p 2solids (soluble) in, Ch 30, p 5starch in, Ch 30, p 5sugars in, Ch 30, p 5

    Coffee (soluble/instant)carbohydrates in, Ch 30, pp 511

    Colchicinein drugs, Ch 20, pp 1112

    Cole-type cropsazinphos-methyl pesticide residues on,

    Ch 10, p 39

    1998 AOAC INTERNATIONAL

  • milk, Ch 17, pp 12B12Cin dairy products, Ch 17., pp. 12D-13

    Coliform organismsin chilled, frozen, precooked, or pre-

    pared foods, Ch 17, pp 34in dairy products, Ch 17, pp 1112Cin eggs in egg products, Ch 17, pp 23and E. coli in all foods, Ch 17, pp 1718and E. coli in water, Ch 17, pp 1517in foods, Ch 17, pp 1315, 1721in shellfish growing waters, Ch 17, p 15in tree nut meats, Ch 17, pp 45see also Fecal coliforms

    Coliform countsin dairy products, Ch 17, pp 12E12Fin milk, Ch 17, p 12D

    Colilery methodtotal coliforms and E. coli in water,

    Ch 17, pp 1517Collaborative study guidelines, App D,pp 111Collards

    filth in, Ch 16, p 35 N-methylcarbamate residues on, Ch 10,

    pp 32C33Color

    of beer, Ch 27, p 1of black mal, Ch 27, p 26of brewing sugars and sirups, Ch 27,

    p 33of caramel malt, Ch 27, p 25of distilled liquors, Ch 26, pp 12of egg yolks, Ch 34, p 1in oils and fats, Ch 41, p 42of raw cane sugars, Ch 44, p 1in spices, Ch 43, p 1in vanilla extract, Ch 36, p 7in vinegars, Ch 43, p 12of white wines, Ch 28, p 1

    Color additivesin butterfat, Ch 33, p 56Fin cheese, Ch 33, p 62in cream, Ch 33, p 50dye (pure) in, Ch 46, pp 1012 in evaporated milk, Ch 33, p 53extracts of, Ch 46, p 13FD&C, in foods, Ch 46, pp 34free acid in, Ch 46, p 25halogens in, Ch 46, p 24in ice cream and frozen desserts,

    Ch 33, p 73inorganic salts in, Ch 46, p 25insoluble matter in, Ch 46, p 12intermediates in, Ch 46, pp 1320 in macaroni products, Ch 32, pp 4041melting point of, Ch 46, p 25metals and other elements in, Ch 46,

    pp 2123 in milk, Ch 33, p 31natural coloring matters, Ch 46, p 4

    oil-soluble, in foods, Ch 46, pp 23pigments and lakes, Ch 46, p 1separation and identification, Ch 46,

    pp 113 soluble matter in, Ch 46, p 25soluble, and their lakes, Ch 46, p 1specifications and methods for colors

    appearing in previous editions, Ch 46, pp 910

    subsidiary and lower sulfonated dyes,Ch 46, p 20

    synthetic organic, analysis, Ch 46, pp 410

    synthetic organic, in foods, Ch 46, pp 12, 1011

    volatile matter in, Ch 46, p 12yellow AB in macaroni products, Ch 32,

    pp 4041see also Specific colors

    Color classificationof honey, Ch 44, p 20of maple products, Ch 44, p 31

    Colorimetric methodsaldehydes in lemon, orange, and lime

    extracts, Ch 36, pp 1314ammonia in crabmeat, Ch 35, p 6arsenic in feeds, Ch 5, p 5benzene hexachloride pesticide residues,

    Ch 10, p 39benzocaine in drugs, Ch 18, p 28bifuran in feeds, Ch 5, p 12bromide in water, Ch 11, p 242(ptertbutylphenoxy)-1-methyl 2-

    chloroethyl sulfite (aramite) pesti-cide residues, Ch 10, p 40

    calcium gluconate in drugs, Ch 18,pp 78

    carbaryl pesticide residues, Ch 10, pp 4142

    carotenoids in macaroni products, Ch 32, pp 4142

    chlordane (technical) and formulations,Ch 7, p 61

    chlorophyll in plants, Ch 3, pp 2628citral in lemon and orange extracts,

    Ch 36, p 14citric acid in cheese, Ch 33, p 65cobalt in feeds, Ch 4, p 33cobalt in fertilizers, Ch 2, p 28color in vanilla extract, Ch 36, p 7copper in feeds, Ch 4, p 33copper in food, Ch 9, p 10copper in milk and milk products, Ch 33,

    p 31copper in plants, Ch 3, p 8creatinine in meat, Ch 39, p 13DDT pesticide residues, Ch 10, p 43diacetyl in beer, Ch 27, pp 78disulfiram in drug tablets, Ch 19,

    pp 3132

    -estradiol in drugs, Ch 21, p 1ethopabate in feeds, Ch 5, p 10fluoride in water, Ch 11, pp 1213,

    2830fluorine in feeds, Ch 4, pp 3334fluorine on apples and pears, Ch 9,

    p 10furazolidone in feeds, Ch 5, p 12glucoamylase activity in

    industrial enzyme preparations,Ch 45, pp 4141A

    gliadin as a measure of gluten in foods,Ch 32, pp 1314

    glycarbylamide in feeds, Ch 5, p 13hydroxyproline in meat and meat prod-

    ucts, Ch 39, pp 1314hypochlorites and chloramines in milk,

    Ch 33, pp 2829indole in crabmeat, oysters, and shrimp,

    Ch 35, p 18iodide in water, Ch 11, p 24iron in beer, Ch 27, pp 1213iron in distilled liquors, Ch 26, p 8iron in plants, Ch 3, p 8iron in water, Ch 11, pp 1314ketosteroids in drugs, Ch 21, p 1lactic acid in eggs, Ch 34, p 9lead on apples and pears, Ch 9, p 15liming materials, Ch 1, pp 69listeria in foods, Ch 17, pp 113115malathion pesticide residues, Ch 10,

    p 53manganese in feeds, Ch 4, pp 3435manganese in fertilizers, Ch 2, pp 3132manganese in plants, Ch 3, p 9menthol in cigarette filler, Ch 3, p 34 mercury in foods, Ch 9, p 22methanol in distilled liquors, Ch 26, p 15methoxychlor pesticide residues, Ch 10,

    p 54methyl anthranilate in nonalcoholic bev-

    erages, Ch 29, pp 56molybdenum in plants, Ch 3, pp 910niacin and niacinamide in drugs, foods,

    and feeds, Ch 45, pp 1213nihydrazone in feeds, Ch 5, p 17nitrate and nitrite nitrogen in feeds,

    Ch 4, pp 2223nitrites in cured meat, Ch 39, pp 89nitrofurazone in feeds, Ch 5, p 12nitrogen (ammonia) in water, Ch 11,

    pp 910nitrogen (nitrate) in water, Ch 11,

    pp 1011nitrogen (total) in water, Ch 11, pp 89nitrogen in beer, Ch 27, p 8parathion in formulations, Ch 7, p 91parathion pesticide residues, Ch 10,

    p 58

    1998 AOAC INTERNATIONAL

  • phenol in hazardous substances, Ch 8,pp 56

    phenylephrine HCl in drugs, Ch 18, pp 2223

    phosphorus in fruits and fruit products,Ch 37, p 8

    phosphorus (total) in foods, Ch 45,pp 41A41B

    phosphorus in wines, Ch 28, p 7piperonyl butoxide in formulations,

    Ch 7, p 46propyl gallate in food, Ch 47, pp 67protein in feeds, Ch 4, pp 17pyrogallol in hair dyes, Ch 15, p 9salicyclic acid in food and beverages,

    Ch 47, pp 2324Salmonella in foods, Ch 17, pp 7174,

    8789sodium cyclamate and calcium cycla-

    mate in canned fruit, Ch 47, p 44 sodium lauryl sulfate in egg white,

    Ch 47, pp 3839sorbic acid in wines, Ch 28, p 14Bsulfamethoxine in feeds, Ch 5, p 25sulfur dioxide in beer, Ch 27, pp 1314sulfurous acid in dried fruit, Ch 47, p 27thiourea in orange peel, Ch 47,

    pp 3637-tocopherol and -tocopheryl acetate in

    foods and feeds, Ch 45, pp 3034-tocopheryl acetate (supplemental) in

    foods and feeds, Ch 45, pp 3536total dietary fiber (determined as neutral

    sugar residues, uronic acid resi-dues, and klason lignin, Ch 45,pp 7579

    trimethylamine nitrogen in seafood, Ch 35, p 7

    urea in feeds, Ch 4, pp 1314vitamin A in mixed feeds, premixes, and

    human and pet foods, Ch 45,pp 14

    vitamin D in vitamin preparations, Ch 45, pp 1923

    zinc in fertilizers, Ch 2, p 33zinc in food, Ch 9, p 31zirconium in antiperspirants, Ch 15,

    pp 45Coloring matter

    in distilled liquors, Ch 26, pp 12in green coffee, Ch 30, p 1in macaroni products, Ch 32, pp 4041see also Color additives

    Column chromatographic methodsbutyric acid in fat, Ch 41, pp 1213color additives in foods, Ch 46, pp 12fatty acids in eggs, Ch 34, p 10glycerides in monoglyceride concen-

    trates, Ch 41, pp 4243

    hydrocarbons (saturated) in glycerides,Ch 41, pp 4041

    see also Chromatographic methods; Gaschromatographic methods; Liquidchromatographic methods

    Combustion methodsbromine, chlorine, or iodine determina-

    tion, Ch 12, pp 13carbon and hydrogen determination,

    Ch 12, pp 35crude protein in cereal grains and oil

    seeds, Ch 32, pp 2122crude protein in meat and meat products,

    Ch 39, pp 67nitrogen (total) in fertilizer, Ch 2, pp 1213protein (crude) in feed, Ch 4, pp 1819sulfur determination, Ch 12, pp 1013

    Concentrationnomograph relating absorptivity, absor-

    bance, and, App C, p 17 (vol 1)Condensed milk

    filth in, Ch 16, p 11sampling, Ch 33, pp 23

    Condimental seedsfilth in, Ch 16, pp 3840, 43

    Conductivity valueof maple sirup, Ch 44, p 34

    Confectioneryalcohol in sirups used in, Ch 44, p 19ether extract of, Ch 44, pp 1819paraffin in, Ch 44, p 19shellac in, Ch 44, p 19starch in, Ch 44, p 18

    Convection oven methodmoisture in frozen french-fried potatoes,

    Ch 42, p 14Cooking

    seafood products, Ch 35, p 2Copper

    in beer, Ch 27, pp 1112in Bordeaux mixtures, Ch 7, pp 4, 1516in coal fly ash, Ch 9, pp 3134in copper carbonate formulations, Ch 7,

    p 11in copper naphthenate formulations,

    Ch 7, p 11in distilled liquors, Ch 26, pp 67in edible oils and fats, Ch 9, pp 78in feeds, Ch 4, pp 31, 33in fertilizers, Ch 2, pp 2526, 29 in food, Ch 9, p 10fungicides, Ch 7, p 1112in infant formulas, Ch 50, pp 1416in liver, Ch 14, pp 12in milk, Ch 33, p 31in pesticide formulations, Ch 7, pp 4, 11in pet foods, Ch 3, pp 34in plants, Ch 3, pp 24, 8in ready-to-feed milk-based infant for-

    mulas and pet foods, Ch 50, p 14

    in serum, Ch 14, p 2in tea, Ch 9, pp 89; Ch 30, p 13in wastewater, Ch 9, pp 3444 in water, Ch 11, pp 1517in wines, Ch 28, p 7

    Copper carbonate formulations, Ch 7, p 11Copper catalyst method

    protein in feeds, Ch 4, p 19Copper naphthenate formulations, Ch 7,p 11Copper salts

    in feeds, Ch 4, p 31Copper serum method

    water (added) in milk, Ch 33, p 26

    Copper-reducing substancesin spices, Ch 43, p 3

    Coprostanolin heat-processed materials, Ch 16,

    pp 5758Cordials and liqueurs