standard operating procedure - training procedure · standard operating procedure – ems-0100.005...

129
Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Revision #: 1 Prepared By: Beth Eckert, Industrial Chemist Revision Date: 11/1/00 Approved By: Larry Cummings, Asst. Superintendent of WWTD Signature: Effective Date: 11/4/99 Page 1 of 2 ****THIS IS AN UNCONTROLLED COPY OF A CONTROLLED DOCUMENT PRINTED 01/31/01 AT 10:28 AM**** City of Gastonia Wastewater Treatment 1.0 Purpose 1.1 This procedure is to establish a guide for the training of current and future personnel on the EMS and related documents and procedures. 2.0 Associated Equipment 2.1 None 3.0 Associated Reference Material 3.1 Document Control Matrix - EMS-0101.002A 3.2 Procedure Training Sign-In Sheet –EMS-0101.005A 3.3 Training Matrix – EMS-0101.005B 4.0 Procedure 4.1 All employees within the WWTD will be trained on the EMS policy and to a general EMS awareness level. 4.2 Personnel that can have a significant impact on the environment through their work practices will be trained on: 4.2.1 The importance of conformance to the environmental policy, requirements of the environmental management system, and emergency preparedness and response requirements. Roles and responsibilities related to these will be communicated. 4.2.2 The potential or actual significant environmental impacts of their work activities. 4.2.3 The relevant procedures identified in the training matrix and potential environmental consequences of departure from those procedures. 4.2.4 Training will be tracked on Procedure Training Sign-In Sheets (EMS-0101.005A) and the Training Matrix Form (EMS-0101.005B). 4.3 Training requirements of contractor personnel will be established under the terms of the contract. Follow-up will be done annually to evaluate conformance with the contract. 4.4 Training roles of personnel will be established in designation of roles and responsibilities. 4.5 The Training Matrix Form (EMS-0101.005B) indicates which employees require training for each procedure. Notify the EMS coordinator of any changes in the employee training requirements.

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Page 1: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Standard Operating Procedure – EMS-0100.005 Name: Training Procedure

Revision #: 1

Prepared By: Beth Eckert, Industrial Chemist Revision Date: 11/1/00

Approved By: Larry Cummings, Asst. Superintendent of WWTD Signature:

Effective Date: 11/4/99

Page 1 of 2

****THIS IS AN UNCONTROLLED COPY OF A CONTROLLED DOCUMENT PRINTED 01/31/01 AT 10:28 AM****

City of Gastonia

Wastewater Treatment

1.0 Purpose 1.1 This procedure is to establish a guide for the training of current and future personnel on the

EMS and related documents and procedures.

2.0 Associated Equipment 2.1 None

3.0 Associated Reference Material 3.1 Document Control Matrix - EMS-0101.002A

3.2 Procedure Training Sign-In Sheet –EMS-0101.005A

3.3 Training Matrix – EMS-0101.005B

4.0 Procedure 4.1 All employees within the WWTD will be trained on the EMS policy and to a general EMS

awareness level.

4.2 Personnel that can have a significant impact on the environment through their work

practices will be trained on:

4.2.1 The importance of conformance to the environmental policy, requirements of the

environmental management system, and emergency preparedness and response

requirements. Roles and responsibilities related to these will be communicated.

4.2.2 The potential or actual significant environmental impacts of their work activities.

4.2.3 The relevant procedures identified in the training matrix and potential environmental

consequences of departure from those procedures.

4.2.4 Training will be tracked on Procedure Training Sign-In Sheets (EMS-0101.005A) and

the Training Matrix Form (EMS-0101.005B).

4.3 Training requirements of contractor personnel will be established under the terms of the

contract. Follow-up will be done annually to evaluate conformance with the contract.

4.4 Training roles of personnel will be established in designation of roles and responsibilities.

4.5 The Training Matrix Form (EMS-0101.005B) indicates which employees require training for

each procedure. Notify the EMS coordinator of any changes in the employee training

requirements.

Page 2: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Revision #: 1

Name – Number: Training Procedure – EMS-0100.005 Revision Date: 11/1/00 Effective Date: 11/4/99

Page 2 of 2

****THIS IS AN UNCONTROLLED COPY OF A CONTROLLED DOCUMENT PRINTED 01/31/01 AT 10:28 AM****

4.6 All new employees will receive training on policy and EMS awareness upon reporting to

work by the EMS Coordinator or designated personnel and all current EMS related

procedures within 30 days of their first working day.

4.6.1 Supervisors must make arrangements with the EMS Coordinator to ensure training is

completed as required when a new employee reports to work with the Division.

4.7 An employees will receive training on new or revised procedures upon implementation.

4.7.1 Training will not be required on revised procedures where the intent of the procedure

is not revised merely logistics i.e. spelling, grammar, numbering, etc...

4.8 Retraining will be done as a result of an incident where a procedure was not properly

followed.

4.9 All trained personnel must sign the sign-in sheet (EMS-0101.005A) to document their

training and understanding of the procedure

4.9.1 The sign-in sheet must be submitted to the EMS Coordinator for recording on the

Training Matrix (EMS-0101.005B).

5.0 Deviations from this procedure must be documented by completing a Corrective/Preventative Action Report (EMS-0101.004).

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 1 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

EMS MANAGEMENT DOCUMENTSEnvironment Management System Manual

EMS-0100.000 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

EMS Review Procedure EMS-0100.001 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Legal and Other Requirements Listing

EMS-0101.001 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Pressure Vessel Inspection Information (Legal Requirements Addendum)

EMS-0101.001A 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Document Control Procedure

EMS-0100.002 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Document Control Training Matrix

EMS-0101.002A 1 As Needed

As Needed ! U: Drive

Individual Training Matrix EMS-0101.002B Draft As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

EMS-0100.012 2 As Needed

As Needed U: Drive /T: Drive /see distribution list EMS-0100.003C

Corrective/Preventative Action Report Procedure

EMS-0100.004 2 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Corrective/Preventative Action Report Form

EMS-0101.004 2 As Needed

As Needed ! U: Drive

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 2 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Training Procedure EMS-0100.005 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Procedure Training Sign-In Sheet

EMS-0101.005 0 As Needed

As Needed ! U: Drive

Roles and Responsibilities Listing

EMS-0100.006 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Objective and Targets - Improvement Plan Summary

EMS-0101.007 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

External Communications Procedure

EMS-0100.008 1 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Compliance Review Procedure

EMS-0100.009 Not Created

As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Summary of Activities and NPDES Permit Limit/SOC Violations

EMS-0101.009 1 As Needed

As Needed ! U: Drive

Risk Management Plan EMS-0100.010 In Revision

As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Lab Sup. Office 3. Public Library

Environmental Management System Audit

EMS-0100.011 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Aspects and Impacts Procedure

EMS-0100.003 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Aspect Ranking Form EMS-A&I-1 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 3 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Significant Aspects Determination Form

EMS-A&I-2 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Significant Aspects Listing Form

EMS-A&I-3 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

Monitoring and Measuring Procedure

EMS-0100.013 0 As Needed

As Needed ! U: Drive 1. Long Creek Operations 2. Crowders Conf. Room 3. PW Director’s Office

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 4 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

LONG CREEK OPERATIONS DOCUMENTSProceduresEmergency Response Plan WLC-0100.010

Main Lift Failure Procedure WLC-0300.001 0 As Needed

As Needed ! U: Drive 1. LC Operations Room

Long Creek / Duhart / Catawba Procedure for Significant Rain Events

WLC-0100.003 2 As Needed

As Needed ! U: Drive 1. LC Operations Room 2. Catawba Pump Station on wall by pump controls 3. Duhart Pump Station on wall by pump controls

Spill Clean Up and Reporting Procedure

WLC-0100.001 0 As Needed

As Needed ! U: Drive 1. LC Operations Room

Intermediate Lift Failure Procedure

WLC-1700.001 0 As Needed

As Needed ! U: Drive 1. LC Operations Room

Chemical Receiving Procedures

WLC-4200.001 0 As Needed

As Needed ! U: Drive 1. LC Operations Room

On Call Schedule WLC-0101.003 1 As Needed

As Needed

Daily Operations Sheet 3 yrs Daily ! Datatrend 1. Operations Room (daily log book) 2. Supply Building

Microscopic Exam Form 2 / week Operations Room / Supply Building

Sample Collection Schedule WLC-0100.002 0 Daily ! U: Drive 1. LC Operations Room 2. Senior Plant Supervisor's Office 3. Asst. Superintendent's Office 4. LC Lab Supervisor's Office 5. LC Laboratory 6. Crowders Lab Supervisor's Office 7. Crowders Laboratory

Special Sample Request Form

As Needed Lab

Portable pH / DO Meter Calibration Form

Daily Operations Room / Supply Building

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 5 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Temperature Check on DO/pH/Chlorine Sampling Units

Quarterly Operations Room / Supply Building

Chlorine / Sulfur Dioxide Delivery Checklist

Every Delivery

Operations Room / Supply Building

Chlorine / Sulfur Dioxide Change Out Checklist

Every Change

Operations Room / Supply Building

Chlorine System Operating Manual

As needed Operations Room

Generator Logs Every Run Operations Room / Supply Building

Valve Exercise Program Quarterly Operations Room / Supply Building

H2S Gas Monitoring Report Tuesday / Thursday

Operations Room / Supply Building

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Weekly Operations Room / Supply Building

Lock Out / Tag Out Log Book

As needed Operations Room / Supply Building

Operators Log Book Every Change

Operations Room / Supply Building

Fire Extinguisher Testing Monthly / Yearly

See Saftey Equipment Schematic

Eye Wash / Shower Inspection

Weekly See Saftey Equipment Schematic

First Aid Kit Monthly See Saftey Equipment Schematic

Respirators / SCBA’s Weekly See Saftey Equipment Schematic

Equipment Work Orders As Needed Hansen / Hard Copy in Senior Operators Office

Operations Check Form - Old Blower Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - New Blower Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - Chlorine/SO2 Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - Filter Building

3 Times Per Shift

At Each Operation / Supply Room

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 6 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Operations Check Form - Secondary/Screw Pumps

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - Digester Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - DAF Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - Chemical Feed Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - New Main Lift Building

3 Times Per Shift

At Each Operation / Supply Room

Operations Check Form - Old Main Lift Building

3 Times Per Shift

At Each Operation / Supply Room

Temperature Check Influent / Effluent Log

Daily Operations Room/ Supply Building

CL2/SO2 Hand Analyzer Calibration

Monthly Operations Room

Chemical Feed Log Sheet Daily Chemical Feed Area

Effluent Flow Meter Calibration Form

Quarterly Operations Room / Supply Building

ISI Calibration Report Quarterly Operations Room / Supply Building

Influent Flow / RAS / WAS Meter Calibration Form

Quarterly Operations Room / Supply Building

Stationary DO Meter Calibration Form

Biweekly Operations Room / Supply Building

CROWDER OPERATION DOCUMENTSCrowder Spill Procedure WCR-0100.001 0 As

NeededAs Needed ! U: Drive

1. CR Operations RoomSampling Procedure WCR-0100.002 0 As

NeededAs Needed ! U: Drive

1. CR Operations Room

Process Control WCR-0100.003 0 ! U: Drive 1. CR Operations Room

Emergency Response Plan WCR-0100.010 ! U: Drive 1. CR Operations Room

Main Lift Failure Procedure WCR-0300.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Hi-Ran Panel Failure WCR-0300-002 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 7 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Blower Operation Procedure WCR-1000.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Waste Gas Burner Lighting Procedure

WCR-3000.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Holding Digester Transfer to Land Application Start Up

WCR-3100.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Holding Digester Transfer to Land Application Shut Down Procedure

WCR-3100.002 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Chemical Receiving Procedures

WCR-4200.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Return Sludge Procedure WCR-5700.001 0 As Needed

As Needed ! U: Drive 1. CR Operations Room

Main Lift Failure Procedure As Needed

As Needed ! U: Drive 1. CR Operations Room

Spill Clean Up and Reporting Procedure

As Needed

As Needed ! U: Drive 1. CR Operations Room

Daily Operations Sheet 3 yrs Daily Datatrend / Operations Room (daily log book)/ Supply Building

Microscopic Exam Form 2 / week Operations Room / Supply Building

Sample Collection Schedule WCR-0101.002 1 Daily ! U: Drive 1. Crowders Operations in Procedure Manual 2. Crowders Creek Operations Room Bulletin Board 4. Assistant Superintendent’s Office 5. Crowder's Creek Laboratory 6. CR Lab Supervisor's Office 7. LC Laboratory

Special Sample Request Form

As Needed Lab

Portable pH / DO Meter Calibration Form

Daily Operations Room / Supply Building

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 8 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Temperature Check on DO/pH/Chlorine Sampling Units

Quarterly Operations Room / Supply Building

Chlorine / Sulfur Dioxide Delivery Checklist

Every Delivery

Operations Room / Supply Building

Chlorine / Sulfur Dioxide Change Out Checklist

Every Change

Operations Room / Supply Building

Chlorine System Operating Manual

As needed Operations Room

Generator Logs Every Run Operations Room / Supply Building

Valve Exercise Program Quarterly Operations Room / Supply Building

H2S Gas Monitoring Report Tuesday / Thursday

Operations Room / Supply Building

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Weekly Operations Room / Supply Building

Lock Out / Tag Out Log Book

As needed Operations Room / Supply Building

Operators Log Book Every Change

Operations Room / Supply Building

Fire Extinguisher Testing Monthly / Yearly

See Saftey Equipment Schematic

Eye Wash / Shower Inspection

Weekly See Saftey Equipment Schematic

First Aid Kit Monthly See Saftey Equipment Schematic

Respirators / SCBA’s Weekly See Saftey Equipment Schematic

Equipment Work Orders As Needed Hansen / Hard Copy in Senior Operators Office

Temperature Check Influent / Effluent Log

Daily Operations Room/ Supply Building

CL2/SO2 Hand Analyzer Calibration

Monthly Operations Room

Chemical Feed Log Sheet Daily Chemical Feed Area

Page 11: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 9 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Effluent Flow Meter Calibration Form

Quarterly Operations Room / Supply Building

ISI Calibration Report Quarterly Operations Room / Supply Building

Influent Flow / RAS / WAS Meter Calibration Form

Quarterly Operations Room / Supply Building

Stationary DO Meter Calibration Form

Biweekly Operations Room / Supply Building

LONG CREEK LABORATORY DOCUMENTSStandard Methods Software (reference use only not a controlled document)

Standard Methods

General Laboratory Techniques

WLC-0100.101 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Standard Curve Bench Sheet

WLC-0101.101 Not Created

3 years Daily ! U: Drive

Quality Control Testing WLC-0100.102 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Laboratory Checks and Calibrations

WLC-0100.103 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Temperature Log WLC-0101.103A Not Created

3 years Daily ! U: Drive

Thermometer Calibration Chart

WLC-0101.103B 0 3 years Daily ! U: Drive

Balance Calibration Log WLC-0101.103C 0 3 years Daily ! U: Drive

Autoclave Logbook WLC-0101.103D N/A 3 years As Needed Long Creek Laboratory

Safety Shower and Eyewash Test Log

WLC-0101.103E 0 3 years Daily ! U: Drive

Page 12: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 10 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Emergency Water Supplies Checklist

WLC-0101.103F 0 3 years As Needed ! U: Drive

Accumet 50 Meter pH Calibration Log Book

WLC-0101.103G N/A 3 years As Needed Long Creek Laboratory

Orion 720A Meters 1 & 2 pH Calibration Log Book

WLC-0101.103H N/A 3 years As Needed Long Creek Laboratory

VWR 8015 Meter pH Calibration Log Book

WLC-0101.103I N/A 3 years As Needed Long Creek Laboratory

Reagent Log Book WLC-0101.103J N/A 3 years As Needed Long Creek Laboratory

Annual QC/Safety Schedule Checklist

WLC-0101.103K 0 3 years As Needed ! U: Drive

Washing and Preparation of Glassware and Bottles

WLC-0100.104 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Sample Bottle Set Up and Receiving

WLC-0100.105 2 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Chain of Custody for LC – Blank

WLC-0101.105A 0 3 years As Needed ! U: Drive

Chain of Custody for LC – Page 1 – Long Term Monitoring

WLC-0101.105B 4 3 years Monthly ! U: Drive

Chain of Custody for LC – Page 1 – Monday, Thursday

WLC-0101.105C 4 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 1 – Saturday, Sunday

WLC-0101.105D 4 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 1 – Tuesday, Friday

WLC-0101.105E 6 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 1 – Wednesday

WLC-0101.105F 6 3 years 1x/week ! U: Drive

Chain of Custody for LC – Page 2 – Monday, Thursday

WLC-0101.105G 7 3 years 2x/week ! U: Drive

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 11 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Chain of Custody for LC – Page 2 – Tuesday, Wednesday, Friday

WLC-0101.105H 2 3 years 3x/week ! U: Drive

Chain of Custody for LC – Page 2 – Wednesday 1x Month

WLC-0101.105I 2 3 years Monthly ! U: Drive

Chain of Custody for LC – Page 3 – Tuesday, Wednesday, Friday

WLC-0101.105J 2 3 years 3x/week ! U: Drive

Chain of Custody for LC – Page 3 – Wednesday, 1x Month

WLC-0101.105K 2 3 years Monthly ! U: Drive

Chain of Custody for LC – Page 3 – Monday, Thursday

WLC-0101.105L 1 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – 3rd Friday

WLC-0101.105M 2 3 years Monthly ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Friday (Except 1st & 3rd)

WLC-0101.105N 2 3 years 2x/Month ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Long Term Monitoring

WLC-0101.105O 1 3 years Monthly ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Monday, Thursday

WLC-0101.105P 5 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Saturday, Sunday

WLC-0101.105Q 3 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Tuesday

WLC-0101.105R 2 3 years 1x/week ! U: Drive

Chain of Custody for LC – Page 4 – To Crowders – Wednesday

WLC-0101.105S 0 3 years 2x/week ! U: Drive

Chain of Custody for LC – Page 5 – Grab Samples – Long Term Monitoring

WLC-0101.105T 0 3 years Monthly ! U: Drive

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 12 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Chain of Custody for LC – Page 5 – Grab Samples

WLC-0101.105U 0 3 years Daily ! U: Drive

Chain of Custody for LC – Page 1 – Holiday

WLC-0101.105V 1 3 years Daily ! U: Drive

Data Verification WLC-0100.106 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Data Entry WLC-0100.107 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Mercury Spill Clean Up Procedure

WLC-0100.108 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Inorganic Acid & Base Spill Clean Up Procedure

WLC-0100.109 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Laboratory Waste Chemical Storage/Disposal

WLC-0100.110 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Sample Receiving WLC-0100.111 1 3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Alkalinity Analysis WLC-0100.121 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Alkalinity/Volatile Acid Bench Sheet

WLC-0101.121 Not Created

3 years Daily ! U: Drive

Ammonia Nitrogen Analysis WLC-0100.122 2 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Ammonia Nitrogen Dechlorination Log

WLC-0101.122A 0 3 years Daily ! U: Drive

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 13 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Ammonia Nitrogen – Bench Sheet

WLC-0101.122B 0 3 years Daily ! U: Drive

Ammonia Nitrogen Distillation Method

WLC-0100.123 Not Created

3 years Quarterly ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Ammonia Nitrogen Distillation – Bench Sheet

WLC-0101.123 Not Created

3 years Quarterly ! U: Drive

Biochemical Oxygen Demand Analysis

WLC-0100.124 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Biochemical Oxygen Demand Bench Sheet

WLC-0101.124 Not Created

3 years As Needed ! U: Drive

Biochemical Oxygen Demand – Winkler Method

WLC-0100.149 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Chemical Oxygen Demand Analysis

WLC-0100.125 Not Created

3 years Monthly ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Chemical Oxygen Demand – Bench Sheet

WLC-0101.125 Not Created

3 years Monthly ! U: Drive

Conductivity Analysis WLC-0100.126 Not Created

3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Conductivity Bench Sheet WLC-0101.126A Not Created

3 years As Needed ! U: Drive

Conductivity Quarterly Temperature Check Bench Sheet

WLC-0101.126b Not Created

3 years As Needed ! U: Drive

Cyanide Analysis WLC-0100.127 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Cyanide – Screening Sheet WLC-0101.127A Not Created

3 years Daily ! U: Drive

Page 16: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 14 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Cyanide – Bench Sheet WLC-0101.127B Not Created

3 years Daily ! U: Drive

Fecal Coliform Analysis WLC-0100.128 0 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Fecal Coliform – Bench Sheet

WLC-0101.128 1 3 years Daily ! U: Drive

Nitrates Analysis WLC-0100.134 0 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Nitrates – Bench Sheet WLC-0101.134 0 3 years Daily ! U: Drive

Nitrate & Nitrite Analysis – FIAS Method

WLC-0100.136 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Nitrate & Nitrite – FIAS Method Bench Sheet

WLC-0101.136 Not Created

3 years Daily ! U: Drive

pH Analysis WLC-0100.137 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

pH Bench Sheet WLC-0101.137 Not Created

3 years Daily ! U: Drive

Ortho-Phosphorus Analysis WLC-0100.138 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Ortho-Phosphorus – Bench Sheet

WLC-0101.138 Not Created

3 years Daily ! U: Drive

Total Phosphorus Analysis WLC-0100.139 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Total Phosphorus – Bench Sheet

WLC-0101.139 Not Created

3 years Daily ! U: Drive

Page 17: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 15 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Residual Chlorine Analysis WLC-0100.140 1 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Residual Chlorine – Bench Sheet

WLC-0101.140A 0 3 years Daily ! U: Drive

PAO Standardization Bench Sheet

WLC-0101.140B Not Created

3 years Daily ! U: Drive

Lime Stabilization Sludge pH Analysis

WLC-0100.142 0 3 years As Needed ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Lime Stabilization Sludge pH Bench Sheet

WLC-0101.142 2 3 years As Needed ! U: Drive

Solids - % Total Solids/% Total Volatile Solids Analysis

WLC-0100.143 DRAFT 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Solids - % Total Solids/% Total Volatile Solids Bench Sheet

WLC-0101.143 DRAFT 3 years Daily ! U: Drive

Solids - Total Solids/Total Volatile Solids Analysis

WLC-0100.144 Not Created

3 years 2x/week ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Solids - Total Solids/Total Volatile Solids Bench Sheet

WLC-0101.144 Not Created

3 years 2x/week ! U: Drive

Total Suspended/Total Volatile Suspended Solids Analysis

WLC-0100.145 DRAFT 3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Total Suspended/Volatile Suspended Solids Bench Sheet

WLC-0101.145A DRAFT 3 years Daily ! U: Drive

Total Suspended/Volatile Suspended Solids Quarterly Drying Check Bench Sheet

WLC-0101.145B DRAFT 3 years Daily ! U: Drive

Page 18: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 16 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Total Kjeldahl Nitrogen Analysis

WLC-0100.146 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

Total Nitrogen – Dechlorination Log

WLC-0101.146A 0 3 years Daily ! U: Drive

Total Kjeldahl Nitrogen – Bench Sheet

WLC-0101.146B Not Created

3 years Daily ! U: Drive

Volatile Acids Analysis WLC-0100.147 Not Created

3 years Daily ! U: Drive 1. Long Creek Lab 2. LC Lab Supervisors Office

CROWDERS LABORATORY DOCUMENTSGeneral Laboratory Techniques

WCR-0100.101 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Standard Curve Bench Sheet

WCR-0101.101 Not Created

3 years Daily ! U: Drive

Quality Control Testing WCR-0100.102 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Laboratory Checks and Calibrations

WCR-0100.103 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Refrigerator Temperature Log

WCR-0101.103A 0 3 years Daily ! U: Drive

Oven Temperature Log WCR-0101.103B 0 3 years Daily ! U: Drive

Balance Calibration Log WCR-0101.103C 0 3 years Daily ! U: Drive Autoclave Log WCR-0101.103D 0 3 years As Needed ! U: Drive

Fecal Bath Temperature Log WCR-0101.103E 0 3 years Daily ! U: Drive

Incubator/Cold Room Temperature Log

WCR-0101.103F N/A 3 years Daily ! U: Drive

Accumet 25 Meter pH Calibration Log Book

WCR-0101.103G N/A 3 years As Needed Crowders Laboratory

Page 19: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Accumet 50 Meter pH Calibration Log Book

WCR-0101.103H N/A 3 years As Needed Crowders Laboratory

Denver 225 Meter pH Calibration Log Book

WCR-0101.103I N/A 3 years As Needed Crowders Laboratory

Reagent Log Book WCR-0101.103J N/A 3 years As Needed Crowders Laboratory

Annual QC/Safety Schedule Checklist

WCR-0101.103K 0 3 years As Needed ! U: Drive

Drierite Drying & Changing Log

WCR-0101.103L 0 3 years As Needed ! U: Drive

Washing and Preparation of Glassware and Bottles

WCR-0100.104 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Sample Bottle Set Up and Receiving

WCR-0100.105 0 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Chain of Custody for Crowders – Generic

WCR-0101.105A 1 3 years As Needed ! U: Drive

Chain of Custody for Crowders – Grabs – Daily

WCR-0101.105B 0 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Grabs – LTM

WCR-0101.105C 0 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Land Application %TS

WCR-0101.105D 1 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Land Application - Fecal

WCR-0101.105E 1 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Page 1 – Tuesday, Thursday

WCR-0101.105F 2 3 years 1x/week ! U: Drive

Chain of Custody for Crowders – Page 1 – Friday

WCR-0101.105G 2 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Page 1 – Long Term Monitoring

WCR-0101.105H 3 3 years 3x/week ! U: Drive

Page 20: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 18 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Chain of Custody for Crowders – Page 1 – Monday

WCR-0101.105I 2 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Page 2 – Monday & Friday

WCR-0101.105J 2 3 years 3x/week ! U: Drive

Chain of Custody for Crowders – Page 2 – Tuesday, Wednesday, Thursday

WCR-0101.105K 2 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Page 3 – 2nd, 4th & 4th Friday

WCR-0101.105L 2 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Page 3 – 3rd Friday

WCR-0101.105M 2 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Page 3 – Long Term Monitoring

WCR-0101.105N 3 3 years 2x/Month ! U: Drive

Chain of Custody for Crowders – Page 3 – Monday

WCR-0101.105O 1 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Page 3 – Thursday

WCR-0101.105P 1 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Page 3 – Tuesday

WCR-0101.105Q 2 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Page 3 – Wednesday

WCR-0101.105R 1 3 years 1x/week ! U: Drive

Chain of Custody for Crowders – Sent to Long Creek - Friday

WCR-0101.105S 2 3 years 2x/week ! U: Drive

Chain of Custody for Crowders – Sent to Long Creek - LTM

WCR-0101.105T 3 3 years Monthly ! U: Drive

Chain of Custody for Crowders – Sent to Long Creek - Monday

WCR-0101.105U 1 3 years Daily ! U: Drive

Page 21: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 19 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Chain of Custody for Crowders – Sent to Long Creek - Tuesday

WCR-0101.105V 2 3 years Daily ! U: Drive

Chain of Custody for Crowders – Sent to Long Creek – Wed, Thurs.

WCR-0101.105W 1 3 years Daily ! U: Drive

Chain of Custody for Crowders – Saturday

WCR-0101.105X 2 3 years Daily ! U: Drive

Data Verification WCR-0100.106 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Data Entry WCR-0100.107 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Mercury Spill Clean Up Procedure

WCR-0100.108 Draft 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Inorganic Acid & Base Spill Clean Up Procedure

WCR-0100.109 Draft 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Laboratory Waste Chemical Storage/Disposal

WCR-0100.110 Draft 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Sample Receiving WCR-0100.111 0 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

WCR-0100.112 0 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office 3. CR Operations Room

Alkalinity Analysis WCR-0100.121 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Page 22: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Alkalinity/Volatile Acid Bench Sheet

WCR-0101.121 Not Created

3 years Daily ! U: Drive

Ammonia Nitrogen Analysis WCR-0100.122 Draft 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Ammonia Nitrogen Dechlorination Log

WCR-0101.122A Not Created

3 years Daily ! U: Drive

Ammonia Nitrogen – Bench Sheet

WCR-0101.122B Not Created

3 years Daily ! U: Drive

Ammonia Nitrogen Distillation Method

WCR-0100.123 0 3 years Quarterly ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Ammonia Nitrogen Distillation -Bench Sheet

WCR-0101.123 Not Created

3 years Quarterly ! U: Drive

Biochemical Oxygen Demand Analysis

WCR-0100.124 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Biochemical Oxygen Demand Bench Sheet

WCR-0101.124 Not Created

3 years As Needed ! U: Drive

Biochemical Oxygen Demand – Winkler Method

WCR-0100.149 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Chemical Oxygen Demand Analysis

WCR-0100.125 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Chemical Oxygen Demand – Bench Sheet

WCR-0101.125 Not Created

3 years Daily ! U: Drive

Conductivity Analysis WCR-0100.126 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Conductivity Bench Sheet WCR-0101.126A Not Created

3 years As Needed ! U: Drive

Page 23: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 21 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Conductivity Quarterly Temperature Check Bench Sheet

WCR-0101.126B Not Created

3 years As Needed ! U: Drive

ADMI Color Analysis WCR-0100.150 1 3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

ADMI Color Sample Preparation Log

WCR-0101.150A 0 3 years As Needed ! U: Drive

ADMI Color Sample Calculation Sheet

WCR-0101.150B 0 3 years As Needed ! U: Drive

Cyanide – Screening Sheet WCR-0101.127A Draft 3 years Daily ! U: Drive

Fecal Coliform Analysis WCR-0100.128 0 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Fecal Coliform – Bench Sheet

WCR-0101.128 1 3 years Daily ! U: Drive

Metals – Flame Analysis WCR-0100.129 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Metals – Bench Sheet WCR-0101.129 Not Created

3 years As Needed ! U: Drive

Metals – Furnace Analysis Procedure

WCR-0100.130 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Metals – Mercury Analysis WCR-0100.131 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Mercury Digestion Log Sheet

WCR-0101.131 Not Created

3 years As Needed ! U: Drive

Metals Digestion Procedure – For Silver

WCR-0100.132 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Hot Plate Digestion Log Sheet

WCR-0101.132 Not Created

3 years As Needed ! U: Drive

Page 24: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 22 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

Metals Digestion Procedure – Microwave

WCR-0100.133 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Microwave Digestion Log Sheet

WCR-0101.133 Not Created

3 years As Needed ! U: Drive

Nitrates Analysis WCR-0100.134 0 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Nitrates –Bench Sheet WCR-0101.134 0 3 years Daily Share Drive / Crowders Laboratory

pH Analysis WCR-0100.137 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

pH Bench Sheet WCR-0101.137 Not Created

3 years Daily ! U: Drive

Ortho-Phosphorus Analysis WCR-0100.138 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Ortho-Phosphorus – Bench Sheet

WCR-0101.138 Not Created

3 years Daily ! U: Drive

Total Phosphorus Analysis WCR-0100.139 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Total Phosphorus – Bench Sheet

WCR-0101.139 Not Created

3 years Daily ! U: Drive

Residual Chlorine Analysis WCR-0100.140 0 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Residual Chlorine – Bench Sheet

WCR-0101.140A 1 3 years Daily ! U: Drive

Standardization of 0.00564 N PAO Bench Sheet

WCR-0101.140B Not Created

3 years Monthly ! U: Drive

Page 25: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 23 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title Document # Revision Retain Frequency Controlled Copy Locations

40 Day Vector Test Analysis WCR-0100.141 Not Created

3 years As Needed ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

40 Day Vector Test – Bench Sheet – 1

WCR-0101.141A Not Created

3 years As Needed ! U: Drive

40 Day Vector Test – Bench Sheet – 2

WCR-0101.141B Not Created

3 years As Needed ! U: Drive

Solids - % Total Solids/% Total Volatile Solids Analysis

WCR-0100.143 0 3 years 2x/week & As needed

! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Bench Sheet for Solids – Percent, Total and Volatile

WCR-0101.143A 0 3 years As needed ! U: Drive

Calculation Sheet for Solids – Percent, Total and Volatile

WCR-0101.143B 0 3 years As needed ! U: Drive

Solids – Total Solids/Total Volatile Solids Analysis

WCR-0100.144 0 3 years 2x/week ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Total Suspended/Total Volatile Suspended Solids Analysis

WCR-0100.145 0 3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

Total Suspended/Total Volatile Suspended Solids Bench Sheet

WCR-0101.145A 0 3 years Daily ! U: Drive

Total Suspended/Total Volatile Suspended Solids Quarterly Drying Check Bench Sheet

WCR-0101.145B 0 3 years Daily ! U: Drive

Total Nitrogen – Dechlorination Log

WCR-0101.146A Draft 3 years Daily ! U: Drive

Volatile Acids Analysis WCR-0100.147 Not Created

3 years Daily ! U: Drive 1. Crowders Laboratory 2. CR Lab Supervisor's Office

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

EMS MANAGEMENT DOCUMENTSEnvironment Management System Manual

EMS Review Procedure

Legal and Other Requirements Listing

Pressure Vessel Inspection Information (Legal Requirements Addendum)

Document Control Procedure

Document Control Training MatrixIndividual Training Matrix

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

Corrective/Preventative Action Report Procedure

Corrective/Preventative Action Report Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Training Procedure

Procedure Training Sign-In Sheet

Roles and Responsibilities Listing

Objective and Targets - Improvement Plan Summary

External Communications Procedure

Compliance Review Procedure

Summary of Activities and NPDES Permit Limit/SOC ViolationsRisk Management Plan

Environmental Management System Audit

Aspects and Impacts Procedure

Aspect Ranking Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Significant Aspects Determination Form

Significant Aspects Listing Form

Monitoring and Measuring Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

LONG CREEK OPERATIONSProceduresEmergency Response Plan

Main Lift Failure Procedure

Long Creek / Duhart / Catawba Procedure for Significant Rain Events

Spill Clean Up and Reporting Procedure

Intermediate Lift Failure ProcedureChemical Receiving ProceduresOn Call Schedule

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request Form

Portable pH / DO Meter Calibration Form

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Page 30: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 28 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery Checklist

Chlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating Manual

Generator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log BookOperators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Operations Check Form - Old Blower BuildingOperations Check Form - New Blower BuildingOperations Check Form - Chlorine/SO2 BuildingOperations Check Form - Filter Building

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Operations Check Form - Secondary/Screw PumpsOperations Check Form - Digester BuildingOperations Check Form - DAF BuildingOperations Check Form - Chemical Feed BuildingOperations Check Form - New Main Lift BuildingOperations Check Form - Old Main Lift BuildingTemperature Check Influent / Effluent Log

CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

CROWDER OPERATION DOCrowder Spill Procedure

Sampling Procedure

Process Control

Emergency Response Plan

Main Lift Failure Procedure

Hi-Ran Panel Failure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Blower Operation Procedure

Waste Gas Burner Lighting ProcedureHolding Digester Transfer to Land Application Start Up

Holding Digester Transfer to Land Application Shut Down Procedure

Chemical Receiving Procedures

Return Sludge Procedure

Main Lift Failure Procedure

Spill Clean Up and Reporting Procedure

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request FormPortable pH / DO Meter Calibration Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery ChecklistChlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating ManualGenerator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log Book

Operators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Temperature Check Influent / Effluent Log CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

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Page 34: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

LONG CREEK LABORATORYStandard Methods Software (reference use only not a controlled document)

General Laboratory Techniques

Standard Curve Bench Sheet

Quality Control Testing

Laboratory Checks and Calibrations

Temperature Log

Thermometer Calibration ChartBalance Calibration Log

Autoclave Logbook

Safety Shower and Eyewash Test Log

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Page 35: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Emergency Water Supplies Checklist

Accumet 50 Meter pH Calibration Log BookOrion 720A Meters 1 & 2 pH Calibration Log Book

VWR 8015 Meter pH Calibration Log Book

Reagent Log Book

Annual QC/Safety Schedule ChecklistWashing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for LC – Blank

Chain of Custody for LC – Page 1 – Long Term Monitoring

Chain of Custody for LC – Page 1 – Monday, Thursday

Chain of Custody for LC – Page 1 – Saturday, Sunday

Chain of Custody for LC – Page 1 – Tuesday, Friday

Chain of Custody for LC – Page 1 – Wednesday

Chain of Custody for LC – Page 2 – Monday, Thursday

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Page 36: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 2 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 2 – Wednesday 1x Month

Chain of Custody for LC – Page 3 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 3 – Wednesday, 1x Month

Chain of Custody for LC – Page 3 – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – 3rd Friday

Chain of Custody for LC – Page 4 – To Crowders – Friday (Except 1st & 3rd)

Chain of Custody for LC – Page 4 – To Crowders – Long Term Monitoring

Chain of Custody for LC – Page 4 – To Crowders – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – Saturday, Sunday

Chain of Custody for LC – Page 4 – To Crowders – Tuesday

Chain of Custody for LC – Page 4 – To Crowders – Wednesday

Chain of Custody for LC – Page 5 – Grab Samples – Long Term Monitoring

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 5 – Grab Samples

Chain of Custody for LC – Page 1 – Holiday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Alkalinity Analysis

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Ammonia Nitrogen – Bench SheetAmmonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation – Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench Sheet

Biochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Conductivity Quarterly Temperature Check Bench SheetCyanide Analysis

Cyanide – Screening Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Cyanide – Bench Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Nitrates Analysis

Nitrates – Bench Sheet

Nitrate & Nitrite Analysis – FIAS Method

Nitrate & Nitrite – FIAS Method Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench Sheet

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Page 40: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Residual Chlorine Analysis

Residual Chlorine – Bench Sheet

PAO Standardization Bench Sheet

Lime Stabilization Sludge pH Analysis

Lime Stabilization Sludge pH Bench Sheet

Solids - % Total Solids/% Total Volatile Solids Analysis

Solids - % Total Solids/% Total Volatile Solids Bench Sheet

Solids - Total Solids/Total Volatile Solids Analysis

Solids - Total Solids/Total Volatile Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Volatile Suspended Solids Bench SheetTotal Suspended/Volatile Suspended Solids Quarterly Drying Check Bench Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Total Kjeldahl Nitrogen Analysis

Total Nitrogen – Dechlorination Log

Total Kjeldahl Nitrogen – Bench Sheet

Volatile Acids Analysis

CROWDERS LABORATORY DOCUMENTSGeneral Laboratory Techniques

Standard Curve Bench SheetQuality Control Testing

Laboratory Checks and Calibrations

Refrigerator Temperature LogOven Temperature Log

Balance Calibration LogAutoclave Log

Fecal Bath Temperature Log

Incubator/Cold Room Temperature Log

Accumet 25 Meter pH Calibration Log Book

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Accumet 50 Meter pH Calibration Log BookDenver 225 Meter pH Calibration Log BookReagent Log Book

Annual QC/Safety Schedule Checklist

Drierite Drying & Changing Log

Washing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for Crowders – Generic

Chain of Custody for Crowders – Grabs – DailyChain of Custody for Crowders – Grabs – LTM

Chain of Custody for Crowders – Land Application %TS

Chain of Custody for Crowders – Land Application - Fecal

Chain of Custody for Crowders – Page 1 – Tuesday, Thursday

Chain of Custody for Crowders – Page 1 – Friday

Chain of Custody for Crowders – Page 1 – Long Term Monitoring

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Page 43: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Page 1 – Monday

Chain of Custody for Crowders – Page 2 – Monday & Friday

Chain of Custody for Crowders – Page 2 – Tuesday, Wednesday, Thursday

Chain of Custody for Crowders – Page 3 – 2nd, 4th & 4th Friday

Chain of Custody for Crowders – Page 3 – 3rd Friday

Chain of Custody for Crowders – Page 3 – Long Term Monitoring

Chain of Custody for Crowders – Page 3 – Monday

Chain of Custody for Crowders – Page 3 – Thursday

Chain of Custody for Crowders – Page 3 – Tuesday

Chain of Custody for Crowders – Page 3 – Wednesday

Chain of Custody for Crowders – Sent to Long Creek - Friday

Chain of Custody for Crowders – Sent to Long Creek - LTM

Chain of Custody for Crowders – Sent to Long Creek - Monday

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Page 44: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Sent to Long Creek - Tuesday

Chain of Custody for Crowders – Sent to Long Creek – Wed, Thurs.

Chain of Custody for Crowders – Saturday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

Alkalinity Analysis

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Page 45: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

Ammonia Nitrogen – Bench Sheet

Ammonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation -Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench SheetBiochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

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Page 46: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Conductivity Quarterly Temperature Check Bench SheetADMI Color Analysis

ADMI Color Sample Preparation Log

ADMI Color Sample Calculation Sheet

Cyanide – Screening Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Metals – Flame Analysis

Metals – Bench Sheet

Metals – Furnace Analysis Procedure

Metals – Mercury Analysis

Mercury Digestion Log Sheet

Metals Digestion Procedure – For Silver

Hot Plate Digestion Log Sheet

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Page 47: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Metals Digestion Procedure – Microwave

Microwave Digestion Log Sheet

Nitrates Analysis

Nitrates –Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench SheetResidual Chlorine Analysis

Residual Chlorine – Bench Sheet

Standardization of 0.00564 N PAO Bench Sheet

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Page 48: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

40 Day Vector Test Analysis

40 Day Vector Test – Bench Sheet – 1

40 Day Vector Test – Bench Sheet – 2

Solids - % Total Solids/% Total Volatile Solids Analysis

Bench Sheet for Solids – Percent, Total and Volatile

Calculation Sheet for Solids – Percent, Total and Volatile

Solids – Total Solids/Total Volatile Solids Analysis

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Total Volatile Suspended Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Total Nitrogen – Dechlorination Log

Volatile Acids Analysis

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

EMS MANAGEMENT DOCUMENTSEnvironment Management System Manual

EMS Review Procedure

Legal and Other Requirements Listing

Pressure Vessel Inspection Information (Legal Requirements Addendum)

Document Control Procedure

Document Control Training MatrixIndividual Training Matrix

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

Corrective/Preventative Action Report Procedure

Corrective/Preventative Action Report Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Training Procedure

Procedure Training Sign-In Sheet

Roles and Responsibilities Listing

Objective and Targets - Improvement Plan Summary

External Communications Procedure

Compliance Review Procedure

Summary of Activities and NPDES Permit Limit/SOC ViolationsRisk Management Plan

Environmental Management System Audit

Aspects and Impacts Procedure

Aspect Ranking Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Significant Aspects Determination Form

Significant Aspects Listing Form

Monitoring and Measuring Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

LONG CREEK OPERATIONSProceduresEmergency Response Plan

Main Lift Failure Procedure

Long Creek / Duhart / Catawba Procedure for Significant Rain Events

Spill Clean Up and Reporting Procedure

Intermediate Lift Failure ProcedureChemical Receiving ProceduresOn Call Schedule

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request Form

Portable pH / DO Meter Calibration Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery Checklist

Chlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating Manual

Generator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log BookOperators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Operations Check Form - Old Blower BuildingOperations Check Form - New Blower BuildingOperations Check Form - Chlorine/SO2 BuildingOperations Check Form - Filter Building

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Operations Check Form - Secondary/Screw PumpsOperations Check Form - Digester BuildingOperations Check Form - DAF BuildingOperations Check Form - Chemical Feed BuildingOperations Check Form - New Main Lift BuildingOperations Check Form - Old Main Lift BuildingTemperature Check Influent / Effluent Log

CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

CROWDER OPERATION DOCrowder Spill Procedure

Sampling Procedure

Process Control

Emergency Response Plan

Main Lift Failure Procedure

Hi-Ran Panel Failure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Blower Operation Procedure

Waste Gas Burner Lighting ProcedureHolding Digester Transfer to Land Application Start Up

Holding Digester Transfer to Land Application Shut Down Procedure

Chemical Receiving Procedures

Return Sludge Procedure

Main Lift Failure Procedure

Spill Clean Up and Reporting Procedure

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request FormPortable pH / DO Meter Calibration Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery ChecklistChlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating ManualGenerator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log Book

Operators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Temperature Check Influent / Effluent Log CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

LONG CREEK LABORATORYStandard Methods Software (reference use only not a controlled document)

General Laboratory Techniques

Standard Curve Bench Sheet

Quality Control Testing

Laboratory Checks and Calibrations

Temperature Log

Thermometer Calibration ChartBalance Calibration Log

Autoclave Logbook

Safety Shower and Eyewash Test Log

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Emergency Water Supplies Checklist

Accumet 50 Meter pH Calibration Log BookOrion 720A Meters 1 & 2 pH Calibration Log Book

VWR 8015 Meter pH Calibration Log Book

Reagent Log Book

Annual QC/Safety Schedule ChecklistWashing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for LC – Blank

Chain of Custody for LC – Page 1 – Long Term Monitoring

Chain of Custody for LC – Page 1 – Monday, Thursday

Chain of Custody for LC – Page 1 – Saturday, Sunday

Chain of Custody for LC – Page 1 – Tuesday, Friday

Chain of Custody for LC – Page 1 – Wednesday

Chain of Custody for LC – Page 2 – Monday, Thursday

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 2 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 2 – Wednesday 1x Month

Chain of Custody for LC – Page 3 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 3 – Wednesday, 1x Month

Chain of Custody for LC – Page 3 – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – 3rd Friday

Chain of Custody for LC – Page 4 – To Crowders – Friday (Except 1st & 3rd)

Chain of Custody for LC – Page 4 – To Crowders – Long Term Monitoring

Chain of Custody for LC – Page 4 – To Crowders – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – Saturday, Sunday

Chain of Custody for LC – Page 4 – To Crowders – Tuesday

Chain of Custody for LC – Page 4 – To Crowders – Wednesday

Chain of Custody for LC – Page 5 – Grab Samples – Long Term Monitoring

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Page 60: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 58 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 5 – Grab Samples

Chain of Custody for LC – Page 1 – Holiday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Alkalinity Analysis

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Ammonia Nitrogen – Bench SheetAmmonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation – Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench Sheet

Biochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Conductivity Quarterly Temperature Check Bench SheetCyanide Analysis

Cyanide – Screening Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Cyanide – Bench Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Nitrates Analysis

Nitrates – Bench Sheet

Nitrate & Nitrite Analysis – FIAS Method

Nitrate & Nitrite – FIAS Method Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Residual Chlorine Analysis

Residual Chlorine – Bench Sheet

PAO Standardization Bench Sheet

Lime Stabilization Sludge pH Analysis

Lime Stabilization Sludge pH Bench Sheet

Solids - % Total Solids/% Total Volatile Solids Analysis

Solids - % Total Solids/% Total Volatile Solids Bench Sheet

Solids - Total Solids/Total Volatile Solids Analysis

Solids - Total Solids/Total Volatile Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Volatile Suspended Solids Bench SheetTotal Suspended/Volatile Suspended Solids Quarterly Drying Check Bench Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Total Kjeldahl Nitrogen Analysis

Total Nitrogen – Dechlorination Log

Total Kjeldahl Nitrogen – Bench Sheet

Volatile Acids Analysis

CROWDERS LABORATORY DOCUMENTSGeneral Laboratory Techniques

Standard Curve Bench SheetQuality Control Testing

Laboratory Checks and Calibrations

Refrigerator Temperature LogOven Temperature Log

Balance Calibration LogAutoclave Log

Fecal Bath Temperature Log

Incubator/Cold Room Temperature Log

Accumet 25 Meter pH Calibration Log Book

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Accumet 50 Meter pH Calibration Log BookDenver 225 Meter pH Calibration Log BookReagent Log Book

Annual QC/Safety Schedule Checklist

Drierite Drying & Changing Log

Washing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for Crowders – Generic

Chain of Custody for Crowders – Grabs – DailyChain of Custody for Crowders – Grabs – LTM

Chain of Custody for Crowders – Land Application %TS

Chain of Custody for Crowders – Land Application - Fecal

Chain of Custody for Crowders – Page 1 – Tuesday, Thursday

Chain of Custody for Crowders – Page 1 – Friday

Chain of Custody for Crowders – Page 1 – Long Term Monitoring

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Page 1 – Monday

Chain of Custody for Crowders – Page 2 – Monday & Friday

Chain of Custody for Crowders – Page 2 – Tuesday, Wednesday, Thursday

Chain of Custody for Crowders – Page 3 – 2nd, 4th & 4th Friday

Chain of Custody for Crowders – Page 3 – 3rd Friday

Chain of Custody for Crowders – Page 3 – Long Term Monitoring

Chain of Custody for Crowders – Page 3 – Monday

Chain of Custody for Crowders – Page 3 – Thursday

Chain of Custody for Crowders – Page 3 – Tuesday

Chain of Custody for Crowders – Page 3 – Wednesday

Chain of Custody for Crowders – Sent to Long Creek - Friday

Chain of Custody for Crowders – Sent to Long Creek - LTM

Chain of Custody for Crowders – Sent to Long Creek - Monday

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Sent to Long Creek - Tuesday

Chain of Custody for Crowders – Sent to Long Creek – Wed, Thurs.

Chain of Custody for Crowders – Saturday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

Alkalinity Analysis

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

Ammonia Nitrogen – Bench Sheet

Ammonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation -Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench SheetBiochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Conductivity Quarterly Temperature Check Bench SheetADMI Color Analysis

ADMI Color Sample Preparation Log

ADMI Color Sample Calculation Sheet

Cyanide – Screening Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Metals – Flame Analysis

Metals – Bench Sheet

Metals – Furnace Analysis Procedure

Metals – Mercury Analysis

Mercury Digestion Log Sheet

Metals Digestion Procedure – For Silver

Hot Plate Digestion Log Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Metals Digestion Procedure – Microwave

Microwave Digestion Log Sheet

Nitrates Analysis

Nitrates –Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench SheetResidual Chlorine Analysis

Residual Chlorine – Bench Sheet

Standardization of 0.00564 N PAO Bench Sheet

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

40 Day Vector Test Analysis

40 Day Vector Test – Bench Sheet – 1

40 Day Vector Test – Bench Sheet – 2

Solids - % Total Solids/% Total Volatile Solids Analysis

Bench Sheet for Solids – Percent, Total and Volatile

Calculation Sheet for Solids – Percent, Total and Volatile

Solids – Total Solids/Total Volatile Solids Analysis

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Total Volatile Suspended Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Total Nitrogen – Dechlorination Log

Volatile Acids Analysis

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

EMS MANAGEMENT DOCUMENTSEnvironment Management System Manual

EMS Review Procedure

Legal and Other Requirements Listing

Pressure Vessel Inspection Information (Legal Requirements Addendum)

Document Control Procedure

Document Control Training MatrixIndividual Training Matrix

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

Corrective/Preventative Action Report Procedure

Corrective/Preventative Action Report Form

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Training Procedure

Procedure Training Sign-In Sheet

Roles and Responsibilities Listing

Objective and Targets - Improvement Plan Summary

External Communications Procedure

Compliance Review Procedure

Summary of Activities and NPDES Permit Limit/SOC ViolationsRisk Management Plan

Environmental Management System Audit

Aspects and Impacts Procedure

Aspect Ranking Form

Page 74: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Significant Aspects Determination Form

Significant Aspects Listing Form

Monitoring and Measuring Procedure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

LONG CREEK OPERATIONSProceduresEmergency Response Plan

Main Lift Failure Procedure

Long Creek / Duhart / Catawba Procedure for Significant Rain Events

Spill Clean Up and Reporting Procedure

Intermediate Lift Failure ProcedureChemical Receiving ProceduresOn Call Schedule

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request Form

Portable pH / DO Meter Calibration Form

Page 76: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 74 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery Checklist

Chlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating Manual

Generator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log BookOperators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Operations Check Form - Old Blower BuildingOperations Check Form - New Blower BuildingOperations Check Form - Chlorine/SO2 BuildingOperations Check Form - Filter Building

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Operations Check Form - Secondary/Screw PumpsOperations Check Form - Digester BuildingOperations Check Form - DAF BuildingOperations Check Form - Chemical Feed BuildingOperations Check Form - New Main Lift BuildingOperations Check Form - Old Main Lift BuildingTemperature Check Influent / Effluent Log

CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

CROWDER OPERATION DOCrowder Spill Procedure

Sampling Procedure

Process Control

Emergency Response Plan

Main Lift Failure Procedure

Hi-Ran Panel Failure

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Blower Operation Procedure

Waste Gas Burner Lighting ProcedureHolding Digester Transfer to Land Application Start Up

Holding Digester Transfer to Land Application Shut Down Procedure

Chemical Receiving Procedures

Return Sludge Procedure

Main Lift Failure Procedure

Spill Clean Up and Reporting Procedure

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request FormPortable pH / DO Meter Calibration Form

Page 79: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 77 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery ChecklistChlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating ManualGenerator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log Book

Operators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Temperature Check Influent / Effluent Log CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Page 80: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 78 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

LONG CREEK LABORATORYStandard Methods Software (reference use only not a controlled document)

General Laboratory Techniques

Standard Curve Bench Sheet

Quality Control Testing

Laboratory Checks and Calibrations

Temperature Log

Thermometer Calibration ChartBalance Calibration Log

Autoclave Logbook

Safety Shower and Eyewash Test Log

Page 81: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 79 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Emergency Water Supplies Checklist

Accumet 50 Meter pH Calibration Log BookOrion 720A Meters 1 & 2 pH Calibration Log Book

VWR 8015 Meter pH Calibration Log Book

Reagent Log Book

Annual QC/Safety Schedule ChecklistWashing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for LC – Blank

Chain of Custody for LC – Page 1 – Long Term Monitoring

Chain of Custody for LC – Page 1 – Monday, Thursday

Chain of Custody for LC – Page 1 – Saturday, Sunday

Chain of Custody for LC – Page 1 – Tuesday, Friday

Chain of Custody for LC – Page 1 – Wednesday

Chain of Custody for LC – Page 2 – Monday, Thursday

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 2 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 2 – Wednesday 1x Month

Chain of Custody for LC – Page 3 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 3 – Wednesday, 1x Month

Chain of Custody for LC – Page 3 – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – 3rd Friday

Chain of Custody for LC – Page 4 – To Crowders – Friday (Except 1st & 3rd)

Chain of Custody for LC – Page 4 – To Crowders – Long Term Monitoring

Chain of Custody for LC – Page 4 – To Crowders – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – Saturday, Sunday

Chain of Custody for LC – Page 4 – To Crowders – Tuesday

Chain of Custody for LC – Page 4 – To Crowders – Wednesday

Chain of Custody for LC – Page 5 – Grab Samples – Long Term Monitoring

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 5 – Grab Samples

Chain of Custody for LC – Page 1 – Holiday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Alkalinity Analysis

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Ammonia Nitrogen – Bench SheetAmmonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation – Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench Sheet

Biochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Conductivity Quarterly Temperature Check Bench SheetCyanide Analysis

Cyanide – Screening Sheet

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Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 83 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Cyanide – Bench Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Nitrates Analysis

Nitrates – Bench Sheet

Nitrate & Nitrite Analysis – FIAS Method

Nitrate & Nitrite – FIAS Method Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench Sheet

Page 86: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 84 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Residual Chlorine Analysis

Residual Chlorine – Bench Sheet

PAO Standardization Bench Sheet

Lime Stabilization Sludge pH Analysis

Lime Stabilization Sludge pH Bench Sheet

Solids - % Total Solids/% Total Volatile Solids Analysis

Solids - % Total Solids/% Total Volatile Solids Bench Sheet

Solids - Total Solids/Total Volatile Solids Analysis

Solids - Total Solids/Total Volatile Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Volatile Suspended Solids Bench SheetTotal Suspended/Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Page 87: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 85 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Total Kjeldahl Nitrogen Analysis

Total Nitrogen – Dechlorination Log

Total Kjeldahl Nitrogen – Bench Sheet

Volatile Acids Analysis

CROWDERS LABORATORY DOCUMENTSGeneral Laboratory Techniques

Standard Curve Bench SheetQuality Control Testing

Laboratory Checks and Calibrations

Refrigerator Temperature LogOven Temperature Log

Balance Calibration LogAutoclave Log

Fecal Bath Temperature Log

Incubator/Cold Room Temperature Log

Accumet 25 Meter pH Calibration Log Book

Page 88: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 86 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Accumet 50 Meter pH Calibration Log BookDenver 225 Meter pH Calibration Log BookReagent Log Book

Annual QC/Safety Schedule Checklist

Drierite Drying & Changing Log

Washing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for Crowders – Generic

Chain of Custody for Crowders – Grabs – DailyChain of Custody for Crowders – Grabs – LTM

Chain of Custody for Crowders – Land Application %TS

Chain of Custody for Crowders – Land Application - Fecal

Chain of Custody for Crowders – Page 1 – Tuesday, Thursday

Chain of Custody for Crowders – Page 1 – Friday

Chain of Custody for Crowders – Page 1 – Long Term Monitoring

Page 89: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 87 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Page 1 – Monday

Chain of Custody for Crowders – Page 2 – Monday & Friday

Chain of Custody for Crowders – Page 2 – Tuesday, Wednesday, Thursday

Chain of Custody for Crowders – Page 3 – 2nd, 4th & 4th Friday

Chain of Custody for Crowders – Page 3 – 3rd Friday

Chain of Custody for Crowders – Page 3 – Long Term Monitoring

Chain of Custody for Crowders – Page 3 – Monday

Chain of Custody for Crowders – Page 3 – Thursday

Chain of Custody for Crowders – Page 3 – Tuesday

Chain of Custody for Crowders – Page 3 – Wednesday

Chain of Custody for Crowders – Sent to Long Creek - Friday

Chain of Custody for Crowders – Sent to Long Creek - LTM

Chain of Custody for Crowders – Sent to Long Creek - Monday

Page 90: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 88 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Sent to Long Creek - Tuesday

Chain of Custody for Crowders – Sent to Long Creek – Wed, Thurs.

Chain of Custody for Crowders – Saturday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

Alkalinity Analysis

Page 91: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 89 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

Ammonia Nitrogen – Bench Sheet

Ammonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation -Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench SheetBiochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Page 92: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 90 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Conductivity Quarterly Temperature Check Bench SheetADMI Color Analysis

ADMI Color Sample Preparation Log

ADMI Color Sample Calculation Sheet

Cyanide – Screening Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Metals – Flame Analysis

Metals – Bench Sheet

Metals – Furnace Analysis Procedure

Metals – Mercury Analysis

Mercury Digestion Log Sheet

Metals Digestion Procedure – For Silver

Hot Plate Digestion Log Sheet

Page 93: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 91 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Metals Digestion Procedure – Microwave

Microwave Digestion Log Sheet

Nitrates Analysis

Nitrates –Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench SheetResidual Chlorine Analysis

Residual Chlorine – Bench Sheet

Standardization of 0.00564 N PAO Bench Sheet

Page 94: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 92 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

40 Day Vector Test Analysis

40 Day Vector Test – Bench Sheet – 1

40 Day Vector Test – Bench Sheet – 2

Solids - % Total Solids/% Total Volatile Solids Analysis

Bench Sheet for Solids – Percent, Total and Volatile

Calculation Sheet for Solids – Percent, Total and Volatile

Solids – Total Solids/Total Volatile Solids Analysis

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Total Volatile Suspended Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Total Nitrogen – Dechlorination Log

Volatile Acids Analysis

Page 95: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 93 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

EMS MANAGEMENT DOCUMENTSEnvironment Management System Manual

EMS Review Procedure

Legal and Other Requirements Listing

Pressure Vessel Inspection Information (Legal Requirements Addendum)

Document Control Procedure

Document Control Training MatrixIndividual Training Matrix

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

Corrective/Preventative Action Report Procedure

Corrective/Preventative Action Report Form

Page 96: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 94 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Training Procedure

Procedure Training Sign-In Sheet

Roles and Responsibilities Listing

Objective and Targets - Improvement Plan Summary

External Communications Procedure

Compliance Review Procedure

Summary of Activities and NPDES Permit Limit/SOC ViolationsRisk Management Plan

Environmental Management System Audit

Aspects and Impacts Procedure

Aspect Ranking Form

Page 97: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 95 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Significant Aspects Determination Form

Significant Aspects Listing Form

Monitoring and Measuring Procedure

Page 98: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 96 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

LONG CREEK OPERATIONSProceduresEmergency Response Plan

Main Lift Failure Procedure

Long Creek / Duhart / Catawba Procedure for Significant Rain Events

Spill Clean Up and Reporting Procedure

Intermediate Lift Failure ProcedureChemical Receiving ProceduresOn Call Schedule

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request Form

Portable pH / DO Meter Calibration Form

Page 99: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 97 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery Checklist

Chlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating Manual

Generator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log BookOperators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Operations Check Form - Old Blower BuildingOperations Check Form - New Blower BuildingOperations Check Form - Chlorine/SO2 BuildingOperations Check Form - Filter Building

Page 100: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 98 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Operations Check Form - Secondary/Screw PumpsOperations Check Form - Digester BuildingOperations Check Form - DAF BuildingOperations Check Form - Chemical Feed BuildingOperations Check Form - New Main Lift BuildingOperations Check Form - Old Main Lift BuildingTemperature Check Influent / Effluent Log

CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

CROWDER OPERATION DOCrowder Spill Procedure

Sampling Procedure

Process Control

Emergency Response Plan

Main Lift Failure Procedure

Hi-Ran Panel Failure

Page 101: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 99 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Blower Operation Procedure

Waste Gas Burner Lighting ProcedureHolding Digester Transfer to Land Application Start Up

Holding Digester Transfer to Land Application Shut Down Procedure

Chemical Receiving Procedures

Return Sludge Procedure

Main Lift Failure Procedure

Spill Clean Up and Reporting Procedure

Daily Operations Sheet

Microscopic Exam Form

Sample Collection Schedule

Special Sample Request FormPortable pH / DO Meter Calibration Form

Page 102: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 100 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Temperature Check on DO/pH/Chlorine Sampling Units

Chlorine / Sulfur Dioxide Delivery ChecklistChlorine / Sulfur Dioxide Change Out Checklist

Chlorine System Operating ManualGenerator Logs

Valve Exercise Program

H2S Gas Monitoring Report

Methane / H2S / SO2 / CL2 Gas Monitor Inspection

Lock Out / Tag Out Log Book

Operators Log Book

Fire Extinguisher Testing

Eye Wash / Shower Inspection

First Aid Kit

Respirators / SCBA’s

Equipment Work Orders

Temperature Check Influent / Effluent Log CL2/SO2 Hand Analyzer Calibration

Chemical Feed Log Sheet

Page 103: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 101 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Effluent Flow Meter Calibration Form

ISI Calibration Report

Influent Flow / RAS / WAS Meter Calibration Form

Stationary DO Meter Calibration Form

LONG CREEK LABORATORYStandard Methods Software (reference use only not a controlled document)

General Laboratory Techniques

Standard Curve Bench Sheet

Quality Control Testing

Laboratory Checks and Calibrations

Temperature Log

Thermometer Calibration ChartBalance Calibration Log

Autoclave Logbook

Safety Shower and Eyewash Test Log

Page 104: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 102 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Emergency Water Supplies Checklist

Accumet 50 Meter pH Calibration Log BookOrion 720A Meters 1 & 2 pH Calibration Log Book

VWR 8015 Meter pH Calibration Log Book

Reagent Log Book

Annual QC/Safety Schedule ChecklistWashing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for LC – Blank

Chain of Custody for LC – Page 1 – Long Term Monitoring

Chain of Custody for LC – Page 1 – Monday, Thursday

Chain of Custody for LC – Page 1 – Saturday, Sunday

Chain of Custody for LC – Page 1 – Tuesday, Friday

Chain of Custody for LC – Page 1 – Wednesday

Chain of Custody for LC – Page 2 – Monday, Thursday

Page 105: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 103 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 2 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 2 – Wednesday 1x Month

Chain of Custody for LC – Page 3 – Tuesday, Wednesday, Friday

Chain of Custody for LC – Page 3 – Wednesday, 1x Month

Chain of Custody for LC – Page 3 – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – 3rd Friday

Chain of Custody for LC – Page 4 – To Crowders – Friday (Except 1st & 3rd)

Chain of Custody for LC – Page 4 – To Crowders – Long Term Monitoring

Chain of Custody for LC – Page 4 – To Crowders – Monday, Thursday

Chain of Custody for LC – Page 4 – To Crowders – Saturday, Sunday

Chain of Custody for LC – Page 4 – To Crowders – Tuesday

Chain of Custody for LC – Page 4 – To Crowders – Wednesday

Chain of Custody for LC – Page 5 – Grab Samples – Long Term Monitoring

Page 106: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 104 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for LC – Page 5 – Grab Samples

Chain of Custody for LC – Page 1 – Holiday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Alkalinity Analysis

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

Page 107: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 105 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Ammonia Nitrogen – Bench SheetAmmonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation – Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench Sheet

Biochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Conductivity Quarterly Temperature Check Bench SheetCyanide Analysis

Cyanide – Screening Sheet

Page 108: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 106 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Cyanide – Bench Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Nitrates Analysis

Nitrates – Bench Sheet

Nitrate & Nitrite Analysis – FIAS Method

Nitrate & Nitrite – FIAS Method Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench Sheet

Page 109: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 107 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Residual Chlorine Analysis

Residual Chlorine – Bench Sheet

PAO Standardization Bench Sheet

Lime Stabilization Sludge pH Analysis

Lime Stabilization Sludge pH Bench Sheet

Solids - % Total Solids/% Total Volatile Solids Analysis

Solids - % Total Solids/% Total Volatile Solids Bench Sheet

Solids - Total Solids/Total Volatile Solids Analysis

Solids - Total Solids/Total Volatile Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Volatile Suspended Solids Bench SheetTotal Suspended/Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Page 110: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 108 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Total Kjeldahl Nitrogen Analysis

Total Nitrogen – Dechlorination Log

Total Kjeldahl Nitrogen – Bench Sheet

Volatile Acids Analysis

CROWDERS LABORATORY DOCUMENTSGeneral Laboratory Techniques

Standard Curve Bench SheetQuality Control Testing

Laboratory Checks and Calibrations

Refrigerator Temperature LogOven Temperature Log

Balance Calibration LogAutoclave Log

Fecal Bath Temperature Log

Incubator/Cold Room Temperature Log

Accumet 25 Meter pH Calibration Log Book

Page 111: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 109 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Accumet 50 Meter pH Calibration Log BookDenver 225 Meter pH Calibration Log BookReagent Log Book

Annual QC/Safety Schedule Checklist

Drierite Drying & Changing Log

Washing and Preparation of Glassware and Bottles

Sample Bottle Set Up and Receiving

Chain of Custody for Crowders – Generic

Chain of Custody for Crowders – Grabs – DailyChain of Custody for Crowders – Grabs – LTM

Chain of Custody for Crowders – Land Application %TS

Chain of Custody for Crowders – Land Application - Fecal

Chain of Custody for Crowders – Page 1 – Tuesday, Thursday

Chain of Custody for Crowders – Page 1 – Friday

Chain of Custody for Crowders – Page 1 – Long Term Monitoring

Page 112: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 110 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Page 1 – Monday

Chain of Custody for Crowders – Page 2 – Monday & Friday

Chain of Custody for Crowders – Page 2 – Tuesday, Wednesday, Thursday

Chain of Custody for Crowders – Page 3 – 2nd, 4th & 4th Friday

Chain of Custody for Crowders – Page 3 – 3rd Friday

Chain of Custody for Crowders – Page 3 – Long Term Monitoring

Chain of Custody for Crowders – Page 3 – Monday

Chain of Custody for Crowders – Page 3 – Thursday

Chain of Custody for Crowders – Page 3 – Tuesday

Chain of Custody for Crowders – Page 3 – Wednesday

Chain of Custody for Crowders – Sent to Long Creek - Friday

Chain of Custody for Crowders – Sent to Long Creek - LTM

Chain of Custody for Crowders – Sent to Long Creek - Monday

Page 113: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 111 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Chain of Custody for Crowders – Sent to Long Creek - Tuesday

Chain of Custody for Crowders – Sent to Long Creek – Wed, Thurs.

Chain of Custody for Crowders – Saturday

Data Verification

Data Entry

Mercury Spill Clean Up Procedure

Inorganic Acid & Base Spill Clean Up Procedure

Laboratory Waste Chemical Storage/Disposal

Sample Receiving

Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

Alkalinity Analysis

Page 114: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 112 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Alkalinity/Volatile Acid Bench Sheet

Ammonia Nitrogen Analysis

Ammonia Nitrogen Dechlorination Log

Ammonia Nitrogen – Bench Sheet

Ammonia Nitrogen Distillation Method

Ammonia Nitrogen Distillation -Bench Sheet

Biochemical Oxygen Demand Analysis

Biochemical Oxygen Demand Bench SheetBiochemical Oxygen Demand – Winkler Method

Chemical Oxygen Demand Analysis

Chemical Oxygen Demand – Bench Sheet

Conductivity Analysis

Conductivity Bench Sheet

Page 115: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 113 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Conductivity Quarterly Temperature Check Bench SheetADMI Color Analysis

ADMI Color Sample Preparation Log

ADMI Color Sample Calculation Sheet

Cyanide – Screening Sheet

Fecal Coliform Analysis

Fecal Coliform – Bench Sheet

Metals – Flame Analysis

Metals – Bench Sheet

Metals – Furnace Analysis Procedure

Metals – Mercury Analysis

Mercury Digestion Log Sheet

Metals Digestion Procedure – For Silver

Hot Plate Digestion Log Sheet

Page 116: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 114 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

Metals Digestion Procedure – Microwave

Microwave Digestion Log Sheet

Nitrates Analysis

Nitrates –Bench Sheet

pH Analysis

pH Bench Sheet

Ortho-Phosphorus Analysis

Ortho-Phosphorus – Bench Sheet

Total Phosphorus Analysis

Total Phosphorus – Bench SheetResidual Chlorine Analysis

Residual Chlorine – Bench Sheet

Standardization of 0.00564 N PAO Bench Sheet

Page 117: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Document Control Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 115 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 6/29/00Date Printed: 1/31/2001

Document Title

40 Day Vector Test Analysis

40 Day Vector Test – Bench Sheet – 1

40 Day Vector Test – Bench Sheet – 2

Solids - % Total Solids/% Total Volatile Solids Analysis

Bench Sheet for Solids – Percent, Total and Volatile

Calculation Sheet for Solids – Percent, Total and Volatile

Solids – Total Solids/Total Volatile Solids Analysis

Total Suspended/Total Volatile Suspended Solids Analysis

Total Suspended/Total Volatile Suspended Solids Bench Sheet

Total Suspended/Total Volatile Suspended Solids Quarterly Drying Check Bench Sheet

Total Nitrogen – Dechlorination Log

Volatile Acids Analysis

Page 118: Standard Operating Procedure - Training Procedure · Standard Operating Procedure – EMS-0100.005 Name: Training Procedure Cit Revision #: 1 ... Spill Clean Up and Reporting Procedure

Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 116 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

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Awareness Training N/A N/A 5/9/2000 5/9/2000 8/11/2000 8/29/2000 NR 5/9/2000 5/12/2000 9/11/2000 5/12/2000 5/12/2000 5/9/2000

Environment Management System Manual EMS-0100.000 0 NR 2/14/2000 NREMS Review Procedure EMS-0100.001 0

8/30/2000 2/14/2000 NR 4/10/2000 5/8/2000

Document Control Procedure EMS-0100.002 0 2/14/2000 NR 4/10/2000 5/8/2000

Aspects and Impacts Procedure EMS-0100.003 0 5/15/2000 2/14/2000 NR 5/10/2000 5/8/2000

Corrective/Preventative Action Report Procedure

EMS-0100.004 25/9/2000 5/9/2000 8/30/2000 8/29/2000 NR 5/9/2000 8/28/2000 9/11/2000 8/30/2000 8/30/2000 5/9/2000

Training Procedure EMS-0100.005 1 12/18/2000 NR 4/10/2000 12/18/2000

Roles and Responsibilities Listing EMS-0100.006 0 8/30/2000 2/14/2000 8/30/2000 8/29/2000 NR 4/10/2000 1/27/2000 5/8/2000

Objective and Targets - Improvement Plan Summary

EMS-0100.007 1 NR 8/29/2000 NRExternal Communications Procedure EMS-0100.008 1 6/28/2000 6/28/2000 8/11/2000 8/29/2000 NR 6/28/2000 6/29/2000 9/11/2000 8/30/2000 8/30/2000 8/4/2000

Environmental Management System Audit EMS-0100.011 0 NR 5/8/2000

Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

EMS-0100.012 3NR 9/1/2000 NR

Monitoring and Measuring Procedure EMS-0100.013 0 NR NRLegal and Other Requirements EMS-0101.001 1 NRLong Creek Operation ProceduresMain Lift Failure Procedure WLC-0300.001 0 NRLong Creek / Duhart / Catawba Procedure for Significant Rain Events

WLC-0100.003 3

Spill Clean Up and Reporting Procedure WLC-0100.001 0 NRIntermediate Lift Failure Procedure WLC-1700.001 0 NRLime Stabilization Process Instructions WLC-3000.001 0Land Application Tanker Loading Procedure WLC-3000.002 0Chemical Receiving Procedures WLC-4200.001 0 NRCrowders Creek Operation ProceduresCrowder Spill Procedure WCR-0100.001 0Sampling Procedure WCR-0100.002 1Process Control WCR-0100.003 0 1/0/1900

Main Lift Failure Procedure WCR-0300.001 0Hi-Ran Panel Failure WCR-0300-002 1Blower Operation Procedure WCR-1000.001 0

EMS Management Procedures

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

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Waste Gas Burner Lighting Procedure WCR-3000.001 0Holding Digester Transfer to Land Application Start Up

WCR-3100.001 0

Holding Digester Transfer to Land Application Shut Down Procedure

WCR-3100.002 0

Chemical Receiving Procedures WCR-4200.001 0Return Sludge Procedure WCR-5700.001 0Long Creek Laboratory ProceduresSample Bottle Set Up and Receiving WLC-0100.105 3Mercury Spill Clean Up Procedure WLC-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WLC-0100.109 0

Sample Receiving WLC-0100.111 1Ammonia Nitrogen Analysis WLC-0100.122 2Fecal Coliform Analysis WLC-0100.128 0Nitrates Analysis WLC-0100.134 1Total Phosphorus WLC-0100.139 1Residual Chlorine Analysis WLC-0100.140 4Lime Stabilization Sludge pH Analysis WLC-0100.142 2% Total & % Volatile Solids WLC-0100.143 2Total Suspended/Volatile Suspended Solids WLC-0100.145 1

Chemical Hygiene Plan WCR-0100.100 0Sample Bottle Set Up and Receiving WCR-0100.105 0Mercury Spill Clean Up Procedure WCR-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WCR-0100.109 0

Laboratory Waste Chemical Storage/Disaposal WCR-0100.110 0

Sample Receiving WCR-0100.111 0Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

WCR-0100.112 0

Ammonia-Nitrogen Analysis WCR-0100.122 0Ammonia Nitrogen Distillation Method WCR-0100.123 0Fecal Coliform Analysis WCR-0100.128 1 11/6/2000

Crowders Creek Laboratory Procedures

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

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Nitrates Analysis WCR-0100.134 0Total Phosphorus Analysis WCR-0100.139 0Residual Chlorine Analysis WCR-0100.140 040 Day Vector Attraction Analysis WCR-0100.141 0Solids - % Total Solids/% Total Volatile Solids Analysis

WCR-0100.143 0

Solids – Total Solids/Total Volatile Solids Analysis

WCR-0100.144 0

Total Suspended/Total Volatile Suspended Solids Analysis

WCR-0100.145 0

ADMI Color Analysis WCR-0100.150 1Fecal Coliform Analysis - Method for After Hours Spill Samples

WCR-0100.152 0

Clean Hood Operation WCR-0100.153 0

Field Procedures for Clean Mercury Grab Sampling

WPR-0100.002 0

Protocol for Performing Chronic Toxicity Screening of Industrial Discharges to the City of Gastonia Wastewater Treatment Plants

WPR-0100.003 0

WWTP Bioassays and User Toxicity Sampling and Reporting Procedures

WPR-0100.004 01/12/2001 1/9/2001 1/9/2001 1/16/2001 1/16/2001

Pretreatment

1. Shaded area indicates training is required. 2. Date is date most recent documented training on that revision was received. 3. NR Indicates training is not required since person wrote or approved the procedure. Page 118 of 127

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Awareness Training N/A N/A

Environment Management System Manual EMS-0100.000 0EMS Review Procedure EMS-0100.001 0

Document Control Procedure EMS-0100.002 0Aspects and Impacts Procedure EMS-0100.003 0Corrective/Preventative Action Report Procedure

EMS-0100.004 2

Training Procedure EMS-0100.005 1Roles and Responsibilities Listing EMS-0100.006 0Objective and Targets - Improvement Plan Summary

EMS-0100.007 1

External Communications Procedure EMS-0100.008 1Environmental Management System Audit EMS-0100.011 0Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

EMS-0100.012 3

Monitoring and Measuring Procedure EMS-0100.013 0Legal and Other Requirements EMS-0101.001 1Long Creek Operation ProceduresMain Lift Failure Procedure WLC-0300.001 0Long Creek / Duhart / Catawba Procedure for Significant Rain Events

WLC-0100.003 3

Spill Clean Up and Reporting Procedure WLC-0100.001 0Intermediate Lift Failure Procedure WLC-1700.001 0Lime Stabilization Process Instructions WLC-3000.001 0Land Application Tanker Loading Procedure WLC-3000.002 0Chemical Receiving Procedures WLC-4200.001 0Crowders Creek Operation ProceduresCrowder Spill Procedure WCR-0100.001 0Sampling Procedure WCR-0100.002 1Process Control WCR-0100.003 0Main Lift Failure Procedure WCR-0300.001 0Hi-Ran Panel Failure WCR-0300-002 1Blower Operation Procedure WCR-1000.001 0

EMS Management Procedures

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5/11/2000 5/9/2000 5/11/2000 5/11/2000 5/12/2000 5/9/2000 5/9/2000 8/21/2000 5/9/2000 11/17/1999 11/17/1999 11/17/1999 5/9/2000 5/9/2000

3/8/2000 2/14/2000

3/8/2000 2/14/2000

3/8/2000 2/14/2000

3/8/2000 2/14/2000

5/9/2000 5/9/2000 7/20/2000 7/20/2000 7/20/2000 7/22/2000 7/25/2000 7/26/2000 7/25/2000 7/25/2000 7/25/2000 7/20/2000 7/26/2000

12/18/2000 2/14/2000 2/10/2000

3/8/2000 2/14/2000 7/20/2000 7/19/2000 7/20/2000 7/19/2000 7/25/2000 8/21/2000 7/20/2000 7/25/2000 7/25/2000 7/25/2000 7/20/2000 7/26/2000

7/20/2000 7/19/2000 7/20/2000 7/19/2000 7/25/2000 8/21/2000 7/20/2000 7/25/2000 7/25/2000 7/25/2000 7/20/2000 7/26/2000

6/28/2000 6/28/2000 6/28/2000 7/7/2000 7/13/2000 12/14/2000 6/29/2000 6/28/2000 8/21/2000 12/14/2000 6/29/2000 6/28/2000 6/28/2000 6/29/2000

9/1/2000 4/13/2000

3/28/2000 2/1/2000 3/28/2000 7/21/2000 3/6/2000 2/11/2000 7/22/2000 2/2/2000 9/12/2000 7/20/2000 3/9/2000 2/1/2000 2/1/2000 3/27/2000 7/18/2000

7/25/2000 NR 7/18/2000 7/20/2000 7/19/2000 7/19/2000 7/19/2000 7/18/2000 9/12/2000 7/18/2000 7/20/2000 7/18/2000 7/18/2000 7/20/2000 7/18/2000

4/14/2000 4/13/2000 4/13/2000 7/21/2000 4/13/2000 4/13/2000 7/22/2000 4/13/2000 9/12/2000 7/20/2000 4/13/2000 4/13/2000 4/13/2000 7/18/2000

1/10/2001 1/10/2001 1/10/2001 1/10/2001 1/10/2001 1/10/2001

1/10/2001 1/10/2001 1/10/2001 1/10/2001 1/10/2001 1/10/2001

4/14/2000 4/13/2000 4/13/2000 7/21/2000 4/13/2000 4/13/2000 7/22/2000 4/13/2000 9/12/2000 7/20/2000 4/13/2000 4/13/2000 4/13/2000 7/18/2000

1. Shaded area indicates training is required. 2. Date is date most recent documented training on that revision was received. 3. NR Indicates training is not required since person wrote or approved the procedure. Page 119 of 127

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Waste Gas Burner Lighting Procedure WCR-3000.001 0Holding Digester Transfer to Land Application Start Up

WCR-3100.001 0

Holding Digester Transfer to Land Application Shut Down Procedure

WCR-3100.002 0

Chemical Receiving Procedures WCR-4200.001 0Return Sludge Procedure WCR-5700.001 0Long Creek Laboratory ProceduresSample Bottle Set Up and Receiving WLC-0100.105 3Mercury Spill Clean Up Procedure WLC-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WLC-0100.109 0

Sample Receiving WLC-0100.111 1Ammonia Nitrogen Analysis WLC-0100.122 2Fecal Coliform Analysis WLC-0100.128 0Nitrates Analysis WLC-0100.134 1Total Phosphorus WLC-0100.139 1Residual Chlorine Analysis WLC-0100.140 4Lime Stabilization Sludge pH Analysis WLC-0100.142 2% Total & % Volatile Solids WLC-0100.143 2Total Suspended/Volatile Suspended Solids WLC-0100.145 1

Chemical Hygiene Plan WCR-0100.100 0Sample Bottle Set Up and Receiving WCR-0100.105 0Mercury Spill Clean Up Procedure WCR-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WCR-0100.109 0

Laboratory Waste Chemical Storage/Disaposal WCR-0100.110 0

Sample Receiving WCR-0100.111 0Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

WCR-0100.112 0

Ammonia-Nitrogen Analysis WCR-0100.122 0Ammonia Nitrogen Distillation Method WCR-0100.123 0Fecal Coliform Analysis WCR-0100.128 1

Crowders Creek Laboratory Procedures

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11/6/2000

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Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 121 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Nitrates Analysis WCR-0100.134 0Total Phosphorus Analysis WCR-0100.139 0Residual Chlorine Analysis WCR-0100.140 040 Day Vector Attraction Analysis WCR-0100.141 0Solids - % Total Solids/% Total Volatile Solids Analysis

WCR-0100.143 0

Solids – Total Solids/Total Volatile Solids Analysis

WCR-0100.144 0

Total Suspended/Total Volatile Suspended Solids Analysis

WCR-0100.145 0

ADMI Color Analysis WCR-0100.150 1Fecal Coliform Analysis - Method for After Hours Spill Samples

WCR-0100.152 0

Clean Hood Operation WCR-0100.153 0

Field Procedures for Clean Mercury Grab Sampling

WPR-0100.002 0

Protocol for Performing Chronic Toxicity Screening of Industrial Discharges to the City of Gastonia Wastewater Treatment Plants

WPR-0100.003 0

WWTP Bioassays and User Toxicity Sampling and Reporting Procedures

WPR-0100.004 0

PretreatmentJi

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1/9/2001

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Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 122 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Awareness Training N/A N/A

Environment Management System Manual EMS-0100.000 0EMS Review Procedure EMS-0100.001 0

Document Control Procedure EMS-0100.002 0Aspects and Impacts Procedure EMS-0100.003 0Corrective/Preventative Action Report Procedure

EMS-0100.004 2

Training Procedure EMS-0100.005 1Roles and Responsibilities Listing EMS-0100.006 0Objective and Targets - Improvement Plan Summary

EMS-0100.007 1

External Communications Procedure EMS-0100.008 1Environmental Management System Audit EMS-0100.011 0Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

EMS-0100.012 3

Monitoring and Measuring Procedure EMS-0100.013 0Legal and Other Requirements EMS-0101.001 1Long Creek Operation ProceduresMain Lift Failure Procedure WLC-0300.001 0Long Creek / Duhart / Catawba Procedure for Significant Rain Events

WLC-0100.003 3

Spill Clean Up and Reporting Procedure WLC-0100.001 0Intermediate Lift Failure Procedure WLC-1700.001 0Lime Stabilization Process Instructions WLC-3000.001 0Land Application Tanker Loading Procedure WLC-3000.002 0Chemical Receiving Procedures WLC-4200.001 0Crowders Creek Operation ProceduresCrowder Spill Procedure WCR-0100.001 0Sampling Procedure WCR-0100.002 1Process Control WCR-0100.003 0Main Lift Failure Procedure WCR-0300.001 0Hi-Ran Panel Failure WCR-0300-002 1Blower Operation Procedure WCR-1000.001 0

EMS Management Procedures

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5/9/2000 11/23/1999 5/9/2000 5/9/2000 5/9/2000 5/11/2000 2/3/2000 5/11/2000 5/9/2000 5/11/2000 5/12/2000

2/14/2000

2/14/2000

2/14/2000

2/14/2000

5/9/2000 7/18/2000

2/14/2000

2/14/2000 2/3/2000 2/1/2000 2/1/2000 2/1/2000 2/1/2000 2/3/2000 2/1/2000 2/1/2000 2/1/2000 7/18/2000

7/25/2000

6/28/2000 6/29/2000

9/5/2000 9/5/2000

2/11/2000

8/15/2000 8/15/2000

7/18/2000

4/13/2000

4/13/2000

NR NR 8/20/2000 8/17/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 11/28/2000 8/15/2000 11/30/2000

NR NR 12/4/2000 12/4/2000 11/30/2000

NR NRNR NR 8/20/2000 8/17/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

NR NR 12/4/2000 12/4/2000

NR NR 8/20/2000 8/17/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Waste Gas Burner Lighting Procedure WCR-3000.001 0Holding Digester Transfer to Land Application Start Up

WCR-3100.001 0

Holding Digester Transfer to Land Application Shut Down Procedure

WCR-3100.002 0

Chemical Receiving Procedures WCR-4200.001 0Return Sludge Procedure WCR-5700.001 0Long Creek Laboratory ProceduresSample Bottle Set Up and Receiving WLC-0100.105 3Mercury Spill Clean Up Procedure WLC-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WLC-0100.109 0

Sample Receiving WLC-0100.111 1Ammonia Nitrogen Analysis WLC-0100.122 2Fecal Coliform Analysis WLC-0100.128 0Nitrates Analysis WLC-0100.134 1Total Phosphorus WLC-0100.139 1Residual Chlorine Analysis WLC-0100.140 4Lime Stabilization Sludge pH Analysis WLC-0100.142 2% Total & % Volatile Solids WLC-0100.143 2Total Suspended/Volatile Suspended Solids WLC-0100.145 1

Chemical Hygiene Plan WCR-0100.100 0Sample Bottle Set Up and Receiving WCR-0100.105 0Mercury Spill Clean Up Procedure WCR-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WCR-0100.109 0

Laboratory Waste Chemical Storage/Disaposal WCR-0100.110 0

Sample Receiving WCR-0100.111 0Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

WCR-0100.112 0

Ammonia-Nitrogen Analysis WCR-0100.122 0Ammonia Nitrogen Distillation Method WCR-0100.123 0Fecal Coliform Analysis WCR-0100.128 1

Crowders Creek Laboratory Procedures

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NR NR 8/20/2000 8/17/2000 8/16/2000 12/1/2000 12/1/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

NR NR 8/20/2000 8/17/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

NR NR 8/20/2000 8/23/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

NR NR 8/20/2000 8/23/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

NR NR 8/20/2000 8/23/2000 8/16/2000 12/1/2000 12/4/2000 8/16/2000 6/14/2000 8/15/2000 11/30/2000

11/6/2000 11/6/2000

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Nitrates Analysis WCR-0100.134 0Total Phosphorus Analysis WCR-0100.139 0Residual Chlorine Analysis WCR-0100.140 040 Day Vector Attraction Analysis WCR-0100.141 0Solids - % Total Solids/% Total Volatile Solids Analysis

WCR-0100.143 0

Solids – Total Solids/Total Volatile Solids Analysis

WCR-0100.144 0

Total Suspended/Total Volatile Suspended Solids Analysis

WCR-0100.145 0

ADMI Color Analysis WCR-0100.150 1Fecal Coliform Analysis - Method for After Hours Spill Samples

WCR-0100.152 0

Clean Hood Operation WCR-0100.153 0

Field Procedures for Clean Mercury Grab Sampling

WPR-0100.002 0

Protocol for Performing Chronic Toxicity Screening of Industrial Discharges to the City of Gastonia Wastewater Treatment Plants

WPR-0100.003 0

WWTP Bioassays and User Toxicity Sampling and Reporting Procedures

WPR-0100.004 0

PretreatmentD

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Bow

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1/10/2001

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Awareness Training N/A N/A

Environment Management System Manual EMS-0100.000 0EMS Review Procedure EMS-0100.001 0

Document Control Procedure EMS-0100.002 0Aspects and Impacts Procedure EMS-0100.003 0Corrective/Preventative Action Report Procedure

EMS-0100.004 2

Training Procedure EMS-0100.005 1Roles and Responsibilities Listing EMS-0100.006 0Objective and Targets - Improvement Plan Summary

EMS-0100.007 1

External Communications Procedure EMS-0100.008 1Environmental Management System Audit EMS-0100.011 0Sewer Overflow / Reporting Procedure (Press Release);Media List; Distribution list; Emergency Phone list

EMS-0100.012 3

Monitoring and Measuring Procedure EMS-0100.013 0Legal and Other Requirements EMS-0101.001 1Long Creek Operation ProceduresMain Lift Failure Procedure WLC-0300.001 0Long Creek / Duhart / Catawba Procedure for Significant Rain Events

WLC-0100.003 3

Spill Clean Up and Reporting Procedure WLC-0100.001 0Intermediate Lift Failure Procedure WLC-1700.001 0Lime Stabilization Process Instructions WLC-3000.001 0Land Application Tanker Loading Procedure WLC-3000.002 0Chemical Receiving Procedures WLC-4200.001 0Crowders Creek Operation ProceduresCrowder Spill Procedure WCR-0100.001 0Sampling Procedure WCR-0100.002 1Process Control WCR-0100.003 0Main Lift Failure Procedure WCR-0300.001 0Hi-Ran Panel Failure WCR-0300-002 1Blower Operation Procedure WCR-1000.001 0

EMS Management Procedures

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5/11/2000 5/9/2000 5/11/2000 5/11/2000 5/12/2000 5/9/2000 5/11/2000 5/9/2000 5/9/2000 5/9/2000 5/9/2000 11/17/1999

2/14/2000 2/14/2000 7/31/2000 7/25/2000 7/31/2000 7/21/2000 2/14/2000

2/14/2000 2/14/2000 2/14/2000

2/14/2000 2/14/2000 2/14/2000

2/14/2000 2/14/2000 2/14/2000

5/9/2000 7/31/2000 5/9/2000 5/9/2000 5/9/2000 5/9/2000 5/9/2000 6/20/2000 12/13/2000 6/21/2000 6/21/2000 8/24/2000

12/18/2000 12/18/2000 12/18/2000

2/14/2000 8/10/2000 2/22/2000 2/22/2000 2/22/2000 2/14/2000 2/22/2000 2/23/2000 2/23/2000 2/23/2000 2/14/2000

1/9/2001 1/9/2001 1/9/2001 1/9/2001 12/13/2000 12/13/2000 12/13/2000 12/13/2000 12/13/2000

6/28/2000 6/28/2000 6/29/2000 6/29/2000 6/29/2000 6/28/2000 6/29/2000 6-29-2000 5/23/2000 6/29/2000 6/29/2000 6/29/2000

9/5/2000 9/11/2000 9/11/2000 9-11-200 9-11-200 9/11/2000

3/16/2000

4/18/2000

4/18/2000

1. Shaded area indicates training is required. 2. Date is date most recent documented training on that revision was received. 3. NR Indicates training is not required since person wrote or approved the procedure. Page 125 of 127

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Training MatrixControlled Version on Computer U: Drive - All printed copies are uncontrolledPage 126 of 127

EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Waste Gas Burner Lighting Procedure WCR-3000.001 0Holding Digester Transfer to Land Application Start Up

WCR-3100.001 0

Holding Digester Transfer to Land Application Shut Down Procedure

WCR-3100.002 0

Chemical Receiving Procedures WCR-4200.001 0Return Sludge Procedure WCR-5700.001 0Long Creek Laboratory ProceduresSample Bottle Set Up and Receiving WLC-0100.105 3Mercury Spill Clean Up Procedure WLC-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WLC-0100.109 0

Sample Receiving WLC-0100.111 1Ammonia Nitrogen Analysis WLC-0100.122 2Fecal Coliform Analysis WLC-0100.128 0Nitrates Analysis WLC-0100.134 1Total Phosphorus WLC-0100.139 1Residual Chlorine Analysis WLC-0100.140 4Lime Stabilization Sludge pH Analysis WLC-0100.142 2% Total & % Volatile Solids WLC-0100.143 2Total Suspended/Volatile Suspended Solids WLC-0100.145 1

Chemical Hygiene Plan WCR-0100.100 0Sample Bottle Set Up and Receiving WCR-0100.105 0Mercury Spill Clean Up Procedure WCR-0100.108 0Inorganic Acid & Base Spill Clean Up Procedure

WCR-0100.109 0

Laboratory Waste Chemical Storage/Disaposal WCR-0100.110 0

Sample Receiving WCR-0100.111 0Switching Temperature Control Units on Environmental Rooms at Crowders Laboratory

WCR-0100.112 0

Ammonia-Nitrogen Analysis WCR-0100.122 0Ammonia Nitrogen Distillation Method WCR-0100.123 0Fecal Coliform Analysis WCR-0100.128 1

Crowders Creek Laboratory Procedures

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NR 8/24/2000 8/24/2000 8/24/2000 8/24/2000 NRNR 11/21/2000 11/21/2000 11/21/2000 11/21/2000 NR

NR 11/21/2000 11/21/2000 11/21/2000 11/21/2000 NRNR 4/6/2000 4/6/2000 4/6/2000 4/6/2000 NRNR 6/29/2000 6/29/2000 6/29/2000 6/29/2000 NRNR 5/31/2000 5/31/2000 5/31/2000 5/31/2000 NRNR 8/24/2000 8/24/2000 8/24/2000 8/24/2000 NRNR 7/31/2000 7/31/2000 7/31/2000 7/31/2000 NRNR 9/20/2000 9/27/2000 9/27/2000 9/27/2000 NRNR 1/9/2001 6/29/2000 6/29/2000 6/29/2000 6/29/2000 NRNR 1/9/2001 1/9/2001 1/9/2001 1/9/2001 NRNR 9/14/2000 9/14/2000 9/14/2000 9/14/2000 NR

NR 3/13/2000 5/3/2000 3/13/2000 3/13/2000 NRNR 7/24/2000 7/24/2000 7/27/2000 7/21/2000 NR

NR 7/24/2000 7/24/2000 7/26/2000 7/27/2000 7/21/2000 NR

NR 10/19/2000 10/20/2000 10/20/2000 10/20/2000 10/20/2000 NRNR 3/13/2000 3/13/2000 3/13/2000 NR

NR 4/4/2000 NR

NR 8/31/2000 8/31/2000 11/2/2000 8/31/2000 8/31/2000 NRNR NRNR 8/31/2000 NR

1. Shaded area indicates training is required. 2. Date is date most recent documented training on that revision was received. 3. NR Indicates training is not required since person wrote or approved the procedure. Page 126 of 127

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EMS Form # EMS-0101.002AFormat Revision 1

Date Updated: 7/26/00Date Printed: 1/31/2001

Document Title Document # Rev

Nitrates Analysis WCR-0100.134 0Total Phosphorus Analysis WCR-0100.139 0Residual Chlorine Analysis WCR-0100.140 040 Day Vector Attraction Analysis WCR-0100.141 0Solids - % Total Solids/% Total Volatile Solids Analysis

WCR-0100.143 0

Solids – Total Solids/Total Volatile Solids Analysis

WCR-0100.144 0

Total Suspended/Total Volatile Suspended Solids Analysis

WCR-0100.145 0

ADMI Color Analysis WCR-0100.150 1Fecal Coliform Analysis - Method for After Hours Spill Samples

WCR-0100.152 0

Clean Hood Operation WCR-0100.153 0

Field Procedures for Clean Mercury Grab Sampling

WPR-0100.002 0

Protocol for Performing Chronic Toxicity Screening of Industrial Discharges to the City of Gastonia Wastewater Treatment Plants

WPR-0100.003 0

WWTP Bioassays and User Toxicity Sampling and Reporting Procedures

WPR-0100.004 0

PretreatmentAr

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NR NRNR 8/11/2000 NRNR 5/2/2000 5/24/2000 NR

NR NR

NR NR

NR 5/3/2000 NRNR 8/16/2000 9/28/2000 NR

NR NR1/2/2001

NR 3/13/2000 5/3/2000 3/13/2000 3/13/2000 NR

1. Shaded area indicates training is required. 2. Date is date most recent documented training on that revision was received. 3. NR Indicates training is not required since person wrote or approved the procedure. Page 127 of 127