sme report of limited phase ii environmental site … · limited phase ii environmental site...

above ground storage tank

air quality

asbestos/lead-based paint

baseline environmental assessment

brownfield redevelopment

building/infrastructure restoration

caisson/piles

coatings

concrete

construction materials services

corrosion

dewatering

drilling

due care analysis

earth retention system

environmental compliance

environmental site assessment

facility asset management

failure analyses

forensic engineering

foundation engineering

geodynamic/vibration

geophysical survey

geosynthetic

greyfield redevelopment

ground modification

hydrogeologic evaluation

industrial hygiene

indoor air quality/mold

instrumentation

masonry/stone

metals

nondestructive testing

pavement evaluation/design

property condition assessment

regulatory compliance

remediation

risk assessment

roof system management

sealants/waterproofing

settlement analysis

slope stability

storm water management

structural steel/welding

underground storage tank

REPORT OF LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT

FORMER H.K. PORTER FACILITY 1849 EAST SABINE STREET HUNTINGTON, INDIANA

SME Project Number: 068260.00.002 October 9, 2013

Prepared for: Mr. Anthony Goodnight, PE Director of Public Works City of Huntington 300 Cherry St. Huntington, Indiana 46750

©2013 SME Soil and Materials Engineers, Inc.

Soil and Materials Engineers, Inc. 5847 W. 74th St.

Indianapolis, IN 46278-1757

tel (317) 876-0200 fax (317) 876-0300

www.sme-usa.com

Kenneth W. Kramer, PE

Founder

Mark K. Kramer, PE

Timothy H. Bedenis, PE

Gerald M. Belian, PE

Andrew J. Emmert, CPA

Chuck A. Gemayel, PE

James M. Harless, PhD, CHMM

Larry P. Jedele, PE

Cheryl A. Kehres-Dietrich, CGWP

Gerard P. Madej, PE

Timothy J. Mitchell, PE

Robert C. Rabeler, PE

Daniel 0 . Roeser, PG

Christopher R. Byrum, PhD, PE

Daniel R. Cassidy, CPG

John E. Dingeldein, PE

Sheryl K. Fountain, SPHR

Davie J. Hurlburt, PE

Anthony L. Jarem, PE

Laurel M. Johnson, PE

Jeffery M. Krusinga, PE, GE

Jeffrey R. Lanier, PE

Michael S. Meddock, PE

Louis J. Northouse, PE

Rohan W. Perera, PhD, PE

Joel W. Rinkel, PE

Jason A. Schwartzenberger, PE

Larry W. Shook, PE

Thomas H. Skotzke

Michael J. Thelen, PE

Anthony B. Thomas, PE

Keith D. Toro, PE

John C. Zarzecki, GET, CDT, NOE

OFFICES

Indiana Michigan

Ohio

October 9, 2013

Mr. Anthony Goodnight, PE Director of Public Works City of Huntington 300 Cherry St. Huntington, Indiana 46750

RE: Limited Phase II Environmental Site Assessment Report Former H.K. Porter Facility 1849 East Sabine Street Huntington, Indiana SME Project Number: 068260.00.002

Dear Mr. Goodnight

Soil and Materials Engineers, Inc. (SME) has completed a Limited Phase II Environmental Site Assessment (ESA) of the above referenced property, hereinafter referred to as the Property. The enclosed Limited Phase II ESA report presents SME's interpretation of site conditions at the time the Limited Phase II ESA was completed based on field observations and laboratory supplied data.

The Limited Phase II ESA was requested to assess recorded and readily observable recognized environmental conditions associated with the Property. SME understands The City of Huntington will rely upon the professional opinions and representations contained in the report in accordance with the terms and conditions agreed upon for the project. This reliance is not to be construed as a warranty or guarantee on the part of SME.

Thank you for the opportunity to provide these services. If you have any questions concerning this report, or if additional services are required, please call.

Very truly yours,

SOIL AND MATERIALS ENGINEERS, IN

-U1J£L ~ (yC~ ~e~::u 1chael S. Meddock,P.E. Staff Geologist Vice President

Distribution: 2 Hard Copies, 2 CDs

©2013 SME consultants in the geosciences, materials, and the environment

Phase II Environmental Site Assessment 1849 East Sabine Street, Huntington, Indiana

SME Project Number 068260.00.002 October 9, 2013

TABLE OF CONTENTS

1.0 INTRODUCTION ...................................................................................................... 1

1.1 Site Description and Background ............................................................................. 1 1.2 Pu1~ose ................................ ,. ....................................................................................... 2

2.0 SCOPE OF ASSESSMENT ....................................................................................... 3

3.0 PROCEDURES ........................................................................................................... 5

3 .1 Soi l Boring Soil Sampling ............ .. ...... .... .. .... ... .. .. ..... .. ... ... .. ... ... ..... ...... ........... .... .... 5 3.2 Soil Boring Groundwater Sampling .... .... ..................................................... ..... .... ... 6 3.3 Soil Boring Sampl ing Quality Assurance and Quality Control (QA/QC) ... ....... .. .. .. 6 3.4 Chemical Analyses ................. ...... ............................. ................. .. ...... ......... .... ........ . 7

4.0 RESULTS .................................................................................................................... 8

4.1 Surface and Subsurface Conditions ..................................................................... ..... 8 4.2 Results of Chemical Analyses ........ ..... .. .............. .... ......... ... ..... .. .. ......... ....... .. ... ..... .. 8

4.2.1 Soil Sample Analyses ...... ..... .... .... ... ........ ... .... .... .. .. .. ...... .. .. .. .. .. .. ... ....... .... ... .. 8 4.2.2 Groundwater Sample Analyses ....... ..... .. ........... ..... .......... ................... ....... .... 9 4.2.3 Surficial Asbestos Soil Sample Analyses .... .. .. .. .. ....... .. .. ....... ...... ... .. ..... .. ... ... 9

4.3 Data Verification/Validation and Usability .. ............... .. ... .. .. ... ... ......... ....... ..... ... ...... 9

Figure 1 - USGS 7.5 Minute Topographic Map Figure 2 - Sample Location Diagram

TABLES: Table 1 - Soil Analytical Results Table 2 - Groundwater Analytical Results Table 3 - Surficial Soil Asbestos Analytical Results

APPENDIX A: Soil Boring Logs

APPENDIXB: Laboratory Data Reports

©2013 SME

Limited Phase II Environmental Site Assessment 1849 East Sabine Street, Huntington, Indiana

1.0 INTRODUCTION

SME Project Number 068260.00.002 October 9, 2013 - Page l

Soil and Materials Engineers, Inc. (SME) prepared this report to present the results of a

Limited Phase II Environmental Site Assessment (ESA) at the former H.K. Porter site located at

1849 East Sabine Street, Huntington, Huntington County, Indiana (the Property). The Property

location is shown on Figure 1. This Limited Phase II Environmental Assessment was conducted

in accordance with our approved August 21, 2013 task order (P01837.13-Task Order 02).

1.1 Site Description and Background

The Property currently consists of a vacant; approximately 108,000 square foot

manufacturing building and a 6,200 square foot, two-story office building that are present on

approximately 11.7 acres of land. Manufacturing was conducted on the site from at least 1919.

The operations conducted on the site from approximately 1924 until circa 2000 have been related

to the manufacturing of asbestos containing automotive parts (brake pads, clutch facings, etc.).

According to the 2007 Indiana Department of Environmental Management (IDEM) Pre

CERCLIS Screening Report, asbestos was originally stored in a warehouse located about three

blocks from the main plant but was later stored onsite. The asbestos was transported from the

storage locations to the mixing area whereupon it was used in the manufacturing process.

Approximately 220 pounds of asbestos and 400 pounds of lead were used per day during peak

production. IDEM also conducted a Preliminary Assessment (PA) of the site and surrounding

area in 2007. This assessment included screening 33 surface soil locations with an x-ray

fluorescence (XRF) instrument to assess the levels of metals in soil. Elevated concentrations of

lead were identified at several on and off site locations in excess of current IDEM standards.

In 2002, Tetra Tech sampled 55-gallon drums, five-gallon buckets, trenches, benzene

mixing tanks, and floor sweepings during their inspection of the site. Analytical results for the

samples collected indicated the presence of benzene, toluene, ethylbenzene, xylene (BTEX) and

asbestos. The Tetra Tech report concluded that the site met the criteria for a removal action

under 40 CFR 300.415(b)(2).

©2013 SME

Limited Phase II Environmental Site Assessment I 849 East Sabine Street, Huntington, Indiana

1.2 Purpose

SME Project Number 068260.00.002 October 9, 2013 - Page 2

SME designed the scope of this assessment in response to City of Huntington's request to

assess the types and magnitude of potential impact to the Property. Please note that the extent of

impacts was not defined as part of this assessment. SME prepared this report to document the

encountered subsurface conditions, soil and groundwater sampling procedures, and the results of

soil and groundwater chemical analysis.

©2013 SME

Limited Phase II Environmental Site Assessment 1849 East Sabine Street, Huntington, lndiana

SME Project Number 068260.00.002 October 9, 20 I 3 - Page 3

2.0 SCOPE OF ASSESSMENT

The assessment was designed to preliminarily investigate the primary exposure pathway,

direct contact with soil; the secondary pathway, direct contact with groundwater; and the third,

vapor intrusion. The pathways were investigated to evaluate if soil and groundwater contains

chemicals-of-concern at concentrations exceeding (IDEM) Residential Screening Levels.

SME advanced soil borings or collected surficial soil samples (SBl through SB3, AST,

and AS-1 through AS-5) to assess potential environmental impact from historic operations. Soil

boring samples SB 1 and SB2 were advanced to identify potential releases from the benzene

mixing area, solvent recovery area, and solvent UST. Soil boring SB3 was advanced to address

potential releases from the former benzene tank along the east side of the building. Surficial

grab samples AS-1 through AS-5 were collected to determine if asbestos from operations had

impacted soil on site. Surface sample AST was collected to assess the area around the above

ground storage tank that had formerly contained diesel fuel.

The borings were advanced to a maximum depth of thirteen feet below ground surface

(bgs ), and soil samples were collected for visual classification, field screening for evidence of

contamination, and/or chemical analyses. Specifically, one soil sample was collected from each

boring location at the interval displaying the highest indicator of impact. Surficial samples were

collected by hand auger and were advanced to a maximum depth of one foot bgs.

Temporary pre-packed groundwater wells were installed at SB2 and SB3 (Figure 2).

Equipment refusal was reached at approximately 6.5 feet bgs in SBl and SB2, as well as at 13

feet bgs in SB3 due to encountering bedrock. Groundwater was not encountered at SB 1. One

groundwater sample was collected from both SB2 and SB3. A summary of the soil and

groundwater samples collected and analyzed for this assessment is presented in Table 1.

Based on previous usage of the Property, the soil and groundwater samples were

submitted for laboratory analyses of one or more of the following parameters: volatile organic

compounds (VOCs), semi-volatile organic compounds (SVOCs), asbestos, and/or lead. Except

as described below, the soil and groundwater samples were collected and analyzed as described

in the task order.

© 2013 SME

• Due to equipment refusal before encountering groundwater at SB 1, a well could not be completed.

• A surficial soil sample was obtained in the vicinity of the heating oil tank instead of by advancing a soil boring.



©2013 SME

• An additional sample was obtained from a boring placed 4 feet north of SB2 and was identified as SB2A. The sample was collected as the initial boring was to be placed in this location, however, equipment refusal was met and the boring was relocated.


3.0 PROCEDURES


Procedures for the soil boring sampling activities, temporary groundwater monitoring

well installation and sampling, decontamination, and chemical analyses are summarized in the

following subsections. SME completed the soil borings and collected soil and groundwater

samples at the Property on September 16, 2013.

3.1 Soil Boring Soil Sampling

Soil borings SB 1 through SB3 were advanced using a hydraulic, direct-push Geoprobe

machine equipped with clean, disposable 4 foot vinyl acetate liners. Hand auger samples AST

and AS 1 through ASS were advanced by hand auguring to the specified depth. The hand auger

was decontaminated using laboratory grade disinfectant after each sample was collected. The

soil in each 4 foot interval was visually evaluated, and representative samples were collected

from each soil unit for visual classification. SME visually classified the soil samples from the

soil borings in general accordance with the Unified Soil Classification System (USCS).

A portion of each soil sample was used for field screening of ionizable VOCs using a

calibrated photoionization detector (PID) equipped with a 10.6 eV lamp. Field screening

consisted of placing a portion of the sample in a sealed plastic bag and allowing the sample to

warm and release ionizable VOCs. The tip of the PID was inserted in the headspace of the bag,

and PID readings were recorded on SME's field activity report.

The amount of soil collected at each sampling location was dependent on chemical

analyses requirements. First, soil samples intended for VOC laboratory analyses were removed

from the boring liner and were placed in methanol-preserved and deionized water-preserved 40-

milliliter (mL) glass vials following U.S. Environmental Protection Agency (U.S. EPA) Method

5035A. Soil volumes sufficient for analyses of additional parameters were then removed from

the boring liner and homogenized prior to transfer to pre-cleaned, four or eight-ounce, glass jars

provided by the analytical laboratory.

SME returned residual soil cuttings generated from the soil borings to the corresponding

boreholes after sampling activities were completed. The surface disturbance at each boring

location was repaired with hydrated bentonite chips.

©2013 SME


3.2 Soil Boring Groundwater Sampling


Groundwater was encountered during drilling at monitoring wells SB2 and SB3 at depths

of approximately 3.5 feet and 10 feet bgs, respectively. Groundwater was not present in the soil

boring SBl which terminated at a depth of 6.5 feet bgs. SME installed a temporary

groundwater monitoring well at SB2 and SB3. Each of the temporary groundwater monitoring

wells were constructed of 5-foot long, 1-inch diameter, and 0.010-inch slotted PVC screen with a

pre-packed sand screen attached to 1-inch diameter PVC riser. Each well was installed such that

the screen intersected the water table.

Prior to sampling, SME purged the wells using a disposable bailer. After well purging,

SME collected groundwater samples from the temporary groundwater monitoring wells using the

disposable polyethylene bailer. The groundwater samples intended for laboratory analyses were

transferred directly into one or more of the following laboratory-supplied containers: 40-mL

glass vials preserved with hydrochloric acid (VOC analyses); 500-mL plastic bottles preserved

with nitric acid (metals analyses).

After purging and groundwater sampling, SME removed the temporary wells, filled the

boring to the ground surface with bentonite chips, and used the development water to hydrate the

bentonite chips. The surface disturbance at the boring locations was repaired with native soils.

3.3 Soil Boring Sampling Quality Assurance and Quality Control (QA/QC)

In order to minimize cross-contamination, a new pair of disposable nitrile sampling

gloves was used for collection of each sample. Soil sampling equipment was decontaminated

before each use with a laboratory grade detergent and rinsed with distilled water. Clean, un-used

polyethylene tubing and well materials were used for groundwater purging and sampling.

SME collected field duplicate samples (soil and groundwater) to evaluate the precision

of sampling activities. SME collected a trip blank and groundwater equipment blank to

evaluate the potential impacts of cross-contamination associated with sample collection,

storage, and transport. A soil equipment blank was not collected as samples were collected

within single use acetate liners.

Field instrument calibration, sample handling and custody requirements, and laboratory

analytical methods, analysis reporting limits (RLs), QA/QC procedures, and reporting protocols

were consistent with those of SME's standard practice.

©2013 SME


3.4 Chemical Analyses


SME submitted 10 soil, 2 groundwater, and 4 QA/QC samples for chemical analysis of

one or more of the following parameters: VOCs, SVOCs, lead and/or asbestos. IA TL in Mt.

Laurel, New Jersey analyzed the soil samples for asbestos using the EPA Reg 1. 1994, Asbestos

In Soil, Sludges, and Sediment analytical method. Pace Analytical in Indianapolis, Indiana

analyzed the soil and groundwater samples for voes and lead using the referenced methods:

• VOCs - United States Environmental Protection Agency (USEP A) Method SW-846-5053A/8260,

• SVOCs - United States Environmental Protection Agency (USEPA) Method SW-846-8270, and

• Metals - USEP A Methods S W846-6020, 7196, and 7 4 70

©2013 SME


4.0 RESULTS

SME Project Number 068260.00.002 October 9, 20 I 3 - Page 8

The surface and subsurface conditions encountered during soil boring activities and the

results of chemical analyses are described in the following subsections.

4.1 Surface and Subsurface Conditions

Soil samples were visually classified in general accordance with the USCS. Detailed

information regarding the soil conditions encountered at each soil boring is documented in Soil

Boring Logs in Appendix A1• The boring locations are shown on Figure 2. The soil profile

across the site was highly varied. Solvent odors were noted in soil boring SB2 at depths of 4 to

6.5 feet bgs and were accompanied by high PID readings of up to 3,258 ppm. Soil boring SB2 is

at the location of the solvent UST that is present.

4.2 Results of Chemical Analyses

Results of chemical analyses performed on soil and groundwater samples collected by

SME are summarized in the following paragraphs and tabulated in Tables 1 through 3. Results

of chemical analyses were compared to the Indiana Department of Environmental Management

(IDEM) Remediation Closure Guide (RCG) Residential Screening Levels. Laboratory analysis

reports are included in Appendix B.

4.2.1 Soil Sample Analyses

Eight VOCs and lead were measured in multiple soil samples at concentrations above

laboratory reporting limits. Of these, one soil sample exceeded the Direct Contact - Residential

IDEM RCG Screening Levels for lead. None of the volatile organics exceeded the direct contact

screening level which also accounts for inhalation of particulates and vapors.

Soil samples from SB2 and SB2-A exceeded the Soil Migration to Groundwater -

Residential Indiana Department of Environmental Management (IDEM) Remediation Closure

Guide (RCG) Screening Levels for 1,2,4-trimethylbenzene and/or lead. Both of the above listed

chemicals were noted in the groundwater sample at SB2 at concentrations above the Drinking

Water Protection Criteria- Residential Tap IDEM RCG Screening Levels.

1 Soil boring logs are not provided for samples collected with a hand auger.

© 2013 SME


4.2.2 Groundwater Sample Analyses


During analysis, 10 VOCs and lead were detected in one or more groundwater samples

above laboratory reporting limits. The chemical constituents 1,2,4-trimethylbenzene, benzene,

naphthalene, and lead in SB2 were detected at concentrations greater than the Residential Tap

IDEM RCG Screening Levels. Benzene in the groundwater sample from SB2 also exceeded

both the IDEM RCG Groundwater Volatilization to Indoor Air Inhalation - Residential and

Commercial/Industrial Screening levels. Lead was also detected in SB3 at a concentration

exceeding the IDEM RCG Residential Tap Screening Level. No other target analytes were

detected at concentrations above laboratory reporting limits in the groundwater samples.

4.2.3 Surficial Asbestos Sample Analyses

SME collected five surficial soil samples for analysis of asbestos. Soil sample AS-3

contained asbestos at 2.6% by volume. The remaining samples analyzed did not contain asbestos

at detectable concentrations. There are currently no state or federal standards for a safe

concentration of asbestos in soil. The results are summarized in Table 3.

4.3 Data VerificationNalidation and Usabilitt

SME evaluated the representativeness of the data collected during this Phase II ESA to

determine if the data set was valid and of usable quality. The laboratory QA/QC results are

detailed in the Case Narrative included in Appendix C. The data set generated is of usable

quality and meets the Property-specific objectives.

© 2013 SME



In the process of obtaining information in preparation of this report, procedures were

followed that represent reasonable practices and principles in a manner consistent with that level

of care and skill ordinarily exercised by members of this profession currently practicing under

similar conditions.

Report prepared by: Steve Reutter, Staff Geologist

Report reviewed by: Mike Meddock, PE, Vice President.

©20 13 SME

FIGURES

FIGURE 1 - USGS 7.5 MINUTE TOPOGRAPHIC MAP

FIGURE 2 - PROPERTY FEATURES AND SAMPLE LOCATIONS

© 2013 SME

LEGEND

APPROXIMATE PROPERTY LOCATION

O' 2000'

SCALE: 1" = 2000'

Oct 04, 2013 - 2:37pm - jblake

www.sme-usa.com

Indiana Michigan

Ohio

Base map obtained from ©Delorme Topo North America TM 10.

USGS QUADRANGLE(s) REFERENCED

ANDREWS (IN) TOPO QUAD, 1994 BIPPUS (IN) TOPO QUAD, 1992

HUNTINGTON (IN) TOPO QUAD, 1994 MAJENICA (IN) TOPO QUAD, 1992

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©2013 SME

TABLES

TABLE 1 - SOIL ANALYTICAL RESULTS

TABLE 2-GROUNDWATER ANALYTICAL RESULTS

TABLE 3 - SURFICIAL SOIL ASBESTOS ANALYTICAL RESULTS

TABLE 1SOIL ANALYTICAL RESULTS

FORMER HK PORTER 1849 SABINE STREET, HUNTINGTON, INDIANA

Table 1Page 1 of 1

AST SB1 SB2 A SB2 DUP01 Soil SB2 5.5-6.5' SB3 Trip Blank

Soil

Sample Depth (ft. below grade) Surface 0-2 5.5-6.5 5.5-6.5 5.5-6.5 8.0-8.5 -

Date Collected 9/16/2013 9/16/2013 9/16/2013 9/16/2013 9/16/2013 9/16/2013 -

1,2,4-Trimethylbenzene 95-63-6 87 220 220 0.44 NA <0.0067 5.6 0.57 0.35 <0.10 <0.00501,3,5-Trimethylbenzene 108-67-8 180 180 180 2.5 NA <0.0067 0.53 0.27 0.2 <0.10 <0.0050Ethylbenzene 100-41-4 76 270 480 16 NA <0.0067 1.6 0.23 0.18 <0.10 <0.0050Xylenes, Total 1330-20-7 260 260 260 200 NA <0.013 1.7 0.82 0.71 <0.21 <0.010Isopropylbenzene 98-82-8 270 270 270 13 NA <0.0067 1 <0.14 <0.13 <0.10 <0.0050n-Butylbenzene 104-51-8 110 110 110 50 NA <0.0067 0.62 <0.14 <0.13 <0.10 <0.0050n-Propylbenzene 103-65-1 260 260 260 20 NA <0.0067 2.3 <0.14 <0.13 <0.10 <0.0050sec-Butylbenzene 135-98-8 NE NE NE NE NA <0.0067 <0.48 <0.14 <0.13 0.12 <0.0050Other VOCs CS CS CS CS CS <RL <RL <RL <RL <RL <RL <RL

Phenol 108-95-2 25,000 100,000 100,000 52 3.7 NA NA NA NA NA NAOther SVOCs CS CS CS CS CS <RL NA NA NA NA NA NA

Lead 7439-92-1 400 800 1,000 270 NA <1.8 541 NA 13.3 9.5 NANotes:1. Only analytes measured at concentrations above their respective Method Reporting Limit in at least on sample are listed.2. Screening Levels taken from IDEM Remediation Closure Guide Table A-6 of Appendix A, dated March 22, 2012 - Updated March 1, 2013. 3. Detected results shown in BOLD. Results exceeding one or more criteria are shaded.4. VOCs - Volatile Organic Compounds. Refer to the analytical report for the full list of VOC analytes.5. CS - Criterion is specific to individual constituent.6. <RL - concentrations of all non-listed constituents were below their respective Reporting Limits.7. NE - No Established Criteria.8. SVOCs -Semi-Volatile Organic Compounds. Refer to the analytical report for the full list of SVOC analytes.11. NA - Not Analyzed (not in assessment scope of work).

VOCs

PAHs/SVOCs

Metals

Analyte (see laboratory report for

analysis methods)CAS Number

IDEM REMEDIATION CLOSURE GUIDE SCREENING LEVELS (mg/kg)

Sample Identification

CHEMICAL ANALYSES RESULTS (mg/kg)

Direct Contact Residential2

Direct Contact Commercial /

Industrial2

Direct Contact

Excavation2

Soil Migration to

Groundwater Residential2

TABLE 2GROUNDWATER ANALYTICAL RESULTS


Table 2Page 1 of 1

Sample Identification SB2 GW SB3 GW DUP01 GW

(SB3 GW)TRIP

BLANKDrinking

Water Protection Criteria-

Residential Tap²

Groundwater Volatilization to

Indoor Air Inhalation - Residential²

Groundwater Volatilization to Indoor Air Inhalation - Industrial²

Date Collected 9/16/2013 9/16/2013 9/16/2013 9/16/2013

VOCs 1,2,4-Trimethylbenzene 95-63-6 0.015 NE NE 0.207 <0.0050 <0.0050 <0.00501,3,5-Trimethylbenzene 108-67-8 0.087 NE NE 0.0566 <0.0050 <0.0050 <0.00502-Butanone (MEK) 78-93-3 4.9 NE NE 0.0731 <0.0250 <0.0250 <0.0250Benzene 71-43-2 0.005 0.024 0.120 0.327 <0.0050 <0.0050 <0.0050Ethylbenzene 100-41-4 0.7 NE NE 0.466 <0.0050 <0.0050 <0.0050Isopropylbenzene (Cumene) 98-82-8 0.39 NE NE 0.0366 <0.0050 <0.0050 <0.0050Naphthalene 91-20-3 0.0014 0.091 0.460 0.0055 <0.0014 <0.0014 <0.0014n-Hexane 110-54-3 0.25 NE NE 0.011 <0.0050 <0.0050 <0.0050n-Propylbenzene 103-65-1 0.53 NE NE 0.0503 <0.0050 <0.0050 <0.0050Xylene (Total) 1330-20-7 10 NE NE 0.978 <0.010 <0.010 <0.010Other VOCs CS CS CS CS <RL <RL <RL <RLMetals Lead 7439-92-1 0.015 NE NE 3.61 0.122 0.115 NANotes:1. Only analytes measured at concentrations above their respective Method Reporting Limit in at least on sample are listed.2. Screening Levels taken from IDEM Remediation Closure Guide Table A-6 of Appendix A, dated March 22, 2012 - Updated March 1, 2013. 3. Detected results shown in BOLD. Results exceeding one or more criteria are shaded.4. VOCs - Volatile Organic Compounds. Refer to the analytical report for the full list of VOC analytes.5. CS - Criterion is specific to individual constituent.6. <RL - concentrations of all non-listed constituents were below their respective Reporting Limits.7. NE- Not Established.8. NA-Not Analyzed


analysis methods)CAS Number

IDEM REMEDIATION CLOSURE GUIDE SCREENING LEVELS (mg/L)

TABLE 3SURFICIAL SOIL ASBESTOS ANALYTICAL RESULTS


Table 3Page 1 of 1

Sample Identification AS-1 AS-2 AS-3 AS-4 AS-5

Date Collected 9/16/2013 9/16/2013 9/16/2013 9/16/2013

Location East of office building

North of office

building

South of office

building

Near bag house area

Near bag house area

AsbestosAsbestos ND ND 2.6% ND NDNotes:1. There is currently no IDEM regulatory standard for asbestos in soil2. Samples AS-1 through AS-3 were down wind from from the former baghouse.3. ND-Not detected above laboratory reporting limits


analysis methods)

APPENDIX A

SOIL BORING LOGS

©2013 SME

1.0

6.5

Organic- Dark Brown

Silt- Trace Sand- Trace Gravel- Light Brown(ML)

END OF BORING AT 6.5 FEET.

28

30

<1

<1

<1

<1

LS1

LS2

Driller hit refusal (bedrock) at 6.5 feet.

DATE STARTED: 9/16/13 COMPLETED: 9/16/13

LOGGED BY: LEW CHECKED BY: CGS

BORING METHOD: Direct Push

RIG NO.: GeoprobeOPERATOR: SCS

GROUNDWATER & BACKFILL INFORMATION

GROUNDWATER WAS NOT ENCOUNTERED

NOTES: 1. The indicated stratification lines are approximate. In situ, the transition between materials may be gradual.2. No odors were noted, and no staining was observed.

BACKFILL METHOD: Auger Cuttings & BentoniteChips

BORING SB 1

PROJECT LOCATION: City of Huntington, Indiana

PROJECT NAME: HK Porter PROJECT NUMBER: 068260.00.002

CLIENT: City of Huntington, Indiana

PAGE 1 OF 1

SY

MB

OLI

CP

RO

FIL

E

SURFACE ELEVATION: Not SurveyedPROFILE DESCRIPTION SO

ILAN

ALYT

ICAL

SAM

PLE

TEM

POR

ARY

WEL

L SC

REE

N

REC

OVE

RY

(inch

es)

PID

(ppm

)

SAM

PLE

TYPE

/NO

.IN

TER

VAL

REMARKS

soil and materials engineers, inc.michigan, ohio and indiana

DE

PT

H (

FE

ET

)

0.0

2.5

5.0

7.5

10.0

12.5

0.2

4.0

4.5

6.5

Coarse Gravel (Fill)

Fine to Coarse Sand- Brown- Moist- BrickPieces (Fill)

Fine to Coarse Sand- Gray- Moist to Wet(Fill)

Silt- Trace Sand- Trace Gravel- Light Brown(ML)


24

30

8.6

8.9

2577

3258

LS1

LS2

A groundwater sample was collected from atemporary monitoring well; the well screen wasset between 1 feet and 6 feet below groundsurface.

Solvent odors were noted from 4 feet to 6.5 feet.Gray staining was observed from 4 feet to 6 feet.

Driller hit refusal (bedrock) at 6.5 feet.





GROUNDWATER & BACKFILL INFORMATION NOTES: 1. The indicated stratification lines are approximate. In situ, the transition between materials may be gradual.2. Dup01 soil sample taken from SB2. SB2-A was taken 4 feet north of SB2 from 5.5 feet to 6.5 feet below

ground surface and had a PID reading of 3456. SB2-A was submitted for VOCs analyses only.DEPTH (FT)


DURING BORING: 3.5

BORING SB 2




PAGE 1 OF 1

SY

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ILAN

ALYT

ICAL

SAM

PLE

TEM

POR

ARY

WEL

L SC

REE

N

REC

OVE

RY

(inch

es)

PID

(ppm

)

SAM

PLE

TYPE

/NO

.IN

TER

VAL

REMARKS


DE

PT

H (

FE

ET

)

0.0

2.5

5.0

7.5

10.0

12.5

0.3

0.6

10.0

13.0

Asphalt ConcreteFine to Medium Sand- Trace Silt- TraceGravel- Light Brown- Moist (Fill)

Silt- Trace Sand- Trace Gravel- Brown toGray- Moist (ML)

Fine to Coarse Sand- Trace Gravel- TraceSilt- Gray- Wet (SP)


28 1.8

1.8

1.9

1.5

28.9

N/A

N/A

LS1

LS2

LS3

LS4

A groundwater sample was collected from atemporary monitoring well; the well screen wasset between 8 feet and 13 feet below groundsurface.Solvent odors were noted from 4 feet to 12 feet.

Driller hit refusal (bedrock) at 13 feet.





GROUNDWATER & BACKFILL INFORMATION NOTES: 1. The indicated stratification lines are approximate. In situ, the transition between materials may be gradual.2. Dup soil sample taken from SB3 was taken 4 feet south of SB3.3. No staining was observed.

DEPTH (FT)


DURING BORING: 10.0

BORING SB 3




PAGE 1 OF 1

SY

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SAM

PLE

TEM

POR

ARY

WEL

L SC

REE

N

REC

OVE

RY

(inch

es)

PID

(ppm

)

SAM

PLE

TYPE

/NO

.IN

TER

VAL

REMARKS


DE

PT

H (

FE

ET

)

0.0

2.5

5.0

7.5

10.0

12.5

APPENDIXB

LABO RA TORY DATA REPORTS

©2013 SME

/\.S<.lFS'l'OS TFSTlNC 1..ABOgATOHTES

September 26, 2013

Soil & Materials Engineers Inc 5847 West 74th Street Indianapolis, IN 46278

Addendum to iATL Report Number 315245

9000 Commerce Parkway, Mount Laurel, NJ 08054

Telephone: 856-231-9449 Fax: 856-231-9818

www.iatl.com

Samples analyzed using EPA Region I Protocol for Screening Soil and Sediment Samples for Asbestos Content, 1994

Additional Sample Descriptions as provided by the Analyst:

AS 1 I 512482 7 - Soil Description: - Silt, Sand, Humus, Natural Cellulose Building Material: None Detected

AS2 I 5124828 ····Soil Description: - Silt, Sand, Humus, Natural Cellulose Building Material: None Detected

AS3 I 5124829 - Soil Description: - Silt, Sand, Ifomus, Natural Cellulose Building Material: Chrysotile Clumps

AS4 / 5124830 - Soil Description: - Silt, Sand, Pebbles, Natural Cellulose Building Material: Cinder

AS5 I 5124831 - Soil Description: - Silt, Sandy Natural Cellulose Building Material: Glass Slugs

DUP02Soil I 5124832 - Soil Description: - Silt, Sand Natural Cellulose Building Material: None Detected

Quality Analysis since 1986 Page 1 of 1

9000 Commerce Parkway, Suite B •Mount Laurel, NJ 08054

Phone: 877-428-4285/856-231-9449 e Fax: 856-231-9818

Chain of Custody -Bulk Asbestos -

Contact Information Client Company: SME -------------- Project Number: _0_68_2_6_0_.0_0_.0_0_2 _____ _

0 ffi c e Address: 584 7 W. 7 4th Street Project Name: _H_K_P_o_rt_e_r _______ _

City, State, Zip: Indianapolis, Indiana 46278 Primary Contact: _L_a_u_ra_W_e_ls_h ______ _

Fax Number: 317-876-0300 Office Phone: 317-876-0200 -------------- ------------Em a ii Address: [email protected] Ce 11 Phone: 317-879-6172 ------------

PLM Instructions: D PLM: Bulk Asbestos Building Materials EPA 600 R-93/116, 1993

PLM: Bulk Asbestos Building Materials EPA 600 M-4/82-020, 1982 PLM: Bulk Asbestos Building Materials NIOSH 9002, 1985 PLM: Bulk Asbestos Building Materials NYSDOH-ELAP 198.1, 2002 PLM: Bulk Asbestos Building Materials NYSDOH-ELAP 198.6, 2010 TEM: Bulk Asbestos Building Materials NYSDOH-ELAP 198.4, 2009

PLM: Point Counting PC:viaELAP 198.1 PC: 400 Points PC: 800 Points * PC: 1600 Points*

PLM: Instructions for Multi-Layered Samples D Analyze and Report All Separable Layers per EPA 600

PLM: Analyze Until Positive (Positive Stop) AUP: by Homogenous Area as Noted AUP: by Material Type as Noted

PLM: NOB via 198.6 0 PLM: Friable via EPA 600 2.3

If <l % by PLM, to TEM via 198.4 * If <l % by PLM, Hold for Instructions

lii1 * ** Report Composite for Drywall Systems per NESHAP I!!!! PLM: Non-Building Material ' (Dust, Wipe, Tape)

Report All Layers and Composite Where Applicable Iii Soil or Vermiculite Analysis' Only Analyze and Report Specifically Noted Layer CARB 435

Special Instructions: Asbestos analysis using US EPA Region I, 1994: Please e-mail results to [email protected].

*Additional charge and turnaround may be requ~;ed **Alternative Method (ex: EPA 600/R-041004) may be recommended by Laboratory

Turnaround Time Preliminary Results Requested Date: _________ _ Dverbal Email Fax

Specific date I time

10 Day Iii 5 Day D 3 Day 0 2 Day I Day* 12 Hour** 6 Hour** RUSH** *End of next business day unless otherwise specified.** Matrix Dependent. ***Please notify the lab before shipping***

- 1 -

Client: SME

9000 Commerce Parkway, Suite B •Mount Laurel, NJ 08054

Phone: 877-428-4285/856-231-9449 • Fax: 856-23 l-98 l 8

Sample Log -Bulk Asbestos -

Project: HK Porter - 068260.00.002

Sampling Date/Time: 9/16/13; 1315-1325

Bulk Asbestos Sample Lo!!

Client Sample# iATL# Location/Description Notes

AS1 5124827 Soil Northwest portion of property.

AS2 C)1'?48'>8 '· .~. i... J t:.. Soil Northwest portion of property.

AS3 5124829 Soil Northwest portion of property.

AS4 51;24830 Soil Northwest portion of property.

ASS r.::1,,4c3r .J ·~ "' . •.: Soil Northwest portion of property.

DUP02SOIL c:· 1 •· 4 ~. 3 2 ~.)""' >.; Soil Northwest portion of property.

- 2 -

9000 Commerce Parkway, Ste B

Mount Laurel, NJ 08054

Toll Free 877-428-4285

Local: 856-231-9449

Fax: 856-231-9818CERTIFICATE OF ANALYSIS

Client: Report Date:

Project No.:

Project:

BULK SAMPLE ANALYSIS SUMMARY

Soil & Materials Engineers Inc

5847 West 74th Street

Indianapolis IN 46278

068260.00.002

HK Porter

9/26/2013

Report No: 315245

% Asbestos Type % Non-Asbestos Fibrous Material Type % Non-Fibrous Material

Client No.:

Lab No.:

AS1

5124827 Description / Location:

Northwest Portion Of Property

None Detected None Detected 2 Cellulose 98

Brown Soil

Note: Analysis by EPA Reg 1. 1994, Asbestos in soil, sludges, sediments.


Client No.:

Lab No.:

AS2




Brown Soil



Client No.:

Lab No.:

AS3



PC 2.6 Chrysotile 2 Cellulose PC 95.4

Black Soil



Client No.:

Lab No.:

AS4




Black Soil


NIST-NVLAP No. 101165-0 NY-DOH No. 11021 AIHA-LAP, LLC No. 100188This confidential report relates only to those item(s) tested and does not represent an endorsement by NIST-NVLAP, AIHA or any agency of the U.S. government

This report shall not be reproduced except in full, without written approval of the laboratory.

Accreditation

EPA 600/R-93/116, by Polarized Light MicroscopyAnalytical Method:

Comments: Quantification at <0.25% by volume is possible with this method. (PC) Indicates Stratified Point Count Method performed. (PC-Trace) means that asbestos was detected but is not

quantifiable under the Point Counting regimen. Analysis includes all distinct separable layers in accordance with EPA 600 Method. If not reported or otherwise noted, layer is either not

present or the client has specifically requested that it not be analyzed (ex. analyze until positive instructions). Small asbestos fibers may be missed by PLM due to resolution limitations of

the optical microscope. Therefore, PLM is not consistently reliable in detecting asbestos in non-friable organically bound (NOB) materials. Quantitative transmission electron microscopy

(TEM) is currently the only method that can pronounce materials as non-asbestos containing.

Analysis Performed By:

Page 1 of 2

Approved By:

Frank E. Ehrenfeld, III

Laboratory Director9/26/2013

R. Caran

___________________________

Date:

9000 Commerce Parkway, Ste B

Mount Laurel, NJ 08054

Toll Free 877-428-4285

Local: 856-231-9449

Fax: 856-231-9818CERTIFICATE OF ANALYSIS

Client: Report Date:

Project No.:

Project:

BULK SAMPLE ANALYSIS SUMMARY

Soil & Materials Engineers Inc

5847 West 74th Street

Indianapolis IN 46278

068260.00.002

HK Porter

9/26/2013

Report No: 315245


Client No.:

Lab No.:

AS5




Brown Soil



Client No.:

Lab No.:

DUP02SOIL




Brown Soil


NIST-NVLAP No. 101165-0 NY-DOH No. 11021 AIHA-LAP, LLC No. 100188This confidential report relates only to those item(s) tested and does not represent an endorsement by NIST-NVLAP, AIHA or any agency of the U.S. government

This report shall not be reproduced except in full, without written approval of the laboratory.

Accreditation

EPA 600/R-93/116, by Polarized Light MicroscopyAnalytical Method:

Comments: Quantification at <0.25% by volume is possible with this method. (PC) Indicates Stratified Point Count Method performed. (PC-Trace) means that asbestos was detected but is not

quantifiable under the Point Counting regimen. Analysis includes all distinct separable layers in accordance with EPA 600 Method. If not reported or otherwise noted, layer is either not

present or the client has specifically requested that it not be analyzed (ex. analyze until positive instructions). Small asbestos fibers may be missed by PLM due to resolution limitations of

the optical microscope. Therefore, PLM is not consistently reliable in detecting asbestos in non-friable organically bound (NOB) materials. Quantitative transmission electron microscopy

(TEM) is currently the only method that can pronounce materials as non-asbestos containing.

Analysis Performed By:

Page 2 of 2

9/26/2013

R. Caran

Date:

a~r i · www.pacelabs.com

$~onA ··. · Requlnid Client lnfo~tion: : · - --· - -- -- ---

!f°mperiy:-s \,..\~

Section D RequlredCftem lili'orri!ation

SAMPLE ID (A-Z. 0-e/ ,-)

!: ,I ~pie IDs MUST BE UNIQUE

sections . ~Ired Project ll'ifDrination:.

· Reportto:Chm.sh~· · CopyTo. _

.Matrix Codes MATRIX l CODE

Drinking Wafer .water Waste Water Product SOIVSoOd OJI Wipe Air Tissue other

ow WT WW

J> SL OL WP AR TS OT

COMPOSITE START

,.__~------------......... --.... --........... . CHA,N-OF-CUSTODY /.Analytical Request Document The ChaJii-of-Custody Is a LE;GAL DOCUMliNT. All relevant fields must be completed accurately.

sectlonC __ l~volce tnfo_ITT!atiOn: . Attention: · ¢/ J'""" 16~icn/ l

COMPOSITE END/GRAB

Company Name:.

Preservatives -· z i·~

. :f:t'9u~fe(tC-A1t~~1sJif~~~ (Y#J'.I) ..

·~· l!l 6 8

1m· .. · ~-

,a:::

- --· . ~·-

. r OTH!tR ----·

-~r-if

J ~ii~~~~===Em=ct::r==r=u=r•il:--=rmtrm: ... - i-~ - -IJ-.

__ -_~A"f'!ic_ "-· tlMe . A~!§~~-~1 -· ~-~~li-- ·TlM~- SAMPl.ECONDmoNs"'" oi5 ~'l~~'~ .• -·- -- 1- - - ~i · 1~0 I-.- r-- r .. Jl I - . . -vi- - ,- - ,- - I -,. -- 1 - T.· --'01!'-i -1':'~~- ~\ALt....-~ __ __ _ - ~.,..-._.,__~- __ __ ~- __j__?.o:t4_t _· -~---=----l'_j__ ~-- . - _.I . - _ J,~ "·r '!l''_.-.0:-. v-~- >' - - - ...._

. ~

.. . ~~ -~- - - ~ I ()~5 1 ?i.. '/ N '/'

ORIGINAL '$1:MP~e::~~:~:~:~:6 ___ - ~ _ -·-··· _ _ _ _ _ -~ · ~ j [ f ~ ~ I~

SIGNATU~ of SAMPLE~tJJ///(J ~;~:~ec: £18 .. 1\a I~ l I~ 8 l ~ l •important Note: By ~gnlng thls form you are accepUng Paoe's NET 30 day payment terms and agreeing to late charges of 1.5% per m{nth r/r any Invoices nOt paid within 30 days.

., . , F-ALL-Q..020rev.07, 15-May-2007

/' __ ..... aceAnaJyt/cat Client Name: _.._.S ....... M~e,-""------f

Courlerfred Ex 0 UPS 0 USPS 0 Client Cbommercial Oace other

Tracking#: $930 (?q3&"" 3-::rio ..,,/ Custody Seal on Cooler/Box Present: 0 yes p no Seals intact: 0 yes

Packing Material: O Bubble Wrap )ZfBubble Bags [}Jone -»Other

Thermometer Used 1 2 3 4 6 A B c{g)E Type of Ice: ~ Blue None

Cooler Temperature (. ic,.. Ice Visible In Sample Containers: (Corrected, If applicable)

Temp should be above freezing to a~c

Chain of Custod Present:

Chain of Custody Filled Out:

Chain of Custody Relin uished:

Sampler Name & Signature on COC:

Short Hold Time Analysis (<72hr :

Rush Turn Around Time Requested:

Containers Intact:

Sample Labels match COC:

-Includes date/time/ID/Analysis All containers needing acid/base pres. have been checked?

exceptions: ~lform, TOC, O&G

All containers needing preservation are found to be in compliance with EPA recommendation.

Comments:

ONo ON/A 1.

ONo ON/A 2.

ONo ON/A 3,

ON/A 4.

ON/A 5.

ON/A 6.

fos ONo

DYes~ ON/A

Project # _ _....STJf~· _la_rf7_· _l _

0 no Date/Time 5035A kits placed In )Ji: oq 1"312.> tO?k

0 Samples on ice, cooling process has begun

Dyes

Heads ace in VOA Vials ( >6mm): ONo ON/A 10. \GW t) l)

Trip Blank Present: ONo ON/A 11.

Samples Arrived within Hold Time: DYes ONo ON/A 12.

Sufficient Volume: DYes ONo ON/A 13.

Correct Containers Used: DYes ONo ON/A 14.

Client Notification/ Resolution: c rt~ J~'IAJ Datemme: Person Contacted:

Field Data Required? Y I N

Comments/ Resolution:

Project Manager Review:

Form F-IN-0290-rev.04, 28Apr2011

•.

\/LA-t~)

Sample Container Count /2.Analyticaf ( __,,,,,-~" -~ CLIENT: ' ~Mt-i I

COC PAGE :. t of 1.-COC ID# 1i0fb 6Qf2- Project # Sb 'rfJ r 1 ( Sample line

Item DG9H AG1U WGFU AGOU R 4/6 BP2N BP2U BP2S BP3N BP3U BP3S AG3S AG1H Comments

1 t 4 2 \ 4-3 \ 4· 4 \ k 5 I 6 \ 7 I 8 I 9 I 10 I 11 -; I -· 12 8 (

Container Codes

DG9H 40ml HCL amber voa vial AGOU 1 OOmL unpreserv.ed amber glass BP1N 1 liter HN03 .Plastic DG9P 40ml TSP amber vial

AG1U 1 liter unpreserved amber glass AG1H 1 liter HCL amber glass BP1S 1 liter H2S04 plastic DG9S 40ml H2S04.ambervial

WGFU 4oz clear soil iar AG1S 1 liter H2S04 amber glass BP1U 1 liter unpreserved plastic DG9T 40ml Na Thio amber vial

R terra ·core kit AG1T 1 liter Na Thlosulfate amber al BP1Z 1 liter NaOH, Zn, Ac DG9U 40ml unpreserved amber vial -BP2N 500ml HN03 plastic AG2N 500ml HN03 amber glasS BP2A 500ml NaOH, Ase Acid plastic I Wipe/Swab

BP2U 500ml unpreserved plastic AG2S ~· ·--· 500ml H2S04 amber glass BP20 500ml NaOH plastic JGFU 4oz unpreserved amber wide

BP2S 500mL H2S04 plastic AG2U 500ml unpreserved ~mber gla BP2Z 500ml NaOH, Zn Ac U SummaCan --·

BP3N 250ml HN03 plastic AG3U 250ml unpreserved amber gla AF Air Filter VG9H 40ml HCL clear vial ·-

BP3U 250ml unpreserved Piasti.£__ . . . . _ BG1H 1 liter HCL clear alass BP3C 250ml NaOH plastic VG9T 40ml Na Thio. clear vial ---· BP3S 250ml H2S04 plastic BG1S 1 liter H2S04 clear glass BP3Z 250ml NaOH, Zn Ac plastic VG9U 40ml unpreserved clear vial

I-· ........ 4 ••

AG3S 250ml H2S04 glass amb~r--··-- BG1T 1 liter Na Thiosulfate clear ala t---

c Air Cassettes VSG Headspace septa vial & HCL

AG1S 1 liter H2S04 amber glass BG1U 1 liter unpreserved glass DG9B 40ml Na Bisulfate amber vial WGFX 4oz wide jar w/hexane wipe -- 1--• ·-BP1U 1 liter unpreserved Plastic BP1A 1 liter NaOH, Ase Acid Plastic DG9M 40ml MeOH clear vial ZPLC ZiPloc Baa

F-IN-Q-270-rev.02,19Apr2012

I !

I I

Sample Container Count

CLIENT:; 8M~ COC PAGE '2- of 1/-COC ID# ! - Project# $)d}f£}-J ( Sample line

Item DG9H AG1 U WGFU AGOU R 4 / 6 BP2N BP2U BP2S BP3N BP3U BP3S AG3S AG1 H

1 3 \ 2 I 3 ~ 4 '

' 3

5 4 6

7

8

9

10

11

12

Container Codes

DG9H 40mL HCL amber voa vial AGOU 1 OOmL unpreserved amber glass BP1N 1 liter l-:f N03 plastic AG1U 1 liter unpreserved amber alass AG1H 1 liter HCL amber glass BP1S 1 liter H2S04 olastic

WGFU 4oz clear soil jar AG1S 1 liter H2S04 amber glass BP1U 1 liter unpreserved plastic R terra ·core kit AG1T 1 liter Na Thiosulfate amber gl BP1Z 1 liter NaOH, Zn, Ac

BP2N 1 500mL HN03 plastic AG2N 500mL HN03 amber glass BP2A 500mL NaOH, Ase Acid plastic BP2U ! 500mL unpreserved plastic AG2S 500mL H2S04 amber glass BP20 500mL NaOH plastic BP2S · 500mt. H2S04 plastic AG2U 500mL unpreserved amber gla BP2Z 500mL NaOH, Zn Ac BP3N 250mL HN03 plastic AG3U 250mL unpreserved amber gla AF Air Filter -BP3U 250mL unpreserved plastic BG1H 1 liter HCL cleat glass BP3C 250mL NaOH plastic ·-· BP3S 250mL H2S04 plastic · BG1S 1 liter H2S04 clear glass BP3Z 250mL NaOH, Zn Ac plastic --· -~-AG3S 250mL H2S04 glass amber BG1T 1 liter Na Thiosulfate clear gla C Air Cassettes AG1S 1 liter H2S04 amber glass BG1U 1 liter unpreserved glass DG9B 40mL Na Bisulfate amber vial -BP1U 1 liter unoreserved plastic BP1A 1 liter NaOH, Ase Acid plastic DG9M 40mL MeOH clear vial

F-IN-Q-270-rev.02, 19Apr2012

/2.Ana/ylk;al. r~al.N-~ .....

Comments

l-!1J) "'KvrJ ~IA,1',/v <&v ~ b~~ " 0S2-A

• 5PJ-~ -ft

f/7)(.;) (J't/lr;.,"' (c\ .

DG9P 40mL TSP amber vial

DG9S 40mL H2S04 amber vial

DG9T 40mL Na Thio amber vial

DG9U 40mL unpreserved amber vial

I Wipe/Swab

JGFU 4oz unpreserved amber wide

U SummaCan

VG9H 40mL HCL clear vial

VG9T 40mL Na Thio. clear vial --VG9U 40mL unpreserved clear vial ·-

VSG Headspace septa vial & HCL

W.GFX 4oz wide jar w/hexane wipe --~-

ZPLC Ziploc Baa

#=CL#

October 01, 2013

LIMS USE: FR - CHRIS SHAWLIMS OBJECT ID: 5086871

5086871Project:Pace Project No.:

RE:

Mr. Chris ShawSME, Inc.5847 W 74th StreetIndianapolis, IN 46278

HK Porter

Dear Mr. Shaw:Enclosed are the analytical results for sample(s) received by the laboratory on September 17, 2013.The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Tina Sayer forKenneth [email protected] Manager

Enclosures

cc: Mr. Mike Meddock, Soil Materials & Engineering, Inc.

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.7726 Moller Road

Indianapolis, IN 46268

(317)875-5894

Pace Analytical Services, Inc.1233 Dublin Road

Columbus, OH 43215

(614)486-5421

Page 1 of 49

#=CP#

CERTIFICATIONS

Pace Project No.:Project:

5086871HK Porter

Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042

Louisiana/NELAC Certification #: 04076Ohio VAP Certification #: 101170-0Pennsylvania Certification #: 68-04991West Virginia Certification #: 330





(317)875-5894


Columbus, OH 43215

(614)486-5421

Page 2 of 49

#=SS#

SAMPLE SUMMARY


5086871HK Porter

Lab ID Sample ID Matrix Date Collected Date Received

5086871001 SB1(0-2) Solid 09/16/13 11:19 09/17/13 10:25

5086871002 SB2(5.5-6.5) Solid 09/16/13 11:45 09/17/13 10:25

5086871003 DUP01 Soil Solid 09/16/13 08:00 09/17/13 10:25

5086871004 SB3-S(8.0-8.5) Solid 09/16/13 13:27 09/17/13 10:25

5086871011 DUP01 GW Water 09/16/13 08:00 09/17/13 10:25

5086871012 SB2 GW Water 09/16/13 15:45 09/17/13 10:25

5086871013 SB3 GW Water 09/16/13 16:30 09/17/13 10:25

5086871014 AST (Surface) Solid 09/16/13 15:00 09/17/13 10:25

5086871015 Trip Blank Water Water 09/16/13 08:00 09/17/13 10:25

5086871016 Trip Blank Soil Solid 09/16/13 08:00 09/17/13 10:25

5086871017 SB2 A Solid 09/16/13 12:16 09/17/13 10:25





(317)875-5894


Columbus, OH 43215

(614)486-5421

Page 3 of 49

#=SA#

SAMPLE ANALYTE COUNT


5086871HK Porter

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

5086871001 SB1(0-2) EPA 6010 1 PASI-IFRW

EPA 8260 75 PASI-IAMV

ASTM D2974-87 1 PASI-IDDM

5086871002 SB2(5.5-6.5) EPA 6010 1 PASI-IFRW



5086871003 DUP01 Soil EPA 6010 1 PASI-IFRW



5086871004 SB3-S(8.0-8.5) EPA 6010 1 PASI-IFRW



5086871011 DUP01 GW EPA 6010 1 PASI-IFRW

EPA 8260 75 PASI-IDAE

5086871012 SB2 GW EPA 6010 1 PASI-IFRW


5086871013 SB3 GW EPA 6010 1 PASI-IFRW


5086871014 AST (Surface) EPA 8270 68 PASI-IKES


5086871015 Trip Blank Water EPA 8260 75 PASI-IDAE

5086871016 Trip Blank Soil EPA 8260 75 PASI-IAMV

5086871017 SB2 A EPA 8260 75 PASI-IAMV






(317)875-5894


Columbus, OH 43215

(614)486-5421

Page 4 of 49

#=AR#

ANALYTICAL RESULTS


5086871HK Porter

Sample: SB1(0-2) Lab ID: 5086871001 Collected: 09/16/13 11:19 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050

Lead 541 mg/kg 09/24/13 12:11 7439-92-109/23/13 10:592.0 1

8260/5035A Volatile Organics Analytical Method: EPA 8260

Acetone ND mg/kg 09/28/13 16:02 67-64-10.13 1Acrolein ND mg/kg 09/28/13 16:02 107-02-80.13 1Acrylonitrile ND mg/kg 09/28/13 16:02 107-13-10.13 1Benzene ND mg/kg 09/28/13 16:02 71-43-20.0067 1Bromobenzene ND mg/kg 09/28/13 16:02 108-86-10.0067 1Bromochloromethane ND mg/kg 09/28/13 16:02 74-97-50.0067 1Bromodichloromethane ND mg/kg 09/28/13 16:02 75-27-40.0067 1Bromoform ND mg/kg 09/28/13 16:02 75-25-20.0067 1Bromomethane ND mg/kg 09/28/13 16:02 74-83-90.0067 12-Butanone (MEK) ND mg/kg 09/28/13 16:02 78-93-30.033 1n-Butylbenzene ND mg/kg 09/28/13 16:02 104-51-80.0067 1sec-Butylbenzene ND mg/kg 09/28/13 16:02 135-98-80.0067 1tert-Butylbenzene ND mg/kg 09/28/13 16:02 98-06-60.0067 1Carbon disulfide ND mg/kg 09/28/13 16:02 75-15-00.013 1Carbon tetrachloride ND mg/kg 09/28/13 16:02 56-23-50.0067 1Chlorobenzene ND mg/kg 09/28/13 16:02 108-90-70.0067 1Chloroethane ND mg/kg 09/28/13 16:02 75-00-30.0067 1Chloroform ND mg/kg 09/28/13 16:02 67-66-30.0067 1Chloromethane ND mg/kg 09/28/13 16:02 74-87-30.0067 12-Chlorotoluene ND mg/kg 09/28/13 16:02 95-49-80.0067 14-Chlorotoluene ND mg/kg 09/28/13 16:02 106-43-40.0067 1Dibromochloromethane ND mg/kg 09/28/13 16:02 124-48-10.0067 11,2-Dibromoethane (EDB) ND mg/kg 09/28/13 16:02 106-93-40.0067 1Dibromomethane ND mg/kg 09/28/13 16:02 74-95-30.0067 11,2-Dichlorobenzene ND mg/kg 09/28/13 16:02 95-50-10.0067 11,3-Dichlorobenzene ND mg/kg 09/28/13 16:02 541-73-10.0067 11,4-Dichlorobenzene ND mg/kg 09/28/13 16:02 106-46-70.0067 1trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 16:02 110-57-60.13 1Dichlorodifluoromethane ND mg/kg 09/28/13 16:02 75-71-80.0067 11,1-Dichloroethane ND mg/kg 09/28/13 16:02 75-34-30.0067 11,2-Dichloroethane ND mg/kg 09/28/13 16:02 107-06-20.0067 11,1-Dichloroethene ND mg/kg 09/28/13 16:02 75-35-40.0067 1cis-1,2-Dichloroethene ND mg/kg 09/28/13 16:02 156-59-20.0067 1trans-1,2-Dichloroethene ND mg/kg 09/28/13 16:02 156-60-50.0067 11,2-Dichloropropane ND mg/kg 09/28/13 16:02 78-87-50.0067 11,3-Dichloropropane ND mg/kg 09/28/13 16:02 142-28-90.0067 12,2-Dichloropropane ND mg/kg 09/28/13 16:02 594-20-70.0067 11,1-Dichloropropene ND mg/kg 09/28/13 16:02 563-58-60.0067 1cis-1,3-Dichloropropene ND mg/kg 09/28/13 16:02 10061-01-50.0067 1trans-1,3-Dichloropropene ND mg/kg 09/28/13 16:02 10061-02-60.0067 1Ethylbenzene ND mg/kg 09/28/13 16:02 100-41-40.0067 1Ethyl methacrylate ND mg/kg 09/28/13 16:02 97-63-20.13 1Hexachloro-1,3-butadiene ND mg/kg 09/28/13 16:02 87-68-30.0067 1


without the written consent of Pace Analytical Services, Inc..Date: 10/01/2013 11:45 AM



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ANALYTICAL RESULTS


5086871HK Porter

Sample: SB1(0-2) Lab ID: 5086871001 Collected: 09/16/13 11:19 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



n-Hexane ND mg/kg 09/28/13 16:02 110-54-3 N20.0067 12-Hexanone ND mg/kg 09/28/13 16:02 591-78-60.13 1Iodomethane ND mg/kg 09/28/13 16:02 74-88-40.13 1Isopropylbenzene (Cumene) ND mg/kg 09/28/13 16:02 98-82-80.0067 1p-Isopropyltoluene ND mg/kg 09/28/13 16:02 99-87-60.0067 1Methylene Chloride ND mg/kg 09/28/13 16:02 75-09-20.027 11-Methylnaphthalene ND mg/kg 09/28/13 16:02 90-12-0 N20.013 12-Methylnaphthalene ND mg/kg 09/28/13 16:02 91-57-6 N20.013 14-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 16:02 108-10-10.033 1Methyl-tert-butyl ether ND mg/kg 09/28/13 16:02 1634-04-40.0067 1Naphthalene ND mg/kg 09/28/13 16:02 91-20-30.0067 1n-Propylbenzene ND mg/kg 09/28/13 16:02 103-65-10.0067 1Styrene ND mg/kg 09/28/13 16:02 100-42-50.0067 11,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 16:02 630-20-60.0067 11,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 16:02 79-34-50.0067 1Tetrachloroethene ND mg/kg 09/28/13 16:02 127-18-40.0067 1Toluene ND mg/kg 09/28/13 16:02 108-88-30.0067 11,2,3-Trichlorobenzene ND mg/kg 09/28/13 16:02 87-61-60.0067 11,2,4-Trichlorobenzene ND mg/kg 09/28/13 16:02 120-82-10.0067 11,1,1-Trichloroethane ND mg/kg 09/28/13 16:02 71-55-60.0067 11,1,2-Trichloroethane ND mg/kg 09/28/13 16:02 79-00-50.0067 1Trichloroethene ND mg/kg 09/28/13 16:02 79-01-60.0067 1Trichlorofluoromethane ND mg/kg 09/28/13 16:02 75-69-40.0067 11,2,3-Trichloropropane ND mg/kg 09/28/13 16:02 96-18-40.0067 11,2,4-Trimethylbenzene ND mg/kg 09/28/13 16:02 95-63-60.0067 11,3,5-Trimethylbenzene ND mg/kg 09/28/13 16:02 108-67-80.0067 1Vinyl acetate ND mg/kg 09/28/13 16:02 108-05-40.13 1Vinyl chloride ND mg/kg 09/28/13 16:02 75-01-40.0067 1Xylene (Total) ND mg/kg 09/28/13 16:02 1330-20-70.013 1SurrogatesDibromofluoromethane (S) 97 %. 09/28/13 16:02 1868-53-785-118 1Toluene-d8 (S) 115 %. 09/28/13 16:02 2037-26-571-128 14-Bromofluorobenzene (S) 77 %. 09/28/13 16:02 460-00-456-144 1

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 5.4 % 09/20/13 14:160.10 1





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ANALYTICAL RESULTS


5086871HK Porter

Sample: SB2(5.5-6.5) Lab ID: 5086871002 Collected: 09/16/13 11:45 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



Lead 13.3 mg/kg 09/24/13 12:13 7439-92-109/23/13 10:591.9 1


Acetone ND mg/kg 09/28/13 16:42 67-64-12.8 25Acrolein ND mg/kg 09/28/13 16:42 107-02-82.8 25Acrylonitrile ND mg/kg 09/28/13 16:42 107-13-12.8 25Benzene ND mg/kg 09/28/13 16:42 71-43-2 2d0.14 25Bromobenzene ND mg/kg 09/28/13 16:42 108-86-10.14 25Bromochloromethane ND mg/kg 09/28/13 16:42 74-97-50.14 25Bromodichloromethane ND mg/kg 09/28/13 16:42 75-27-40.14 25Bromoform ND mg/kg 09/28/13 16:42 75-25-20.14 25Bromomethane ND mg/kg 09/28/13 16:42 74-83-90.14 252-Butanone (MEK) ND mg/kg 09/28/13 16:42 78-93-30.71 25n-Butylbenzene ND mg/kg 09/28/13 16:42 104-51-80.14 25sec-Butylbenzene ND mg/kg 09/28/13 16:42 135-98-80.14 25tert-Butylbenzene ND mg/kg 09/28/13 16:42 98-06-60.14 25Carbon disulfide ND mg/kg 09/28/13 16:42 75-15-00.28 25Carbon tetrachloride ND mg/kg 09/28/13 16:42 56-23-50.14 25Chlorobenzene ND mg/kg 09/28/13 16:42 108-90-70.14 25Chloroethane ND mg/kg 09/28/13 16:42 75-00-30.14 25Chloroform ND mg/kg 09/28/13 16:42 67-66-30.14 25Chloromethane ND mg/kg 09/28/13 16:42 74-87-30.14 252-Chlorotoluene ND mg/kg 09/28/13 16:42 95-49-80.14 254-Chlorotoluene ND mg/kg 09/28/13 16:42 106-43-40.14 25Dibromochloromethane ND mg/kg 09/28/13 16:42 124-48-10.14 251,2-Dibromoethane (EDB) ND mg/kg 09/28/13 16:42 106-93-40.14 25Dibromomethane ND mg/kg 09/28/13 16:42 74-95-30.14 251,2-Dichlorobenzene ND mg/kg 09/28/13 16:42 95-50-10.14 251,3-Dichlorobenzene ND mg/kg 09/28/13 16:42 541-73-10.14 251,4-Dichlorobenzene ND mg/kg 09/28/13 16:42 106-46-70.14 25trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 16:42 110-57-62.8 25Dichlorodifluoromethane ND mg/kg 09/28/13 16:42 75-71-80.14 251,1-Dichloroethane ND mg/kg 09/28/13 16:42 75-34-30.14 251,2-Dichloroethane ND mg/kg 09/28/13 16:42 107-06-20.14 251,1-Dichloroethene ND mg/kg 09/28/13 16:42 75-35-40.14 25cis-1,2-Dichloroethene ND mg/kg 09/28/13 16:42 156-59-20.14 25trans-1,2-Dichloroethene ND mg/kg 09/28/13 16:42 156-60-50.14 251,2-Dichloropropane ND mg/kg 09/28/13 16:42 78-87-50.14 251,3-Dichloropropane ND mg/kg 09/28/13 16:42 142-28-90.14 252,2-Dichloropropane ND mg/kg 09/28/13 16:42 594-20-70.14 251,1-Dichloropropene ND mg/kg 09/28/13 16:42 563-58-60.14 25cis-1,3-Dichloropropene ND mg/kg 09/28/13 16:42 10061-01-50.14 25trans-1,3-Dichloropropene ND mg/kg 09/28/13 16:42 10061-02-60.14 25Ethylbenzene 0.23 mg/kg 09/28/13 16:42 100-41-40.14 25Ethyl methacrylate ND mg/kg 09/28/13 16:42 97-63-22.8 25Hexachloro-1,3-butadiene ND mg/kg 09/28/13 16:42 87-68-30.14 25





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Columbus, OH 43215

(614)486-5421

Page 7 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: SB2(5.5-6.5) Lab ID: 5086871002 Collected: 09/16/13 11:45 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



n-Hexane ND mg/kg 09/28/13 16:42 110-54-3 N20.14 252-Hexanone ND mg/kg 09/28/13 16:42 591-78-62.8 25Iodomethane ND mg/kg 09/28/13 16:42 74-88-42.8 25Isopropylbenzene (Cumene) ND mg/kg 09/28/13 16:42 98-82-80.14 25p-Isopropyltoluene ND mg/kg 09/28/13 16:42 99-87-60.14 25Methylene Chloride ND mg/kg 09/28/13 16:42 75-09-20.57 251-Methylnaphthalene ND mg/kg 09/28/13 16:42 90-12-0 N20.28 252-Methylnaphthalene ND mg/kg 09/28/13 16:42 91-57-6 N20.28 254-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 16:42 108-10-10.71 25Methyl-tert-butyl ether ND mg/kg 09/28/13 16:42 1634-04-40.14 25Naphthalene ND mg/kg 09/28/13 16:42 91-20-30.14 25n-Propylbenzene ND mg/kg 09/28/13 16:42 103-65-10.14 25Styrene ND mg/kg 09/28/13 16:42 100-42-50.14 251,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 16:42 630-20-60.14 251,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 16:42 79-34-50.14 25Tetrachloroethene ND mg/kg 09/28/13 16:42 127-18-40.14 25Toluene ND mg/kg 09/28/13 16:42 108-88-30.14 251,2,3-Trichlorobenzene ND mg/kg 09/28/13 16:42 87-61-60.14 251,2,4-Trichlorobenzene ND mg/kg 09/28/13 16:42 120-82-10.14 251,1,1-Trichloroethane ND mg/kg 09/28/13 16:42 71-55-60.14 251,1,2-Trichloroethane ND mg/kg 09/28/13 16:42 79-00-50.14 25Trichloroethene ND mg/kg 09/28/13 16:42 79-01-60.14 25Trichlorofluoromethane ND mg/kg 09/28/13 16:42 75-69-40.14 251,2,3-Trichloropropane ND mg/kg 09/28/13 16:42 96-18-40.14 251,2,4-Trimethylbenzene 0.57 mg/kg 09/28/13 16:42 95-63-60.14 251,3,5-Trimethylbenzene 0.27 mg/kg 09/28/13 16:42 108-67-80.14 25Vinyl acetate ND mg/kg 09/28/13 16:42 108-05-42.8 25Vinyl chloride ND mg/kg 09/28/13 16:42 75-01-40.14 25Xylene (Total) 0.82 mg/kg 09/28/13 16:42 1330-20-70.28 25SurrogatesDibromofluoromethane (S) 88 %. 09/28/13 16:42 1868-53-7 D485-118 25Toluene-d8 (S) 127 %. 09/28/13 16:42 2037-26-571-128 254-Bromofluorobenzene (S) 101 %. 09/28/13 16:42 460-00-456-144 25







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Columbus, OH 43215

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Page 8 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: DUP01 Soil Lab ID: 5086871003 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



Lead ND mg/kg 09/24/13 12:16 7439-92-109/23/13 10:591.8 1


Acetone ND mg/kg 09/28/13 18:01 67-64-12.6 25Acrolein ND mg/kg 09/28/13 18:01 107-02-82.6 25Acrylonitrile ND mg/kg 09/28/13 18:01 107-13-12.6 25Benzene ND mg/kg 09/28/13 18:01 71-43-2 2d0.13 25Bromobenzene ND mg/kg 09/28/13 18:01 108-86-10.13 25Bromochloromethane ND mg/kg 09/28/13 18:01 74-97-50.13 25Bromodichloromethane ND mg/kg 09/28/13 18:01 75-27-40.13 25Bromoform ND mg/kg 09/28/13 18:01 75-25-20.13 25Bromomethane ND mg/kg 09/28/13 18:01 74-83-90.13 252-Butanone (MEK) ND mg/kg 09/28/13 18:01 78-93-30.65 25n-Butylbenzene ND mg/kg 09/28/13 18:01 104-51-80.13 25sec-Butylbenzene ND mg/kg 09/28/13 18:01 135-98-80.13 25tert-Butylbenzene ND mg/kg 09/28/13 18:01 98-06-60.13 25Carbon disulfide ND mg/kg 09/28/13 18:01 75-15-00.26 25Carbon tetrachloride ND mg/kg 09/28/13 18:01 56-23-50.13 25Chlorobenzene ND mg/kg 09/28/13 18:01 108-90-70.13 25Chloroethane ND mg/kg 09/28/13 18:01 75-00-30.13 25Chloroform ND mg/kg 09/28/13 18:01 67-66-30.13 25Chloromethane ND mg/kg 09/28/13 18:01 74-87-30.13 252-Chlorotoluene ND mg/kg 09/28/13 18:01 95-49-80.13 254-Chlorotoluene ND mg/kg 09/28/13 18:01 106-43-40.13 25Dibromochloromethane ND mg/kg 09/28/13 18:01 124-48-10.13 251,2-Dibromoethane (EDB) ND mg/kg 09/28/13 18:01 106-93-40.13 25Dibromomethane ND mg/kg 09/28/13 18:01 74-95-30.13 251,2-Dichlorobenzene ND mg/kg 09/28/13 18:01 95-50-10.13 251,3-Dichlorobenzene ND mg/kg 09/28/13 18:01 541-73-10.13 251,4-Dichlorobenzene ND mg/kg 09/28/13 18:01 106-46-70.13 25trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 18:01 110-57-62.6 25Dichlorodifluoromethane ND mg/kg 09/28/13 18:01 75-71-80.13 251,1-Dichloroethane ND mg/kg 09/28/13 18:01 75-34-30.13 251,2-Dichloroethane ND mg/kg 09/28/13 18:01 107-06-20.13 251,1-Dichloroethene ND mg/kg 09/28/13 18:01 75-35-40.13 25cis-1,2-Dichloroethene ND mg/kg 09/28/13 18:01 156-59-20.13 25trans-1,2-Dichloroethene ND mg/kg 09/28/13 18:01 156-60-50.13 251,2-Dichloropropane ND mg/kg 09/28/13 18:01 78-87-50.13 251,3-Dichloropropane ND mg/kg 09/28/13 18:01 142-28-90.13 252,2-Dichloropropane ND mg/kg 09/28/13 18:01 594-20-70.13 251,1-Dichloropropene ND mg/kg 09/28/13 18:01 563-58-60.13 25cis-1,3-Dichloropropene ND mg/kg 09/28/13 18:01 10061-01-50.13 25trans-1,3-Dichloropropene ND mg/kg 09/28/13 18:01 10061-02-60.13 25Ethylbenzene 0.18 mg/kg 09/28/13 18:01 100-41-40.13 25Ethyl methacrylate ND mg/kg 09/28/13 18:01 97-63-22.6 25Hexachloro-1,3-butadiene ND mg/kg 09/28/13 18:01 87-68-30.13 25





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Page 9 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: DUP01 Soil Lab ID: 5086871003 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



n-Hexane ND mg/kg 09/28/13 18:01 110-54-3 N20.13 252-Hexanone ND mg/kg 09/28/13 18:01 591-78-62.6 25Iodomethane ND mg/kg 09/28/13 18:01 74-88-42.6 25Isopropylbenzene (Cumene) ND mg/kg 09/28/13 18:01 98-82-80.13 25p-Isopropyltoluene ND mg/kg 09/28/13 18:01 99-87-60.13 25Methylene Chloride ND mg/kg 09/28/13 18:01 75-09-20.52 251-Methylnaphthalene ND mg/kg 09/28/13 18:01 90-12-0 N20.26 252-Methylnaphthalene ND mg/kg 09/28/13 18:01 91-57-6 N20.26 254-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 18:01 108-10-10.65 25Methyl-tert-butyl ether ND mg/kg 09/28/13 18:01 1634-04-40.13 25Naphthalene ND mg/kg 09/28/13 18:01 91-20-30.13 25n-Propylbenzene ND mg/kg 09/28/13 18:01 103-65-10.13 25Styrene ND mg/kg 09/28/13 18:01 100-42-50.13 251,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 18:01 630-20-60.13 251,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 18:01 79-34-50.13 25Tetrachloroethene ND mg/kg 09/28/13 18:01 127-18-40.13 25Toluene ND mg/kg 09/28/13 18:01 108-88-30.13 251,2,3-Trichlorobenzene ND mg/kg 09/28/13 18:01 87-61-60.13 251,2,4-Trichlorobenzene ND mg/kg 09/28/13 18:01 120-82-10.13 251,1,1-Trichloroethane ND mg/kg 09/28/13 18:01 71-55-60.13 251,1,2-Trichloroethane ND mg/kg 09/28/13 18:01 79-00-50.13 25Trichloroethene ND mg/kg 09/28/13 18:01 79-01-60.13 25Trichlorofluoromethane ND mg/kg 09/28/13 18:01 75-69-40.13 251,2,3-Trichloropropane ND mg/kg 09/28/13 18:01 96-18-40.13 251,2,4-Trimethylbenzene 0.35 mg/kg 09/28/13 18:01 95-63-60.13 251,3,5-Trimethylbenzene 0.20 mg/kg 09/28/13 18:01 108-67-80.13 25Vinyl acetate ND mg/kg 09/28/13 18:01 108-05-42.6 25Vinyl chloride ND mg/kg 09/28/13 18:01 75-01-40.13 25Xylene (Total) 0.71 mg/kg 09/28/13 18:01 1330-20-70.26 25SurrogatesDibromofluoromethane (S) 89 %. 09/28/13 18:01 1868-53-7 D485-118 25Toluene-d8 (S) 132 %. 09/28/13 18:01 2037-26-5 S571-128 254-Bromofluorobenzene (S) 102 %. 09/28/13 18:01 460-00-456-144 25







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(614)486-5421

Page 10 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: SB3-S(8.0-8.5) Lab ID: 5086871004 Collected: 09/16/13 13:27 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



Lead 9.5 mg/kg 09/24/13 12:18 7439-92-109/23/13 10:592.1 1


Acetone ND mg/kg 09/28/13 19:20 67-64-12.1 25Acrolein ND mg/kg 09/28/13 19:20 107-02-82.1 25Acrylonitrile ND mg/kg 09/28/13 19:20 107-13-12.1 25Benzene ND mg/kg 09/28/13 19:20 71-43-2 2d0.10 25Bromobenzene ND mg/kg 09/28/13 19:20 108-86-10.10 25Bromochloromethane ND mg/kg 09/28/13 19:20 74-97-50.10 25Bromodichloromethane ND mg/kg 09/28/13 19:20 75-27-40.10 25Bromoform ND mg/kg 09/28/13 19:20 75-25-20.10 25Bromomethane ND mg/kg 09/28/13 19:20 74-83-90.10 252-Butanone (MEK) ND mg/kg 09/28/13 19:20 78-93-30.51 25n-Butylbenzene ND mg/kg 09/28/13 19:20 104-51-80.10 25sec-Butylbenzene 0.12 mg/kg 09/28/13 19:20 135-98-80.10 25tert-Butylbenzene ND mg/kg 09/28/13 19:20 98-06-60.10 25Carbon disulfide ND mg/kg 09/28/13 19:20 75-15-00.21 25Carbon tetrachloride ND mg/kg 09/28/13 19:20 56-23-50.10 25Chlorobenzene ND mg/kg 09/28/13 19:20 108-90-70.10 25Chloroethane ND mg/kg 09/28/13 19:20 75-00-30.10 25Chloroform ND mg/kg 09/28/13 19:20 67-66-30.10 25Chloromethane ND mg/kg 09/28/13 19:20 74-87-30.10 252-Chlorotoluene ND mg/kg 09/28/13 19:20 95-49-80.10 254-Chlorotoluene ND mg/kg 09/28/13 19:20 106-43-40.10 25Dibromochloromethane ND mg/kg 09/28/13 19:20 124-48-10.10 251,2-Dibromoethane (EDB) ND mg/kg 09/28/13 19:20 106-93-40.10 25Dibromomethane ND mg/kg 09/28/13 19:20 74-95-30.10 251,2-Dichlorobenzene ND mg/kg 09/28/13 19:20 95-50-10.10 251,3-Dichlorobenzene ND mg/kg 09/28/13 19:20 541-73-10.10 251,4-Dichlorobenzene ND mg/kg 09/28/13 19:20 106-46-70.10 25trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 19:20 110-57-62.1 25Dichlorodifluoromethane ND mg/kg 09/28/13 19:20 75-71-80.10 251,1-Dichloroethane ND mg/kg 09/28/13 19:20 75-34-30.10 251,2-Dichloroethane ND mg/kg 09/28/13 19:20 107-06-20.10 251,1-Dichloroethene ND mg/kg 09/28/13 19:20 75-35-40.10 25cis-1,2-Dichloroethene ND mg/kg 09/28/13 19:20 156-59-20.10 25trans-1,2-Dichloroethene ND mg/kg 09/28/13 19:20 156-60-50.10 251,2-Dichloropropane ND mg/kg 09/28/13 19:20 78-87-50.10 251,3-Dichloropropane ND mg/kg 09/28/13 19:20 142-28-90.10 252,2-Dichloropropane ND mg/kg 09/28/13 19:20 594-20-70.10 251,1-Dichloropropene ND mg/kg 09/28/13 19:20 563-58-60.10 25cis-1,3-Dichloropropene ND mg/kg 09/28/13 19:20 10061-01-50.10 25trans-1,3-Dichloropropene ND mg/kg 09/28/13 19:20 10061-02-60.10 25Ethylbenzene ND mg/kg 09/28/13 19:20 100-41-40.10 25Ethyl methacrylate ND mg/kg 09/28/13 19:20 97-63-22.1 25Hexachloro-1,3-butadiene ND mg/kg 09/28/13 19:20 87-68-30.10 25





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Sample: SB3-S(8.0-8.5) Lab ID: 5086871004 Collected: 09/16/13 13:27 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



n-Hexane ND mg/kg 09/28/13 19:20 110-54-3 N20.10 252-Hexanone ND mg/kg 09/28/13 19:20 591-78-62.1 25Iodomethane ND mg/kg 09/28/13 19:20 74-88-42.1 25Isopropylbenzene (Cumene) ND mg/kg 09/28/13 19:20 98-82-80.10 25p-Isopropyltoluene ND mg/kg 09/28/13 19:20 99-87-60.10 25Methylene Chloride ND mg/kg 09/28/13 19:20 75-09-20.41 251-Methylnaphthalene ND mg/kg 09/28/13 19:20 90-12-0 N20.21 252-Methylnaphthalene ND mg/kg 09/28/13 19:20 91-57-6 N20.21 254-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 19:20 108-10-10.51 25Methyl-tert-butyl ether ND mg/kg 09/28/13 19:20 1634-04-40.10 25Naphthalene ND mg/kg 09/28/13 19:20 91-20-30.10 25n-Propylbenzene ND mg/kg 09/28/13 19:20 103-65-10.10 25Styrene ND mg/kg 09/28/13 19:20 100-42-50.10 251,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 19:20 630-20-60.10 251,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 19:20 79-34-50.10 25Tetrachloroethene ND mg/kg 09/28/13 19:20 127-18-40.10 25Toluene ND mg/kg 09/28/13 19:20 108-88-30.10 251,2,3-Trichlorobenzene ND mg/kg 09/28/13 19:20 87-61-60.10 251,2,4-Trichlorobenzene ND mg/kg 09/28/13 19:20 120-82-10.10 251,1,1-Trichloroethane ND mg/kg 09/28/13 19:20 71-55-60.10 251,1,2-Trichloroethane ND mg/kg 09/28/13 19:20 79-00-50.10 25Trichloroethene ND mg/kg 09/28/13 19:20 79-01-60.10 25Trichlorofluoromethane ND mg/kg 09/28/13 19:20 75-69-40.10 251,2,3-Trichloropropane ND mg/kg 09/28/13 19:20 96-18-40.10 251,2,4-Trimethylbenzene ND mg/kg 09/28/13 19:20 95-63-60.10 251,3,5-Trimethylbenzene ND mg/kg 09/28/13 19:20 108-67-80.10 25Vinyl acetate ND mg/kg 09/28/13 19:20 108-05-42.1 25Vinyl chloride ND mg/kg 09/28/13 19:20 75-01-40.10 25Xylene (Total) ND mg/kg 09/28/13 19:20 1330-20-70.21 25SurrogatesDibromofluoromethane (S) 90 %. 09/28/13 19:20 1868-53-7 D385-118 25Toluene-d8 (S) 99 %. 09/28/13 19:20 2037-26-571-128 254-Bromofluorobenzene (S) 103 %. 09/28/13 19:20 460-00-456-144 25







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Sample: DUP01 GW Lab ID: 5086871011 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: Water



Lead 115 ug/L 09/23/13 08:23 7439-92-109/20/13 09:4710.0 1

8260 MSV Indiana Analytical Method: EPA 8260

Acetone ND ug/L 09/28/13 06:47 67-64-1100 1Acrolein ND ug/L 09/28/13 06:47 107-02-850.0 1Acrylonitrile ND ug/L 09/28/13 06:47 107-13-1100 1Benzene ND ug/L 09/28/13 06:47 71-43-25.0 1Bromobenzene ND ug/L 09/28/13 06:47 108-86-15.0 1Bromochloromethane ND ug/L 09/28/13 06:47 74-97-55.0 1Bromodichloromethane ND ug/L 09/28/13 06:47 75-27-45.0 1Bromoform ND ug/L 09/28/13 06:47 75-25-25.0 1Bromomethane ND ug/L 09/28/13 06:47 74-83-95.0 12-Butanone (MEK) ND ug/L 09/28/13 06:47 78-93-325.0 1n-Butylbenzene ND ug/L 09/28/13 06:47 104-51-85.0 1sec-Butylbenzene ND ug/L 09/28/13 06:47 135-98-85.0 1tert-Butylbenzene ND ug/L 09/28/13 06:47 98-06-65.0 1Carbon disulfide ND ug/L 09/28/13 06:47 75-15-010.0 1Carbon tetrachloride ND ug/L 09/28/13 06:47 56-23-55.0 1Chlorobenzene ND ug/L 09/28/13 06:47 108-90-75.0 1Chloroethane ND ug/L 09/28/13 06:47 75-00-35.0 1Chloroform ND ug/L 09/28/13 06:47 67-66-35.0 1Chloromethane ND ug/L 09/28/13 06:47 74-87-35.0 12-Chlorotoluene ND ug/L 09/28/13 06:47 95-49-85.0 14-Chlorotoluene ND ug/L 09/28/13 06:47 106-43-45.0 1Dibromochloromethane ND ug/L 09/28/13 06:47 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 09/28/13 06:47 106-93-45.0 1Dibromomethane ND ug/L 09/28/13 06:47 74-95-35.0 11,2-Dichlorobenzene ND ug/L 09/28/13 06:47 95-50-15.0 11,3-Dichlorobenzene ND ug/L 09/28/13 06:47 541-73-15.0 11,4-Dichlorobenzene ND ug/L 09/28/13 06:47 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 09/28/13 06:47 110-57-6100 1Dichlorodifluoromethane ND ug/L 09/28/13 06:47 75-71-85.0 11,1-Dichloroethane ND ug/L 09/28/13 06:47 75-34-35.0 11,2-Dichloroethane ND ug/L 09/28/13 06:47 107-06-25.0 11,1-Dichloroethene ND ug/L 09/28/13 06:47 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 09/28/13 06:47 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 09/28/13 06:47 156-60-55.0 11,2-Dichloropropane ND ug/L 09/28/13 06:47 78-87-55.0 11,3-Dichloropropane ND ug/L 09/28/13 06:47 142-28-95.0 12,2-Dichloropropane ND ug/L 09/28/13 06:47 594-20-75.0 11,1-Dichloropropene ND ug/L 09/28/13 06:47 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 09/28/13 06:47 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 09/28/13 06:47 10061-02-65.0 1Ethylbenzene ND ug/L 09/28/13 06:47 100-41-45.0 1Ethyl methacrylate ND ug/L 09/28/13 06:47 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 09/28/13 06:47 87-68-35.0 1n-Hexane ND ug/L 09/28/13 06:47 110-54-3 N25.0 1





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Sample: DUP01 GW Lab ID: 5086871011 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: Water



2-Hexanone ND ug/L 09/28/13 06:47 591-78-625.0 1Iodomethane ND ug/L 09/28/13 06:47 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 09/28/13 06:47 98-82-85.0 1p-Isopropyltoluene ND ug/L 09/28/13 06:47 99-87-65.0 1Methylene Chloride ND ug/L 09/28/13 06:47 75-09-25.0 11-Methylnaphthalene ND ug/L 09/28/13 06:47 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 09/28/13 06:47 91-57-6 N210.0 14-Methyl-2-pentanone (MIBK) ND ug/L 09/28/13 06:47 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 09/28/13 06:47 1634-04-44.0 1Naphthalene ND ug/L 09/28/13 06:47 91-20-31.4 1n-Propylbenzene ND ug/L 09/28/13 06:47 103-65-15.0 1Styrene ND ug/L 09/28/13 06:47 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 09/28/13 06:47 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 09/28/13 06:47 79-34-55.0 1Tetrachloroethene ND ug/L 09/28/13 06:47 127-18-45.0 1Toluene ND ug/L 09/28/13 06:47 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 09/28/13 06:47 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 09/28/13 06:47 120-82-15.0 11,1,1-Trichloroethane ND ug/L 09/28/13 06:47 71-55-65.0 11,1,2-Trichloroethane ND ug/L 09/28/13 06:47 79-00-55.0 1Trichloroethene ND ug/L 09/28/13 06:47 79-01-65.0 1Trichlorofluoromethane ND ug/L 09/28/13 06:47 75-69-45.0 11,2,3-Trichloropropane ND ug/L 09/28/13 06:47 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 09/28/13 06:47 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 09/28/13 06:47 108-67-85.0 1Vinyl acetate ND ug/L 09/28/13 06:47 108-05-450.0 1Vinyl chloride ND ug/L 09/28/13 06:47 75-01-42.0 1Xylene (Total) ND ug/L 09/28/13 06:47 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 101 %. 09/28/13 06:47 1868-53-779-116 14-Bromofluorobenzene (S) 100 %. 09/28/13 06:47 460-00-480-114 1Toluene-d8 (S) 102 %. 09/28/13 06:47 2037-26-581-110 1





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Sample: SB2 GW Lab ID: 5086871012 Collected: 09/16/13 15:45 Received: 09/17/13 10:25 Matrix: Water



Lead 3610 ug/L 09/23/13 08:25 7439-92-109/20/13 09:4710.0 1


Acetone ND ug/L 09/28/13 07:52 67-64-1100 1Acrolein ND ug/L 09/28/13 07:52 107-02-850.0 1Acrylonitrile ND ug/L 09/28/13 07:52 107-13-1100 1Benzene 327 ug/L 09/28/13 08:25 71-43-2125 25Bromobenzene ND ug/L 09/28/13 07:52 108-86-15.0 1Bromochloromethane ND ug/L 09/28/13 07:52 74-97-55.0 1Bromodichloromethane ND ug/L 09/28/13 07:52 75-27-45.0 1Bromoform ND ug/L 09/28/13 07:52 75-25-25.0 1Bromomethane ND ug/L 09/28/13 07:52 74-83-95.0 12-Butanone (MEK) 73.1 ug/L 09/28/13 07:52 78-93-325.0 1n-Butylbenzene ND ug/L 09/28/13 07:52 104-51-85.0 1sec-Butylbenzene ND ug/L 09/28/13 07:52 135-98-85.0 1tert-Butylbenzene ND ug/L 09/28/13 07:52 98-06-65.0 1Carbon disulfide ND ug/L 09/28/13 07:52 75-15-010.0 1Carbon tetrachloride ND ug/L 09/28/13 07:52 56-23-55.0 1Chlorobenzene ND ug/L 09/28/13 07:52 108-90-75.0 1Chloroethane ND ug/L 09/28/13 07:52 75-00-35.0 1Chloroform ND ug/L 09/28/13 07:52 67-66-35.0 1Chloromethane ND ug/L 09/28/13 07:52 74-87-35.0 12-Chlorotoluene ND ug/L 09/28/13 07:52 95-49-85.0 14-Chlorotoluene ND ug/L 09/28/13 07:52 106-43-45.0 1Dibromochloromethane ND ug/L 09/28/13 07:52 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 09/28/13 07:52 106-93-45.0 1Dibromomethane ND ug/L 09/28/13 07:52 74-95-35.0 11,2-Dichlorobenzene ND ug/L 09/28/13 07:52 95-50-15.0 11,3-Dichlorobenzene ND ug/L 09/28/13 07:52 541-73-15.0 11,4-Dichlorobenzene ND ug/L 09/28/13 07:52 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 09/28/13 07:52 110-57-6100 1Dichlorodifluoromethane ND ug/L 09/28/13 07:52 75-71-85.0 11,1-Dichloroethane ND ug/L 09/28/13 07:52 75-34-35.0 11,2-Dichloroethane ND ug/L 09/28/13 07:52 107-06-25.0 11,1-Dichloroethene ND ug/L 09/28/13 07:52 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 09/28/13 07:52 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 09/28/13 07:52 156-60-55.0 11,2-Dichloropropane ND ug/L 09/28/13 07:52 78-87-55.0 11,3-Dichloropropane ND ug/L 09/28/13 07:52 142-28-95.0 12,2-Dichloropropane ND ug/L 09/28/13 07:52 594-20-75.0 11,1-Dichloropropene ND ug/L 09/28/13 07:52 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 09/28/13 07:52 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 09/28/13 07:52 10061-02-65.0 1Ethylbenzene 466 ug/L 09/28/13 08:25 100-41-4125 25Ethyl methacrylate ND ug/L 09/28/13 07:52 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 09/28/13 07:52 87-68-35.0 1n-Hexane 11.0 ug/L 09/28/13 07:52 110-54-3 N25.0 1





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2-Hexanone ND ug/L 09/28/13 07:52 591-78-625.0 1Iodomethane ND ug/L 09/28/13 07:52 74-88-410.0 1Isopropylbenzene (Cumene) 36.6 ug/L 09/28/13 07:52 98-82-85.0 1p-Isopropyltoluene ND ug/L 09/28/13 07:52 99-87-65.0 1Methylene Chloride ND ug/L 09/28/13 07:52 75-09-25.0 11-Methylnaphthalene ND ug/L 09/28/13 07:52 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 09/28/13 07:52 91-57-6 N210.0 14-Methyl-2-pentanone (MIBK) ND ug/L 09/28/13 07:52 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 09/28/13 07:52 1634-04-44.0 1Naphthalene 5.5 ug/L 09/28/13 07:52 91-20-31.4 1n-Propylbenzene 50.3 ug/L 09/28/13 07:52 103-65-15.0 1Styrene ND ug/L 09/28/13 07:52 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 09/28/13 07:52 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 09/28/13 07:52 79-34-55.0 1Tetrachloroethene ND ug/L 09/28/13 07:52 127-18-45.0 1Toluene ND ug/L 09/28/13 07:52 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 09/28/13 07:52 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 09/28/13 07:52 120-82-15.0 11,1,1-Trichloroethane ND ug/L 09/28/13 07:52 71-55-65.0 11,1,2-Trichloroethane ND ug/L 09/28/13 07:52 79-00-55.0 1Trichloroethene ND ug/L 09/28/13 07:52 79-01-65.0 1Trichlorofluoromethane ND ug/L 09/28/13 07:52 75-69-45.0 11,2,3-Trichloropropane ND ug/L 09/28/13 07:52 96-18-45.0 11,2,4-Trimethylbenzene 207 ug/L 09/28/13 07:52 95-63-65.0 11,3,5-Trimethylbenzene 56.6 ug/L 09/28/13 07:52 108-67-85.0 1Vinyl acetate ND ug/L 09/28/13 07:52 108-05-450.0 1Vinyl chloride ND ug/L 09/28/13 07:52 75-01-42.0 1Xylene (Total) 978 ug/L 09/28/13 08:25 1330-20-7250 25SurrogatesDibromofluoromethane (S) 103 %. 09/28/13 07:52 1868-53-779-116 14-Bromofluorobenzene (S) 99 %. 09/28/13 07:52 460-00-480-114 1Toluene-d8 (S) 131 %. 09/28/13 07:52 2037-26-5 S581-110 1





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Lead 122 ug/L 09/23/13 08:27 7439-92-109/20/13 09:4710.0 1


Acetone ND ug/L 09/28/13 08:58 67-64-1100 1Acrolein ND ug/L 09/28/13 08:58 107-02-850.0 1Acrylonitrile ND ug/L 09/28/13 08:58 107-13-1100 1Benzene ND ug/L 09/28/13 08:58 71-43-25.0 1Bromobenzene ND ug/L 09/28/13 08:58 108-86-15.0 1Bromochloromethane ND ug/L 09/28/13 08:58 74-97-55.0 1Bromodichloromethane ND ug/L 09/28/13 08:58 75-27-45.0 1Bromoform ND ug/L 09/28/13 08:58 75-25-25.0 1Bromomethane ND ug/L 09/28/13 08:58 74-83-95.0 12-Butanone (MEK) ND ug/L 09/28/13 08:58 78-93-325.0 1n-Butylbenzene ND ug/L 09/28/13 08:58 104-51-85.0 1sec-Butylbenzene ND ug/L 09/28/13 08:58 135-98-85.0 1tert-Butylbenzene ND ug/L 09/28/13 08:58 98-06-65.0 1Carbon disulfide ND ug/L 09/28/13 08:58 75-15-010.0 1Carbon tetrachloride ND ug/L 09/28/13 08:58 56-23-55.0 1Chlorobenzene ND ug/L 09/28/13 08:58 108-90-75.0 1Chloroethane ND ug/L 09/28/13 08:58 75-00-35.0 1Chloroform ND ug/L 09/28/13 08:58 67-66-35.0 1Chloromethane ND ug/L 09/28/13 08:58 74-87-35.0 12-Chlorotoluene ND ug/L 09/28/13 08:58 95-49-85.0 14-Chlorotoluene ND ug/L 09/28/13 08:58 106-43-45.0 1Dibromochloromethane ND ug/L 09/28/13 08:58 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 09/28/13 08:58 106-93-45.0 1Dibromomethane ND ug/L 09/28/13 08:58 74-95-35.0 11,2-Dichlorobenzene ND ug/L 09/28/13 08:58 95-50-15.0 11,3-Dichlorobenzene ND ug/L 09/28/13 08:58 541-73-15.0 11,4-Dichlorobenzene ND ug/L 09/28/13 08:58 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 09/28/13 08:58 110-57-6100 1Dichlorodifluoromethane ND ug/L 09/28/13 08:58 75-71-85.0 11,1-Dichloroethane ND ug/L 09/28/13 08:58 75-34-35.0 11,2-Dichloroethane ND ug/L 09/28/13 08:58 107-06-25.0 11,1-Dichloroethene ND ug/L 09/28/13 08:58 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 09/28/13 08:58 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 09/28/13 08:58 156-60-55.0 11,2-Dichloropropane ND ug/L 09/28/13 08:58 78-87-55.0 11,3-Dichloropropane ND ug/L 09/28/13 08:58 142-28-95.0 12,2-Dichloropropane ND ug/L 09/28/13 08:58 594-20-75.0 11,1-Dichloropropene ND ug/L 09/28/13 08:58 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 09/28/13 08:58 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 09/28/13 08:58 10061-02-65.0 1Ethylbenzene ND ug/L 09/28/13 08:58 100-41-45.0 1Ethyl methacrylate ND ug/L 09/28/13 08:58 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 09/28/13 08:58 87-68-35.0 1n-Hexane ND ug/L 09/28/13 08:58 110-54-3 N25.0 1





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ANALYTICAL RESULTS


5086871HK Porter




2-Hexanone ND ug/L 09/28/13 08:58 591-78-625.0 1Iodomethane ND ug/L 09/28/13 08:58 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 09/28/13 08:58 98-82-85.0 1p-Isopropyltoluene ND ug/L 09/28/13 08:58 99-87-65.0 1Methylene Chloride ND ug/L 09/28/13 08:58 75-09-25.0 11-Methylnaphthalene ND ug/L 09/28/13 08:58 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 09/28/13 08:58 91-57-6 N210.0 14-Methyl-2-pentanone (MIBK) ND ug/L 09/28/13 08:58 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 09/28/13 08:58 1634-04-44.0 1Naphthalene ND ug/L 09/28/13 08:58 91-20-31.4 1n-Propylbenzene ND ug/L 09/28/13 08:58 103-65-15.0 1Styrene ND ug/L 09/28/13 08:58 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 09/28/13 08:58 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 09/28/13 08:58 79-34-55.0 1Tetrachloroethene ND ug/L 09/28/13 08:58 127-18-45.0 1Toluene ND ug/L 09/28/13 08:58 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 09/28/13 08:58 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 09/28/13 08:58 120-82-15.0 11,1,1-Trichloroethane ND ug/L 09/28/13 08:58 71-55-65.0 11,1,2-Trichloroethane ND ug/L 09/28/13 08:58 79-00-55.0 1Trichloroethene ND ug/L 09/28/13 08:58 79-01-65.0 1Trichlorofluoromethane ND ug/L 09/28/13 08:58 75-69-45.0 11,2,3-Trichloropropane ND ug/L 09/28/13 08:58 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 09/28/13 08:58 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 09/28/13 08:58 108-67-85.0 1Vinyl acetate ND ug/L 09/28/13 08:58 108-05-450.0 1Vinyl chloride ND ug/L 09/28/13 08:58 75-01-42.0 1Xylene (Total) ND ug/L 09/28/13 08:58 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 102 %. 09/28/13 08:58 1868-53-779-116 14-Bromofluorobenzene (S) 99 %. 09/28/13 08:58 460-00-480-114 1Toluene-d8 (S) 101 %. 09/28/13 08:58 2037-26-581-110 1





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ANALYTICAL RESULTS


5086871HK Porter

Sample: AST (Surface) Lab ID: 5086871014 Collected: 09/16/13 15:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis


8270 MSSV SHORT LISTMICROWAVE

Analytical Method: EPA 8270 Preparation Method: EPA 3546

Acenaphthene ND mg/kg 09/24/13 09:36 83-32-909/18/13 10:402.2 5Acenaphthylene ND mg/kg 09/24/13 09:36 208-96-809/18/13 10:402.2 5Anthracene ND mg/kg 09/24/13 09:36 120-12-709/18/13 10:402.2 5Benzo(a)anthracene ND mg/kg 09/24/13 09:36 56-55-309/18/13 10:402.2 5Benzo(a)pyrene ND mg/kg 09/24/13 09:36 50-32-809/18/13 10:401.1 5Benzo(b)fluoranthene ND mg/kg 09/24/13 09:36 205-99-209/18/13 10:402.2 5Benzo(g,h,i)perylene ND mg/kg 09/24/13 09:36 191-24-209/18/13 10:402.2 5Benzo(k)fluoranthene ND mg/kg 09/24/13 09:36 207-08-909/18/13 10:402.2 5Benzyl alcohol ND mg/kg 09/24/13 09:36 100-51-609/18/13 10:404.4 54-Bromophenylphenyl ether ND mg/kg 09/24/13 09:36 101-55-309/18/13 10:402.2 5Butylbenzylphthalate ND mg/kg 09/24/13 09:36 85-68-709/18/13 10:402.2 54-Chloro-3-methylphenol ND mg/kg 09/24/13 09:36 59-50-709/18/13 10:404.4 54-Chloroaniline ND mg/kg 09/24/13 09:36 106-47-809/18/13 10:404.4 5bis(2-Chloroethoxy)methane ND mg/kg 09/24/13 09:36 111-91-109/18/13 10:402.2 5bis(2-Chloroethyl) ether ND mg/kg 09/24/13 09:36 111-44-409/18/13 10:402.2 5bis(2-Chloroisopropyl) ether ND mg/kg 09/24/13 09:36 108-60-109/18/13 10:402.2 5bis(2chloro1methylethyl) ether ND mg/kg 09/24/13 09:36 108-60-109/18/13 10:402.2 52-Chloronaphthalene ND mg/kg 09/24/13 09:36 91-58-709/18/13 10:402.2 52-Chlorophenol ND mg/kg 09/24/13 09:36 95-57-809/18/13 10:402.2 54-Chlorophenylphenyl ether ND mg/kg 09/24/13 09:36 7005-72-309/18/13 10:402.2 5Chrysene ND mg/kg 09/24/13 09:36 218-01-909/18/13 10:402.2 5Dibenz(a,h)anthracene ND mg/kg 09/24/13 09:36 53-70-309/18/13 10:401.1 5Dibenzofuran ND mg/kg 09/24/13 09:36 132-64-909/18/13 10:402.2 53,3'-Dichlorobenzidine ND mg/kg 09/24/13 09:36 91-94-109/18/13 10:404.4 52,4-Dichlorophenol ND mg/kg 09/24/13 09:36 120-83-209/18/13 10:402.2 5Diethylphthalate ND mg/kg 09/24/13 09:36 84-66-209/18/13 10:402.2 52,4-Dimethylphenol ND mg/kg 09/24/13 09:36 105-67-909/18/13 10:402.2 5Dimethylphthalate ND mg/kg 09/24/13 09:36 131-11-309/18/13 10:402.2 5Di-n-butylphthalate ND mg/kg 09/24/13 09:36 84-74-209/18/13 10:402.2 54,6-Dinitro-2-methylphenol ND mg/kg 09/24/13 09:36 534-52-109/18/13 10:4010.8 52,4-Dinitrophenol ND mg/kg 09/24/13 09:36 51-28-509/18/13 10:4010.8 52,4-Dinitrotoluene ND mg/kg 09/24/13 09:36 121-14-209/18/13 10:402.2 52,6-Dinitrotoluene ND mg/kg 09/24/13 09:36 606-20-209/18/13 10:402.2 5Di-n-octylphthalate ND mg/kg 09/24/13 09:36 117-84-009/18/13 10:402.2 5bis(2-Ethylhexyl)phthalate ND mg/kg 09/24/13 09:36 117-81-709/18/13 10:402.2 5Fluoranthene ND mg/kg 09/24/13 09:36 206-44-009/18/13 10:402.2 5Fluorene ND mg/kg 09/24/13 09:36 86-73-709/18/13 10:402.2 5Hexachloro-1,3-butadiene ND mg/kg 09/24/13 09:36 87-68-309/18/13 10:402.2 5Hexachlorobenzene ND mg/kg 09/24/13 09:36 118-74-109/18/13 10:402.2 5Hexachlorocyclopentadiene ND mg/kg 09/24/13 09:36 77-47-409/18/13 10:402.2 5Hexachloroethane ND mg/kg 09/24/13 09:36 67-72-109/18/13 10:402.2 5Indeno(1,2,3-cd)pyrene ND mg/kg 09/24/13 09:36 193-39-509/18/13 10:402.2 5Isophorone ND mg/kg 09/24/13 09:36 78-59-109/18/13 10:402.2 51-Methylnaphthalene ND mg/kg 09/24/13 09:36 90-12-0 N209/18/13 10:402.2 52-Methylnaphthalene ND mg/kg 09/24/13 09:36 91-57-609/18/13 10:402.2 5





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Page 19 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: AST (Surface) Lab ID: 5086871014 Collected: 09/16/13 15:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis


8270 MSSV SHORT LISTMICROWAVE

Analytical Method: EPA 8270 Preparation Method: EPA 3546

2-Methylphenol(o-Cresol) ND mg/kg 09/24/13 09:36 95-48-709/18/13 10:402.2 53&4-Methylphenol(m&p Cresol) ND mg/kg 09/24/13 09:3609/18/13 10:404.4 5Naphthalene ND mg/kg 09/24/13 09:36 91-20-309/18/13 10:402.2 52-Nitroaniline ND mg/kg 09/24/13 09:36 88-74-409/18/13 10:4010.8 53-Nitroaniline ND mg/kg 09/24/13 09:36 99-09-209/18/13 10:4010.8 54-Nitroaniline ND mg/kg 09/24/13 09:36 100-01-609/18/13 10:4010.8 5Nitrobenzene ND mg/kg 09/24/13 09:36 98-95-309/18/13 10:402.2 52-Nitrophenol ND mg/kg 09/24/13 09:36 88-75-509/18/13 10:402.2 54-Nitrophenol ND mg/kg 09/24/13 09:36 100-02-709/18/13 10:4010.8 5N-Nitroso-di-n-propylamine ND mg/kg 09/24/13 09:36 621-64-709/18/13 10:402.2 5N-Nitrosodiphenylamine ND mg/kg 09/24/13 09:36 86-30-609/18/13 10:402.2 5Pentachlorophenol ND mg/kg 09/24/13 09:36 87-86-509/18/13 10:4010.8 5Phenanthrene ND mg/kg 09/24/13 09:36 85-01-809/18/13 10:402.2 5Phenol 3.7 mg/kg 09/24/13 09:36 108-95-2 3d09/18/13 10:402.2 5Pyrene ND mg/kg 09/24/13 09:36 129-00-009/18/13 10:402.2 52,4,5-Trichlorophenol ND mg/kg 09/24/13 09:36 95-95-409/18/13 10:402.2 52,4,6-Trichlorophenol ND mg/kg 09/24/13 09:36 88-06-209/18/13 10:402.2 5SurrogatesNitrobenzene-d5 (S) 24 %. 09/24/13 09:36 4165-60-0 S409/18/13 10:4028-101 52-Fluorobiphenyl (S) 27 %. 09/24/13 09:36 321-60-8 S409/18/13 10:4031-94 5p-Terphenyl-d14 (S) 33 %. 09/24/13 09:36 1718-51-009/18/13 10:4026-110 5Phenol-d5 (S) 26 %. 09/24/13 09:36 4165-62-2 S409/18/13 10:4028-101 52-Fluorophenol (S) 24 %. 09/24/13 09:36 367-12-409/18/13 10:4024-104 52,4,6-Tribromophenol (S) 0 %. 09/24/13 09:36 118-79-6 S409/18/13 10:4016-122 5







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Page 20 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: Trip Blank Water Lab ID: 5086871015 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: Water



Acetone ND ug/L 09/28/13 09:31 67-64-1100 1Acrolein ND ug/L 09/28/13 09:31 107-02-850.0 1Acrylonitrile ND ug/L 09/28/13 09:31 107-13-1100 1Benzene ND ug/L 09/28/13 09:31 71-43-25.0 1Bromobenzene ND ug/L 09/28/13 09:31 108-86-15.0 1Bromochloromethane ND ug/L 09/28/13 09:31 74-97-55.0 1Bromodichloromethane ND ug/L 09/28/13 09:31 75-27-45.0 1Bromoform ND ug/L 09/28/13 09:31 75-25-25.0 1Bromomethane ND ug/L 09/28/13 09:31 74-83-95.0 12-Butanone (MEK) ND ug/L 09/28/13 09:31 78-93-325.0 1n-Butylbenzene ND ug/L 09/28/13 09:31 104-51-85.0 1sec-Butylbenzene ND ug/L 09/28/13 09:31 135-98-85.0 1tert-Butylbenzene ND ug/L 09/28/13 09:31 98-06-65.0 1Carbon disulfide ND ug/L 09/28/13 09:31 75-15-010.0 1Carbon tetrachloride ND ug/L 09/28/13 09:31 56-23-55.0 1Chlorobenzene ND ug/L 09/28/13 09:31 108-90-75.0 1Chloroethane ND ug/L 09/28/13 09:31 75-00-35.0 1Chloroform ND ug/L 09/28/13 09:31 67-66-35.0 1Chloromethane ND ug/L 09/28/13 09:31 74-87-35.0 12-Chlorotoluene ND ug/L 09/28/13 09:31 95-49-85.0 14-Chlorotoluene ND ug/L 09/28/13 09:31 106-43-45.0 1Dibromochloromethane ND ug/L 09/28/13 09:31 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 09/28/13 09:31 106-93-45.0 1Dibromomethane ND ug/L 09/28/13 09:31 74-95-35.0 11,2-Dichlorobenzene ND ug/L 09/28/13 09:31 95-50-15.0 11,3-Dichlorobenzene ND ug/L 09/28/13 09:31 541-73-15.0 11,4-Dichlorobenzene ND ug/L 09/28/13 09:31 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 09/28/13 09:31 110-57-6100 1Dichlorodifluoromethane ND ug/L 09/28/13 09:31 75-71-85.0 11,1-Dichloroethane ND ug/L 09/28/13 09:31 75-34-35.0 11,2-Dichloroethane ND ug/L 09/28/13 09:31 107-06-25.0 11,1-Dichloroethene ND ug/L 09/28/13 09:31 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 09/28/13 09:31 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 09/28/13 09:31 156-60-55.0 11,2-Dichloropropane ND ug/L 09/28/13 09:31 78-87-55.0 11,3-Dichloropropane ND ug/L 09/28/13 09:31 142-28-95.0 12,2-Dichloropropane ND ug/L 09/28/13 09:31 594-20-75.0 11,1-Dichloropropene ND ug/L 09/28/13 09:31 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 09/28/13 09:31 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 09/28/13 09:31 10061-02-65.0 1Ethylbenzene ND ug/L 09/28/13 09:31 100-41-45.0 1Ethyl methacrylate ND ug/L 09/28/13 09:31 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 09/28/13 09:31 87-68-35.0 1n-Hexane ND ug/L 09/28/13 09:31 110-54-3 N25.0 12-Hexanone ND ug/L 09/28/13 09:31 591-78-625.0 1Iodomethane ND ug/L 09/28/13 09:31 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 09/28/13 09:31 98-82-85.0 1





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Page 21 of 49

#=AR#

ANALYTICAL RESULTS


5086871HK Porter

Sample: Trip Blank Water Lab ID: 5086871015 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: Water



p-Isopropyltoluene ND ug/L 09/28/13 09:31 99-87-65.0 1Methylene Chloride ND ug/L 09/28/13 09:31 75-09-25.0 11-Methylnaphthalene ND ug/L 09/28/13 09:31 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 09/28/13 09:31 91-57-6 N210.0 14-Methyl-2-pentanone (MIBK) ND ug/L 09/28/13 09:31 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 09/28/13 09:31 1634-04-44.0 1Naphthalene ND ug/L 09/28/13 09:31 91-20-31.4 1n-Propylbenzene ND ug/L 09/28/13 09:31 103-65-15.0 1Styrene ND ug/L 09/28/13 09:31 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 09/28/13 09:31 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 09/28/13 09:31 79-34-55.0 1Tetrachloroethene ND ug/L 09/28/13 09:31 127-18-45.0 1Toluene ND ug/L 09/28/13 09:31 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 09/28/13 09:31 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 09/28/13 09:31 120-82-15.0 11,1,1-Trichloroethane ND ug/L 09/28/13 09:31 71-55-65.0 11,1,2-Trichloroethane ND ug/L 09/28/13 09:31 79-00-55.0 1Trichloroethene ND ug/L 09/28/13 09:31 79-01-65.0 1Trichlorofluoromethane ND ug/L 09/28/13 09:31 75-69-45.0 11,2,3-Trichloropropane ND ug/L 09/28/13 09:31 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 09/28/13 09:31 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 09/28/13 09:31 108-67-85.0 1Vinyl acetate ND ug/L 09/28/13 09:31 108-05-450.0 1Vinyl chloride ND ug/L 09/28/13 09:31 75-01-42.0 1Xylene (Total) ND ug/L 09/28/13 09:31 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 100 %. 09/28/13 09:31 1868-53-779-116 14-Bromofluorobenzene (S) 99 %. 09/28/13 09:31 460-00-480-114 1Toluene-d8 (S) 99 %. 09/28/13 09:31 2037-26-581-110 1





(317)875-5894


Columbus, OH 43215

(614)486-5421

Page 22 of 49

#=AR#

ANALYTICAL RESULTS


5086871HK Porter

Sample: Trip Blank Soil Lab ID: 5086871016 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "wet-weight" basis



Acetone ND mg/kg 09/28/13 19:59 67-64-10.10 1Acrolein ND mg/kg 09/28/13 19:59 107-02-80.10 1Acrylonitrile ND mg/kg 09/28/13 19:59 107-13-10.10 1Benzene ND mg/kg 09/28/13 19:59 71-43-20.0050 1Bromobenzene ND mg/kg 09/28/13 19:59 108-86-10.0050 1Bromochloromethane ND mg/kg 09/28/13 19:59 74-97-50.0050 1Bromodichloromethane ND mg/kg 09/28/13 19:59 75-27-40.0050 1Bromoform ND mg/kg 09/28/13 19:59 75-25-20.0050 1Bromomethane ND mg/kg 09/28/13 19:59 74-83-90.0050 12-Butanone (MEK) ND mg/kg 09/28/13 19:59 78-93-30.025 1n-Butylbenzene ND mg/kg 09/28/13 19:59 104-51-80.0050 1sec-Butylbenzene ND mg/kg 09/28/13 19:59 135-98-80.0050 1tert-Butylbenzene ND mg/kg 09/28/13 19:59 98-06-60.0050 1Carbon disulfide ND mg/kg 09/28/13 19:59 75-15-00.010 1Carbon tetrachloride ND mg/kg 09/28/13 19:59 56-23-50.0050 1Chlorobenzene ND mg/kg 09/28/13 19:59 108-90-70.0050 1Chloroethane ND mg/kg 09/28/13 19:59 75-00-30.0050 1Chloroform ND mg/kg 09/28/13 19:59 67-66-30.0050 1Chloromethane ND mg/kg 09/28/13 19:59 74-87-30.0050 12-Chlorotoluene ND mg/kg 09/28/13 19:59 95-49-80.0050 14-Chlorotoluene ND mg/kg 09/28/13 19:59 106-43-40.0050 1Dibromochloromethane ND mg/kg 09/28/13 19:59 124-48-10.0050 11,2-Dibromoethane (EDB) ND mg/kg 09/28/13 19:59 106-93-40.0050 1Dibromomethane ND mg/kg 09/28/13 19:59 74-95-30.0050 11,2-Dichlorobenzene ND mg/kg 09/28/13 19:59 95-50-10.0050 11,3-Dichlorobenzene ND mg/kg 09/28/13 19:59 541-73-10.0050 11,4-Dichlorobenzene ND mg/kg 09/28/13 19:59 106-46-70.0050 1trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 19:59 110-57-60.10 1Dichlorodifluoromethane ND mg/kg 09/28/13 19:59 75-71-80.0050 11,1-Dichloroethane ND mg/kg 09/28/13 19:59 75-34-30.0050 11,2-Dichloroethane ND mg/kg 09/28/13 19:59 107-06-20.0050 11,1-Dichloroethene ND mg/kg 09/28/13 19:59 75-35-40.0050 1cis-1,2-Dichloroethene ND mg/kg 09/28/13 19:59 156-59-20.0050 1trans-1,2-Dichloroethene ND mg/kg 09/28/13 19:59 156-60-50.0050 11,2-Dichloropropane ND mg/kg 09/28/13 19:59 78-87-50.0050 11,3-Dichloropropane ND mg/kg 09/28/13 19:59 142-28-90.0050 12,2-Dichloropropane ND mg/kg 09/28/13 19:59 594-20-70.0050 11,1-Dichloropropene ND mg/kg 09/28/13 19:59 563-58-60.0050 1cis-1,3-Dichloropropene ND mg/kg 09/28/13 19:59 10061-01-50.0050 1trans-1,3-Dichloropropene ND mg/kg 09/28/13 19:59 10061-02-60.0050 1Ethylbenzene ND mg/kg 09/28/13 19:59 100-41-40.0050 1Ethyl methacrylate ND mg/kg 09/28/13 19:59 97-63-20.10 1Hexachloro-1,3-butadiene ND mg/kg 09/28/13 19:59 87-68-30.0050 1n-Hexane ND mg/kg 09/28/13 19:59 110-54-3 N20.0050 12-Hexanone ND mg/kg 09/28/13 19:59 591-78-60.10 1Iodomethane ND mg/kg 09/28/13 19:59 74-88-40.10 1





(317)875-5894


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(614)486-5421

Page 23 of 49

#=AR#

ANALYTICAL RESULTS


5086871HK Porter

Sample: Trip Blank Soil Lab ID: 5086871016 Collected: 09/16/13 08:00 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "wet-weight" basis



Isopropylbenzene (Cumene) ND mg/kg 09/28/13 19:59 98-82-80.0050 1p-Isopropyltoluene ND mg/kg 09/28/13 19:59 99-87-60.0050 1Methylene Chloride ND mg/kg 09/28/13 19:59 75-09-20.020 11-Methylnaphthalene ND mg/kg 09/28/13 19:59 90-12-0 N20.010 12-Methylnaphthalene ND mg/kg 09/28/13 19:59 91-57-6 N20.010 14-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 19:59 108-10-10.025 1Methyl-tert-butyl ether ND mg/kg 09/28/13 19:59 1634-04-40.0050 1Naphthalene ND mg/kg 09/28/13 19:59 91-20-30.0050 1n-Propylbenzene ND mg/kg 09/28/13 19:59 103-65-10.0050 1Styrene ND mg/kg 09/28/13 19:59 100-42-50.0050 11,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 19:59 630-20-60.0050 11,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 19:59 79-34-50.0050 1Tetrachloroethene ND mg/kg 09/28/13 19:59 127-18-40.0050 1Toluene ND mg/kg 09/28/13 19:59 108-88-30.0050 11,2,3-Trichlorobenzene ND mg/kg 09/28/13 19:59 87-61-60.0050 11,2,4-Trichlorobenzene ND mg/kg 09/28/13 19:59 120-82-10.0050 11,1,1-Trichloroethane ND mg/kg 09/28/13 19:59 71-55-60.0050 11,1,2-Trichloroethane ND mg/kg 09/28/13 19:59 79-00-50.0050 1Trichloroethene ND mg/kg 09/28/13 19:59 79-01-60.0050 1Trichlorofluoromethane ND mg/kg 09/28/13 19:59 75-69-40.0050 11,2,3-Trichloropropane ND mg/kg 09/28/13 19:59 96-18-40.0050 11,2,4-Trimethylbenzene ND mg/kg 09/28/13 19:59 95-63-60.0050 11,3,5-Trimethylbenzene ND mg/kg 09/28/13 19:59 108-67-80.0050 1Vinyl acetate ND mg/kg 09/28/13 19:59 108-05-40.10 1Vinyl chloride ND mg/kg 09/28/13 19:59 75-01-40.0050 1Xylene (Total) ND mg/kg 09/28/13 19:59 1330-20-70.010 1SurrogatesDibromofluoromethane (S) 96 %. 09/28/13 19:59 1868-53-785-118 1Toluene-d8 (S) 100 %. 09/28/13 19:59 2037-26-571-128 14-Bromofluorobenzene (S) 100 %. 09/28/13 19:59 460-00-456-144 1





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(614)486-5421

Page 24 of 49

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ANALYTICAL RESULTS


5086871HK Porter

Sample: SB2 A Lab ID: 5086871017 Collected: 09/16/13 12:16 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



Acetone ND mg/kg 09/28/13 20:38 67-64-19.6 100Acrolein ND mg/kg 09/28/13 20:38 107-02-89.6 100Acrylonitrile ND mg/kg 09/28/13 20:38 107-13-19.6 100Benzene ND mg/kg 09/28/13 20:38 71-43-2 2d0.48 100Bromobenzene ND mg/kg 09/28/13 20:38 108-86-10.48 100Bromochloromethane ND mg/kg 09/28/13 20:38 74-97-50.48 100Bromodichloromethane ND mg/kg 09/28/13 20:38 75-27-40.48 100Bromoform ND mg/kg 09/28/13 20:38 75-25-20.48 100Bromomethane ND mg/kg 09/28/13 20:38 74-83-90.48 1002-Butanone (MEK) ND mg/kg 09/28/13 20:38 78-93-32.4 100n-Butylbenzene 0.62 mg/kg 09/28/13 20:38 104-51-80.48 100sec-Butylbenzene ND mg/kg 09/28/13 20:38 135-98-80.48 100tert-Butylbenzene ND mg/kg 09/28/13 20:38 98-06-60.48 100Carbon disulfide ND mg/kg 09/28/13 20:38 75-15-00.96 100Carbon tetrachloride ND mg/kg 09/28/13 20:38 56-23-50.48 100Chlorobenzene ND mg/kg 09/28/13 20:38 108-90-70.48 100Chloroethane ND mg/kg 09/28/13 20:38 75-00-30.48 100Chloroform ND mg/kg 09/28/13 20:38 67-66-30.48 100Chloromethane ND mg/kg 09/28/13 20:38 74-87-30.48 1002-Chlorotoluene ND mg/kg 09/28/13 20:38 95-49-80.48 1004-Chlorotoluene ND mg/kg 09/28/13 20:38 106-43-40.48 100Dibromochloromethane ND mg/kg 09/28/13 20:38 124-48-10.48 1001,2-Dibromoethane (EDB) ND mg/kg 09/28/13 20:38 106-93-40.48 100Dibromomethane ND mg/kg 09/28/13 20:38 74-95-30.48 1001,2-Dichlorobenzene ND mg/kg 09/28/13 20:38 95-50-10.48 1001,3-Dichlorobenzene ND mg/kg 09/28/13 20:38 541-73-10.48 1001,4-Dichlorobenzene ND mg/kg 09/28/13 20:38 106-46-70.48 100trans-1,4-Dichloro-2-butene ND mg/kg 09/28/13 20:38 110-57-69.6 100Dichlorodifluoromethane ND mg/kg 09/28/13 20:38 75-71-80.48 1001,1-Dichloroethane ND mg/kg 09/28/13 20:38 75-34-30.48 1001,2-Dichloroethane ND mg/kg 09/28/13 20:38 107-06-20.48 1001,1-Dichloroethene ND mg/kg 09/28/13 20:38 75-35-40.48 100cis-1,2-Dichloroethene ND mg/kg 09/28/13 20:38 156-59-20.48 100trans-1,2-Dichloroethene ND mg/kg 09/28/13 20:38 156-60-50.48 1001,2-Dichloropropane ND mg/kg 09/28/13 20:38 78-87-50.48 1001,3-Dichloropropane ND mg/kg 09/28/13 20:38 142-28-90.48 1002,2-Dichloropropane ND mg/kg 09/28/13 20:38 594-20-70.48 1001,1-Dichloropropene ND mg/kg 09/28/13 20:38 563-58-60.48 100cis-1,3-Dichloropropene ND mg/kg 09/28/13 20:38 10061-01-50.48 100trans-1,3-Dichloropropene ND mg/kg 09/28/13 20:38 10061-02-60.48 100Ethylbenzene 1.6 mg/kg 09/28/13 20:38 100-41-40.48 100Ethyl methacrylate ND mg/kg 09/28/13 20:38 97-63-29.6 100Hexachloro-1,3-butadiene ND mg/kg 09/28/13 20:38 87-68-30.48 100n-Hexane ND mg/kg 09/28/13 20:38 110-54-3 N20.48 1002-Hexanone ND mg/kg 09/28/13 20:38 591-78-69.6 100Iodomethane ND mg/kg 09/28/13 20:38 74-88-49.6 100





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#=AR#

ANALYTICAL RESULTS


5086871HK Porter

Sample: SB2 A Lab ID: 5086871017 Collected: 09/16/13 12:16 Received: 09/17/13 10:25 Matrix: SolidResults reported on a "dry-weight" basis



Isopropylbenzene (Cumene) 1.0 mg/kg 09/28/13 20:38 98-82-80.48 100p-Isopropyltoluene ND mg/kg 09/28/13 20:38 99-87-60.48 100Methylene Chloride ND mg/kg 09/28/13 20:38 75-09-21.9 1001-Methylnaphthalene ND mg/kg 09/28/13 20:38 90-12-0 N20.96 1002-Methylnaphthalene ND mg/kg 09/28/13 20:38 91-57-6 N20.96 1004-Methyl-2-pentanone (MIBK) ND mg/kg 09/28/13 20:38 108-10-12.4 100Methyl-tert-butyl ether ND mg/kg 09/28/13 20:38 1634-04-4 1d0.48 100Naphthalene ND mg/kg 09/28/13 20:38 91-20-30.48 100n-Propylbenzene 2.3 mg/kg 09/28/13 20:38 103-65-10.48 100Styrene ND mg/kg 09/28/13 20:38 100-42-50.48 1001,1,1,2-Tetrachloroethane ND mg/kg 09/28/13 20:38 630-20-60.48 1001,1,2,2-Tetrachloroethane ND mg/kg 09/28/13 20:38 79-34-50.48 100Tetrachloroethene ND mg/kg 09/28/13 20:38 127-18-40.48 100Toluene ND mg/kg 09/28/13 20:38 108-88-30.48 1001,2,3-Trichlorobenzene ND mg/kg 09/28/13 20:38 87-61-60.48 1001,2,4-Trichlorobenzene ND mg/kg 09/28/13 20:38 120-82-10.48 1001,1,1-Trichloroethane ND mg/kg 09/28/13 20:38 71-55-60.48 1001,1,2-Trichloroethane ND mg/kg 09/28/13 20:38 79-00-50.48 100Trichloroethene ND mg/kg 09/28/13 20:38 79-01-60.48 100Trichlorofluoromethane ND mg/kg 09/28/13 20:38 75-69-40.48 1001,2,3-Trichloropropane ND mg/kg 09/28/13 20:38 96-18-40.48 1001,2,4-Trimethylbenzene 5.6 mg/kg 09/28/13 20:38 95-63-60.48 1001,3,5-Trimethylbenzene 0.53 mg/kg 09/28/13 20:38 108-67-80.48 100Vinyl acetate ND mg/kg 09/28/13 20:38 108-05-49.6 100Vinyl chloride ND mg/kg 09/28/13 20:38 75-01-40.48 100Xylene (Total) 1.7 mg/kg 09/28/13 20:38 1330-20-70.96 100SurrogatesDibromofluoromethane (S) 91 %. 09/28/13 20:38 1868-53-7 D485-118 100Toluene-d8 (S) 147 %. 09/28/13 20:38 2037-26-5 S571-128 1004-Bromofluorobenzene (S) 110 %. 09/28/13 20:38 460-00-456-144 100







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#=QC#

QUALITY CONTROL DATA


5086871HK Porter

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

MPRP/12095EPA 3050

EPA 60106010 MET

Associated Lab Samples: 5086871001, 5086871002, 5086871003, 5086871004

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 983938


Matrix: Solid

Analyzed

Lead mg/kg ND 2.0 09/24/13 12:07

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

983939LABORATORY CONTROL SAMPLE:LCSSpike

Lead mg/kg 48.650 97 80-120

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

983940MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

5087115009

983941

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Lead mg/kg 60.3 83 75-12581 9 2055.58.1 57.9 52.9





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5086871HK Porter



MPRP/12082EPA 3010

EPA 60106010 MET

Associated Lab Samples: 5086871011, 5086871012, 5086871013




Associated Lab Samples: 5086871011, 5086871012, 5086871013

Matrix: Water

Analyzed

Lead ug/L ND 10.0 09/23/13 07:37

Parameter UnitsLCS



Lead ug/L 9871000 99 80-120

Parameter UnitsMS



MSSpikeResult

5086926005

982882

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Lead ug/L 1000 95 75-12593 2 20100019.3 973 952





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5086871HK Porter



MSV/57659EPA 8260

EPA 82608260 MSV






Matrix: Water

Analyzed

1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/28/13 02:581,1,1-Trichloroethane ug/L ND 5.0 09/28/13 02:581,1,2,2-Tetrachloroethane ug/L ND 5.0 09/28/13 02:581,1,2-Trichloroethane ug/L ND 5.0 09/28/13 02:581,1-Dichloroethane ug/L ND 5.0 09/28/13 02:581,1-Dichloroethene ug/L ND 5.0 09/28/13 02:581,1-Dichloropropene ug/L ND 5.0 09/28/13 02:581,2,3-Trichlorobenzene ug/L ND 5.0 09/28/13 02:581,2,3-Trichloropropane ug/L ND 5.0 09/28/13 02:581,2,4-Trichlorobenzene ug/L ND 5.0 09/28/13 02:581,2,4-Trimethylbenzene ug/L ND 5.0 09/28/13 02:581,2-Dibromoethane (EDB) ug/L ND 5.0 09/28/13 02:581,2-Dichlorobenzene ug/L ND 5.0 09/28/13 02:581,2-Dichloroethane ug/L ND 5.0 09/28/13 02:581,2-Dichloropropane ug/L ND 5.0 09/28/13 02:581,3,5-Trimethylbenzene ug/L ND 5.0 09/28/13 02:581,3-Dichlorobenzene ug/L ND 5.0 09/28/13 02:581,3-Dichloropropane ug/L ND 5.0 09/28/13 02:581,4-Dichlorobenzene ug/L ND 5.0 09/28/13 02:581-Methylnaphthalene ug/L ND 5.0 N209/28/13 02:582,2-Dichloropropane ug/L ND 5.0 09/28/13 02:582-Butanone (MEK) ug/L ND 25.0 09/28/13 02:582-Chlorotoluene ug/L ND 5.0 09/28/13 02:582-Hexanone ug/L ND 25.0 09/28/13 02:582-Methylnaphthalene ug/L ND 10.0 N209/28/13 02:584-Chlorotoluene ug/L ND 5.0 09/28/13 02:584-Methyl-2-pentanone (MIBK) ug/L ND 25.0 09/28/13 02:58Acetone ug/L ND 100 09/28/13 02:58Acrolein ug/L ND 50.0 09/28/13 02:58Acrylonitrile ug/L ND 100 09/28/13 02:58Benzene ug/L ND 5.0 09/28/13 02:58Bromobenzene ug/L ND 5.0 09/28/13 02:58Bromochloromethane ug/L ND 5.0 09/28/13 02:58Bromodichloromethane ug/L ND 5.0 09/28/13 02:58Bromoform ug/L ND 5.0 09/28/13 02:58Bromomethane ug/L ND 5.0 09/28/13 02:58Carbon disulfide ug/L ND 10.0 09/28/13 02:58Carbon tetrachloride ug/L ND 5.0 09/28/13 02:58Chlorobenzene ug/L ND 5.0 09/28/13 02:58Chloroethane ug/L ND 5.0 09/28/13 02:58Chloroform ug/L ND 5.0 09/28/13 02:58Chloromethane ug/L ND 5.0 09/28/13 02:58cis-1,2-Dichloroethene ug/L ND 5.0 09/28/13 02:58





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5086871HK Porter





Matrix: Water

Analyzed

cis-1,3-Dichloropropene ug/L ND 5.0 09/28/13 02:58Dibromochloromethane ug/L ND 5.0 09/28/13 02:58Dibromomethane ug/L ND 5.0 09/28/13 02:58Dichlorodifluoromethane ug/L ND 5.0 09/28/13 02:58Ethyl methacrylate ug/L ND 100 09/28/13 02:58Ethylbenzene ug/L ND 5.0 09/28/13 02:58Hexachloro-1,3-butadiene ug/L ND 5.0 09/28/13 02:58Iodomethane ug/L ND 10.0 09/28/13 02:58Isopropylbenzene (Cumene) ug/L ND 5.0 09/28/13 02:58Methyl-tert-butyl ether ug/L ND 4.0 09/28/13 02:58Methylene Chloride ug/L ND 5.0 09/28/13 02:58n-Butylbenzene ug/L ND 5.0 09/28/13 02:58n-Hexane ug/L ND 5.0 N209/28/13 02:58n-Propylbenzene ug/L ND 5.0 09/28/13 02:58Naphthalene ug/L ND 1.4 09/28/13 02:58p-Isopropyltoluene ug/L ND 5.0 09/28/13 02:58sec-Butylbenzene ug/L ND 5.0 09/28/13 02:58Styrene ug/L ND 5.0 09/28/13 02:58tert-Butylbenzene ug/L ND 5.0 09/28/13 02:58Tetrachloroethene ug/L ND 5.0 09/28/13 02:58Toluene ug/L ND 5.0 09/28/13 02:58trans-1,2-Dichloroethene ug/L ND 5.0 09/28/13 02:58trans-1,3-Dichloropropene ug/L ND 5.0 09/28/13 02:58trans-1,4-Dichloro-2-butene ug/L ND 100 09/28/13 02:58Trichloroethene ug/L ND 5.0 09/28/13 02:58Trichlorofluoromethane ug/L ND 5.0 09/28/13 02:58Vinyl acetate ug/L ND 50.0 09/28/13 02:58Vinyl chloride ug/L ND 2.0 09/28/13 02:58Xylene (Total) ug/L ND 10.0 09/28/13 02:584-Bromofluorobenzene (S) %. 99 80-114 09/28/13 02:58Dibromofluoromethane (S) %. 102 79-116 09/28/13 02:58Toluene-d8 (S) %. 96 81-110 09/28/13 02:58

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/L 47.250 94 61-1351,1,1-Trichloroethane ug/L 50.950 102 71-1291,1,2,2-Tetrachloroethane ug/L 40.150 80 66-1261,1,2-Trichloroethane ug/L 47.850 96 77-1301,1-Dichloroethane ug/L 46.850 94 75-1301,1-Dichloroethene ug/L 45.050 90 68-1271,1-Dichloropropene ug/L 51.750 103 78-1301,2,3-Trichlorobenzene ug/L 42.350 85 70-1301,2,3-Trichloropropane ug/L 47.150 94 58-142





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Parameter UnitsLCS



1,2,4-Trichlorobenzene ug/L 43.050 86 68-1311,2,4-Trimethylbenzene ug/L 45.550 91 69-1271,2-Dibromoethane (EDB) ug/L 52.550 105 76-1251,2-Dichlorobenzene ug/L 44.450 89 75-1231,2-Dichloroethane ug/L 50.450 101 75-1281,2-Dichloropropane ug/L 51.050 102 74-1211,3,5-Trimethylbenzene ug/L 46.750 93 70-1261,3-Dichlorobenzene ug/L 44.850 90 74-1221,3-Dichloropropane ug/L 49.550 99 74-1231,4-Dichlorobenzene ug/L 42.750 85 76-1202,2-Dichloropropane ug/L 33.250 66 50-1372-Butanone (MEK) ug/L 227250 91 58-1392-Chlorotoluene ug/L 45.950 92 74-1222-Hexanone ug/L 229250 92 54-1402-Methylnaphthalene ug/L 29.9 N250 60 54-1514-Chlorotoluene ug/L 47.550 95 77-1234-Methyl-2-pentanone (MIBK) ug/L 236250 94 58-138Acetone ug/L 221250 88 49-150Acrolein ug/L 7891000 79 41-200Acrylonitrile ug/L 8401000 84 63-137Benzene ug/L 46.050 92 74-122Bromobenzene ug/L 44.050 88 72-127Bromochloromethane ug/L 46.650 93 63-132Bromodichloromethane ug/L 52.550 105 62-136Bromoform ug/L 44.650 89 44-134Bromomethane ug/L 47.350 95 22-181Carbon disulfide ug/L 98.6100 99 59-132Carbon tetrachloride ug/L 45.650 91 56-137Chlorobenzene ug/L 46.050 92 78-123Chloroethane ug/L 50.050 100 60-144Chloroform ug/L 47.150 94 78-126Chloromethane ug/L 40.550 81 42-134cis-1,2-Dichloroethene ug/L 50.550 101 75-122cis-1,3-Dichloropropene ug/L 47.350 95 64-126Dibromochloromethane ug/L 47.250 94 58-128Dibromomethane ug/L 46.850 94 73-125Dichlorodifluoromethane ug/L 42.450 85 35-181Ethyl methacrylate ug/L 192200 96 69-133Ethylbenzene ug/L 46.650 93 66-133Hexachloro-1,3-butadiene ug/L 44.050 88 59-145Iodomethane ug/L 94.5100 94 21-170Isopropylbenzene (Cumene) ug/L 50.050 100 69-124Methyl-tert-butyl ether ug/L 101100 101 69-122Methylene Chloride ug/L 53.150 106 68-132n-Butylbenzene ug/L 46.050 92 70-126n-Hexane ug/L 45.1 N250 90 51-125n-Propylbenzene ug/L 45.550 91 71-122Naphthalene ug/L 40.350 81 68-127





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5086871HK Porter

Parameter UnitsLCS



p-Isopropyltoluene ug/L 49.250 98 72-132sec-Butylbenzene ug/L 46.350 93 70-128Styrene ug/L 49.550 99 74-126tert-Butylbenzene ug/L 41.850 84 51-118Tetrachloroethene ug/L 41.950 84 69-130Toluene ug/L 47.350 95 72-122trans-1,2-Dichloroethene ug/L 50.750 101 72-124trans-1,3-Dichloropropene ug/L 44.850 90 64-121trans-1,4-Dichloro-2-butene ug/L 188200 94 56-133Trichloroethene ug/L 47.350 95 76-126Trichlorofluoromethane ug/L 44.750 89 76-149Vinyl acetate ug/L 220200 110 45-151Vinyl chloride ug/L 45.250 90 59-126Xylene (Total) ug/L 147150 98 70-1244-Bromofluorobenzene (S) %. 104 80-114Dibromofluoromethane (S) %. 103 79-116Toluene-d8 (S) %. 100 81-110

Parameter UnitsMS



MSSpikeResult

5086992001

988305

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1,2-Tetrachloroethane ug/L 50 91 50-13293 3 2050ND 45.6 46.71,1,1-Trichloroethane ug/L 50 100 60-138106 6 2050ND 49.8 52.81,1,2,2-Tetrachloroethane ug/L 50 77 55-12877 1 2050ND 38.7 38.41,1,2-Trichloroethane ug/L 50 94 61-13994 0 2050ND 47.1 47.11,1-Dichloroethane ug/L 50 95 57-14797 2 2050ND 47.7 48.61,1-Dichloroethene ug/L 50 92 55-14592 0 2050ND 45.9 45.81,1-Dichloropropene ug/L 50 109 55-147112 3 2050ND 54.3 55.91,2,3-Trichlorobenzene ug/L 50 78 31-14182 5 2050ND 39.1 40.91,2,3-Trichloropropane ug/L 50 88 58-13389 2 2050ND 43.8 44.61,2,4-Trichlorobenzene ug/L 50 82 25-14386 6 2050ND 40.8 43.21,2,4-Trimethylbenzene ug/L 50 87 18-14989 2 2050ND 43.6 44.71,2-Dibromoethane (EDB) ug/L 50 104 63-129102 2 2050ND 52.0 51.21,2-Dichlorobenzene ug/L 50 85 38-13688 3 2050ND 42.3 43.81,2-Dichloroethane ug/L 50 101 62-138102 1 2050ND 50.5 50.81,2-Dichloropropane ug/L 50 100 59-130105 4 2050ND 50.2 52.31,3,5-Trimethylbenzene ug/L 50 92 20-14793 2 2050ND 45.8 46.61,3-Dichlorobenzene ug/L 50 85 28-14188 4 2050ND 42.3 43.81,3-Dichloropropane ug/L 50 101 62-12799 2 2050ND 50.5 49.61,4-Dichlorobenzene ug/L 50 82 30-13985 3 2050ND 41.1 42.32,2-Dichloropropane ug/L 50 69 37-13973 5 2050ND 34.5 36.42-Butanone (MEK) ug/L 250 88 37-15687 1 20250ND 221 2182-Chlorotoluene ug/L 50 89 27-14291 2 2050ND 44.6 45.32-Hexanone ug/L 250 86 44-14386 1 20250ND 216 2142-Methylnaphthalene ug/L N250 55 24-15162 11 2050ND 27.6 30.94-Chlorotoluene ug/L 50 93 27-14494 1 2050ND 46.5 47.1





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5086871HK Porter

Parameter UnitsMS



MSSpikeResult

5086992001

988305

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

4-Methyl-2-pentanone (MIBK) ug/L 250 90 46-14491 0 20250ND 226 227Acetone ug/L 250 88 39-15683 6 20250ND 237 223Acrolein ug/L 1000 96 33-20090 6 201000ND 963 902Acrylonitrile ug/L 1000 81 48-14980 1 201000ND 808 801Benzene ug/L 50 94 62-12996 1 2050ND 47.1 47.8Bromobenzene ug/L 50 87 39-14089 3 2050ND 43.4 44.5Bromochloromethane ug/L 50 94 49-14297 2 2050ND 47.2 48.3Bromodichloromethane ug/L 50 105 50-142107 3 2050ND 52.3 53.7Bromoform ug/L 50 86 36-12585 1 2050ND 42.9 42.4Bromomethane ug/L 50 113 13-179122 8 2050ND 56.7 61.1Carbon disulfide ug/L 100 103 45-142102 1 20100ND 103 102Carbon tetrachloride ug/L 50 91 46-14296 5 2050ND 45.7 47.9Chlorobenzene ug/L 50 92 49-13694 2 2050ND 46.2 47.1Chloroethane ug/L 50 102 47-160104 2 2050ND 51.1 52.0Chloroform ug/L 50 93 54-15097 4 2050ND 46.5 48.4Chloromethane ug/L 50 80 30-14883 3 2050ND 40.2 41.4cis-1,2-Dichloroethene ug/L 50 98 60-135102 4 2050ND 49.0 51.0cis-1,3-Dichloropropene ug/L 50 89 52-12394 5 2050ND 44.6 47.0Dibromochloromethane ug/L 50 93 48-12594 1 2050ND 46.4 46.8Dibromomethane ug/L 50 94 59-13497 3 2050ND 47.1 48.6Dichlorodifluoromethane ug/L 50 89 24-19792 3 2050ND 44.7 45.9Ethyl methacrylate ug/L 200 93 55-13993 0 20200ND 186 187Ethylbenzene ug/L 50 94 28-15396 2 20508.6 55.8 56.7Hexachloro-1,3-butadiene ug/L 50 84 10-17687 4 2050ND 42.0 43.5Iodomethane ug/L 100 86 17-15788 2 20100ND 86.4 87.8Isopropylbenzene (Cumene) ug/L 50 101 18-152104 2 2050ND 53.6 54.6Methyl-tert-butyl ether ug/L 100 94 63-13096 2 20100ND 93.8 95.6Methylene Chloride ug/L 50 94 45-15696 2 2050ND 47.1 48.0n-Butylbenzene ug/L 50 95 10-161100 5 2050ND 47.7 50.1n-Hexane ug/L N250 112 33-144114 1 2050ND 56.2 56.8n-Propylbenzene ug/L 50 90 16-15090 0 20507.4 52.3 52.5Naphthalene ug/L 50 68 39-14070 2 20504.6 38.8 39.7p-Isopropyltoluene ug/L 50 96 10-163101 5 2050ND 47.8 50.5sec-Butylbenzene ug/L 50 92 10-16095 4 2050ND 46.9 48.7Styrene ug/L 50 102 36-139103 2 2050ND 50.8 51.7tert-Butylbenzene ug/L 50 81 12-13485 5 2050ND 40.5 42.5Tetrachloroethene ug/L 50 85 33-15188 4 2050ND 42.4 44.1Toluene ug/L 50 95 50-13297 2 2050ND 48.0 49.0trans-1,2-Dichloroethene ug/L 50 99 40-153102 3 2050ND 49.7 51.1trans-1,3-Dichloropropene ug/L 50 86 48-12288 3 2050ND 42.8 44.2trans-1,4-Dichloro-2-butene ug/L 200 94 32-13994 0 20200ND 188 188Trichloroethene ug/L 50 96 50-14398 2 2050ND 48.2 49.2Trichlorofluoromethane ug/L 50 95 60-17597 2 2050ND 47.5 48.4Vinyl acetate ug/L 200 94 17-14294 1 20200ND 188 189Vinyl chloride ug/L 50 94 44-14598 3 2050ND 47.1 48.8Xylene (Total) ug/L 150 96 29-145101 5 20150ND 144 1514-Bromofluorobenzene (S) %. 104 80-114101





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5086871HK Porter

Parameter UnitsMS



MSSpikeResult

5086992001

988305

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Dibromofluoromethane (S) %. 105 79-116107Toluene-d8 (S) %. 101 81-110100





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5086871HK Porter



MSV/57668EPA 8260

EPA 82608260 MSV 5035A Volatile Organics

Associated Lab Samples: 5086871001, 5086871002, 5086871003, 5086871004, 5086871016, 5086871017





Matrix: Solid

Analyzed

1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 09/28/13 13:251,1,1-Trichloroethane mg/kg ND 0.0050 09/28/13 13:251,1,2,2-Tetrachloroethane mg/kg ND 0.0050 09/28/13 13:251,1,2-Trichloroethane mg/kg ND 0.0050 09/28/13 13:251,1-Dichloroethane mg/kg ND 0.0050 09/28/13 13:251,1-Dichloroethene mg/kg ND 0.0050 09/28/13 13:251,1-Dichloropropene mg/kg ND 0.0050 09/28/13 13:251,2,3-Trichlorobenzene mg/kg ND 0.0050 09/28/13 13:251,2,3-Trichloropropane mg/kg ND 0.0050 09/28/13 13:251,2,4-Trichlorobenzene mg/kg ND 0.0050 09/28/13 13:251,2,4-Trimethylbenzene mg/kg ND 0.0050 09/28/13 13:251,2-Dibromoethane (EDB) mg/kg ND 0.0050 09/28/13 13:251,2-Dichlorobenzene mg/kg ND 0.0050 09/28/13 13:251,2-Dichloroethane mg/kg ND 0.0050 09/28/13 13:251,2-Dichloropropane mg/kg ND 0.0050 09/28/13 13:251,3,5-Trimethylbenzene mg/kg ND 0.0050 09/28/13 13:251,3-Dichlorobenzene mg/kg ND 0.0050 09/28/13 13:251,3-Dichloropropane mg/kg ND 0.0050 09/28/13 13:251,4-Dichlorobenzene mg/kg ND 0.0050 09/28/13 13:251-Methylnaphthalene mg/kg ND 0.010 N209/28/13 13:252,2-Dichloropropane mg/kg ND 0.0050 09/28/13 13:252-Butanone (MEK) mg/kg ND 0.025 09/28/13 13:252-Chlorotoluene mg/kg ND 0.0050 09/28/13 13:252-Hexanone mg/kg ND 0.10 09/28/13 13:252-Methylnaphthalene mg/kg ND 0.010 N209/28/13 13:254-Chlorotoluene mg/kg ND 0.0050 09/28/13 13:254-Methyl-2-pentanone (MIBK) mg/kg ND 0.025 09/28/13 13:25Acetone mg/kg ND 0.10 09/28/13 13:25Acrolein mg/kg ND 0.10 09/28/13 13:25Acrylonitrile mg/kg ND 0.10 09/28/13 13:25Benzene mg/kg ND 0.0050 09/28/13 13:25Bromobenzene mg/kg ND 0.0050 09/28/13 13:25Bromochloromethane mg/kg ND 0.0050 09/28/13 13:25Bromodichloromethane mg/kg ND 0.0050 09/28/13 13:25Bromoform mg/kg ND 0.0050 09/28/13 13:25Bromomethane mg/kg ND 0.0050 09/28/13 13:25Carbon disulfide mg/kg ND 0.010 09/28/13 13:25Carbon tetrachloride mg/kg ND 0.0050 09/28/13 13:25Chlorobenzene mg/kg ND 0.0050 09/28/13 13:25Chloroethane mg/kg ND 0.0050 09/28/13 13:25Chloroform mg/kg ND 0.0050 09/28/13 13:25Chloromethane mg/kg ND 0.0050 09/28/13 13:25cis-1,2-Dichloroethene mg/kg ND 0.0050 09/28/13 13:25





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Matrix: Solid

Analyzed

cis-1,3-Dichloropropene mg/kg ND 0.0050 09/28/13 13:25Dibromochloromethane mg/kg ND 0.0050 09/28/13 13:25Dibromomethane mg/kg ND 0.0050 09/28/13 13:25Dichlorodifluoromethane mg/kg ND 0.0050 09/28/13 13:25Ethyl methacrylate mg/kg ND 0.10 09/28/13 13:25Ethylbenzene mg/kg ND 0.0050 09/28/13 13:25Hexachloro-1,3-butadiene mg/kg ND 0.0050 09/28/13 13:25Iodomethane mg/kg ND 0.10 09/28/13 13:25Isopropylbenzene (Cumene) mg/kg ND 0.0050 09/28/13 13:25Methyl-tert-butyl ether mg/kg ND 0.0050 09/28/13 13:25Methylene Chloride mg/kg ND 0.020 09/28/13 13:25n-Butylbenzene mg/kg ND 0.0050 09/28/13 13:25n-Hexane mg/kg ND 0.0050 N209/28/13 13:25n-Propylbenzene mg/kg ND 0.0050 09/28/13 13:25Naphthalene mg/kg ND 0.0050 09/28/13 13:25p-Isopropyltoluene mg/kg ND 0.0050 09/28/13 13:25sec-Butylbenzene mg/kg ND 0.0050 09/28/13 13:25Styrene mg/kg ND 0.0050 09/28/13 13:25tert-Butylbenzene mg/kg ND 0.0050 09/28/13 13:25Tetrachloroethene mg/kg ND 0.0050 09/28/13 13:25Toluene mg/kg ND 0.0050 09/28/13 13:25trans-1,2-Dichloroethene mg/kg ND 0.0050 09/28/13 13:25trans-1,3-Dichloropropene mg/kg ND 0.0050 09/28/13 13:25trans-1,4-Dichloro-2-butene mg/kg ND 0.10 09/28/13 13:25Trichloroethene mg/kg ND 0.0050 09/28/13 13:25Trichlorofluoromethane mg/kg ND 0.0050 09/28/13 13:25Vinyl acetate mg/kg ND 0.10 09/28/13 13:25Vinyl chloride mg/kg ND 0.0050 09/28/13 13:25Xylene (Total) mg/kg ND 0.010 09/28/13 13:254-Bromofluorobenzene (S) %. 98 56-144 09/28/13 13:25Dibromofluoromethane (S) %. 94 85-118 09/28/13 13:25Toluene-d8 (S) %. 97 71-128 09/28/13 13:25

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane mg/kg 0.043.05 87 62-1231,1,1-Trichloroethane mg/kg 0.041.05 82 70-1231,1,2,2-Tetrachloroethane mg/kg 0.044.05 88 65-1241,1,2-Trichloroethane mg/kg 0.050.05 100 74-1291,1-Dichloroethane mg/kg 0.046.05 93 73-1301,1-Dichloroethene mg/kg 0.053.05 106 66-1261,1-Dichloropropene mg/kg 0.052.05 104 78-1251,2,3-Trichlorobenzene mg/kg 0.043.05 85 66-1311,2,3-Trichloropropane mg/kg 0.052.05 103 44-157





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Parameter UnitsLCS



1,2,4-Trichlorobenzene mg/kg 0.040.05 80 68-1291,2,4-Trimethylbenzene mg/kg 0.047.05 94 67-1261,2-Dibromoethane (EDB) mg/kg 0.053.05 105 74-1201,2-Dichlorobenzene mg/kg 0.046.05 93 73-1221,2-Dichloroethane mg/kg 0.048.05 96 73-1271,2-Dichloropropane mg/kg 0.052.05 105 75-1181,3,5-Trimethylbenzene mg/kg 0.046.05 93 65-1271,3-Dichlorobenzene mg/kg 0.044.05 89 73-1211,3-Dichloropropane mg/kg 0.053.05 106 72-1211,4-Dichlorobenzene mg/kg 0.046.05 93 75-1192,2-Dichloropropane mg/kg 0.042.05 84 63-1222-Butanone (MEK) mg/kg 0.27.25 108 59-1392-Chlorotoluene mg/kg 0.048.05 95 72-1212-Hexanone mg/kg 0.25.25 100 56-1392-Methylnaphthalene mg/kg 0.042 N2.05 83 63-1484-Chlorotoluene mg/kg 0.047.05 95 75-1234-Methyl-2-pentanone (MIBK) mg/kg 0.26.25 104 63-136Acetone mg/kg 0.26.25 105 46-156Acrolein mg/kg 1.31 126 47-200Acrylonitrile mg/kg 1.11 110 67-130Benzene mg/kg 0.052.05 104 74-119Bromobenzene mg/kg 0.049.05 99 69-129Bromochloromethane mg/kg 0.052.05 103 67-129Bromodichloromethane mg/kg 0.042.05 85 68-121Bromoform mg/kg 0.044.05 88 49-124Bromomethane mg/kg 0.055.05 111 44-142Carbon disulfide mg/kg 0.099.1 99 61-129Carbon tetrachloride mg/kg 0.041.05 83 58-127Chlorobenzene mg/kg 0.048.05 96 77-122Chloroethane mg/kg 0.059.05 118 59-141Chloroform mg/kg 0.047.05 95 75-124Chloromethane mg/kg 0.046.05 92 46-133cis-1,2-Dichloroethene mg/kg 0.050.05 99 72-122cis-1,3-Dichloropropene mg/kg 0.050.05 100 68-115Dibromochloromethane mg/kg 0.046.05 91 60-121Dibromomethane mg/kg 0.045.05 90 72-124Dichlorodifluoromethane mg/kg 0.033.05 67 26-186Ethyl methacrylate mg/kg 0.21.2 103 63-130Ethylbenzene mg/kg 0.049.05 99 72-123Hexachloro-1,3-butadiene mg/kg 0.042.05 84 55-139Iodomethane mg/kg 0.10.1 103 38-149Isopropylbenzene (Cumene) mg/kg 0.049.05 98 65-123Methyl-tert-butyl ether mg/kg 0.11.1 106 68-120Methylene Chloride mg/kg 0.061.05 123 57-142n-Butylbenzene mg/kg 0.044.05 87 68-125n-Hexane mg/kg 0.052 N2.05 104 57-117n-Propylbenzene mg/kg 0.049.05 98 68-122Naphthalene mg/kg 0.047.05 93 67-131





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Parameter UnitsLCS



p-Isopropyltoluene mg/kg 0.046.05 92 66-133sec-Butylbenzene mg/kg 0.049.05 98 64-131Styrene mg/kg 0.047.05 94 70-126tert-Butylbenzene mg/kg 0.045.05 90 46-124Tetrachloroethene mg/kg 0.040.05 80 72-126Toluene mg/kg 0.049.05 98 71-121trans-1,2-Dichloroethene mg/kg 0.047.05 95 69-123trans-1,3-Dichloropropene mg/kg 0.049.05 97 66-114trans-1,4-Dichloro-2-butene mg/kg 0.18.2 89 61-124Trichloroethene mg/kg 0.046.05 91 74-123Trichlorofluoromethane mg/kg 0.044.05 88 72-146Vinyl acetate mg/kg 0.21.2 106 57-131Vinyl chloride mg/kg 0.054.05 109 55-128Xylene (Total) mg/kg 0.15.15 103 66-1244-Bromofluorobenzene (S) %. 112 56-144Dibromofluoromethane (S) %. 96 85-118Toluene-d8 (S) %. 95 71-128





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OEXT/33896EPA 3546

EPA 82708270 Solid MSSV Microwave Short Spike

Associated Lab Samples: 5086871014





Matrix: Solid

Analyzed

1-Methylnaphthalene mg/kg ND 0.33 N209/19/13 16:592,4,5-Trichlorophenol mg/kg ND 0.33 09/19/13 16:592,4,6-Trichlorophenol mg/kg ND 0.33 09/19/13 16:592,4-Dichlorophenol mg/kg ND 0.33 09/19/13 16:592,4-Dimethylphenol mg/kg ND 0.33 09/19/13 16:592,4-Dinitrophenol mg/kg ND 1.6 09/19/13 16:592,4-Dinitrotoluene mg/kg ND 0.33 09/19/13 16:592,6-Dinitrotoluene mg/kg ND 0.33 09/19/13 16:592-Chloronaphthalene mg/kg ND 0.33 09/19/13 16:592-Chlorophenol mg/kg ND 0.33 09/19/13 16:592-Methylnaphthalene mg/kg ND 0.33 09/19/13 16:592-Methylphenol(o-Cresol) mg/kg ND 0.33 09/19/13 16:592-Nitroaniline mg/kg ND 1.6 09/19/13 16:592-Nitrophenol mg/kg ND 0.33 09/19/13 16:593&4-Methylphenol(m&p Cresol) mg/kg ND 0.66 09/19/13 16:593,3'-Dichlorobenzidine mg/kg ND 0.66 09/19/13 16:593-Nitroaniline mg/kg ND 1.6 09/19/13 16:594,6-Dinitro-2-methylphenol mg/kg ND 1.6 09/19/13 16:594-Bromophenylphenyl ether mg/kg ND 0.33 09/19/13 16:594-Chloro-3-methylphenol mg/kg ND 0.66 09/19/13 16:594-Chloroaniline mg/kg ND 0.66 09/19/13 16:594-Chlorophenylphenyl ether mg/kg ND 0.33 09/19/13 16:594-Nitroaniline mg/kg ND 1.6 09/19/13 16:594-Nitrophenol mg/kg ND 1.6 09/19/13 16:59Acenaphthene mg/kg ND 0.33 09/19/13 16:59Acenaphthylene mg/kg ND 0.33 09/19/13 16:59Anthracene mg/kg ND 0.33 09/19/13 16:59Benzo(a)anthracene mg/kg ND 0.33 09/19/13 16:59Benzo(a)pyrene mg/kg ND 0.17 09/19/13 16:59Benzo(b)fluoranthene mg/kg ND 0.33 09/19/13 16:59Benzo(g,h,i)perylene mg/kg ND 0.33 09/19/13 16:59Benzo(k)fluoranthene mg/kg ND 0.33 09/19/13 16:59Benzyl alcohol mg/kg ND 0.66 09/19/13 16:59bis(2-Chloroethoxy)methane mg/kg ND 0.33 09/19/13 16:59bis(2-Chloroethyl) ether mg/kg ND 0.33 09/19/13 16:59bis(2-Chloroisopropyl) ether mg/kg ND 0.33 09/19/13 16:59bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 09/19/13 16:59bis(2chloro1methylethyl) ether mg/kg ND 0.33 09/19/13 16:59Butylbenzylphthalate mg/kg ND 0.33 09/19/13 16:59Chrysene mg/kg ND 0.33 09/19/13 16:59Di-n-butylphthalate mg/kg ND 0.33 09/19/13 16:59Di-n-octylphthalate mg/kg ND 0.33 09/19/13 16:59Dibenz(a,h)anthracene mg/kg ND 0.17 09/19/13 16:59





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Matrix: Solid

Analyzed

Dibenzofuran mg/kg ND 0.33 09/19/13 16:59Diethylphthalate mg/kg ND 0.33 09/19/13 16:59Dimethylphthalate mg/kg ND 0.33 09/19/13 16:59Fluoranthene mg/kg ND 0.33 09/19/13 16:59Fluorene mg/kg ND 0.33 09/19/13 16:59Hexachloro-1,3-butadiene mg/kg ND 0.33 09/19/13 16:59Hexachlorobenzene mg/kg ND 0.33 09/19/13 16:59Hexachlorocyclopentadiene mg/kg ND 0.33 09/19/13 16:59Hexachloroethane mg/kg ND 0.33 09/19/13 16:59Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 09/19/13 16:59Isophorone mg/kg ND 0.33 09/19/13 16:59N-Nitroso-di-n-propylamine mg/kg ND 0.33 09/19/13 16:59N-Nitrosodiphenylamine mg/kg ND 0.33 09/19/13 16:59Naphthalene mg/kg ND 0.33 09/19/13 16:59Nitrobenzene mg/kg ND 0.33 09/19/13 16:59Pentachlorophenol mg/kg ND 1.6 09/19/13 16:59Phenanthrene mg/kg ND 0.33 09/19/13 16:59Phenol mg/kg ND 0.33 09/19/13 16:59Pyrene mg/kg ND 0.33 09/19/13 16:592,4,6-Tribromophenol (S) %. 82 16-122 09/19/13 16:592-Fluorobiphenyl (S) %. 77 31-94 09/19/13 16:592-Fluorophenol (S) %. 89 24-104 09/19/13 16:59Nitrobenzene-d5 (S) %. 72 28-101 09/19/13 16:59p-Terphenyl-d14 (S) %. 91 26-110 09/19/13 16:59Phenol-d5 (S) %. 80 28-101 09/19/13 16:59

Parameter UnitsLCS



2,4-Dinitrotoluene mg/kg 2.73.3 81 39-1032-Chlorophenol mg/kg 2.43.3 72 38-962-Methylnaphthalene mg/kg 2.93.3 87 36-944-Chloro-3-methylphenol mg/kg 2.43.3 71 38-1044-Nitrophenol mg/kg 2.73.3 80 34-104Acenaphthene mg/kg 2.43.3 73 43-99Acenaphthylene mg/kg 2.63.3 77 42-101Anthracene mg/kg 2.73.3 81 46-107Benzo(a)anthracene mg/kg 2.93.3 87 45-108Benzo(a)pyrene mg/kg 2.83.3 84 47-113Benzo(b)fluoranthene mg/kg 3.13.3 92 41-110Benzo(g,h,i)perylene mg/kg 2.33.3 68 42-112Benzo(k)fluoranthene mg/kg 2.73.3 81 44-107Chrysene mg/kg 2.83.3 84 43-103Dibenz(a,h)anthracene mg/kg 2.43.3 73 43-110Fluoranthene mg/kg 2.83.3 83 45-105





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Parameter UnitsLCS



Fluorene mg/kg 2.63.3 79 42-103Indeno(1,2,3-cd)pyrene mg/kg 2.43.3 71 43-111N-Nitroso-di-n-propylamine mg/kg 2.23.3 67 37-96Naphthalene mg/kg 2.43.3 71 44-100Pentachlorophenol mg/kg 2.33.3 68 21-103Phenanthrene mg/kg 2.73.3 80 44-104Phenol mg/kg 2.63.3 79 37-101Pyrene mg/kg 2.83.3 85 44-1052,4,6-Tribromophenol (S) %. 82 16-1222-Fluorobiphenyl (S) %. 76 31-942-Fluorophenol (S) %. 87 24-104Nitrobenzene-d5 (S) %. 72 28-101p-Terphenyl-d14 (S) %. 97 26-110Phenol-d5 (S) %. 82 28-101

Parameter UnitsMS



MSSpikeResult

5086829004

981395

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2,4-Dinitrotoluene mg/kg 3.9 79 15-10278 1 203.9ND 3.1 3.12-Chlorophenol mg/kg 3.9 68 22-9672 6 203.9ND 2.7 2.82-Methylnaphthalene mg/kg 3.9 79 14-10785 8 203.9ND 3.1 3.44-Chloro-3-methylphenol mg/kg 3.9 69 21-10570 3 203.9ND 2.7 2.84-Nitrophenol mg/kg 3.9 73 12-10771 3 203.9ND 2.9 2.8Acenaphthene mg/kg 3.9 70 19-11070 0 203.9ND 2.7 2.7Acenaphthylene mg/kg 3.9 75 21-10675 1 203.9ND 2.9 3.0Anthracene mg/kg 3.9 76 22-11274 3 203.9ND 3.0 2.9Benzo(a)anthracene mg/kg 3.9 76 13-11672 5 203.9ND 3.0 2.9Benzo(a)pyrene mg/kg 3.9 72 11-11970 1 203.9ND 2.8 2.8Benzo(b)fluoranthene mg/kg 3.9 77 10-12666 15 203.9ND 3.0 2.6Benzo(g,h,i)perylene mg/kg 3.9 59 10-11459 0 203.9ND 2.3 2.3Benzo(k)fluoranthene mg/kg 3.9 70 10-11772 3 203.9ND 2.7 2.8Chrysene mg/kg 3.9 73 14-10769 6 203.9ND 2.9 2.7Dibenz(a,h)anthracene mg/kg 3.9 64 10-11963 1 203.9ND 2.5 2.5Fluoranthene mg/kg 3.9 69 17-11065 7 203.9ND 2.7 2.6Fluorene mg/kg 3.9 75 17-11574 2 203.9ND 3.0 2.9Indeno(1,2,3-cd)pyrene mg/kg 3.9 61 11-11160 2 203.9ND 2.4 2.4N-Nitroso-di-n-propylamine mg/kg 3.9 63 18-10365 4 203.9ND 2.5 2.6Naphthalene mg/kg 3.9 68 16-10273 7 203.9ND 2.7 2.9Pentachlorophenol mg/kg 3.9 72 10-10064 11 203.9ND 2.8 2.5Phenanthrene mg/kg 3.9 76 10-12875 1 203.9ND 3.0 3.0Phenol mg/kg 3.9 72 22-9776 7 203.9ND 2.8 3.0Pyrene mg/kg 3.9 70 10-12364 8 203.9ND 2.7 2.52,4,6-Tribromophenol (S) %. 85 16-122832-Fluorobiphenyl (S) %. 73 31-94732-Fluorophenol (S) %. 84 24-10488Nitrobenzene-d5 (S) %. 69 26-9874





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Parameter UnitsMS



MSSpikeResult

5086829004

981395

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

p-Terphenyl-d14 (S) %. 77 26-11069Phenol-d5 (S) %. 74 28-10177





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PMST/8750ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture


Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

5087065001983089SAMPLE DUPLICATE:

Percent Moisture % 14.8 R19 516.2

Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

5086841006983090SAMPLE DUPLICATE:

Percent Moisture % 9.9 R113 511.2





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#=QL#

QUALIFIERS


5086871HK Porter

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PRL - Pace Reporting Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - IndianapolisPASI-I

ANALYTE QUALIFIERS

Compound ND at an estimated RL of 180 ug/L, based on the MDL and DF. AMV 9/30/131dCompound ND at an estimated RL of 34 ug/L, based on the MDL and DF. AMV 9/30/132dDue to the viscosity of the extract, it was run at 5x. KES 9-25-133dSample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3Sample was diluted due to the presence of high levels of target analytes.D4The lab does not hold TNI accreditation for this parameter.N2RPD value was outside control limits.R1Surrogate recovery not evaluated against control limits due to sample dilution.S4Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5





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#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE


5086871HK Porter

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

5086871001 MPRP/12095 ICP/13248SB1(0-2) EPA 3050 EPA 60105086871002 MPRP/12095 ICP/13248SB2(5.5-6.5) EPA 3050 EPA 60105086871003 MPRP/12095 ICP/13248DUP01 Soil EPA 3050 EPA 60105086871004 MPRP/12095 ICP/13248SB3-S(8.0-8.5) EPA 3050 EPA 6010

5086871011 MPRP/12082 ICP/13223DUP01 GW EPA 3010 EPA 60105086871012 MPRP/12082 ICP/13223SB2 GW EPA 3010 EPA 60105086871013 MPRP/12082 ICP/13223SB3 GW EPA 3010 EPA 6010

5086871014 OEXT/33896 MSSV/13484AST (Surface) EPA 3546 EPA 8270

5086871011 MSV/57659DUP01 GW EPA 82605086871012 MSV/57659SB2 GW EPA 82605086871013 MSV/57659SB3 GW EPA 82605086871015 MSV/57659Trip Blank Water EPA 8260

5086871001 MSV/57668SB1(0-2) EPA 82605086871002 MSV/57668SB2(5.5-6.5) EPA 82605086871003 MSV/57668DUP01 Soil EPA 82605086871004 MSV/57668SB3-S(8.0-8.5) EPA 82605086871016 MSV/57668Trip Blank Soil EPA 82605086871017 MSV/57668SB2 A EPA 8260

5086871001 PMST/8750SB1(0-2) ASTM D2974-875086871002 PMST/8750SB2(5.5-6.5) ASTM D2974-875086871003 PMST/8750DUP01 Soil ASTM D2974-875086871004 PMST/8750SB3-S(8.0-8.5) ASTM D2974-875086871014 PMST/8750AST (Surface) ASTM D2974-875086871017 PMST/8750SB2 A ASTM D2974-87





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J ~ii~~~~===Em=ct::r==r=u=r•il:--=rmtrm: ... - i-~ - -IJ-.

__ -_~A"f'!ic_ "-· tlMe . A~!§~~-~1 -· ~-~~li-- ·TlM~- SAMPl.ECONDmoNs"'" oi5 ~'l~~'~ .• -·- -- 1- - - ~i · 1~0 I-.- r-- r .. Jl I - . . -vi- - ,- - ,- - I -,. -- 1 - T.· --'01!'-i -1':'~~- ~\ALt....-~ __ __ _ - ~.,..-._.,__~- __ __ ~- __j__?.o:t4_t _· -~---=----l'_j__ ~-- . - _.I . - _ J,~ "·r '!l''_.-.0:-. v-~- >' - - - ...._

. ~

.. . ~~ -~- - - ~ I ()~5 1 ?i.. '/ N '/'

ORIGINAL '$1:MP~e::~~:~:~:~:6 ___ - ~ _ -·-··· _ _ _ _ _ -~ · ~ j [ f ~ ~ I~

SIGNATU~ of SAMPLE~tJJ///(J ~;~:~ec: £18 .. 1\a I~ l I~ 8 l ~ l •important Note: By ~gnlng thls form you are accepUng Paoe's NET 30 day payment terms and agreeing to late charges of 1.5% per m{nth r/r any Invoices nOt paid within 30 days.

., . , F-ALL-Q..020rev.07, 15-May-2007

of 49

/' __ ..... aceAnaJyt/cat Client Name: _.._.S ....... M~e,-""------f

Courlerfred Ex 0 UPS 0 USPS 0 Client Cbommercial Oace other

Tracking#: $930 (?q3&"" 3-::rio ..,,/ Custody Seal on Cooler/Box Present: 0 yes p no Seals intact: 0 yes

Packing Material: O Bubble Wrap )ZfBubble Bags [}Jone -»Other

Thermometer Used 1 2 3 4 6 A B c{g)E Type of Ice: ~ Blue None

Cooler Temperature (. ic,.. Ice Visible In Sample Containers: (Corrected, If applicable)

Temp should be above freezing to a~c

Chain of Custod Present:

Chain of Custody Filled Out:

Chain of Custody Relin uished:

Sampler Name & Signature on COC:

Short Hold Time Analysis (<72hr :

Rush Turn Around Time Requested:

Containers Intact:

Sample Labels match COC:

-Includes date/time/ID/Analysis All containers needing acid/base pres. have been checked?

exceptions: ~lform, TOC, O&G

All containers needing preservation are found to be in compliance with EPA recommendation.

Comments:

ONo ON/A 1.

ONo ON/A 2.

ONo ON/A 3,

ON/A 4.

ON/A 5.

ON/A 6.

fos ONo

DYes~ ON/A

Project # _ _....STJf~· _la_rf7_· _l _

0 no Date/Time 5035A kits placed In )Ji: oq 1"312.> tO?k

0 Samples on ice, cooling process has begun

Dyes

Heads ace in VOA Vials ( >6mm): ONo ON/A 10. \GW t) l)

Trip Blank Present: ONo ON/A 11.

Samples Arrived within Hold Time: DYes ONo ON/A 12.

Sufficient Volume: DYes ONo ON/A 13.

Correct Containers Used: DYes ONo ON/A 14.

Client Notification/ Resolution: c rt~ J~'IAJ Datemme: Person Contacted:

Field Data Required? Y I N

Comments/ Resolution:

Project Manager Review:

Form F-IN-0290-rev.04, 28Apr2011

•.

\/LA-t~)

of 49

Sample Container Count /2.Analyticaf ( __,,,,,-~" -~ CLIENT: ' ~Mt-i I

COC PAGE :. t of 1.-COC ID# 1i0fb 6Qf2- Project # Sb 'rfJ r 1 ( Sample line

Item DG9H AG1U WGFU AGOU R 4/6 BP2N BP2U BP2S BP3N BP3U BP3S AG3S AG1H Comments

1 t 4 2 \ 4-3 \ 4· 4 \ k 5 I 6 \ 7 I 8 I 9 I 10 I 11 -; I -· 12 8 (

Container Codes

DG9H 40ml HCL amber voa vial AGOU 1 OOmL unpreserv.ed amber glass BP1N 1 liter HN03 .Plastic DG9P 40ml TSP amber vial

AG1U 1 liter unpreserved amber glass AG1H 1 liter HCL amber glass BP1S 1 liter H2S04 plastic DG9S 40ml H2S04.ambervial

WGFU 4oz clear soil iar AG1S 1 liter H2S04 amber glass BP1U 1 liter unpreserved plastic DG9T 40ml Na Thio amber vial

R terra ·core kit AG1T 1 liter Na Thlosulfate amber al BP1Z 1 liter NaOH, Zn, Ac DG9U 40ml unpreserved amber vial -BP2N 500ml HN03 plastic AG2N 500ml HN03 amber glasS BP2A 500ml NaOH, Ase Acid plastic I Wipe/Swab

BP2U 500ml unpreserved plastic AG2S ~· ·--· 500ml H2S04 amber glass BP20 500ml NaOH plastic JGFU 4oz unpreserved amber wide

BP2S 500mL H2S04 plastic AG2U 500ml unpreserved ~mber gla BP2Z 500ml NaOH, Zn Ac U SummaCan --·

BP3N 250ml HN03 plastic AG3U 250ml unpreserved amber gla AF Air Filter VG9H 40ml HCL clear vial ·-

BP3U 250ml unpreserved Piasti.£__ . . . . _ BG1H 1 liter HCL clear alass BP3C 250ml NaOH plastic VG9T 40ml Na Thio. clear vial ---· BP3S 250ml H2S04 plastic BG1S 1 liter H2S04 clear glass BP3Z 250ml NaOH, Zn Ac plastic VG9U 40ml unpreserved clear vial

I-· ........ 4 ••

AG3S 250ml H2S04 glass amb~r--··-- BG1T 1 liter Na Thiosulfate clear ala t---

c Air Cassettes VSG Headspace septa vial & HCL

AG1S 1 liter H2S04 amber glass BG1U 1 liter unpreserved glass DG9B 40ml Na Bisulfate amber vial WGFX 4oz wide jar w/hexane wipe -- 1--• ·-BP1U 1 liter unpreserved Plastic BP1A 1 liter NaOH, Ase Acid Plastic DG9M 40ml MeOH clear vial ZPLC ZiPloc Baa

F-IN-Q-270-rev.02,19Apr2012

of 49

I !

I I

Sample Container Count

CLIENT:; 8M~ COC PAGE '2- of 1/-COC ID# ! - Project# $)d}f£}-J ( Sample line

Item DG9H AG1 U WGFU AGOU R 4 / 6 BP2N BP2U BP2S BP3N BP3U BP3S AG3S AG1 H

1 3 \ 2 I 3 ~ 4 '

' 3

5 4 6

7

8

9

10

11

12

Container Codes

DG9H 40mL HCL amber voa vial AGOU 1 OOmL unpreserved amber glass BP1N 1 liter l-:f N03 plastic AG1U 1 liter unpreserved amber alass AG1H 1 liter HCL amber glass BP1S 1 liter H2S04 olastic

WGFU 4oz clear soil jar AG1S 1 liter H2S04 amber glass BP1U 1 liter unpreserved plastic R terra ·core kit AG1T 1 liter Na Thiosulfate amber gl BP1Z 1 liter NaOH, Zn, Ac

BP2N 1 500mL HN03 plastic AG2N 500mL HN03 amber glass BP2A 500mL NaOH, Ase Acid plastic BP2U ! 500mL unpreserved plastic AG2S 500mL H2S04 amber glass BP20 500mL NaOH plastic BP2S · 500mt. H2S04 plastic AG2U 500mL unpreserved amber gla BP2Z 500mL NaOH, Zn Ac BP3N 250mL HN03 plastic AG3U 250mL unpreserved amber gla AF Air Filter -BP3U 250mL unpreserved plastic BG1H 1 liter HCL cleat glass BP3C 250mL NaOH plastic ·-· BP3S 250mL H2S04 plastic · BG1S 1 liter H2S04 clear glass BP3Z 250mL NaOH, Zn Ac plastic --· -~-AG3S 250mL H2S04 glass amber BG1T 1 liter Na Thiosulfate clear gla C Air Cassettes AG1S 1 liter H2S04 amber glass BG1U 1 liter unpreserved glass DG9B 40mL Na Bisulfate amber vial -BP1U 1 liter unoreserved plastic BP1A 1 liter NaOH, Ase Acid plastic DG9M 40mL MeOH clear vial

F-IN-Q-270-rev.02, 19Apr2012

/2.Ana/ylk;al. r~al.N-~ .....

Comments

l-!1J) "'KvrJ ~IA,1',/v <&v ~ b~~ " 0S2-A

• 5PJ-~ -ft

f/7)(.;) (J't/lr;.,"' (c\ .

DG9P 40mL TSP amber vial

DG9S 40mL H2S04 amber vial

DG9T 40mL Na Thio amber vial

DG9U 40mL unpreserved amber vial

I Wipe/Swab

JGFU 4oz unpreserved amber wide

U SummaCan

VG9H 40mL HCL clear vial

VG9T 40mL Na Thio. clear vial --VG9U 40mL unpreserved clear vial ·-

VSG Headspace septa vial & HCL

W.GFX 4oz wide jar w/hexane wipe --~-

ZPLC Ziploc Baa

sme report of limited phase ii environmental site … · limited phase ii environmental site...

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