sdms document anson environmental · anson environmental sdms document 112048 i eninronmenud audits...

Anson Environmental

SDMS Document

112048

I EninronmenUd Audits Hazardous Waste Asbestos Management GrounduxUer Remediation Storage Tank Management Impact Statements Wetlarui Investigations

256 Main Street Northport, NY 11768

516-757-7090 (fax) 516-757-1229

February 4, 1992:

Dorothy Allen, Project Manager United States Environmental Protection Agency, Region II 26 Federal Plaza New York, NY 10278

Re: Administrative Order Index No. II CERCLA-90208 Anchor Chemical Site 500 West John Street, Hicksville, NY

Dear Mrs. Allen:

Enclosed please find copies of the data sheets for the samples taken to date at the above referenced Site. The data for the original sampling of the nine drywells and catch basin and indoor borings 5 & 6 and the re-sampling of drywells 1-4 for mercury and cyanide have been validated and are presented in the validated format from Environmental Standards Inc.

The unvalidated data for the monitoring wells 1D, 4 and 6 and indoor borings 3 & 4 are enclosed from both CEIMIC (inorganics) and Intech Biolabs (organics). The unvalidated data for indoor borings 1 & 2 and the re-sampling of the remaining drywells from CEIMIC Labs is also enclosed. The organic data for the last two borings has not yet been received from Intech Biolabs but we understand it will be available shortly.

We trust this is satisfactory for your purposes, to call.

If you have any questions, please do not hesitate

Very truly yours.

Dean Anson II Co-Facility Coordinator

cc: Richard G. Leiand, Esq. Mr. Arthur D. Sanders

w/out enclosures:

--•• W Printed on

rtecycled Paper

Stanley Sucharski, BB&L Fred Werfel, Spiegel Associates James Doyle, Esq., USEPA Doug Sullivan, Alliance Technologies

300322

m

Validated Data

All Drywells (f irst sampling)

300323

lEXTIIttTttU ODSIMIC MtlYSIS - AMUTICUL liESUlTS

1 • •

lAnseo Envirtmental Saipl i Nuiber

1 llaboratory Saif i l i nuiber

| - • " " • • " " "

1 jReiarks 1 I " • lunits I 1 , - -f

JSEIIIVOIATIIE COKPOUIIDS j Quant.

1 l l i i i t (»q) 1 1

iPhenol 1 11 1 1 1 " - • - • 1 • |bis(2-ChloroeUiyl)ether | I i

|2-Chlcr»|)benol | 11

1 . . . . . -|— |l,3-I)lchlorolienzene | 11 1 . . ,, , t 1 1 |l,l-Dicblorobenzent | 11 1 . , , ., . 1 1 1 lienzyi Alcohol j 11

1 • • 1 |l,2-Dichlorobenzene | I i 1 1 1 1 iH i tdy lpheno l | I i 1 1 1 1 |bis(2-Chloroito|iro|irl)<th«r | I i 1 ) 1 . . . . . . 1 M-Aethylphenol | I t 1 , , . . , 1 1 1 iM l t roso - i f i -n -Propy ls i i n j | I t 1 1 1 • • • 1 iHexachlorcethane | I t

1 1 • •" imt rob inz in i | I t

jlsophorone | I t

r ' 1' |2-«itrophenol j I t 1 , ., , 1 1 1 |2,4-01ieClirlplienol j - I i 1 1 1 1 iBenzoic Acid | Si 1 . . 1 1 — . . 1 — |bi$(2-Cliloroethoxy)ntbane | 11 1 1 1 - " - ~ | -|2,A-01chlorophenol | I t

<JJ)* 11,2,4-Trichlorobenzene | I t ^ 1 1 J ^ . y._ Itaphthalioe j I t

^ O H-Chloroaniline j I t « l i 1 1

iHtxachlorobutadiene It

|4-thli)rs-3-llethylplienol | I t

Quant, l l i i t (Sol)

33i

33t

33i

33t

33i

331

33t

33i

331

33t

331

331

33i

33i

33i

33t

KSt

33i

33t

33t

331

33t

33i

33t

...

- A l l SOIIDS AEPORTED Oil A DRT HEIGHT BASIS ^ ^ ' - ' I i i i I i t

I I I I ^ 1 I I 1 1 I ' I 1 1 P m z 1 outs 1 DUt4 1 Trip Blank | OUtl | M i \ OUfS j OUiT | 0UI8 | 0UI9 | ORAII | 16-1 |Trip Blank j mutS/MSO |

I I 1 Bit 1 i 1 1 1 I I I 1 811 j j 8t9S-i l 1 8I9S-I2 I 8i9S-i3 j 8t9S-l< | 81t3- l l j 81i3-t2 J81i3-I3 | 8113-iA j 81i3-iS j 81i3-t t JBliS-iT | 8 i t 3 - l t j 81 t3 - l l j 81t3-t8 j

Analyzed | Analyzed j Analyzed j j Analyzed j Analyzed j | | Analyzed | | | j JDupllcate of j

Twice 1 Twice j Twice j | Twice j Twice | j ~ j Twice j | j j | OUtl |

U9/Kg 1 u j / rg | u j / t g j ug/l | u j / l g j ug/lg j uj/ l lg j ug/Kg j ug/tg j ug/Kg | ug/rg j ug/l | ug/ l | ug/Kg |

1 1 i 1 1 1 1 1 1 1 1 1 1 Analyzed j

1 j 1 1 j 1 1 j 1 1 1 1 1 Twice 1

1 1 1 KA 1 1 I I 1 I I I 1 tt 1 1

1 1 1 «• 1 1 I I 1 I I I i K* 1 1

1 1 1 M 1 1 I I 1 I I I 1 M 1 1

1 1 1 ** 1 1 I I 1 i l l 1 1* i 1

i i i Kl i i i i i i i i i >* i i

1 1 1 K* 1 1 I I 1 I I I 1 KA 1 1

i i i <• i i i i i i i i i 1* i i

i i 1 ** i i i i i i i i i "* i 1

1 1 1 DA 1 I I I 1 I I I 1 *• 1 1

1 1 1 1* 1 1 I I 1 I I I 1 Kt 1 1

i 1 1 M 1 lU/DJ 1 I I 1 I I I 1 M 1 lU/UJ 1

1 1 1 AA 1 1 I I 1 1 1 1 1 "* 1 1

1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1

1 1 1 AA 1 1 I I 1 1 1 1 1 KA 1 1

1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1

1 1 1 1* 1 1 I I 1 I I I 1 KA 1 1

1 . 1 1 DO 1 1 " Wi J 1 1 1 I I I 1 KA 1 1

1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1

1 1 1 KA 1 1 I I 1 I I I i KA 1 1

1 1 1 KA 1 UJ/U3 1 I I 1 I I I 1 K« 1 II3/U] 1

9Bti/95ii 1 i I KA i 1 1 i i i i i i KA 1 |

1 1 1 KA 1 1 I I 1 1 1 1 1 KA 1 1

1 KA 1 1 KA 1

1 1 1 ll« 1 1 I I 1 I I I 1 KA 1 1

<«a*/^A«i 1 1 1 NK 1 t I I 1 I I I 1 NA 1 t

CO o o

E X T ^ ^ P o R G A A l t AKAlTiilS - 'AJiALmlAI. KtSlilTS

lAnson Environiental Saiple Kuiber

1 llaboratory Saiple Kuiber

1 iBeiarks

1 Units | . . . 1

ISEKIVOIATIIE COKPOUKOS

1 1

1Hexachlorocyclopentadisne 1

|2,l,e-Tricliloropbei)ol

|2,<l,S-Trichlorophenol 1 1 |2-Chioronaphthalene

1 |2-Kitroaniline i lOiiethylphthalate

lAcenaphttiylene

is-Kitroanil ine 1 1 lAcenaphthene 1 1 |2,4-0initrophenol

I " |4-Kitrophenol 1 1 lOlbenzofuran I 1 |2,4-Oinitrctoluene

|2,6-Dinitrotoluene

1 lOiethylplithalate 1 1 14-Chlorophenylphenylether I " •

iFluorene

1 • • •

|4-Kitroanll lne

1 • — •

|4,6-0initro-2-Ketbyiphenoi

1 -K-Kitrosodiphenylaiine

|4-Broiophenylphenylether

iHexachlorobenzene 1 . . -1 iPentachlorophenoi

1 iPhenanthrene 1

Quant, l i i i t (Aq)

It '

It

Si

It

St

It

It

St

It

Si

Si

It

It

It

It

It

It

Si

St

It

It

It

Si

It

Ouant. l i i i t (Sol)

33i

33i

ISSi

33t

ust

33i

33t

i t s t

33i

isst

16Si

33t

33i

33i

33t

33i

33i

les i

16St

33t

33i

33i

les i

33t

' A l l Su'lIOS

0UI2

8t95-t l

Analyzed Twice

^ l ^

t l -

371 J/32t J

EPOBTED O'K A OBT'UElbHl'BASIS '

0UI3 i 0Ut4 i Trip Blank

i i 811 Bt9S-t2 1 8t9S-t3 | 889S-t4

Analyzed | Analyzed | Twice j Twice |

ug/Kg i ug/Hg i ug/l

1 1

1 1 1 1

1 1 K*

1 1 K*

i i KA

1 i **

« / - 1 1 K»

i i H*

1 1 **

1 1 <*

1 i KA

1 1 "*

i i K*

1 1 "*

i 1 >*

1 1 " 1

1 j * 1

1 1 **

i i **

i i ** 1 1 "*

1 KA

i i 1*

1 1 ** 1 1 i i KA

i 2St J/31t } i KA

-#-DUil 1 OUIS

81i3-t l 1 8183-12

Analyzed | Analyzed Twice I Twice

ug/tg i ug/Kg

1

1

DUt( 1 out?

8183-13 1 8183-84

ug/Kg I ug/Kg

1 i B

1

- i ;—

outs

81B3-tS

Analyzed Twice

ug/Kg

B/-

18it } / l S i i J

—1 i 1 ,J \ 1 k-- m

I I I I " ' " ' ' T 0Ut9 i OBAIK i B8-1 i l r i p Blank i DUIIKS/KSO i

i i j 811 1 I 81t3-t6 |81t3-t7 1 8183-18 | 8183-11 | 8183-88 |

I 1 I joupiicate of|

I I 1 1 OUtl 1

ug/Kg 1 ug/Kg j ug/l ' | ug/l j ug/Kg j

I I 1 1 Analyzed | i l l 1 Twice i

i i i K* i ' 1

1 i i ** i 1

I I 1 "* 1 1

i 1 i KA i 1

B 1 B 1 1 KA 1 - / B 1

i i i KA i i

I I 1 >• 1 1

i i i >* i 1

I . I 1 «* 1 1

i i 1 "* i i i i 1 <* i 1

1 1 1 ** 1 1

I I 1 "* 1 1

i i 1 KA i i

i i i *' 1 i I I 1 ** 1 1

i 1 i <* i i i i 1 KA i {

I I 1 "* 1 1 KA

i 1 i <* i i i i 1 K* i i

i i i «* 1 1

i » J 1 19t J i i KA i 71 J/8t ] I

#

CO o o CO

I C A I I ^ ^ ^ I I I I I O J A K A I Y S L - IHAIVTU'


llaboratory Saiple Kuiber

iBeiarks

iunits

isEHIVOlATIlE COKPOUKOS i Quant, i

1 Illiit (Aq)|

lAnthracene | It |

lOi-n-Butylphthalate | It |

JFluoranthene | It |

iPyrene | It |

iButyibenzylphthalate i It i

|3,3'-Dichlorobenzidlne | 2i |

|8enzo(a)anthracene | 18 |

|bis(2-Ethylhexyl)plithalate | It i

IChrysene | It |

ioi-n-Octylphthalate i It i

|8enzo(b)fluoranttiene | 18 |

|Benzo(k)fluoranthene j IB j

|Benzo(a)pyrene | 18 |

|Indeno(t,2,3-cd)pyrene | 18 |

|Oibenz(a,h)anthracene | 18 |

|Benzo(g,h,l)perylene | It |

iouantitation liiit Kultipiier

|Oate of Saiple Collection

|Oate Saiple Beceived by,laboratory

|Oate Saiple Extracted '

|Oate of Saiple Analysis

Instruient Used for Analysis

L IM.»LTS - KLL DUl'IOS

1 DUt2

i 8t9S-ii

i Analyzed

i Twice

1 nlH

Quant. 1

iiit (Sol) 1

33t |24ii 3/2Sti J

33t i 3ti 3/-

33t i 51ti/S2ti

331 |2S,lti/27,itt

33t 1 U3/UJ

33t 1 UJ/U3

33t 1 UJ/U3

33t 1 U3/UJ

33t 1 U3/UJ

33t 1 UJ/U3

33t 1 UJ/UJ

1 8.48

1 8/18/91

1 8/11/91

1 8/14/91

1 8/28 i B/29

KS-5995B

EI UKitu u'il A

DUi3

8895-82

Analyzed Twice

ug/Kg

1188 J/llii 0

26,iti/

21,ttt

UJ/UJ

U3/U3

UJ/UJ

U3/U3

UJ/UJ

UJ/UJ

UJ/UJ

9.i9

8/11/91

8/11/91

8/14/91

8/28 I 8/29

KS-S99SB

Bt'Hcmni'eAS S '' '

0UI4

889S-i3

Analyzed

Twice

ug/Kg

7ti J/81t J

79i J/86i J

-/49t J

7911 U/

9lii U

52i J/S9t J

UJ/UJ

Iiii J/ltti J

set J/Sit J

SBt J/59t J

UJ/UJ

UJ/UJ

UJ/UJ

S.97

8/18/91

8/11/91

8/14/91

8/38 ( 8/31

KS-S995B

Trip Blank

BIB

8i9S-t4

ug/l

KA

KA

KA

KA

KA

KA

KA

KA

NA

NA

KA

KA

KA

KA

KA

KA

KA

KA

KA

KA

KA

KA

OUtl

8183-81

Analyzed

Twice

ug/Kg

9788 U/

11,tit U

UJ/UJ

UJ/UJ

UJ/UJ

UJ/UJ

UJ/UJ

UJ/UJ

UJ/UJ

t.67

8/11/91

8/12/91

8/14/91

8/38 ( 8/31

KS-5995B

U outs

8183-82

Analyzed

Twice

ug/Kg

63 J/72 J

-/34J

64 J/48 J

UJ/-

UJ/-

ISit U/

IttlU

UJ/-

UJ/UJ

UJ/UJ

UJ/UJ

UJ/UJ

B/UJ

R/UJ

R/UJ

l.t3

8/11/91

8/12/91

8/14/91

8/24 S 8/38

KS-599SB

0UI6

Bll3-t3

ug/Kg

.

Slit

26,iti

9.t9

B/11/91

B/12/91

B/14/91

8/27/91

KS-S99SB

;

0Ut7

8183-84

ug/Kg

5988 U

S.4S

8/11/91

8/12/91

B/14/91

8/27/91

BS-S995B

',"; i

0UI8

8183-85

Analyzed Twice

ug/Kg

398 3 1 -

37ti/34lt

37ti/45it

16tt 3 1 -

9Sti U/

12,ttt U

19tl J/2tti J

UJ/UJ

29ti J/27it J

17ti J/17lt J

14ti J/llit J

UJ/lSti J

UJ/UJ

UJ/UJ

9.t9

8/11/91

B/12/91

B/14/91

8/27 S B/29

KS-S99SB

;,

0Ut9

8183-86

ug/Kg

448 J

348 J

371 J

StitU

2St J

6.97

8/11/91

8/12/91

8/14/91

8/27/91

KS-S99S8

1 ii

OBAIK

8183-87

ug/Kg

488 J

418 J

328 J

3tlJ

27ttU

23t J

5.76

8/11/91

8/12/91

8/14/91

8/28/91

KS-S995B

> .1

B8-1

8163-18

ug/l

B

«

B

1.88

8/11/91

8/12/91

8/16/91

B/23/91

KS-599SB

i • i

Trip Blank

811

8183-11

ug/l

KA

NA

NA

NA

NA

NA

NA

NA

NA

KA

HA

KA

NA

NA

NA

NA

NA

KA

HA

NA

NA

NA

'-page J -J

DUIINS/NSO 1

8183-88 i

Duplicate | of OUtl 1

ug/Kg 1

Analyzed |

Twice 1

-/"J 1

118 J/148 J 1

188 J/248 J 1

188 J/178 J 1

w/- 1

UJ/- 1

6388 U/ 1

S988 U i

128 J/116 J 1

168 J/UJ i

118 J/128 J 1

72J/7tJ 1

UJ/UJ i

R/UJ 1

R/UJ 1

R/UJ i

l.t3 1

8/11/91 i

8/12/91 1

8/14/91 1

8/23 S 8/28 1

KS-599SB 1

m

-A

CO o o CO

l u r j ^ B i v c u i l0ENTIFy!Lu .un/ilUKOS ''- ^JlHATEO lunicniXATIOHS- - nif SOlIDS'Mir^ii.lO ON A U I ».<oHT B A S ^ ^ ^ ' i ^ i ^ f i 1 1 1 1 , ; . , j 6 |

lAnsoj) lAyJronwfltai Saiple Kuiber | 0Ut2 | 0U13 | 0UI4 | Trip Blank | OUtl | OUIS J 0Ut6 | DUI7 | GUIS | 0U>9 J DRAIN ) RB-1 jTrip Blank | DUil | 1 1 1 1 1 811 1 1 1 1 1 1 1 1 1 811 1 1 llaboratory Saiple Kuiber | 8 t95- t l j 8895-82 | 8695-83 | 8695-84 | 8183-61 | 8163-62 | 8163-63 |8163-84 | 8183-85 | 8163-66 | 8183-87 j8183-16 | 8183-11 | 8163-68 |

iBeiarks i i i i i i 1 i i i i 1 i i 1

1 lUnits i ug/Kg | ug/Kg | ug/Kg j ug/l j ug/Kg | ug/Kg | ug/Kg | ug/Kg | ug/Kg i ug/Kg j ug/Kg i ug/l i ug/l | ug/Kg {

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

IVOIATIIE COKPOKEKTS | | | 1 - 1 " 1 I ' l l 1 1 | - | - | KA | 1 1 , , , 1 . — , . . 1 1 I I I 1 1 j — " • - - I - - - - 1 |— 1 1 • 1 1 1 1 " 1 1 1 j - 1 1 iHexane | 18,668 J | | | | I I I I I 1 1 1 I 1

lUnknoun Hydrocarbons (Kuiber of Peaks) 1 55,666(5) J |71,S66(18) J 1 I I 1 1 I I I I I I 1 I

IC9K12 Alkylbenzene |446.868(4) J | 6668 J | | | 1 - 1 I I | I I I 1 1 • • •• ' I ' I 1 "" 1 " 1

llaboratory Art i fac ts | | | 16 R | | 1 S R | | 8 R | 18 B | 18 R | 23 R | | | |

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 i 1 1 1 . j . . 1 1 |. 1 1 .. .1.. 1 I I ISEKIVOIATIIE COKPOKEKTS | | | | KA | | | | | | | | - | KA | |

. . |, , ,, , , -ISaturated Hydrocarbon (Kuiber of Peaks)i246,668(13)J/ |96,866(lS)J/ i 4868(3) J / i il2,978(7) J / | | 1568(1) J |916(1) ji67,866(4) J / | 1261(1) J | | | |7226(13)J/ | 1 1351,566(13) J|77,986(15) J j 3446(3) J j |14.266(5) J j | j 161,366(3) J | | j j j l 6 ,286 ( lS ) j j

IC9H12 Alkylbenzenes |29,586(S) 31 |15,666(2j J / | | | I I I I 1 1 1 1 1 1 1 1 92,686(4) J 1 6366 J j j | I I I I i 1 i i i i

- 1 .... , 1 lUnknowns (Kuiber of Peaks) |166,368(4) J/ |12,666(2) J / | 4146(3) J / | | 7378(3) J / |4256(13) J/ |24,S86(3) J | |16,886(8) J / | 9566(5) J |6736(4) J | | |6968(8) J / | i il51,666(5) J i 15,666(4) J j 3428(2) J j | 9266(3) J |3538(13) J | | ilt ,B68(6) J | i i i i 3386(4) J i

lOecahydronaphthalene Isoier | 2886 J / | 4568 J / | 1 1 1 1 1 1 1 1 1 1 1

i i 1 1*1 ^ 1 i i 1 1 1 i 1 i i i i i i

lAlkyl-substituted Cyclobexane | 3186 J / | 13,586 3 / | | | 3366 J / - | | | | | 1 1 1 1 1 i i 13,861 J i 11,186 J i 1 i i i i 1 i i i i i 1

. . - 1 - - - • • 1 1 1 1 1 inexadecanolc Acid | -/179,668 J i i i i i i i i 1 1 i i i 1

lAlkyl-substituted Phenol | | 3686 J / | | | I I I I 1 1 1 1 1 1

lOxygenated PAH | |2766 J/3666 J | | 1 1 1 1 1 1 1 1 1 1 1

IC18H22 Alkylbenzene | | -/2168 J | 1666 J / | | | | j | | I I I 1 I

1 1 1 1 » » J 1 1 I I I I 1 1 1 1 1 1

| l-Phenyl-l,2-propanedione i i i i 1 U » i |Z^^ i \ \ 11S86 J/1566 i 936 J | | | | |

y.- >i

CO o o CO

00

1 tt ' ^ EXTRH^ORGAHIC AKAKSIS

f ^ i

- ANAimCAl BESUITS


1 llaboratory Saiple Nuiber 1 ,.. , 1 IReiarks 1 " lUnits 1 • • • •

IPESTICIOES

1 1 lalpha-BHC 1 Ibsta-BHC j

Idelta-BHC

1 |gaaa-BHC (lindane) 1 • " " • • • "

iHeptachlor

lAldrin

1 •" • ••

IHeptachlor Epoxide

JEndosulfan I 1

iBleldrin

1 |4,4'-D0E 1 •• ' • • "

lEndrin

1 lEndosulfan II 1 •

|t,t'-DB0

i • • • • • • • • • •

lEndosulfan Sulfate 1 |4,4'-DDT 1 1 •• •

iNethoxychlor f

1 lEndrln Ketone 1 1 lalpha-Chlordane 1 1 ••

IgaMa-Chlordane

1 • iToxaphene

Quant, liiit (Aq)

6.6S

6.85

8.65

t.ts

t.ts

t.ts

i.ts

t.ts

t.lt

t.lt

t.lt

t.ll

t.lt

l.lt

t.lt

I.St

l.lt

I.St

I.St

l.t

Quant, liiit (Sol)

8

8

B

8

8

8

8

8

16

16

16

16

16

16

16

86

16

88

88

168

j /

- All SOIIOS

DUI2

8695-61

ug/Kg

183

166 J

146 J

36

22 J

;. i EPOBTED ON A

DUI3

8695-82

ug/Kg

UJ

R

UJ

UJ

UJ

87 J

41 J

R

R

R

UJ

39 J

R

UJ

UJ

i • • ,

IBf UEIGHT SAS

0Ut4

8695-13

ug/Kg

UJ

B

UJ

UJ

UJ

16 J

St J

R

R

R

UJ

126 J

R

UJ

UJ

S

Trip Blank 811

8695-84

ug/l

NA

HA

KA

KA

NA

HA

KA

KA

KA

KA

NA

HA

HA

HA

KA

HA

HA

KA

KA

KA

A w DUil

8113-11

ug/Kg

KA

HA

HA

KA

KA

KA

KA

HA

HA

NA

NA

NA

NA

NA

HA

HA

KA

KA

KA

KA

QMS

8183-12

ug/Kg

UJ

R

UJ

UJ

UJ

UJ

UJ

« R

«

UJ

UJ

R

UJ

UJ

S

0UI6

8163-83

ug/Kg

UJ

R

UJ

UJ

UJ

18 J

75 J

R

R

R

UJ

24 J

R

UJ

UJ

{

0UI7

8163-11

ug/Kg

UJ

R

UJ

UJ

UJ

19 J

11 J

R

R

R

UJ

7.S J

R

UJ

3.4 J

DUIB

81t3-tS

ug/Kg

UJ

«

UJ

UJ

UJ

42 J

48 J

12 J

R

R

R

UJ

52 J

R

UJ

29 J

DUI9

8183-86

ug/Kg

8.2 J

«

UJ

UJ

UJ

UJ

UJ

B

B

B

UJ

14 J

B

UJ

UJ

DRAIK

8183-67

ug/Kg

UJ

B

UJ

UJ

UJ

UJ

UJ

R

R

R

UJ

OJ

R

UJ

OJ

j.

RB-1

8183-16

ug/l

Trip Blank 811

8163-11

ug/l

KA

KA

HA

HA

KA

KA

NA

NA

HA

KA

HA

KA

KA

KA

HA

KA

KA

KA

HA

KA

• X

-page l \ - 1

OUtl 1

8113-18 1

ug/Kg i

1

1 1

1 S.U 1

1

7.7 J 1

6.2 J 1

- •

l E I I ^ ^ P OKEimiC AKAIV^IS - 'AHAIVTIIAI RE^UITS


llaboratory Saiple Huiber

jReiarks

iUnits

ipCBs i Quant. 1 lliiit (Aq)

iAroclor-1616 i 8.5

|Aroclor-l221 i I.S

|Aroclor-1232 i 6.5

iAroclor-1242 | 8.5

|Aroclor-124B i 6.5

|Aroclor-12S4 | 1.6

|Aroclor-1268 | 1.8

iQuantltation liiit Kultipiier

Quant, liiit (Sol)

88

88

88

86

86

166

168

1 • •'

lOate of Snpie Collection

joate Saiple Received by laboratory

ioate Saiple Extracted

ioate of Saiple Analysis

All SOIIOS BEPORTED OK A DRV UEIGHT BASIS

DUI2 1 0UI3 1 DUI4 | Trip Blank i i i 818

8895-61 i 8695-62 | 8895-63 i 8895-64

ug/Kg i ug/Kg i ug/Kg i ug/l

i i i KA

i i i HA

i i i KA

1 1 1 KA

i i i ** i 1 i KA

i i i KA

1.69 i 1.75 i 1.58 1 KA

8/16/91 i 8/18/91 i 8/11/91 i KA

8/11/91 1 8/11/91 1 B/11/91 1 8/11/91

8/14/91 1 8/14/91 1 8/14/91 | 8/14/91

B/27/91 1 8/28/91 | 8/28/91 | 8/28/91

1 1 1

DUil

8183-81

ug/Kg

KA

HA

KA

KA

HA

HA

KA

HA

KA

8/11/91

8/14/91

8/28/91

'

DUI5

8163-62

ug/Kg

6.43

8/11/91

8/11/91

8/14/91

8/28/91

DUIB

8113-13

ug/Kg

1.75

8/11/91

8/12/91

8/14/91

B/28/91

DUI7

8183-64

ug/Kg

6.49

8/11/91

8/12/91

8/14/91

B/28/91

; 1

DUIB

8163-65

ug/Kg

6.74

8/11/91

8/12/91

8/14/91

8/2B/91

"i

DUI9

8163-16

ug/Kg

6.59

8/11/91

8/12/91

8/14/91

8/28/91

:j

ORAIH

8183-87

ug/Kg

6.48

8/11/91

B/12/91

8/14/91

8/28/91

i —

RB-1

8163-16

ug/l

1.66

8/11/91

8/12/91

8/14/91

8/27/91

!*. i '

Trip Blank 811

8163-11

ug/l

KA

KA

KA

HA

KA

HA

KA

KA

KA

HA

HA

KA

-page 8 ^

DUIIKS/KSD 1

8183-88 i

ug/Kg 1

8.54 1

8/11/91 i

B/12/91 1

8/14/91 1

B/27/91 i

BOTES: Coipound was not detected.

U This coipound should be considered 'not-detected' since it was detected in a blank at a siiiiar level.

R Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the

quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is probably

higher due to a low bias identified during the quality assurance review.

CO

o CO

r-(•..

CO o o CO CO

o

^ B l E OBBAHIC AHAITSIS - AHAlVTICAl RESUITS'- All SOIIOS'REPOBTEO OK A ORTUEiGHT BASIS ^ ^ ^ B ' " ' ' ' ' . ' ' 1 ' ' ' i ' i'* " ' ^ ^ • " Q " '

(Anson Environiental Saipie Kuiier t m t ! S ' - ! r l m i 3«'-J?'(flfW SUaklmS 35'-37'(5M« 3»'-3J'|7ri(> Slink iFlel i SJ4/?k|JM; W - i l ' l m J «'-47'(ffW7 55'-}7'|lWfH «'-47'ff i(Ji( SJM)Tfl? l l isk |Trip BJM | i i i i 921 1 1 i 822 i 822 i | i i ^ | 823 | 8231 i 8232 i llaboratory Saiple Huiber i 8288-81 i 8266-82 i 8268-63 i 8215-81 i 8215-62 i 8215-83 | 8215-84 i 8224-61 i 8224-t2 i 8224-13 i 8224-84 i 8224-85 i 8224-86 j 8224-17 i

IReiarks l i i i l i l l l i Analyzed |Duplicate of | | | | 1 1 i i i 1 i i i i i Twice J0UI7 4 5 ' T 4 7 ' i j i i

iunits i ug/Kg | ug/Kg j ug/l i ug/Kg | ug/Kg i ug/l i ug/l i ug/Kg i ug/Kg i ug/Kg i ug/Kg { ug/l i ug/l j ug/l | 1 1 . 1 1 1 , . . j . ,,., , 1, ,, . .. „. , .. _. ••

ivOlATIlE CONPOUNOS ^Quantitation iouantitationi { i i i 1 1 i 1 1 i i i i i i i l l i i t (Aq) i l i i i t (Sol) i i i i i 1 1 1 1 1 1 1 i 1 i

jchloroiethane i 16 i 18 i i i i j i i i i i i i i i i

jtroioiethane | 11 | 11 | | | | 1 1 1 1 | j I I 1 1 1

ivinyl Chloride i I t i I t i | | i i 1 i | i i i i i i i

iChloroethane | I t | I t | | | | 1 1 1 | | | -/UJ | | | | |

iKethylene Chloride | 5 | 5 i IStt U i 12tt U i 4 J | I t t t U i 5 U i 4 J i 4 J i 5 U i S U i 6 U/7 U i 5 U i 4 J | 4 J i 5 J i

{Acetone i 16 i 18 i S488 R i 4866 R i 46 J i 4268 8 i 22 R j i SB J i 5 B i 5 B \ i R/11 R { 3 R { 22 J i i i

I'Carbon Disulfide | 5 | 5 | i | j 1 i i i i i i i i i i

il,l-Dichioroetliene i 5 | 5 i i i | i i 1 i i i i i i i i

1 1 1 1 - - 1 1 1 1 1 1 1 1 1 1 |l,l-OichloroeUiane | 5 | 5 | | | | 1 1 1 1 1 1 1 t i l l

iTotal 1,2-Dichloroethene j 5 i 5 j i i i i i i i i i i i i i i

ichlorofon | 5 | S | 1 | 1 1 1 1 1 1 1 1 | | | 1

il,2-0ichloroethane i 5 | 5 i i i i i i i i i i i i i i i

|2-Butanone | 16 i 18 i i | i i i i 1 i i i i i 1 i

|l,l,l-Trichloroethane | S j 5 j i i i i t 1 i i j i 1 j I i

ICarbon Tetrachloride | 5 | S | | | | 1 1 1 | | | | | | | |

ivinyl Acetate i 16 i 16 i i i | i i i i i i i i i i i

ieroiodichloroiethane { 5 i 5 i i i i i i i i i i i i i i i

il,l,2,2-Tetrachloroethane i S i 5 j i | i i i l l i i i i i i i

il,2-Dichloropropane i 5 i S | | i | | I I I 1 i 1 1 1 1 i 1 1 .[._ _] 1 1 I — 1 -- - 1 ,._| 1 .,, I i l l !

|trans-i,3-Dlchloropropene | 5 | 5 | | | | | 1 1 1 1 1 1 1 i l l

iTrichloroeChene | 5 | 5 | I I 1 1 1 1 1 1 1 1 1 j | 1

iDlbroiochloroMthane | 5 | 5 | | | | | | | | | | | | j | |

1,1,2-Trichloroethane | 5 | 5 | | | | 1 1 1 1 I i i i i i

iBenzene | 5 | 5 | | | UJ | | | | | j j i i i i i

. i » ^ ^ i < . « » i . iKAirsis' ' .iimcAi! »u. ..'o - A U » L . J S R E P O L L U UK'A DRT

iAnsoi^nTironiental Saiple Kuiber jouil 25'-27'iouil 36'-32'

1 1 1 llaboratory Saiple Huiber | 8288-61 | 8268-82

IBeiarks | |

1 1 1 1 . ,. , _ . 1 •- 1 1 1 1 -lunits 1 ug/Kg | ug/Kg

1 _ 1 .1 IVOIATIIE COKPOUKOS iouantitatlon iouantitationl i i j liiit (Aq) illiit (Sol) i i

|cis-l,3-Dichloropropene | 5 | 5 | | 1 1 1..,. ,1 1 ••• 1 1 1 1

iSroiofori | 5 | S | |

|2-Hexanone | 18 | 18 | | 1 1 . .,

i4-Kethyl-2-Pentanone | 18 i 18 i i

JTetrachloroetbene | 5 | 5 | |

iloluene j 5 i 5 | |

iChlorobenzene | 5 | 5 | |

JEthylbenzene | 5 | 5 | |

IStyrene | 5 | 5 | |

jTotal Xylenes | S | 5 | |

1 1 1 IQuantltation lUit Kultipiier | 136 | 138

iDate of Saiple Collection | B/21/91 | 8/21/91 1 _. . I " • • 1 1 IDate Saiple Received by laboratory | 8/22/91 | 8/22/91

1 . - -

IDate of Saiple Analysis | B/36/91 | 8/36/91

llnstruient Used for Analysis | KS-5995 C | HS-5995 C 1 1 1

iii«n, iJSIS ' •

Field Blank|DUI6 3S'-37' 821 1

8268-83 i 8215-61

ug/l 1 ug/Kg

UJ 1

UJ i

UJ 1

UJ 1

UJ 1

1.6 i 136

8/21/91 1 8/22/91

8/22/91 1 8/23/91

8/29/91 1 8/36/91

HS-599S 0 1 HS-5995 C

" % DUIB 3l'-32'

8215-62

ug/Kg

1.1

8/22/91

8/23/91

8/29/91

KS-539S A

\ Trip Blank

822 8215-63

ug/l

1.1

8/22/91

8/23/31

8/29/91

HS-5995 0

r 1 Field Blank

822 8215-14

ug/l

l.t

8/22/91

8/23/91

8/29/91

HS-S995 0

1 ;

DUI7 4l'-42'

8224-61

ug/Kg

1.8

8/23/91

8/24/91

8/29/91

HS-5995 A

••

DUI7 45'-47'

8224-82

ug/Kg

1.8

8/23/91

8/24/91

8/29/91

KS-599S A

; I —

DUI7 55'-57'

8224-63

Analyzed Twice

ug/Kg

1.2

8/23/91

8/24/91

8/29 ( 8/38

NS-S995 A

-| j —

0UI7A 45'-47'

8224-64

Duplicate of DIII7 45'-47'

ug/Kg

l.t

B/23/91

B/24/91

8/29/91

NS-5995 A

- t • i-

Field Blank 823

8224-65

ug/l

—

1.8

8/23/91

8/24/91

8/29/91

KS-5995 0

i;

Trip Blank 8231

8224-86

ug/l

1.6

8/23/91

8/24/91

8/29/91

HS-5995 0

# , Trip Blank |

8232 i 8224-67 j

ug/l 1

1.1 i

8/23/91 1

8/24/91 1

B/23/91 i

HS-5995 0 i

BOTES:

CO

- Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected

in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the



CO

CO

CO CO

^ ^ i — { i ^ ^ ' ' t ? i " •; • 1 1 - 1 ) j - ~ V i ^ ^ EXTR^^p iRGAKIC AKAlfSIS - AKAlYTICAl BESUITS - , A l l SOIIOS R PORTED OK A DRT UEIGHT BASIS ^ ^ | , ' . . ^ ^ B

iAnsonTiwiromental Saiple Huiber i ou i l 25'-27' iDUIl 3 t ' -32 ' iF ie ld BiankioUIB 3S'-37'ioUt6 3 6 ' i r i T r i p Blank iF ie ld BiankjoUIT 48'-42'iDUI7 45'-47'iDUI7 5S'-57'iDUI7A 45 ' -47 ' iF ie ld B lank i l r ip Blank i l r l p l u n k i 1 1 1 1 821 1 1 1 822 1 822 1 | | | T 823 | 8231 | 8232 | i laboratory Saiple Kuiber i 8266-61 | 8266-62 j 8268-63 | 8215-61 i 8215-62 i 8215-63 i 6215-64 i 8224-61 i 8224-82 i 8224-63 i 8224-64 i 8224-65 i 8224-66 i 8224-67 |

IBeiarks 1 1 1 1 1 1 1 1 1 1 1 i i i i

iuni ts 1 ug/Kg | ug/Kg i ug/ l i ug/Kg i ug/Kg i ug/ l { ug/ l i ug/Kg i ug/Kg { ug/Kg i ug/Kg i ug/ l i ug/ l | ug/ l i

ISEKIVOIATIIE COKPOUKOS IQuantltation |Quant i tat ion| I I I I I I I I I |Dupllcate of | | | | i i l i i i t (Aq) l l i i i t (Sol) i i i i i i i i 1 i iDUI7 45'-47' I | i |

IPhenol 1 11 1 331 1 | | | | 1 K« 1 I | | | | | KA | NA |

ibls(2-Chloroethyl)ether | I t i 331 i i i i i i "« i 1 i i i i i NA | HA i

i2-Chlorophenol i I t i 331 | | i i i i NA | i i { | \ i NA i HA i

ii,3-Dichlorobenzene i 11 { 331 i | i i i j KA i i { | 1 i i KA i KA i

|l,4-Dlchlorobenzene | I t | 331 | | | | | 1 KA | | | i | { i KA | KA |

ioenzyl Alcohol i 16 i 336 i i { i i i HA | j | | i i i KA j HA i

il,2-Dichlorobenzene i 16 J 336 i i i i i i NA | i i i { { i HA i HA i

i2-Kethylphenol i 16 i 338 i | i i i i KA i i i i | | | HA | KA i

|bis(2-Chloroisopropyl)ether i 18 | 336 { i i | i i KA i i | { i i i KA | HA |

|4-Hethylphenol | 18 | 336 | | | | | 1 K« 1 1 | | | | | KA | KA |

iH-Hitroso-di-n-Propylai ins i I t i 331 i i i i i | KA i i i i { { i HA i KA i

iHexachioroothane | I t i 331 i i i 1 i i n * ! i i 1 1 i KA i HA |

iKitrobenzene | I t | 331 | | | | | 1 *• 1 1 1 1 | | KA | HA |

ilsophorona i I t i 331 i i i i i i KA i i i i j i HA i KA |

i2-Kitrophenol i I t i 33t i j i i i i KA i \ \ \ j | M j | t i

|2,4-0i iethylphenol | I t | 33t | | | | | 1 KA | | | | | | KA | KA |

IBenzoic Acid | 56 i 1658 i j i i i i HA i | j { | i HA i KA i

|bis(2-Chloroethoxy)iethane | 18 | 336 | | | | i i «* 1 1 i 1 1 | HA | KA |

|2,4-Dichlorophenol | 18 | 336 | | | | | 1 KA | | | | | | KA | KA |

i l,2,4-Trichlorobenzene i 18 i 336 i i i i | | KA i i i | i i HA i KA i

iKaphthalene | 16 i 336 | | i i | i KA | | j | | HA | KA |

|4-Chloroanil ine | 16 | 336 | | | | | 1 KA | | | | j | HA | KA j

inexachlorobutadiene i 16 i 336 i i i i | | HA i | i { | i KA i HA i

i4-Chloro-3-KethylphenoI \ 16 336 | i KA j | | | u KA | I 1 . 1 _ 1 __ _ . [ . . [ . 1 ..| — 1 — 1 1 1 1 . . [ 1 1 1 1 i2-Hethylnaphthalene i l 8 | 336 | i i | i i KA i i i i { | i HA i KA i

CO o o CO CO

-Wk ^^ iiKAiyn', ilTS "-'

Anson^mromental Saipie Huiber

laboratory Saiple Huiber

Beiarks

lUnits 1 1 1 1 ISEHIVOIATIIE COKPOUKOS

1 1 • • • "

iHexachlorocyclopentadiene 1 |--|2,4,6-Trichlorophenol

1 2,4,5-Trichlorophenoi

|2-Chloronaphthalene

1 ' |2-Kitroaniline 1 lOiiethylphthalate 1 1 lAcenaphthylene t

r |3-Nitroaniline 1 1 " lAcenaphthene 1 1 |2,4-01nltrophenol 1 I " |4-Kitrophenol 1 1 • •

lOlbenzofuran

1 — • • • •

|2,4-0initrotoluene 1 1 |2,6-01nitrotoluene 1 1 iDiethylphthalate 1 1 14-Chlorophenylphenylethir 1 |. , IFluorene 1 1 |4-Kitroaniline 1 |— |4,6-Oinitro-2-Hethylphenol

H-Hltrosodiphenylaiine

|4-Broiophenylphenylether

IHexachlorobenzene

1 •

IPentachlorophenoi

Phenanthrene

1

Quantitation liiit (Aq)

18

11

51

It

St

It

It

St

It

5t

St

It

11

It

It

It

It

51

St

It

It

It

St

It

Quantitation liiit (Sol)

33t

33t

1656

338

1656

338

338

1656

336

lest

1651

331

33t

33t

331

33t

33t

1651

1656

336

336

336

1656

336

.... ..-.IDS Rl

DUil 25'-27'

8268-81

ug/Kg

i w u DUil 3l'-32'

8286-62

ug/Kg

S....:. .i'sAsis'^

Field Blank|DUI6 3S'-37' 821 i

8288-83 i 8215-81

ug/l i ug/Kg

" 1

1

- m DUI6 3 6 ^ ^

8215-82

ug/Kg

) •' ,

W 1 Trip Blank |

822 8215-83

ug/l

HA

HA

HA

KA

KA

KA

KA

KA

KA

KA

HA

HA

HA

KA

KA

KA

KA

HA

HA

KA

HA

HA

KA

KA

; (

Field Blank 1 822

8215-64

ug/l

i J i

DUI7 48'-42'|DUI7 45'-47'

8224-81 i 8224-62

ug/Kg i ug/Kg

1 1

1

-, r^> r---i ,.^-.. m 0UI7 SS'-57'|DUI7A 45'-47'|Field Biank|Trip Blank Trip Hank i

i i 823 i 8231 8232 j 8224-63 i 8224-64 ii 8224-65 i 8224-66 8224-67 i

I I I 1 I I I 1

1 1 ..|..... ,„..| ug/Kg 1 ug/Kg 1 ug/l | ug/l ug/l |

ioupllcate of 1 i i0UI7 45'-47' i i

1 1 HA HA 1

i i HA NA 1

i i HA HA i

1 i KA HA i

1 1 KA KA 1

i i KA KA 1

i i KA KA 1

i i KA KA i

1 1 HA KA 1

1 1 HA HA 1

i 1 KA KA 1

1 1 KA KA 1

1 1 KA KA 1

i 1 KA KA i

1 1 HA HA 1

1 1 KA KA 1

1 i KA KA i

i i KA KA i

i 1 HA HA i

i KA KA i

i i KA KA i

i 1 KA KA i

i i KA KA 1

i 1 KA 1 KA 1

CO

CD CO

E X T ^ ^ ORGAHIC AKAirSIS - 'AKAlTTfcAl Rts'UlTS - A l l SOIIOS REPORTED OK A DRT UEIGnf BASIS' ' ^ ^ ' ^ '' ''''~ . i j ^ B

iAnsonl i iv l ron ienta i Saiple Kuiber ioUl l 25'-27' iDUIl 3 l ' -32 ' iF ie ld BlankiouiB 3S'-37'ioui6 3 6 ' ^ i T r i p Blank iField BiankioUIT 4l'-42'iDUI7 45'-47'ioUI7 55'-57'ioUI7A 45 ' -47 ' iF ie ld BlanklTrip Blank iTr lp lTank i 1 1 1 1 821 1 1 1 822 1 822 1 | | | | 823 | 8231 | 8232 | i laboratory Saiple Huiber | 8268-11 | 8268-62 | 8286-63 | 8215-81 | 8215-62 j 8215-83 | 8215-64 | 8224-61 i 8224-82 i 8224-63 i 8224-84 | 8224-65 i 8224-86 i 8224-67 { 1 . . . _. __ _. 1 _i _ 1 1. 1- - ,. I 1 1 1 ,... I I I I I I 1 •• • 1 1 1 1 1 1 1 1 1 1 1 1 1 — 1 1 iBeurks | | 1 1 1 I I I 1 1 | 1 1 1 i

iun i ts i ug/Kg i ug/Kg i ug/ l i ug/Kg | ug/Kg i ug/l i ug/ l i ug/Kg i ug/Kg j ug/Kg | ug/Kg i ug/ l i ug/ l i ug/ l i

isENIVOlATIlE COHPOUHOS iouant i tat ion iQuant i tat ioni i i i i i i i i i ioupiicate of { i i | i 1 l i i i t (Aq) i l i i i t (Sol) i i i 1 i i i 1 | | |0UI7 45'-47' i j i |

lAnthracene | 11 | 336 | | | 1 | 1 I * 1 1 1 | | | | HA | KA | 1 , . _____ | ._.,,, 1 ,_|...-.,. , 1 ' • • 1 i l l

lOi-n-Butylphthalate | 18 | 336 | | | | 1 1 KA | | | | | | | KA | KA |

iFluoranthene | 18 | 336 | | | | | 1 KA | | j | j | | KA | KA |

IPyrene | 18 | 336 | | | | | 1 KA | | | | I ' I | HA | HA |

IButyibenzylphthalate | 16 | 338 | | 1 | | 1 KA | | | | | | | KA | KA |

|3,3'-Dicblorobenzidine | 26 | 668 | | | | | 1 KA | | | | | | | HA | HA |

iBenzo(a)anthracene i 16 J 331 i i i i i | KA i i i i i i i HA i HA i

|bis(2-Ethylhexyl)phthalate | 16 | 338 | 346 U | 348 U | | 346 U | 2186 U | HA | | | 348 U | | | | KA | KA |

ichrysene i 16 i 336 i i 1 1 i i KA i i i | i { i KA | HA i

iDl-n-Dctylphthalate | 16 | 338 | | | | | 1 « ' 1 1 1 1 1 1 | HA | KA |

|Benzo(b)fluoranthene | I t | 33t | | | | | 1 KA | | | | | | | KA | KA |

|Benzo(k)fluoranthene | I t | 33t i i i i 1 KA i i | | | | | KA | KA |

iBenzo(a)pyrene i 11 | 33t i i i i i i KA i i i i { i i KA i KA i

|Indeno(l,2,3-cd)pyrene | I t | 33t | | 1 | | 1 KA | | | | | | | KA | HA |

|Oibenz(a,h)anthracene | I t | 33t | | | | | 1 *« 1 1 1 | | | | HA | HA |

|Benzo(g,h,i)perylene | I t | 33t | | | | | 1 >* 1 1 1 | | | | KA | KA |

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 IQuantltation l i i i t Ku l t ip i ie r | l . t 3 | 1.13 | l . t t | 1.13 | 1.16 | KA | 1.66 | 1.63 | 1.13 i 1.21 i l . t t j l . t t { KA i NA j

ioate of Saiple Collection i 8/21/91 i 8/21/91 i B/21/91 i 8/22/91 i 8/22/91 i KA i 8/22/91 i 8/23/91 i B/23/91 i 8/23/91 | 8/23/91 | 8/23/91 i HA | KA |

ioate Saiple Beceived by laboratory i 8/22/91 i 8/22/91 i 8/22/91 i 8/23/91 i 8/23/91 i KA i 8/23/91 i 8/24/91 i 8/24/91 { 8/24/91 i 8/24/91 i B/24/91 i KA | HA 1

ioate Saiple Extracted i B/24/91 i 8/24/91 j B/23/91 i 8/26/91 j 8/26/91 i KA { 8/27/91 i 8/26/91 i 8/26/91 i 8/26/91 j 8/26/91 i 8/26/91 i KA i HA i

IDate of Saiple Analysis | 8/36/91 | 8/36/91 | B/27/91 | 8/36/91 | B/36/91 | HA | 8/38/91 | 8/38/91 | 8/38/91 | 8/38/91 | 8/31/91 | 8/36/91 | KA | KA |

l l ns t ru ien t Used for Analysis i KS-5995B i KS-5995B i KS-5995B | KS-5995B i KS-5995B i KA i KS-5995B i IS-5995B j NS-5995B | NS-5995B | KS-5995B | KS-5995B | IA j KA | 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

|CIP ^ V l V E i y IDEKTIFIED COKPOUKOS - ESTIKATED COKCEHTBATIOHS - A l l SOIIOS REPORTED OK A ORT UEIGHT B * S ^ I I ^ W |

lAnson Environiental Saiple Kuiber |0UI1 25'-27'|DUIl 36'-32'|Fieid Blank|DUI6 35'-37'|DUI6 3 l ' -32 ' |Tr ip Blank |Field Blank|DUI7 48'-42'|DUI7 45'-47'|DUI7 55'-57'|DUI7A 45'-47'|Field Blank|Trip Blank |Trip Blank | i i i i 821 i i i 822 i 822 i i { | i i 8 2 3 i 8231 i 8232 i ilaboratory Saiple Kuiber i 828t-t l | 82t l- t2 i 8268-83 i 8215-81 i 8215-62 i 8215-63 | 821S-84 i 8224-11 i B224-t2 i 8224-63 i 8224-64 i 8224-65 i 8224-66 i 8224-87 i

ineiarks i 1 i i i i i i i i i 1 1 i i

1 •• I I I I 1 I I I 1 1 1 1 1 1 1 lunits 1 ug/Kg | ug/Kg | ug/l | ug/Kg | ug/Kg | ug/l | ug/l | ug/Kg | ug/Kg | ug/Kg | ug/Kg | ug/l | ug/l | ug/l |

icOKPOUKOS i j i i i i i i 1 i VOAs iouplicate of i i i i i i i i i i i i i 1 i Twice i0UI7 45'-47' i i i i

IVOIATIIE COKPOKEKTS I | | I 1 - 1 1 1 1 1 1 I ' I 1 1

IHexane | 866 R | 866 R | | 886 R | | | | | | | | | I SJ |

llaboratory Art i facts 1 | 1 i i i 1 1 | 16 R | 16 B | 6 R | 6 R | 14 R/18 R | 18 B | | 9 B | S R |

1 1 1 1 1 1 1 1 1 1 1 1 ' 1 1 1 1

isEHIVOlATIlE COKPOKEKTS i - i - i " i " i i KA i - i - i - i - i - i - i HA i KA |

isulfur (SB) i i 1 i i 456 J i i i i i i { i i i

lUnknowo (Kuiber of Peaks) 1 1 1 1 1 S58(2) J | | | | | | I I I I

KOTES:

- Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected

in a blank at a siiilar level. B Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the



GO

CO CO cn

CO.-

, j ^ ^ - ^^ ^ ^ E X T R M I F D R G A H I C AKAITSIS - AKAlfTICAl RESUITS - / l l SOIIOS BEPORTED OK A ORT UEIGHT BASIS ^ ^ ^ ' - ^ ^ P

lAnson Environiental Saipie Huiber |OUil 2S'-27'|0U|1 36 ' -32 ' |F ie ld Blank|DUi6 35'-37'|DUI6 38'-32' |Tr ip Blank |Field Blai)k|DU(7 4t'-42'|DUI7 45'-47'|DUt7 5S'-57'|DUi7A 45 ' -47 ' |F ie ld Blank|Trip Blank |Tr ip Blank | i i 1 1 821 1 1 i 822 1 822 i i i i { 823 i 8231 | 8232 | i laboratory Saiple Huiber | 8268-61 { 8266-62 i 8266-13 i 82 iS- t i j 8215-12 j B21S-t3 j 821S-t4 j 8224-11 i 8224-12 i 8224-83 i 8224-84 i 8221-85 i 8224-86 i 8224-87 i

iKeurks | | | | | I I I | | | I I I I

iuni ts i ug/Kg | ug/Kg i ug/ l i ug/Kg i ug/Kg i ug/ l j ug / l i ug/Kg i ug/Kg | ug/Kg | ug/Kg | ug / l { ug/ l { ug/ l i

ipesticides iQuantltat ion |Quant i tat ion! l i i i i i i i i |Duplicate of | | i | 1 i l l i i t (Aq) j l i l i t (Sol) i i i i 1 i i 1 i i ioUl? 45'-47' i i i i

ialpha-BHC i 6.65 { 8 | j i i i j HA j j i i j i i HA i HA i

Ibeta-BHC | t . t S i 8 i i i i i 1 KA | { { i { i i NA j NA {

Idelta-BHC 1 t . t s i s i i i i i i KA 1 | | { i i i NA j HA i

Igava-BHC (lindane) | 6.65 1 8 | | | | | 1 KA | | | | I ' I | KA | HA | 1 1 1 ! - . , . [ ' • .. [ I ' l l 1 1 1 I - ' I 1 1 1

iHepUchlor | 8.65 | 8 | | | | | 1 KA | | | | | | | HA | HA |

jA ld r in 1 1.65 | 8 | | | | | 1 KA | | | | | | | KA | HA |

IHeptachlor Epoxide | 8.85 | 8 | i i i j i KA i i | \ \ \ | KA | HA |

lEndosulfan I | 6.65 | 8 | | | | | 1 KA | | | | | 1 | KA | KA |

iDle ldr in | 6.16 | 16 i i i i | i ' KA { i | { | i i KA | KA i

|4,4'-DDE 1 6.16 | 16 | | | | | 1 KA | | | | | | | KA | NA |

isndrin | 6.16 i 16 i i i i i i HA i { { j i { i NA { NA { 1 1 1 1 •• " • 1 1 1 . . . . |. . . . . 1 . . . 1 1 1 ... . j I 1 1 1 1

lEndosulfan I I | 6.16 | 16 | | | | | 1 KA | | | | | | | KA | HA | 1 1 1 - 1" • 1 1 -•'" I • . . . - - 1 I •-. 1 1 ... . .1 ! „ . , ..,. 1 1 t 1 1

|I,4'-DDD 1 t . l t 1 16 1 1 1 1 1 1 KA 1 | | | | | | KA | HA |

icndoiulfan Sulfate i t . l t j 16 i i | i i | KA i i i i j i i KA i KA {

|4,4'-D0T 1 l . l t 1 16 1 1 1 1 1 1 KA 1 | | | | | | KA | HA |

iKeUloxychlor | t . 5 l | Bt | | | I I 1 KA | | | | | | | KA | HA |

1Endrin Ketone | t . l t | 16 | | | | | | HA | | | | | | | KA | KA |

lalpha-Chlordane | t .S t | 86 | | | | | 1 KA | | | | | | | KA | HA |

Igaaa-Chlordane i 6.56 | 88 i | | i i | KA i i i i i j i NA j HA {

IToxaphene | 1.6 | 166 | | | | | 1 KA | | | j | | | KA | HA |

CO CO

^ M . ......Jc AKAlL. U K A I V T L iuiTS - n. . J I I O S R L . „ , . J O H A O I ^ , .....^BASIS^ ^ ^ t i V i i I I y -i • i ^ J ^ V >

lAnson Environiental Saiple Kuiber |DUI1 2S'-27'iDUIl 38'-32'|Fieid Biankiouie 35'-37'iDUI6 36'-32'iTrip Blank ipield BiankiDUI7 4I'-42'|DUI7 4S'-47'|DUI7 5S'-57'iDUI7A 4S'-47'iField Blankilrip Blank i l r i p Blank i

i i 1 i 821 i i i 822 i 822 i i i i i 823' j 8231 i 8232 j

ilaboratory Saipie Huiber i 8266-61 i 8268-82 | 8266-83 i 8215-61 i 8215-82 i 8215-83 i 8215-84 i 8224-11 { 8224-82 i 8224-83 i 8224-84 i 8224-85 i 8224-66 i 8224-87 i

IBeiarks 1 1 1 1 1 1 1 1 1 1 - 1 1 1 1 1

iunits 1 ug/Kg | ug/Kg | ug/l | ug/Kg i ug/Kg i ug/l j ug/l j ug/Kg j ug/Kg i ug/Kg i ug/Kg i ug/l i ug/l | ug/l i

iPCBs IQuantltation jQuantitation! i i i i i i i i i |Dupiicate of | | | |

i i l i i i t (Aq) i l i i i t (Sol) 1 i i i i i i i i 1 i0UI7 45'-47' i i i i

|Aroclor-1816 | 8.5 | 86 | | | | | | KA .| | | | | | | KA | KA |

|Aroclor-1221 | 6.S | 86 | | | | | | KA | | | | | | | KA | HA |

|Aroclor-1232 i 6.5 i 86 i i | | i i KA | i i 1 i i i KA i KA {

|Aroclor-1242 i 8.5 i BB i i i i i i KA i i i i i - i i KA i HA i

|Arocior-1248 | 6.5 | 86 | | | | | | KA . | | | | | | | KA | HA |

|«roclor-1254 | 1.1 | 166 | | | | | 1 KA | | | | | | | HA | HA |

|Aroclor-126t | l . t | 16t | | | | | 1 KA | | | | | | | KA | HA |

IQuantltation l i i i t Kultipiier | 1.43 | 1.43 { 1.14 | 1.43 | t.43 | KA | 1.12 { t.43 i t.43 | t.St | 1.41 | l . t t | KA i KA i

lOate of Saiple Collection | 8/21/91 | 8/21/91 | 8/21/91 | B/22/91 | 8/22/91 | KA | 8/22/91 | 8/23/91 | 8/23/91 | 6/23/91 | 8/23/91 | 8/23/91 | HA | KA |

IDate Saiple Beceived by laboratory | 8/22/91 | 8/22/91 | 8/22/91 | 8/23/91 | 8/23/91 | KA | 8/23/91 | 8/24/91 | 8/24/91 | 8/24/91 | 8/24/91 | 8/24/91 | HA | HA |

lOate Saiple Extracted | 8/24/91 | 8/24/91 | 8/26/91 | 8/26/91 | 8/26/91 | KA | B/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | HA | HA |

lOate of Saiple Analysis | 9/13/91 | 9/13/91 | 9/4/91 | 9/5/91 | 9/5/91 | HA | 9/5/91 | 9/5/91 | 9/5/91 | 9/6/91 | 9/6/91 | 9/4/31 | KA | HA |

KOTES: - Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected

in a blank at a siiilar level. R Unreliable result - Coipound lay or u y not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the

quality assurance review (data validation). UJ This coipound was not detected, but the quantitation lliit is probably


CO

CO CO

B. INORGANIC TCL DATA

300338

Ci3 O

CO

7 ^ p - I l«LRESIi • |Al

Al^Pnironientai Saiple Kuiber

laboratory Saiple Kuiber

_ - - -

Percent Solids

lunits 1

i 1 IHORGAKIC ElEKEKTS | Detection

lUilt (Ag) 1 1 lAluiinui P 1 23.6 1 1

1 "1 lAntiiony P | 32.6 J Arsenic F i 4.6 1 1

1 1 iBariui P 1 5.6 1 1 1 " • • • • •- r

iBerylliui P | 1.6

1 |-Itadiiui P 1 4.6 (-• •• 1

ICalciui P 1 77.6 1 1 1 " • |-jChroiiui P 1 5.8

1 1 ICobait P 1 17.t

1 !•• "

ICopper P 1 16.6 1 1 I " - •• • - |

Ilron P 1 95.8 1 1 , 1 • •• 1

Ilead F/P| 1.6,111 1 1

1 1 iNagnesiui P | 118 1 1 1 - j- '• iNanganess P | 2.6 1 1 1 - •!• ••

JHercury CV| 6.28 1 1

1 1 iNickel P j 27.6

1 ipotassiui P i 818 1 1 1 |. .. . IStleniui F I 5.8 1 1 1 1 ISilver P 1 7.1

isodiui P 1 118 1 ,.,.,. 1 ,, 1 1 iThalliui F j 1.8 1 1 1 j-IVanadiui P | 7.6

Zinc P 12.1

{Cyanide AS| 16.1 1 1

.... —

Detection

liiit (Sol)

4.6

6.4

6.86

1.8

8.26

6.86

15.4

l.t

3.4

3.2

19.t

1.21/22.2

23.6

6.46

6.16

5.4

162

1.6

1.4

23.6

8.21

1.4

2.4

2.3

I stj . .on

R8-1 11499-123 BlB3-i6

-

ug/l

Rinse Blank

126

3.6

168

•

R

R

282

R

TEO i I UEIOHTi i ^ ^ ... .. ^^^

FB821 81499-lSS 8268-63

ug/l

Field

Blank

114

3.1

184

5.8

lit

4.1

R

R

375

8(5.3x)

FB822 tl499-18S 8215-64

ug/l

Field

Blank

lie

3.1

198

7,6

2.8

R

R

365

R(7.7x)

FB823

tl499-23S

8224-85

-

ug/l

Field Blank

126

S.t

3.1

145

6.8

278

4.7

7.8

R

R

316

R(5.lx)

O U I ^ ^

11499-tlS

8895-81

63.2»

ig/Kg

7838 J

9.6 J

3.7 J

98.2

1.2 f.

8.7 R

16,386 J

463 J

8.7

266 J

19,568 J

1216

9351 J

152 J

8.21 J

21.5 J

459

R

948 J

8.33

79.1 J

1778 J

438 J

DUI3 86499-125 8195-12

79.8»

ig/Kg

4858 J

UJ

3.8 J

44

t.9 8

2.7 fl

22,988 J

111 J

7.6

49.4 J

11,511 J

617

11,911 J

94.13

R

12.6 3

332

R

474 J

41.1 J

236 J

R

0UI4 lt499-t3S

8895-83

77.18

•g/Kg

2636 J

UJ

1.3 J

34.4

1.8 R

1.5 R

7118 3

31.7 3

18.2 J

6638 J

154

3468 J

55.9 J

R

7.2 3

267

R

293 «

28.5 J

113 3

B

1 S

DUil

H499-I4S

8183-11

86.68

ig/Kg

2638 J

UJ

1.2 J

18.2

6.B1R

2.8 R

9788 J

36.1 J

4.2

17.7 J

6418 3

124

5288 J

54.6 J

B

8.3 J

327

R

262 R

22.6 3

81.3 J

R

• -pagi . 1

DUI5 8I499-85S 1 8183-82

96.78

iq/jQ 1

1586 J 1

OJ 1

8.79 J

9.7 !

8.63 R

1311 J

17.4 J

5.3 J

3818 ]

81.3

951J 1

53.3 J

R

4.7 J

221

K

129 R

5.3 3

24.6 J

R

NOTES: - Elsunt was not detected. U This analyte should be considered 'not-detected' since

it was detected in a blank at a siiilar level. R Unreliable result - Analyte lay or lay not be present

In this saiple. 3 Quantitation is approxiiate due to liiitations identified

during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation iiiit

is probably higher due to low bias identified during the quality assurance review.

(Ix) This eleient was not analyzed for and not detected; however, due to saiple dilutions, the reported detection iiiit is equal to the 'norial' detection liiit nltiplied by the factor in parentheses.

ANAlfTICAl NETHOO: P - Inductively Coupled Piasia F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer

CO o o CO

' ^ ' u^^Mnimi

lAnson Environiental llaboratory Saiple N

1 1

- AKAiniCAL RESUlfS - A

Saiple Kuiber uiber

1 iPercent Solids

lUnits 1

IIH0R6AHIC ElEKEHTS

1 1 , 1 1Aluiinui 1 1 lAntiiony

1 Arsenic

1 IBariui 1 IBerylliui 1 j - ••

iCadiiui 1

1 ICalciui 1 1 iChroiiui 1 ICobalt r ICopper 1 ••

Ilron 1

1 Ilead

iHagnesim 1 1 iKanganese

1 iKercury 1 1 iKlckel

ipotassiui 1 1 iSeleniui

ISilver 1 1 ISodiui

IThalliui I IVanadiui 1

J IZinc

ICyanide 1 1 —

1

1 Detection iliiit (Aq)

P 1 23.8

P 1 32.8

F i 4.8

P i 5.8

P 1 1.8

P 1 4.8

P 1 77.8

P 1 5.8

P i 17.8

P i 16.8

P i 95.8

F/Pi 1.8/111

P 1 118

P 1 2.8

Cvi t.2t

P 1 27.t

P 1 818

F 1 S.B -P 1 7.1

P 1 118

F 1 1.8

P 1 7.8

P i 12.8

AS| It.t

Detection liiit (Sol)

4.6

6.4

6.86

1.8

6.28

6.88

1S.4

1.8

3.4

3.2

19.8

6.28/22.2

23.6

8.48

8.18

5.4

162

1.8

1.4

23.6

8.28

1.4

2.4

2.3

; I SOliOS REPOI

DUI6

8183-83

67.68

ig/Kg

9918 J

UJ

(18x)

82.1

1.4 R

6.2 R

9218 J

248 J

11.2

88.2 J

2l,4tt J

112t

6878 J

128 J

B

18.9 J

615

R

993 J

8.28 J

71.2 J

512 J

R

TED OK A DRY 1

DUt7 88499-87S 8183-84

82.48

ig/Kg

3318 J

UJ

1.6 J

15.3

8.91 R

1.3 R

8136 J

54.2 J

3.1

27.8 J

7268 J

157

3758 J

62.8 3

9.3 3

186

B

286 R

18.6 3

78.5 J

2.9 J

EIGHT BASIS

DUIB •1499-185 8183-15

56.68

ig/Kg

11,168 J

9.5 J

3.6 J

S6.8

1.8 R

4.4 R

22,888 J

198 J

11.3

138 3

22.768 J

( U 2 8 ^

14,168 J

162 J

«

28.4 J

548

fl

1248 J

81.8 J

675 J

R

i i

0UI9 86499-89S 8163-86

83.18

ig/Kg

2868 3

UJ

1.2 J

23.3

1.1 B

l.B R

4228 J

37.4 3

5.4

41.7 J

18,988 J

122

2B18 J

189 J

R

11.3 J

268

fl

447 J

28.4 J

138 J

«

~1 DRAIK

68499-16S 8183-87

91.38

ig/Kg

1416 J

UJ

1.5 J

26.8

8.94 R

3.8 R

3658 J

71.6 J

3.4

44.4 J

15,668 J

216

1158 J

13S J

R

17.4 J

215

494 J

17.6 J

254 J

R

> ' DUtlHSD 11499-115 8183-88

79.78

•g/Kg

Duplicate of OUtl

21813

12 J

1.1 J

15.8

8.85 R

1.9 R

6311 J

25.6 J

15.9 3

5888 J

148

3998 J

48.3 3

R

5.9 J

249

R

234 R

IB J

56.5 J

R

I ;

OUIl 25'-27' 11499-135 8268-61

95.88

ig/Kg

1536 J

UJ

5.9

8.56 fl

76.6 fl

2.7 R

2896 J

1.8

225 J

44.4 J

fl

175

R

75.2 fl

2.8 J

4.2 J

R

i !

DUil 3t'-32' tt499-14S 8288-82

96.38

ig/Kg

1336 J

UJ

1.6 J

- .... . 6.3

6.66 R

119 fl

4.1 R

2.6 J

2398 J

2.5

164 J

38.5 J

«

fl

91.6 R

2.6 J

5.4 3

R _

i

i i

-page 2

DUI6 35'-37' i 8I499-16S i 8215-61 i

95.88 1

•9/(9 1

i

list J 1

UJ 1

2.3 J i

4.9 i

t.73 fl 1

51.3 fl i

6.7 3 i

3581 J 1

1.8 i

91.9 J i

31.2 J 1

1 i

K i

129 fl i

3.B J 1

4.5 J i

K 1

,. t

KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since

it was detected in a blank at a siiilar level, fl Unreliable result - Analyte u y or lay not be present

in thie saiple. J Quantitation is approxiiate due to liiitations identified

during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation iiilt

is probably higher due to low bias identified during the quality assurance review,

(ix) This elHent was not analyzed for and not detected; however, due to saiple dilutions, the reported detection liiit is equal to the 'norial' detection liiit lultiplied by the factor in parentheses.

AKAlfTICAl HETHOD: P - Inductively Coupled Plasu F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer

CO. o-o CO

m - i< - (i. ..lilRESui.. ''Al

Ansonlnviromental Saipie Huiber laboratory Saiple Huiber

,,. , Reurks

lUnits

1 IHORGAKIC ElEKEKTS

1 1 1 lAluiinui P 1 1 [Antiiony P 1 1 lArsenic F 1 ••

IBariui P 1 1 IBerylliui P 1 1 iCadiiui P 1 1 ICalciui P 1 IChroiiui P 1

1 ICobalt P 1 1 ICopper P 1 [Iron P 1

1 Ilead F/ 1 1 iRagnesiui P 1 1 IKanganese P 1 1 IKercury t \ 1 1 IKlckel P

1 iPotassiui P ISeleniui F 1

1 Silver P

Sodiui P

ThalUui F

Vanadiui P

Zinc P

Cyanide A

i Detection iliiit (Aq)

i 23.1

i 32.1

i <•*

1 S.t

1 1-*

1 *•'

i 77.1

i S.t

1 17.t

1 16.8

1 95.8

1 1.8/111

1 118

1 2.8

1 8.28

1 27.8

1 Bit

1 S.t

1 '•'

1 118

1 !•*

i M

i 12.8

S 16.8

•1


4.6

6.4

t.Bt

l.t

t.2t

8.88

15.4

1.8

3.4

3.2

19.8

8.28/22.2

23.6

8.48

8.16

5.4

162

1.8

1.4

23.6

8.28

1.4

2.4

2.3

I soiL..... JI

DUI6 38'-32' 88499-17S 8215-12

96.18

•g/Kg

1578 3

UJ

1.1 J

8.5

8.42 R

163 3

7.6 J

2.4 J

2628 J

6.7

255 J

52.1 J

R

147

R

184 J

3.8 J

18.5 3

fl

TED U .. .... 'i

DUI7 4l'-42' 11499-195 8224-81

95.B8

ig/Kg

1848 J

UJ

8.98 J

8.4

8.46 fl

38.2 R

3.7 R

2798 J

1.8

129 J

21.2 J

R

'

R

88.8 J

2.8 J

S.B J

B

s! i EIGHT'.™... =

0UI7 45'-47' 86499-285 8224-82

97.48

ig/Kg

1688 J

UJ

1.3 J

7.8

6.59 R

37.7 8

3.5 B

2748 J

8.7B

85.9 J

38.3 3

R

R

94.1 J

UJ

2.7 J

3.3 J

fl

\

m i 55'-57' II499-21S 8224-83

84.68

ig/Kg

878 J

UJ

8.96 J

7.3

8.51 8

39.9 R

3.2 R

2528 J

8.84

118 J

1B.9 J

R

R

8B.3 J

2.2 J

3.2 3

R

- p a g ' l ^ l

DUI7A 45'-47'| 88499-22S i 8224-84 i

97.48 1

•9/l!9 1

Duplicate of | DUI7(45'-47')i

655 J i

UJ i

1.7 J 1

6.4 1

8.46 fl 1

37.4 R 1

2.9 R i

2488 J i

1.8 i

51.1 J 1

14.9 J 1

fl i

R 1

87.9 J i

2.8 J 1

3.2 3 1

> 1 1

KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since

it was detected in a blank at a siiilar level, fl Unreliable result - Analyte lay or u y not be present

in this.saiple. J Quantitation is approxiute due to liiitations identified

during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation lliit

is probably higher due to low bias identified during the quality assurance review.

(Ix) This eleient was not analyzed for and not detected; however, due to saiple dilutions, the reported detection lliit is equal to the 'norial' detection liiit lultiplied by the factor in parentheses.

AKAlYTICAl HETHOD: P - Inductively Coupled Plasu F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer

1 . _ ^ . — . 1 ^ ^ ^ lAHAlYTI, lUlTS -\ .\

iAns^^mroniental Saiple Kuiber i TAKK 16 i {laboratory Saipie Huiber i 911312-tl i

1 Reurks | | 1.,. I t 1 1 1 lUnits 1 ug/l | 1 ,, j 1 ioRGAKIC ElEKEKTS i i 1 1 1

IBenzene | 7 U | 1 1 1 1 I I ICarbon Tetrachloride | 6 U | 1 1 1 1 1 1 IChlorobenzene | 7 U | 1 1 1 1 1 1 IChlorofori 1 S U | 1 .... 1 ..1 1 1 1 |l,2-0ichioroethane | 6 U | 1 1 1 1 1 1 |l,l-Dichloroethylene 1 S U | 1 1 1 1 1 1 iKetbylethylketone | 12 U | I 1 1 •• 1 1

1Tetrachloroethylene | 6 U |

1 r 1 ITrichloroethylene | 6 U |

1 1 1 1 Ivinyl Chloride | 11 U | I 1 . i 1 1 1 jPyridine | 2368 U | 1 .... 1 i 1 1 IDate Saiple Collected | 6/11/91 |

IDate leachate Generated i 6/1B/91 i 1 ..,. 1 ..1 lOate leachate Analyzed i 6/26/91 |

KOTES: - Coipound was not detected. U This coipound was analyzed for but was not detected at or above

the level indicated. R Unreliable result - Coipound u y or lay not be present in this saiple. 3 Quantitation is approxiute due to liiitations identified during

the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation iiiit is

probably higher due to low bias during the quality assurance review.

The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.

CO o o CO

1 1 iTEHTATIVEir IDEKTIFIED COHPOUHOS |

1 lAnson Environiental Saiple Huiber | TAKK 16 | ilaboratory Saiple Kuiber i 911312-11 i

iunits i ug/l i 1 I 1 1 1 1 {Unknown | 8 J | 1 > , .. 1 1 1 ••! {Acetone { 318 R {

inethylent Chloride i 211 J { 1 1 1

j o R l ^ H l l Y S I S - AKAlYTICAl RESUIT

1 Anson Environiental Saipie Huiber {laboratory Saiple Kuiber

{Reurks 1 1 {Units

isEKIVOlATIlE ElEKEHTS

1 1 1 {2,4-Oinitrotoluene 1,. . , . 1 {Hexachlorobenzene 1 . . 1 ' ' {Hexachloro-1,3-butadiene 1 1 {Hexachloroethane

1 {nitrobenzene

{1,4-Dichiorobenzene 1 1 {Kethylphenols (total)

{Pentachlorophenol

{2,4,5-Trichlorophenol

i2,4,6-Trichiorophenol

{Date Saiple Collected 1 ioate leachate 6enerated

1 {Date leachate Extracted 1 1 {Date leachate Analyzed

~-i l-\ S -page 2 {

TAKK 16 { 911312-11 i

ug/l {

i

52 U {

46 U i

46 U 1

59 U 1

38 0 {

52 U {

52 U {

268 0 1

278 U 1

53 U 1

6/11/91 {

6/17/91 {

6/18/91 {

6/28/91 {

KOTES: - Coipound was not detected. 0 This coipound was analyzed for but was not detected at or above

the level indicated. R Unreliable result - Coipound u y or u y not be present in this saiple. J Quantitation is approxiute due to liiitations identified during

the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is



CO o o CO >£» CO

\ ^ ' ' ' I D R G A U V F Y S I S - AKAlYTICAl RESUIT

[Anson Environiental Saiple Kuiber {laboratory Saiple Kuiber

{Reurks

lUnits

ORGAKOCHlOfllHE PESTICIDES

jgaMa-BHC

1 [Heptachlor IHeptachlor Epoxide

1Endrin

IHethoxychlor

IToxaphene

Chlordane

Date Saiple Collected

Date leachate Generated

IDate leachate Extracted

Date Extract Analyzed

f„:P'9'.3 —

TAKK 16 918312-11

ug/l

t.210

t.l7 U

1.17 U

8.33 U

8.19 U

3.3 U

8.16 U

S/11/91

? 1

6/18/91 1

6/21/91 1

1


the level indicated. R Unreliable result - Coipound u f or u y not be present in this saiple. J Quantitation Is approxiiate due to liiitations identified during

the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is



CO

o CO

1

, . . . J ^ ^ . . . . . UKAIYTL .JUIT l- P lAnsonrnvironiental Saiple Nuiber {laboratory Saiple Nuiber 1 1 {Reurks 1 1 {Units 1 1 {HERBICIDES

1 1 12.4-0 1 1 12.4.5-TP (Silvex)

ioate Saiple Collected

{Date leachate 6enerated 1 1 {Date leachate Extracted 1 1 {Date Extract Analyzed

1

•V-,- • ' i

TAKK 16 i 918312-81 1

ug/l 1

i

148 UB 1

58 UR i

6/11/91 1

6/2B/91 1

7/2/91 1

7/9/91 {


the level indicated, fl Unreliable result - Coipound u y or •ay not be present in this sample. J Quantitation is approxiute due to ILeitations identified during

the quality assurance review (data validation). UJ This compound was not detected, but the quantitation ii^lt is

probably higher due to low bias during the quality assurance review. Ufl This coipound was analyzed for but was not detected; however.

the analysis was deeied unreliable.


CO

o CO •Cke

1 ^ ^ w • AHAlniinL JlESUlTS' -page's

i_ 1

{Anson Environiental Sample ilaboratory Saiple Kuiber 1

1 1 Kuiber { TAKK 16 {

i 918312-81 j 1 1

1 I I {Reurks | | 1 1 1 1 {Units

{TCIP HETAIS

1 1 1 lA i t tn l t 1 1 {Bariui 1 1 {Cadiiua

{Chroaiu^ 1 1 {lead 1 1 {Hercury 1 1 ISeleniui

1 {Silver 1

1 1 1 u g / l {

i {

1 »t 1 \

{ 2 8 1 {

1 16U 1

{ 18U (

1 1)1 u i

{ 1.8 U {

i 388 U i

i 28U { _ 1

1 1 {CHACTERISTICS i 1 1 1 1 {Flashpoint (at 288 1 1 IpH 1 1 {Reactive Cyanide 1 1 '• {fleactive Sulfide 1

f; 1 1

1 Ko (

1 ' • * 2 1

i S88 u i

1 21110 1


the level Micatel. R Unreliable result - Coipound u y or •ay not be present in this sample. J Quantitation is approxiiate due to liiitations Identified during , the quality assurance review (data validation).

UJ This coipound was not detected, but the quantitation iiiit is probably higher due to low bias during the quality assurance review.


CO o o CO ^

Validated Data

Indoor borings 5 & 6 Re-sampling drywells 1-4

30034?

CO o o CO • ( ^ CO

H i f e ^ --"S'S ' ..'nCAl Ri.vL, J - Air'miu^'REPORTEU 08 A DRY U E l k BASIS ' ^ ^ B -page 1 |

{Anson E l S w e n t a l Saiple Kumber ilB 15 (15-17') ilB 15 (35-37') {iB 16 (31-32') ilB 16 (48-42') { Field Blanks { Field Blanks { Trip Blank { 'laboratory Saaple Kuiber i 12868-84 i 12168-85 i 12168-11 | 12861-12 | 12161-13 i 12861-86 { 12168-17 i f ., ,, , . . . . 1 1 ,1, 1 t 1 I . I

{Reurks { 1 1 1 i Field Blank j Field Blank { Trip Blank {

1 • " ' 1 1 1 ' ' 1 • - | — — " 1 — - 1 — —1 {Units 1 ug/Kg { ug/Kg { ug/Kg { ug/Kg j ug/l | ug/l { ug/l |

ivOLATIlE COHPOUHOS {Quantitation {Quantitationl 1 1 1 1 { i {

{ j l i i i t (Aq) j l i l i t (Sol) j i { i ' i i 1 1

ithloroiethane j I t j I t | i j i ~ i 1 1 {

{Broioiethane { I t { I t { { { { { { | |

{Vinyl Chloride { 18 | 18 { | | { { | { {

{Chloroethane { 18 { 18 { UJ { UJ { UJ | UJ { { | {

{Kethylene Chloride { 5 { 5 j 6 U { 6 U { 5 U j S U { 3 J i 4 J { 4 J {

iAcetone j 11 i I t j 118 U j 118 U j 19 U { 12 U i 9 J i 31 J { 34 J | 1 1 1 j 1 1 1 1 1 1 1 {Carbon Disulfide { 5 | 5 | { | { 1 . j 1 i

{1.1-Dichloroethene | 5 | 5 | | { | | j |

il.l-Oichloroethane j 5 { 5 i j { { j j j 1 I . . . . . . . . 1 | . . 1 . . . I . . 1 , 1 1 — — | . . 1 1 1 1 . | - . . | —1 . . . | {Total 1.2-Oichloroethene { 5 | 5 { { { { { { |

{thlorofori { 5 i 5 i j i j 15 i 15 { {

il.2-Dichloroethane { 5 j 5 j i j { i { {

1 — "" 1 1 1 1 1 ' ' ~l 1 1 1 {2-Butanone { 18 | 18 { { | | { { |

il.l.l-Trichioroethane { 5 j 5 j i j j { j j 1 . 1 - - - - , . - , 1 , -• 1 - - 1 t 1 1 1 1 1 1 1 1 1 1- 1 1 {Carbon Tetrachloride { 5 { 5 { | { | { { {

1 "" " I I I I I 1 1 { 1 {Vinyl Acetate { 18 { 18 | { | | { { {

. . „ 1 1 {Bro^odichioroiethane { S { 5 { | | { j j j

il,1.2.2-Tetrachloroethane ) 5 { 5 i j j j { { { 1 1 1 1 1 1 . I I I I 1 1 1 1 1 1 1 1 1 . . . 1 |l,2-Dlchloropropane | 5 { 5 { { | | { | |

{trans-l.S-Oichioropropene { 5 { 5 { j | j i i j 1 1 j . 1 1 1 1 1 1 {Trichloroetheas j 5 { 5 { { { j j j j

. 1 . , ^ , 1 . . - — . 1 1 1 1

'Dibroiochloroiethane { 5 { 5 { { | { | | j

|l,l,2-Trichioroethane { 5 { 5 { | { { | j j

{Benzene | 6 { 5 { j { | { { {

I. h

KOTES: Coipound uas not detected.

U This coipound should be considered 'not-detected' since it was detected in a blank at a siiilar level.

R Unreliable result - Coipound iay or lay not be present in this saiple.

J Quantitation is approxiiate due to liiitations Identified during the quality assurance review (data validation).

UJ This coipound was not detected, but the quantitation liiit is probably higher due to a lou bias identified during the quality assurance review.

|.L VOIATIIE i nBK AKAIYSIS - AKAlYTICAl RESUITS - All SOIIOS REPORTED ON A DRV UEIGHT BASIS -page 2

1 1 1 1 1 1 1 1 1 {Anson Environiental Saiple Kuiber {IB IS (15-17') {IB 15 (35-37') {IB 16 (38-32') {IB 16 (48-42') { Field Blanks { Field Blanks { Tr ip Blank {

{ laboratory Saiple Kuober { 12868-84 j 12868-65 j 12868-11 j 12868-62 j 12868-83 j 12868-16 i 12861-17 i

{Reurks { I I I I F ie ld Blank { Field Blank { Tr ip Blank {

i un i t s i ug/Kg { ug/Kg { ug/Kg j ug/Kg j u g / l j ug / l { ug / l {

ivOlATIlE COHPOUHOS iouan t i t a t i on JQuanti tat ionj i { i i i { {

i i l i i i t (Aq) i l i i i t (Sol) i { 1 i i i { { | - l i i i l i l l l i {c is- l ,3-Dichloropropene | 5 { 5 { { { { { | { { 1 1 . ' . . _ i . 1 . . . 1 __ 1 1 _ _i 1 . 1 __i 1— 1 1 1 1 1 1 1 — 1 1 — 1 {B ro io fo r i { 5 { 5 { { | { { { { { I 1 . „ i 1 1 1 1 1 1 1 . . . . , 1 1 1 1 1 ..|.. 1 | - 1 1 1 1 {2-Hexanone { 18 { 18 { { | { { { | {

| . . . . . — ] . - — . 1 - 1 1 I I I I 1 1 {4-Kethyl-2-Pentanone { 16 { 16 { { | { { { { {

{Tetrachloroethene { 5 { 5 { | | | { { { {

{Toluene { S { 5 { | { { { { { {

{Chlorobenzene { 5 { 5 { | { { { { { {

{Ethylbenzene { 5 j 5 j j j i i { i i

{Styrene { 5 j 5 i ' j { i i { i j

i l o t a i Xylenes j 5 i 5 { j j { j j { j 1 1 , 1 1 , , 1 , 1 1 1 1 1 , 1 1 1 1 - " — -| 1 1 r - - | 1 - 1 { { { 1 1 1 1 1 1 {Quanti tat ion l i i i t K u l t i p i i e r { 1.2 { 1.2 { 1.8 { l . t { l . t { 1.8 | 1.6 {

{Date of Saiple Co l lec t ion i 12/8/91 i 12/B/91 i 12/7/91 i 12/7/91 ' i 12/7/91 i 12/8/91 i ' HA i

{Date Saipie Received by laboratory | 12/18/91 | 12/18/91 | 12/11/91 | 12/18/91 | 12/11/91 | 12/11/91 | 12/11/91 {

1 - - 1 1 1 1 1 1 r 1 {Date of Saiple Analysis I 12/17/91 { 12/17/91 { 12/17/91 { 12/17/91 { 12/18/91 { 12/18/91 { 12/18/91 {

{ Ins t ru ien t Used for Analysis { GC/HS-5995A { GC/HS-5995A j GC/KS-5995A { GC/NS-5995A { GC/KS-5995A { GC/NS-5995A { GC/KS-5995A { 1 1 1... 1 1 1 1 1 1

BOTES: Coipound was not detected.

U This coipound should he considered 'not-detected' since it was detected in a blank at a siiilar level.

R Unreliable result - Coipound lay or may not be present in this saipie.

J Quantitation is approxiiate due to liiitations identified during the quality assurance review (data validation).

UJ This coipound uas not detected, but the quantitation liiit is probably higher due to a low bias identified during the quality assurance review.

CO;

CO

o o CO C l

o

{EXTRACTABIE 0R6AKIC AKAIYSIS - AKAlYTICAl RESUITS - All SOIIDS REPORTED OK A DRY UEIGHT BASIS

iAnson Environiental Saiple Huiber (IB 15 (15-17') (IB 15 (35-37') ilB 16 (31-32') ilB 16 (48-42') jlahoratory Saiple Kuiber ( 12868-84 | 12868-85 | 12866-11 j 12868-12 1 . . . . . 1 . 1. 1 . , 1 , 1 1 1 1 ~ — 1 (Reurks I I I I

{Units 1 ug/Kg { ug/Xg | ug/Kg | ug/Kg 1 . . . . ! . , . . 1 . . 1 . .1 1 1. 1 .- — — . . | . - . . — 1 . - | . . | 1 — | . ISEKIVOIATIIE COHPOUHOS IQuantltation {Quantitation! { { { j j l i ^ i t (Aq) ( l i i i t (Sol) { i ( j 1 1 1 1 1 1 1 IPhenol ( 18 ( 338 { { | ( i._ . . 1 . .1 1 1 1 1 1 1 1 1 1 1 1 |bis(2-Chloroethyl)ether { 18 ( 331 { | ( (

(2-Chloropbenol | 18 | 338 | | | ( 1. 1 ..1 1 1 .1 _

1 1 1 1 1 1 — 1 (1,3-Oichlorobenzene | 18 ( 338 ( ( ( (

(1,4-Oichlorobenzene | 11 j 331 j | | { i „ , . . . 1 . .1 . , 1 . . , . 1 1 .1 1 1 1 1 — 1 1 1 — {Benzyl Alcohol | I t { 331 { { { { 1 . , . . . .1 1 1 1 , 1 . . 1 1 1 1 1. 1 1 1 {1,2-Dichlorobenzene | I t | 331 | { | ( i „ .1 .1 .1 .1 1 .1 1— 1 1 1 1 1 1 |2-Nethylphenol ( I t { 331 { { | | 1 . , . . . 1 1 1 . ) 1 1 1 1 1 1 1 1 1 {bis(2-ChIoroisopropyl)ether | I t | 33t | ( { { I . . . . . . . 1 1 . 1 . 1 1 . . 1 ; . . . . 1 — 1 1 1 1 1 1 (.. Jiyipbenol { I t | 331 { | ( | 1 . . . . . . - j . . | 1 - : 1 I -1 (H-Nitroso-di-n-Propylaiine i I t | 331 | j j • j 1 ,1 1. . 1 1 1 1 . 1— . | - | . . — 1 1 . 1 . | (Hexachloroethane | I t ( 33t ( | ( (

initrobenzene i It j 331 j i j i 1 1 1 1 1 1 1 1— 1 1 1 1 1 {Uophorou [ I t { 331 { ( { ( 1 1 - 1 1 1 1 1 1 1 1 1 1 1 1 (2-Hitrophenol { It { 331 ( | ( {

i2,4-Diicthylphenol { It ( 331 i ( j i 1„ . , 1 1 1 1 . . . .1 1 | . . . . 1 1 1. 1 . 1 . | (Benzoic Acid { St ( 16S6 ( I I I 1 t 1 1 1 1 1 1 1 1 1 1 1 1 |bis(2-ChloroeChoKy)iethane | 11 { 331 | { ( ( 1 1 1 . 1 1 1 1

|2,4-Dichlorophinol ( 18 { 331 { ( { { ) _ ^ 1 I 1 1 . 1 1 1 " 1 1 1 1 1 1 (1,2,4-Trichiorobenzene { It ( 33t { { { (

(Naphthalene ( I t j 33t j ( | { 1 . , 1.. ..1 1 1 1 1 1 1 1 1 1 1 1 {4~Chloroaniiine { I t ( 331 ( { { { { 1 1 1 1 .1 .1 1 1 1 1 1 1 1 1 1 (HtMchlorobutadiene ( 11 ( 331 | { { {

|4-ciiIoro-3-Nethyipiienoi I 11 | 338 | | | j

jz-Hethyinaphthaiene { It { 331 j { ( j 1 1.. . . | 1 1

'^k •

Field Blanks 12168-13

Field Blank

ug/l

i .-. .

-page 3 |

Field Blanks | Trip Blank {

12861-16 { 12868-17 i

Field Blank { Trip Blank (

ug/l ( NA {

1 ** 1

i *' i i ** i i "* i 1 '* {

i NA {1

i K* [ i

i <* |li

1 ** 1

1 ** i

1 ** 1

i "* i i K* i

i >* i i 1* i

1 «* 1

1 ** 1

i <* i i Kl i

1 "* (

i HA i

i K* i

i ** ( 1 KA 1

i KA i

NOTES:

Compound was not detected.

This coipound should be considered 'not-detected' since

it was detected in a blank at a siiilar level.

Unreliable result - Coipound lay or lay not be present

in this sample.

Quantitation is approxiute due to lUitations identified

during the quality assurance review (data validation).

UJ This compound was not detected, but the quantitation

liiit is probably higher due to a low bias identified

during the quality assurance review.

NA Not analyzed.

-•• i & --i ' 5 ^ k - - !• ~ EXTRACTABIE O f l d ^ H l T S I S - AKAlYTICAl RESUITS - All SOIIOS REPOBTEO OH A DRY UEIGHT 8ASIS ^ B -page 4

iAnson Environiental Saiple Kuiber (IB IS (15-17') (18 15 (35-37') (IB 16 (31-32') (IB 16 (41-42') ( Field Blanks j Field Blanks j Trip Blank

ilaboratory Saiple Kuiber i 12868-84 ( 12868-85 j 12868-81 ( 12868-12 j 12866-13 i 12868-66 i 12868-87

{>.. .,ks ( { { { ( Field Blank ( Field Blank ( Trip Blank

1 • " • • 1 1 1 1 1 1 1 (Units { ug/Kg ( ug/Kg ( ug/Kg ( ug/Kg { ug/l { ug/l { KA

isEKIVOlATIlE COKPOUKOS iouantitation (Quantitationj 1 1 i i i i i ( liiit (Aq) (lliit (Sol) { ( ( { ( i i

iHexachlorocyclopentadiene ( 18 ( 336 ( ( ( ( i i ( H A

(2,4.6-Trichlorophenol ( 18 ( 338 { ( ( ( ( { ( H A

1 - ~ ~ l — "1" 1 1 1 1 1 1 1 (2,4.5-Trichlorophenol ( 5 8 { 1658 ( ( { ( { { ( H A 1. 1 .. 1 .. .1.. . . 1 1 1 1.. .. 1 — 1 1 1 1 1 1 1 1 1 (2-Chioronaphthalene { 18 { 338 ( { { { { ( ( H A

(2-Kitroanliine { 58 ( 1658 { { { { { ( ( H A 1 _ 1 ...|__ 1. ( { { { {

(Oiiethylphthaiate { 18 ( 338 { { ( { ( ( ( KA

(Acenaphthylene { 18 ( 338 { { { { ( ( ( H A 1 1 .1 I-. . 1 1 I-- 1 1 1 1 1 1 • •-- 1 . . 1 . 1 | . 1 . 1 1 |_ 1

(3-Kitroaniline { 58 ( 1658 { { { ( ( ( ( H A

(Acenaphthene { 18 ( 338 { ( ( { - ( i i KA

1 -initrophenol { 58 ( 1658 { ( ( { ( ( ( KA

i4-Kitrophenol { 58 ( 1658 { ( ( { i { i KA

(Dibenzofuran ( 16 ( 336 { ( ( { ( ( ( KA

i2.4-Dinitrotoluene i 18 ( 338 { { ( { i { j KA

i2.6-Oinitrotoluene { 18 ( 338 ( ( ( ( { { ( H A

1" ~1 " 1— " " 1 1""" 1 1 1 1 1 1 (Diethylphthalate { 18 ( 338 ( ( ( ( { { ( H A

i4-Chlorophenylphenylether { 18 ( 338 ( ( ( ( { { i HA 1 I I I I 1 ™ -1- 1 - — 1 — — -1 . _ _l

(Fluorene ( 18 { 338 { { { { ( ( ( HA |

(4-Kitroaniiine ( 58 ( 1658 ( ( { { ( { ( H A

{4,6-0initro-2-HeChylphenol { 58 { 1658 ( ( ( ( { { { KA

(K-Hitrosodiphenylaiine { 18 { 336 ( ( i i { i i KA

(4-Broiophenylphenylether ( 18 ( 338 { ( { ( ( ( ( KA

(Hexachlorobenzene ( 18 ( 336 { { ( ( ( ( ( KA 1 1 1 I 1 .1 1 .

(P....achlorophenol ( 58 ( 1658 { i { i ( i i KA

Phenanthrene 18 338 1 KA

i;.

KOTES:

- Coipound was not detected.

U This coipound should be considered 'not-detected' since

it was detected in a blank at a siiilar level.

B Unreliable result - Coipound u y or u y not be present

in this saipie.

J Quantitation is approxiute due to liiitations identified

during the quality assurance review (data validation).

UJ This coipound was not detected, but the quantitation

liiit is probably higher due to a low bias identified


HA Hot analyzed.

^ ^ .J^ l u m a m i W K u AKAIYSIS - AKAIYTICAI RESUITS - A H soiios REPORTED OK A DRY UEISHT BASIS ^ ^ -page s (

.. 1 1 |.. 1 1 _ 1 1 JAnson Environiental Sample Kuiber (IB 15 (15-17') jlB IS (35-37') {iS 16 (38-32') {IB 16 (41-42') | Field Blanks i Field Blanks i Trip Blank i llaboratory Saiple Kuiber i 12868-84 j 12868-65 i 12868-81 j 12868-62 i 12868-83 { 12868-86 j 12661-17 j

ifleurks i i { i i Field Slank i Field Blank { Trip Blank {

{Units i ug/Kg i ug/Kg i ug/Kg j ug/Kg { ug/l i ug/l j KA j

isEHIVOlATIlE COKPOUKOS iQuantltation (Quantitationi i { i i i i i i i liiit (Aq) jlilit (Sol) i j i ( i { { i

iAnthracene { 11 { 331 { j i i j i ( KA {

ioi-n-Butylphthalate j 11 j 331 i ( \ \ \ \ j KA {

(Fiuoranthene j It i 331 j j j { j { { KA j

(Pyrene { 11 { 331 { ( ( { { { { HA { 1 . . 1 1 |_ 1 j 1 j 1 1 . .. t

jsutylbenzylphthaiate j 11 { 331 j j j | j j { NA j 1 • 1 |- t • • 1 • I - - |-- - • •• 1 •• '

{3.3'-Dichlorobenzidine j 21 j 666 j j { j { j j HA j

{Benzo(a)anthracene { tt { 331 { { { { { j ( KA {

(bis(2-Ethylhexyl)phthalate { 11 { 331 { { 131 J ( { 411 ( { { HA {

jchrysene i 11 j 338 i { i { { \ { NA i

joi-n-Octylphthalate i 18 j 338 i i j { j \ { HA { !-- I l l 1 1 1 1 1 I I 1 1 1 1 1 1 • 1 1 {Benzo(b)fiuoranthene { 18 ( 338 { ( { { ( { { KA - {

(Benzo(k)fluoranthene { 18 ( 338 { { { { - { ( { HA {

|8enzo(a)pyrene { 18 { 338 { { ( { { ( ( NA { •• { • " { " {

ilndeno(l,2.3-cd)pyrene j 18 { 338 i i { j { { j HA {

{Oibenz(a,h)anthracene j 18 i 338 j { { { j ( ( KA {

{Benzo(g,h.i)perylene { 18 { 338 { { ( { { ( ( NA {

1 1 1 { 1 1 { { { (Quantitation liiit Kultipiier ( 1.18 { I.IB { 1.83 ( 1.83 { 1.88 { 1.86 { KA {

(Date of Saiple Collection { 12/8/91 ( 12/8/91 { 12/7/91 { 12/7/91 { 12/7/91 { 12/8/91 { KA ( 1 _ 1 1 1 ( 1 _ .. 1

1 1 1 1 1 1 1 1 1 (Date Saipie Received by laboratory { 12/11/91 ( 12/16/91 { 12/18/91 { 12/16/91 ( 12/18/91 { 12/18/91 ( NA (

(Date Saiple Extracted { 12/11/91 { 12/11/91 ( 12/11/91 { 12/11/91 { 12/18/91 ( 12/18/91 { KA {

ioate of Saiple Analysis i 12/16/91 i 12/16/91 i 12/16/91 i 12/16/91 i 12/16/91 { 12/16/91 i U \ 1 1 1 1 1 1

(Instruient Used for Analysis { GC/KS-5995B { 6C/KS-5995B { 6C/KS-5995B { 6C/KS-5995B { 6C/HS-5995B ( 6C/KS-5995B ( KA {

KOTES: - Coipound uas not detected. U This coipound should be considered 'not-detected' since

it was detected in a blank at a siiiiar level. R Unreliable result - Coipound u y or lay not be present

in this saiple. J Quantitation is approxiiate due to liiitations identified

during the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation

liiit is probably higher due to a low bias identified during the quality assurance review.

KA Hot analyzed.

ic iP - I £mTTVFiv , i i ) £ | ( i l f j ' " "•."OUKOS r . "•STIKATEI] . ,RATI0K1 i; SOlIOt , , . , ; . > ; E 0 ONfc^mr » U 5 H I B A b ^ ^ B -page 6

( A n s i f l ^ P l n i e n t a l Saiple Kuiber (IS 15 (15-17 ' ) (IB 15 (35-37 ' ) (IB 16 (31-32 ' ) {IB 16 (48-42 ' ) { Field Blanks | Field Blanks | Trip Blank ( ( l abora tory Saiple Nuiber j 12668-14 j 12861-65 j 12868-81 ( 12868-12 i 12861-83 j 12868-86 j 12861-17 j

i f l e u r k s i 1 i i i Field Blank j Field Blank \ Trip Blank j

j u n i t s j ug/Xg j ug/Kg { ug/Xg { ug/Kg j ug/L j ug/ l j ug/L i

icOKPOUNOS i i { i i { 1 1 1 1 1 1 1 1 1 1 1

(VOIATIIE COKPOKEKTS 1 - 1 - 1 - 1 - 1 - 1 - I - I 1 1 . 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

(SEKIVOIATIIE COKPOKEKTS { { | ( 1 - 1 - { KA ( 1 . 1 . 1 1 1 l i l t

1 1 1 1 1 1 1 i 1 ( l abora to ry Ar t i f ac t s (Aldols , e t c . ) { 4688 R { 5811 R ( 4111 R | 4588 R ( | | (

(Unknown ( ( 428 J | ( ( { | { 1 ( 1 1 1 1 .. 1 1 1

KOTES: - Coipound was not detected. U This coipound should be considered 'not-detected' since

it was detected in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present



liiit is probably higher due to a low bias identified during the quality assurance review. Hot analyzed. HA

CO o o CO

CO o o CO Ul

• J i iORGAHi; i lS - ; [ A l RESi i A l l Sli lORTED 1 . [ UEIGHll . ' S f ^ ^ ! « i i ! -pagii.

n R i Env i ron ienta l Saiple Kuiber i lB 15 (15-17 ' ) j l B IS (35-37 ' ) (IB 16 (38-32') j lB 1 ^ 4 1 - 4 2 ' ) i F ie ld Blanks ( F ie ld Blanks ( Trip Blank ( l labora tory Saiple Nuiber i 12161-14 j 12661-85 i 12161-81 j 12168-82 j 12868-83 j 12 t6 t - t 6 j 12661-17 j

1 1 1 1 1 ' 1 1 '1 1 (Reurks ( { { { { F ie ld Blank { F ie ld Blank { Trip Blank {

jUni ts i ug/Kg { ug/Kg { ug/Kg { ug/Kg | ug / l { u g / l | KA j

jpes t ic ides JQuant i ta t ion JQuant i ta t ion j i J J { j j i j j l i i i t (Aq) j l i l i t (Sol) { j { i { i j j

1 1 1 1 1 1 1 1 1 .| -. 1 (alpha-BHC ( t . t S { 8 { { { { ( { { KA {

jbeta-BHC j 8.85 j 8 j { j j j j { NA j

jdelta-BHC i 8.85 j 8 j j j j { j j HA j

(gaina-BHC ( l indane) j 8.85 i B j j i j j j j KA j

JHeptachlor i 8.15 i 8 j i j j i j j NA j

(A ld r in { 8.85 { 8 { { { { { { { NA {

| . 1 1 1 —1 1 1 1 |— 1 1 (Heptachlor Epoxide { 8.85 { 3 { { ( { { ( { KA (

(Endosulfan I { 8.85 { 8 ( ( { { { { { NA {

{D ie ld r i n { 8.18 ( 16 { { { { | { { NA (

i ( . ( ' -ODE i 8.18 i 16 j j { j j { { HA i 1 . . . • _

(Endrin { 8.18 { 16 ( { ( { { ( ( KA {

iEndosulfan I I { t . l t j 16 j i i j ( j j NA {

{4.4'-DDD i t . l t { 16 i i i { ' i i i NA i

JEndosulfan Sul fate ( t . l t ( 16 { ( { { { ( { NA (

i4,4'-OOT i 8.18 i 16 i i i i i i { HA i 1 1 , 1 .1 1 . . ,1 ,, ,, 1 1 1 ,1 1 1 - 1 1 1 1 I I • . |.. 1 ..|... 1 (Nethoxychior ( 8.58 ( 8 { ( { { { ( ( HA {

(Endrin Ketone { 8.18 ( 16 { { ( ( { { ( NA {

(aipha-Chlordane { 8.51 ( 86 { { ( { { { ( NA ( 1 1 1 ~l 1 1 1 1 1 1 1 (gama-Chiordane ( 8.58 { 88 ( { { { { { { NA (

{Toxaphene { l.t { 161 { ( ( { { ( { NA {

NOTES: - Coipound uas not detected. U This coipound should be considered "not-detected* since

it uas detected in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present



iiiit is probably higher due to a low bias identified during the quality assurance review.

HA Hot analyzed.

El^^H ( E l ^ ^ K QRGAKIC AKAIYSIS - AKAlYTICAl RESUITS - All SOIIDS REPORTED OH A DRY UEIGHT BASIS -page I

(Anson Environiental Saiple Huiber (IB IS (15-17') ilB 15 (35-37') ilB 16 (31-32'j (IB 16 (48-42') { Field Blanks | Field Blanks { Trip Blank i

(laboratory Saipie Huiber j 12861-14 j 12868-15 j 12861-11 j 12168-82 j 12861-83 j 12868-86 ( 12868-67 j

{Reurks i i i i 1 Field Blank | Field Blank j Trip Blank j

jUnits 1 ug/Kg | ug/Xg | ug/Kg | ug/Xg ( ug/l ( ug/l ( KA j

(PCBs (Quantitation (Quantitation( | 1 1 1 i 1 j

j { liiit (Aq) (liiit (Sol) j { { i ( i j i

JAroclor-lBlB { 8.5 j 88 j { ( { j j ( HA i

{Aroclor-1221 j 8.5 j 86 j { ( j j j ( KA j

(Aroclor-1232 j 8.5 j 88 j ( j { j j ( NA j

iArocior-1242 j 8.5 j 88 ( j j ( j ( j HA j

(Aroclor-1248 ( 8.5 { 88 { { { { | ( { NA |

(Aroclor-1254 ( 1.8 { 168 { { { { { { | NA (

iAroclor-1261 { 1.8 ( 168 ( { j ( j j j KA j

(Quantitation liiit Nultiplier { 1.16 { 1.16 { 1.81 j 1.83 j 1.82 \ 1.82 i HA i

(Date of Saiple Collection { 12/8/91 { 12/8/91 ( 12/7/91 ( 12/7/91 { 12/7/91 { 12/8/91 ( NA (

(Date Saipie Received by labcratory { 12/18/91 { 12/18/91 { 12/16/91 ( 12/16/91 { 12/18/91 { 12/16/91 ( NA {

(Date Saiple Extracted { 12/11/91 i 12/11/91 i 12/11/91 i 12/11/91 i 12/18/91 { 12/18/91 i KA {

(Date of Saiple Analysis { 12/14/91 j 12/13/91 j 12/13/91 j 12/13/91 j 12/13/91 j 12/13/91 j KA j

KOTES:

- Coipound uas not detected.

U This coipound should be considered 'not-detected' since

it uas detected in a blank at a siiilar level.

R Unreliable result - Coipound lay or lay not be present

in this saipie.

J Quantitation is approxiiate due to liiitations identified

during the quality assurance revieu (data validation).

UJ This coipound uas not detected, but the quantitation

iliit is probably higher due to a low bias identified


HA Hot analyzed.

CO

o CO Ul

B. INORGANIC DATA

300356

CO

o CO

'•j^^^ i ANAl: buiTsi' . ISOLI

j Anson E ^ W n i e n t a l Saiple Nuiber (laboratory Saiple Nuaber

(Percent Solids

junits

(INORGANIC ElENENTS ( Detection 1 { Uiit (Ag) 1 1 . .

(Aluiinui P ( 72.8 I . . , .. .. . 1

(Antiisny P { 45.1 1. .. .1 ..

(Arsenic F ( 2.8

(Bariui P { 3.8 1.. .. _. 1 . .. |.. .. — — — 1 — (Berylliui P ( 1.8

. . . . „i 1 1— (Cadiiui P { 4.8 1 .... 1 . . . . (Calciui P ( 38.1

1 1 (Chroiiui P ( 7.8 1 . 1 ._ 1 1 (Cobalt P ( 18.8 j . . . 1

jcopper P ( 2.8 1 . . 1 - --1 • • 1

(Iron P { 9.8 1.. .. 1 . . 1 — 1 — (lead F ( 1.8 1 , 1 . .__ (Hagnesiui P ( 48.8 1 ... ,1 ... r • ••- 1

(Hanganese P ( l.t

JHercury CV j t.2 1, , . 1 . .. 1 1 (Nickel P ( 12.8 1 .. ... 1 1 1 (Potasslui P ( 2148 1 1 1 1 (Seleniui F ( 4.8 1 1 (Silver P ( 6.8 |.. . . . — 1 — (Sodiui P ( 4458 :.. 1 |.. — — — 1 (Thalliui F ( 2.8 1 — ~ " ~ l — — (Vanadiui P ( 4.8

1 1 (Zinc f ( 2.8 1 1 1 1 (Cyanide A { 16


14.4

9.8

8.4

8.6

6.2

1.8

7.6

1.4

2.8

•

8.4

1.8

8.2

8.8

8.2

6.1

2.4

428

1.8

1.2

898

6.4

8.8

8.4

1.8

DS',.vrua. J ON A U l wctuHT BASl'^ '

IBIS 15-17' (IB 15 35-37' IB 16 31-32' II69I-I5S j 16696-165 j 11691-675

97.48 i 97.48 j 96.68

ig/Kg i ig/Kg i ig/Xg

683 i 1366 i 1111

{ 1.57 { t.75

2.6 ( 4.4 ( 3.7

1.56 U i 1.77 U i 1.51 U

1,1 U j 8.96 0 j 8.68 U • 1

69.6 R ( 21.2 R { 26.5 R

4.6 { 3.8 ( 2.4

1 1

7.4 U ( 5.8 U { 3.7 U

3918 ( 3491 ( 2241

8.74 ( 1.2 ( 8.85

192 ( 148 ( 112

35.8 { 38.2 1 64.3

i 2.3 U {

UJ i UJ 1 UJ

UJ { UJ i UJ

2.6 U i 2.7 U { 3.1 U

5,4 R 1 4.6 R 1 4.2 R

- - ; r-

IB 16 41-42' II698-I8S

96.68

ig/Kg

1181

1.7

1.8

8.68 0

1.4 U

19.7 R

3.8

5.4 U

3311

1.8

lie

47.4

UJ

UJ

2.6 U

8.4 J

• Field Blanks 8869I-I9S

1.18

ug/l

Field Blank

3.8

93.8

14.8

261

1.8

UJ

6.1 J

-page 1 (

Field Blank ( II69I-18S j

l.lt j

ug/i (

Field Blank j

j

3.8 i

5.1 (

78.1 1

j

11.6 (

77.6 {

118 (

j

14.8 i

UJ (

1

6.8 J 1

KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since it uas

detected in a blank at a siiilar level. R Unreliable result - Analyte lay or u y not be present in this

saiple. J Quantitation is approxiiate due to liiitations identified during

the quality assurance review (data validation). UJ This analyte uas not detected, but the quantitation liiit is

probably higher due to a low bias identified during the quality assurance review.

ANAlYTICAl NETHOO: f - Inductively Coupled Plasia F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption A - Auto Analyzer OS - Oistiilation/Spectrophotoietric

IHORGAKIC AHAl'R

! ! ! J > i ; » i

'AKATYTicirKSii[fP-~Aiilo[iDslEPORfErOHToRYliniiiTlE^^ -page 2 ^ ^

(Anson Environaental Saaple Ruabcr j DU 11 ( DU 12 ( DU 13 ( DU 14 i Field Blank i {> atory Saaple Huiber ( 11691-115 ( 11698-825 { 88698-83S i 88698-845 i 88698-811S i

(Percent Solids ( 84.28 ( 59.88 ( 78.38 j 76.48 i 6.88 i 1 ,. .1 1 - -1 ... |._ 1 1 (Units ( ig/Kg { •g/Kg { ag/Kg ( ag/Kg ( ug/l {

iIHORGAKIC ElEKEHTS i Detection { Detection ( i i i (Field Blank { i . j Halt ( H a l t (Sol) ( j { { j (

JHercury CV ( 8.2 ( 8.1 ( ( ( ( ( (

(Cyanide A ( 18 { 1.8 ( ( ( i ( ( 1 .1 ( ( 1 1 ( 1 1

KOTES: - Eleaent was not detected. U This analyte should be considered 'not-detected' since it was

detected in a blank at a similar level, fl Unreliable result - Analyte u y or aay not be present in this

saaple. J Quantitation is approxiute due to liaitations identified during

the quality aesurance review (data validation). UJ This analyte was not detected, but the quantitation Halt is

probably higher due to a low bias identified during the quality assurance review.

AKAIYTICAI HETHOD: CV - Cold Vapor Atoaic Absorption A - Auto Analyzer

CO o o CO

00

Unvalidated Data

Monitoring Wells 1D, 4 & 6

300359

M'-: • i^Ki'~ni\! CAS<5 N G = ; H i~ B1 1

;AHPL.E I D

r / : : • .1. J . S.^ •••C

F-Bl 1 2 6 M W - 4 ( 7 5 - 7

M l , ! . - !• r,

MW—ID( i 2 0

l-.tl.i 1" ( .-Lj"; / . •

MW-T ( 6 0 - 6 :

L a o ) D i e XiJ :

0 0 6 4 9 - 0 2 s . 0 0 6 4 9 0 4 S

0 0 6 4 9 - 0 8 3

j") r . ,il.,/j. Q _ , ; i I C;

r i •"• A :(i Q •— I •> '^^ Q

. JI

.1C P .1 n t s r s 1 s m s n fc c o r r e c t i o n s a P G 1 .i e ci ' UJers I C P b a c k q r o u , - i d c o r r e c t i o n s a . D o l i e d ?

I f yss—'i- ' jere r a w d a t a , a e n s r - a t s d b B f o r e a D D l i c a t i o n o f b a c k c r o L i n d c o r r s c t i o r " : ; : V .':::i c ; / j^J f

<~. D n d .i. t .i o n s '"! -51 a. D a. c k a. cj f 1 , ' - f = i.',i,;. r i-H !-i-,=, 1 1 • . . ! i e c a r m s a n a

'._ ! ] &? i_ •._' I I <... I -;:.-\ • „ ',. •• !_' t j '.. I ; L t_ •.._ T H E .,•_ "... -r i a. .L y n i i '..i i '_• i U ',_•}If l.j .•_ -i:^ ' - '.zr: : h : vz =;

-i- 1 n n n v

an -ins? conditions data jcopy data package and .ti i.skstts' has been authori

r>ci aoov f? . , t h e d a t < : ; n r a i n e a '...! I•E •,_ '__= < 1!!...''„.i >_ '.t? 1 ! cz ; r . G -n?. i_' J . c r '..J CT. '._•:=*. -.n u i L J f i t ..•_ •_ '.-

...I ;...' V : ne !...aaG l a n a a e r _••. I i •=•. '..J r r • :-• <.j c - := .1 y i f r: © s •:n => v S i i T .1 B D i_' y =._ ; ! fr" i •-_• .L .;. '..J V-f .L. i k U

. a n a t LI r a ; (^^Oi^^JjdL i ^ iad ie;

//z.Ao

.ana t a r e

/^Au, / I M -

: ^ ^ ^

oK

1 c

/ ' / . - -

/ r i a n f •

.LiM

300360

• I 01

}" C E I M I C

; : C E I M I C C S B B N O ,

s a .11 .'•' w a t e r .) : W A T E R

Q w / m e d ) 3 LOW

^ N b u N

: r a c t : A N S O N

S A S N o , ; 6 i j b N o : , ' r

L a p S a m p . L e

•= . , - , >. i ! - \ ' .

i c e n t r a c i o n u n i - '.—' t ! I ! L J .-• ! •-. ' - I ".J i V w e 1 a n t :

H n a .

.'' -'-r .,:1 '••/ — V V.' - Z J

7440-36-0 7440-3S-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4

7439-96-5 7439-97-6 7440-02-0 7440-09-7 77S2-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6

; H.Lur"inLUT! 1 Antimonv J Arsenic ! BariLiiTi 1 Beryl 1ium i Cadmium i Calcium i Chromium ICobalt i CoDoer ! I ron ! Lead 1Naanesium i Nanc!-an ese 1 Mercurv 1 N i c k -e 1

1 Potassium ': Selenium 1 SiIver i Sodium ;Thai 1ium ;Vanadium 1 Z i n c 1 Cyanide

i t ;

i \

3 , Citj 1 4 , 0 0 I

) ! " E u ( I i i 1

7 „ 0 0 i

! I i

. j , r j a '-J':.* 1

4 0 . 0 0 i

2 . 0 0 I

2 1 4 0 . 0 0 I

4 , 0 0 !

6 . 0 0 !

4 4 5 0 , 0 0 i

y ' i I ' . ' )

H' .. s'ii';

l.jl W

P; i

I p I

' F'

! Cl-

H a - i - ! • - , r - : JLORLESS . a r ; e>; t u r e ;

. o r A -f t e r - O R L E S S C i a r i H-' C L E A R H r r. 1

Tien c s :

300361

INORHAN;

i^^^^Name; CLINIC

L .b Code; CEIMIC

Matrix (soil/water)

L ;vel ( low/med) ;

"/•— S o 1 i id s ;

P31 12

ANSON

WATER

or i^'er'O

\ c a n t r a t i c n Li n i t s ( u q .• • r mq.-'r-..q

• c*. I,.' •.,.' C:'. 11! !_' J. '™ .1 i-' a ^-' -' •—' -T .-•

Da. tEr R e c e i v e d ; 1 1 . / 2 2

w e i g h t ) : (..JG/L

.-H'-z: N a

i 7 4 2 9 ~ - 9 0 - - 5

i 7 4 4 0 - 3 8 - 2

\ 7 4 4 0 - 4 1 - 7 ! 7 4 4 0 - 4 3 - 9 ' 7 - ' ' 4 0 —" !") — '"'

I 7 4 4 0 - 4 8 - 4 I 7 4 4 0 - 5 0 - S

i 7439—92—1 ! 7 4 3 9 - 9 5 - 4

i 7 4 3 9 - 9 7 - 6 I 7 4 4 0 - 0 2 - 0 i 7 4 4 0 - 0 9 - 7 L 7 7 8 2 - 4 9 - 2 I 7 4 4 0 - 2 2 - 4

j -7.440—23—0

I 7 4 4 0 - 6 6 - 6

COLORLESS

COLORLESS

C D n c e n t"" a t i (D r

H.Luminum Antimony I Arsenic E'ariu.m i Beryl 1ium i Cadmium ; Calc.iu.m i Chromium i

f^ r- f-. .-^ ,-^ --• '

I r o n ; L e a d i M a a n e s .i u m \ M - a n g a n e s e i M e r c u r y ! N i c k e l I P o t a s s i u m 1 S e l e n i u m i o 1 .L V <e r i

S o d i u m : T h a i I i u m \ V a n a d i u m ! T .; — — i

.'_ JL n c : C v a n i d e i

1 1 Ci „ 0 0 ! B i

2 . CMj 1 iJ 1 5 , 0 0 i B I

4 . 0 0 ! U i

j . i J i j I 1.

/ , i J U

f^6 . 0 0 i B i 1 . 1 0 i B 1

4 0 . CiC> '. U i 1 (••>, C ) C ) : p. I

2 1 4v.; , Oij ! U i 4 . 0 0 I U I W . ~ T , • • . . " . . '

1 ! E

4 4 5 0 , 0 0 ! U : 2 , 0 0 i U i 4 . 0 0 i U i

14,00 i-B 1 1 Cl *")(") ' i i '

clarity Betors: CLLAR

Claritv A-fter: CLEAR

B -: t

IP ; ! I '.

i ! !

p ;

Texture:

Arti-f-aci

'—/mmenr.:

IN

'.)

300962 ' 03

TNnRF 1-: 1 -H f~l'-... T - . .J . 1 •„_' J„' !-'. S r-* ...J E E E._ E__ ;

Name: CEIMIC

ab Code: CEIMIC

Matrix (soi1/water):

....,5vei ( low/med) :

"" Sol ids :

1 •oni-::en t r- ^

C o n t r a c t : ANSON

C a s e N o , ANSON >3HS N'~ „ N o ,

W.H i t r t L a b S a m o 1 s I D : <I> 0 6

P , - . •!- £-1 Pn= EI r - --1 - \ ' '=i '"< " 1 -i '--

tion Units (ua/L o r (na/ h-.i d r V we .i o in t .

i l o r B e f o r

i o r H - h r e r ;

ICAS No.

: 7429 ; 7440 1 7440 ; 7440 1 7440 i 7440 1 7440 i 7440 1 7440 ! 7440 i 7439 ! 7439 1 7439 1 7439 1 7'-4 3 9 i 7440 1 7440 1 77S2 i 7440 i 7440 i 7440 i 7440 ; 7440

i

i

-90--3^6--38---39--4 1 --43--70--47--48--50--39--92--95--96--97 -02--09--49-_•"?•"?„

^ ' ~ y ~ v .

-23-_ i-; '"7= _

-66-

— "

-0 ".IC

_"T

_"7

-9 _ -7.

_-T

-4 -8 -6 -1 -4 -5 -.6 -0 -~7

_ - ~ y

-4 -5 -0 ~ . t -

-6

! Analyte

1 Aluminum ;Antimony 1 Arsenic i E-iarium 1 Eiery 1 I ium i Cadmium 1 Calcium 1 Chromiufn i Cobalt 1 Copper i I ron 1 Lead 1 Macnesium i M-anqanese 1 Mercury INickel \ P.otassium 1 Selenium !SiIver 1 Sodium i Thai 1ium ; V-an-adium 1 Zinc i Cyanide

I... o Ti C

; i 12, 4 0 ,

4 ,

1

on

00 C'O OC*

OCi 00 OC)

CiC* OCi 00 3C! CiC) 00 2Ci OC) C'O

C'O O'C) CiO C'O C!0 C>CJ

C 1

Bl Ui

1 j •

B ! U 1 Bl Li 1 U l B l B 1 B 1

Ul Bl U l U 1 U! 1 1 '•

U 1 U ; U l Bi B i Ul

COLORLESS

COLORLESS

Clai"-ity &:e-fore: CJLEAR

Clarity After: CLEAR

W

IM

IP I i r

I P I I D I I ! ;

I P - E

IP i I C ' ;'

! !~ (

I ! t

: P I

I !- i

IF' I I P i I r :

H E ' - t i t a c u S \

- j m m e n t . s :

'CRN I IN

300363 04

,!0F<6ANIC

L ^ ^ ^ N a m s : CE I M I C

i . .ase hio,

J G n t r -a c t : A ! l S (.J N

s o i 1 . / w a t e r ) : W A T E R m o l e I D : 0 0 .

vErl ( l-ow./med ) ; I ON

: e n t .r .a r i c n i. J n i • mq./ K. 'v w e i q h t ) : i..JO/

7 4 4 0 - 3 S - 2 7 4 4 0 - 3 9 - 3 7 4 4 0 - 4 1 - 7 7 4 4 0 - 4 3 - 9 7 4 4 0 - 7 0 - 2 7 4 4 0 - 4 7 - 3 7 4 4 0 - 4 5 3 - 4 7 4 4 0 - 5 0 - 8

7 4 3 9 - 9 2 - 1 7 4 3 9 - 9 5 - 4

7 4 3 9 - 9 6 - 5 7 4 3 9 - 9 7 - 6 7 4 4 C-'—C-' 2—C' 7 4 4 0 - 0 9 - 7

7 4 4 0 - 2 2 - 4

7 4 4 0 - 2 8 - 0 7 4 4 0 - 6 2 - 2 7 4 4 0 - 6 6 - 6

P i n a i v t e ? I C o i n c e n t r a t i o n I C

Aluminum I Antimony I Arsenic Barium • Beryl 1iumI Cadmium I

Chromium I Cobalt I Copper I I ron I Lead I MaqnesiumI M-ai-iganese I ! B e r '_ '..l B y !

Nickel ! Potassium 1 Selenium I Silver I Sodium I Thai 1ium I Vanadium I Zinc I Cvanide I

41 . I ) ! ; ; ! i

•.;• n

4 . -1 - ! ~ 7

-7 a

10 .

1 o,. 6 6 .

1 , inrin:; • - - ' • — ' = •

Cj a

• - • 3

1 ••"? J . . ; _ u

2 14Ci . 4 ,

6 . 4 4 5 0 m

u u CiO '") '"

C'Ci

i-i '-.i

'•-••Ci

CiCi

•60

- - • • - '

CiCi

0 0 0 0 0 0 (")0

H

u • - t

u

t.^

B B r i A _ '

( j

f j

u B 1 •—;

u 1 i

9 , C'Ci I B , Ci, OCi 1 U

i r-j K - {-; (za -f. B-^ I*- i;:a 1

. a r H-B-te?

COLORLESS

COLORLESS

.: i a r:

Clarity After: CLEAR

I F 1

P

IF I IP ; ! C B

T e x t u r e ;

A r t i f i

--'-^mmeniis :

300364 OS

Name: CEIMIC

ata Code: CEIMIC

!v|ui--4( 7 5 - 7 -

C a s e N o . : ANSON j H b N o , ; /L7 V-iO a Z I" r o -I 1 I a;

- 9 v e 1 ( l o w / m e d i : LOIAJ

L a b S a m e I s I D : C iCi649 —CiS:

D a t e R e c e i v e d : 1 1 .•'' 2 9 . / 9 1

" j - S o l i d s :

; o n c e n - c r a - J B s E.J ! j . o r Bmq/Kq d r v MR/!•::• R

N o , i -^ .m

I 7429—9Ci—5

i 7 4 4 0 - 3 3 - 2 I 7 4 4 C i - 3 9 - 3

! 7 '440—4^3-9 I 7 4 4 0 - 7 0 - 2 • 7 4 4 0 - 4 7 - 3 I 7 4 4 0 - 4 3 - 4 i 744Ci—5Ci—8 I 7 4 3 9 - S 9 - 6 I 7 4 3 9 - 9 2 - 1 I 7 4 3 9 - 9 5 - 4 : 7 4 3 9 - 9 6 - 5 1 7 4 3 9 - 9 7 - 6 I 744Ci-Ci2-Ci I 7 4 4 i O - C ) 9 - 7

I 7440-22-4

j 7440-23-0 :7440-62-2 17440-66-6

I H ium m u m I Antimonv i Arsenic I Barium i Beryl 1ium I Cadmium I Calcium 1 Chromium I Cobalt I CoDoer I I ron i Lead I Magnesium I Mangaunese ! M s r c v . r v iNickel 1 F-'otassium i Selenium j SiIver 1 Sodium iThailium

L- o n cent r a. t .i o n

;•;.. uu 7.90 0. 74

snadium

Cvan i de

'U H

' •J - / i.i

63 „ 7Ci 3 = 20 1 n 3 0

126Ci .0C> I---, CJ o

^J m Y O

12.50 12.30 Ci. 1 Ci

3 7 7 , OCi

1.10 783.00

0,42 2 . I Ci

U I P, '

Ul

u; U i I ; '•

Ui Ul

3 0 i U i

Color BefoB-e: BROWN

i Dior After: YELLOW

r 1 := B- -i -!- s y t) e — o r E

0 1 a r .i t V A -f t e r ;

I P B B

1 i-

I p

p

T e x t u r e ; MEDIUM

A r t i f a c t :

:immenr_s

FORM I - I N

300365 06

INORGAN: H N H B .

iN-ame ;

n r.ni-i-;^'.

M a t r i x (

CEIMIC

CEIMIC

I / ./ w<=i r e r . '

C CJ n t •'• a c t : A N S U iNi

C a s e N o . : ANSON SAS N o . :

; C I L L a b ;3amp.L(

L-.-,,,Vel t. .1 ow/,med ) : OW

ai=-: i~\

Dncentration Units (uq/L or mo/Kq dr

-„-

*"~

, - • — .

—

..,..

( ^ w —

.-.-

":.olor

..-•lor

'•-•dimmer

B

A

t

e

f

,-

fore:

ter: -

.

B

1 CAS No. i

i 7429-90-5 17440-36-0 17440-33-2 17440-39-3 17440-41-7 \7440-43-9 17440-70-2 !7440-47-3 17440-43-4 I7440-50-S !7439-S9-6 17439-92-1 17439-95-4 i 7439-96-5 17439-97-6 [ 7440'-Ci2-C) ;7440-09-7 17732-49-2 I 7440-22-4 17440-23-5 • 7-44 Ci-23-0 i 7440-62-2 i 7440-66-6

i

BROWN

YELLOW

•

Analyte iC : !

Aluminum 1 Antimonv Arsenic 1 SaB"-ium i Beryl 1ium i iCadmiufTi 1 Calcium 1 Chromiufii 1 Cobalt i Copper i I ron 1 Le^ad i Magnesium 1 Manaanese1 Mercu.ry 1 Nickel 1 Potassium i Selenium 1 Silver i Sodiium 1 Thallium 1 Vanadiu.m i Zinc i Cyanide i

Claritv

Clarity

3ncentration

S 1 1 , CiCi S. 60 Ci. S O 2 , 7Ci (-•. "7 - 7

0.77 •3Ci, CiCi 3 . 40 1 . 90

7 i")

1 96Ci 3 CiCi 2,10

28 , 50 25 . 40

C i . 1 1 2 . 30

409 ,00 0 = 91 1 , 1 Ci

8 5 1 , CiCi

0 .46 2 , 30 2 ., 50 '7 3 C)

Before:

After:

B

C 1

U i Pr !

-0 1

B 1 ! i !

B i

Ui B i

B 1

i..JI Ui Ul Ui Ui Ul Li 1 Bl Bi t j \

1

(--,

*

i.'Vi

IM 1

i F"' i i F' ! 1 F i ! C- '•

i P i • -P '

1P i IF' i IP 1 ! ?~ !

1 P i I F i I P i ; F'

ICV;

B i " B

1 P i

1 F i

IP 1 1 P i I C" '

1 P i

i .-• !

1 1

T 3 ;i

Art

l-R

a t e F s s c e i v e d : 1

w.eiq n't

FORM I

4 )

300366 07

M •a m e : C £ IMIC

i sb Code; CEIMIC

Matri;•; ( soil /vsater ) : SCI

i-,; Vel (low/med ) ; L0W

1 INORGANIC ANALYSIS DATA SHEE'

ANSON 1W-6

a s *=" No,

'r^ Sol ids

D n c e n t r a t i o n Units ( u q / i_ a r m q / K q d

; oLLl NO . ;

Lab Sample ID: OOi

Liate iReceived ; 11.-'

weiqht): MG/KB

B™ H 1 1 '

• 49-1 OS

•

1 CAS No .,

1 7 4 2 9 - 9 0 - 5 1 7 4 4 C i - 3 . 6 - 0 1 7 4 4 0 - 3 8 - 2 i 7 4 4 0 - 3 9 - 3 1 7 4 4 0 - 4 1 - 7 1 7 4 4 0 - 4 3 - 9 i 7 4 4 0 - 7 0 - 2 ; 7 4 4 0 - 4 7 - 3 1 7 4 4 0 - 4 3 - 4 1 7 4 4 C ) - 5 C ! - 3 1 7 4 3 9 - 8 9 - 6 1 7 4 3 9 - 9 2 - 1 1 7 4 3 9 - 9 5 - 4 1 7 4 3 9 - 9 6 - 5 i 7 4 3 9 - 9 7 - 6 1 744C!—Ci2-Ci 1 7 4 4 0 - 0 9 - 7

1 7 7 8 2 - 4 9 - 2 1 7 4 4 0 - 2 2 - 4 1 7 4 4 0 - 2 3 - 5 1 7 4 4 0 - 2 8 - 0 1 7 4 4 0 - 6 2 - 2 1 7 4 4 0 - 6 6 - 6

1 A n a l y t e I f

1 A l u m i n u m i 1 A n t i m o n v 1 i A r s e n i c i i B a r i u m 1 1 B^ery 1 i i u m i iC^admium 1 1 C a l c i u m 1 1 Ch i ' -omium 1 I C o b a l t 1 i i C o P D e r i i I r o n ! I L e a d 1 1 M a q n e s i u m 1 1 i ' i a n o a n e s e i I M e r c L i r y 1 i N i c k e l 1 i P o t a s s i L i m 1 1 S e l e n i u m 1 I S i l v e r i 1 S o d i u m i 1 T h a i l i u m i i V a n a d i u m i I Z i n c 1 1 C y a n i d e 1

j . o n c e n t r a t i ^ o n

5 1 5 , 0 0 9 , 8 0 0 . 8 5 2 . 2 0 1 , 10 0 , 3 7

3 3 , 7 0 3 . 7 0 2 , 2 0 2 . CiCi

1 3 6 0 . 0 0 1 , .3Ci

3 4 . 6 0 1 4 , 8 0

Ci. 1 Ci 2 . 6 0

4 6 5 , 0 0 0 . 3 9 1 , 3 0

9 6 7 , CiCi 0 . 4 4 2 . 4 0 1 , 7 0 2 . 1 Ci

U B B

U B

u g

B

u u u u u u u B B

u

• I < I

Q iM i • i

\ F 1 ; c 1 < 1 1

! !~ 1

i P ; i P 1 IP I IP 1 i P i i p 1 IP i

* i p 1 I F 1 IP 1 IP 1 iCV 1 ! P 1 i P 1

W I F 1 IP i IP i I CT J

IP 1 IP i

• i

Dolor Before: BROWN

.t..p 1Qr After: YELLOW

'"3mmen 15 :

Clarity Before:

Clarity After;

Texture;

Artif-acts

ivi p B-. T i i |-,-|

'ORM I - IN

300367 •^ 08

SAMP f^ C--"'' £-• Q i-i — p "r

MW- .1. u ^iame : C o n t r a c t : ANSON

C a s e N o . : ANSON SAS N o . : B •. B~ I - , - ^ r-B •—, " B ' _ i rB B " E. •• LJ w !._' q ' - - ' a '.-^ ' . - . .1. '. B I ' _ •

M a t r i ;•; ( s o i 1 / w •a t e r ) : •S 011

^•.,^vel ( i o w / m e d ) ; LOW

• ' • - S o l i d s : 8 7 , 1

C o n c e n t r a t . i o n U n i t s (uc!.^''L o r mq. /Kq d r y w e i g h t ) : MO./KB

L a b S a m p l e I D : OOi

D a t e R e c e i v e d : 1 1 /

4 9 - 0 1

2 1 / 9 1

I "7 ''I 4 f i — 7 hi—7

I 7 4 4 0 - 3 9 - 3 I 7 4 4 0 - 4 1 - 7 i 7 4 4 0 - 4 3 - 9 ! 7 4 4 C i - 7 C i - 2 i 7 4 4 0 - 4 7 - 3 i 7 4 4 0 - 4 3 - 4 ; 744Ci—5Ci—8 ' 7 ' ' ' .39 —89—1^,

1 7 4 3 9 - 9 2 - 1 I 7 4 3 9 - 9 5 - 4

I 7439—97—B^

I 7 4 4 0 - 0 9 - 7 i 7 7 8 2 - 4 9 - 2 ; 7 4 4 0 - 2 2 - 4

I 7 4 4 0 - 2 S - 0

1 7 4 4 C i ~ 6 6 - 6

C o l o r B e f o r e : BROWN

i__) lo r A f t e r : YELLOW

P - i m m e n t s :

An .a 1 y t e i CBOTI C e n t r a t i o n

AlLiminum 1

Antimonv i Arsenic i Bariu.BTi i

Beryl liLun i

Cad (Tl ium 1

Calcium 1 Chromium i

Cobalt 1 Copper 1 I ron i

Lead 1

Maa.nesium 1 Manqanese i

Me re Li rv 1 N i ck e1 i

Potassium i

Selenium i Silver i

.S.odium 1

Thailium 1

Vanadium 1 Zinc 1

Cyanide 1

5

14

7

7

1.3

! 0 • ^ '

0 0

31 Ti

1

1

50

0 26 8 (j

2 69

0 1

68 0

1 • ~ ^

•B I

, OCi

. 30

.44 , SO

,52 ,69

. 10

. 10

,70

. 70

, 00 ,80

,30 . 10

,09 .10

. CiC' •7 -i

, CiCi

. 0C>

.35

, 90

, SO

,50

i C L a r i t y B e f o r e ;

C l a r i t y A f t e r :

:v

F P p

C P P F P P F

p

T e ;•; t u r e ;

A r t i f a c t s ;

. i J ± '-J B !

c n p r.i T •ORr

300368

0^* 09

INORGANIC ANALYSIS DATA SHEET

Mi.i.... -r p . .' B -;,,•••,_.. 1 -,--T, -1 B

:£IMir

1 /w^ateB"-)

trac •I- . .••M\ic:;|-f^,i

K-.,? "'e.;. !. low.-'miea.i :

C a s e !Mo, : ANSC'N

SOIL

LOW

8Ci, 7

Concentration '..Jnits (ug/L or mg/Kg dry weight): MG/KG

Lab S'ampl.e ID: 0Ci649-C>3S

Date Received: 11/22/91

.-•HH N o .

7429-•7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-_ — .

-90-—•-< 0 -

-38--39--41--43--70--47--43--50--39--92--95--96--97--02--09--49-_oo.

- •" 7 -

-23--62--66-* " " * " " • " "

„c::

-Ci ~2 _;T

-7 -9 ~.ii!

-"

-4 -8 -6 -1 -4 -5 -6 -Ci -~7

"2 -.4

"••-J

-Ci _ • - • >

-6 "**"*""

AIuminLim Antimony AE"-ssnic Bar iu.m Bervl 1 iu.m CadmiLim Calciij.m Chromiu.m Cobalt Copper I ron Lead MagnesiLim Man0anese Mercurv Nickel Potassium SeleniLim SiIver Sodium Thailium Vanadiu.m Zinc Cyanide

H n a 1 V -i- f jncen t; a tion

OS , 00 3. 1 Ci

Ci, 63

2 , 2Ci

0.54 0,72

24,40 1 ,40 .L a W'J

2.20 36 ,00 1 .30 7, .50

12 ,60 0 , 1 1

34. OCi 0, S3 1 . 1 Ci

99,00 Ci. 41

1 .60 1 ,30 2 , o<:)

Cl

J i

Ul Bl Bi Bl Ul Bl Bl Ui Bi

1

1

Bl i

Ul Ul Ul Ul Ul Ui Ui Bi B 1 Ul

1

.•olor Before: BROWN

L-v lor After: YELLOW

Dmments;

Clarity Before;

Claritv After:

Q

W

p,

F'

c E

P P P o B

p P P F

h

P P F o B

P c

Texture: MEDIUM

Artifacts:

FORM IN

• t

.300369 "" 10

-r;-. B B", C ' E'.-. A B- ,i T E~ A K i A I V' '--- r'—• r-' /'•-. - " /-•. ,:::: i.

MW- I \ a ' : . ' — <Z'y.i

N a m e ; C

I D B . n n f^ : 1.

i ' la.tr .i X ( s o i

. e v e l ( low..-

S o l i d s

'EIMIC

;E IMIC

. 1 /w-ater ) :

'med ) :

C.ase

SOIL

i_,OW

No. • ANSO

in t r a c t : ANSON

SAS No„ : iU N o ,

1 h P. :a m i-j 1 s a m p l e i i j : OCiCj49~OG

.D a t e F\ e c e i v e d : 11./ 2 '6./ 91

C o n c e n t r . a t i c m i J n i t s ' I .-. ^ mg/Kg d r y w e i g h t ) : MG/KG

^

p

Color IBefore:

Color After:

Comm.ents:

1

iCAS No.

17429-90-5 17440-36-0 :7440-38-2 17440-39-3 17440-41-7 17440-43-9 .17440-70-2 i 7440-47-3 17440-4S-4 17440-50-8 i 7439-39-6 17439-92-1 17439-95-4 i 7439-96-5 17439-97-6 i 7440-02-0 ;7440-09-7 i 7782-4-9-2 17440-22-4 i 7440-23-5 17440-28-0 17440-62-2 17440-66-6

BROWN

YELLOW

B

Analyte 1 Con

Aluminum 1 Antiiiionv i Arsenic i BariLim i Beryl lii-im ! Cadmium 1 CalciLim 1 Chromium 1 Cobalt 1 Copper i I ron 1 Lead 1 Maqnesium1 Manqanese i Mercury 1 Nickel 1 F'otassium 1 Selenium i Silver 1 Sod iu.m 1 Thallium 1 Vanadiu.m 1 Zinc i Cyanide i

Clarity B

c

e

Clarity Af

FORM I

entration

717.00 3 , 9Ci 0.53 3. 1 Ci 0,59 0 , 79

•3C!, 5Ci 2.60 2 . OCi 2, 40

1540,00 1 . 1 0

19.70 21 ,20 0.12 2.40

421.00 0.34 1 ,20

876,00 O , 47 2.20 2 = 2Ci 2.60

fore:

ter:

- IN

c

u B B B u B

U B

B

u U U U u u u B B U

Q

*

W

B B

W 1 ! B B

B B

P 1

P 1 F 1 P 1 P 1 P 1 P 1 P 1 P 1 P 1 P ]

F I P 1 P 1 CV 1 P i P 1 F 1 P 1 P 1 F i P 1 P 1 C 1

1 i

Ts/< ture;

.Artifacts:

7

MED

-'88

aoosTO / ' • t t

lA VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

m b Name: INTECH Lab Code: INTECH

59-61' Contract: 68-D9-0048

Case No.: 42-64 SAS No.: SDG J o. : ANSON

Matrix: (soil/water) SOIL

Sample wt/vol: 5.0

Leve1: (1ow/med) LOW

% Moisture: not dec. 13.

Column: (pack/cap) PACK

CAS NO.

Lab Sample ID: If/|/< 2--'

(g/mL) G Lab File ID: C9759


Date Analyzed: 11/27/91

Dilution Factor: 1.00

CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q COMPOUND

74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2- 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorometharie 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6- 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5— 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene

1330-20-7 Xylene (total)

11. 11. 11. 11. 6.

13. 6. 6. 6. 6. 6. 6.

11. 6. 6.

11. 6. 6. 6. 6. 6. 6. 6. 6. 6.

11. 11. 6. 6. 6. 6. 6. 6. 6.

U U U U B B U U U U U U U U U U U U U u U U U U U u u u u u u u u u

FORM I VOA 1 /87 Rev .

19 3003*rt

IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

m b Name: INTECH ab Code: INTECH Case No.


Sample wt/vol: 5.0 (g/mL) G

Level: (low/med) LOW



Number TICs found: 0

59-61' Contract: 68-D9-0048

42-64 SAS No.: SDG No. ANSON

Lab Sample ID: T l ( l ( ' t ^ - /

Lab File ID: C9759




CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG

CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

L ^• 110. "ll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22, 23. 24. 25. 26. 27. 28. 29. 30.

COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC 1/87 Rev .

20 300372


EPA SAMPLE NO.

^ P D Name: INTECH

Lab Code: INTECH Case No.

Matrix: (soil/water) WATER

Sample wt/vol: 5.0


,3 Moisture: not dec. 100.

.„Column: (pack/cap) PACK

F-BLANK Contract: 68-D9-0048

42-64-85SAS No.: SDG .No.: ANSON

Lab Sample ID: J H f l ^ l - - ^

CAS NO.

(g/mL) ML Lab File ID: A6395



Dilution Factor: l.OO

CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND

74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-3 5-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dlchloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-4 3-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-b Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 3. 9. 5. 5. 5. 5. 16. 5.

10. 5. 5. 10. 5. 5. 5. 5. 5. 5. 5. 5. 5. 10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ J U U U U

U U U U U U U U U U U U U U U U U U u u u u u


25 300373


Contract: 68-D9-0048

EPA SAMPLE NO.

^ ^ b Name: INTECH

^ E b Code: INTECH Case No.: 42-64-85SAS No.

^-Matrix: (soil/water) WATER

— Sample wt/vol: 5.0 (g/mL) ML

"Level: (low/med) LOW

~~% Moisture: not dec. 100.


F-BLANK

: SDG No.: ANSON

Lab Sample ID: J Z/Zf '^

Lab File ID: A6395




Number TICs found: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

t 9. |io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.


FORM I VOA-TIC 1 /87 R e v .

26 300374


EPA SAMPLE NO.

b Name: INTECH

Lab Code: INTECH Case No


Sample wt/vol: 5.0





. : 42-64 SAS No.: SDGJ^o.: ANSON

Lab Sample ID: J ' / l / t ^ l - ^




CAS NO. COMPOUND

Dilution Factor:


1.00

Q


107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyi-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene


13. 13. 13. 13. 7.

110. 6. 6. 6. 6. 6. 6.

13. 6. 6.

13. 6. 6. 6. 6. 6. 6. 6. 6. 6.

13. 13. 6. 6. 6. 6. 6. 6. 6.

U U u u B B U U U U U U U u u u u u u u u u u u u u u u u u u u u u

m FORM I VOA

32 1/87 Rev.

300375


EPA SAMPLE NO,

120-122' ^iab Name: INTECH Contract: 68-D9-0048

^Piab Code: INTECH Case No.: 42-64 SAS No.: SDG No

i;:; Matrix: (soil/water) SOIL




ANSON

Lab Sample ID: r////f -V

^Sample wt/vol: 5.0

«Level: (low/med) LOW

- % Moisture: not dec. 23.

-"Column: (pack/cap) PACK

Number TICs found:

Dilution Factor:


1 . 0 0

-

,-.-

.....

1

—

„,.

—

•c-.--.

CAS NUMBER ================

1. 2. 3. 4. 5. 6. 7. 8. 9.

k 10. Pll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.

COMPOUND NAME RT EST. CONC.

II II II lO

II it

FORM I VOA-TIC 1 /87 Rev .

33 300376


EPA SAMPLE NO.

Contract: 68-D9-0048 F-BLANK

fPk Name: INTECH

; Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

_ Matrix: (soil/water) WATER Lab Sample ID: j : \ l ( ( ^ l - 9

.,5ample wt/vol: 5.0

-Level: (low/med) LOW

-* Moisture: not dec. lOO.

-Column: (pack/cap) PACK

CAS NO.






74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene

1UU61-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene i 00-41-4 Ethylbenzene iuu-4 2-b Styrene

1J30-20-7 Xylene (total)

10. 10. 10. 10. 3.

14. 5. 5. 5. 5.

13. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ

U U U U

U U U U U U U U U U U U U U U U U U

u u u u u


38 360377



EPA SAMPLE NO.

F-BLANK b Name: INTECH

&b Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

Matrix: (soil/water) WATER Lab Sample ID: 3:///4/-5

"Sample wt/vol: 5.0




- Number TICs found: 0





CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

k ^• |io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26.

28. 29. 30.

COMPOUND NAME RT EST. CONC.

.

Q

1

FORM I VOA-TIC 1 /87 Rev.

39 300378


EPA SAMPLE NO.

T-BLANK Fb Name: INTECH Contract: 68-D9-0048

Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

_.Matrix: (soil/water) WATER Lab Sample ID: j n i i ^ l - ( ?

-Sample wt/vol: 5.0 (g/mL) ML

—Level: (low/med) LOW

—% Moisture: not dec. 100.

—Column: (pack/cap) PACK

CAS NO. COMPOUND

Lab File ID: A6397




CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q

74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-!>entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 3. 10. 5. 5. 5. 5. 5. 5. 10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ U U U U U U U U U U U U U U U U U U U U U U U u u u u u u

FORM I VOA 1/87 Rev.

45 300379

«



EPA SAMPLE NO.

T-BLANK b Name: INTECH

ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

Matrix: (soil/water) WATER Lab Sample ID: Ju((¥i -6

"Sample wt/vol: 5.0










CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

k • iio. ^11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.

COMPOUND NAME ============================

RT EST. CONC. Q


46 300380


EPA SAMPLE NO.

^ ^ b Name: INTECH

Lab Code: INTECH Case No.: 42-64


._ Sample wt/vol: 5.0

_ Level: (low/med) LOW

.,..„% Moisture: not dec. 52.

— Column: (pack/cap) PACK

60-62' Contract: 68-D9-0048

SAS No.: SDG.No.: ANSON

Lab Sample ID: J l ( / U ^ ^ (




CAS NO. COMPOUND

Dilution Factor:


1.00


107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 ^Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 • cis-l,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-I»entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene


21. 21. 21. 21. 14. 54. 10. 10. 10. 10. 10. 10. 21. 10. 10. 21. 10. 10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 10. 10. 10. 10. 10. 10. 10.

u u u u B B U U U U U U U u u u u u u u u u u u u u u u u u u u u u

FORM I VOA 1/87 Rev .

50 300381


EPA SAMPLE NO.

•

b Name: INTECH

b Code: INTECH Case No.: 42-64

- Matrix: (soil/water) SOIL

"Sample wt/vol: 5.0


"% Moisture: not dec. 52.


.. Number TICs found: 0

60-62' Contract: 68-D9-0048

SAS No.: SDG No.: ANSON

Lab Sample ID: X^///^^~f




Dilution Factor:


1 . 0 0

CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

fe. • •LO.

rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25.

27. 28. 29. 30.

COMPOUND NAME

,

RT EST. CONC. Q


51 300382


EPA SAMPLE NO.

^ ^ Name: INTECH

Lab Code: INTECH

75-77' Contract: 68-D9-0048

Case No.: 42-64 SAS No.: SDG Ho.: ANSON


..Sample wt/vol: 5.0

,._Level: (low/med) LOW

.=.% Moisture: not dec. 23.

--Column: (pack/cap) PACK

(g/mL) G

CAS NO. COMPOUND

Lab Sample ID: JTZ/Z/^f"'^

Lab File ID: C9762




CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q

74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride

108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 ' Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-25-2 Bromof orm 108-10-1 4-Methyl-2-f'entanone 591-78-6 2-Hexanone 127-18-4— Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4—-• Ethylbenzene 100-4 2-5 styrene 1330-20-7 Xylene (total)

13. 13. 13. 13. 7.

39. 6. 6. 6. 6. 6. 6.

13. 6. 6.

13. 6. 6. 6. 6. 6. 6. 6. 6. 6.

13. 13. 6. 6. 6. 6. 6. 6. 6.

U U u u B B U U U U U U U U U u U U U U U U u u u u u u u u u u u u


56 300383


EPA SAMPLE NO.

«

b Name: INTECH

ab Code: INTECH Case No.: 42-64


Sample wt/vol: 5.0





75-77 ' C o n t r a c t : 6 8 - D 9 - 0 0 4 8

SAS N o . : SDG N o . : ANSON

L a b S a m p l e I D : J f i l l ^ ^ - 1

(g /mL) G L a b F i l e I D : C9762



Dilution Factor:


1 . 0 0

CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

k • |io. ^11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22, 23. 24. 25. 26. 27. 28. 29. 30.


.


57 300384



EPA SAMPLE NO,



Matrix: (soil/water) WATER Lab Sample ID: J|/// f-3

Sample wt/vol: 5,0




(g/mL) ML

CAS NO, COMPOUND

Lab File ID: A6398





-~

--,

• ~ '

m I P

,,.-

^ .

-—

' • " • • •

74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane

540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 1U8-10-1 4-Methyl-2-Pentanone b9i-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane

108-88-3 Toluene 1U8-90-7 Chlorobenzene iuo-41-4 ——Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 3.

41. 5. 5. 5. 5.

12. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ

U U U U

U U U U U U U U U U U U U U U U U U

u u u u u


g2 300385

«



EPA SAMPLE NO.


'ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

Matrix: (soil/water) WATER Lab Sample ID: S U H ^ ^ - 1

-Sample wt/vol: 5.0

'Level: (low/med) LOW


"Column: (pack/cap) PACK

„ Number TICs found: 0


Date Received: 11/2 6/91




CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

i. ^• IlO. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.


•


30038G

63


EPA SAMPLE NO.

T-BLANK pb Name: INTECH Contract: 68-D9-0048


Matrix: (soil/water) WATER Lab Sample ID: J U l f y t ' 9

Sample wt/vol: 5.0

Leve1: (1ow/med) LOW

,% Moisture: not dec. 100.

^Column: (pack/cap) PACK

CAS NO.






74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethehe 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorometharie 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-5>entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 3.

38. 5. 5. 5. 5. 5. 5.

10. 5. 5. 10. 5. 5. 5. 5. 5. 5. 5. 5. 5. 10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ

U U U U U U U U U U U U U U U U U U U U U U U u u u u u

FORM I VOA 1 /87 Rev.

69 300387

«



EPA SAMPLE NO.

T-BLANK b Name: INTECH

ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

Matrix: (soil/water) WATER Lab Sample ID: J{( ( (bk- f

Sample wt/vol: 5.0




, Number TICs found: 0






CAS NUMBER

1. 2. 3. 4. 5. 6. 7. 8.

k. 9-• 10. Fii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.

COMPOUND NAME _-

RT EST. CONC. Q


70 3003Q8


EPA SAMPLE NO.

#

60-62' b Name: INTECH Contract: 68-D9-0048

Lab Code: INTECH Case No.: 11185 SAS No.: SDG No


(g/mL) G Sample wt/vol: 5.0




CAS NO. COMPOUND

ANSON

Lab Sample ID: J U I l ^ ^ ' l

Lab File ID: C9877





74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichlor6ethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane


10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-&entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 styrene 1330-20-7 Xylene (total)

13. 13. 13. 13. 7.

26. 6. 6. 6. 6. 6. 6.

13. 6. 6.

13. 6. 6. 6. 6. 6. 6. 6. 6. 6.

13. 13. 6. 6. 6. 6. 6. 6. 6.

U U U U B B U U U U U U U U U U U U U U U u u u u u u u u u u u u u


75 300389


EPA SAMPLE NO.

^ ^ b Name: INTECH

^ R b Code: INTECH Case No.: 11185

"'••Matrix: (soil/water) SOIL

—Sample wt/vol: 5.0 (g/mL)

'' Leve1: (1ow/med) LOW

*"% Moisture: not dec. 23.

"column: (pack/cap) PACK

-._ Number TICs found: 0

60-62' Contract: 68-D9-0048


Lab Sample ID: T(HI^9-\

G Lab File ID: C9877



Dilution Factor:


1 . 0 0

CAS NUMBER

1. 2. 3, 4. 5. 6. 7. 8. 9.

110. Fll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27. 28. 29. 30.



76 300390


EPA SAMPLE NO.

:.ab Nane: INTECH




L,evel: (low/med) LOW


rolumn: (pack/cap) PACK

74-76' Contract: 68-D9-0048

11185 SAS No.: SDG No.: ANSON

Lab Sample ID: XUllBf-'^^

Lab File ID: C9878



CAS NO, COMPOUND

Dilution Factor:

CONCENTRATION tJNITS: (ug/L or ug/Kg) UG/KG

1 . 0 0

Q

7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane 54 0-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7 -18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 -Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene iuu-4 2-b Styrene


12. 12. 12. 12. 6.

11. 6. 6. ' 6. 6. 6. 6.

12. 6. 6.

12. 6. 6. 6. 6. 6. 6. 6. 6. 6.

12. 12. 6. 6. 6. 6. 6.

1:

u u u u B BJ U U U U U U U U U U U u u u u u u u u u u u u u u u u u

FORM I VOA 1 /87 R e v .

300391 81

m IE

VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Name: INTECH

::.:jab Code: INTECH

74-76' Contract: 68-D9-0048

Case No.: 11185 SAS No.: SDG No.: ANSON

-Matrix: (soil/water) SOIL

•Sample wt/vol: 5.0

-jevel: (low/med) LOW




Lab Sample ID: J/Z/Z f-Z






CAS NUMBER

1. 2. 3. 4. 5. 6. 7,

^ 8 .

P9. • 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27.

29. 30.



300392 82


EPA SAMPLE NO.

F-BLANK Lab Name: INTECH Contract: 68-D9-0048

Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No


ANSON

Lab Sample ID: J Ull^^-^

Sample wt/vol: 5.0



polumn: (pack/cap) PACK

CAS NO.



Date Analyzed: 12/ 2/91



74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 7 5-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 7 9-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene /9-34-b 1,1, 2, 2-Tetrachloroethane

108-8 8-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene lOO-42-b Styrene


10. 10. 10. 10. 4. 7. 5. 5. 5. 5.

17. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U u u u BJ J

U U U U

U u u u u u u u u u u u u u u u u u u u u u u


300 393^ 87

^Sb


EPA SAMPLE NO.

lb Name: INTECH

•U.ab Code: INTECH Case No.: 42-64-85SAS No

-Matrix: (soil/water) WATER

"•Sample wt/vol: 5.0

-'-Bevel: (low/med) LOW


~:olumn: (pack/cap) PACK

F-BLANK

(g/mL) ML


SDG No.: ANSON

Lab Sample ID: Xltil$^~'^

Lab File ID: A6403




Number TICs found; CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

]

CAS NUMBER

1. 2. 3 . 4 . 5. 6.

fc.^-^ 8 . W s . • 10. 11. 12, 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.

COMPOUND NAME RT =======:=

EST. CONC. Q


300394 88



EPA SAMPLE NO.

T-BLANK ab Name: INTECH

"Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON

Matrix: (soil/water) WATER Lab Sample ID: Z K l ^ P ' ^

Sample wt/vol: 5.0




CAS NO,






74-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane


10061-02-6 trans-1,3-Dichloropropene 7 5-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene


10. 10. 10. 10. 4. 3. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ J

U U U U U U U u u u u u u u u u u u u u u u u u u u u u

FORM I VOA

94

1/87 Rev.

300395

^ib


EPA SAMPLE NO.

Name: INTECH


" atrix: (soil/water) WATER

'Sample wt/vol: 5.0





T-BLANK Contract: 68-D9-0048

42-64-85SAS No.: SDG No.: ANSON

Lab Sample ID: XKI^^S' '






CAS NUMBER

1. 2. 3. 4. 5. 6.

^ V. \ % . P 9 . • 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27.

29. 30.


FORM I VOA-TIC 1 /87 R e v .

95 300396

IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

I I 1111142-02

ab Name: INTECH Contract: 68-D9-0048 i

Lab Code: INTECH Case No.:fl-^V-^r SAS No.: SDG No. :/^/<?/

«.a t r 1 X : [soil /water] SOIL

^•ample wt/vol: 30.10 [g/mL] G

Level: [low/med] LOU)

Moisture: />-oTdec. j" eitc • O

Extraction: [SepF/Cont/Sonc] SONC

.OC Cleanup: [Y/N] N pH: 7.5

Lab Sample ID: ff-^J'^

Lab File ID: >BeO30

^ Date Received: IQ'^S 1/91

Date Extracted% #1/25/91


Dilution Factor: \ • \fi

CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG

108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-

106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-•68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-cl^lo^oetl^yl )ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene - B e n z y l a Icolno 1 -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -3&4-MethyIpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene -1 sophorone -2-Ni t ropheno1 -2,4-Dimethyl phenol - B e n z o i c acicJ -bis(2-Chloroethoxy)methane -2,4-Dichlorophenol -1,2,4-Tr ichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -HexachlorocyclopentacJiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene

Q

1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 i 380 1 380 1 380 1 380 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 360 1 360 1 1900 1 380 1 380 1 . 380

1 i lU 1 lU 1 lU 1 iU 1 lU 1 IU i IU 1 iU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 iU 1 IU 1 IU i IU 1 IU 1 IU 1 iU 1 IU 1 1 r l 3b03S^

FORM I S U - 1 187

IC 5EMI VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

I 1111142-02 ab Na-^e: INTECH

„ab Cod?: INTECH Case No.

iatrix: [soil/water] SOIL

Contract: 68-09-0048 I

: ( f l ^ l f ( ( ^ , ^ rS f^S No.: SDG No.: ' ^ ^ / ^ ' ^

lample ut'-vol: 30.10 [g/mL] G

Level: [low/med] LOW

, Moisture: fiat d e c . 0 f t l - |3


-PC Cleanup: [Y/N] N pH: 7.5

Lab Sample ID: t^^- (*Y

Lab File ID: >B8030


Date Extracted: 11/25/91


Dilution Factor: \ . 00


99-83-51-

100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan i1ine -Acenaphthene • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o 1 •Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenan threne -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene

Q

1 1900 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 1900 1 1900 1 380 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 380 1 76 0 1 380 1 380 1 180 1 380 i 380 t 380 1 380 1 360 1 380 1 380

I iU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I : IU IU IU IU IU IU IU I

FORM I SU-2 188

300398

IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIUELY IDENTIFIED COMPOUNDS

tab Name: INTECH

..atrix: f. soil/water) SOIL

-Cample wt-^vol: 30.10 (g/mL) G

Level: (low/med) LOU)

Moisture: /Widec . |' . ied • 1}

Extraction: (SepF/Cont/Sonc) SONC

PC Cleanup: (Y/N) N pH: 7.5



EPA SAMPLE NO,

I 1111142-02 I

/ Lab Sample ID: ^^"^3

Lab File ID: >Be030

Date Received: ;iyi/211/9



Dilution Factor: | •00


CAS NUMBER : = = = = = = s=r = B a

1.

COMPOUND NAME

Unknown

RT E B ^ ^ C3 e

2 . 2 5

EST. CONC.

1 5 0 .

Q

FORM I S U - T I C

189 1/87 Rev.

300399


EPA SAMPLE NO,

I 1111142-03 '~3b Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : 4*'tV^^^ SAS No.: SDG No.: /^^/^/^

atrix: [soil/water] UJATER

Sample wt/vol: 1000 [g/mLl ML

s^evel: [low/med] LOU)

""Moisture: dec 100.

Extraction: [SepF/Cont/Sonc] SERF

=C Cleanup: [Y/N] N pH: 8.0

Lab Sample ID: f - S ^ / ^ l ^

Lab File ID: >B8027

Date Receieved:'^ll'^^l^^l

Date Extracted! 4l/22/91



CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L

108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-•47-8-•68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene •1,4-Dichlorobenzene -Benzyl alcohol •1,2-Dichlorobenzene •2-Methylphenol •bis(2-chloroisopropyl)ether •4-Methyl phenol •N-Nitroso-di-n-propy lamine -Hexachloroe thane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzoic acid -bis(2-Ch1oroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol •2-Chloronaphthalene •2-Ni t roan i1ine •Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene

Q

1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I S U - 1 194 300460

IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

I I I 1111142-03 I

Tab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case Ho. : S-2-if^'f^ SAS No.: SDG No. : -^/v//^

Iatrix: [soil/water] WATER Lab Sample ID: ^ " 6 ^ 4 ^ ^

Sample wt/vol: 1000 [g/mLl ML Lab File ID: >B8027

.tevel: [low/med] LOW Date Rece i©vedt-*gil/21/91

Mo 1s t u re dec 100,


;PC Cleanup: [Y/N] N pH: 8.0

Date Extracted: -11/22/91



CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L

99-83-51-100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-•99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan iIine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 -Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethy1hexy1)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene

Q

1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I SU-2 195 300401



EPA SAMPLE NO,

I I 1111142-03

ib Nam« INTECH Contract: 68-D9-0048

atrix: (soil/water) WATER

Sample wt•vo1: 10 00 (g/mL) ML

a eve 1 : i 1 ow/med ) LOW

^Moisture: dec. 100.

Extraction: (SepF/Cont/Sonc) SERF


"fvlumber T ICs f o u n d : 0

Lab Sample ID: f - ^ L A ' ^ ^ ^

Lab File ID: >B8027

Date Received: H'^21/91



Di lut ion Factor: ) .00

CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L

-••- 1 I I I CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q

j ' ~ = = = = S S = = = = = S : = B K j S S B B C E S S S B S S S S K S B n s e S S E S S S S S S S K K S : 1 S S B X B K S I S S 1 S S S B S B S B S K B S E | B B S S S

V ' 1 I I I I I

r 1 I I I J. 1 I I I

-,- 1 I I I I I I I I

1 I I I

I I I I I 1 1 I I I

T 1 I I 1 I I I I I

1 1 I I I --• 1 I I I

r 1 I I I I I I I 1 '

- ^ 1 ' I I 1

FORM I SU-TIC

196

1/87 Rev.

300402


EPA SAMPLE NO.

I I 1111142-04

"ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : 2-^'^5'~SAS No.: SDG No.:^/v/«'«<

atrix: [soil/water] SOIL

^ample wt/vol: 30.52 [g/mLl G

,„evel: [low/med] LOW

" Moisture: / ^ f dec . a; fiV^ • 2 3


PC Cleanup: [Y/N] N pH: 8.0

Lab Sample ID: 1 2 M - f * "

Lab File ID: >B8031

Date Received: -4|L/21/91



Dilution Factor: }•oO

CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG

108-111-95-

541-106-100-95-95-

108-106-621-67 98-78 88 105 65-

111' 120-120-91-

106^ 87-59^ 91-77-88-95-91-88-

131-208-606-

-95-2--44-4--57-8--73-1--46-7-•51-6-•50-1-•48-7-•60-1--44-5-•64-7--72-1--95-3--58-1--75-5--67-9--85-0--91-1--83-2--82-1-•20-3--47-8--68-3--50-7--57-6--47-8-•06-2--95-4--58-7--74-4-•11-3--96-8-•20-2-

•Phenol •bis(2-chloroethyl)ether •2-Chloropheno1 •1,3-Dichlorobenzene •1,4-Dichlorobenzene -Benzyl alcohol •1,2-Dichlorobenzene -2-Methylphenol •bis(2-chloroisopropyl)ether -3&4-MethyIpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)methane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene - 4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene

Q

1 43 0 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 430 1 430 1 43 0 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 430 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 430 1 430 1 430 1 2100 1 430 1 430 1 43 0


FORM I S U - 1 HJU

300403


EPA SAMPLE NO.

I I 1111142-04

Tab Name: INTECH Contract: 68-D9-0048 I

"tab Code: INTECH Case No.: ^ l - y f ^ f ^ ' SAS No.: SDG No.: < 4 ^ / < ^

Iatrix: [soil/water] SOIL

Sample wt/vol: 30.52 [g/mLl G

,,^evel: [low/med] LOW

't Moisture: /y«f d e c . 11 U t^ . JZ


;PC Cleanup: [Y/N] N pH: 8.0

Lab Sample ID: ] 7 c ' \ ' i l

Lab File ID: >B8031

Date Received: i|/'21/91



Dilution Factor: l.oo


99-83-51-100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-•81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

•3-Ni t roan i1ine •Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Dibenzofuran -2,4-Dinitrotoluene •Diethylphthalate -4-Chlorophenyl-phenyl ether •Fluorene -4-Ni t roan i1i ne -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-EthyIhexy1)phthalate -Di-n-octylphthalate -Benzo(b)fiuoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene •Dibenz(a,h)anthracene -Benzo(g,h,i)perylene

Q

1 2100 1 43 0 1 43 0 1 2100 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 850 1 430 1 43 0 1 220 1 43 0 1 430 1 43 0 1 430 1 430 1 430 1 430

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU

I J IU IU IU IU IU IU IU I

FORM I SU-2 200 300404



EPA SAMPLE NO,

I I 1111142-04

£ab Name: INTECH Contract: 68-D9-0048

,,„a t r 1 X : i s o i 1 / wa t e r ) SO IL

-ample wt-'vol: 30.52 (g/mL) G

Level: '.low/med) LOW

Moisture: ^ o f d e c . 7-1 . U«^. 2 3




Lab Sample ID: ) l< i - i ' i l

Lab File ID: >Be031

Date Received: €i./21/91



Dilution Factor: \ . .00


_ CAS NUMBER 1 COMPOUND NAME

^^^ . - 1 Unknown

1 1 1 1

1 1 1

1 1 -L 1

T" 1 1 1

1 1 1

r 1 1 . 1

-.- \

1 1

^ ^

RT : B B B B a

5 . 04

EST. CONC. E ^ B B B B B B B B

2 1 0 . B B S= B

Q

FORM I S U - T I C 201 1/87 Rev.

300405


EPA SAMPLE NO,

I 1111142-05 .ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH _.Case No.: A2'^f-^^rSAS No.: SDG H o . : ^ ^ i ^ * ^

Iatrix: [soil/water] WATER Lab Sample ID: ^ - $ U J < ^

Sample wt/vol: lOOO [g/mLl ML Lab File ID: >B8028

«ievel: [low/medl LOW Date Rece ieved:''|^1/21/91

"•"'. Moisture: dec 100. Date Extracted! 11/22/91


;PC Cleanup: [V/N] N pH: 8.0


Dilution Factor: f.OO


108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-

106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -4-Methylphenol -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-DimethyIpheno1 -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan iIine •Dimethylphthalate •Acenaphthylene •2,6-Dinitrotoluene

Q

1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 90 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU . 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I S U - 1 206 300406


EPA SAMPLE NO,

1111142-05 ,ab Name: INTECH Contract: 68-D9-0048 . I

Lab Code: INTECH Case No.: f -tV-??' 5^5 ^o. : SDG Ho. :/l^f^fi^

,„,atrix: [soil/water] WATER Lab Sample ID: f — ^ t ^ ^ ^

-example wt/vol: 1000 [g/mL] ML Lab File ID: >B8028

Level: [low/med] LOW Date Rece ievedr^l/21/91

Moisture: dec 100. Date Ext ractedJ'l^ 1/2 2/91




Dilution Factor: |.00


99-83-51-

100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-64-

206-129-85-.91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

•3-Ni t roan iIine •Acenaphthene •2,4-Dinitrophenol •4-Nitropheno1 •Dibenzofuran •2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenyl amine •4-Bromophenyl-phenylether •Hexachlorobenzene •Pentachloropheno1 •Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e

Q

1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 5 0 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 3 1 10 1 10 1 10 1 10 1 10 1 10 1 10

1 i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU . 1 IU 1 1 1

FORM I SU-2 207 300407

IF >EMIUOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO,

I 1111142-05 .ab Nc- INTECH Contract: 68-D9-0048 I

latri.: soil/water) WATER

-Sample ct 'vo1: 10 00 (g/mL) ML

"'iteve 1 : '1 ow/med ) low

~oMoi£ti^re: dec. 100.


;PC Cleanup: (Y/N) N pH: 8.0


Lab Sample ID: ^ - ^ ^ , ^ ^ <

Lab File ID: >B8028

Date Received: 1^/21/91



Di lut ion Factor: i.00


CAE NUMBER 1 COMPOUND NAME 1 =: = = = = = =r=: = = = = = = B B | B S B S E B B B B B B B S S B S B B B B B B B S B B B B

1 I

W • 1 1 1

1 1 1

"1 1 1 1

—: 1 1 1

1

1 1 J 1

.... j

1 1

1 1 -1 1

" i ^ ^

RT EST. CONC. S B B S B B B B B B ^ B

Q

FORM I SU-TIC

208 1/87 Rev.

30040&


EPA SAMPLE NO.

1111164-01 .ab NaT-e: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Ease H o . - A i ' ( A ^ ^ ^ SAS No.: SDG No. :/?/l/c*v

Lab Sample ID: 4<^ ?

Lab File ID: >68065

Date Received: ;r|S i 26/91

I Moisture: .voTdec. ^% o(ti:> 5*2.


.PC Cleanup: [Y/N] N pH: 7.5

..Jatrix: [soil/water] SOIL

.Sample wt--vol: 30.25 [g/mL] G

tieve 1 : [low/med] LOW

Date Extractedl!!3.1/27/91


Dilution Factor: ).oo


108 111 95

541 106 100 95 95

108 106 621 67 98 78 88 105 65'

111. 120. 120. 91. 106 87 59 91 77 88 95 91-88.

131-208-606-

-95-2--44-4--57-8--73-1--46-7--51-6--50-1--48-7--60-1--44-5--64-7--72-1--95-3--58-1--75-5--67-9--85-0--91-1--83-2--82-1--20-3--47-8--68-3--50-7--57-6--47-8--06-2--95-4--58-7--74-4--11-3-•96-8--20-2-

-Pheno I -bis(2-chloroet -2-Chloropheno I -1,3-Dichlorobe -1,4-Dichlorobe -Benzyl alcohol -1,2-Dichlorobe -2-Methylphenol -b is(2-ch loro is -3&4-Methylphen -N-Ni t roso-d i-n -Hexachloroetha -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylph -Benzoic acid -bis(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor •Naphthalene -4-Chloroan i1 in -Hexachlorobuta -4-Chloro-3-met -2-Methylnaphth -Hexachlorocycl -2,4,6-Trichlor -2,4,5-Tr ichlor •2-Chloronaphth -2-Nit roan i1ine -DimethyIphthaI -Acenaphthylene -2,6-Dini troto1

hy1)ether

nzene nzene

nzene

opropyl)ether ol -propylamine ne

eno I

hoxy)methane eno 1 obenzene

e d iene hyIpheno1 a lene opentad iene opheno I opheno 1 a lene

ate

uene

Q

690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690

3400 690 690 690 690 690 690 690 690 69 0 690 690 690 3400 690 690 690

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU

I

FORM I SU-1 212 300409


EPA SAMPLE NO,

I 1111164-01

ab Nan-,e: INTECH

Lab Code: INTECH Case No,


Contract: 68-D9-0048 I

U t - e ^ ' $ ^ SAS No.: SDG Ho . :/}/\^/(^<^

Sample ut/vol: 30.25 [g/mL] G

•Sevel: [low/med] LOU

~. Moisture: voTdec. f i ^ ^*€ ' ^^



Lab Sample ID: t ° ' i ^ ^

Lab File ID: >B8065




Dilution Factor: |.oo

CAS NO. COMPOUND CONCENTRATION UNITS: lug/L or ug/Kg] UG/KG

99 83 51

100 132 121 84^

7005 86^

100 534 86

101-118 87 85

120 84

206 129 85 91 56

218 117-117. 205^ 207 50

193 53-

191'

-09-2--32-9--28-5--02-7--64-9--14-2-•73-7-•72-3--73-7-•01-6-•52-1-•30-6--55-3-•74-1--86-5--01-8--12-7--74-2--44-0--00-0--68-7--94-1--55-3-•01-9-•81-7--84-0--99-2--08-9--32-8--39-5-•70-3-•24-2-

-3-Ni t roan i1ine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 -Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methylphenol •N-Nitrosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate •Fluorant hene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fiuoranthene -Ben2o(a)pyrene - Indeno(1,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e

Q

3400 690 690

3400 690 690 690 690 690

3400 3400 690 690 690

3400 690 690 690 690 690 690 1400 690 690 690 690 690 690 690 690 690 690


FORM I SU-2 213 3004tO



EPA SAMPLE NO,

I 1111164-01 C'ab Name: INTECH

...atrix: tsoil/water) SOIL

'-ample wt/vol: 30.25 (g/mL) G


Moisture: .••'Tdec. f/. . fiiec • f i^


. C Cleanup: (Y/N) N pH: 7.5



Lab Sample ID: «>-^Z

Lab File ID: >B8065

Date Received: 4^-^26/91



Dilution Factor: \.oo


CAS NUMBER

m-

m

COMPOUND NAME 1 RT B B B B B B B B B B B B B B S B B B B B B B B B B B B B | B B B B B B B B

Unknown i 3.62

EST. CONC,

48 0 .

Q

FORM I S U - T I C

214 1/87 Rev. ^ ^.

3004U


EPA SAMPLE NO.

I I 1111164-02

•.ab Na-e: INTECH

Tab Cede: INTECH


Case No.: 4'? •'^^"?^ SAS No.: SDG No.: ^o,/<^^


Sample wt-vol: 30.21 [g/mLl G

.-...evel: [low/med] LOW

"i Moisture: -^aTdec . a.- c/et • t l



Lab Sample ID: "75'-?7

Lab File ID: >B8066




Dilution Factor: f.oo


108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-111-120-120-91-106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -3&4-MethyIphenoI -N-Nitroso-di-n-propylamine -Hexachloroethane -Ni t robenzene - Isophorone -2-Ni t ropheno1 -2>4-Dime thy I phenol -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -l,2,4-Trichloroben2ene -Naphthalene -4-Chloroani1ine -Hexachlorobutad iene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dime thyIphthalate -Acenaphthylene -2,6-Dinitrotoluene

Q

1 43 0 1 430 1 430 1 430 1 43 0 1 43 0 1 430 1 43 0 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 430 1 43 0 1 2100 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 430 1 430 1 2100 1 430 1 430 1 43 0


FORM I SU-1 218 3004\2'


EPA SAMPLE NO,

I 1111164-02 .ab Name: INTECH

Tab Code: INTECH


Sample wt/vol: 30.21 [g/mL] G

.,..eve 1 : [ 1 ow/med ] LOW

Ji Moisture: .yoT dec . ^3 C , 2 3

"Extraction: [SepF/Cont/Sonc] SONC

';PC Cleanup: [Y/N] N pH: 7.5


Case No. : 4-^-^^-^rsAS No.: SDG No . : ^^/c^^

Lab Sample ID: 7f-77

Lab File ID: >B8066

Date Received: -11/26/91

Date Extracted: 3.1/27/91


Dilution Factor: \ . c o

C H S NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG

99-83-51-

100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-•81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan i1ine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 - D i b e n z o f u r a n - 2 , 4 - D i n i t r o t o l u e n e • D i e t h y l p h t h a l a t e • 4 - C h l o r o p h e n y 1 - p h e n y l e t h e r • F l u o r e n e •4-Nitroani1ine •4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachlorophenol -Phenanthrene -Anthracene -Di-n-butylphthalate -F1uoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Ben2o(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Ben2o(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene •Dibenz(a,h)anthracene •Benzo(g,h,i)perylene

Q

1 2100 1 43 0 1 430 1 2100 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 43 0 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 860 1 43 0 1 430 1 43 0 1 430 1 430 1 43 0 1 430 1 430 1 430 1 430


FORM I SU-2 219 30041^'



EPA SAMPLE NO,

1111164-02 Ilab Name: INTECH

..Jatriv: (soil/water) SOIL

"ample wt/vol: 30.21 (g/mL) G


i Moisture: ..-ordec. i'j . fl^<', 2 3


• PC Cleanup: (Y/N) N pH: 7.5



Lab Sample ID: 75'-77

Lab F i l e ID : >B8066 •?*••

Date R e c e i v e d : 3 ^ / 2 6 / 9 1

Date Extracted; 11/27/91


Dilution Factor: ( . 0


CAS NUMBER COMPOUND NAME

Unknown

RT : ^ ^ B s

3.61

EST. CONC. E B B B B S B S B B B

520.

Q

FORM I SU-TIC 220 1/87 Rev,

300414


EPA SAMPLE NO.

I I I I111164-02RE I

I .ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : 2-^^-^T SAS No.: SDG Ho. : ^'^i^f*-

J a t n x : [soil/water] SOIL Lab Sample ID: 1 ^ ~ ^ 7

Sample wt/vol: 30.21 [g/mL] G Lab File ID: >B80e4

Tleve 1 : [ low/med ] LOW

; Moisture: /voT'dec. 7" ifitc 2 3


.;PC Cleanup: [Y/N] N pH: 7 .3

Date Received: "tl/26/91



Dilution Factor: ).oo


108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroethyl)ether •2 -Ch lo ropheno1 - 1 , 3 - D i c h l o r o b e n z e n e • 1 , 4 - D i c h l o r o b e n z e n e •Benzyl a l c o h o l • 1 , 2 - D i c h l o r o b e n z e n e •2-Me t h y I p h e n o 1 •bis(2-chloroisopropyl)ether •3&4-MethyIpheno1 •N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - I sophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methy 1 naphtha Iene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine •Dime thyIphthalate •Acenaphthylene •2,6-Dinitrotoluene

Q

^ i-

43 0 43 0 43 0 43 0 43 0 43 0 43 0 43 0 430 43 0 43 0 43 0 43 0 43 0 430 43 0

2100 43 0 43 0 43 0 43 0 43 0 43 0 43 0 430 43 0 43 0 430 430

2100 430 43 0 430

1 1 IU I IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 ,, A 3<i04l5

FORM I S U - 1


EPA SAMPLE NO.

I I111164-02RE I .ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case Ho. : ^ 2 - ( f ^ - f ^ Sf^S No.: SDG No. : A i ^ '

.Jatnx: [soil/water] SOIL Lab Sample ID: 7S^ 7 7

-Sample wt/vol: 30.21 [g/mLl G

Tevel: [low/medl LOW

. Moisture: ,voT dec. M / i f - 5 3


:PC Cleanup: [Y/N] N pH: 7.5

CAS NO. COMPOUND

Lab File ID: >B8064

Date Received: ;^/26/91



Dilution Factor: .<jo

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q

99-83-51-100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan i1ine -Acenaphthene • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o I •Dibenzofuran -2,4-Dinitrotoluene -DiethyIphthalate -4-Chlorophenyl-phenylet her •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methyIpheno1 •N-Nitrosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene •Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene •ButyIbenzyIphtha late -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-EthylhexyI)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)py'~ene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e

1 2100 1 43 0 1 430 1 2100 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 860 1 430 1 430 1 43 0 1 43 0 1 43 0 1 430 1 430 1 43 0 1 430 1 43 0


FORM I SU-2 225 300416



EPA SAMPLE NO.

I111164-02RE Lab Name: INTECH

liatri-;: i soil/water) SOIL

"":.ample wt/vol: 30.21 (g/mL) G


b Moisture: .yoT d e c . 23 • ^ ^ • 2.1


-oPC Cleanup: (Y/N) N pH: 7.5



Lab Sample ID: 75^-77

Lab File ID: >B8084

Date Received: Jt!4/26/91



Dilution Factor: \-oo


1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q j = = = = s: = = = = s= = B B B B B ( ts = x = m K m m K ^ = ^ B X s = a s B = a s s = a = a x | B B B B S B B S | B B B B B B B B B B B B B | = s i — s s

^ 1 . - - [Unknown 1 3 .58 1 600. 1 J

I I I I I

I I I I I 1 1 I I I

, 1 I I I 1 1 - I I I

1 1 I I I 1 1 I I 1

i 1 I I I I I I I I

1 1 I I 1 ~ 1 I I I

1 1 I I 1 I I I I I

. ^ 1 . I I 1 B 1 I I I

FORM I SU-TIC 226 1/87 Rev. 3064it


EPA SAMPLE NO.

I I I 1111164-03 I

_ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case Ho. : ' ^ ^ - t f ^ ' ^ SAS No.: SDG No.: t^^J^^

-Matrix: [soil/water] WATER

Sample wt/vol: 1000 [g/mL] ML


yi Moisture: dec 100.


SPC Cleanup: [Y/N] N pH: 7.5

Lab Sample ID: r - $ t / i ^ K

Lab File ID: >B8083

Date Receieved: il/26/91



Di lut ion Factor: ).00


108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-

106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl aIcoho 1 •1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -4-Methylphenol -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene -1 sophorone -2-Nitropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichloropheno1 -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutad iene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Tr ichloropheno1 -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate •Acenaphthylene -2,6-Dinitrotoluene

Q

1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 ^1

FORM I S U - 1 230 3'0041B


EPA SAMPLE NO,

I 1111164-03 ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : ^'^*''?^ SAS No.: SDG No.: ^ ^ i < > ^

,. atriv: [soil/water] WATER

—ample wt/vol: 1000 [g/mLl ML

H'evel: [low/med] LOW

Mo ISt ure: dec 100.



CAS NO, COMPOUND

Lab Sample ID: r - $ L ^ ^ ^

Lab File ID: >B8083

Date Receieved: :ll/26/91

Date Extracted: il/27/91


Di lut ion Factor: |.00

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L Q

99-83-51-100-172-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-•44-0-•00-0-68-7-•94-1-55-3-01-9-81-7-84-0-99-2-•08-9-•32-8-•39-5-70-3-24-2-

-3-Ni t roan iIine •Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Dibenzofuran •2,4-Dinitrotoluene •Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1i ne •4,6-Dinitro-2-methylphenol •N-Nitrosodiphenylamine •4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 - Ph enanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e

1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU . 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I SU-2 231 300419



EPA SAMPLE NO,

I 1111164-03 •tab Name: INTECH Contract: 68-D9-0048

..'-.atri>: (soil/water) WATER

^ample wt/vol: 1000 (g/mL) ML


Mo ISt ure: dec. 100.

Extraction: CSepF/Cont/Sonc) SERF



Lab Sample ID: lf-'SLi^»'K

Lab File ID: >B6083

Date Received: .^/26/91



Di lut ion Factor: /.00


•... CAS NUMBER COMPOUND NAME B S S B B B B B :

RT EST. CONC, Q

FORM I S U - T I C

232 1/87 Rev.

300420

m IB

E.EMIUOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.

I 1111185-01 .ab Name: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : f/-^*'-^f~ SAS No.: SDG No.: ' ' A''

iatrix: [soil/water] SOIL

^Sample wt/vol: 30.40 [g/mLl G

„^eve 1 : [low/medl LOW

""' Moisture: /VoTdec. 1 1 ffec- 1 \



Lab Sample ID: ( jO^y i

Lab File ID: >B8095




Dilution Factor: l.oO


108^ 111 95

541-106^ 100-95-95-

108-106-621-67-98-78 88.

105' 65

111-120-120-91-106' 87 59 91 77 88-95-91-88-

131-208-606-

-95-2--44-4--57-8--73-1--46-7--51-6-•50-1--48-7--60-1--44-5--64-7--72-1--95-3--58-1--75-5--67-9--85-0-•91-1-•83-2-•82-1--20-3--47-8--68-3--50-7--57-6--47-8-•06-2-•95-4-58-7-•74-4-•11-3-•96-8-20-2-

-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 - 1 , 3 - D i c h l o r o b e n z e n e - 1 , 4 - D i c h l o r o b e n z e n e - B e n z y l a l c o h o l - 1 , 2 - D i c h l o r o b e n z e n e - 2 - M e t h y l p h e n o l - b i s ( 2 - c h l o r o i s o p r o p y l ) e t h e r - 3 & 4 - M e t h y I p h e n o 1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dime thyIpheno1 -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1 ,2,4-Tr ichlorobenzene -Naphthalene -4-Chloroani1ine - He xachlorobutadiene -4-Chloro-3-methyIpheno1 -2-Methylnaphthalene - Hexach1orocycI open tadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol •2-Chloronaphthalene •2-Ni t roan i1ine •Dimethylphthalate •Acenaphthylene •2,6-Dinitrotoluene

Q

1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 430 1 43 0 1 430 1 2100 1 430 1 430 1 430 1 r»o tr


FORM I SU-1 300421


EPA SAMPLE NO,

I 1111185-01 ab Narr.e: INTECH Contract: 68-D9-0048 I

Lab Code: INTECH Case No. : 42-irV'^5 SAS No.: SDG No.: -^V^^

atrix: [soil/water] SOIL

.Sample wt/vol: 30.40 [g/mL] G

-evel: [low/med] LOW

""'Moisture: /v^Tdec. f^ ^t^. 13



Lab Sample I D : ^ - ^ ? '

Lab File ID: >B8095




Dilution Factor: \.(jo


99' 83^ 51-

100-132-121-84-

7005-86-

100-534-86^

101-118-87^ 85

120^ 84

206^ 129 85 91 56

218 117. 117. 205^ 207. 50-

193 53-

191-

•09-2-•32-9-•28-5-•02-7-•64-9-•14-2-73-7-•72-3-73-7--01-6-•52-1--30-6--55-3--74-1-•86-5--01-8--12-7-•74-2--44-0--00-0--68-7--94-1--55-3--01-9-•81-7--84-0--99-2--08-9-•32-8--39-5-•70-3-•24-2-

•3-Ni t roan i1ine •Acenapht hene •2,4-Dinitrophenol •4-Ni t ropheno1 •D ibenzo furan •2,4-Dinitrotoluene •Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol •N-Nitrosodiphenyl amine •4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate •Fluoranthene -Pyrene - B u t y l b e n z y l p h t h a l a t e - 3 , 3 ' - D i c h l o r o b e n z id i n e - B e n z o ( a ) a n t h r a c e n e - C h r y s e n e -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene • B e n z o ( a ) p y r e n e - I n d e n o ( l , 2 , 3 - c d ) p y r e n e • D i b e n z ( a , h ) a n t h r a c e n e - B e n z o ( g , h , i ) p e r y l e n e

Q

1 2100 1 43 0 1 430 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 43 0 1 43 0 1 2100 1 43 0 1 430 1 43 0 1 430 1 43 0 1 43 0 1 850 1 430 1 430 1 36 1 43 0 1 430 1 430 1 430 1 430 1 430 1 43 0

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I SU-2 23G 300422



"tab Name: INTECH Contract: 68-D9-0048

EPA SAMPLE NO.

I I I 1111185-01 1 I _l

• atrix: (soil/water) SO IL

""ample wt--vol: 30.40 (g/mL) G

Level: Clow/med) LOU

Mo 1 s t u r e : .'>6t"dec . j 3 . (/((:, 2 I


,.PC Cleanup: (Y/N) N pH: 8.0


Lab Sample ID: j, _^2

Lab File ID: >B8095

Date Received: lPl/27/91



Dilution Factor: \ . o o


CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q { = B S : = = =:=: = =: = = S B B S B \ = S S X K t S ^ B S = = = = ^ S S = ^ m a S S S S i = aSXSS | B B B B S B B S 1 B B B B B B B B B B B B B J B B B B S

i l ^ l . 1 4 1 - 7 9 - 7 l 3 - P e n t e n - 2 - o n e , 4 - m e t h y l - ( 8 1 2 . 6 7 1 1 7 0 . 1 J ^ ^ 2 . . - - l A l d o l C o n d e n s a t i o n 1 3 . 5 5 1 8 5 0 0 . 1 3

1 1 I I I

i 1 I I '

1 1 I I 1

I I I I I '- 1 I I I

1 1 I I I I I I I I

1 1 I I I 1 I I 1

I I I I I j. 1 I I I

T" 1 I I I I I i l l

^ ^

FORM I SU-TIC 1/87 Rev.

237 300423'

IB Z.EMIUOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

I 1111185-02 .at \ < f ' f - INTECH Contract: 68-D9-0048 I

ab Core: INTECH Case No. : ^ 2 - ^ ^ ' ?^'SAS No.: SDG No . :/?/v/^/^

riatri,-: [soil/water] SOIL

• ample .. t • WQ 1 : 30.51 [g/mL] G

Level: Llow/med] LOW

J Mo 1 5 • _ - e : ,'j'ot dec . |g siic- \%

-E:xtrac';cn: [ SepF/Con t/Sonc ] SONC

CiPC Cleanup: [Y/N] N pH: 7.3

COMPOUND

Lab Sample ID: 7f- 76.'

Lab File ID: >B8096




Dilution Factor: \ .00

CHS NO.

1 106-1 ill-1 ''? -! - 4 1 -1 10 6-i 100-i 95-i 95-i 108-1 106-i 621-i 67-i 98-1 78-1 86-1 105-1 65-i 111-1 12 0-1 120-t 91-1 106-i 87-1 59-i 91-i 77-i 88-i 95-1 91-i 88-i 131-1 208-1 606-

-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-

-2 -4 -8 -1 -7 -6 -1 .7 •1

-5 -7 •1

•3

-1 -5 .9 •0

-1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 •2

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG

-Pheno 1 -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylpheno 1 •bis(2-chloroisopropyl)ether •3&4-MethyI phenol •N-Nitroso-di-n-propylamine •Hexachloroethane -Nit robenzene • Isophorone -2-Ni t ropheno 1 -2,4-DimethyIpheno 1 -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-me t hy1pheno 1 -2-Methylnaphthalene -Hexachloroeyclopentad iene -2,4,6-Trichlorophenol -2,4,5-Tr1chloropheno 1 -2-Chloronaphthalene -2-Ni t roan i1i ne -DimethyIphthalate -Acenaphthylene -2,6-Dinitrotoluene

Q

1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 2000 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 2000 1 400 i 400 1 400

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1

1 ^ 1

FORM I SU-1 •2T3 ^00424


EPA SAMPLE NO,

I 1111185-02 ,ab Name: INTECH Contract: 68-D9-0048 I

• ab Code: INTECH Case No. : /^Z-t'^-^r SAS No.: SDG No.:rfxK/*>'

itatrix: [soil/water] SOIL Lab Sample ID: l ^ - f k /

ample wt/vol: 30.51 [g/mLl G


Moisture: «yol dec . \% o u t - l ^ :

Fxtraction: [SepF/Cont/Sonc] SONC

..-.-C Cleanup: [Y/N] N pH: 7.3

COMPOUND CAS NO.

i 99-1 83-i 51-1 100-i- 172-i 121-i 84-i 7005-i 86-1 100-1 534-1 86-i 101-1 118-i 87-i 85-1 120-1 84-i 206-1 129-i 85-1 91-i 56-1 218-1 117-1 117-1 205-1 207-1 50 1 193 1 53-1 191-

-09--32--28--02--64--14--73--72--73--01--52--30--55--74--86--01--12--74--44--00--68--94--55--01--81--84--99--08--32--39--70--24-

-2 -9 -5-•7

-9 -2 -7 -3 -7--6 -1--6--3 -1 -5 -8 -7 -2 -0 -0 -7 -1 -3 -9 -7 -0 -2 -9 -8 -5 -3 -2

Lab File ID: >B8096

Date Received: ,11/27/91



Dilution Factor: |.ofl

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q

• 3 - N i t r o a n i 1 i ne • A c e n a p h t h e n e • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o 1 • D i b e n z o f u r a n - 2 , 4 - D i n i t r o t o l u e n e • D i e t h y l p h t h a l a t e • 4 - C h l o r o p h e n y 1 - p h e n y l e t h e r • F l u o r e n e • 4 - N i t r o a n i 1 i n e • 4 , 6 - D i n i t r o - 2 - m e t h y l p h e n o l -N -N i t r o s o d i p h e n y l a m i n e - 4 - B r o m o p h e n y 1 - p h e n y l e t h e r - H e x a c h l o r o b e n z e n e • P e n t a c h l o r o p h e n o 1 • P h e n a n t h r e n e • A n t h r a c e n e • D i - n - b u t y l p h t h a l a t e •F l u o r a n t h e n e • P y r e n e -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine - Be nzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene - Benzo(k)fiuoranthene -Benzo(&)pyrene -lndeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene

1 2000 1 400 1 400 1 ' 2000 1 400 1 400 1 400 1 400 1 400 1 2000 1 2000 1 400 1 400 1 400 1 2000 1 400 1 400 1 400 1 400 1 400 1 400 1 800 1 400 i 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU ! IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

FORM I SU-2 244 300425



EPA SAMPLE HO.

I 1111185-02 'Lab Name: INTECH Contract: 68-D9-0048

.iatrix: ( s o i 1 / wa t e r ) SO IL

ample wt/vol: 30.51 (g/mL) G


. Moisture: ,>oTdec. j^ . (/ c. (g


-:.PC Cleanup: (Y/N) N pH: 7.3


Lab Sample ID: 7 ^- '^ ("

Lab File ID: >B8096

Date Received:>iJC4/27/91



Dilution Factor: ).C0


CAS NUMBER

3 .

4127-47 -3

COMPOUND NAME 1 RT B B B B B B B B B B B B S B B B B S B B B S a S B S B B | B B B B B B B B

Cyclopropane, 1,1,2,2-tetram 1 2.66 Aldol Condenset ion (/'/vkfo'o**-/'-J 1 3.55 Unknown Alkane 1 24.35

EST. CONC,

2 0 0 . 7 6 0 0 .

5 6 0 .

Q

J J 3

FORM I S U - T I C

245 1/87 Rev.

300426


EPA SAMPLE NO.

I I 1111185-03

Lab Name: INTECH Contract: 68-D9-0048 I

ab Code: INTECH Case No. : f l" ^-^r SAS No.: SDG Ho.-./J^jf'

Matrix: [soil/water] WATER

...ample wt/vol: 1000 [g/mLl ML

~eve1: [low/med] LOW

SMoisture: dec 100.

xtraction: [SepF/Cont/Sonc] SERF

GPC Cleanup: [Y/N] N pH: 7.0

COMPOUND

Lab Sample ID: F- C/f/VK

Lab File ID: >B8C70

Date Receieved: 11/27/91



Di lut ion Factor: | .00

CAS t

i 108-i 111-i 95-i. 541-i 106-i 100-1 95-i 95-1 108-1 106-1 621-1 67-i 98-i 78-i 88-i 105-i 65-i 111-1 120-i 120-1 91-i 106-i 87-1 59-1 91-1 77-1 88-1 95-1 91-1 88-i 131-1 208-i 606-

-10.

-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-

-2 -4 -8 -1 -7 -6 -1 -7 -1 -5 -7 -1 -3 -1 -5 -9 -0 -1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 •2

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L

-Phenol -b i s(2-ch 1 oroe -2-Chloropheno -1,3-DichIorob -1,4-Dichlorob -Benzyl a Icoho -1,2-Dichlorob -2-Methylpheno •b is(2-ch loro 1 •4-Methylpheno •N-Ni t roso-d i-•Hexachloroeth •N i t robenzene • I sophorone -2-Ni t ropheno1 -2,4-Dimethylp -Benzoic ac id -b i s(2-Ch1oroe -2,4-Dichlo rop -1,2,4-Trich lo -Naphthalene -4-Ch1o roan i 1 i -Hexach1orobu t -4-Chloro-3-me -2-Methylnapht -Hexachlorocyc -2,4,6-Trich lo -2,4,5-Tr ich1o •2-Ch1oronaph t •2-N11 roan i1 in -D1 me thyIphtha -Acenapht hy1 en -2,6-DinItroto

thy 1)ether 1 enzene enzene 1 enzene 1 sopropy1)ether 1 n-p ropylamine ane

heno 1

thoxy)methane heno 1 robenzene

ne ad iene t hy1pheno1 ha lene 1 open t ad i ene ropheno 1 ropheno 1 halene e late e luene

Q

1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 i 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 O C 4

dXai

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 -IU 1 IU 1 IU i IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 1 1

300427


EPA SAMPLE NO,

I I 1111185-03

Lab Name: INTECH Contract: 68-09-0048 I

.ab Code: INTECH Case No.:^2-^f'^r SAS No.: SDG No. : , , /'v

_Matri,.: [soil/water] WATER Lab Sample ID: ^•'/f ^^^

Sample wt/vol: 1000 [g/mL] ML Lab File ID: >BM70

"".evel: [low/med] LOW

% Mo 1 St ure: dec 100.

Date Receieved: :\l/27/91


extraction: [SepF/Cont/Sonc] SERF

G.PC Cleanup: [Y/N] N pH: 7.0


Di lut ion Factor : |. 00


99-83-51-

100-132-121-84-

7005-86-

100-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-Sl-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan i1ine -Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Di benzofuran •2,4-Dinitrotoluene -Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methylphenol •N-Ni trosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene •Pentachloropheno1 •Phenanth rene •Anth racene • D i - n - b u t y l p h t h a l a t e •F1uo r a n t h e n e • P y r e n e • B u t y l b e n z y l p h t h a l a t e • 3 , 3 ' - D i c h l o r o b e n z i d i n e • B e n z o ( a ) a n t h r a c e n e • C h r y s e n e •bis(2-Ethylhexyl)phthalate •Di-n-octyIphthalate •Benzo(b)fiuoranthene •Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e

Q

1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10


FORM I SU-2 252 300428

IF ;.EMIUQLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

I 1111185-03 XI a b N 6 -: e : NTECH Contract: 68-D9-0048

,.„atri": soil/water) WATER

-•-ample i-.' vol: 1000 (g/mL) ML

Teve1: 'low/med) LOW

Moi?'_re: dec. 100.




Lab Sample ID: f - ^ ^ t ^ ^ K

Lab File ID: >B8070




Dilut ion Factor: j.00


CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q

^ ^ 1 . - - l U n k n o w n 1 5 . 08 1 1 2 . 1 J

" ' I I I I I I I I

1 ' 1 1 1

i 1 I I I " 1 I I I

I I I I I X 1 I I I

r 1 I I I

i 1 I I I

I I I I I

i~ 1 I I I

.1. 1 i 1 1

-,- 1 I I I

I I I I I 1 ' 1 1 1

^ ^ I I I

FORM I SU-TIC 1/87 Rev,

253 300429

ID PESTICIDE ORGANICS ANALYSIS DATA SHEET

..ab Name: INTECH


Iatrix: (soil/water) SOIL

Sample wt/vol: 30. (g/mL) G

jevel: (low/med) LOW

% Moisture: not dec. 13. dec. 13.


GPC Cleanup: (Y/N) N pH: 7.5

EPA SAMPLE NO.

59-63' Contract: 68-D9-0048

42-64 SAS No.: SDG No.: ANSON

Lab Sample ID:

Lab File ID: GP1134

Date Received: iU/21/91

Date Extracted:>!11/25/91


CAS NO, COMPOUND

Dilution Factor:


1 . 0 0

Q

319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor

3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin

33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD

1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-4 3-5 Methoxychlor

53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene

12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 53 4 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260

9.2 9.2 9.2 9.2 9.2 9.2 9.2 9.2 18. 18. 18. 18. 18. 18. 18. 92. 18. 92. 92. 180. 92. 92. 92. 92. 92.

180. 180.

U U U U U U U U U U U U U U U U U U U U U U U U U U u

FORM I PEST 1 /87 R e v .

347 300430


EPA SAMPLE NO.

.ab Name: INTECH

Lab Code: INTECH


Case No.: 42-64 SAS No.: SDG No.: ANSON

"matrix: (soil/water) WATER

Sample wt/vol: 1000. (g/mL)ML

.evel: (low/med) LOW

% Moisture: not dec.100. dec. 0.

extraction: (SepF/Cont/Sonc) SERF


CAS NO. COMPOUND

Lab Sample ID: J l l f / ^ l ~ 3

Lab File ID: GP1138






319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC 76-44-8 Heptachlor 3 09-00-2 Aldrin 1024-57-3 Heptachlor 9 59-98-8 Endosulfan 60-57-1 Dieldrin 72-55-9 4 , 4 '-DDE 72-20-8 Endrin

3 3213-65-9 Endosulfan 72-54-8 4 , 4 ' -DDD

1031-07-8 Endosulfan 50-29-3 4 , 4 '^DDT

(Lindane)

epoxide I

II

sulfate

7 2-4 3-5 Methoxychlor 53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene

12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 1109 6-82-5 Aroclor-1260

.050

.050

.050

.050

.050

.050

.050

.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0

U U U U U U U U U U U u u u u u u u u u u u u u u u u

FORM I PEST 1/87 Rev.

351 300431


EPA SAMPLE NO,

,ab Name: INTECH

Lab Code: INTECH Case No.: 42-64



_,evel: (low/med) LOW


..xtraction: (SepF/Cont/Sonc) SONC

r.-pc Cleanup: (Y/N) N pH: 8.0

120-122' Contract: 68-D9-0048


Lab Sample ID:

Lab File ID: GP1135




CAS NO. COMPOUND

Dilution Factor:


1 . 0 0

Q





53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-3 5-2 Toxaphene

12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-12 54 11096-82-5 Aroclor-1260

10. 10. 10. 10. 10. 10. 10. 10. 20. 20. 20. 20. 20. 20. 20.

100. 20.

100. 100. 200. 100. 100. 100. 100. 100. 200. 200.

U U U U U U U U U U u u u u u u u u u u u u u u u u u

FORM I PEST

354

1 /87 R e v .

300432


EPA SAMPLE NO.

..ab Name: INTECH

Lab Code: INTECH





jevel: (low/med) LOW


Jxtraction: (SepF/Cont/Sonc) SERF


CAS NO. COMPOUND

Lab Sample ID: Jj/f/^-^-^

Lab File ID: GP1139









1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor


12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 53469-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-12 60

.050

.050

.050

.050

.050

.050

.050

.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0

U U U U U U U U U U U U U U U U U U u u u u u u u u u


300433

358


EPA SAMPLE NO,

,ab Name: INTECH

Lab Code: INTECH

60-62' Contract: 68-D9-0048


atrix: (soil/water) SOIL


evel: (low/med) LOW


xtraction: (SepF/Cont/Sonc) SONC

QPC Cleanup: (Y/N) N pH: 7.5

CAS NO. COMPOUND

Lab Sample ID: J'/z/Z f-/

Lab File ID: GP1147






319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 7 6-44-8 Heptachlor

3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4, 4'-DDE 72-20-8 Endrin


1031-07-8 -Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor

53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 510 3-74-2 gamma-Chlordane 8 001-35-2 Toxaphene

12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260

17. 17. 17. 17. 17. 17. 17. 17. 33. 33. 33. 33. 33. 33. 33.

170. 33.

170. 170. 330. 170. 170. 170. 170. 170. 330. 330.

U U U U U U U U U U U U U U U U U U U U U U U U U U U


300434

361


EPA SAMPLE NO.

,ab Name: INTECH

Lab Code: INTECH

75-77' Contract: 68-D9-0048


atrix: (soil/water) SOIL




xtraction: (SepF/Cont/Sonc) SONC


CAS NO. COMPOUND

Lab Sample ID: J l / / l l r^-2^

Lab File ID: GP1149








33213-65-9 Endosulfan II 72-54-8 4,4'-DDD

1031-07-8 Endosulfan sulfate 50-29-3 4, 4'-DDT 72-43-5 Methoxychlor

53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8 001-35-2 Toxaphene

12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-12 60

10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 21. 21. 21. 21. 21.

100. 21.

100. 100. 210. 100. 100. 100. 100. 100. 210. 210.

U U U U U U U U U U U U U u u u u u u u u u u u u u u


365 300435'


EPA SAMPLE NO.

ab Name: INTECH

'Lab Code: INTECH



'atrix: (soil/water) WATER


evel: (low/med) LOW


xtraction: (SepF/Cont/Sonc) SERF


CAS NO, COMPOUND

Lab Sample ID: 7//// -

Lab File ID: GP1143







309-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin



53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-3 5-2 Toxaphene

12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260

.050

.050

.050

.050

.050

.050

.050

.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0

U U U U U U U U U U u u u u u u u u u u u u u u u u u


369 300436


EPA SAMPLE NO.

...ab Name: INTECH

Lab Code: INTECH

Contract: 68-D9-0048 60-62'

Case No.: 85-2060 SAS No.:

"Iatrix: (soil/water) SOIL


..evel: (low/med) LOW




CAS NO. COMPOUND

SDG No.: ANSON

Lab Sample ID: J7////^$^- I

Lab File ID: GP2240


Date Extracted: 12/ 3/91









12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260

10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 21. 21. 21. 21. 21.

100. 21.

100. 100. 210. 100. 100. 100. 100. 100. 210. 210.

U U U U U U U U U U U U u u u u u u u u u u u u u u u

FORM I PEST 1 /87 Rev .

300437

372


EPA SAMPLE NO.

.ab Name: INTECH

Lab Code: INTECH Case No.: 85-2060 SAS No







74-76' Contract: 68-D9-0048

SDG No.: ANSON

Lab Sample ID: J//r/ r-Z-

Lab File ID: GP2241





CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG






12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 53469-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260

9.6 9.6 9.6 9.6 9.6 9.6 9.6 9.6 19. 19. 19. 19. 19. 19. 19. 96. 19. 96. 96. 190. 96. 96. 96. 96. 96.

190. 190.

U U U u u u u u u u u u u u u u u u u u u u u u u u u

FORM I PEST

378

1/87 Rev.

300438

^ b


EPA SAMPLE NO.

ib Name: INTECH

•Lab Code: INTECH



•Iatrix: (soil/water) WATER

"Sample wt/vol: 940. (g/mL)ML

l,evel: (low/med) LOW




CAS NO. COMPOUND

Lab Sample ID: J U i ] ^ f ^ 3

Lab File ID: GP2221






319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 7 6-44-8 Heptachlor 3 09-00-2 Aldrin

1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 -4 , 4 ' -DDE 72-20-8 Endrin




12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 iio::7-69-i Aroclor-1254 1109 6-82-5 -Aroclor-1260

.053

.053

.053

.053

.053

.053

.053

.053 .11 .11 .11 .11 .11 .11 .11 .53 .11 .53 .53 1.1 .53 .53 .53 .53 .53 1.1 1.1

U U U U U U U U U U U U U U U U U U U U U U U U U U U


300439 382

Unvalidated Data

Indoor borings 3 & 4

300440


EPA SAMPLE NO,

}h Name: INTECH

Lab Code: INTECH

10-12' Contract: 68-D9-0048



Sample wt/vol: 5.0

..Level: (low/med) LOW

„% Moisture: not dec. 1.

-Column: (pack/cap) PACK

CAS NO.

Lab Sample ID:






7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1, 1-Dichloroethene 75-34-3 1,1-Dichloroethane

540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform

107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1, 1,1-Trichloroethane 5 6-23-5 Carbon Tetrachloride

108-05-4 Vinyl Acetate 7 5-2 7-4 Bromodichloromethane 7 8-87-5 1, 2-Dichloropropane

10 0 61-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 7 9-00-5 1, 1, 2-Trichloroethane 71-4 3-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane

108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 10 0-41-4 Ethylbenzene 100-4 2-5 Styrene

lJ-JO-20-7 Xylene (total)

10. 10. 10. 10. 6.

25. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5, 5. 5. 5. 5.

U U U U B

U U U U U U U U U U U U U U U U U U U U U

u u u u u

FORM I VOA 1 / 8 7 R e v ,

IS

300441

IE VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO,

b Name: INTECH

ab Code: INTECH Case No.


Sample wt/vol: 5.0





10-12' Contract: 68-D9-0048


Lab Sample ID:




Dilution Factor:


1 .00

CAS NUMBER

1. 110-54-3 2 . 3 . 4 . 5. 6. 7 . 8.

L ^• klG. • l l . 12. 13. 14 . 15. 16. 17. 18. 19. 20. 21. 22. 23 . 24 . 25. 26. 27. 28. 29. 30.

COMPOUND NAME

Hexane

RT

18.83

EST. CONC.

5.

Q

J

FORM I VOA-TIC 1/87 R e v .

- 19 30044?


EPA SAMPLE NO,

ib Name: INTECH

Lab Code: INTECH


Case No.: 61-68 SAS No.: SDG No

15-17'

ANSON


Sample wt/vol: 5.0




CAS NO.

Lab Sample ID:






7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 54 0-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 6.

19. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U B

U U U U U U U U U U U U U U U U U U U U U U U U U u U u


r, —

300443



m b Name: INTECH ab Code: INTECH Case No


Sample wt/vol: 5.0





EPA SAMPLE NO,

15-17' J (n«Ai~oZ

ANSON


.: 61-68 SAS No.: SDG No.

Lab Sample ID:




Dilution Factor:


1.00

- ^ J ^

---

CAS NUMBER

1. 1 1 0 - 5 4 - 3 2 . 3 . 4 . 5 . 6 . 7 . 8 .

k ^• | i o . F l l .

1 2 . 1 3 . 1 4 . 1 5 . 1 6 . 1 7 . 1 8 . 1 9 . 2 0 . 2 1 . 2 2 . 2 3 . 2 4 . 2 5 . 2 6 .

2 8 . 2 9 . 3 0 .

COMPOUND NAME

H e x a n e (DOT)(8CI9CI )

RT

1 8 . 8 2

EST. CONC,

5 .


r. n

300444


EPA SAMPLE NO,

b Name: INTECH

Lab Code: INTECH Case No,




Lab Sample ID:

Sample wt/vol: 5.0 (g/mL) ML




CAS NO. COMPOUND

Lab File ID: C9558





7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 75-34-3 1, 1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-9 3-3 2-Butanone 71-55-6 1,1, 1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1,2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-3 4-5 1,1, 2 , 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 10 0-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 5.

68. 5. 5. 5. 5.

26. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 4. 5. 5. 5. 5.

U U U U B

U U U U

u u u u u U . U u u u u u U U u u u u J U U U U

FORM I VOA 1 / 8 7 R e v .

r-. o

30044^



EPA SAMPLE NO,

Name: INTECH

::ab Code: INTECH Case No,

'Matrix: (soil/water) WATER

Sample wt/vol: 5.0




' Number TICs found: 0


61-68 SAS No.: SDG No

Lab Sample ID:

F-BLANK

ANSON

(g/mL) ML Lab File ID: C9558





CAS NUMBER

1. 2 . 3. 4 . 5. 6. 7. 8.

^ ^ • lf°-PLI. 12. 13 . 14 . 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24 . 25. 26. 27. 28. 29. 30.


FORM I VOA-TIC 1 / 8 7 R e v ,

\J v

300446


EPA SAMPLE NO,

m b Name: INTECH Contract: 68-D9-0048

Lab Code: INTECH Case No.: 61-68 SAS No.: SDG No


(g/mL) G

IB#3 ^ f . Z 7

Sample wt/vol: 5.0




CAS NO. COMPOUND

ANSON

Lab Sample ID: Xlllo^^-?

Lab File ID: C9686





7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane

540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform

107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 5 6-23-5-^ Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene

100 61-02-6 trans-1, 3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-7 8-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1, 2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene


10. 10. 10. 10. 5.

26. 5. 5. 5. 5. 5. c 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ B U U U U u u U u u u u u U u u u U U U u U u U u u u u u


. -iO 300447



^kab Name: INTECH Contract: 68-D9-0048

^ ^ b Code: INTECH Case No.: 61-68 SAS No.: SDG No.

-Matrix: (soil/water) SOIL

(g/mL) G

EPA SAMPLE NO.

IB#3 2.5--Z7

Sample wt/vol: 5.0





ANSON

Lab Sample 10:3(1'°^*"^

Lab File ID: C9686





CAS NUMBER

1. 2. 3 . 4 . 5. 6. 7. 8. 9.

|10. Fll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27 . 28. 29. 30.



4x

3O044&'


EPA SAMPLE NO.

Fb Name: INTECH Contract: 68-D9-0048



(g/mL) G

30-32'

Sample wt/vol: 5.0


.% Moisture: not dec. 2.


CAS NO, COMPOUND

ANSON

Lab Sample ID: i W l o i S ' ^

Lab File ID: C9668





7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 5 6-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane


100 61-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10.

' I : 15. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U B B U U U U U U U U U U U U U U U U U U U U u u U U U U u U

FORM I VOA 1/87 Rev,

4v>

300449



EPA SAMPLE NO,

•. b Name: INTECH ab Code: INTECH Case No.







30-32 Contract: 68-D9-0048


Lab Sample ID: T\\\o(,$-<t'

Lab File ID: C9668



Dilution Factor:


1 .00

CAS NUMBER

1. 2 . 3. 4. 5. 6. 7. 8.

L ^• IlO. "ll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27. 28. 29. 30.



300450


EPA SAMPLE NO.

# b Name: INTECH Contract: 68-D9-0048



5.0 (g/mL) G

35-37'

Sample wt/vol:


% Moisture: not dec. 3


CAS NO, COMPOUND

ANSON

Lab Sample ID: J i \ io( i r$-4

Lab File ID: C9669


Daite Analyzed: 11/22/91



7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-9 3-3 2-Butanone 71-55-6 1, 1, 1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1,2-Dichloropropane


10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-7 8-6 2-Hexanone 12 7-18-4 Tetrachloroethene /9-34-b 1,1, 2, 2-Tetrachloroethane

108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene


10. 10. 10. 10. 6.

15. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U B B U U U U U U U U U U U u u u u u u u u u u u u u u u u u


J 2

300451

IE VOLATILE ORGANICS ANALYSIS DATA SHEET - TENTATIVELY IDENTIFIED COMPOUNDS

«

b Name: INTECH

ab Code: INTECH

EPA SAMPLE NO,

35-37 Contract: 68-D9-0048



Sample wt/vol: 5.0




Number TICs found; 0

Lab Sample ID: J(//o < -






CAS NUMBER

1. 2 . 3. 4. 5. 6. 7. 8.

L ^• kio. ^ 1 1 . 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24. 25. 26. 27. 28. 29. 30.


FORM I VOA-TIC 1/87 R e v .

r •"I

300452


EPA SAMPLE NO,

Ib Name: INTECH





Lab Sample ID:





CAS NO, COMPOUND

Lab File ID: C9564





74-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1, 1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene

100 61-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 —Ethylbenzene 10 0-42-5 Styrene


10. 10. 10. 10. 5.

33. 5. 5. 5. 5.

20. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5.

I : 5 . 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U B

U U U U

U u U U U U U U U u u u u u u u u u u u u u u


300453



^tob Name: INTECH

^ R b Code: INTECH Case No,

-••Matrix: (soil/water) WATER

'Sample wt/vol: 5.0

•"Level: (low/med) LOW




EPA SAMPLE NO,

F-BLANK

61-68

(g/mL) ML



Lab Sample ID:

Lab File ID: C9564





CAS NUMBER

1. 2. 3. 4 . 5. 6. 7. 8.

. 9-|10. Wii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.


FORM I VOA-TIC 1/87 Rev.

300454


lb Name: INTECH



EPA SAMPLE NO.

T-BLANK Contract: 68-D9-0048


Lab Sample ID:


..Level: (low/med) LOW

..% Moisture: not dec. 100.


CAS NO. COMPOUND

Lab File ID: C9565





""

•

7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1, 1-Dichloroethene 75-34-3 1, 1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1, 1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1, 2-Dichloropropane

10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-4 3-2 Benzene

10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 7S-34-5 1,1, 2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene

• 100-41-4 Ethylbenzene 10 0-4 2-5 Styrene 1330-20-7 Xylene (total)

10. 10. 10. 10. 4.

330. 5. 5. 5. 5. 5. 5.

10. 5. 5.

10. 5. 5. 5. 5. 5. 5. 5. 5. 5.

10. 10. 5. 5. 5. 5. 5. 5. 5.

U U U U BJ

E u u U u u u u u u u u u u u u u u u u u u u u u u u u u


300456

I IE VOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO,

fab Name: INTECH

ab Code: INTECH Case No.: 61-68

"Matrix: (soil/water) WATER


SAS No.: SDG No,

Lab Sample ID:

T-BLANK Xli

ANSON

Sample wt/vol: 5.0





(g/mL) ML Lab File ID: C9565





CAS NUMBER

1. 2. 3. 4 . 5. 6. 7. 8. 9.

|io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24 . 25. 26. 27. 28. 29. 30.

COMPOUND NAME RT

.

EST. CONC. Q

FORM I VOA-TIC 1/87 Rev.

G8

300456


EPA SAMPLE NO,

I 1111061-01 Lab Name: INTECH Contract: 68-09-0048 I

\h CocJe: INTECH Case Ho. : ^) - ( fh SAS No.: SDG No.: /^/vSo.t/

Matrix: [soiI/water] SOIL

-Sample wt/vol: 30.00 [g/mLl G

Level: [low/meidl LOU)

'% Moisture: j, dec. I.


GPC Cleanup: [Y/Nl N pH: 7.0

Lab Sample ID:

Lab File ID: >B7957



Date Analyze(d: 11/20/91

Dilut ion Factor : \ .00


108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-€ ^ -

111-120-120-91-

106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phenol -bis(2-chloroet -2-Chloropheno1 -1,3-Dichlorobe •1,4-Dichlorobe •Benzy1 a Icoho1 -1,2-Dichlorobe •2-Methylpheno1 •bis(2-chIorois -3&4-MethyIphen -N-Nitroso-di-n •Hexachloroetha •Nit robenzene - Isophorone •2-Ni t ropheno1 -2,4-DimethyIph -Benzoic acid •b is(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor -Naphthalene •4-Chloroan i1 in •Hexachlorobuta •4-Chloro-3-met •2-Methylnaphth •Hexach1oroeycl •2,4,6-Tr ichlor -2,4,5-Tr ichlor •2-Chloronaphth •2-Ni t roan i1ine •Dime thyIphtha1 •Acenaphthylene •2,6-DinItroto1

hy1)ether

nzene nzene

nzene

opropyl)ether ol -propylamine ne

eno 1

hoxy)methane eno I obenzene

e d iene hy1pheno1 a lene opentad iene opheno I opheno 1 a 1 ene

ate

uene

FORM I SU-1

Q

340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340

1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340


•^ -«t •J^v

30045?:


EPA SAMPLE NO,

I 1111061-01

#


b Code: INTECH Case No.: /-^S . SAS No.: SDG No.: / i ^ ^ o ^

Matrix: [soil/water] SOIL



„ - \ Moisture: I, dec. |.


"GPC Cleanup: [Y/N] N pH: 7.0

Lab Sample ID:

Lab File ID: >B7957




Dilution Factor: (.00


99 83 51-

100-132 121-84-

7005 86 100 534 86 101 118 87-85-

120-84-

206-129-85-91-56

218' 117 117 205 207-50-

193-53

191.

-09-2--32-9--28-5--02-7--64-9-•14-2-•73-7--72-3--73-7--01-6--52-1--30-6--55-3--74-1--86-5--01-8--12-7--74-2--44-0--00-0-•68-7-•94-1--55-3--01-9--81-7--84-0--99-2-•08-9--32-8--39-5--70-3--24-2-

•3-Ni t roan i1 -Acenaphthen •2,4-Dinit ro •4-Ni t rophen •D ibenzofura -2,4-Dini tro •Diethylphth -4-Chlorophe -F1uorene -4-Ni t roan i1 -4,6-Din i t ro -N-Ni t rosod i -4-Bromophen -Hexachlorob •Pent achloro •Phenanthren •An thracene •Di-n-butyIp •Fluoranthen •Pyrene •ButyIbenzy1 -3,3'-Dichlo •Benzo(a)ant -Chrysene -bis(2-Ethyl -Di-n-octyIp •Benzo(b)flu •Benzo(k)f lu -Benzo(a)pyr - Indeno(1,2, -Dibenz(a,h) -Benzo(g ,h , i

1 ne e pheno1 ol n to luene a late ny1-phenylether

ine -2-methylphenol phenylam ine y 1 -phenylether enzene pheno1

htha late e

phthalate robenz id i ne hracene

hexyl)phthalate htha la te oran thene oran t hene ene 3-cd)pyrene anth racene )pe rylene

1700 340 340 1700 340 340 340 340 340 1700 1700 340 340 340

1700 340 340 340 340 340 340 670 340 340 190 340 340 340 340 340 340 340

Q

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I 3 IU IU IU IU iU IU IU

FORM I SU-2 1 ' - ' Xuvj

300458

f, IF

SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIUELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

I 1111061-01 ab Name: INTECH Contract: 68-D9-0048 I

..Matrix: (soil/water) SOIL

-Sample wt/vol: 30.00 (g/mL) G


% Mo ISture: |. dec. |.




Lab Sample ID:

Lab File ID: >B7957




Dilution Factor: \ .oo


CAS NUMBER

1. 2. 3.

4127-47-3

COMPOUND NAME

Cyclopropane, 1,1,2 ,2-tetram Aldol Condensation t"y / i/ Aj) Unknown

RT

2.71 3.64

27.86

EST. CONC,

300. 9800. 170.

Q

J J J

FORM I SU-TIC 1/87 Rev

lo7 .. 300459


EPA SAMPLE NO.

I 1111061-02 Lab Name: INTECH

ib Code: INTECH


Sample wt/vol: 3 0.00 [g/mL] G

.Level: [low/med] LOU

-% Moisture: Z. dec. 2- .


'GPC Cleanup: [Y/N] N pH: 7.1


Case No.: ^I '^B' SAS No.: SDG Ho. : / ^ ^ t'^'^

Lab Samp 1e ID:

Lab File ID: >B7958


Date Extracted: 11/15-'91


CAS NO. COMPOUND

Di lut ion Factor:


108-95-2 Phenol 111-44-4 bis (2-ch loroethyl )ether 95-57-8 2-Ch loropheno 1

541-73-1 1,3-Dich lorobenzene 106-46-7 1,4-Dichlorobenzene 100-51-6 Benzyl alcohol 95-50-1 1,2-Dich lorobenzene 95-48-7 2-Methylphenol 108-60-1 b is(2-chloroisopropyl)ether 106-44-5 3&4-Me thy I phenol 621-64-7 N-Nitroso-d1-n-propy lamine 67-72-1 Hexach loroethane 98-95-3 Nit robenzene 78-58-1 Isophorone 88-75-5 2-N It ropheno I 105-67-9 2,4-Dimethylphenol 65-35-0 Benzoic acid 111-91-1 bis(2-Chloroethoxy) me thane 12 0-83-2 2,4-Dichlorophenol 120-82-1 1,2,4-Inch lorobenzene 91-2 0-3 Naphthalene

106-47-8 4-Chloroani 1 ine 87-68-3 He xach lorobutad iene 59-5 0-7-^ 4-Chloro-3-methylphenol 91-57-6 2-Methylnaphthalene 77-47-8 Hexach lorocyc lopentad iene 88-06-2 2,4,6-Tr ich loropheno I 95-95-4 2,4,5-Trichlorophenol 91-58-7 2-Ch loronaphtha lene 88-74-4 2-Ni t roam I ine 131-11-3 Dimethylphthalate 208-96-8 Acenaphthylene 606-20-2 2,6-Dinitrotoluene

FORM I SU-1

\ 0</

Q

340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU tu IU IU IU IU IU IU IU IU IU IU IU 1

3G. 300460


EPA SAMPLE NO.

I 1111061-02

#


b Code: INTECH Case No.: ^|-^S SAS No.: SDG No.: ^^.-/o^



.-Level: [low/med] LOW

% Moisture: 2.- dec. 2..



Lab Sample ID:

Lab Flle ID: >B7958




Dilution Factor: \,o<)

CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q

99-83-51-100-132-121-84-

7005-86-

100-534-86-101-118-87-85-120-84-

206-129-85-91-56-

218-117-117-205-2 07-50-

193-53-

191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-•44-0-00-0-68-7-94-1-55-3-01-9-•81-7-•84-0-•99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan i1ine -Acenaphthene -2 ,4-Din i t ropheno1 -4-Ni t ropheno1 -D ibenzofuran -2,4-Dinitrotoluene •Diethylphthalate •4-Chlorophenyl-phenylether -Fluorene •4-Ni t roan i1i ne •4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butyIphthalate -Fluoranthene -Pyrene -ButylbenzyIphtha late -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Be n z o(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd;vyrene - D i b e n z ( a , h ) a n t h r a c e n e - B e n z o ( g , h , i ) p e r y l e n e

FORM I SU-2

1 1700 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 1700 1 1700 1 340 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 340 1 680 1 340 1 340 1 320 1 340 1 340 1 340 1 340 1 340 1 340 1 340

1 IU iU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU 1 J IU IU IU IU IU IU IU 1

IG J

300461



EPA SAMPLE NO.

1 1111061-02 Lab Name: INTECH Contract: 68-D9-0048




.% Moisture: 2-. dec. 2. .



- Number TICs found: 3

Lab Sample ID:

Lab File ID: >B7958




Dilut ion Factor: 1-^0


I I I I I 1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q

1 1 . - - lUnknown 1 2 . 7 1 1 3 1 0 . 1 J ^ 2 . - - 1 A l d o l - C o n d e n s a t ionfvo(/L-c-r(ivK-v».^ 3 . 6 4 1 1 1 0 0 0 . 1 3 P 3 . - - lUnknown 1 2 7 . 8 6 1 1 7 0 . 1 3

1 * 1 1 1 1

FORM I S U - T I C 1/87 Rev,

iG.:>

30046e


EPA SAMPLE NO.

I 1111061-03 Lab Name: INTECH Contract: 68-D9-0048 I

sb Code: INTECH Case No.: ^ \ ' ( ?^ SAS No.: SDG No.: I^^^<^H

Matrix: [soil/water] WATER Lab Sample ID:

Sample wt/vol: 1000 [g/mL] ML Lab File ID: >B7949

Level: [low/med] LOW Date Receieved: 11/11/91

% Moisture: dec 100. Date Extracted: 11/14/91



COMPOUND ,


Dilution Factor: f.OO

CAS NO.

1 108-1 111-1 95-1 541-1 106-l 100-1 95-1 95-1 108-1 106-1 621-1 67-1 98-1 78-1 88-1 105-1 65-1 111-1 120-1 120-1 91-1 106-1 87-1 59-1 91-1 77-1 88-1 95-1 91-1 88-1 131 1 208 i 606

•95-•44-•57-•73-•46-•51-•50--48--60--44-•64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06^ -95--58--74. -11 -96 -20

2-4-•8-1-•7-•6-•1-

• 7

-1-•5-

• 7 -

•1-

-3-•1

•5-

-9 -0-•1-

-2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 -2

CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L

Pheno 1 bis(2-chloroethyl)ether 2-Chloropheno 1 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl alcohol 1,2-Dichlorobenzene 2-Methylphenol bis(2-chloroisopropyl)ether 4-MethylphenoI N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene I sophorone 2-NitrophenoI 2,4-Dimethylphenol Benzoic acid bis(2-Chloroethoxy)me thane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroani1ine Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene

----2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-NitroaniIine Dimethylphthalate Acenaphthy Iene 2,6-Dinitrotoluene

FORM I SU-1

Q

1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10

10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU \ IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU IU 1 1

IV.:;

300463


EPA SAMPLE NO,

1111061-03 Lab Name: INTECH

fb Code: INTECH Case No.


Sample wt/vol: 1000 [g/mL] ML

Level: [low/medl LOW

% Moisture: dec 100.




I P ) ' ( J ^ SAS No.: SDG No.: /}A-i<5'

Lab Sample ID:

Lab File ID: >B7949






99-83-51-100-132-121-84-

7005-86-

100-534-86-101-118-87-85-120-84-

206-129-85-91-56-

218-117-117-205-207-50-193-53-191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roan iii -Acenaphthene -2,4-Dinitrop -4-Ni t ropheno -Dibenzofuran -2 ,4-Dini trot •Die thyIphtha •4-Chlorophen •Fluorene •4-Nit roan i1i •4,6-Din i t ro--N-Ni t rosod i p •4-Bromopheny •Hexachlorobe -Pentachlorop -Phenanthrene -Anthracene -Di-n-butyIph -Fluoranthene -Pyrene -ButyIbenzyIp -3,3'-Dichlor -Benzo(a)anth -Chrysene •bis(2-Ethylh -Di-n-octyIph •Benzo(b)fluo •Benzo(k)fluo -Benzo(a)pyre - Indeno(1,2,3 •Dibenz(a ,h )a -Benzo(g ,h , i )

ne

heno 1 1

0 luene late y1-phenylether

ne 2-me thyIpheno1 heny1 ami ne 1 -phenylet her nzene heno 1

tha late

htha late obenz id ine racene

exy1)phtha 1 ate tha la te ranthene rant hene ne -cd)pyrene n thracene perylene

50 10 10 50 10 10 10 10 10 50 50 10 10 10 50 10 10 10 10 10 10 20 10 10 3 10 10 10 10 10 10 10

FORM I SU-2

Q

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I J IU IU IU IU IU IU IU

IV; 300464



EPA SAMPLE NO.

I 1111061-03 Lab Name: INTECH Contract: 68-D9-0048

• . Tatrix: (soil/water) WATER

"Sample wt/vol: 1000 (g/mL) ML


?6 Moisture: dec. 100.




Lab Samp 1e ID:

Lab File ID: >B7949



Date Analyzed: 11/2 0/91



1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q 1

1 1 . - - lUnknown 1 5 . 1 3 1 1 2 . 1 J f i 1

"' 1 1 1 1 I I

. t 1 1 1 I I

A I I I I W I I I I

- 1 1 I I I I

- 1 1 I I I I

- - 1 1 I I I I

- 1 1 I I I I

1 1 I I I I

FORM I SU-T IC 1 / 8 7 Rev

IV,}

300465


EPA SAMPLE NO.


b Code: INTECH Case No.: U'lp9' SAS No.: SDG No. : JV; /*

Lab Sample ID:

Lab File I D : >B7965




Dilution Factor: \.oo




% Moisture: 2-. dec. 2..




108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-•95-4-58-7-74-4-11-3-96-8-20-2-

•Pheno1 -bis(2-chloroethyl)ether •2-Chloropheno1 •1,3-Dichlorobenzene •1,4-Dichlorobenzene •Benzyl a Icoho1 •1,2-Dichlorobenzene •2-Methylphenol •bis(2-chloroisopropyl)ether •3&4-Methylpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane •Nit robenzene • Isophorone -2-Ni t rophenoI -2,4-Dime thy IphenoI -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-TrichlorophenoI -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan iIine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene

FORM I SU-1

Q

340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU - 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1

IGO,, 30046iB


EPA SAMPLE NO,

Lab Name: INTECH

l^b Code: INTECH Case No.: 6/- ^




-% Mo isture : 2. dec . .



I I 1111068-03


SAS No.: SDG No.: /^ /y io^

Lab Sample ID:

Lab File ID: >B7965






99-83-51-10 0-132-121-84-

7005-86-10 0-534-86-

101-118-87-85-

120-84-

206-129-85-91-56-

218-117-117-205-207-50-

193-53-191-

09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-

-3-Ni t roa -Acenapht -2,4-Dini -4-Ni t rop -Dibenzof -2,4-Dini -Die thyIp •4-Chloro •Fluorene •4-Ni t roa -4,6-Dini •N-Ni t ros •4-Bromop •Hexachlo •Pent achI -Phenanth -An thrace •Di-n-but -Fluorant •Pyrene -ButyIben -3,3'-Dic -Benzo(a ) -Chrysene -bis(2-Et -Di-n-oct -Benzo(b) •Benzo(k ) -Benzo(a ) - Indeno (1 •D ibenz (a •Benzo(g ,

n iIine hene t ropheno 1 heno 1 uran t roto luene htha late phenyl-phenylether

n i I ine tro-2-methy I phenol odiphenyI amine henyl-phenylet her robenzene oropheno I rene ne y Iphtha late hene

zyIphthalate h I orobenz i d ine anthracene

hyIhexyI)phthalate y Iphtha late f luo ran thene f luoranthene pyrene ,2 ,3-cd)pyrene ,h )anth racene h,i)pe ry1ene

1700 340 340 1700 340 340 340 340 340 1700 1700 340 340 340 1700 340 340 340 340 340 340 680 340 340 320 340 340 340 340 340 340 340

FORM I SU-2

Q

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I 3 IU IU IU IU IU IU IU

300467



EPA SAMPLE NO,




.Level: (low/med) LOW

% Moisture: 2. dec. 2-.


GPC Cleanup: (Y/N) N pH: 8.C


Lab Sample ID:

Lab File ID: >B7965




Dilution Factor: ). oo


1 CAS NUMBER 1 COMPOUND NAME 1 RT ( ss = s5=:s: = 35 = =: = 3=a»3sss= | =s = = = = = = = = = = = as = =i = = = = = = = = = = = = = | s= = ss = » = = =

1 1 . - - lUnknown 1 1.70 ^ 2 . - - 1 Aldol Condensat ion-Pro/ycr(/» «V«i#'/K,) 3.6 0 P 3. - - lUnknown 1 5.19 1 4 . - - lUnknown 1 7.52

EST. CONC,

2 0 0 . 3 7 0 0 .

1 4 0 . 2 7 0 .

FORM 1 S U - T I C

Q

3 3 3 3

1 /87 Re^-t f - o

300488

ib SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

I 1111068-05 Lab Name: INTECH

kb Code: INTECH Case No ( ? l - l , ^




C c - i t r a c t : 6 8 - D 9 - 0 0 4 8 I

SAS N o . : SDG N o . : / iA^So/V

Lab Sample I D :

Lab F i l e I D : >B7966

D a t e R e c e i v e d : 1 1 / 1 2 / 9 1

% M o i s t u r e : 2 . d e c . 2 .



CAS NO. COMPOUND



Di lut ion Factor


1 108-1 111-1 95-1 541-1 106-1 100-1 95-1 95-1 108-1 106-1 621-1 67-1 98-1 78-1 88-1 105-1 65-1 111-1 120-1 120-1 91-1 106-1 87-1 59-1 91-1 77-1 88-1 95-1 91-1 86-1 131-1 208-1 606-

-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-

•2 • 4 -8 -1 -7 -6 •1 -7 •1 -5 -7 -1 -3 -1 -5 -9 -0 -1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 -2

Phenol bis(2-chloroethyl)ether 2-Chloropheno1 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl alcohol 1,2-Dichlorobenzene 2-Methylphenol bis(2-chloroisopropyl)ether 3&4-Methylphenol N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-NitrophenoI 2,4-Dime thy I phenol Benzoic acid bis(2-Chloroethoxy)me thane 2,4-DichlorophenoI 1,2,4-Trichlorobenzene Naphthalene 4-Chloroani1ine Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene HexachlorocycI open tadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroani1ine Dime thyIphthalate Acenaphthylene 2,6-Dinitrotoluene

FORM I SU-1

\ . o O

1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 1700 i 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 1700 1 330 1 330 1 330


300469


EPA SAMPLE NO.

I I 1111068-05


lb Code: INTECH Case No.: 6/-^^ SAS No.: SDG No.: A ' ^ i O i v




% Moisture: 2. dec. 2 -



Lab Sample ID:

Lab File ID: >B7966






99-09-2 3-Ni t roan il ine 83-32-9 Acenaphthene 51-28-5 — 2,4-Dinitrophenol 100-02-7 4-Nit ropheno 1 132-64-9 Dibenzofuran 121-14-2 2,4-Din it roto luene 84-73-7 Diethylphthalate

7005-72-3 4-Chlorophenyl-phenylet her 86-73-7 Fluorene 100-01-6 4-Nit roan i 1 ine 534-52-1 4,6-Dinitro-2-methylphenol 86-30-6 N-Nitrosodiphenylamine 101-55-3 4-Bro mo phenyl-phenylether 118-74-1 Hexach lorobenzene 87-86-5 Pentach loropheno 1 85-01-8 Phenanthrene 12 0-12-7 Anthracene 84-74-2 Di-n-butylphthalate

2 06-44-0 Fiuoranthene 129-0 0-0 Pyrene 85-68-7 Butylbenzylphthalate 91-94-1 3,3'-Dich lorobenz id ine 56-55-3 Benzo (a )anthracene

218-01-9 Chrysene 117-81-7 bis(2-Ethylhexyl)phthalate 117-84-0 Di-n-octylphthalate 2 05-99-2 Benzo (b)f luoranthene 207-08-9 Be nzo (k)f luoranthene 5 0-32-8 Benzo(a)pyrene 193-39-5 Indeno (1,2, 3-cd) pyrene 53-70-3 D ibenz ( a, h) an thracene 191-24-2 Benzo (g,h, I ) perylene

1700 330 330 1700 330 330 330 330 330 1700 1700 330 330 330 1700 330 330 330 330 330 330 670 330 330 240 330 330 330 330 330 330 330

FORM I SU-2

Q

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I J IU IU IU IU IU IU IU

13i

300470



EPA SAMPLE NO,




Level: (low/med) LOU

% Moisture: 2.. dec. Z-




Lab Sample ID:

Lab File ID: >B7966




Dilution Factor: \ . o v


1 1 I I I 1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q 1 = = = s s s = : s s z = = B S S S = | ==5 = = = = = = = = =s = = = = = = = = = = = = = = = s== | = = = = = = = = | = = = = = = = = = = = = = ' j = = = = =

1 1 . - - l A l d o l C o n d e n s e t ion-/' i^o<^f^t//»«^'^j 3 . 6 1 1 43 0 0 . 1 J ^ L 2 . - - lUnknown 1 7 . 5 3 1 3 0 0 . 1 J ^ B 3 . - - lUnknown 1 1 2 . 3 8 1 1 3 0 . 1 J

I I I I I I I I I I 1 1 I I I I I I I I

' 1 1 I I I I I I I I 1 1 I I ' I I I I I I I I I I 1 1 I I 1 I I I I I I I I I I I t I i i 1 1 I I I 1 1 I I ! I I I I I

- 1 1 I I ' I ' I I I I

1 1 I I I I I I I I

"" i 1 I I I I I 1 1 1

FORM I S U - T I C 1/8 7 . I-}

300471


EPA SAMPLE NO,

1111068-07 Lab Name: INTECH Contract: 68-D9-0048 I

kb Code: INTECH Case No.: i)l-(?2^ SAS No.: SDG No.: A / ^ J O ^



Leve1: [low/med] LOW

% Moisture: 2. dec. 2-.



Lab Sample ID:

Lab File ID: >B7962






108-111-95-

541-106-100-95-95-

108-106-621-67-98-78-88-

105-65-

111-120-120-91-106-87-59-93-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-•83-2-82-1-20-3-47-8-•68-3-50-7-57-6-•47-8-•06-2-95-4-58-7-74-4-11-3-96-8-20-2-

•Phenol -b is(2-chloroet -2-Chloropheno1 -1,3-Dichlorobe -1,4-Dichlorobe -Benzyl alcohol -1,2-Dichlorobe -2-MethylphenoI -bis(2-ch loro is -3&4-Methylphen -N-Nitroso-d i-n -Hexachloroetha -Nit robenzene -1 sophorone -2-Ni t rophenoI -2,4-Dimethylph -Benzo ic acid -bis(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor -Naphthalene -4-Chloroan i1 in -Hexachlorobuta -4-Chloro-3-me t -2-Methylnaphth -HexachlorocycI -2,4,6-Trichlor -2,4,5-Tr ichlor -2-Chloronaphth -2-Ni t roan i1ine -Dimethylphthal -Acenaphthy Iene -2,6-Dinitrotol

hyl)ether

nzene nzene

nzene

opropyl)et her ol -propyl am i ne ne

eno I

hoxy)methane eno I obenzene

e d iene hylphenoI a lene opent ad iene opheno1 opheno I a lene

a t e

u e n e

FORM I SU-1

Q

300472

IC

S E M I U O L A T I L E O R G A N I C S A N A L Y S I S DATA SHEET EPA SAMPLE NO.

I 1111068-07

Lab Name: INTECH C o n t r a c t : 6 8 - D 9 - 0 0 4 8 I

i ^ ^ C o d e : INTECH Case N o . : ( f l ' i r ^ SAS N o . : SDG N o . : ^ ^ J c ^


Sample w t / v o l : 30.21 [g/mLl G

-Level: [low/med] LOW

-% M o i s t u r e : 1 . d e c . 1,

'Extraction: [SepF/Cont/Sonc] SONC


Lab Sample ID:

Lab Flle ID: >B7962




Dilution F a c t o r : \.0<^

CAS NO, COMPOUND

C O N C E N T R A T I O N U N I T S :

[ug/L or ug/Kg] UG/KG

99-83-51-

100-

132-121-84-

7005-86-

100-534-86-

101-118-

87-

85-120-84-

206-129-85-91-

218-117^ 117^ 205-207-

50-193-

53-191-

•09-2-•32-9-•28-5-•02-7-•64-9-•14-2-•73-7-•72-3-•73-7-•01-6-•52-1-•30-6-•55-3-•74-1-•86-5-•01-8-•12-7-•74-2-•44-0-•00-0-•68-7-•94-1-•55-3-•01-9--81-7--84-0--99-2-•08-9-•32-8-•39-5-•70-3-•24-2-

-3-Ni t roan i1ine

- Ac enaphthene •2,4-Dinitrophenol -4-Ni t rophenoI -Dibenzofuran -2,4-Dinitrotoluene •Diethylphthalate -4-Chlorophenyl-phenylet her -Fluorene -4-Nitroani1ine •4,6-Dinitro-2-me thyIphenoI -N-Nitrosodiphenyl amine •4-Bromophenyl-phenylet her -Hexachlorobenzene -Pentachloropheno1

- Ph enanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene

-bis(2-Ethylhexyl )phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)f luoranthene -Benzo(a)pyrene

- Indeno(1,2,3-cd)pyrene -Dibenz(a,h)anthracene •Benzo(g,h,i)perylene

Q

1 1700 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 1700 1 1700 1 340 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 340 1 680 1 340 1 340 1 220 1 340 1 340 1 340 1 340 1 340 1 340 1 340

1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU I IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 1 ' 1

FORM I SU-2

300473



Lab Name: INTECH Contract: 68-D9-0048

EPA SAMPLE NO,

I 1111068-07 I



Level: (low/med) LOU

% Moisture: X . dec. 2-.




Lab Sample ID:

Lab File ID: >B7962




Di lut ion Factor : I. "S ®


CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q

1. - - lAldol C o n d e n s e t ion-Piro(/ieT ((/*«6<Diif ) 3.62 1 3 7 0 0. 1 3 2. - - lUnknown 1 5.22 1 170. 1 J

k 3 . - - lUnknown 1 7.56 1 240. 1 J

' 1 I I I

FORM I SU-TIC 1/87 Rev.

C u X

300474

IB SEMIUOLATILE 'ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO,


.Lab Code: INTECH Case No.: ^1-^g SAS No.: SDG No.:/?/^/<^^


"Sample wt/vol: 1000 [g/mL] ML


H Moisture: dec 100.


_GPC Cleanup: [Y/N] N pH: 7.0

Lab Sample ID:

Lab File ID: >B7950






108-111-95-

541-106-100-95-95-108-106-621-67-98-78-88-

105-65-

111-120-120-91-106-87-59-91-77-88-95-91-88-

131-208-606-

95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-5 0-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-

-Phen -bis( -2-Ch -1,3-•1,4--Benz -1,2--2-Me -bis( -4-Me -N-Ni -Hexa -Nit r - Isop -2-Ni -2,4--Benz -bis( -2,4-•1,2, -Naph -4-Ch •Hexa •4-Ch -2-Me -Hexa •2,4, -2,4, -2-Ch -2-Ni -D ime -Acen -2,6-

ol 2-ch 1 oroet lorophenoI Di ch 1 orobe Dich lorobe yI a 1 echo 1 Dichlorobe thyIpheno1 2-ch 1 oro i s thy Ipheno1 t roso-d i-n chloroe tha obenzene horone t ropheno 1 Dime thyIph 0 ic ac id 2-Chloroet Dichlo roph 4-Tr ich 1 or thalene loroan i 1 i n ch lorobu t a loro-3-met thylnaphth chlorocyc1 6-Tr ichlor 5-Tr i chlor 1 oronaph t h t roan i I ine thyIphtha1 aphthy1ene D in 11 rot o 1

hyl)e ther

nzene nzene

nzene

opropyI)ether

-propylamine ne

eno I

hoxy)me thane eno I obenzene

e d iene hyIpheno1 a 1 ene opent ad i ene opheno 1 opheno 1 a 1 ene

ate

uene

10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 50 10 10 10

Q

IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU < . \ j >J

FORM I SU-1 300475'


EPA SAMPLE NO.

I 1 I 1111068-08 I


Lab Code: INTECH Case No.: ^|-^0 SAS No.: SDG No. : ,/??/v/(?

Matrix: [soil/water] WATER Lab Sample ID:

Sample wt/vol: 1000 [g/mL] ML Lab File ID: >B7950

Level: [low/med] LOW Date Receieved: 11/12/91

% Mo Isture: dec 100.






CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L Q

99-09-2- 3-NitroaniIine 83-32-9 Acenaphthene 51-28-5 2,4-Din it ropheno 1 100-02-7 4-Ni t ropheno 1 132-64-9 Dibenzofuran 121-14-2 2,4-Din it roto luene 84-73-7 •--Diethylphthalate

7005-72-3 4-Chlorophenyl-phenylether 86-73-7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-me thylphenol 86-30-6 N-Nitrosodi pheny I am ine 101-55-3 4-Bromophenyl-phenylether 118-74-1 Hexach lorobenzene 87-86-5 -. Pent ach loropheno 1 85-01-8 Phenanthrene 120-12-7 Anthracene 84-74-2 Di-n-butylphthalate

2 06-44-0 Fiuoranthene 129-00-0 Pyrene 85-68-7 Butylbenzylphthalate 91-94-1 -3,3'-Dichlorobenzidine 56-55-3 Be nzo (a )an thracene

218-01-9; Chrysene 117-81-7 bis(2-Ethylhexyl)phthalate 117-84-0 Di-n-octylphthalate 205-99-2 Be nzo (b)f luoranthene 2 07-08-9 Benzo (k)f luoranthene 50-32-8 Benzo(a)pyrene 193-39-5 Indeno (1,2,3-cd )pyrene 53-70-3 D 1 benz ( a, h) an thracene 191-24-2 Benzo(g,h, i )perylene

1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10

1 IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I

^ 200

FORM I SU-2 300476



EPA SAMPLE NO.


Matrix: (501 I/water) WATER

Sample wt/vol: 1000 (g/mL) ML

^Level: (low/med) LOW

% Moisture: dec. 100.



' Number TICs found: 0

Lab Samp 1e ID:

Lab Flle ID: >B7950




Dilut ion Factor: | .00


CAS NUMBER 1 COMPOUND NAME 1 RT — = — — — — — — s = = = = = = = 1 s = = s s B s s s 3 B = s = m s = ass = s = s = sss = r: | a;ss=!as = = tt =

i 1

EST. CONC. Q

FORM I S U - T I C 1 /87 Rev .

210 300477


L a b Name:

m rmecU C o n t r a c t

ab code: l U f f C ) ) Case No.: ^i~^^ SAS No.:

Matrix: (soil/vater) "jfVi TEi

Sample wt/vol: / 0 ^ (q/nL)/^^

Level: (low/med) L O W

% Moisture: not dec. /tV dec. 0

Extraction: (SepF/Cont/Sonc) . " ^ u F

GPC Cleanup: ( Y / N ) ^ PH; 7t^

EPA SAMPLE NO.

SDG NO.: f^l/U^nJ

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted: > ' y ^ j ^ l

Date Analyzed: /I Mo / 9 f

M i / / j ) M I

CAS NO. COMPOUND

Dilution Factor:

CONCENTRATION UNITSJ (ug/L or ug/Kg)

NITS;

LO.

1 319-84-6 alPha-BHC 1 .0-6 1 L 1 1 319-85-7 beta-BHC 1 . C ^ \ ' 1 1 319-86-8 delta-BHC I , a^ 1 U 1 1 58-89-9 qamma-BHC (Lindane) | ,0"^ 1 V \ 1 76-44-8 Heptachlor 1 ,t'>f 1 \J 1 1 309-00-2 Aldrin 1 •O'i 1 i; 1 1 1024-57-3 Heptachlor epoxide | 'trf \ U 1 1 959-98-8 Endosulfan I \ .Of 1 ./ 1 1 60-57-1 Dieldrin 1 .f './O 1 1 1 72-55-9 4.4'-DDE 1 ./O 1 , 1 1 72-20-8 Endrin | </C 1 (' 1 1 33213-65-9 Endosulfan II 1 .jO | o 1 1 72-54-8 4.4'-DDD I /c? 1 ,/ 1 1 1031-07-8 Endosulfan sulfate | ./O | j 1 50-29-3 4.4'-DDT 1 -lO | | 1 72-43-5 Methoxychlor 1 ,SO 1 ; 1 1 53 4 94-70-5 Endrin Ketone \ . lO 1 ' 1 1 5103-71-9 alpha-Chlordane I , ^ \ j \ 1 5103-74-2 gamma-Chlordane | . S O \ <J j 1 8001-35-2 Toxaphene 1 /,0 1 i/ 1 1 12674-11-2 Aroclor-1016 1 -^ 1 j \ \ 11104-28-2 Aroclor-1221 1 - S 1 1 1 11141-16-5 Aroclor-1232 1 ' ^ 1 ; 1 1 53469-21-9 Aroclor-1242 1 ,5" 1 ^ 1 1 12 672-29-6 Aroclor-1248 1 , >' 1 1 1 11097-69-1 Aroclor-1254 1 h O \ ^ \ 1 11096-82-5 Aroclor-1260 I A 9 | j |


2V7 300478


Lab Name: I A/TEC P

EPA SAMPLE NO.

I f=)c]6 6 L M K

'Lab Code: I U T E ' C ) ) Case No.: ^^'^^ SAS No.:

Matrix: (soil/water) Wf JEf

Sample wt/vol: / (Wl^ (q/nL) t /IL

Leve 1: (1 ow/med) L O W

% Moisture: not dec. /?/// dec. C?

Extraction: (SepF/Cont/Sonc) V 5 E V ^

GPC Cleanup: ( Y / N ) ^ pH:7(y

Contract: ftJll^^/U j )35-(K?fc$'-c? rQ

SDG NO.: ^)L/^/l/

Lab Saaple ID:

Lab File ID:

Date Received:

Date Extracted; / / / / 4 / 9 /

Date Analyzed: //

CAS NO. COMPOUND

Dilution Factor:

CONCENTRATION UNITS/ ( u g / L o r uq /Kq) i l h / L -

3 1 9 - 8 4 - 6 3 1 9 - 8 5 - 7 3 1 9 - 8 6 - 8 5 8 - 8 9 - 9 7 6 - 4 4 - 8 3 0 9 - 0 0 - 2 1 0 2 4 - 5 7 - 3 9 5 9 - 9 8 - 8 6 0 - 5 7 - 1 7 2 - 5 5 - 9 72-20-8 3 3 2 1 3 - 6 5 - 9 72-54-8 1 0 3 1 - 0 7 - 8 5 0 - 2 9 - 3 7 2 - 4 3 - 5 5 3 4 9 4 - 7 0 - 5 5 1 0 3 - 7 1 - 9 5 1 0 3 - 7 4 - 2 8 0 0 1 - 3 5 - 2 1 2 6 7 4 - 1 1 - 2 1 1 1 0 4 - 2 8 - 2 1 1 1 4 1 - 1 6 - 5 5 3 4 6 9 - 2 1 - 9 1 2 6 7 2 - 2 9 - 6 1 1 0 9 7 - 6 9 - 1 1 1 0 9 6 - 8 2 - 5

-a lpha-BHC -beta-BHC " • d e l t a - B H C -gamma-BHC ( L i n d a n e ) - H e p t a c h l o r \ - A l d r i n -Heptachlor epoxide^ -Endosulfan I ^ -Dieldrin •4, 4 • -DDE -Endrin -Endosulfan .XI -4,4" -DDD -Endosulfan sulfate -4 ,4 • -DDT Methoxychlor_ Endrin ketone -alpha-Chlordane_ -gamma-Chlordane' -Toxaphene_ -Aroclor-1016 -Aroclor-1221' -Aroclor-1232' - A r o c l o r - 1 2 4 2 ] - A r o c l o r - 1 2 4 8 ' -Aroc lor -1254]^ - A r o c l o r - l 2 6 0 '

/ g ^ . ^ r . !££ 'CS •J2£

.J21. <cr • CS-

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300479


Lab Name: r/lTTFCH Contract : M^^/1/ Lab Code: j j l / n f C n Case No.: ^ '"^^ SAS No.

Matrix: (soil/water) O Q J ^

Sample wt/vol: .S<0'P (q/mL) W


% Moisture: not dec. I. dec. I»

Extraction: (SepF/Cont/Sonc) .bO/^L

GPC Cleanup: ( Y / N ) ^ PH: 7 - ^

SDG

EPA SAMPLE NO.

j r6 *^ 'C'-)P' I

I H^h/mi ' l

NO.: 2ZM

5H A

Lab Sample ID:

Lab File ID: _

Date Received:

Date Extracted: H J / ^ n ^

Date Analyzed: )l j ' ^ ^ T ^

Dilution Factor: \ > 0

CAS NO. COMPOUND CONCENTRATION UNITSX (ug/L or ug/Kg) I jJz/klZ

1 319-84-6 alPha-BHC 1 € . 0 1 U 1 1 319-85-7 beta-BHC 1 xD 1 J 1 1 319-86-8 delta-BHC 1 ^ 0 I U | 1 58-89-9 qamma-BHC (Lindane) I ^ 0 1 (/ 1 1 76-44-8 Heptachlor 1 )^€ 1 J 1 1 309-00-2 Aldrin 1 fc \ U \ 1 1024-57-3 Heptachlor epoxide I l$-V | J | 1 959-98-8 Endosulfan I \ 2i-0 \ U \ 1 60-57-1 Dieldrin 1 /(, \ J \ 1 72-55-9 4.4'-DDE 1 /(, 1 ;/ 1 1 72-20-8 Endrin 1 / 1 U | 1 33213-65-9 Endosulfan II 1 /<- 1 ; 1 1 72-54-8 4.4'-DDD 1 / 1 o 1 1 1031-07-8 Endosulfan sulfate 1 / 1 J 1 1 50-29-3 4.4'-DDT 1 / (, I , .' 1 1 72-43-5 Methoxychlor 1 ^-Q I i,' 1 1 53494-70-5 Endrin Ketone I /A 1 // 1 1 5103-71-9 alpha-Chlordane I l?p 1 ly 1 1 5103-74-2 qamma-Chlordane j ^ 0 1 ,/ 1 1 8001-35-2 Toxaphene 1 /^ C 1 i M 1 12674-11-2 Aroclor-1016 1 ^0 | U 1 1 11104-28-2 Aroclor-1221 1 ^ 0 1 J 1 1 11141-16-5 Aroclor-1232 1 fC 1 J 1 1 53469-21-9 Aroclor-1242 1 <5'i 1 >.; 1 1 12672-29-6 Aroclor-1248 1 '^0 1 J, 1 1 11097-69-1 Aroclor-1254 1 /^C'' | ^ | 1 11096-82-5 Aroclor-1260 1 /^(P 1 'J 1


300480


Lab Name; rmjzU Contract •.MtM iLab code: J I U T T C H Case No.: ^'~^^ SAS No.:

Matrix: ( so i l /water ) SClTt.

Sample wt /vol : 3 0 - 0 (q/mL) ^


% Moisture: not dec. 2. dec. >

Extraction: (SepF/Cont/Sonc) ^ t W ^

GPC Cleanup: (Y/N)J^ pH: 7- ^

EPA SAMPLE NO.

I JXh^H IS -17 ' I

SDG NO.: M ^

Lab Sample ID:

Lab File ID:

Date Received:

Date Ext rac ted : //'Iio 91

Date Analyzed: / / / ^ J ' ^ l

Dilution Factor:

CAS NO. COMPOUND CONCENTRATION UNZTSl , (ug/L or uq/Kq) (/b/C (7

319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 53494-70-5 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5

-alpha-BHC -beta-BHC -delta-BHC -gamma-BHC (Lindane) -Hept achl or \ -Aldrin -Heptachlor epoxide^ -Endosulfan I '_ -Dieldrin -4,4'-DDE -Endrin -Endosulfan LI -4,4'-DDD -Endosulfan sulfate -4,4' -DDT • Methoxychlor__ Endrin Ketone -alpha-Chlordane_ -gamma-Chlordane] -Toxaphene '_ -Aroclor-1016_ -Aroclor-1221' -Aroclor-1232' -Aroclor-1242] -Aroclor-1248] -Aroclor-1254] -Aroclor-1260'

XO. S£L .£>£.

Jj l

u W

JL

± /o

f J.

i O. ^

) 0

u

j i .

-Ll

.LL

-iA-^

± ±


239 300481

I D EPA SAMPLE NO. P E S T I C I D E ORGANICS ANALYSIS DATA SHEET

I J 6 # 3 A S ' ^ ' 1

ryl/lK^ contract: J | ! 5 M L I _2 l iL£££ :L . I

.WLab Code: '3^(1?^ Case No.: ^ 1 - ^ ^ SAS No.: SDG No.: U K U ^ A J

Lab Name:

Matrix: (soil/water)_5_^XL

Sample wt/vol: S O J ^ (g/v^) \7


% Moisture: not dec. ,y- dec. < '

Extraction: (SepF/Cont/Sonc) S ^ ^ ^

GPC Cleanup: (Y/N).^ pH: 8'-fP

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:,

Date Analyzed:

<A)

lj)5]9\

JlJM^ QI

CAS NO. COMPOUND

Dilution Factor:

CONCENTRATION UNITSl . (ug/L or uq/Kq) (;(7/r(7

iO

1 3 1 9 - 8 4 - 6 a lpha-BHC 1 }f£) \ U \ 1 3 1 9 - 8 5 - 7 beta-BHC 1 le 0 1 ^ 1 1 3 1 9 - 8 6 - 8 d e l t a - B H C 1 ^ . 0 1 L' 1 1 58-89-9 qamma-BHC (Lindane) I g'.D 1 (/ 1 1 76-44-8 Heptach lor 1 g\C> 1 'J 1 1 309-00-2 A l d r i n 1 ^.p 1 i; \ 1 1024-57-3 Heptach lor epox ide I < .0 1 u' 1 1 9 5 9 - 9 8 - 8 - Endosulfan I 1 ^ . 1 .' 1 1 60-57-1 D i e l d r i n 1 /A I I 1 72-55-9 4.4'-DDE 1 Jb 1 r 1 1 72-20-8 Endrin 1 /I. 1 ,,' 1 1 33213-65-9 Endosulfan .11 I /i, 1 . t 1 72-54-8 4,4'-DDD \ JC I I 1 1031-07-8 Endosulfan s u l f a t e 1 / 6 1 . 1 1 50-29-3 4,4'-DDT I /C 1 \J I 1 72-43-5 Methoxychlor 1 y?0 I -j 1 1 53494-70-5 Endrin Ketone 1 //, I , i 1 5103-71-9 a lpha -Ch lo rdane 1 jfo 1 ^ 1 I 5103-74-2 qamma-Chlordane I jU 1 i, 1 1 8001-3 5-2 Toxaphene 1 j/^O I 1 1 12674-11-2 Aroclor -1016 1 %o 1 1 1 11104-28-2 Aroc lo r -1221 1 iC 1 ; 1 1 11141-16-5 Aroclor -1232 1 KP \ o> \ 1 534 6 9 - 2 1 - 9 A r o c l o r - 1 2 4 2 i hV 1 ' 1 1 1 2 6 7 2 - 2 9 - 6 A r o c l o r - 1 2 4 8 1 S'/l 1 •.' 1 1 11097-69-1 Aroclor-1254 1 /hO \ 1 1 1 1 0 9 6 - 8 2 - 5 A r o c l o r - 1 2 6 0 I / l [ J | J j

FORM I PEST 1/87 Rev. ^ ' ( y r^> ' ^

300482

Lab

^FLab

Mat:

Samj

Lev*

% M<

Extl

GPC

--

•

--.

-

— •

ID PESTICIDE ORGANICS ANALYSIS DATA

Name: i A / ) t C ) ^ Contract

Code: J U I ^ C ) ) Case No.: ^ t - i > i SAS No.

rix: (soil/water) OT'L

3le wt/vol: 3 0 . ^ \ (q/mL) L7

il: (low/med) L Q W

sisture: not dec. ^- dec. 2 .

raction: rSenF/Cont/Sonc) ^ ^ C

Cleanup: (Y/N) Kj PH: 7 5

CONGE] CAS NO. COmOUND (ug/L

1 319-84-6 alpha-BHC 1 319-85-7 beta-BHC 1 319-86-8 delta-BHC 1 58-89-9 qamma-BHC (Lindane) 1 76-44-8 Heptachlor 1 309-00-2 Aldrin I 1024-57-3 Heptachlor epoxide 1 959-98-8 Endosulfan I 1 60-57-1 Dieldrin 1 72-55-9 4.4'-DDE 1 72-20-8 Endrin 1 33213-65-9 Endosulfan .11 1 72-54-8 4, 4'-DDD 1 1031-07-8 Endosulfan sulfate 1 50-29-3 4, 4'-DDT 1 72-43-5 Methoxychlor 1 53494-70-5 Endrin Ketone 1 5103-71-9 alpha-Chlordane 1 5103-74-2 qamma-Chlordane 1 8001-35-2 Toxaphene 1 12674-11-2 Aroclor-1016 1 11104-28-2 Aroclor-1221 1 11141-16-5 Aroclor-1232 1 53469-21-9 Aroclor-1242 1 12672-29-6 Aroclor-1248 1 11097-69-1 Aroclor-1254 1 11096-82-5 Aroclor-1260

EPA SHEET

1 X6«

: SDG No.:

Lab Sample ID:

Lab File ID:

Date Received: //

Date Extracted: //^

Date Analyzod: / J j

Dilution Factor:

1TRATI0N UNITS;i , or uq/Kq) (7(7/ r(7

1 £.0

1 j : . Q

1 2-c 1 6.0 ' ^-^ 1 r^o 1 Co 1 u 1 / / 1 //, 1 /^ 1 /y 1 J 1 /6 1 ??o 1 )C 1 ^ D 1 ^ D 1 /U-> 1 S" 1 SO 1 ^ ( ? 1 K D

1 ^u 1 /Jiip 1 /If?

SAMPLE NO.

Ml tU

Q

1 iJ 1 1 0 1 1 L 1 1 f 1 1 I.' 1 1 -J 1 1 / 1 1 ^ 1

1 '' 1 1 ./ 1 1 '.' i 1 _„ Ji i t 1 1

' i. ) , ' 1 ^ 1

1 ^ 1

1 1,' 1 1 u' 1 1 1 1 1 V 1 1 ' ' 1 1 \'! 1 1 U 1

1 -. I 1 ^' 1


C O i

300483


Lab Name: JM£Ci Contract •.MbML 'Lab Code: J^ tV^Cn Case No.: L)-^'^ SAS No.:

Matrix: ( so i l /water ) SOd-L

Sample wt /vol : S 0 ( ^ (g/nL) W


% Moisture: not dec, c - dec. <?<•

Ext rac t ion : (SepF/Cont/Sonc) 5^/VC

GPC Cleanup: ( Y / N ) ^ pH: / ^ ^

EPA SAMPLE NO.

_ I t / ^ / ' j / p ^ - 7

SDG NO.: ^ H j m j

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted

Date Analyzed:

Dilution Factor:

CAS NO. COMPOUND CONCENTRATION UNITS (ug/L or ug/Kg)

HITS;, /

319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 53494-70-5 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5

-alpha-BHC -beta-BHC ~ -delta-BHC -gamma-BHC (Lindane) -Heptachlor [ -Aldrin -Heptachlor epoxide_ -Endosulfan I ] -Dieldrin -4,4* -DDE -Endrin -Endosulfan II •4,4' -DDD -Endosulfan sulfate •4 ,4 • -DDT ] Methoxychlor_ Endrin Ketone -alpha-Chlordane_ -gamma-Chlordane] -Toxaphene -Aroclor-1016 -Aroclor-1221] -Aroclor-1232' -Aroclor-1242] -Aroclor-1248] -Aroclor-1254] -Aroclor-12 6 o'

• O

. 0 £JL. JLD-

z± Q_

(7

AL

J J L mLU

.LL

-"nfr

i L -W-

^ L

FORM I PEST 1/87 Rev, o ^ -

300484

TOTAL ME:TAI...S &. CYANIDE COVER F'AGE - INORGANIC ANALYSES DATA PACKAGi;;:

;ib Name;

I^Pcode:

. : :M V\O „ ;;

.-,

; CEI11IC

; CEIMIC C a s e No.,;!

7 / 8 8

SAMPLE ID F.lEf.1.109 FBi.:i.: IB»*3 IB*43 I B n 3 IB*^3 IB** 3 IBM- I I B « 4

1.0 2 5 - • 2 7 3 0 - - 3 4 3 5 - 3 9 3 5 - 3 9 D 3 5 - - 3 9 S 1 0 - 1 2 .15-.1.7

Contract:: ANSON

SAS No,.;; SDG No., s FB;H09

_.ab Samp>Ie I D , 006 : l .9 -08S 006:l.9--04S 0 0 6 1 9 •0.1.S 0061 .9 -02S 0061.9^^03S 0061.9--03S2 006. I .9-03DS 0061 .9 -06S 0 0 6 1 9 - 0 7 S

Wi^^ ' ICP i n t e r e l e m e n t c o r r e c t i o n s a p p l i e d ? Y e s / N o NG Were ICF' b a c k g r o u n d c o r r e c ^ t i o n s a p p l i e d ? Y e s / N o YES

I f y e s - w e r e raw da ' ta g e n e r a t e d b e - f o r e aI:JP:1. i ca l.:i.on o-f hacI'-.g r o u i i d c:or r e c t i o n s 7 Y e s / N o N0

r jmrnen i-ss

I certi-fy that this dat-a package is in compliance with the terms and jnditions of the contract., both technically and for comp le ten (ess., for Uier than the conditions detailed above,. Release of the data contained

in this hardcopy data package and in the computer-readable data submitted I-'I floppy diskette has been authorized by the Laboratory Manager or the I \naqer's designee,, as verified by the following signaturo?,,

.Signature;; ..O...m.Uf<i.:...^kM<::r. H mis;; ..^Btlk.lil.'S. S.h..LLk..^.

_.ni(f.A.}_ .._ •;...•i-.ie;; .._.J^/]o/;H(A^.n±,<L, .5y.j?.?.'!;.. /.?c) „ Late;;

COVER PAGE •• IN Rev,. 6/89

300485

TOTAL I1ETAI...S &. CYANIDE

INORGANIC ANALYSIS DATA SHEET SAMPLE ID

: FB;L:L09 ab Name;; CEII1IC Contract;: ANSON I.._

Lab Code;: CEIMIC Case No.. :: ANSON SAS No„:: SDG No„:: FBI 109

jitrix (soil/water):: WATER Lab Sample ID:: 00619-08S

•evel (low/med):: LOW Date Received s 11/12/91

;r Solids;; 0,.0

("on cen tra ti on Un i ts (uq/L or mg / Kci d r y we iq ht) s UG/L

: j l o r B e f o r e : ; C

C o l o r A f t e r ; : COLGRLESJii

CAS No. An a 1 y t e I Con c&^n t r a t i on

7429-7440-7440-7440-7440-7440-7440-7440" 7440-7440" 7439" 7439-7439-7439" 7439" 7440-7440" 7782-7440-7440" 7440" 7440" 7440" 7440-

•90-" 5 -36-0 •3S--2 •39-3 -41-7 -43-9 •70-2 -47-3 •48-4 -50-8 •89-6 •92-1 -95-4 •96-5 •97-6 •02-0 •09-7 •49-2 -22-4

I Aluminum I Antimony lArsenic 1 E-iarium I .Beryllium I Cadmium [Calcium I Chromium ICobalt ICopper I Iron ; Lead I Magnesium !Manganese I Mercury INickel ! Po (..assium I Selenium ISilver :

D Ibodium -28-0 -31-5

•C)(-.>~i>

I Thallium ITin I Vanadium I Z i ri c I Cyanide

102 ,.00 45„00 2»00 3.00 6 „ 00 4.. 00

108„00 7.. 00

10,. 00 8„00

74,. 00 1.00

61..00 1,. 00 0.. 20 12,00

2140 ..00 4 .00 6.. 00

4450„00 2.. 00

4., 00 2.. 00

10.. 00

C1 a ri ty Before:: CLEAR

Clarity After;: CLEAR

Q

W

M

p"~

F-' F F' F' F' F-F' P F' F' F" F' P CV P F' I"' P P F NR !=•

F' C

Textures

Artifacts

...•c.;>mmen l..r

FOr:;M I - I N 3

300486

TOTAL METAL &. CYANIDE

INORGAhllC ANALYSIS DATA SHEET

ab Name;; CEIMIC

.ab Code;: CEIMIC

Contracts ANSON

Case NO..S ANSON SAS No.

SAMPLE ID

FBlllO

SDG No„= FBI109

vvtrix (soil/water);: WATER

»vel (low./med)s LOW

Solids;; 0..0

Lab Sample ID:; 00619-04G

Date Received:: 11/12/91

Con cen t I'a t i on Un i ts (ug /L o i" mg /Kg d r y we i g h t) s UG/L

Before:;

ICAS No..

I 7429-90-5'" 17440-36-0 I 7440-38-2 17440-39-3 17440-41-7 ;7440-43-9 ;7440-70-2 ;7440-47-3 17440-48-4 17440-50-8 I 7439-89-6 17439-92-1 ;7439-95-4 17439-96-5 17439-97-6 ;7440-02-0 17440-09-7 I 7782-49-2 I 7440-22-4 17440-23-5 17440-28-0 17440-31-5 I 7440-62-2 I 7440-66-6 [

coiloRLiss

1 Analyte

1 Aluminum 1 Antimony 1 Arsenic 1 E<arium I Beryllium' 1 Cadmium I 1 Calcium I I Chromium I ICobalt I ICopper I 1 Iron I I Lead I I Magnesium,' 1 Manganese 1 1 Mercury I INickel 1 1 F'otassium 1 |So:-?lenium I ISilver I 1 Sodium 1 1 Thallium I ITin 1 [Vanadium 1 I Z i ri c 1 ICyanide I

"'"Cla'ri-l

1 1

Concentration IC 1

_______ _...

45«O0IU 2„001U 3.00 IU 6,00 1 4,00 IU

131..00 IB 7„00|U

10.00IU 5„00 IB

62-00 IB 1« 401B

48..00 IB 1.. 00 1 B 0„20|U

12-OOIU 2140 ..00 I U

4„001U 6.. 00 I U

4450„00 IU 2..00IU

I 1

4„00|U 7^00 IB

10„00|U 1

.y""Befores CLEAR

1 1

Q IM 1

1 P ' IP IF IP 11"' IP IP IP IP IP IP IF I F' IP ICV IP IP IF IP IP IF I NR IP IP IC

"" Ter < ture-( ) I o r

C o l o r A f t e r : : COLORLESS

(.5\.:immeri •Ls;

C l a r i t y A f t e r : : CLEAR A r t i f a c t s : ;

300487

•ORI' I K / 8 8

roTAi... Mi;;:TALS &. C Y A N I D E


I

I IBi*3 25-27 VIb Name;; CEIMIC Contracts ANSON I_

ab Code;: CEIMIC Case No„s ANSON SAS No.s SDG No,, s FBI 109

.fttrix (soil/water)s SOIL Lab Sample IDs 00619-0IS

-;o v e 1 (1 o w / m e d ) ;: L.. 0 W D a t e R e c e i v e d s 11 /12/91

l:i.d-: 97., 9

Concentration Units (ug./l... or mg./|<g dry weight) s MG/KG

ICAS No.

M.?....

I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7439 I 7439 I 7439 I 7439 I 7439 I 7440 I 7440 I 7782 I 7440 I 7440 I 7440

9 0 - 5 - 3 6 - 0 - 3 8 - 2 - 3 9 - 3 - 4 1 - 7 - 4 3 - 9 - 7 0 - 2 • 4 7 - 3 ••48-4 - 5 0 - 8 •89 -6 • 9 2 - 1 • 9 5 - 4 •96 -5 •97 -6 - 0 2 - 0 - 0 9 - 7 •49 -2 X.. A.. '-T

28-0 7440-31-5

K.I .<.. A. .

/ • . - . . • < - .

•7440. 7440- ' . - , < : > • •

An a 1 y te I Con cG-?n l-. rat i on

Hlum m u m ; Antimony I Arsenic I Eiarium 1 Beryllium I Cadmium I Calcium I Chromium | Cobalt I Copper I Iron I Lead I Magnesium I Manganese I Mercury I Nickel I F'otassium I Selenium I Silver I Sodium I Thallium I Tin I Vanadium I Zinc I Cyanide I

15 50 ..00 4.. 00 0 „ 86 5,00 0. 0, 36

37.. 30 3„00 0.89 1,. 50

lllOuOO 1.. 20

127 ..00 26,. 90 0.. 09 1„10

191„00 0 „ 40 0.. 54

397.00 0.. 20

2 „ 00 2.. 80 2.. 00

C Q

'*E"

N*

*

N N

*

M

CV F" P F P P F NR

f jlor Before;; BLACK C1 a !'• i •[. y B e i ' a r e :; Texture FINE

C'-ilor After; YELLOW Clarity After Artifacts

tummen 'I;.

300488

FORM I ^7/BB

lames CEIMIC

:ode;: CEIMIC

TOTAL METAI...S &. CYANIDE

1 [NGRGANIC ANALYSIS DATA SHEET

Contracts ANSON

SAMPLE ID

I IBn3 30-34

Lab Code;: UhlMlU Case NOi, s ANSOh

VI t !'• i X (;; o i ]. / w a t e !'•) s S O I I...

Bve]. (low/me?d) s

SAS No,,;; SDG No„:; FBI 109

Lab Sample IDs 00619-02S

Date Receiveds 11/12/91 LOW

.ids;; 97.7

Concentration Units (ug./|... or mg/Kg dry weight) s MG/KG

^ ^ ^ # -^•^

( >loi-' Befoi-es

C o l o r A f t e r s

Ci.:immen ts;;

-—-»- — — .—— .-.-- —-

I C A S No..

1 7429-90-5"" I 7440-36-0 17440-38-2 I 7440-39-3 ; 7440.-41-. 7 ;7440-43-9 I 7440-70-2 I 7440-47-3 I 7440-48-4 17440-50-8 17439-89-6 17439-92-1 17439-95-4 17439-96-5 17439-97-6 I 7440-02-0 I 7440-09-7 I 7782-49-2 I 7440-22-4 17440-23-5 I 7440-28-0 17440-31-5 17440-62-2 !7440-66-6 I -

BLACK

YELLOW

__......_..»__»..._.... -

Analyte I C(

Aluminum ! Antimony 1 Arsenic 1 Barium I Bei'yilium I Cadmium I Calcium I ChromiLim I Cobalt I Copper I I I'on 1 Lead 1 Magnesium 1 Manganese 1 Mercury I Nickel I F'o Lass ium 1 Selenium I Silver I Sodium I Thallium I Tin I Vanadium I Z :i. ri c I Cyanide 1

Clarity

Clarity

incentration I C

2140700 I"" 3 .. 80 I U 0..45IB

12„30 IB 0.. 34 I B 0,. 59 1

74.. 00 I B 6 „ 0 0 I 1.. 6 0 I B 3 „ 50 I

6360.. 00 1 0.. 94 1

473.. 00 I 93.30 1 0,.10IU 1.. 50 1 B

228 ..00 IB 0.34 1 U 0.. 51 IU

375.,001U 0.. 17IU

6.00 I 8., 90 1 2.. 00 1 Ll

Befores

Afters

. » _ . ..M — M — « •—• ~

Q

...._..-

N>fi

;{•:

NW N

*

—..«...«. _ ..„ ™

"***"""

M I

-;-,

F' 1 F" I F' 1 I"' I P-' 1 F' I F' 1 P I P I I"' I F 1 F' 1 F' I C V I F' I F' I F 1 P I F' I F I NR 1 F' I P I C 1

Textures

Artifacts

FINE

300489

"ORM I IN

TOTAL METALS &. CYANIDE


I

I IB**3 35-39 I ' — -_„„_ . ab Mame;; CEIMIC Contracts ANSON

Lab Code:; CEIMIC Case No., s ANSON SAS No„s SDG No., s FBI 109

..atrix (soil/water) s SOIL Lab Sample IDs 00619-03S

-evel (low/med)s LOW Date Receiveds 11/12/91

97.. 8

Con cen tration Uni ts (ug/L or mg/Kg dry weight)s MG/KG

.-:: bo.I, Ids;;

y.\.ov- Bef ores BLACK

' o lo i flT'ters

commen t s s

CAS No..

74'29-90-5~ 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

LACK

ELLOW

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium ' Chromium I Cobalt I Coppo?r I Iron 1 Lead I Maqnox'sium ' Manganese Mojrcury Nickel F'otassium ' Selenium Silver Sodium Thallium Tin Vanadium Z :i. n c Cyanide

„.„„..._.

Clari1

C o n c e ri t ration

1520700 4.60 0.,80 7,. 60 0..41 0.92

32.. 10 9.. 60 1.. 00 2„20

9140 ..00 1.. 00

152.. 00 47.. 90 0..10 1..20

219.. 00 0 „ 37 0..61

455.00 0.. 18

6.10 12.90 1„90

•.y Be fores

•.y Afters

C

—

I..I B B B

B

U B

B

1..1 U U U U U U

U

""

Q

" " * E

N*

*

NW N

>!•:

M

p~

F' F F-F' F' P F' F' P F' F F' F' CV F-' P F P P F NR F-F' C

Te;

Ar-

<tures

:ifact

FINE

300490

l-ORM I IN

TOTAL METALS «; CYAhllDE

INORGANIC ANALYSIS DATA SHEET SAMF'LE ID

I IB**4 10-12 ab Names CEIMIC Contracts ANSON I

Lab Codes CEIMIC Case No-s ANSON SAS No., s SDG No„s FBI 109

atrix (soil/water)s SOIL Lab Sample IDs 00619-06S

!-eveI (low/med )s LOW Date Received s 11/12/91

>;; Sol ids s 98 ..7

Con cen t ra t i on Un i ts (ug/L oi- mq./Kg d r y wo?i g h t) s MG/KG

Dior Be fores

Color A-f ter s

tommen ts s

CAS No..

7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-

90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 "49-2 -22-4 7440

7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

BLACK

YELLOW

Analyte

Aluminum Antimony Arseni c Barium Beryl1ium Cadmium Calcium Chromium Cobalt Copper I ron Lead Magnesium Manganese Mercury Nickel F'otassium Selenium Silver Sodium Thallium Tin Vanadium Z :i. n c Cyanide

C' 1 a !'• i

Con c e n t r a •!: i o n

94 5. 4. 0. 3. O. 0.

O,. 4- u

8410. 1.

179.. 49. O.. 1.

196.. 0. 0-

403, O,

00 10 57 90 28 92 60 70 92 50 00 90 00 80 10 10 00

00 18

3.. 40 5.80 1.90

C

Ll

Q

"*E"

M*

*

NW

*

/ Before s

Clarity After:

M

F' I"' F' F' F-F' F' F-F F' F' CV F' F' F F' F' F NR I"' F' C

T e x t u r e s FINE

A r t i f a c t s s

300491

FOR IN / . ' \ . j I.? 8

TOTAL METALS & CYANIDE

1 INORGANIC ANALYSIS DATA SHEET

SAMPLE ID

I IB#4 15-17 \ \b Names CEIMIC Contracts ANSON I _ _

Lab Code;; CEIMIC Case No., s ANSON SAS No,, s SDG No.s FBI 109

Ldtrix (soil/water)s SOIL Lab Sample IDs 00619-078

r;vel (low/med)s LOW Date Receiveds 11/12/91

^ Sol idss 98.4

Con cen t ra t i on Un i ts (ug/L o r mg/Kg d ry we ig h t)s MG/KG

7429" 7440" 7440-7440" 7440" 7440" 7440" 7440-7440" 7440-7439-7439" 7439" 7439" 7439" 7440-7440" 7782" 7440-7440" 7440-7440-7440-7440

^lo „

9 0 - 5 " •36-0 •38-2 •39-3 •41-7 4 3 - 9

" 7 0 - 2 - 4 7 - 3 - 4 8 - 4 - 5 0 - 8 - 8 9 - 6 - 9 2 - 1 - 9 5 - 4 " 9 6 - 5 - 9 7 - 6 " 0 2 - 0 - 0 9 - 7

'•t .•• A . .

"22-4 -23-5 "28-0 -31-5 .. /. '-:•... o \..' X.. I I . .

-66-6

( )lor Befores BLACK

r-)lor After;: YELLOW

Commen 'Ls s

Analyte

Aluminum An'timony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt CoppOlM'-I ron Lead Magnesium Manganese Mercury Nickel F'otassium Selenium Sils.'er Sodium Thallium Tin Vanadium Z i 11 c Cyanide

C1 a r i

tration

••349755

4.. 50 0..24 3.. 10 0.. 30 0.40

73.. 60 2,. 90 0 „ 99 1.80

3160.00 0,. 83

154„00 33.20 0.. 10 1 „ 20

212.. 00 0,. 39 0.. 59

441.00 0., 19

1.. 90 4,. 10 2 „ 00

Cl — '

UI BI BI Bl Ul Bl

Ul Bl

BI

Ul UI Ul Ul Ul Ul Ul

B"

UI

Q

">KE"

^i*•

-"IW N

*

E<ef ore;

C 1 a I" :i. t ••/ A f t (•>? i"

M

F P P CV P P F P P F NR I"' F' C

Tex

Art

tures FINlii

ifactss

300492

•OR Ih 7 / 3 8

Unvalidated Data

Indoor borings 1 & 2 Re-sampling drywells 5-9, catch basin

300493

TOTAL METALS &. CYANIDE: COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name;; CEIMIC Contracts ANSON

i^ Code;; CEIMIC Case No.s ANSON SAS No.s SDG No., s CATCH.._BA

' No„ :; 7/88 SAMPLE ID CATCHB DW5 DW6 DW7 DW8 DU)9 FB0104 FB0105 IBllO IBllOD IBllOS IB115 IB210 IB215

I'

ll

II

I!

i >

I

i

II

I!

II

I!

ti

ll

i !

! i

i i

i I

1

Lab Sami 00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-

Dle ID. -OlS -02S -03S -•04S ••05S -06S - U S -12S -07S -07S2 -07DS -08S -09S -lOS

ICF' interelement corrections applied? Yes/No HO ICF' background corrections applied? Yes./No YES If y(-?s-were raw data generated before-? application of background corrections? Yes/No NO

i.,ommer] ts

cerl:.ify thai:, this data package is in compliance with the terms and conditions of the contract., both technically and for completeness,, for * other than the conditions detailed above.. FU-?leaso? of the data contained n this hardcopy data package and in the computer-readable data submitted ..j-i floppy diskette has been authorized by the Laboratory Manager or the Manager's designee^ as verifi(-?d by the following signature.

iqnaturei

' ^^-^^ ' ' '^^ ' ..-.^a^.Mc RhA,.^. COVER PAGE - IN Rev..6/89

300494

3

I ^ ^ Names CEIMIC

TOTAL METALS ,S-: CYANIDE

5A ;;5F'IKE SAMF'LE REiCOVERY

Contracts ANSON

SAMPLE ID

IBllOS

SDG No.. T. CATCH_BA

Level (low./med)s LOW

Lab Codes CEIMIC Case No.s ANSON SAS No.s

L,.\trixs SOIL

"-Solids for Samples 99.0

Concentration Units (ug/L or mg/kg dry weight)s MG/KG

i '"

Analyte

'Iluminum In timony

I Arsenic I.Bar ium •ieryllium

,oadmium 1 Calcium ^l^omium ^^^alt I Copper ' ': ron .ead

; riagnesium I M a n g a n e s e lercury

...lickel 1 Potassium ">elenium •: i .1 ve r

1 Sodium '.Thallium Vanadium

(•Zinc 1 Cyanide

Control L i m i t

;\;R

75-125 75-125 75-125 75-125 75-125

75-125 75-125 75-125

75-125

75-125 .75-125 75-125

75-125 75-125

75-125 75-125 75-125 75-125

Spiked Sample Result (SSR) f

-«--»-„.—.„__....,.„....„_--„_____„

80.8080 1 7.19011

357.35981 8„6300 I 9.8068 1

37.26581 87 ..4767 I 47.0726 1

6„0698 i

145.5329 1 0.37961

89„63421

1.7723 i 12.1604 1

9.1644 1 91.5955 1 90.2226 I 14.43431

1 Sample :i Result (SR)

I 9.61071 I 1.4869 I 1 7.2570 1 I 0.78451 I 1.17681

I 11.5720 1 I . 1.7652 1

4.31501

1 1„96361

1 66.8824 1 1 0.09621 I 2.3536 1

1 0.48481 1 0„9307 I

I 0.1616 1 1 8.04161 I 7„6493 I I 1.2500 1

u

S p :i. ke Added (SA)

98,. 07 7.35

>92„27 9.81 9.81

39 „ 23 98.07 49 „ 03

3.67

98 „ 07 0.40

98.07

1.84 9.81

9.18 98 ,.07 98 „ 07 16.67

ZP.

B:

89. 80. 88.

oo,. 89. 87.

111.

80. 94. 89.

96. 114.

99, 85. 84. 86.

IQ _ • _ .

41 6 1 3 1 01 01

5IN

O 1 A- t

91

X.. 1

91 01

3 1 01

81 X . . 1

^~ 1

61

Ml

NRl F' 1 F 1 F' 1 P I F' I NR I F' I P 1 F- I NRI F 1 N R t F' 1 CVI P I NR I F 1 F' I NR I F ' P I F' 1 C 1

Comments s

FORM V (PART 1) - IN 7/88

300495 4

!re Names CEIMIC

Lab Codes CEIMIC

.vatrixs SOIL

TOTAL.. METALS &. CYANIDE

5B. POST DIGEST SPIKE SAMPLE RECOVERY

Contracts ANSON

Case No„s ANSON lo „ s

SAMPLE ID

IBllOA

SDG No „ s CATCH._BA

Level (low/med)s LOW

Concentration Unitss ug/L

—— — —

i ^ '

1 Analyte

, Aluminum 1 Antimony iirsenic Barium

1 Beryllium 'Cadmium I^alcium

,Chromium ICobalt ^^^p('?r

1 Lead ' 'lagnesium 'langanese

1 Mercury INickel -'otassium

, ..Selenium ISilver • .Sodium Thallium

I Vanadium 'Zinc i. yan ide

t _„„._„.„

.., ™. . . . ..._ ™ . . . . - » . . . . .

Control 1.. .1. m i t

rv.R

( MnrncvM"! tii>::

"""'"

S p i ked Sam p1e Result (SSR) C

161.00

«.

** "*•• "* -* **— — * " ~ " ~ — • -*" •*** •*" ••** •

Sample Result (SR)

59 „ 00

_. _—

C

_„„, _-,-.-- — - . . ™ ™ ™ -

Spike Added (SA)

100.0

ZR

102.0

— —

* • • • * " "

Q

—-—

I'i

NR NR NR NR NR NR NR F' NR NR NR NR NR NR NR NR NR NR NR NR NR Hfl HR hIR

FORM V (PART 2) - IN 7/88

300496 5

TO'TAL ME:'IAL;B &: CYANIDE

SAMPLE ID DUF'LICATES

IBllOD

lames CEIMIC Contracts ANSON

.sb Codes CEIMIC Case No.;; ANSON SAS No.s SDG No.s CATCH....BA

Ma 11- i X ( so i 1 / wa ter ) s SO IL Leve 1 (1 ow/med ) s LOW

:v Solids for Samples 99.0 Z Solids for Duplicates 99.1

Concentration Units (ug./L or mg/kg dry weight) s MG/KG

Analyte

Aluminum An timony Ai'sen i c Barium .Beryllium Cadmium Calcium Chromium Cobalt Copper Iron ead

Magnesium Manganese Mercury Nickel F'otassium Selenium Silvo^r Sodium Thallium 'vV an ad ium 'Z. i n c Cyanide

Control L i m :i. t

1.0 980.7

2.0

0.5

;.9

Sample (S) C

1609. 9. 1. 7. 0. 1.

911. 11. 1. 4.

5641. 1.

.<;;w;7i

66 0 X . . <

163 0 0

173. 0 8 7 1

8843 6107 4869 2570 7845 1768 0517 5720 7652 3150 8520 9636 1817 8824 0962 3536 3813 4848 9807 7765 1616 0416 6493 2500

Duplicate (D) C

1741. 9. 0. 7. 0. 0.

1020. 5. X., n

4. 4778.

A.. H

344. 71. 0.

219. 0. 1.

148. 0. 4. 8.

1741 8010 8784 4007 6001 8001 9021 4005 0002 6005 8778 3891 0344 4071 0878 4003 4219 5270 OOOl 4148 1757 4004 0008 5572

RF'D

-•-•-

51.5 2.0

26.6 38 „ 1 11.4 72.7

200.0 6.4 16.6 19.6 18.7 6.5

36.4 29 „ 3

2.0 15.7

58 „ 5 4.5

Q

*

Ml

P~\ P 1 F 1 F' 1 P I P 1 P 1 F' I F- 1 F' 1 P I F I F' I P 1 CVI P 1 P 1 F 1 F' 1 F' 1 F 1 F' 1 F' 1 C I

300497 FORM VI - I N V 8 8

TOTAL MEiTALS & CYANIDE

9 ICP SERIAL DILUTIONS

SAMF'LE ID

IBllOL Names CEIMIC Contracts ANSON _ .

ab Codes CEIMIC Case No.s ANSON SAS No.s. SDG No.s CATCH._.BA

Matrix (soil/water)s SOIL Level (low/med)s LOW

C^on cen 1: r a t i on l.Jii i ts s uq /I...

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese ni?>rc.K.\ry Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc

Initial Sample F;esul t (I)

„ _ „ _ _ „ . „ . . .

49.00

37 „ 00 4 „ 00 6.00

4645.00 59.00 9.00

22 „ 00 28765.00

1454.00 341.00

12.00 833.00

5.00 886.00

41-00 ,39.00

B

'r.-ji~>r-xa.l Dilution

Result (S) C

siiiTooT"" 245.00 IU

20.00 IB 20.00 IB 20.00 IU

4780.00 IB 75.001 45.00 IU 25.00 IB

29560.00 1

1465.00 IB 355.001

65.00 IB 1535.00 IB

15.001B 820.00 IB

45.00 IB 45.00 IB

Difference

1.1

45.9 400 „ 0 100.0

2.9 A . . / I* x

13.6 2.8

0.8 4.1

441.7 84.3

200.0 7 „ 4

9.8 15.4

Q M

P~ P NR P P F-F' P P P P NR P P NR P P NR F' P NR P P

•ORM IX - IN

30049S'

TOTAL. METAI..S & CYANiLDE

SAMPLE ID INORGANIC ANALYSIS DATA SHEET

CATCHB Name;; CEIMIC Contracts ANSON I

,...ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA

••-atrix (soil/water) s SOIL Lata Sample IDs 00006~01S

l._evel (low/med )s LOW Date Received s 01/07/92

Sol idss 92.1

Concentration Unilis (ug/L or mg/Kg dry weight) s MG/KG

CAS No.

7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-

90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 92-1 95-4 96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 60 o

66—6

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mo? r cury Nic ke1 F'otassium Selenium Silver Sodium Thallium Vanadium Z i n c Cyanide

Con cen t nx t i 011

0.09

.00

C

U

U

Q

Color Befores BROWN

fco1o r Af te r s YELLOW

I Dmmei^i tn;. s

Clari ty Before s

C1 a r i ty Af "te r s

M

NR hIR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C

Textures MEDIUM

Ar^tif actss

•ORM - IN 7 /88

8 300499

TOTAL METALS &: CYANIDE


SAMPLE ID

DW5 lame s CE IMIC Con t r<- c t s ANSON

•b-ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No-s CATCH_BA

'a t r i x (so i1/wa te r)s SOIL La b Sam p1e IDs 00006-028

C'evel (low/med )s L_OW Date Received s 01/07/92

Sol idss 95.9

Concentration Units (ug/L or mg/Kg dry weight) s MG./KG

CAS No.

•7429-7440" 7440-7440" 7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-

• 90 -5 • 3 6 - 0 •38 -2 •39 -3 •41 -7 •43 -9 •70 -2 •47 -3 4 8 - 4 •50 -8 8 9 - 6 •92 -1 9 5 - 4 •96 -5 9 7 - 6 0 2 - 0 0 9 - 7 •49-2 2 2 - 4 •23 -5 •28 -0 O.C. .^.

•66-6

A n a l y t e

Aluminum Antimony A r s e n i c Barium B e r y l l i u m Cadmium Calcium C h r o m i u m C o b a l t C o p p e r I r o n l._ead M a g n e s i u m Manganese M e r c u r y N i c k e 1 F ' o t a s s i u m Selen ium S i l v e r Sodium T h a l l i u m Vanadium Z inc C y a n i d e

C o n c e n t r a t i o n

0 . 0 9

1 „ 9 0

U

LJ

Q

• ^ ' o l o r B e f o r e s BROWN

u o l o r A f t e r s YELLOW

o m m e n t s s

C 1 a !'• i t y B B f o r e ;

C l a r i t y A f t e r s

M

NR NR NR' hIR hlR NR NR NR HR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C

Textures MEDIUM

Artifactss

•0R:M I - IN 7 / 8 8

300500

TOTAL.. METALS & CYANIDE

INORGANIC ANALYSIS DATA SHEET SAMF'LE ID

1 DW6 Name;; CEIMIC Contracts ANSON 1

,.ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA

" vitrix (soil/water) s SOIL Lab Sample IDs 00006-038

Level (low/med )s LOW Date F\'eceiveds 01/07/92

84.7 SolIdss

Concentration Units (ug/l._ or mg/Kg dry weight) s MG/KG

CAS No.

7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-

•90-5 •36-0 •38-2 •39-3 •41-7 •43-9 •70-2 •47-3 48-4 •50-8 89-6 92-1 95-4 96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 6 r-i r y

<.. .C

66-6

Analyte

Aluminum Ant.imony Arsenic E<arium Beryllium Cadmium Calcium Chromium Cobalt Co p pe r Iron Lead Magnesium Manganese Mercury N i c ke 1 Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide

Con CBn t ra. -tion

0.09

2.30

U

Ll

f' olor Bef ores BROWN

color Afters YELLOW

C1 a r :L t y B e fore;

Clarity Afters

Q M

NR NR' NR NR NF,' NR NR NR NR NR NR hIR NR NR CV NR NR NR NR hIR NR NR NR C

Textures MEDIUM

Artifactss

ommen '..s s

FORM I - I 7 /88

10 300501



DW7 i Names CEIMIC Contracts ANSON 1

:;ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH__BA


..e'-.'el (low/med) s L.OW Date Received s 01/07/92

Sol idss 87.0

Concentration Units (ug/L. or mg/Kg dry weight) s MG/KG

CAS No.

7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-

•90 -5 •36 -0 •38 -2 - 3 9 - 3 - 41 -7 - 43 -9 •70 -2 •47 -3 •43 -4 •50 -8 •89 -6 •92 -1 9 5 - 4 •96-5 9 7 - 6 •02-0 0 9 - 7 •49-2 A.. A.. ' 'T

A..\.> \ . '

•28-0 •62-2 •66-6

•-"olor Befores BROWN

Color Afters YELLOW

omments s

Analyte

Aluminum Antimony Arsenic Barium E<eryllium Cadmium Calcium Chromium Cobalt Copposr I ron Le^ad Magnesium Manganese Mercury Nickel F'otassium Se1en i um Silvo^r Sodium Thallium Vanadium Z i n c Cyanide

Con cen t ra t i on

0.34

1.90

C

U

Q

Clari•ty Before:

C .1 a r i 1: y A f l'. e r:;

M

NR NR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C

Textures MEDIUM

Artifactss

FORM I IN 1 j_7/8S

300502

TOTAL METALS &: CYANIDE

INORGANIC ANALYSIS DATA SHEET SAMPLE IT!

DW8 lames CEIMIC Contracts ANSON I„

ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA


..evel (low/med )s LOW Date Received s 01/07/92

Sol idss 89.2


CAS No.

7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439" 7439-7439-7439-7439-7440^ 7440-7782-7440-7440-7440-7440-7440-

90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 -48-4 -50-8 -89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 -49-2 -22-4 -23-5 -28-0 6'_.'-.'> X . . X . .

-66-6

Analyte

Aluminum Antimony Arsenic Ba r i um Beryllium Cadmium Calcium Chromium Cobalt Copper I I'on L_ead Magnesium Manganese Mercury N i c l'-.e 1 Potassium Selenium S i1ve r Sodium Thallium Vanadium Z i n c Cyanide

Con cen tra ti on

0.26

,00 U

Q

c^olor Befores BROWN

Color Afters YELLOW

.•)mmen ts s

C1 a r i t y B e f o r • e;

Clarity Afters

M


Textures MEDIUM

Artifactss

FORM I 7 / 8 8

300503


INORGAhllC ANALYSIS DATA SHEET SAMPLE ID

• I I i

I DW9 I Names CEIMIC Contracts ANSON 1 1

-...ata Codes CEIMIC Case No.s ANSON SAS No.s SDG No-s CATCH__BA

Tutrix (soil/water)s SOIL Lata Sample IDs 00006-068

Level (low/med )s LOW Date Received s 01./07/92

76 „ 7 bolIds s

Concentration Units (ug./L or mg/Kg dry weight) s MG/KG

CAS No.

7429-7440 7440 7440 7440 7440 7440 7440 7440 7440 7439 7439 7439 7439 7439' 7440 7440 7782 7440' 7440 7440' 7440 7440

90-5 -36-0 -38-2 -39-3 -41-7 -43-9 -70-2 -47-3 -48-4 -50-8 -89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 -49-2 -22-4 -23-5 -28-0

—66-6

C - i l o r B e f o r e s BROWN

C o l o r A f t e r s YELLOW

( »mmo>?n t s s

Analyte

Aluminum Antimony Arsenic Barium Eie ry 11 i um Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyan i do?

Con cen tration

0.12

2.20

C

*•"

U

Ll

Q M


Clarity Before;

Clarity Afters

Textures MEDIUM

Artifactss

FORi'i I - :I:N

30050*

TOTAL. METALS &. C Y A N I D E

>AMF'LE I D INORGANIC ANALYSIS DATA SHEET

. # . "BO 104

Contracts ANSON I._ 1

Case No. s ANSON SAS hlo - s SDG No. s CATCH._BA

Lata Sample IDs 00006-1IS

Date Receiveds 01/07/92

L^WF Names CEIMIC

Cab Codes CEIMIC

I Atrix (soil/water)s WATER

l._evel (low/med )s LOW

: Sol idss 0.0

Concentration Units (ug/L_ or mg/Kg dry weight) s UG/L

CAS No.

7429 7440 7440 7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-

-90-5 -36-0 -38-2 -39-3 -41-7 -43-9 -70-2 -47--48--50-8 -89-6 -92--95--96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 A O — O

6 6 - 6

-4

-1 -4

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury N i c l--.e 1 F'otassium Selenium Silver Sodium Thallium Vanadium 2!i nc Cyan i do?

Con co?n t r a t i on

84. 49.

r ^ J i - ,

3 . 4. 4.

6. 9.

13. 37. 1.

41., A. . K

0. 10.

290. 3, 9.

70. 1. 6. 5.

10,

on

00 00 00 00 00 00 00 00 00 00 00 00 00 00 20 00 00 00 00 00 00 00 00 00

1

CI 1

ui UI UI UI BI Ul UI UI Ul BI UI UI UI Ul UI Bl UI Ul Bl UI Ul Ul Ul Ul

1

r Jlor Befores YELLOW

Co1o r Af te r s COLORLESS

( )mmen ts s

Clarity Befores CLEAR

Clarity Afters CLEIAR

Q M

F' F F' P P F' P P P F' F F' F' CV P P F P F'

C

T e x t u r o ? s

A r t i f a c t s ;

FORM I I h-l

14 300505'

TOTAL MEIALS & CYAhllDE


SAMPLE ID

I l~B0105 I Names CEIMIC Contracts ANSON I I

_ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA

'"'atrix (soil/water) s WATER Lab Sample IDs 00006-128

Level (low/med)s LOW Date Receiveds 01/07/92

Sol idss 0.0

Con CErnt trati on Un i ts (ug/L or mg/Kg d r y wei g ht) s UG/L

CAS No.

7429^' 7440-7440-7440-7440-7440^ 7440-7440-7440-7440-7439-7439-7439-7439-7439-7440^ 7440-7782-7440-7440-7440-7440-7440-— .............

-90--36--38--39--41--43-• • " / O -

-47--48--50--89--92--95--96--97--02--09--49" -22--23--28--62--66-" "" "" "

-'•5 -0 „ r y

A-

-3 -7 -9

J i . ,

-3 -4 -8 -6 -1 -4 -5 -6 •0 •7 I

A., 1

•4 I -5 -0 ' " .C.

-6 " • " ' " • "

Analyte

Aluminum Antimony Arsenic Barium Bt?ryllium Cadmium Calcium Chromium Cotaalt Copper I ron Lead Magnesium Manganese Mo? r cury Nickel F'otassium So? 1 en ium Silvo?r Sodium Thallium Vanadium Z .1. n c Cyanide

Con co?n t r a t i on

84.00 49.00 2.00 3.00 4.00 4.00

7-,6 „ 0 0 9.00 9-00 6-00

220-00 1 „ 00

41.00 8.00 0.20 10.00

290-00 3.00 3.00

84.00 1.00 6 „ 00 5.00

10.00

1

CI Q 1 I

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1

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I , 1 , ,,. , „,,

M

P F' F P F' P F' F' P P P F F' F-CV P P F F' P F F' P C

f'olor Befores YELLOW

color Afters COLORLESS

ommo?i"i ts s

Clarity Befores CI...EAR

Clarity Afters CLEAR

Textures

Artifactss

•ORM I I hi 7 /88

15 300506

TOTAL METALS & CYANIDE

(Names CEIMIC

i.ab Codes CEIMIC


Contracts ANSON

Case No„s ANSON SAS No„s

^.MPLE ID

IBllO

SDG No -s CATCH BA

atrix (soil./wato?r) s SOIL,

.evel (low/med)s LOW

Solidss 99.0

\» v.. 1 1 \ , t CV \. .1. V^ • 1 V

1

;CAS No. 1

17429~90~5~ I 7440-36-0 17440-38-2 I 7440-39-3 17440-41-7 17440-43-9 17440-70-2 I 7440-47-3 I 7440-48-4 17440-50-8 I 7439-89-6 17439-92-1 17439-95-4 17439-96-5 17439-97-6 17440-02-0 17440-09-7 I 7782-49-2 17440-22-4 17440-23-5 17440-28-0 17440-62-2 17440-66-6

1 1

^ 1 1 .1. v. i.f \, V,\ \J ^ 1

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Me r cu ry Nickel Potassium Selenium Silvo?r Sodium Thallium Vanadium Zinc Cyanide

v./ I "*V.< ' ' ^ y ^ » * / *"»V.. a. U| 1 1 ^ / M

Con cen t ra t i on ,' C ,' Q

l6io7oo1~1 9„601UI 1. 50 I B I 7-30IBI 0 - 78 IB1 1 - 201 1

911-00 IB 1 11.601 I N* 1 - 80 IUI 4 - 301B1

5640.00 1 I 2.001 I

285.00 IBI 66-901 1 0-lOIUI 2-40 IB I

163-00 IB I 0 - 48 IUI 0„981BI

174.001B1 0.16IU1 8.001B1 7.601 I 1.201UI

I \ \ . * e

n I

p~l F' I F I F" I P I F- 1 P I F- I F' I F' I P I F I P I F- I CVI p : p 1 F 1 p 1 p 1 F I F' I P 1 C I

Lab Sample IDs 00006-078


MG/KG

r-"-)lor Before s BROWN

Color Afters YELLOW

:)mmo?n ts s

Clarity E<eforo?;

Clarity Afters

Textures MEDIUM

Artifactss

m •ORM I IN 7 / 8 8

16 300507

TOTAL METALS .?,; CYANIDE


IB115 Names CEIMIC Contracts ANSON 1

rab Codes CEIMIC Case No.s ANSON SAS No-s SDG No-s CATCH_E<A


..evel (1 ow./m(:?d) 3 LOW Date F«;eceiveds 01/07/92

Sol idss 97-4


CAS No.

7'429-90-5"" 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-B 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 „_.„.„ — ».„..-_„...

Analyte

Aluminum An timony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide

Con cen t ra t i on

liooToo 8.10 1.90 6.50 0-50 0.83

160.00 4.50 1.50 2.80

5350.00 1.20

243.00 54.30 0.09 2.50

198.00 0.57 0.50

164.00 0.19 3.30 6-50 1 „ 90

CI Q

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BI I N*

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iTolor Afters YELLOW

:)mmentss

Clarity Bo?fore:

Clarity Afters

Textures COARSE

Artifactss

w •ORM I IN

300508


SAMPLE ID INORGANIC ANALYSIS DATA SHEET

IB210 Names CEIMIC

--ab Codes CEIMIC

Contracts ANSON

Case No-s ANSON SAS No. SDG No-s CATCH BA

atrix (soil/water): SOIL

Level (low./mo?d)s LOW

Lab Sample IDs 00006-09S


Solids 98-4

Concentration Units (ug/L or mg/Kg dry weight): MG/KG

1 1

ICAS No-1 ' ,...•.... ,1

I 7429-90-5 17440-36-0 17440-38-2 I 7440-39-3 17440-41-7 17440-43-9 I 7440-70-2 I 7440-47-3 ;7440-48-4 1 7440-50-8 I 7439-89-6 1-7439-92-1 • 174,39-95-4 ' 17439-96-5 17439-97-6 I 17440-02-0 17440-09-7 I I 7782-49-2 17440-22-4 I 17440-23-5 17440-28-0 I 17440-62-2 17440-66-6 , ' ....,,

* . » . M . . « » . . ~ _ . » - _ « . '

Analyte

Aluminum Antimony Arsenic E<ar ium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury , Nickel Potassium I Selenium Silver Sodium Thallium I Vanadium Zinc Cyanide ,

Concentration _______

9.30 1.00 6.50 0.76 0-76

134-00 5-30 1-70 2.80

4300.00 2.30

305.00 53-00 0-09 2-50

207.00 0.54 0.57

132-00 0-18 3.40 8-70 1-30

CI Q

Ul Bl BI Bl Ul BI 1 N*

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Bl

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"^olor Before s BROWN

"Color Afters YELLOW

omments s

C l a r i t y E<eforo?;

C l a r i t y A f t e r s

Textures COARSE

Artifactss

m FORM IH

300509



SAMF'LE ID

IB215 Contracts ANSON

Case No. s ANSOhl SAS No. s

^amB^ CEIMIC

:;:.;ab Codes CEIMIC

atriX (soi1/water)s SOIL

Level (Iow./med)s LOW

Solidss 97.2

Concentration Units (ug/L or mg/Kg dry weight): MG/KG

SDG No.s CATCH_BA

Lata Sample IDs 00006-108


CAS No,

7429 7440 7440-7440 7440-7440 7440-7440^ 7440^ 7440^ 7439^ 7439-7439-7439^ 7439-7440-7440-7782-7440-7440-7440-7440-7440-

90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 92-1 95-4 96-5 -97-6 02-0 09-7 49-2 22-4 23-5 28-0

J C J i -

66—6

^olor Before?s E<ROWN

color Afters YELLOW

ommentss

Analyte

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium S :L 1 ve r Sodium Thallium Vanadium Z i n c Cyan i do?

Concentration

784. 9. 0. 3. 0. 0.

34 . A.. I

1 . A.. I

?950. 1 .

1 4 8 .

0. * A ^ m

9 1 . 0 . 0.

84 . 0 . A. . II

6 . 1 .

on

00 60 89 10 78 78 10 90 80 70 00 30 00 20 09 00 50 56 59 10 19 40 30 90

CI

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UI BI

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Ul

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C1 a r i t y Bo?fo r e s

C l a r i t y A f ' t e r s

M

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F' F F' P P P P P P P F F' P CV F' F' F P F' F F' F-C

Textures

Artifacts

COARSE

m FORM I - I hi 7 /88

19 300510

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