quantitative characterization of the pore network of a macroporous soil using µ x-ray ct sofie...

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Quantitative characterization of the pore network of a macroporous soil using µ X-ray CT Sofie Herman, department of Land Management, K.U. Leuven [email protected]

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Quantitative characterization of the pore network of a macroporous soil using µ X-ray CT

Sofie Herman, department of Land Management, K.U.

[email protected]

Introduction Geometry of pore space: understand

water flowRichards’ eq and effective hydraulic

properties Macropores (cracks, root channels,…)

Preferential flowPore network models

Need to quantify soil structure and pore network of a macroporous soil

General research outline

Hydraulic characterization

K(), h()

Characterization of porous structure and derivation of macropore network

Simulation of flow (and transport) in a pore scale model

Comparison between measured and simulated variables

sandy loam macroporous

soil

K(), h()

Field and laboratory methods: e.g. multistep outflow method, tensio-infiltrometer measurements

µCT and image analysis

Interaction between different flow domains

Microfocus X-ray CT Sample: 5 cm diameter, 5 cm

height Scan parameters:

135 kV and 0.1 mA Cu-filter (0.82 mm) to reduce beam-

hardening Resolution:

0.1 mm 0

10

20

30

40

50

60

70

-30 -20 -10 0 10 20 30distance from CR (mm)

att

. co

eff

. µ

(m

-1)

sand with Cu fi lter (0.82 mm)

sand without fi lter

Determination and characterization of the pore network Macropores-matrix

separation by binarization

Macropore volume: 10 %

Pore size distribution and connectivity function by means of mathematical morphology

Pore size distribution Opening of the image with spheres

of increasing diameter Opening: erosion followed by

dilation

Original image Erosion of the original image

Dilation of the eroded image:Smaller parts removedStruct. Elem.

0. 11 0. 57 1. 02 1. 47 1. 92 2. 37 2. 83 3. 28 3. 73 4. 18

pore diameter (mm)

0

0. 1

0. 2

0. 3

% o

f m

acro

pore

s (-

)

Pore size distribution Result: cumulative PSD, pore size

classes depend on pixel size

D>0.11mm D>1.02 mm

D>3.5 mmD>2.83 mmD>1.92 mm

Connectivity function Connectivity: Euler-

Poincaré-characteristic:

N: number of isolated componentsC: total number of redundant connectionsH: number of holes

as a function of the pore size class

0. 34 0. 79 1. 24 1. 70 2. 15 2. 60 3. 05 3. 50 3. 96

pore diameter (mm)

0

0. 01

0. 02

0. 03

0. 04

V (

-) V

HCNEV

Determination of soil hydraulic properties Generation of a pore network with the

same pore size distribution and connectivity function by the Topnet model (Vogel, 1998)

Drainage is simulated (initial state: saturation) by applying pressure steps that correspond to a given pore size (Young-Laplace) within the model.

Water retention and hydraulic conductivity curves are estimated under drainage

Pore network generated by the Topnet model based on the PSD and connectivity data

Pores drained at P=-2cm

- 1 0 1 2 3pF

0

0. 1

0. 2

0. 3

0. 4

0. 5

wat

er c

onte

nt (

cm3

cm-3

)

T opnet model

f it T opnet t o VG eq

- 1 0 1 2 3pF

- 10

- 8

- 6

- 4

- 2

0

2

log

K (

cmhr

-1

)f it t o VG- M ualem eq

T opnet model

Face-centered cubic gridCylindrical pores with fixed radius r

Distribution of water content

calculated=0.27 cm3cm-3 <-> measured=0.32 cm3cm-3

-

=µwater

µwe

t

µdr

y

highlow

Moisture content

Swelling/shrinking Variable aperture of macropores

depending on the degree of saturation

dry wet

0 1 2 3

length (mm)

10

20

30

40

50

atte

nuat

ion

coef

fici

ent

(m-

1)

dry(m- 1)

wet(m- 1)

FWHMdry=0.48mm

FWHMwet=0.33mm

Conclusions The macropore network was characterized

quantitatively in terms of the pore size distribution and connectivity by µCT

Effective hydraulic properties were estimated from a static pore network model

µCT offers the potential to visualize dynamic phenomena that occur during wetting/drying cycles such as shrinking and swelling of pores

Future objectives Describe and measure swelling of

pores as a function of moisture content

Simulate drainage/imbibition of soil by a dynamic model

Incorporate swelling into the model