p're design report · inc., an o'brien & gere limited company h b u ^ ' ^ 5000...
TRANSCRIPT
P're Design Report
S R O O I 9 I 7
PREDESIGN REPORT
BLOSENSKI LANDFILLCHESTER COUNTY, PENNSYLVANIA
APPENDIX 5-1
QBRiEN 5 GE
September 25, 1990
Mr. Lewis LuchieRegional Water Quality ManagerPennsylvania Department of Environmental Resources1875 New Hope StreetNorristown, PA 19401
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County
File: 3277.001
Dear Mr. Luchie:
Enclosed are three copies of an "Application for Discharge of Groundwater to Surface Waters ofthe State of Pennsylvania" pertaining to an aquifer performance test to be conducted at the abovereferenced site. By this application, notification is provided of intent to conduct this testing fromOctober 16, 1990 to October 18, 1990.
Aquifer performance testing will be limited to one 56-hour period and will involve less than 135,000gallons of groundwater pumped from one test well. The groundwater may contain low ppm levelsof VOCs. Groundwater pumped during the aquifer performance test will be treated through an airstripper. Air stripper offgas will be treated by activated carbon adsorption. The maximumprojected release of VOCs to an unnamed, intermittent tributary of Indian Spring Run is expectedto be less than 5 pounds.
The on-site temporary groundwater treatment system will be supplied and operated by OBGTechnical Services, Inc., a subcontractor to O'Brien and Gere Engineers, Inc. O'Brien and GereEngineers has contracted with the U.S. Army Corps of Engineers to prepare pre-design documentsto be used for design of the site cleanup. Our scope of services for this project includes conductingthis short-term on-site testing to support the preliminary design of ground water recovery andtreatment facilities.
O'Brien & Gere Engineers, Inc., an O'Brien & Gere Limited Company"""00 3'ittonfieid Parkway / PO Box '—" -... -
anc offices in major U.S. cities
« «,,«.. v*. >^wii> i_iiv^tii\,^t^, iiiw., aii w uiiidi m V^K^IC i_nimeu wurnuany5000 Bnnonfield Parkway / PO Box 4873 / Syracuse. NV 13221 7(315) 437-6100 FAX (315) 4 3- 5 ^ I Q i Q
Mr. Lewis LuchieSeptember 25, 1990Page -2-
Please contact me or John LaManche at (315) 437-6100 with any questions or comments.
Very truly yours,
O'BRIEN & GERE ENGINEERS, INC.
J. Kevin Farmer,Managing Engineer
cc: John J. Keegan, O'Brien and Gere Engineers, Inc.John J. LaManche, O'Brien and Gere Engineers, Inc.Geoffrey J. Seibel, O'Brien and Gere Engineers, Inc.James A. Fox, OBG Technical Services, Inc.
BROOI920
9/25/90APPLICATION FOR DISCHARGE pp OROT7NDWATFP
TO SURFACE WATERS OF THE STATF pF
Name of Discharge Location: Blosenski Landfill Superfund Site
Location: West Cain Township, Chester County, Pennsylvania (40°0ri2" N, 75°54'33"W)
Description of Discharge: Treated groundwater discharge from 8 hour well drawdown test and 48hour aquifer pump test.
Operator of Discharge: OBG Technical Services, Inc., Syracuse, NY 13221
Location of Discharge Source: Test well located on the Blosenski Landfill Site (see enclosed figure).
Anticipated Date(s) of Discharge: October 16-18, 1990 (56 hours duration)
Receiving Water: Intermittent unnamed tributary of Indian Spring Run located 500 feet north ofthe site.
Anticipated Quality of Discharge Source (untreated): See Table 1 for anticipated characteristics.
Anticipated Quality of Discharge Source (treated): See Table 2 for anticipated characteristics.
Anticipated Quantity of Discharge: 33,600 gallons - 134,400 gallons (10-40 gpm; 56 hours)
Treatment Technologies for Groundwater: Air stripping and vapor phase carbon adsorption.
SROOI92I
9/25/90
TABLE 1
BLOSENSKI LANDFILL SUPERFUND SITERAW GROUNDWATER CHARACTERISTICS
Substance Maximum Concentration fug/LV*
Benzene 11,000Toluene 600Ethylbenzene 54Total Xylenes 78Chlorofaenzene 341,1,1-Trichloroethane 4301,2-Dichloroethane 741,1-Dichloroethane 270Chloroethane 93Tetrachloroethane 5Trichloroethene 2601,2-Dichloroethene 8901,1-Dichloroethene 21Vinyl Chloride 450Chloroform 270Methylene Chloride 2,000Acetone 43,0002-Butanone 3502-Hexanone 214-Methyl-2-pentanone 7
* Maximum concentration taken from Table 1.0 of the September 29, 1986 United States EPASuperfund Record of Decision: Blosenski Landfill, PA (EPA/ROD/R03-86/029). These data weredeveloped from samples collected in late 1984 and early 1985 during the Remedial Investigation.The total mass of these substances in the untreated influent should not exceed 60 pounds and islikely to be considerably less.
ftROOI922
•
9/25/90TABLE 2
BLOSENSKI LANDFILL SUPERFUND SUEANTICIPATED TREATED GROUNDWATER CHARACTERISTICS*
Substance Maximum Concentration (usfL) **BenzeneTolueneEthylbenzeneTotal Xylenes <50Chlorobenzene <51,1,1-Trichloroethane <501,2-Dichloroethane <501,1-Dichloroethane <50Chloroethane <50TetrachloroethaneTrichloroethene1,2-Dichloroethene1,1-DichloroetheneVinyl ChlorideChloroformMethylene Chloride
<°-Butanone2-Hexanone4-Methyl-2-pentanone
* Treatment to consist of air stripping and vapor phase carbon adsorption.
fTabS'Tt?0 56 ?ncentf ions derived ed on maximum influent concentrations{.lame 1), stopping column characteristics, air and wafpr fl™, ,* u- ^ T
flROOI923
DIRECT LINE NO. (315) 463-7554
QBRHEN 5 GERE
DATE: IQ/-2.4
NUMBER OF PAGES BEING SENT 3 (INCLUDING THIS ONE).
TO: ___
COMPANY
TELEPHONE ) 27C -
F ROM: KeJ /AS/
MESSAGE:
fafc THC
•5>i6-4r37 -<*V
IF YOU DO NOT RECEIVE ANY OF THESE PAGES PLEASE CONTACTTHE TELECOPY OPERATOR AT {315} 437-1990 EXTENS10N1593 ASSOON AS POSSIBLE.
THANK YOU
TRANSMISSION COMPLETED AND CONFIRMED
DATE ____________ TIME _____SIGNATURE
O'Brien & Gv Engineers. Inc., an O'Brien & Gere Limited Company H B U ' 5000 Brittorr.s.c Parkway / PO Box 4873 / Syracuse, NY 13221 / (315) 437-6100 FAX (315} 463-7554
October 23, 1990
Mr. Lewis LuchieRegional Water Quality ManagerPennsylvania Department of Environmental Resources1875 New Hope StreetNorristown, PA 19401
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County
File: 3277.001
Dear Mr. Luchie:
A letter to your department dated September 25, 1990 included three copies of an "Application forDischarge to Surface Waters of the State of Pennsylvania" pertaining to an aquifer performance testto be conducted at the above referenced site. Steve O'Neill of PADER has requested thatadditional information pertaining to the sampling of the air stripper influent and effluent aqueousstreams be provided. This letter contains the sampling plan approved by the U.S. Army Corps ofEngineers for the samples that will be collected during the aquifer performance test and indicatesthe analytical methods that will be used to conduct the analyses.
Samples will be collected from the air stripper influent and effluent aqueous streams for each ofeight air to liquid ratios to be investigated. These samples will be tested in the laboratory forvolatile organics by EPA Method 8010/8020. Air stripper influent and effluent aqueous sampleswill also be collected on two occasions and analyzed for pH, total suspended solids, chemical oxygendemand, biochemical oxygen demand, and total organic carbon. Air stripper influent and effluentaqueous samples will also be collected on one occasion and tested for priority pollutant metals,base/neutral/acid extractables (EPA Method 8270), pesticides/PCBs (EPA Method 8080), totalKjeldahl nitrogen, ammonia, oil and grease, phosphorus, chloride, sulfate, and total coliforms (EPAMethod 9131). The air stripper effluent aqueous stream from the stripper will also be analyzed onone additional occasion for base/neutral/acid extractables and pesticides/PCBs.
Aquifer pump testing is expected to commence on Tuesday, October 30,1990. It is anticipated thatthe samples will collected on October 30 and 31,1990 during daylight hours (7:00 a.m. to 7:00 p.m.).It is expected that two to four air stripper influent and effluent samples will be collected on October30 and four to six such samples will be collected on October 31.
O'Brien & Gere Engineers. Inc.. an O'Brien i Gere Limited Comoany " **5CCO Bm-onfieia Parkwav / FO Box-871 Sv~.c'_se. ',v ' 322' •": ~) -i^~-n".CZ
Mr. Lewis LuchieOctober 23, 1990Page -2-
The analytical results generated by the sampling plan described above should provide sufficient datato characterize this discharge to surface water. Please feel free to contact me or John LaMancheat (315) 437-6100 with any questions or comments.
Very truly yours,
O'BRIEN & GERE ENGINEERS, INC.
7f • .- N ->~__ ,^/&^^_,———————
J. Kevin Farmer, PJE.Managing Engineer
wp-4
cc: John J. Keegan, O'Brien & Gere Engineers, Inc.John J. LaManche, O'Brien & Gere Engineers, Inc.Geoffrey J. Seibel, O'Brien & Gere Engineers, Inc.James A. Fox, OBG Technical Services, Inc.
SROOI926
September 25, 1990
Mr. Thomas McGinleyEngineering Services ChiefPennsylvania Department of Environmental Resources1875 New Hope StreetNorristown, PA 19401
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County
File: 3277.001
Dear Mr. McGinley:
Enclosed are three copies of a completed "Request for Determination of Requirement for PlanApproval/Operating Permit Application" pertaining to an aquifer performance test to be conductedat the above referenced site. By this application, an exemption is sought from plan approval andpermitting requirements for this source pursuant to the authority contained in 25 PA Code Section127.14(8).
Aquifer performance testing will be limited to one 56-hour period and will involve less than 135,000gallons of groundwater pumped from one test well. This temporary on-site testing is planned tocommence October 16, 1990 and end October 18, 1990. The groundwater may contain low ppmlevels of VOCs. Groundwater pumped during the aquifer performance test will be treated throughan air stripper. Air stripper offgas will be treated by activated carbon adsorption. The maximumprojected release of air toxics is less than 50 pounds.
The on-site temporary groundwater treatment system will be supplied and operated by OBGTechnical Services, Inc., a subcontractor to O'Brien and Gere Engineers, Inc. O'Brien and GereEngineers has contracted with the U.S. Army Corps of Engineers to prepare pre-design documentsto be used for design of the site cleanup. Our scope of services includes conducting thic short-termon-site testing to support the preliminary design of ground water recovery and treatment facilities.
O'Brien & Gere Engineers, Inc., an O'Brien & Gere Limited Company fl[ R 0 0 « J £• '5000 Britionfield Parkway / PO Box 4873 / Syracuse, NY 13221 / (315) 437-6100 FAX (315} 463-755'4
ana offices in ma/or U.S. cities
Mr. Thomas McGinleySeptember 25, 1990Page -2-
Please contact me or John LaManche at (315) 437-6100 with any questions or comments.
Very truly yours,
O'BRIEN & GERE ENGINEERS, INC.
(_XJ. Kevin Farnfer, P.E.Managing Engineer
cc: John J. Keegan, O'Brien and Gere Engineers, Inc.John J. LaManche, O'Brien and Gere Engineers, Inc.Geoffrey J. Seibel, O'Brien and Gere Engineers, Inc.James A. Fox, OBG Technical Services, Inc.
flROOI928
_ --17 R«v. 9/83 -
COMMONWEALTH OF PENNSYLVANIADEPARTMENT OF ENVIRONMENTAL RESOURCES
BUREAU OF AIR OUAUTY CONTROL
Request for Determination of Requirementfor Plan Approval/Operating Permit Application
(Submit In Triplicate)Blosenski Landfill GroundwaterAir Stripper Offgas _ , . „ . Oct. 16-18 1990p- tf Source: _______11____-—————'— Date of Installation: 10> iy*uU.S. Army Corps of Engineers for
of Sourea: Joseph M.. Blosenski. Jr. Employer l.D. No.: _JLS_________%0'Brien & Gere Engineers, Inc., 5000 Brittonfield Pkwy, P.O. Box 4873,
lihng Address: Syracuse. NY 1322l ___________________________________.
D———. J. Kevin Farmer______ Telephone: ' f3151 437-6100______U'Brien § Gere Engineers, Inc.
cation of Sourcata):
Kings Highway Route 540 Municipality: West Cain Township
tt ,ted Emissions: County: Chester County
Pouutant
IH»W
Q ntrty•us/yr
VOCs
0.85
48
•
Vice'^President, O'Brien § Gere Engineers,TitleSeptember 25, 1990_______________Date
OFFICIAL USE ONLY
Received: .«——•«_«»_ ________ — — —— Reviewed 3y:
r««rttto tft« autnomv contained in 23 PA Code «1 27.1-W8) ttw TtwcoureaO) do«nat oua«V *w txtmonon from crf«n aacraval/oor-ureaisi is txamottd from tft« aian aoortvii and gt> nutting rw mttnng rvouifaRMMia undtr PA Cod* i 1 27. 1 4(8) and oi»n aoorovai
to. This d«tim»inanon do«s not ucwnot ttt* sources) from aooticaeortsi must b« sutentnd. Th« Otoarcmont is oranibttad fromm ne* with all otfl«r aaoiicafit* air quality ragtjJaoons. acting on an aooiieanon until 30. davs after m« muntaoaiitv and
county hav« recaiv«d noofieaoon by ttw comoany. ?wtin«r« formsan anaehtd.
Tin*
Oan flRQQ1929
,ton*u*a ww*~.—jr ow*.. .—.. ,-.-- - ............... _,,-_..„, ,, ,<at.~Ajdfy/t-
(Indude: procasa description, axhaust volume, stack data, schematic flow diagram, material data safaty sheet, steSee following sheets for Process description, etc.
OFFICIAL USE ONLY
Remarks:
SROOI930
9/25/90
AIR DISCHARGE PROCESS DESCRIPTION. ETC.
Name of Discharge Location: Blosenski Landfill Superfund Site
Location: West Cain Township, Chester County, Pennsylvania (40°01'12" N, 75"54'33"W)
Description of Discharge: Treated offgas discharge from air stripping of pumped groundwaterdeveloped during 8 hour well drawdown test and 48 hour aquifer pumptest.
Operator of Discharge: OBG Technical Services, Inc., Syracuse, NY 13221
Anticipated Date(s) of Discharge: October 16-18, 1990 (56 hours duration)
Anticipated Quality of Groundwater Source (untreated): See Table 1 for anticipated characteristics.
Anticipated Quality of Groundwater Source (treated): See Table 2 for anticipated characteristics.
Anticipated Quantity of Discharge: 333,600 cubic feet - 6,720,000 cubic feet (100-2000 cfhi; 56hours)
Treatment Technologies for Ain Vapor phase carbon adsorption.
flROOI93l
9/25/90
TABLE 1
BLOSENSKI LANDFILL STJPERFUND SITERAW GROUNDWATER CHARACTERISTICS
Substance Maximum Concentration fug/L)*
Benzene 11,000Toluene 600Ethylbenzene 54Total Xylenes 78Chlorobenzene 341,1,1-Trichloroethane 4301,2-Dichloroethane 741,1-Dichloroethane 270Chloroethane 93Tetrachloroethane 5Trichloroethene 2601,2-Dichloroethene 8901,1-Dichloroethene 21Vinyl Chloride 450Chloroform 270Methylene Chloride 2,000Acetone 43,0002-Butanone 3502-Hexanone 214-Methyl-2-pentanone 7
* Maximum concentration taken from Table 1.0 of the September 29, 1986 United States EPASuperfund Record of Decision: Blosenski Landfill, PA (EPA/ROD/R03-86/029). These data weredeveloped from samples collected in late 1984 and early 1985 during the Remedial Investigation.The total mass of these substances in the untreated influent should not exceed 60 pounds and islikely to be considerably less.
8ROQI932
9/25/90TABLE 2
BLOSENSKI LANDFILL SUPERFUND SITEANTICIPATED TREATED GROUNDWATER CHARACTERISTICS* '
Substance Maximum Concentration fap/r ) **
BenzeneToluene <50EthylbenzeneTotal Xylenes <50Chlorobenzene <51,1,1-Trichloroethane <501,2-Dichloroethane <501,1-Dichloroethane ,,..50Chloroethane <50Tetrachloroethane < Trichloroethene <501,2-Dichloroethene <501,1-Dichloroethene <5Vinyl Chloride <50Chloroform <50Methylene Chloride <50Acetone <50QO2-Butanone <3QO2-Hexanone < in4-Methyl-2-pentanone <5
* Treatment to consist of air stripping and vapor phase carbon adsorption.
** 5PecJed discharge concentrations derived based on maximum influent concentrations(T?5. P' sfriPPkg c011111111 characteristics, air and water flow rates, Henry's Law constantssolubilities, temperatures, and other pertinent physical characteristics. These estimate dischargeconcentrations are very conservative. Actual discharge concentrations are expected to beconsiderably lower than the values identified above.
flROOI933
COMMONWEALTH OF PENNSYLVANIADEPARTMENT OF ENVIRONMENTAL RESOURCES
E PENNSYLVANIA•••••HA 1875 New Hope StreetF fcr' —"* Norristown, PA 19401
215 270-1975I
October 29, 1990
I
I
I8
1I1
I
I
O'Brien and Gere Engineers, Inc.a 5000 Brittonfield ParkwayI P. 0. Box 4873
Syracuse, NY 13221
Attention: J. Kevin Farmer, P.E.Managing Engineer
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County
Dear Mr. Farmer:
This is in reply to your September 25, 1990 and October 23, 1990 letters andyour October 22, 1990 telephone conversation with Steve O'Neil of my staffregarding your request to conduct a 8-hour well drawdown test and a 48-houraquifer pump test with temporary discharge of approximately 134,400 gallons oftreated water to an unnamed tributary of Indian Spring Run located to the northof the site.
Verbal approval of this temporary discharge was granted during the October 22,1990 telephone conversation with the understanding that a sampling plan would besubmitted. Your October 23, 1990 submission of the sampling plan satisfied thiscondition. You are hereby authorized to commence with the pump test andtemporary discharge in accordance with the outlines provided in the abovereferenced letters and you are requested to submit a report on the findings uponcompletion of the pump test and receipt of all sampling analyses.
Very truly yours,
tx'
I LEWIS LUCHIE, JR. (Regional Water Quality Manager
cc: Mr. DanyliwWest Cain TownshipOperations SectionRe 30 (3) 299
- .-17 R«w. 9/8S
COMMONWEALTH OF PENNSYLVANIADEPARTMENT OF ENVIRONMENTAL RESOURCES
BUREAU OF AIR QUALITY CONTROL
Request for Determination of Requirementfor Plan Approval/Operating Permit Application
(Submit In Triplicate)Blosenski Landfill GroundwaterAir Stripper Off gas Oct 16-18Date of Installation: Uct' 16 18>U.S. Army Corps of Engineers for
ui • ai SmiPM. Joseph M. Blosensfc],, Jr, ftTin«««"«' «-O- No? MA
ifi at Parson; J, J£gvin Farmer .
ngineers, Inc., 5000 Brittonfield Pkwy, P.O. Box 4873,
Tfltonhnn«:O'Brien § Gere Engineers, Inc.
s. an of Sourcata):
rwr AHrirB,«. Kinps Highway Route 340 MnniHnaKtv
s itad Emissions:
s 'lutant VOCs
ifIbs/nr o.ss
Q rrtityIbs/yr 48
SEP 2 6 19903ta necflh/MJ;
uam torn* authority conuiiMd In 28 PA Cad«i12'urcaijj i* •xvmotad from tn« rtan aeeraval and p«rx* no. Th« detarmmanon de«« not wta*npttft« soumi no whn all atticr aeoiicaala .quality rtguiat
" - \Sv O\\ O-Vv^v ~ J*>C I1» ">i . . j
OCT1 5 1990
County:
Signature
Vice/W
f315) 437-6100
West Cain Township
Chester County
7 - • V - ext-,
' ' ' rsside^t, O'Brien S Gere Ena-ine^T
.Title September 25, 1990Date
OFFICIAL USE ONLY Request No. 15-A01-092
K ( \/IX ovKvV - ~~*\
M4(81tn« Tlwaaure sidOMnotaiiaifyfarnamption/ramoianaMco i BBf'mrttmg r»- timing njquiiwnwns under PA Cod* i127.1*<8J and sianaoarovaim<3) from aooteanonOJ must &• subnvtud. Th« Oaaanmant is orahibited fromion. •acting en an aoolieation untri 30. ctavs afTtf tn« muntooaiitv and
county have r*cnv«d noafieanon by tft* camganv. Pemn«nt farmsan attaencd.
, €^-~J — Sfmwiw
Q ."",f ' • •
.0«ra fl.ROO!935
Sourca Description (attach additional sriaattsi if necessary):ndude: procasa daacription, axhaust volume, stack data, schematic flow diagram, material data safety sheet, tie.)
See following sheets for Process description, etc.
ocr i«aw
OFFICIAL USE ONLY
PREDESIGN REPORT
BLOSENSKI LANDFILLCHESTER COUNTY, PENNSYLVANIA
APPENDIX 5-2
/IROOI937
January 2, 1991
Mr. Lewis Luchie, Jr.Regional Water Quality ManagerPennsylvania Department ofEnvironmental Conservation1875 New Hope StreetNorristown, PA 19401
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County, PA
File: 3277.001
Dear Mr. Luchie:
An "Application for Discharge of Groundwater to Surface Waters of the State ofPennsylvania" was completed and forwarded to your office on September 25,1990 pertainingto an aquifer performance test to be performed at the Blosenski Landfill Superfund Site.Verbal approval of the temporary discharge of groundwater to surface waters was relayedby Steve O'Neil of your staff with the stipulation that a sampling plan for the test besubmitted to your department. The submission of the sampling plan was completed onOctober 23, 1990, and written approval by your department was granted on October 29,1990 (Attachment A). This letter serves as the report required to be submitted to yourdepartment following completion of the aquifer performance test and receipt of all samplinganalyses.
The aquifer performance test was conducted at the Blosenski Landfill Superfund Site fromNovember 7, 1990 to November 9, 1990. Groundwater pumped to the surface during theaquifer performance test was treated and then discharged to surface waters of the State of
flROGI938
Mr. Lewis Luchie, Jr.January 2, 1991Page 2
Pennsylvania (unnamed tributary of Indian Spring Run). The groundwater pumped duringthe aquifer performance test was treated through an air stripper, with air stripper offgastreatment by activated carbon adsorption. The gas to liquid ratios (G:L, dimensionless)utilized by the air stripper and associated durations were (in chronological order):
G:L Activity Operational Duration134:1 Well Development 1 hour447:1 Well Drawdown 0.5 hours224:1 Well Drawdown 1.5 hours157:1 Well Drawdown 2.7 hours147:1 Performance Test 1.5 hour128:1 Performance Test 1.5 hours119:1 Performance Test 1.5 hours108:1 Performance Test 1.25 hours101:1 Performance Test 1.5 hours89:1 Performance Test 2 hours68:1 Performance Test 1.25 hours52:1 Performance Test 1.5 hours147:1 Performance Test 36 hours
53.7 hours
For the development of the well, the volumetric air flowrate was set at the maximumachievable by the blower (628 cfrn) and the groundwater flowrate was constant (35 gpm).During the well drawdown test, the volumetric air flowrate was set at the maximumachievable by the blower (628 cfm), and the groundwater flowrate was manipulated by thehydrogeologists. During the air stripping pilot test portion of the 48-hour performance test,the groundwater flowrate was not adjusted, and the volumetric air flowrate was varied. Forthe remainder of the 48-hour performance test, the volumetric air flowrate was set at themaximum achievable by the blower (628 cfm). A total of 89,971 gallons of ground waterwas discharged during the well development, drawdown and aquifer performance test.
Attachment B contains the analytical schedule followed during the testing. EnvironmentalHealth Research and Testing, Inc. of Cincinnati, Ohio provided the analytical services.Volatile organics analyses (EPA Method 601/602) were completed for aqueous influent andeffluent samples at all air to liquid ratios utilized during the aquifer performance test.
flROO!939
Mr. Lewis Luchie, Jr.January 2, 1991Page 3
Semi-volatile organics (EPA Method 625), PCB/pesticide (EPA Method 608), and indicatorparameter analyses were also completed during the course of the testing.
Attachment C contains a summary of detectable volatile organics in the aqueous influentand effluent samples. The average benzene concentration in the effluent aqueous streamfrom the air stripper was approximately 0.083 rng/L. The average effluent concentrationsfor each of the remaining volatile organics detected in the influent aqueous stream were lessthan 0.011 mg/L.
Indicator parameter analyses were completed and are summarized in Attachment D. Allpriority pollutant metals concentrations were below respective analytical method detectionlimits. All semi-volatile organics (EPA Method 625), and PCB/pesticide (EPA Method 608)concentrations were also below respective analytical method detection limits. AttachmentE contains copies of the analytical reports for the priority pollutant metals, semivolatiles andPCB/pesticide analyses.
The aquifer performance test was successful. The temporary treatment system was highlyeffective in transferring volatile organics to the air from the ground water. This air wassubsequently treated by activated carbon prior to discharge.
Please call me or John LaManche at (315) 437-6100 with any questions or comments.
Very truly yours,
O'BRIEN & GERE ENGINEERS, INC.
ys •-••' ••- V r-t^ ' *^
J. Kevin Farmer, P.E.Managing Engineer
cc: John J. Keegan, O'Brien & Gere Engineers, Inc.John J. LaManche, O'Brien & Gere Engineers, Inc.Geoffrey J. Seibel, O'Brien & Gere Engineers, Inc.
ATTACHMENT A
AROOI9IH
COMMONWEALTH OF PENNSYLVANIADEPARTMENT OF ENVIRONMENTAL RESOURCES
1875 New Hope StreetNorristown, PA 19401
215 270-1975
October 29, 1990
O'Brien and Gere Engineers, Inc.5000 Brittonfield ParkwayP. 0. Box 4873Syracuse, NY 13221
Attention: J. Kevin Farmer, P.E.Managing Engineer
Re: Blosenski Landfill Superfund SiteWest Cain TownshipChester County
Dear Mr. Farmer:
o , Lre?i7 ?So£ m. **£**** 25, 1990 and October 23, 1990 letters andyour October 22, 1990 telephone conversation with Steve O'Neil of my staffregarding your request to conduct a 8-hour well drawdown test and a 48-houraquifer pump test with temporary discharge of approximately 134,400 gallons oftreated water to an unnamed tributary of Indian Spring Run located to the northor the site.
°f thlS ^ discharge was granted during the October 22,6 "S1! Sn "standing that a sampling plan would beYour October 23, 1 990 submission of the samplingllan satisfied this
condition. You are hereby authorized to commence with the pump test andtemporary discharge in accordance with the outlines provided in the above
f tfS and 70U arV«fl«st:ed to submit a report on the findings uponcompletion of the pump test and receipt of all sampling analyses.
Very truly yours,
LEWIS LUCHIE, JR.Regional Water Quality Manager
cc: Mr. DanyliwWest Cain TownshipOperations SectionRe 30 (3) 299
ATTACHMENT B 12/21/90
BLOSENSKI LANDFILL SUPERFUND SITEWEST CALN, PENNSYLVANIA
AIR STRIPPER PILOT TEST ANALYTICAL PROGRAM
SAMPLES COLLECTED 11/7/90 - 11/9/90
G:L SAMPLE ANALYSESRATIO ID*
=====================r=================s==r===============s==============
AS-I-150 |EPA 601,602,625,608,Priority Pollutant Metals,TSS,BOD5,JTOC,COD,TKN,NH3,O&G,Phosphorus,Chloride,Sulfate
AS-E-150 JEPA 601,602,625,608,Priority Pollutant Metals,TSS,BOD5,jTOC,COD,TKN,NH3,O&G,Phosphorus,ChIoride,SuI fate
AS-I-1500 JEPA 601,602AS-E-150D JEPA 601,602AS-I-130 JEPA 601,602AS-E-130 jEPA 601,602AS-I-120 JEPA 601,602AS-E-120 JEPA 601,602,625,608,Priority Pollutant MetalsAS-E-120D JEPA 601,602AS-I-100 JEPA 601,602AS-E-100 JEPA 601,602AS-I-90 JEPA 601,602AS-E-90 JEPA 601,602AS-I-80 JEPA 601,602,TSS,BODS,TOC,CODAS-E-80 JEPA 601,602,TSS,8005,TOC,CODAS-I-60 JEPA 601,602AS-E-60 JEPA 601,602AS-I-50 |EPA 601,602AS-E-50 JEPA 601,602
147:1
147:1
147:1147:1128:1128:1119:1119:1119:1108:1108:1101:1101:189:189:168:168:152:152:1
AS-I,E - Number Letter
~ ' t * \Air Influent or G:L D - DuplicateStripper Effluent
ARQGI91+3
ATTACHMENT C 12/21/90BLOSENSKI LANDFILL SUPERFUND SITE
AIR STRIPPING PILOT TESTSELECTED VOLATILE ORGANICS ANALYTICAL RESULTS
SAMPLES COLLECTED 11/7/90 - 11/9/90
WATER WATER WATER WATERG:L PARAMETER INFLUENT INFLUENT EFFLUENT EFFLUENTRATIO DUPLICATE DUPLICATE
=—ssssss sssssssssssssssssssssssssssssrsssssssssssssssssssssssssasug/L ug/L ug/L ug/L
147:1 Carbon Tetrachloride 0.50 * 19.76 0.50 * 0.50 *Chlorobenzene 17.35 17.55 1.86 1.55Chloroethane 7.04 7.53 0.50 * 0.5 *Chloroform 128.59 132.27 11.70 10.351,1-DiChloroethane 47.83 49.82 3.21 2.901,2-Dichloroethane 0.50 * 0.84 0.50 * 0.50 *1,1-Dichloroethene 14.02 14.89 0.50 * 0.50 *trans-1,2-Dichloroethene 130.81 \ 137.03 9.81 9.30Tetrachloroethene 1.27 1.29 0.50 * 0.50 *1,1,1-Trichloroethane 112.91 117.48 6.33 7.18Trichloroethene 56.83 59.00 3.00 4.98Vinyl Chloride 12.54 13.79 0.50 * 0.50 *Benzene 1022.00 1290.00 81.67 80.85
128:1 Carbon Tetrachloride 0.50 * - 0.50 *Chlorobenzene 17.42 - 1.44Chloroethane 8.20 - 0.50Chloroform 114.97 - 8.201,1-Dichloroethane 45.15 - 2.301,2-Dichloroethane 0.50 * - 0.50 *1,1-Dichloroethene 11.83 - 0.50 *trans-1,2-Dichloroethene 126.78 - 7.55Tetrachloroethene 1.04 - 0.50 *1,1,1-Trichloroethane 104.93 - 4.62Trichloroethene 51.34 - 2.64Vinyl Chloride 13.99 - 0.50 *Benzene 1320.00 - 60.75
119:1 Carbon Tetrachloride 0.50 * - 0.50 * 0.50 *Chlorobenzene 17.43 - 1.60 1.64Chloroethane 0.50 * - 0.50 * 0.50 *Chloroform 100.27 - 8.11 8.121,1-OiChloroethane 39.82 - 2.32 2.331,2-Dichloroethane 0.50 * - 0.50 * 0.50 *1,1-Dichloroethene 9.35 - 0.50 * 0.50 *trans-1,2-Dichloroethene 109.97 - 7.64 7.45Tetrachloroethene 1.28 - 0.50 * 0.50 *1,1,1-Trichloroethane 98.22 - 4.91 5.50Trichloroethene 49.55 - 0.50 * 0.50 *Vinyl Chloride 10.61 - 0.50 * 0.50 *Benzene 1294.00 - 65.71 68.33
108:1 Carbon Tetrachloride 0.50 * - 0.50 *Chlorobenzene 16.35 - 1.87Chloroethane 0.50 - 0.5 *•Chloroform .. 86.63 - 9.881,1-Dichloroethane 32.25 - 3.131,2-Dichloroethane 0.50 * - 0.50 *1,1-Dichloroethene 6.40 - 0.50 *trans-1,2-Dichloroethene 93.19 - 10.22Tetrachloroethene 0.5 * - 0.50 *1,1,1-Trichloroethane 86.58 - 5.41Trichloroethene 47.69 - 0.50 *Vinyl Chloride 0.50 * - 0.50 *Benzene 1261.00 - 74.08
* - less than
flROOI9l*l*
ATTACHMENT C 12/21/90BLOSENSKI LANDFILL SUPERFUND SITE
AIR STRIPPING PILOT TESTSELECTED VOLATILE ORGANICS ANALYTICAL RESULTS
SAMPLES COLLECTED 11/7/90 - 11/9/90
WATER WATER WATER WATERG:L PARAMETER INFLUENT INFLUENT EFFLUENT EFFLUENTRATIO DUPLICATE DUPLICATE
ug/L ug/L ug/L ug/L==SS333S=S3S3SS33SS3S3=S==3333=S33333S=33S3S3S333S3333333333=3333333=S3333S33333:!
101:1 Carbon Tetrachloride 5.00 * - 0.50 *Chlorobenzene 17.20 - 1.96Chloroethane 5.00 * - 0.5 *Chloroform 98.10 - 9.621,1-Dichloroethane 37.40 - 3.121,2-Dichloroethane 5.00 * - 0.50 *1,1-Dichloroethene 9.50 - 0.50 *trans-1,2-Dichloroethene 110.20 - 9.74Tetrachloroethene 5.00 * - 0.50 *1,1,1-Trichloroethane 131.40 • 6.13Trichloroethene 55.50 - 3.11Vinyl Chloride 5.00 * - 0.50Benzene 1201.10 - 81.50
89:1 Carbon Tetrachloride 5.00 * - 0.50 *Chlorobenzene 17.20 - 2.43Chloroethane 5.00* - 0.50Chloroform 95.20 - 12.061,1-Dichloroethane 36.20 - 3.631,2-Dichloroethane 5.00 * - 0.50 *1,1-Dichloroethene 5.00 * - 0.50 *trans-1,2-Dichloroethene 106.60 - 12.22Tetrachloroethene 5.00 * - 0.501,1,1-Trichloroethane 124.30 - 6.29Trichloroethene 59.10 - 3.63Vinyl Chloride 5.00 * - 0.50 *Benzene 1267.80 - 94.53
68:1 Carbon Tetrachloride 5.00 * - 0.50 *Chlorobenzene 22.10 - 2.94Chloroethane 5.00 * - 0.50 *Chloroform 96.60 -. 17.051,1-Dichloroethane 34.10 - 5.041,2-Dichloroethane 5.00 * - 0.50 *1,1-Dichloroethene 5.00 * - 0.50 *trans-1,2-Dichloroethene 103.70 - 18.00Tetrachloroethene 5.00 * - 0.50 *1,1,1-Trichloroethane 135.90 - 7.15Trichloroethene 68.60 - 4.40Vinyl Chloride 5.00 * - 0.50 *Benzene 1286.70 - 122.61
52:1 Carbon Tetrachloride 5.00 * - 0.50 *Chlorobenzene 17.30 - 1.98Chloroethane 5.00 * - 0.50 *Chloroform 85.40 - 10.921,1-Dichloroethane 30.00 - 3.231,2-Dichloroethane 5.00 * - 0.50 *1,1-Dichloroethene 5.00 * - 0.50 *trans-1,2-Dichloroethene 91.50 - 11.61Tetrachloroethene 5.00 * - 0.50 *1,1,1-Trichloroethane 117.70 - 4.44Trichloroethene 37.10 - 0.50 *Vinyl Chloride 5.00 * - 0.50 *Benzene 1210.70 - 81.19
* - less than
ATTACHMENT C 12/21/90BLOSENSKI LANDFILL SUPERFUND SITE
AIR STRIPPING PILOT TESTSELECTED VOLATILE ORGANICS ANALYTICAL RESULTS
SAMPLES COLLECTED 11/7/90 - 11/9/90
WATER WATER WATER WATERG:L PARAMETER INFLUENT INFLUENT EFFLUENT EFFLUENTRATIO DUPLICATE DUPLICATE
ug/L ug/L ug/L ug/L
AVERAGES Carbon Tetrachloride 2.75 - 0.50Chlorobenzene 17.79 - 2.01Chloroethane 4.53 - 0.50Chloroform 100.72 - 10.941,1-Dichloroethane 37.84 - 3.251,2-Dichloroethane 2.75 - 0.501,1-Dichloroethene 8.26 - 0.50trans-1,2-Dichloroethene 109.09 - 10.85Tetrachloroethene 3.01 - 0.501,1,1-Trichloroethane 113.99 - 5.66Trichloroethene 53.21 - 2.29Vinyl Chloride 7.21 - 0.50Benzene 1232.91 - 82.76
* - less than
flROOJ9ti6
H
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ATTACHMENT E
flROOI9l*8
«i r\L. , .^-vwi. , . .—._M !oi i mtu i L:O iSEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELU
PLE SOURCE: Blosenski Landfill________
WORK ORDER NO.: _N/A________________ EHRT PROJECT NO.: J2307
DATE EXTRACTED: 11-12-90_____________ DATE ANALYZED: J1-1MO
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: _ 500.00
ANALYST: K. Nusekabel_____________ FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: AS-l-150______________ EHRT SAMPLE NO.: 29360
LAB NOTEBOOK NO.: 149. Pq. 83_____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS___________ ug/L
1. Phenol < e.OO2. Bis(2-Chloroethyl) Ether < 4.003. 2-Chlorophenol < 4.004. 1,3-Dichlorobenzene < 12.005. 1,4-Dichlorobenzene < 12.006. Benzyl Alcohol < 6.007. 1,2-Dichlorobenzene < 12.008. 2-Methylphenol < 6.009. Bis-(2-Chloroisopropyl) Ether < 8.0010. 4-Methylphenol < 6.0011. N-Nitroso-Di-n-Propylamine < 8.0012. Hexachloroethane < 12.0013. Nitrobenzene < 6.0014. Isophorone < 4.0015. 2-Nitrophenol < 8.0016. 2,4-Dlmethylphenol < 6.0017. Benzole Acid < 40.0018. Bis(2-Chloroethoxy)Methane < 4.0019. 2,4-Dichlorophenol < 8.0020. 1,2,4-Trichlorobenzene < 12.0021. Naphthalene < 2.0022. 4-Chloroaniline < 20.0023. Hexachlorobutadiene < 24.0024. 4-Chloro-3-Methylphenol < 6.0025. 2-Methyinaphthalene < 2.0026. Hexachlorocyclopentadiene < 24.0027. 2,4,5-Trichlorophenol < 10.0028. 2,4,6-Trichlorophenol
Pann 1
(Jl JSTOMER SAMPLE NO.: AS-i-150 ____________ EHRT SAMPLE NO
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphtrialateAcenaphthylene2,6-Dinitrotoluene3-NitroaniiineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-DinitrotolueneDiethyiphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinitro-2-MethylphenolN-Nitrosodiphenyiamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthaJateDi-n-OctyiphthalateBenzo(b) RuorantheneBenzo(k) RuorantheneBenzo(a) PyreneIndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Ruorophenol2,4,6-Tribromophenol
< 6.00< 20.00< 6.00 < 4.00 m< 12.00 ^< 20.00< 4.00< 80.00< 40.00< 12.00< 12.00< 4.00< 12.00< 6.00< 40.00< 40.00< 6.00< 12,00< 10.00< 40.00< 4.00< 4.00< 2.00< 4.00 < 4.00 m< 6.00< 20.00< 6.00< 6.00
6.92< 4.00< 20.00< 20.00< 12.00< 20.00< 20.00< 20.00
PERCENT RECOVERY
58.50%52.70%37.10%
10.00% *10.00% * 418.30% ^
' A low recovery was obtained on the phenol surrogates. The surrogate recovery was also very low on the matrixSee and matrix spike duplicate. The sample matrix is probably responsible for these low recoveries sroe it Q C A
i reduces on 3 analyses of the same sample. Paqe 2 fl T\ u \T f 3 <J u
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
. JSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELU
\MPLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12307
-ATE EXTRACTED: 11-09-90___________ DATE ANALYZED: 11-09-90
\MPLETYPE: Water Sample_______ METHOD NO.: EPA 608
ANALYST: M. Cooper_________ LAB NOTEBOOK NO.: 158. Pg. 54
^JSTOMER SAMPLE NO.: AS-l-150___________ EHRT SAMPLE NO.: 29360
RESULTCOMPOUNDS .
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfanl < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfanll < Q.0213. 4i4'-DDD < 0.0214. Endosulfan Sulfate . < 0.000415. 4,4'-DDT < Q.001216. Methoxychlor < 0.000417. Endrin Ketone < o.0418. Chlordane < o.2019. Toxaphene < 3.00
flROO!95i
jSTOMER SAMPLE NO.: AS-l-150___________ EHRT SAMPLE NO.: 29360
20. Aroclor-1016 < 95021. Arocior-1221 < 0.5022. Aroclor-1232 < Q$Q23. Arodor-1242 < 0.5024. Aroclor-1248 < g.5025. Aroclor-1254 < g.5026. Arocior-1260 < g.50
SURROGATE RECOVERY
Dibutyichlorendate - ___ 99.00%
flROOI952Pane 2
SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. • MR. MIKE PETTERELU
PLE SOURCE: Blosenski Landfill
WORK ORDER NO.: _N/A________________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-12-90______________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 1000.00
ANALYST: K. Nusekabel___________ RNAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: AS-E-150_____________ EHRT SAMPLE NO.: 29361
LAB NOTEBOOK NO.: 149. Pg. 83____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS___________ ug/L
1. Phenol < 3002. Bis(2-Chloroethyl) Ether < 2.003. 2-Chlorophenol < £.004. 1,3-Dichiorobenzene < 5005. 1,4-Dlchlorobenzene " < §006. Benzyl Alcohol < 3007. 1,2-Dlchlorobertzene < QQQ8. 2-Methylphenol < 3 009. Bis-(2-Chloroisopropyl) Ether < 4.0010. 4-Methylphenol < 30011. N-Nitroso-Di-n-Propylamine < 4.0012. Hexachloroethane < g.OO13. Nitrobenzene < 30014. Isophorone < 2.0015. 2-Nitrophenol < 4>0o .16. 2,4-Dimethylphenol < 3.0017. Benzole Acid < 20.0018. Bis(2-Chloroethoxy)Methane < 2.0019. 2,4-Dichlorophenol < 4.0020. 1,2,4-Trichlorobenzene < e.0021. Naphthalene < I.QQ22. 4-Chloroanillne < iQ.OO23. Hexachlorobutadiene < 12.0024. 4-Chloro-3-Methylphenol < 3.0025. 2-Methylnaphthalene < 1.0026. Hexachlorocyclopentadiene < 12.0027. 2,4,5-Trichlorophenol < SQQ
flROOI953 < 5-°°
CUSTOMER SAMPLE NO.: AS-E-150
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthyiene2,6-Dinitrotoluene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenoiDibenzofuran2,4-DinitrotdueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-NitroaniIine4,6-Dinitro-2-MethylphendN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthenePyreneButylbenzylphtnalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctyiphthalateBenzo(b)RuorantheneBenzo(k)RuorantheneBenzo(a)Pyrenelndeno(1 ,2,3-cd)PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobipnenylTerphenyl-d14
Phenol-d52-Ruorophenol2,4,6-Tribromophenol
< 3.00< 10.00< 3.00 < 2.00 M< 6.00< 10.00< 2.00< 40.00< 20.00< 6.00< 6.00< 2.00< 6.00< 3.00< 20.00< 20.00< 3.00< 6.00< 5.00< 20.00< 2.00< 2.00< 1.00< 2.00 M< 2.00 < 3.00< 10.00< 3.00< 3.00< 2.00< 2.00< 10.00< 10.00< 6.00< 10.00< 10.00< 10.00
PERCENT RECOVERY
72.00%57.40%50.90%
10.00% *10.00% * m12.20% ^
A low recovery was obtained on the phenol surrogates due to the sample matrix.
Pane?
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCS ANALYSIS
JSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
,MPLE SOURCE: Blosenski Landfill _______________
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12307
TE EXTRACTED: 11-09-90___________ DATE ANALYZED: 11-09-90
MPLETYPE: Water Sample_______ METHOD NO.: EPAj308_
ANALYST: M. Cooper__________ LAB NOTEBOOK NO.: 158, Pg. 54
-JSTOMER SAMPLE NO.: AS-E-150___________ EHRT SAMPLE NO.: 29361
RESULTCOMPOUNDS
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC * < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosuifanl < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfanll < 0.0213. 4,4'-DDD < 0 0214. Endosulfan Suifate < 0.000415. 4,4'-DDT " < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < o.0418. Chlordane < 0.2019. Toxaphene < 3.00
aROOI955Paae 1
• JSTOMER SAMPLE NO.: AS-E-150___________ EHRT SAMPLE NO.: 29361
20. Aroclor-101621. Aroclor-1221 < '22. Aroclor-1232 <23. Arodor-1242 < Q^24. Arodor-1248 < Q'25. Aroclor-1254 < '26. Aroclor-1260 <
SURROGATE RECOVERY
Dibutylchlorendate - 166.00%
AROQI956Pa no n
COVER PfiGE - INDRGflNIC ANALYSES DfiTfi PACKAGE
-z 'jamg; ENVIR. _HEAi_TH_RESEARCH_TE Contract: QBG
D C.-c=: w38 __ Case No.: BLOSE 3AS No.: 123iZi7_ SDG Mo.
EPfl Samp is No. La/b gampiB ID.flSE150 , q
Were ICP iritsralsmer-t corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No NO
Comment 5:
Rei-=ase of the data contained in this hardcopy data package and in thecoiJtpuTsr-^sadable data submitted on floppy diskette has been authorized b%the Lsijoratory Manager or the Manager's designee, as verified by thefollowing signature.
Lafc Manager:
:OVER PA5E - IN
flROOI957
1 EPA SAMPLE NO.INORGANIC ANALYEE5 DATA SHEET
! II ASE150 I
_ = - .-••-: ENVIR. _HEflLTH_RE5SARCH_TE Cortrsct; QBG_____ i___________!
_a= :.-G5: was__ Case No.: SLOSH SPS No.: 1£307_ SDS No.: £00000
Plat'.--- ^=-oil/watsr:v : WATER Lab Sample ID: £9351___
Le-<=: (ic-w/med;: ___ Date Received: ll/06/9i2i
Concentration Units (ug/L c-- mg/kg% dry weight): UB/L_
uc i ;•,-• •?•=->" re:
Color After-;
Comments:
1iCAS No,1: 7i£9-9S-5i "-40-36-8; -443-30-2i 7- -0-39-3: 74413-41-7: 7440- 3-91 7440-70-5I 7*40-47-317 40-48-4; 7440-50-3i 7439-89-51 7439-92- i; 439-95-4I 7439-95-517439-97-6; 7440-02-01 7440-09-7i 7782-49-2i 7 40-22-4i 7440-£3-51 7440-23-01 7440-62-81 7440-66-5!
;
i i! Analyts ! Concent Ti iiAluiiunum !i. Antimony ii Arsenic !.'Barium 11 Bery 1 1 i urn ii Cadmium ii Calcium1 Chromium ii Co bait i1 Cop per i1 Iron !1 Lead i1 Mannes i urn iIManaanesel1 Mercury _ !1 Nickel !1 Potassium1 Selenium !! Silver :1 Sod i urn 1i Th a 1 1 i i-.m_ : _____I Vanac i urn !1 Zinc ;ICvaniae i1 !
Clarity Before
Clarity A^ter:
'atio
10.72.2
S.481.8
5.3
5.0
Ifl. 9
•7i <"-'. j.
4. fi
.-, 4L_ • *4 /->i . r
95.5
2. 4
.
t I
n ! C 1 G! 11 1IU!IU!1 iIU!I U I! iiU!! 1IU!I II U I1 I1 !
i U II U Ii !l U i!UI1 II U I1 !I U I
i 11 i
1 1!M 11 iINR:iP 1IF !I N R IIP !IP iINRIIP IINRIIP IINR!IP ;! NR 1INR!1 CV 1IP !I N R IIF iIP :INRIIP !INR:IP 1INR!I 1
Texture:
Artifacts:
U
~DR(« : - IN
1 -EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
I ASI150LSD -Jame: ENVIR. _HEALTH_RESEARCH_TE Contract: OB6_____ I________
Lafc Code: W8S__ Case No.: BLOSE SAS No.: 1S307_ SDS No.: 000000
Matrix (soil/watsr): WATER Lab Sample ID: 293S8A__
Level (low/med): ___ Date Received: 11/0S/9®
*• C C11 1 u 5 • _.___ _____ __
Concentration Units (ug/L or rng/kg dry weight): UG/L_
11
ICflS No.i17423-90-5i 7440-35-01 7440-33-c17440-35-3(7440-41-71 7440-43-91 7440-70-2! 7440-47-3; 7440-48-4i 7*40-50-817439-89-6i 7*39-32-117439-95-4! 7439-95-51 7439-97-6i 7440-02-0i 7440-09-71 7782-49-21 744S-£2-41 7 -40-23-5i 7440-23-0I 7448-G2-21 7 40-56-51
1
i i! Analyte 1 Concent r1 " i1 Aluminum i1 Ant i mony I' Arsenic 1! Barium 11 Bery Hi urn II Cadmium i! Calcium !! Chromium 11 Cobalt !1 Cop per 1! Iron !I Lead 1I Magnesium I1 Manqanese 1I Mercury 11 Nickel 11 Potassium!1 Selenium 1I Silver 11 Sod i urn 1I Thallium !I Vanad i urn I!Zinc 1(Cyanide I1 1
•at ion
10.72.2
0. 40
1.3
5.3
5.0
10.9
0. 14.5
2. 11.9
95.5
£.4
! 1IC1 Q1 iI 1IU!IUI1 1I U II U I1 IIUI1 1IUII 1iUI1 11 1I U II U I1 1IUIIUI! IIUI1 1I U I1 !1 1
i 1IM 1I 1INRIIP iIF 1! NR !IP !IP iINR:IP iINRIIP !INR!IP 1iNR!INR!I CV 1IP !1 MR 1IF iIP 1INRIIP i; NR iIP 1INR!1 I
Color Esfors: ,„ _____ Clarity Before:
AS-I-150
Color After: _______ Clarity After: ____ Artifacts:
Comment s :
FORM I - INftROOl959
&• EPA SAMPLE NO.DU
•--.--.-: INvI
:.:=: W88
":,. .soii/w
'?ii-fr for S
Co
1 • • i1 i
ip' :itfi,'iim !
1 Arsenic I1 Bar i urn 1! Bery Hi urn i(Cadmium 'i Calcium ii Chromium 1I Co 55 it 1
•i Copper 11 Iron 11 Lead i
i Plane; =ii!5=5iIMsrcurv i. NiCHel I
Ssier i um _!1 £ 1 1 ••. sr ' ;'Sec urn •
i - 1 r.c i!Cy5"-l_!S• i
R. HEALTH RESEARCH ~E Conr
Case No.
atcr>: WATER
SK-ple: ___
ncsnt rat i on Jn its
1 1Control ! iLimit i I Sam pi
! 11 1
58.0 I I10.0 1 1
! 15.0 1 I5 . 0 II
! i10. 0 ! 1
I !£5. 0 I I
1 !5. 1? ! 1
1 !1 1
0. 2 i 1MZl. 3 ;
: I5. 3 i 1
.1C. 0 i! i
1S.O Mi 1t i
£0. 3 1 Ii 1i j
. Dl PCST: DLi_cc
(ug/L ; 'ng
! i1 !
e (S) Cl 1! 1
1 : i10. ~800 mi i2. £858 ! U 1 1
1 ! 18. 4C80 i U i i1.S0881U! 1
i ' !
5. 3880 mi i- i i
c- 3S7SIUI '! i !
18. ?SiZi81U! i) • i
t i8. 1308m; if. £02811' ,
i i
L. -4£0'L;; iL. 3£<D3 i U i !
i i I95. fS38;iJ! !
i i i2. •~C8£;LH :
i :i i
ract: GBG
3 AS No. : l£387_
Leva 1
'/. Solids for
/kg ciry weight) :
I1
Duplicate (D) Cl!
1 110. 7008i'Ji£. £858 1 U 1
i i8. 4888 i UI1.8000 IUI
5. 3808 lUli 1
5. 8878! UIi i
18. 90801 U!1 i; !
0. 18881 L;4. 5880! UI
1 !2. 1 420 1 U 11.3888 IUI
1 I95.3888MJ1
i i2. 4808 | U I
1 i,' 'i
i ASI150D 11 1
SDB No. : 0880128
(low/med) : —— — -™_.
Duplicate: ___
UG/L_
1 M l !1 I 1 1 I1 RPD 1 IQI Ml1 i l l !1 II ! NR 11 1 I IP i1 1 1 IF !i M l M P1 M '0 ,1 N I P :1 Ml NR i1 M ! P ii ! 1 I NR :
1 1 I P '1 II ! NR i1 M : P •1 i ! i NP1 I I ! N R ;I ! 1 ' CY •I M , P •1 I I i N R i! ! 1 1 F '1 U IP lj I • :r,'Ri! I I I ? !
1 ! i i!M?l: 1 1 : P :i II i MR :I H i !
flROQ!960
£AJITIAL AND CONTINUING CALIBRATION VERIFICATION
-ic M=.-*e: ENVIR._HEAL7H_RESEARCH_TE Contract: 05S.
L.«fc -Iocs: *IS£__ Case No.: BLQSE 3AS No.; 1£387_ SDG No.: 838880
Initial Col:.sr.=tion Scares: SPE'<_______
ionti ruling Calibration Source: SPEX_____
Concentration Units: ua/L1 111 ;
'final yes !l |i Glum :n urn 'lAntin-cnyJ1 Arsenic >'i Bar i urn !i Beryl 1 i'.imii Cadmium i1 Calcium !j Chromium.,:iCoPalt ~!:'C;-oner i! Iron !: Lead '; Magnesium!: rianq = ns=e •i Mercurv i! NICKS! _ I1 Pot <?.3S i urn i•Selenium _i: Silver ;1 Sod i urn 1i Thallium J! Vanadium :I Zinc '! Cyanide ii :
* „ i T - 1t n 1 : i 3 i
7--'ue
533.58,
588.588.
588.
5'38.
588.
'J*
538.
— _10-" 183.
_1 80C.
-588.
iC' 18 i
10 !8 1
!0 i
!8 1
I.3 !
1i
12 i•2 i
i0 !3 1
li
8 !1
8 1i1
i
Calibration iPound :/.RCi.'' i
i1
587,50!47.981
!
476. 38 1498. 48 !
1549. 08 1
11
439.80!1
483. £81!1
5.481498. 70 1
I10.58!97. 18!
!9 6.58!
1494.901
I!
i181.5!95. 3 1
i_95. 3 !J98. 1 1
I189.31
!_97. 3 i
i36.6!
189. £i98. 1 1
i185.8!97. 1!
194.51
199.81
11
Continuing Calibration i ; iTrue Found tfRii) Found SRCDM M!
1 |
58S.58.
588.588.
580.
588.
588.
5.588.
£8.188.
..1008.
588.
iS !8 !
10 i
8 i:
8 !1
8 1I
8 !It
8 !8 i
18 i8 !
i8 i
18 1
11
583.49.
471.483.
548.
479.
47S.
5.483.
19.96.
961.
493.
138138!
!
38158!
178 i
i38!
148!
1i
38!£8!
198170!
198!
1781
1I
1
181._99.
_94.j95.
189.
,.95.
_35.
186._S6.
.99.96.
95.
93.
1-? ri i6 i
ii4171
17!
I01
i
7!Ii
816i
15!7!
1I
£!1
71I!
l ! ;.': :i I I P -
1 i ! NR !1 MP 1! i iP !i I iiNR! Mr!i i I N R 1; MP:! Mr-.-RiI I I P !i i i NR :i I INR!
I 1 CMI 1 !P !1 1 i NR 1! i IF :i I I P !! I I N R I1 MP :! i 1 NR !i i .a :i ! NR i1 i ;
:i) Control Limits: Mercury 88-l£0> Other Metals 98-110! C>snide 35-115
FORM II (PART 1) - :-N
SRGOI961
£AINITIAL AND CONTINUING CALIBRATION VERIFICATION
:jf«=: EfiVIR. _-iEAL PH _RESEARCH_TE. Contract: DBS.
Case No.: BLDSE SS5 No.: 1£3Q7 SD5 "Jo.: 088088
In i-i = i Cal ir.ratior; Source:
C on* in i.'.i rig
t i
1
iAl..':-v.:p !1 Ant ir;o •'••'-, '! Av-se-'-iic !; B~.vi:..n 'il Berv Hi urn ii Cacr.ii urn i! CoO. c i j'"i '•:Ch»-.;mi^T iiCc.nalr !'Cipzsr! Ir:r, i: L=-?c • •:s/bc-asi-.-m!
•1-7! '] = .•"= = 3'
M=>-c'.:ry !N-z:-'=l
' p,- -.-,— • :;r.- .•' Eel =r.i ..m :! S i 1 ,'.=r i! SOG i ur,i r:Th = lli;.;r- '' Vanad i :-x !: Z i f ic ;iCyanir.3 1' i
Ca 1 i brat i on Source : 5PE.V
Cone snt ration Unit
I nit:, si Calibration !True round #R(D! True
1 i i !12388.3 i 11753.331 98. 3 l l£S33. 3 :
! ' l ii : 1
13C0. 3 t 983.3®. 95.3! 1888.3 :1083.8 . 1825.231 10£. 5: 1C3C. 0 !
! ' { '£8CG.3 '• 1919.08: 95. j! iCGS. 3 1
'• I ' :irAOil- ^ C'"-'-1- ' t"1! ' 1 <?,£ 'J' •' = " - 7 -TI ijOil'v. J • Jil.r3. W"J i 1'it, <•• r -••tti-i'. kj ;
> i i t' 1 r
£88. C1 ! 531.58! 95.'"" 53C. •-? !i l .
i i •
5CS:8. C ' ^347.38!_9a. i; S088. 0 iI |
i ! ! i£383.3 1 1973.38! 58. y- £083.'? !
i ' i£083.8 i £855.88! 10:. 2' £388.8 i
! i i4(3158.3 : 4135. 381 183. 4 : 4308.2 !
i i i '! ; ;
s; ug/L.
Cont inuing Cal i brat ionFound tfRd; Found %R •'
; I 1
l S. 38! 131.4! ii ' 11 J i
iei7.C3!l3i.7! I1074.30I1S7. :i| 1
1 i !1971.38! 95. £: i
! ' !w^filF^T. W'i1 f * i-1 / , ._• 1
' i 1
£39. 931 181. £i !1 I; i1 i
8090. 30! 101. 1! !! ! !i ! !
202£.00I101.3I !i 1 1
2118.301135.9! i1 i
4£55. 80! 135.41 1i i 11 1 1
! r ti !
I ' t
1 !»•'='
| - ,
• -:~ i
; I N R I• ! P '
! IP '! 1 "•£ .
1 • - '
• INF,!! IP .! 1 MC '
1 iP !! ! r-.'R !i iNR!M'jRi' : r t
! I NR 1I 1 NR ;M~ '1 1 Nfi i: IP: IMP,I I P !1 I N R i( !
(I.1 Control :_:r;iit = : Mercury 38-lcv? Ifsr ""etais 98-110? -vanids 35-115
AR001962
BLANKS
_=- Name: ENVIR. _HEAL7H_RE=EARCH_-E Contract: 055
_sb LOSS: W1
3 •-•• a n s -'• — T " ."".v"!« sr p z\ r ~ \r A ' - > i
— ""5D-5'.~ ~,t icn
1
1
i r-.luriiiriLirf ilAr'timony !s-r-sviiu i:3c>>HiMi ii.:5""y' i - 1 Ufn iCacrn i uni i
~"• w i'__ vfl'
; Chromium ii C D sv • ~ I
; Coccsr Ii iron !' L=ac! i'Magnesium!' Manganese li Mercury..,. 11 Nickel !i Potassium!i Selenium !! Silver "lSod i urn i— i- - i l ..... ;' : i Icli A - '.I III . i
' Vanadium _!Ilinc i'Cyamds-.... !' !
33 __
B 1 ?"ik
Blank.
Case No. 5 BLOSE SflS No. : 1£I£7_ 3DG No. ; 01Z300S
Mat r i x i so i 1 / wat er > : WfiTER
Ccncsritrst ion Units Oag/L or nig/kg. ; 'S/L
T ,. 4 4- .' - '•» :' ' 1 1 1 s. in . i i t.M =: A A U .
Blankiug/L;
10.£.
3.^ •
__ _ „•-'•
cr•._/«
10.
8.4.
£•4X •
•"=",*W •
."•.£.«
«;w
-Ta "w
•3
q
4X
s1J.•3
VJ
4.
J
(
1Ci
1i !!U'IU!I i;_r• U!. i .Ji U i1 11 1
IUII !1 i
.J _;! 1
":uiILMi !1 1 1 11 U 1
i ' ' 1_ ' 'W 1i i
"" ! ' ;(
IUI.J J
• !
i ii !
Continuing Calibration M Prspa-Blank. (ug/L) i ! ration
i C £ C 3 CM Blank1 :
13.c!.
3.1.
C1w> •
c-u*
18.
3.4.
.•"r£.•
•1i •
l_jSff
.»,Uri
-T/
C
u
3
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3
9
<5.
4i
g
w*
4
1 !!UI;uii iI U iIUI1 !i U iI IIBIf I1 1
i Ii iI 1IU!IUI! 1iUI!U!' i: I-.1 1IU!! 11 1
i ; i MI i i M 13.i i : i ; 2 .I ! • Mi i ! 1 i 3.1 i I I I 1 .I ! 1 ! II I ; 1 ; 5 .I I 1 I II I 1 i i 5 .! ! i ! !II : 1 ! 18.! i ; ! I1 ; i ! i1 ! 1 ! ! 3.i i I I ! 4 .I I I I Ii 1 I I I 2 .i 1 ! i i 1.! ! I l lI I I I I 9 5 .I I ! I !I I 1 M 2 .
' • 1 1 ! II I i M
738£88
488388
t1
.- :
!
I ;> i
I U IIUI!_:IU!IU!I I
388 1 U i1 i
818
938
188583
148988
588
408
IB!1 i! J1 1i !
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1 JIUI:_ii |
i
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i:
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INRIPINRiPi NIC
i r
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INR! CV_IPINRIFIPINRi ni r
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i
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11
11i
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11
FORM III - IN
aROOI963
1C? INTERFERENCE CHECK SAMPLE
_=u -..vis: ENVIR. _HEALTH_FE3EflRCH_TE Contract: -3-ES
i_ac '.ode: W88—— Case No.: SLOSE SAS No: 1£387_ SDG No.: 003383
1C? ID NuiiiBai-: £433______ ICS Source: _________
Corvcs-Mtrat ion units: ug/L
l TrSol.
• Ana./ts AiIAlurnir.:.mi_.533E30l! Antimony i 1i A--'=s''". ic ; li Bar i urr i I1 E@rv i 1 i am : !!CadrijM 1 1!Caiciur.i._ 1538838!1 Chromium ' IlEobait ' '•i Coppsr 1 l1 1 r ?n : 230000 1i -.sad i i! Magnes i urn 1 560 36 'if"a'.".ga"-ssel i!*"<='"- :ry : :"nicxel .' 1
: 'r:t ?.==.-. tmi3=le*njri! ' iISilvjy : ;1 Sod i urn ' !iThslliu^ ;! .'=."tsaium ' 1'Zinc 1 li ' i
1us :Sol. 1AB 1
1
_500000 11i
50015001100BI
500000 !50015001500!
_200003 !10001
_500000 15001
1
:338!i•ii1
500110001
1
Initial FoundSo i . So 1 .A AB
_4Sl403!_4326i33.l
15£~.
....... 1 459.i 910.
_4S79'38!_455888.4=2.
1 557,423.
_1"4833! 191163.| oq:_
_48ai36! 533383.1 =37.!
1 35a.
982.t
i
1 571.
1
3111;
01313101010131013:3131
3!
i01
'
i
3131
1
••'.R
_95.
105.97.91.97.93.
113._84.3="- _• .JQ....
130.101.
QC
_98.
114.0.
Ii Final round1 Sol. Sol.1 A AB %R1
5 1 _455388 1l' i
2181 131
_4S0530.1
1 529.490.
1 924.3i_475£C!3!_4S£338.A| l~ 494.41 101bl 1762081217 1 _492900 141
i :i ;
6 'i iii2! 1
11 1
8121 I
1 1
532.l 402.'i
1 1012._58£730.: 560.
1 932.
31i1
01013101010101
1013101
i31
I
_95.
185.33.92.
_97.98.106.80.
101.133.196.;-• —
__?_j*
i
iii
1 !li
Si3'412 *
Q 'w .
4 I41
£:513i
£'i 1 i
1i1
_li
1 11 538.
955.1
3101
I
107.95.
51c- ;
1
H AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLJ
MPLE SOURCE: Blosenski Landfill _____________________
WORK ORDER NO.: N/A________________ EHRT PROJECT NO.: 12319
DATE EXTRACTED: 11-12-90______________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample______________ SAMPLE VOLUME: 1000.00
ANALYST: K. Nusekabel___________ FINAL VOLUME: _LOO
CUSTOMER SAMPLE NO.: AS-E-120___________ EHRT SAMPLE NO.: 29453
LAB NOTEBOOK NO.: 149, Pg. 83____________ METHOD NO.: EPA 8270
RESULTCOMPOUNDS____________ ug/L
1. Phenol < 3.002. Bis(2-Chloroethyl)Ether < 2.003. 2-Chlorophenol < 2.004. 1,3-Dichlorobenzene < 6.005. 1,4-Dichlorobenzene < 6.006. Benzyl Alcohol < 3.007. 1,2-Dichlorobenzene . < 6.008. 2-Methylphenol < 3.009. Bis-(2-Chloroisopropyl) Ether < 4.0010. 4-Methylphenol < 3.0011. N-Nitroso-Di-n-Propylamine < 4.0012. Hexachloroethane < 6.0013. Nitrobenzene < 3.0014. Isophorone < 2.0015. 2-Nitrophenol < 4.0016. 2,4-Dimethylphenol < 3.0017. Benzole Acid > < 20.0018. Bis(2-Chloroethoxy)Methane < 2.0019. 2,4-Dichlorophenol < 4.0020. 1,2,4-Trichlorobenzene < 6.0021. Naphthalene < 1.0022. 4-Chloroaniline < 10.0023. Hexachlorobutadiene < 12.0024. 4-Ch!oro-3-Methylphenol < 3.0025. 2-Methylnaphthalene < 1.0026. Hexachlorocyclopentadiene < 12.0027. 2,4,5-Trichlorophenol < 5.0028. 2,4,6-Trichlorophenol < 5.00
flROOi965
CUSTOMER SAMPLE NO.: AS-E-120______________ EHRT SAMPLE NO.:
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroaniiineDimethyfphthalateAcenaphthylene2,6-Dinitrotoluene3-NrtroanilineAcenaphthene2,4-Dinrtrophenol4-NltrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinitro-2-MethylphenolN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthenePyreneButylbenzyiphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl) PhthalateDi-n-OctylphthalateBenzo(b) RuorantheneBenzo(k)RuorantheneBenzo(a)Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyi-d14
Phenol-d52-Ruorophenol2,4,6-Tribromophenol
< 3.00< 10.00< 3.00 ^< 2.00 V< 6.00< 10.00.< 2.00< 40.00< 20.00< 6.00< 6.00< 2.00< 6.00< 3.00< 20.00< 20.00< 3.00< 6.00< 5.00< 20.00< . 2.00< 2.00< 1.00< 2.00 M< 2.00 < 3.00< 10.00< 3.00< 3.00< 2.00< 2.00< 10.00< 10.00< 6.00< 10.00< 10.00< 10.00
PERCENT RECOVERY
68.50%58.70%56.00%
10.00%* ^10.00% * M13.80%
* A recovery lower than 10% was obtained on surrogates due to heavy emulsion „ n , -, - -AROOI966
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCS ANALYSIS
JSTOMER NAME: PEG LABORATORIES. INC. • MR. MIKE PETTEREL
V1PLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12319
UHTE EXTRACTED: 11-13-90__________ DATE ANALYZED: 11-13-90
MPLETYPE: Water Sample_______ METHOD NO.: EPA 608
AMALYST: M. Cooper__________ LAB NOTEBOOK NO.: 158. Pg. 56
CUSTOMER SAMPLE NO.: AS-E-120___________ EHRT SAMPLE NO.: 29453
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < Q.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT - < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < . o.0418. Chlordane < o.2019. Toxaphene < 3.00
flROOI967
JSTOMER SAMPLE NO.: AS-E-120___________ EHRT SAMPLE NO.: 29453
20.21.22.23.24.25.26.
Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260
< 0.50< 0.50< 0.50< 0.50< 0.50< 0.50< 0.50
SURROGATE RECOVERY
Dibutylchlorendate - ____65.30%
AROOI968Pans?
COVER PAGE - IMORGAN1C ANALYSES DATA PACKAGE
;rM5: EN'.'Ifi. _HEALTH_iE5EARCH_TE Contract: DBG
_ac I.-ce: -'26__ ."35.25 No. : 3LG5E SAS No. : 1£319_ SDG No. : 888388
OU Mo.: ___
EPP Samale No. i_s_D Sample ID._AS£i£3_ £3453
Wers ICP inter 5 lenient correct ions acpiied ? v==/No V'EE
Were ICP background corrections applied 7 Yes/No Y'EEIf yes - were raw data generated beforeapplication of background corrections ? Yes/No NO
Cornnisnt =;CE-5_L ABO RATQRI E=_-_BLOSENSK I _LANDF I LL_DATE_DF_ANAL YS IS 11 /12/ 99___ICP_S.STAKE_MBl55_P346_rtETHOD_S01«/_FURNflCi_P. BARNWELL_NB154_PG£2___~ O R _ J . RADER_NB157_P6c2_METHOD_7470_____
Rel=5=? of th= data contaiisd in this hardcopy data package and in thecofnD:.:t5r->-=5d.3uis "5ta submitted on floDpy diskette has been author:z=cth= i.sbcrat.-r-y Manager or the "tanapsr's designee, as verified by thef•: 1 lew; rig =; i3t:at:-!»*5.
Lab Manager:
Osta:COVER 3P3E - IN
flRQOI969
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET __
i ASE120_.-.c J------ : ENVIR. _KEALTH_RESEARCH_TE Contract: QB5_____ i__________
Case No.: BLG5E SA5 No.: 12319_ 5D6 No.: 008000
Matrix 'soil/water,' : WATER Lab Sample ID: 25453
Level • lo^/mec) : ___ Date Received: i 1/09/90
'.-. ' -•.- D.--
Concentrat ion
ii!CA3 No.
! 7429-33-517440-35-iZi1 7440-3 E-2! 7 40-39-317440-4 1-717440-42-rI 7440-70-217443-47-3I 744:3-4.9-4! 7440-53-317439-69-617439-92-11 7439-95-4! 7439-96-5i 7439-97-6
17732- 5-2i 7440-22-41 744i?-23-5i 744i?-2S-3i 7440-62-21 7440-56-61i
ore s
:=r :
Units (ug/L or r.ig.'kg dry
i : ii Ana i , t s ; Concent rat i on iI •: ii Alu.TiiiV.iM I! Ant ;mony i 13. 7 ii Arsenic i 2. 2 !(Barium '• •.i Beryllium; 0. -M3 '! Cad mum i 1.6 1iCaiciui" i i1 Chromium i 5. 3 ii Cobalt i • I.'Copper ! 5. 0 ii Iron I !I Lead i 10.9 1IMaqnesiumi iIManqanesei i! Mercury ! 0. 1 1i Nicks I ! 4.6 ;1 Pot as si urn; if Selenium : 2. 1 !! Silver \ 1.9 !! So a i urn i |! Thallium • 35.5 I1 Vanadium i iiZinc ! £.411C van ids i i! ... ..... 1 1
Clarity Before:
Clarity After:
weight;1
i
r1 ' nj!
UiUI!
UIUi
1U!
!
UI1
Ui11!
UIUI
1UIUi
iUI
1
UI:i
: L'G/L_
j
' f:1 •'
i i-NR!i p !
•F ;INR!IF iIP !!NRiIPI N R Ii Ei N R iIP ii NR i! NR !ICVIIP i!NR!, r iIP iI N R IIP IINR!IP iINR!i i
Texture:
Artifacts:
i .'™'
: - INflROOI970
U.S. EPfi - CLP
£AINITIAL AND CONTINUING CALIBRATION VERIFICATION
LSD Name: ENV'Ifi. _HEALTH_RESEARCH_TE Contract: OBG
Lab Cods: Wfl3__ Case No.: BLOSE SAS No.: li£319_ 5DG No.: 000000
Initial Calibration Source: SPEX
Cont iryjinn Cs : i brat i on Source: SPEX
Concent rat i on Un i t
i IlAnalyte f! Ii 01 -..mi n urn '! Antimony !i Arsenic 1i Ban urn !i Bery Hi urn i! Cadmium i'Calcium 1I Chromium 'i Co bait 1! Copper ii Iron 1! Lead iIMaqnesiurnli Manqanese i1 Mercury 1(Nickel 1! Potassium!1 Selenium !1 Silver 1i Sod i urn 1i Thallium 1I Vanad i urn 1IZinc li Cyanide ii l
InitialTrue
i500. 0 !50.3 !
I
500.0 !300.0 i
1500.0 <•
1500.0 !
i530. 0 !
11
5.0 150Q.0 1
I10.0 !
100.3 !i
1000.3 !i
500.0 :!i
Cai ibrat ionFound ;'.R(i)
15S7.50J 101. 547.90! 95.3
i476.30! 95.3490.401 98.1
I549. 00! 10S. 8
I489.001 97.3
1483.201 96.6
• !It
5.481109.6490.70! 98. 1
110.501105.097. 10! 97. 1
1946.50! 94.6
1494. 90! 99.0
I1
I11 Truei1 11 500.0 !
1 50. 0 1! 1i__500. 0_!i 500.0 I
1 11 500.0 I
1 1I 500.0 I
1 I1 500.0 1
I 1I 11 5.0 i1 500.0 11 11 20.0 !1 100.0 II 1!_1000. 0 11 "l1 500. 0 1
1 !1 1
s: ug/L
Cont i nu i no Ca 1 i brat i onFound #Rrt) Found
i I508.301101.7!49.301 99.5!
I i471.80! 34.4!483.60! 96.71
1 !548. 70! 109. 7!
'1 I479.80! 96.01
I l478.401 95.71
I 11 !
5.301106.0!483.20! 95.6!
1 !19.901 99.5!96.701 96.71
! i951.90! 96.2!
1 !493.701 98.7!
! 1I 1
1 i !i 1 !
•/.R (1)1! Ml! 1 ;
1 I I NR 1i f 1 P f
i IF iI ! NR II IP i! IP 11 ! NR !1 IP i1 1 N.9 11 IP !
1 1 1 NR !1 I IP i1 i ! NR !1 I ! NR I! i f CV !1 I I P !1 i 1 NR I1 IIP !1 I I P !1 I I N RIi : i P i! I I N R If I I P !I i ! NR i! 1 1 !
•:i) Control Limits: Mercury 80-126! Other Metals 90-110! Cyanide 85-115
~ORM II (PART 1) - IN _ ,SROOI971
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
_rr •;=:=: ENVIR. _HEALTH_RESEARCH_7E Contract: DBG
-r« I-;-as: jJ88 Case No.
x nitiai Hal
: BLQSE 3AS No. : J
i r-r at i on Source : SPEX
.2319_ SDG No. : 000000
Cont i.''.:i rig Calibration Source: SPEX
1
i
iifi
i
j
i
!
1!11
1
i
Anai/te ii
Aluminum 1Ant : ri:ony_ 1
Barium !Bery 1 1 i urn 1Cadmium. ICa-lciurn !Chromium_lCobalt lCo --per !I >*,;.,•; !
Leas ___ IMagnesium!Manganese-'Me'' cur. _. i
Pot as si urn 1Selsrdun- _!Silver 1Sod . urn 1Tha Hi. ,,-;!_!Variaa i urn iZinc 1Cyan ice !
t
Concent
Initial CalibrTrue Found
I12000.0 111760.
J
i
108C. 0 1 988._lSi3l2,(ZM_10£S.
"l "20-30,8 i 1919.
I5030.0 1 5299.
I500.0 1 581.
!i»
88C0. 3 i 7847.!I
2000.0 i 1978.1
2000. 0 1 2065.1
4030.3 1 4125.11
00
00
00
00
00
50
00
00
00
00
ration LSf'its: uo.-'L
: ! iat ion • • Continuing Calibration !!•/.R(l)f True Found %R'1> Found '-'.Rd;!.1 M
i 1 I
i 98.
ij
i 95.I 102.l
i 96.1! 10S.II 96.
i
! 98.111.98.I1103.
1103.1i
i31 12000.
I:
3!_1000.ai 1300.
101 2300.
01 5000.I
91 £00.i!!
1 I 3000.11
9! 2000.1
2 1 _230S.i
4 I _4000.
1
: !
0 '12170.00!l 1i j
0 ! 1017.00!3 i 1074.001
i 13 1 1971.001
! 10 ! 5364,00!
: i3 i 609.90!
I if 1
! 1| j
0 I 3030.00!| !
I I
0 j 2026.00!j j
0 ! 2118.001i I
0 : 4255.00!1 1!• !
J
101.41i
i I l i N R; i IP! 1 ! NR
!T111
1! i i 1 NR i
101.71107.41
198.61
1107.3!
I101.61
i11
101. 1 11
1
101.3!1
105.9!1
105.411!
! 1 IPi ! IPI 1 iNRi IIPi 1 1 NR1 1 IP1 f INR1 MP1 1 INR1 1 INR1 i 1 NR! IIP1 1 1 NR1 1 INR! IIPI I I N R! IIPI ! I NRI I IP1 i INR
! 1
i!
1
|
j
I
1
11
1
I
1
1
1
1
1
!1:
(1) Control Limits: Mercury 80-120' Other Metals 90-1105 Cyanide 85-115
BLANKS
« Name: ENVIR. _HEAL7H_FE5EARCH_TE Contract: OBG
Las Cods: Wi
Prspa^rtion
Pveparat ion
i li I1 1! iIPnalyte i1 !'Aluminum 1! Antimony 1(Arsenic iI Barium 1f Beryllium!1 Cadmium 11 Calcium 1i Chromium !, /-t _ •. • _ ,i L'-<o<sit !! Copper 1! Iron 1! Leadi Magnesium i> Manganese 1I Mercury i(Nickel i1 Pot as si urn!i Selenium !! S i 1 ver 1! Sodium I! Thallium 1I Vanad i urn iI Zinc 11 Cyanide I1 I
38 __ Ca
Blank Matrix (
Blank Concentr
11
Initial . !Caiib. !Blank 1(us/L) Cl
11 !
10.7 IU!2.2 IUi
1 I0.4 IUI1.8 IUI
I i5.3 IUI..
1 !5. 0 IUI
I 110. 9 ! 1
1 iI I
0.1 ;ui_4.6 IUI
1 I2.1 IUI ._1.9__IUI_
1 I95.5 I I
1 1£.4 IUI _
1 1I I
se No. : BLOSE SAS No. : 1£Z
soil ./water): WATER
at ion Units (ug/L or nig /kg) :
Cont inuing Cal i brat ionBlank. (ug/L)
1 C 2 C 3
i i 1 !10.7 IU! 1£. £ IUI 1
I I !0. 4 IUI 11.8 IUI I
I i !5.3 IUI I
1 ! 1 15.0 IB! I 1
I I I I10. 9 1 1 I !
! 1 I !1 ' I !
0. 1 ! U 1 II4.5 IU! 1 1
1 ! 1 i2. 1 I U 1 111.9 IUI I 1
1 ! I I95. 5 1 f •• II
I I 1 1£ . 4 I U I . 1 1
I I I I! I 1 I
19_ 3DS No. : 000000
UG/L_
I! I!M II !I i Prepa- 1 1!! ration M I
C! i Blank Cl i MM I I !
I l l I I I N R i1 M 10. 700IUMP ff ! ! S. 200 i U ! ! F 1! ! I 1 ! 1 NR 11 II 0.400 IUI IP
! 1! 1.S00IUIIP !i l l 1 I I N R !Ili 5. 300 1 U 1 ! P 1III i ! ! NR1 II 5. =310161 IP IIII ! 1 ! NR Ii l l 1 0 . 9001 M P 1III 1 1 INR 1I I I I I N R 1I I 0 . 10CIUI I C V 11 | 4.600IUMP 11 I 1 MNR 1II 2. 140 IUI IF 1I ( 1.980IUI IP__II I 1 M N R 1i | 95.5001 MP_!Ill 1 I INR !! M £.400IUIIP_Ii l l ! 1 I N R !I i! ! M 1
FORM III - IN
flROOI973
PREDESIGN REPORT
BLOSENSKI LANDFILLCHESTER COUNTY, PENNSYLVANIA
APPENDIX 5-3
ftRQOI97l+
Environmental Health Research and Testing, Inc.
3235 Omni Drive Cincinnati, Ohio 45245 (513) 752-2950 FAX (513) 752-2261
January 8, 1991 xjT c '\
O'BRIEN AND GERE ENGINEERS, INC.ATTN: Mr. Tee Tong-ngork5000 Brittonfield Pkwy - Suite 300P.O. Box 4942Syracuse, New York 13221
Dear Mr. Tong-ngork:
Please find enclosed the results of analysis for the 13 samples received on January 2, 1991.
If you have any further questions, please feel free to contact me at (513) 752-2950.
Sincerely,
Mona Risk, Ph.D.Director of Chemistry
MR:jw
Enclosures
cc: Charles McGuth
NATIONAL OFFICES
Cincinnati, Ohio • Lexington, Kentucky • Research Triangle Park, North Carolina • _Denver, Colorado • Birmingham, Alabama • Philadelphia, Pennsylvania • San Francisco, California * Mflnfi) I{fy(d)i j Q ~j S
'
flROOI976
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
METHOD OF SHIPMENT:
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-0200 ftROO i 977
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY:
LOCATION:
SAMPLED BY:
ORGAN.ZATION: 0 .
STATIONNUMBER SAMPLE LOCATION DATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONTAINERS
ANALYSISREQUIRED
METHOD OF SHIPMENT: r^- \ a f^
T
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 49421 Syracuse, NY 13221 / (315) 437-0200 - n n n , A -. -978
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: QBG____
Lab Code: W88__ Case No.: BLOSE SAS No.: 1£495_ SDB No. : 000000
SOW No.: ___
EPA Sample No. Lab Sample ID._NCC100_ 30654_____NCC105_ 30655_____NCC85__ 30651____NCC90__ 30652_____NCC95__ 30653_____NCC95D_ 30656____NCL100_ 30660____NCL105_ 30661ft____NCL105D 3066 IB____NCL105S_ 30661____NCL85__ 30657_____NCL90__ 30658_____NCL95__ 30659_____NCRAW__ 306££____
NCRAWF 30663
Were ICP interelement corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No N0_
Comments:BLOSENSKI J.ANDF I LL_DATE_OF_ANALYS I S_JANUARY_4, _1991 ______________ICP_G.STAKE_NB156_PG78 METHOD_6010/ FURNACE_P.BARNWELL 169 PG3 METHODAS7060/ COLD VflPOR M. COOPER NB157 PG48 METHOD 7470
Release of the data contained in this hardcopy data package and in thecomputer-readable data submitted on floppy diskette has been authorized bythe Laboratory Manager or the Manager's designee, as verified by thefollowing signature. L Q 'A
Lab Manager:
Date: l\COVER PAGE - IN 7/87
flROOI979
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS. INC.
SAMPLE SOURCE: N/A
WORK ORDER NO.: N/A PROJECT NO.: 12495
ANALYSIS PERFORMED: Total Suspended Solids Analysis
ANALYSIS METHOD: Std. Method 209C
ANALYST: M. Reddy
DATE ANALYZED: 01 -03-91
LAB NOTEBOOK NO.: 137, Pg. 80
SAMPLE NO.EHRT NO. CUSTOMER NO.
30651 NC-C-8.5
30652 NC-C-9.0
30653 NC-C-9.5
30654 NC-C-10.0
30655 NC-C-10.5
30656 NC-C-9.5-D
30657 NC-L-8.5
30658 NC-L-9.0
30659 NC-L-9.5
30660 NC-L-10.0
30661 NC-L-10.5
30662 NC-RAW
RESULTS(mq/L)
146
164
182
174
172
142
188
312
452
502
310
134
Detection Limit: < 20 mg/L
Page1 flROOI980
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _____
I II NCC85 I
Lab Name: ENVIR. _HEALTH_RESEflRCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 1£495_ SDG No.: 000000
Matrix (soil/water): WATER Lab Sample ID: 30651___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
Color Before:
Color After:
Comments:
1ICAS No.
1I74S9-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-2| 7440-47-31 7440-48-41 7440-50-81 7439-89-617439-92-117439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-7
1 7782-49-21 7440-22-41 7440-23-51 7440-28-0
1 7440-62-21 7440-66-611
1 1 I I1 Analyte IConcentrationlCI Q1 1 I I1 Aluminum 11 Antimony 11 Arsenic 1
1 Barium 11 Beryl Ii urn 11 Cadmium 1(Calcium 11 Chromium 11 Cobalt 11 COD oer 11 Iron 1! Lead 1I Magnesium)1 Manganese 11 Mercury 1INickel 11 Potassium!(Selenium 11 Silver 1
1 Sodium 1(Thallium 1
1 Vanad i urn 1(Zinc 1(Cyanide 11 1
Clarity
Clarity
1 11 1
2.2 IUI1 11 1
1.3 iUI1 1
5.3 IUI1 11 11 1
10.9 IUI1 11 i
0. 1 IUI '4.6 IUI
1 If 11 11 11 I1 11 11 !1 1
Before:
After:
i 1IM 11 1INRIINRIIF IINRIINRIIP 1
_INRIIP 1INRIINRIINRIIP 1INRIINRI1CVIIP 1INRIINRIINRIINRIINRIINRIINRIINRI1 1
Tex'
Art
NC-C-8. 5POST DIGEST SPIKE (ARSENIC) = 103'/. RECOVERY
FORM I - IN 7/87
&ROQ1981
U.S. EPA - CLP.
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: ENVIR. _HEALTH_RESEARCH_TE
Code: W88 Case No. : BLOSE
rix (soil/water): WATER
?1 (low/med) :
olids: ___
Concentration Units (ug/L
1 11 NCC90 1
Contract: OBG 1 I
SAS No. : 12495_ SDG No. : 000000
Lab Sample ID: 30652
Date Received: 01/02/91
or rng/kg dry weight): UG/L_
1 1 1 1 1 1 1ICAS No. 1. Analyte IConcentrationlCI Q IM 1
1 1 1 1 1 1 117429-90-5 1 Aluminum 117440-36-0 (Antimony 117440-38-2 (Arsenic i17440-39-3 1 Barium 117440-41-7 1 Beryllium!17440-43-g | Cadmium 117440-70-2 1 Calcium 117440-47-3 1 Chromium 117440-48-4 1 Cobalt I17440-50-8 1 Copper 117439-89-6 I Iron 117439-92-1 ILead I1 7439-95-4 1 Magnes i urn 117439-96-5 (Manganese!17439-97-6 1 Mercury 117440-02-0 (Nickel 11 7440-09-7 1 Pot ass i urn 117782-49-2 1 Selenium 117440-22-4 (Silver 117440-23-5 (Sodium 117440-28-0 1 Thai Hum 117440-62-2 1 Vanadium 117440-66-6 (Zinc 11 ICvanide 11 I 1
or Before: Clarity
or After: Clarity
merits:
I I INRII I INRI
2. 2 IUI IF 1I I INRII I INRI
1.3 IUI IP 1. ! 1 INRI
5.3 IUI IP II I INRI1 1 INRII I INRI
10.9 IUI IP 1I I INRII I INRI
0.1 IUI ICVI4. 6 IUI IP 1
1 1 INRII I INRII f INRII I INR!I I INRI1 I INRII I I N R 1I I INRII I I I
Before: Texture:
After: Artifacts:
NC-C-9. 0
FORM I - IN 7/87
fiROQI982
U.S. EPA - CLP
1 EPfl SAMPLE NO.INORGANIC ANALYSES DATA SHEET
i Name: ENV!
Code: W88_
rix (soil/i
B! (low/mec
olids:
Cc
or Before:
or After:
ments:
IR. HEALTH RESEARCH TE Contract: OB6
1 11 NCC95 i1 1
_ Case No. : BLOSE SAS No. : 12495_ SD6 No. : 000000
nater) : WATER Lab Sample ID: 30653 ___
1) : ___ Date Received: 01/02/91
mcentration Units (ug/L or mg/kg dry weight): UG/L_
1ICAS No.11 7429-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-217440-47-3| 7440-48-41 7440-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-71 778£-49-21 7440-22-4
1 7440-23-51 7440-28-01 7440-62-21 7440-66-611
1 I I . I1 Analyte (Concent rat ionlCI QI 1 I I(Aluminum 1 1 1(Antimony 1 1 1(Arsenic 1 2.2 IUI(Barium I ! 1(Beryllium! 1 11 Cadmium 1 1.8 IU I1 Calcium 1 1 11 Chromium 1 5. 3 IUII Cobalt 1 1 11 Copper 1 1 I1 Iron 1 1 1ILead 1 10.9 IUIIMaqnesiumi 1 1
1 Manqanese 1 1 11 Mercury 1 0. 1 1 U 1(Nickel 1 4.6 IUI(Potassium! 1 11 Selenium 1 1 11 Silver 1 1 11 Sodium 1 1 11 Thai Hum 1 1 11 Vanadium 1 1 1I Zinc 1 1 1(Cyanide I 1 I1 • I I I
Clarity Before:
Clarity After:
1 1IM 1! 1INRIINRIIF 1INR!INRIIP 1INR!IP 1INRIINRIINRIIP 1INRIINRIICVIIP 1INRIINR!INR!INRIINR!INRIINRIINRI1 1
Texture:
' Artifacts: __
NC-C-9. 5
FORM I - IN 7/87
flROOI983
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: ENVIR. HEALTH RESEARCH TE
Code: W88 __ Case No. : BLOSE
*ix (soil/water): WATER
;1 (low/med): ___
Dlids: ___
Concentration Units (ug/L
1 11 NCC10J0 1
Contract: OBG I 1
SAS No. : 12495_ SDG No. : 000000
Lab Sample ID: 30654 ___
Date Received: 01/02/91
or mg/kg dry weight): UG/L_
I 1 I 1 1 1 IICAS No. 1 Analyte IConcentrationIC! Q IM 11 1 1 1 1 1 117429-90-5 1 Aluminum 11 7440-36-0 1 Ant i mony 117440-38-2 I Arsenic 117440-39-3 1 Barium 117440-41-7 (Beryllium I17440-43-9 I Cadmium 117440-70-2 1 Calcium 117440-47-3 1 Chromium !17440-48-4 1 Cobalt 117440-50-8 (Copper 117439-89-6 I Iron 117439-92-1 (Lead 117439-95-4 1 Magnesium 117439-96-5 1 Manganese!17439-97-6 I Mercury 117440-02-0 1 Nickel 117440-09-7 1 Potassium!17782-49-2 1 Selenium I17440-22-4 (Silver 117440-23-5 1 Sodium 117440-28-0 I Thai Hum 117440-62-2 I Vanadium 117440-66-6 IZinc I
1 1 Cyanide 11 1 1
or Before: Clarity
or After: Clarity
ment s :
I I INR!I I INRI
2.2 IUI IF II I INRI1 1 INRI
1.8 IUI IP 11 1 INR!
5.3 IUI IP 11 f INR!I I INRII I INRI
10.9 IUI IP II ! INRI1 I INRI
0. 1 1 U 1 1 CV 14.6 IUI IP 1
1 1 . INRI1 I INRII I INR!I 1 INRII I INRI1 1 INRI1 1 INRII I INRII I I I
Before: Texture:
After: Artifacts:
NC-C-10.0
FORM I - IN 7/87
U.S. EPA - CLP
1 EPA SAMPLE NO.INORBANIC ANALYSES DATA SHEET
I II NCC105 I
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No.: 000000
Matrix (soil/water): WATER Lab Sample ID: 30655____
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
1 1 1 M i lICAS No. 1 Analyte 1 Concent rat ionlCI Q IM 11 1 1 1 1 1 I17429-90-5 1 Aluminum 1 1 117440-36-0 1 Antimony 1 1 117440-38-2 1 Arsenic 1 2.2 IUI17440-39-3 1 Barium 1 1 117440-41-7 IBervlliuml 1 117440-43-g (Cadmium 1 1.8 IUI17440-70-2 1 Calcium I I I17440-47-3 | Chromium 1 5.3 IUI17440-48-4 1 Cobalt 1 1 117440-50-8 (Copper 1 1 117439-89-6 1 Iron I I I17439-92-1 ILead I 10.9 IUI17439-95-4 IMaqnesiuml 1 117439-96-5 IManaanese! 1 11 7439-97-6 1 Mercury 1 0. 1 1 U 117440-02-0 1 Nickel I 4.6 IUI17440-09-7 1 Pot ass i urn 1 1 117782-49-2 1 Selenium 1 I I17440-22-4 (Silver 1 1 117440-23-5 1 Sodium 1 I I17440-28-0 1 Thai Hum 1 I I17440-62-2 1 Vanadium I 1 117440-66-6 IZinc 1 I I1 ICvanide 1 1 11 1 1 I I
or Before: Clarity Before:
or After: Clarity After:
ments:
INRIINRIIF 1INRIINRIIP 1INRIIP 1INRIINRIINRIIP 1
__ INRIINR!ICV!IP 1INRIINRIINRIINRIINRIINRIINRIINRI1 1
Texture:
Artifacts:
NC-C- 10.5
FORM I - IN 7/87
flROOJ985
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
I NCC95DLab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG______ I_______
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30656___
Level (low/med): ___ Date Received: 01/02/91
•/. Solids: ___
Concentration Units (ug/L or rng/kg dry weight): UG/L_
1 1 1 I IICAS No. 1 Analyte 1 Concent r at i on ICI Q1 I I I I17429-90-5 1 Aluminum 117440-36-0 (Antimony 117440-38-2 1 Arsenic I17440-39-3 1 Barium 117440-41-7 | Beryl Hum!17440-43-9 1 Cadmium 117440-70-2 1 Calcium 117440-47-3 (Chromium 117440-48-4 I Cobalt 117440-50-8 1 Copper 117439-39-6 1 Iron 117439-92-1 ILead 117439-95-4 IMaonesiuml1 7439-96-5 1 Mannanese 117439-97-6 1 Mercury 117440-02-0 1 Nickel 11 7440-09-7 1 Pot ass i urn 117782-49-2 (Selenium 117440-22-4 (Silver 117440-23-5 1 Sodium 117440-28-0 1 Thai Hum 117440-62-2 1 Vanadium 117440-66-6 IZinc 11 1 Cyanide I1 I I
I 11 1
2.2 IUI1 1I 1
1.8 IUI1 I
5.3 IUI1 11 11 1
10.9 IUI1 !1 1
0.1 IUI4.6 IU!
I 1I 11 11 11 11 11 11 11 1
1 1IM 11 1INRIINRIIF 1INRIINRIIP 1INR!IP IINRIINRIINRIIP 1INRIINRIICV!IP 1INR!INRIINRIINRIINRIINRIINRIINRI1 1
Color Before: ______ Clarity Before: _______ Texture:
Color After: ______ Clarity After: ____ Artifacts:
Comments:
NC-C-9.5-D
FORM I - IN 7/87
flROOJ986
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: ENVIR. HEALTH RESEARCH TE
Code: W88 Case No. : BLOSE
rix (soil/water): WATER
=1 (low/med): ___
olids: _____
Concentration Units (ug/L
1 11 • NCL85 1
Contract: OBG 1 |
SAS No. : 1£495_ SDS No. : 000000
Lab Sample ID: 30657 ___
Date Received: 01/02/91
or mg/kg dry weight): UG/L_
1 I ! 1 1 1 1ICAS No. 1 Analyte 1 Concent r at ionlCI Q !M 11 1 1 I 1 1 117429-90-5 1 Aluminum 117440-36-0 1 Antimony 117440-38-2 1 Arsenic 117440-39-3 1 Barium 117440-41-7 1 Beryllium!17440-43-9 1 Cadmium 117440-70-2 i Calcium I17440-47-3 1 Chromium 117440-48-4 1 Cobalt 117440-50-8 1 Copper 117439-89-6 1 Iron 117439-92-1 ILead 117439-95-4 1 Magnesium!17439-96-5 1 Manganese!17439-97-6 1 Mercury 117440-02-0 1 Nickel 11 7440-09-7 1 Pot ass i urn I17782-49-2 1 Selenium 117440-22-4 (Silver 117440-23-5 1 Sodium 117440-28-0 (Thallium 117440-62-2 1 Vanadium 117440-66-6 I Zinc 11 1 Cyanide 11 1 i
or Before: Clarity
or After: Clarity
rnents:
I I INRII I INRI
2.2 IUI IF 1I I INRII I INRI
1.3 IUI IP 1I 1 INRI
5.3 IUI IP 1I I INRI1 1 INRI( I INRI
10.9 IUI IP 1I I INRI1 1 INR!
0. 1 1 U 1 1 CV 14.6 IUI IP 1
I I INRII I INRII I INRII f INRII I INRI1 1 INR!I I INRII I INRII I I I
Before: Texture:
After: Artifacts:
NC-L-8. 5
FORM I - IN 7/87
AROOI987
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ____
I NCL90Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_______ I________
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30658___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
Color Before:
Color Afters
Comments!
1ICAS No.I1 7429-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-2| 7440-47-31 7440-48-41 7440-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-6
1 7440-02-01 7440-09-71 7782-49-21 7440-22-41 7440-23-51 7440-28-017440-62-21 7440-66-61I
1 i I I1 Analyte (Concent rati on ICI Q
I 1 I I1 Aluminum 1 1 11 Ant i mony I 1 11 Arsenic 1 2.2 IUI1 Barium 1 1 11 Beryl liuml 1 11 Cadmium I 1.8 IUI(Calcium 1 1 11 Chromium 1 5. 3 IUI1 Cobalt 1 1 I1 Copper I 1 1llron 1 1 1(Lead 1 10.9 I UIIMaanesiuml 1 11 Manganese 1 1 11 Mercury I 0.1 IUI1 Nickel 1 4. 6 IUI1 Potassium! 1 1ISelenium 1 1 I1 Silver 1 1 11 Sodium 1 1 11 Thai Hum 1 1 1(Vanadium 1 1 1IZinc 1 1 11 Cyanide 1 1 11 1 I I
Clarity Before:
Clarity After:
1 11M 11 IINRIINRIIF 1INRIINRIIP 1INRIIP 1INR!INRIINRIIP 1INR!INRIICVIIP IINRI
_INR!INRIINR!INRIINRIINRIINRI1 1
Texture:
Artifacts:
NC-L-9.0
FORM I - IN 7/87
AROOI988
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ____ __
I NCL95 ILab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDB No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30659___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
1 1 1 I I I !ICAS No. 1 Analyte IConcentrationlCI Q IM 11 1 f I I I !17429-90-5 1 Aluminum 117440-36-0 (Antimony I17440-38-2 (Arsenic I(7440-39-3 1 Barium 117440-41-7 1 Beryl Hum!17440-43-g | Cadmium 117440-70-2 (Calcium 117440-47-3 1 Chromium 117440-48-4 1 Cobalt 117440-50-8 ICopoer 117439-89-6 1 Iron 117439-92-1 I Lead 117439-95-4 IMaqnesiumi17439-96-5 1 Manqanese 117439-97-6 1 Mercury 117440-02-0 1 Nickel 11 7440-09-7 1 Pot ass i urn 117782-49-2 1 Selenium 117440-22-4 1 Silver 117440-23-5 (Sodium 117440-28-0 (Thallium 117440-62-2 (Vanadium 117440-66-6 (Zinc 11 1 Cyanide 11 1 1
1 11 1
2.2 IUI1 I1 1
1.8 IUI1 1
5.3 IUII 11 11 1
10.9 IUI1 11 1
0.1 IUI
4.6 iUI1 11 II 11 !1 11 1I 11 11 1
INRIINRIIF 1INRIINR!IP IINRIIP 1INRIINRIINRIIP 1INRIINRIICVIIP IINRIINRIINRIINRIINRIINRIINRIINRII 1
Color Before: _______ Clarity Before: _______ Texture:
Color After: ______ Clarity After: ____ Artifacts:
Comments:
NC-L-9. 5POST DIGEST SPIKE (ARSENIC) = 107/4 RECOVERY
FORM I - IN 7/87
flROOI989
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ___________
II NCL100
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG______ I________
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30660___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or rng/kg dry weight): UG/L_
I 1 1 I IICAS No. 1 Analyte (Concent r at ion 1C I Q1 1 1 I I17429-90-5 1 Aluminum 117440-36-0 1 Antimony 117440-38-2 1 Arsenic 117440-39-3 1 Barium 117440-41-7 | Beryl Hum!17440-43-9 1 Cadmium 117440-70-2 1 Calcium 117440-47-3 1 Chromium 117440-48-4 1 Cobalt 117440-50-8 1 Copper 117439-89-6 1 Iron 117439-92-1 ILead I1 7439-95-4 1 Maqnesi urn 117439-96-5 IMannanesel17439-97-6 1 Mercury 117440-02-0 1 Nickel 117440-09-7 1 Potassium 117782-49-2 1 Selenium 1(7440-22-4 1 Silver 117440-23-5 1 Sodium 117440-28-0 1 Thai Hum I17440-62-2 I Vanadium 117440-66-6 IZinc 11 (Cyanide 11 1 1
1 11 1
2.2 IUI1 11 1
1.8 IUI1 1
5.3 IUI1 11 1I 1
10.9 IUI1 11 I
0.3 1 I4.6 IUI
1 1I 11 11 I1 11 11 11 11 1
I 1!M 11 1INR!INRIIF 1INRIINRI
_JPJINRIIP 1INRIINRIINRIIP 1INRIINRIICVIIP 1INR!INRIINR!INRIINRIINRIINR!INRI1 1
Color Before: ______ Clarity Before: ____ Texture:
Color After: _______ Clarity After: ____ Artifacts:
Comments:
NC-L-10.0
FORM I - IN 7/87
flROOI990
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ____________
I II NCL105 I
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30661A__
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
1ICAS No.i17429-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-21 7440-47-3| 7440-48-41 7440-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-71 7782-49-21 7440-22-41 7440-23-51 7440-28-01 7440-62-21 7440-66-611
1 I I II Analyte IConcentrationlCI Q1 1 I 11 Aluminum 1(Antimony 11 Arsenic 11 Barium 11 Beryl liuml(Cadmium 1(Calcium 11 Chromium 11 Cobalt 1I Copper 11 Iron 11 Lead 1IMaqnesiuml1 Manaanese i1 Mercury 1INickel 11 Potassium!(Selenium 1(Silver I1 Sod i urn 11 Thai Hum 11 Vanad i urn iIZinc I1 Cyanide 11 1
1 11 !
2.2 IUII 11 1
1.8 IUI1 1
5.3 IUI1 11 11 I
10.9 IUIi 11 i
0.9 1 1 .4.6 IUI
r i1 11 11 11 11 I1 11 11 I
1 1IM 11 IINRIINRIIF 1INRIINRIIP 1INRIIP 1INRIINRIINRIIP 1INRIINRIICVIIP IINRIINRIINRIINRIINRIINRIINRIINRII 1
Color Before: ____. Clarity Before: ____ Texture:
Color After: ______ Clarity After: ____ Artifacts:
Comments:
NC-L-10.5
FORM I - IN 7/87
U.S. EPA - CLP
6 EPA SAMPLE NO.DUPLICATES ____________
I II NCL105D I
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No.: 000000
Matrix (soil/water): WATER Level (low/med): ___
% Solids for Sample: ___ "f> Solids for Duplicate: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_I i——————f-j——————————-——•———————-—————__ ^I I Control II II II I I I IlAnalyte I Limit II Sample (S) ClI Duplicate (D) ClI RPD I I Q I Ml
.11_____M_I_JJ IJNRI
INRIJ IJFJI I "l NR II I JNRII IPJ
I NR I
1 Aluminum 11 Antimony 1i Arsenic 11 Barium 11 Beryl liumlI Cadmium 1(Calcium 11 Chromium 11 Cobalt 11 Copper 11 Iron 11 Lead 11 Magnesium!1 Manqanese f1 Mercury 1INickel 1I Pot ass i urn 1I Selenium 11 Silver 1ISodium 1(Thallium 11 Vanad i urn 1(Zinc 1(Cyanide 11 i
1 11 1
10.0 I I1 II 1
5.0 I 11 1
10.0 1 I
1 11 11 1
5.0 1 11 i1 1
0.2 I 140. 0 II
1 11 11 I1 1i 11 11 11 11 1
I I I I I I 1I I I I I I 1
2. 2050 1 U 1 I 2. 2050 1 U i 1 1IN 1 1 I 1I I I I I I 1
1.8000IUII 1.B000IUII II I I I I I 1
5. 3000 IUI! 5. 3000 1 U 1 1 1I I I I I I 1I I I I I I 1I I I I I I 1
10. 9000IUII 10. 90001 Ull I
I I I I I I 1I I I I N 1
0.93001 1 1 0.83001 II 11.4 I4.6000IUII 4.6000IUI! 1
1 1 I i l l 1i l l I I I II I I I I I 1I I I I I I 1I I I 1 1 1 1I I I I I I I1 1 I I I I 1I I I I I I II I I I I I 1
I IJPJI I JNRII! INRII I JNRII 1JPJI I JNRII I JNRII IJCVII IJPJI ! JNRI
I I JNRII IJNR!I I JNRII I JNRII I JNRII I JNRII IJ NR II fl I
FORM VI - IN 7/87
flROOI992
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY _____________
II NCL105S
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG _____ I
Lab Code: WB8 __ Case No. : BLOSE SflS No. : 1£495_ SDB No. s 000000
Matrix (soil/water): WATER Level (low/med): ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
Comments:
I I ! 11 1 Control 1 11 1 Limit 1 Spiked Sample 1lAnalyte I *R 1 Result (SBR) ClI I I 1I Aluminum 1 I I I(Antimony I I I I1 Arsenic 175-125 1 100.0000 I 11 Barium 1 I I I1 Beryl liuml I 1 1ICadmium 175-125 1 550.7000 I 1(Calcium I I i 1(Chromium 175-125 1 534. 9000 1 1(Cobalt I I I I1 Copper I I I Illron I I I II Lead 175-125 1 593.0000 1 1IMaqnesiuml 1 1 11 Manqanese 1 1 1 11 Mercury 175-125 1 1.7500 I 11 Nickel 175-125 1 504.2000 I 11 Potassium! 1 I 1I Selenium 1 ' 1 I I(Silver 1 1 I I1 Sodium I I 1 I(Thallium I I I I1 Vanadium 1 ! I IIZinc I I I I(Cyanide I I I I1 1 1 1 1
11
Sample 1Result (SR) Cl
11 1
1 12. 2050 1 U 1
I II 1
1.8000 IUI
1 15. 3000 1 U 1
1 11 11 1
10.9000IU!1 1I 1
0. 9300 1 14. 6000 1 U 1
1 11 11 11 11 1I I1 I1 11 I
11
Spike 1Added (SA) I
111
100.0!11
500. 0 I
1500. 0 I
111
500. 0 1ri
1.01500. 0 1
111111111
1 1 11 1 1! 1 1
*R IQI Ml1 1 11 INRI1 INRI
100.01 IF I1 INRI1 INRI
110. 11 IP I
1 INRI107.01 IP I
1 INRI1 INRI1 INRI
118.61 IP 11 INRI1 INRI
82.01 ICVI100.81 IP I
1 INRI1 INRIi INRI1 INRI1 INRI1 INRI1 INRI1 INRI1 I 1
FORM V (PART 1) - IN • 7/87
SROOI993
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ___
I I1 NCRAW I
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30662___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or mg/kg dry weight): U6/L_
1 1 1ICAS No. 1 Analyte 11 1 117429-90-5 1 Aluminum 11 7440-36-0 1 Ant imony 117440-38-2 1 Arsenic 117440-39-3 1 Barium 117440-41-7 IBerylliuml17440-43-9 1 Cadmium i17440-70-2 1 Calcium 117440-47-3 I Chromium 117440-48-4 1 Cobalt 117440-50-8 (Copper 117439-89-6 1 Iron 117439-92-1 ILead 117439-95-4 (Magnesium!17439-96-5 1 Manganese 117439-97-6 1 Mercury 117440-02-0 1 Nickel 117440-09-7 I Potassium I17782-49-2 1 Selenium 117440-22-4 (Silver 117440-23-5 1 Sodium 117440-28-0 1 Thai Hum 117440-62-2 1 Vanadium 117440-66-6 IZinc I1 1 Cyanide 11 I 1
I 1Concent r at i on 1 C ! Q
I 11 11 1
2.2 IUI1 11 1
1.8 iUI1 1
5.3 IUI1 11 1I i
10.9 IUI1 1I 1
0.2 1 14.6 IUI
1 11 1I 11 11 11 11 11 11 1
1 !IM 11 1INRIINRI
_IF_IINRIINRIIP IINRIIP 1INRIINRIINRIIP 1INRIINRIICVIIP 1INRIINRIINRIINRIINRIINRIINRIINRI1 1
NC-RAW
Color Before: ______ Clarity Before: ____ Texture:
Color After: ________ Clarity After: ______ Artifacts:
Comments:
FORM I - IN 7/87
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
I NCRAWF ILab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG_____ I___________I
Lab Code: W88__ Case No. : BLOSE SAS No.: 12495_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 30663___
Level (low/med): ___ Date Received: 01/02/91
% Solids: ___
Concentration Units (ug/L or rng/kg dry weight): UG/L_
I 1 i I IICAS No. 1 Analyte IConcentrationlCI Q1 1 1 I I17429-90-5 1 Aluminum 1 1 117440-36-0 1 Antimony 1 1 117440-38-2 1 Arsenic 1 2.2 IUI17440-39-3 1 Barium 1 1 117440-41-7 1 Beryl Hum! I 117440-43-9 1 Cadmium 1 1.8 IUI17440-70-2 (Calcium 1 I I17440-47-3 1 Chromium 1 5.3 IU!17440-48-4 1 Cobalt 1 1 I17440-50-8 1 Copper 1 1 !17439-89-6 1 Iron 1 I I17439-92-1 ILead 1 10.9 IUI17439-95-4 IMaanesiuml 1 I17439-96-5 IMannanesel 1 117439-97-6 1 Mercury 1 0.2 1 117440-02-0 (Nickel 1 4.6 IUI17440-09-7 (Potassium! I 117782-49-2 (Selenium 1 I I17440-22-4 (Silver 1 I I17440-23-5 1 Sodium 1 I 117440-28-0 (Thallium 1 I I17440-62-2 1 Vanadium 1 1 117440-66-6 (Zinc 1 I I1 i Cyanide 1 1 1I i I I I
i iIM 11 1INRIINRIIF 1INRIINRIIP iINRIIP 1INRIINRIINRIIP 1INRIINRIICVIIP iINRIINR!INRIINRIINRIINRIINRIINRI! 1
Color Before: ______ Clarity Before: ____ Texture:
Color After: ______ Clarity After: ____ Artifacts:
Comments:
NC-RAW FILTERED
FORM I - IN 7/87
flROOJ995
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG.
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No.: 000000
Initial Calibration Source: SPEX
Continuing
1 11 1lAnalyte 11 11 Aluminum 11 AntimonyJ1 Arsenic _ 1.I Bar i urn 11 Beryl liuml1 Cad mi urn _ 1(Calcium !1 Chromium 11 Cobalt 11 Copper 11 Iron I1 Lead 11 Magnesium!1 Manganese 11 Mercury 1INickel 11 Potassium!ISeleniumJ(Silver ""l1 Sod i urn 11 Thai H urn J1 Vanad i urn IIZinc 1(Cyanide I1 1
Calibration Source: SPEX
Concentration Units: ug/L
1 1Initial Calibration 1 Continuing Calibration 1
True Found %R ( 1 ) 1 True Found *R ( 1 ) Found *R ( 1 ) 11 1
1 I I 1 I I I I1 I I 1 I I 1 1
20.0 1 20.701103.51 £0.0 1 21.601108.01 21.101105.511 • 1 1 ~ l I I I I1 I I 1 1 I I I
1000.0 1 1097.001109.71 1000.0 1 1068.001106.81 1064.001106.4!1 I I 1 I I I I
2000.0 1 2058.001102.91 2000.0 1 2004.001100.21 1979.001 99.011 I I 1 I I I I1 1 1 1 I I I I
1 I I 1 I I 1 I600.0 1 587.301 97.91 600.0 1 636.601106.11 618.201103.01
1 I I 1 I I I I1 I I 1 1 I I I
5.0 1 5.351107.0! 5.0 1 5.351107.01 5.441108.8!8000.0 1 8496.001106.21 8000.0 1 8217.001102.71 8200.001102.51
1 I I 1 I I 1 I1 I I 1 I I I I1 I I f I 1 I II I I 1 I I 1 11 I I 1 I I I 11 1 1 1 I I 1 1I 1 1 1 I I I I1 1 1 1 I I 1 11 I I 1 I I I I
1 11 11 Ml1 1INRIINRIIF 1INRIINRIIPJINRIIP 1INR~IINRIINRIIPJINR~IINRIICVIIP 1INRIINRIINRIINRIINRIINRIINRIINRI1 1
(1) Control Limits: Mercury 80-120? Other Metals 90-1105 Cyanide 85-115
FORM II (PART 1) - IN 7/87
'HROOI996
U.S. EPA - CLP
2BCRDL STANDARD FOR AA AND ICP
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG.
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SD6 No.: 000000
AA CRDL Standard Source: _________
ICP CRDL Standard Source: SPEX IND.__
Concentration Units: ug/LI i——————————————pj ,I I CRDL Standard for AA I I CRDL Standard for ICP II I I I Initial Final IlAnalyte I True Found %R II True Found *R Found %R II I _______ I I1 Aluminum i 11 Antimony 1 11 Arsenic 1 1(Barium 1 11 Beryl Hum 1 11 Cadmium 1 IICalcium 1 11 Chromium 1 11 Cobalt i 11 Copper 1 11 Iron 1 11 Lead 1 1IMaqnesiuml 1I Manaanese 1 1(Mercury 1 11 Nickel i 11 Potassium! 1(Selenium 1 1[Silver 1 11 Sod i urn 1 11 Thai Hum 1 I1 Vanad i urn 1 1IZinc 1 11 1 1
I I I 1 I I 1I I I 1 1 I 11 I I I I I I .1 II 1 1 1 1I I I 1 I I 11 II 500.01 496.301 99.31 536.401 107.I l l 1 I I 11 II 500.01 461.001 92.21 503.301 100.I l l 1 I I 11 1 1 1 1 1 1I I I 1 I I 11 II 500.01 506.701101.31 542.301 108.I l l 1 I I 1I I I 1 1 I 11 I I 1 1 1 11 II 500.01 467.501 93.51 500.501 100.I l l 1 I I II I I 1 I I 1I I I 1 1 1 11 1 1 1 I I 1I I I 1 I I II I I 1 1 1 ii l l i I I 1I I I 1 I I 1
III11
3!1
71111
511I1
11_l
111I111
FORM II (PART 2) - IN 7/87
flROOI997
U.S. EPA - CLP
3BLANKS
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG.
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No. : 000000
Preparation Blank Matrix (soil/water): WATER
Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_
1 11 11 11 1lAnalyte 11 1(Aluminum 1(Antimony 11 Arsenic 1(Barium 11 Beryl Huml1 Cadmium 11 Calcium 11 Chromium 11 Cobalt 11 Copper 11 Iron 11 Lead 11 Magnesium!1 Manganese 11 Mercury 11 Nickel 11 Pot ass i urn 1(Selenium 1(Silver 11 Sod i urn 1I Thai Hum 11 Vanad i urn 1IZinc 1I Cyanide 1I 1
1Initial 1Calib. IBlank 1(ug/L) Cl
I1 11 1
2.2 IUI1 11 I
1.8 IUII 1
5.3 IUI1 11 11 1
10.9 I II 11 1
0.1 IU!4.6 IUI
i 11 i
1 1I 1
I 11 1
1 11 1
1 1
Continuing CalibrationBlank (ug/L)
1 C 2 C 3
1 I I I1 1 I I
2.2 IUI 2.2 IUII I I Ii 1 1 1
1.8 IUI 1.8 IU!I I I I
5. 3 IUI 5.3 IUII I I 11 1 I II I I I
10.9 1 1 10.9 1 11 1 I II I I I
0.1 IUI 0. 1 IU!4.6 IU 1 4.6 IUI
1 1 I II I I II I I I1 I I II I 1 II I I I1 1 I II I I II I I I
1 11 11 11 1
Cl 11 1
1 I !1 1 11 II1 I I1 1 11 I I1 I 11 1 11 1 I1 1 11 f I1 1 11 1 I1 1 11 1 1I I I1 II1 i 1
1 1 11 1 11 1 1I 1 1
f 1 1I 1 !1 1 1
1 1 11 1 1
Prepa- 1 1 1ration II 1Blank Cl 1 M 1
1 1 1! 1 1 NR 11 1 INR 1
2.200IUIIF 11 ilNR 11 I INR 1
1.800IUIIP 11 1 INR 1
5. 300 1 U 1 1 P I1 1 INR 1I 1 INR 11 1 INR 1
10.9001 IIP I1 1 INR 11 1 INR 1
0. 100IU1 ICV I4.6001UIIP 1
1 I INR 1I 1 INR 11 1 INR 11 1 INR 11 1 INR 11 1 INR 1I IlNR 11 1 INR 11 1 1 1
FORM III - IN 7/87
AROOI998
U.S. EPA - CLP
4ICP INTERFERENCE CHECK SAMPLE
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG.
Lab Code: W88__ Case No. : BLOSE SAS No: 12495_ SDG No. : 000000
ICP ID Number: 2483______ ICS Source: ___________
Concentration Units: ug/L
i i i———————————•——,I True I Initial Found I Final Found Ii Sol. Sol. I Sol. Sol. I Sol. Sol. II Analyte A AB I A AB *R I A AB *R II__________________I_________________I_________________________II Aluminum 15000001 5000001 4490001 477000.01 95.41 4703001 488200.01 97.611 Antimony 1 11 Arsenic 1 11 Barium 1 11 Beryl Hum I I1 Cadmium 1 11 Ca 1 c i urn _ 1 500000 11 Chromium 1 11 Cobalt 1 11 Copper 1 1ilron 120000011 Lead 1 1(Magnesium 150000011 Manqanese 1 11 Mercury 1 11 Nickel 1 11 Pot ass i urn 1 1(Selenium i 11 Silver i 11 Sod i urn 1 1I Thai Hum 1 11 Vanadium 1 1IZinc 1 11 1 1
11
50015001
1000!
_500000 1 .
500150015001
200000 I10001
500000 15001 "
I10001
1I
100011
1500110001
1
1I1i1
_467800I111
18910011
467200 1111111111I1
1 11 1
525.01105.01480.01 96.01958.01 95.81
_494100.0I_98.8I.466.01 93.21574.01114.81438.01 87.61
173800.01 86.911140.01114.01
468100.01 93.61484.0! 96.8!
I I895.01 89.51
f 11 1
962.01 96.211 11 I
472.01 94.41955.01 95.51
1 1
1 1 1I I 1
1 538.01107.611 493.01 98.611 1000.01100.01
_495800 1 _51 1400. 0 1 102. 3 11 486.01 97.211 448.01 89.611 5654.01 Ii 178200.01 89.111 1063.01106.311 479000.01 95.811 496.01 99.211 1 f1 910.01 91.011 1 11 1 11 984.01 98.411 1 11 I 11 484.01 96.811 989.01 98.91I 1 1
FORM IV - IN 7/87
AROOI999
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY
Lab Name: ENVIR. HEALTH RESEARCH TE Contract: OBG
1 11 NCL105S 11 1
Lab Code: W88 __ Case No.: BLOSE SAS No.: 12495_ SDG No.:
Matrix (soil/water): WATER Level (low/med):
Concentration Units (ug/L or mg/kg dry weight): UG/L_
I I I 11 (Control! 11 1 Limit 1 Spiked Sample 1lAnalyte 1 *R 1 Result (SSR) ClI I I !1 Aluminum I I I II Antimony I I I I1 Arsenic 175-125 1 100.0000 1 I1 Barium I I 1 11 Beryl liuml 1 I IICadmium 175-125 1 550.7000 1 1(Calcium I I 1 I1 Chromium 175-125 1 534.9000 1 11 Cobalt I I 1 I1 Copper I I I Illron I I I IILead 175-125 1 593.0000 1 1IMaqnesiumf 1 1 11 Manganese! 1 1 11 Mercury 175-125 1 1.7500 1 11 Nickel 175-125 I 504.2000 I 1(Potassium! 1 1 1(Selenium I I I I1 Silver I I I I1 Sodium I I I IIThallium I I I I(Vanadium I I I IIZinc 1 1 I I(Cyanide I I I II 1 1 I I
1 11 1
Sample 1 Spike 1Result (SR) C! Added (SA) 1 #R
1 11 11 1
2. 2050 1 U 11 1I 1
1.8000 IUI
1 15. 30001 UI
1 11 1! 1
10. 90001 UI
1 1_. ———— L 1
^ 0. 9300 1 j\4. 60001 UI
1 11 11 11 11 11 11 11 11 1
11
100.01 100.11
500.01 110.1
500.01 107.111
500.01 118.11
1.0! 82.500.01 100.
111111111
000000
1 1 11 1 11 1 1IQI Ml1 1 11 INR!1 INRI0IJFJ
1 INRIi INRI
11 IP 11 INRI
01 IP I1 INR!1 INRI1 INRI
61 IP 11 INRI1 INRI
01 ICVI81 IP 1
1 INRI1 INRI1 INRI! INRI1 INRI1 INRI1 INRI1 INRII 1 1
Comments:
FORM V (PART 1) - IN „ ,_ rt „ 7/87ARQ02000
U.S. EPA - CLP
6 EPA SAMPLE NO.DUPLICATES
I 1I NCL105D I
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I__________I
Lab Code: W88__ Case No.: BLOSE SAS No.: 12495_ SDG No.: 000000
Matrix (soil/water): WATER Level (low/med): ___
% Solids for Sample: _____ % Solids for Duplicate: ___
Concentration Units (ug/L or mg/kg dry weight): UG/L_
1 1 II1 1 Control 1 1lAnalyte 1 Limit II1 1 II1 Aluminum 1 1 1lAntimony 1 1 11 Arsenic 1 10. 0 1 11 Barium 1 111 Beryl liuml 1 11 Cadmium 1 5.0 1 11 Calcium 1 1 11 Chromium 1 10. 0 1 11 Cobalt 1 II1 Copper 1 1 11 Iron 1 1 11 Lead 1 5. 0 1 1IMaqnesiuml 1 11 Manganese! 1 11 Mercury 1 0. 2 1 11 Nickel 1 40.0 1 I1 Potassium! 1 1(Selenium 1 1 11 Silver 1 II1 Sodium 1 1 1I Thai Hum 1 1 1(Vanadium 1 1 1IZinc 1 II(Cyanide 1 1 11 1 I I
I I I IM I I
Sample (S) CM Duplicate (D) CMM I I
I I I I I II I I 1 I I
2.2050IUII 2.£050IUIII I ! 1 I I1 1 1 I I I
1.8000 IUI I 1.80001 UNI I I I I I
5.3000IUII 5.30001UIII I I I I II I I I I I1 II ' 1 U
10. 9000 IUI 1 10.9000IUIII I I I I I
^- —————— t-Nj. | __ ____ kj |
08. 9300 1 4 1 C0. 8300 1 J \475000TU 1 1 4. 6000 ! U 1 I
I I I I I I1 1 1 I I I1 1 I I I I1 1 1 I I I1 1 1 I I II I I 1 1 1I N I I II I I I I II I I I I I
1 1 ! 1II 1 1
RPD I I Q I Ml1 1 1 1I I INRII I INR!1 1 IF 1I I INRI1 1 INRIII IP 1I I INRI1 i IP iI I INRII I INRII I INRI1 1 IP I1 1 INRI1 1 INR!
11.4 II ICV!H I P !I I INRII I INR!II INRIII INRII I INRII I INRII I INRII I INRI1 1 1 1
flR00200l
f&HRTEnvironmental Health Research and Testing, Inc.
3235 Omni Drive Cincinnati, Ohio 45245 (513) 752-2950 FAX (513) 752-2261
January 1,1991
RECEIVEDO'BRIEN & GERE ENGINEERS, INC.ATTN: Mr. Tee Tong-ngork „5000 Brittonfield Parkway, Suite 300 Jf\N - 'P.O. Box 4942Syracuse, New York 13221 „„,.,-.-
««-«.-•—_ '">r~ ~'"""Dear Mr. Tong-ngork: "~"~
Please find enclosed the results of analysis for the twenty-five (25) samples received on December14, 1990.
If you have any further questions, please feel free to contact me at (513) 752-2950.
Sincerely,
Mona Risk, Ph.D. . Q*»cV-Director of Chemistry
MR:ds
Enclosures
NATIONAL OFFICES
Cincinnati Ohio • Lexington, Kentucky • Research Trianglfl ffykfflfittlrtMHmafj 11000900?3 • Birmingham, Alabama • Philadelphia, Pennsylvania • ii/TrLlcWatcUfWnt • Miami, FlorA ft U U d U U £.
Siiii ii !n snnnnnDDDn
3R002003
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY:
LOCATION:
SAMPLED BY:
ORGANIZATION:
STATIONNUMBER SAMPLE LOCATION OATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONTAINERS
ANALYSISREQUIRED
Q) - O iv.-?© TS) 60- fai /W ,,Ti)c>
Vtr**^1-, frrxt,
TSc
- o,'""N Tb<L
METHOD OF SHIPMENT:
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 /(315) 437-0200
AROQ2001*
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.V*>* OOi . ISl
SURVEY:
LOCATION:
SAMPLED BY:
ORGANIZATION:
STATIONNUMBER SAMPLE LOCATION DATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONTAINERS
ANALYSISREQUIRED
U/v-iK.FiYi iT4>ft— IS't*
OH) "Z.1/25"
£ f A bO ft
~- O-IAI "N(ly |(S< ,K, LW-.kfvvv SQ ~ 0«( Uoft
BU-, bog
(S) tbft — t.Ol1*. v/
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished 8 DATEal
TIMEIbVBfi
Received by Laboratory:— •« — •— »\S>r n *t j — ra V- o
DATE TIME
<
METHOD OF SHIPMENT:
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-0200 ft R fl t'l ? D 0 5
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS,INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A PROJECT NO.: 12444
ANALYSIS PERFORMED: TOC Analysis
ANALYSIS METHOD: EPA Method 9060
ANALYST: J. Bums
DATE ANALYZED: 1 2-1 7-90
LAB NOTEBOOK NO. : 1 35, Pg. 25
SAMPLE NO.EHRT NO. CUSTOMER NO.
30246 ISO-0
30247 ISO-0.1
30248 ISO-0.5
30249 ISO-1
30250 ISO-5
30251 ISO-15
30252 INFLUENT
30253A ISO-OD
30253B ISO-ODDuplicate
30254 ISO-0.1 AD
30255 ISO-0.5AD
30256 ISO-LOAD
30257 ISO-5D
30258 ISO-1 5D
RESULTS(mg/L)
BDL
BDL
BDL
BDL
BDL
BDL
BDL
15.64
14.68
BDL
21.98
25.06
71.52
26.11
Detection Limit: < 10 mg/L
Pase' flR002006
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12444
DATE EXTRACTED: N/A_________ DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: ISO-0.1 EHRT SAMPLE NO.: 30247A
LAB NOTEBOOK NO.: 162, Pg. 42______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodlchloromethane < 0.502. Bromoform < 0.50
13. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene < 0.506. Chloroethane < 0.501*. 2-Chioroethylvinyl Ether < 0.508. Chloroform 6.479. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.4916. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 1.9019. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Page1 flR002007
CUSTOMER SAMPLE NO.: ISO-0.1_________ EHRT SAMPLE NO.: 30247A
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane < 0.5026. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene < 0.5031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-DIchloroethane-d4 - _____96.00%
Toluene-d8 - 98.00%
Bromofluorobenzene - 96.00%
Page2 AROQ2Q08
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12444
DATE EXTRACTED: N/A___________ DATE ANALYZED: 12-15-90
SAMPLE TYPE: Water Duplicate SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: ISO-0.1 EHRT SAMPLE NO.: 30247B
LAB NOTEBOOK NO.: 162. Pg. 42_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene < 0.506. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 7.279. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dlchlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 3.0416. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 2.4319. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Pagel flRQQ2009
CUSTOMER SAMPLE NO.: ISO-0.1_________ EHRT SAMPLE NO.: 30247B
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane < 0.5026. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene < 0.5031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____85.00%
Toluene-d8 - 111.00%
Bromofluorobenzene - 102.00%
Pas92 flROOZOIQ
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12444
DATE EXTRACTED: N/A__________ DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: ISO-0.5 EHRT SAMPLE NO.: 30248
LAB NOTEBOOK NO.: 162. Pg. 42_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene . < 0.506. Chloroethane < 0.507. 2-ChloroethyMnyl Ether < 0.508. Chloroform < 0.509. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane < 0.5016. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene < 0.5019. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Page1 , AR0020M
CUSTOMER SAMPLE NO.: ISO-0.5_________ EHRT SAMPLE NO.: 30248
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane < 0.5026. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene < 0.5031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____94.00%
Toluene-d8 - 96.00%
Bromofluorobenzene - 101.00%
Page 2 /5R0020I2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS. INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12444
DATE EXTRACTED: N/A__________ DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: ISO-1 EHRT SAMPLE NO.: 30249
LAB NOTEBOOK NO.: 162. Pg. 42______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene < 0.506. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform < 0.509. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane < 0.5016. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene < 0.5019. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Pagel 3R0020I3
CUSTOMER SAMPLE NO.: ISO-1__________ EHRT SAMPLE NO.: 30249
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane < 0.5026. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene < 0.5031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____95.00%
Toluene-d8 - 101.00%
Bromofluorobenzene - 97.00%
Page2 AR0020II*
tlMViHUNMENTAL HEALFH KfcStAHCH AMU i fcb TING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS. INC.
MPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A_________________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90 ____ DATE ANALYZED: 12-17-90
SAMPLE TYPE: Water Sample___________ SAMPLE VOLUME: 930.00
ANALYST: K. Nusekabel__________ FINAL VOLUME: ___1.00
CUSTOMER SAMPLE NO.: ISO-0 ____ _______ EHRT SAMPLE NO.: 30259
LAB NOTEBOOK NO.: 166. Pg. 16____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1. Phenol < 5.382. Bis(2-Chloroethyl)Ether < 2.153. 2-Chlorophenol < 2.154. 1,3-Dichlorobenzene < 6.455. 1,4-Dichlorobenzene < 6.456. Benzyl Alcohol < 3.237. 1,2-Dichlorobenzene < 6.458. 2-Methylphenol < 3.239. Bis-(2-Chloroisopropyl)Ether < 4.3010. 4-Methylphenol < 3.2311. N-Nitrosp-Di-n-Propylamine < 4.3012. Hexachloroethane < 6.4513. Nitrobenzene < 3.2314. Isophorone < 2.1515. 2-Nitrophenol < 4.3016. 2,4-Dimethylphenol < 3.2317. Benzole Acid < 21.5118. Bis(2-Chloroethoxy)Methane < 2.1519. 2,4-Dichlorophenol < 4.3020. 1,2,4-Trichlorobenzene < 6.4521. Naphthalene < 1.0822. 4-Chloroaniline < 10.7523. Hexachlorobutadiene < 12.9024. 4-Chloro-3-Methylphenol < 3.2325. 2-Methylnaphthalene < 1.0826. Hexachlorocyclopentadiene < 12.9027. 2,4,5-Trichlorophenol ~" < 5.3828. 2,4,6-Trichlorophenol < 5.38
Pagei 3ROQ2G{5
CUSTOMER SAMPLE NO.: ISO-0________________ EHRT SAMHLE NO.: 30259
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-N'rtroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-N'rtroaniiineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroanillne4,6-Dinitro-2-MethyiphenolN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButylphthalateRuoranthenePyreneButyl benzylphthalate3,3'-D!chlorobenzidlneBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b)RuorantheneBenzo(k)RuorantheneBenzo(a) Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a, h) AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Ruorophenol2,4,6-Tribromophenol
.
< 3.23< 10.75< 3.23< 2.15 .< 6.45 |< 10.75< 2.15< 43.01< 21.51< 6.45< 6.45< 2.15< 6.45< 3.23< 21.51< 21.51< 3.23< 6.45< 5.38< 21.51< 2.15< 2.15< 1.08< 2.15< 2.15< 3.23 4< 10.75 f< 3.23< 3.23< 2.15< 2.15< 10.75< 10.75< 6.45< 10.75< 10.75< 10.75
PERCENT RECOVERY
85.10%78.60%53.30%
25.50%35.30%55.70%
Page2 AR0020I6
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90 DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample_______ METHOD NO.: EPA 608
ANALYST: M. Cooper_________ LAB NOTEBOOK NO.: 158, Pg. 78
CUSTOMER SAMPLE NO.: ISO-0 EHRT SAMPLE NO.: 30259
RESULTCOMPOUNDS ug/L
1. AIpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin ' < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.000318. Chlordane < 0.2019. Toxaphene < 3.00
Page1 SR0020I7
CUSTOMER SAMPLE NO.: ISO-0____________ EHRT SAMPLE NO.: 30259
20. Aroclor-1016 < 0.5021. Aroclor-1221 < 0.5022. Aroclor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 < 0.5025. Aroclor-1254 < 0.5026. Aroclor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - 55.6%
Page2
ENVIRONMENTAL HEALTH Rfci>tAHCH AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
AMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90______________ DATE ANALYZED: 12-17-90
SAMPLE TYPE: Water Sample___________ SAMPLE VOLUME: 900.00
ANALYST: K. Nusekabel __________________ FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: ISO-0.1A ________ EHRT SAMPLE NO.: 30260
LAB NOTEBOOK NO.: 166. Pg. 16____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1. Phenol < 5.562. Bis(2-Chloroethyl)Ether < 2.223. 2-Chlorophenol < 2.224. 1,3-Dichlorobenzene < 6.675. 1,4-Dichlorobenzene < 6.676. Benzyl Alcohol < 3.337. 1,2-Dlchlorobenzene < 6.678. 2-Methylphenol < 3.339. Bis-(2-Chloroisopropyl) Ether < 4.4410. 4-Methylphenol < 3.3311. N-Nitroso-Di-n-Propylamine < 4.4412. Hexachloroethane < 6.6713. Nitrobenzene < 3.3314. Isophorone < 2.2215. 2-Nrtrophend < 4.4416. 2,4-Dimethylphenol < 3.3317. Benzole Acid < 22.2218. Bis(2-Chloroethoxy)Methane < 2.2219. 2,4-Dichlorophenol < 4.4420. 1,2,4-Trichlorobenzene < 6.6721. Naphthalene < 1.1122. 4-Chloroaniline < 11.1123. Hexachlorobutadiene < 13.3324. 4-Chloro-3-Methylphenol < 3.3325. 2-Methylnaphthalene < 1.1126. Hexachlorocyclopentadiene < 13.3327. 2,4,5-Trichlorophenol < 5.5628. 2,4,6-Trichlorophend < 5.56
/JR0020I9
CUSTOMER bAMr^LC Nu.. IOUHJ.IA_______________ cnm OMMru_ i\u.. ou<>bU
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethyiphthalateAcenaphthylene2,6-Dinitrotduene3-NitroanilIneAcenaphthene2,4-Dinitrophend4-NitrophendDibenzofuran2,4-DinitrotdueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinrtrc~2-MethylphendN-Nitrosodiphenyiamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButyiphthalateRuoranthenePyreneButyl benzyiphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b)RuorantheneBenzo(k)RuorantheneBenzo(a)Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g, h,i) Perylene
SURROGATE COMPOUND
Nftrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Ruorophend2,4,6-Tribromophenol
< 3.33< 11.11< 3.33< 2.22< 6.67 i< 11.11< 2.22< 44.44< 22.22< 6.67< 6.67< 2.22< 6.67< 3.33< 22.22< 22.22< 3.33< 6.67< 5.56< 22.22< 2.22< 2.22< 1.11< 2.22< 2.22< 3.33 .< 11.11 |< 3.33< 3.33< 2.22< 2.22< 11.11< 11.11< 6.67< 11.11< 11.11< 11.11
PERCENT RECOVERY
72.40%73.90%37.00%
21.90%31.10%64.80%
_l
Page2 3R002020
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90 DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample________ METHOD NO.: EPA 608
ANALYST: M. Cooper__________ LAB NOTEBOOK NO.: 158, Pg. 78
CUSTOMER SAMPLE NO.: ISO-0.1/f &________ EHRT SAMPLE NO.: 30261
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxkte < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.000318. Chlordane < 0.2019. Toxaphene < 3.00
Pagel flR00202l
CUSTOMER SAMPLE NO.: ISO-0.1 A___________ EHRT SAMPLE NO.: 30261
20. Arodor-1016 < 0.5021. Aroclor-1221 < 0.5022. Aroclor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 < 0.5025. Aroclor-1254 < 0.5026. Arodor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate -111.4%
Page2 AR002022
n ni_.j«-..rMion MI*U ^SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
MPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A______________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90______________ DATE ANALYZED: 12-17-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 900.00
ANALYST: K. Nusekabel___________ FINAL VOLUME: • ___1J)0
CUSTOMER SAMPLE NO.: ISO-0.5A __________ EHRT SAMPLE NO.: 30262
LAB NOTEBOOK NO.: 166. Pg. 16____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1. Phend < 5.562. Bis(2-Chloroethyl)Ether < 2.223. 2-Chlorophend < 2.224. 1,3-Dichlorobenzene < 6.675. 1,4-Dichlorobenzene < 6.676. Benzyl Alcohd < 3.337. 1,2-Dichlorobenzene < 6.678. 2-Methylphend < 3.339. Bis-(2-Chloroisopropyi) Ether < 4.4410. 4-Methylphend < 3.3311. N-Nitroso-Di-n-Propylamine < 4.4412. Hexachloroethane < 6.6713. Nitrobenzene < 3.3314. Isophorone < 2.2215. 2-Nttrophend < 4.4416. 2,4-Dimethylphend < 3.3317. Benzole Acid < 22.2218. Bis(2-Chloroethoxy)Methane < 2.2219. 2,4-Dichlorophenol < 4.4420. 1,2,4-Trichlorobenzene < 6.6721, Naphthalene < 1.1122. 4-Chloroaniline < 11.1123. Hexachlorobutadiene < 13.3324. 4-Chloro-3-Methylphenol < 3.3325. 2-Methylnaphthalene < 1.1126. Hexachlorocyclopentadiene < 13.3327. 2,4,5-Trichlorophend < 5.5628. 2,4,6-Trichlorophend < 5.56
CUSTOMER bAMri-n iNu.. IOU-U.OA_______________ cnm oMMru_
29. 2-Chloronaphthalene < 3.3330. 2-Nitroaniline < 11.1131. Dimethyiphtnalate < 3.3332. Acenaphthylene < 2.2233. 2,6-Dinitrotduene < 6.6734. 3-Nitroanitine < 11.1135. Acenaphthene < 2.2236. 2,4-Dinitrophend < 44.4437. 4-Nitrophend < 22.2238. Dibenzofuran < 6.6739. 2,4-Dinitrotduene < 6.6740. Diethylphthalate < 2.2241. 4-Chlorophenyl-Phenylether < 6.6742. Ruorene < 3.3343. 4-Nttroaniline < 22.2244. 4,6-Dinitro-2-Methylphend < 22.2245. N-Nitrosodiphenylamine < 3.3346. 4-Bromophenyl-Phenyiether < 6.6747. Hexachlorobenzene < 5.5648. Pentachlorophend < 22.2249. Phenanthrene < 2.2250. Anthracene < 2.2251. Di-n-Butylphthalate < 1.1152. Ruoranthene < 2.2253. Pyrene • < 2.2254. Butyibenzylphthalate < 3.3355. 3,3'-Dichlorobenzidine < 11.1156. Benzo(a)Anthracene < 3.3357. Chrysene < 3.3358. Bis(2-Ethylhexyl)Phthalate < 2.2259. Di-n-Octylphthalate < 2.2260. Benzo(b)Ruoranthene < 11.1161. Benzo(k)Ruoranthene < 11.1162. Benzo(a)Pyrene < 6.6763. lndeno(1,2,3-cd)Pyrene < 11.1164. Dibenzo(a,h)Anthracene < 11.1165. Benzo(g,h,i)Perylene < 11.11
SURROGATE COMPOUND PERCENT RECOVERY
NHrobenzene-d5 84.90%2-Ruorobiphenyl 77.80%Terphenyl-d14 83.50%
Phend-d5 23.00%2-Ruorophend 37.40%2,4,6-Tribromophend 66.00%
Page 2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS. INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90________________ DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample_______ METHOD NO.: EPA 608
ANALYST: M. Cooper_________ LAB NOTEBOOK NO.: 158, Pg. 78
CUSTOMER SAMPLE NO.: ISO-0.5B __ EHRT SAMPLE NO.: 30263
RESULTCOMPOUNDS ug/L
1. Alpha-BHC . < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.000318. Chlordane < 0.2019. Toxaphene < 3.00
Page1 ARQG2025
CUSTOMER SAMPLE NO.: ISO-0.5B__________ EHRT SAMPLE NO.: 30263
20. Arodor-1016 < 0.5021. Arodor-1221 < 0.5022. Arodor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 < 0.5025. Arodor-1254 < 0.5026. Aroclor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - 69.7%
page2 . flR002026
i AL. no\L.m tteoeMrtun MINIU » co i UMU,SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
MPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A_____________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90_______________ DATE ANALYZED: 12-18-90
SAMPLE TYPE: Water Sample___________ SAMPLE VOLUME: 900.00
ANALYST: K. Nusekabel FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: ISO-1 .OA EHRT SAMPLE NO.: 30264
LAB NOTEBOOK NO.: 166, Pg. 16______________ METHOD NO.: EPA 625
RESULTCOMPOUNDS___________ ug/L
1. Phend < 5.562. Bis(2-Chloroethyi)Ether < 2.223. 2-Chlorophend < 2.224. 1,3-Dichlorobenzene < 6.675. 1,4-Dichlorobenzene < 6.676. Benzyl Alcohd < 3.337. 1,2-Dichlorobenzene < 6.678. 2-Methylphend < 3.339. Bis-(2-Chloroisopropyl) Ether < 4.4410. 4-Methyiphend < 3.3311. N-Nitroso-Di-n-Propylamine < 4.4412. Hexachlorciethane < 6.6713. Nitrobenzene < 3.3314. Isophorone < 2.2215. 2-N'rtrophend < 4.4416. 2,4-Dimethylphend < 3.3317. Benzole Acid < 22.2218. Bis(2-Chloroethoxy) Methane < 2.2219. 2,4-Dichlorophend < 4.4420. 1,2,4-Trichlorobenzene < 6.6721. Naphthalene < 1.1122. 4-Chloroaniline < 11.1123. Hexachlorobutadiene < 13.3324. 4-Chloro-3-Methylphend < 3.3325. 2-Methyinaphthalene < 1.1126. Hexachlorocyclopentadiene < 13.3327. 2,4,5-Trichlorophend < 5.5628. 2,4,6-Trichlorophend < 5.56
Pagel fi R 0 Q 2 0 2 7
CUSTOMER SAMPLE NO,: ISQ-1.0A______________ EHRT SAMPLE NO.: 30264
29. 2-Chloronaphthalene < 3.3330. 2-Nitroaniline < 11.1131. Dimethylphthalate < 3.3332. Acenaphthylene < 2.2233. 2,6-DInitrotduene < 6.6734. 3-Nitroaniline < 11.1135. Acenaphthene < 2.2236. 2,4-Dinttrophend < 44.4437. 4-Nitrophend < 22.2238. Dibenzofuran < 6.6739. 2,4-Dinitrotduene < 6.6740. Diethylphthalate ' < 2.2241. 4-Chlorophenyl-Phenylether < 6.6742. Ruorene < 3.3343. 4-Nitroaniline < 22.2244. 4,6-Dinitro-2-Methylphend < 22.2245. N-Nitrosodiphenylamine < 3.3346. 4-Bromophenyl-Phenylether < 6.6747. Hexachlorobenzene < 5.5648. Pentachlorophend < 22.2249. Phenanthrene < 2.2250. Anthracene < 2.2251. Di-n-Butylphthalate < 1.1152. Ruoranthene < 2.2253. Pyrene < 2.2254. Butylbenzyiphthalate < 3.3355. 3,3'-Dichlorobenzidine < 11.1156. Benzo(a)Anthracene < 3.3357. Chrysene < 3.3358. Bis(2-Ethylhexyl)Phthalate < 2.2259. Di-n-Octylphthalate < 2.2260. Benzo(b)Ruoranthene < 11.1161. Benzo(k) Ruoranthene < 11.1162. Benzo(a) Pyrene < 6.6763. lndeno(1,2,3-cd)Pyrene < 11.1164. Dibenzo(a,h)Anthracene < 11.1165. Benzo(g,h,i)Perylene < 11.11
SURROGATE COMPOUND PERCENT RECOVERY
Nftrobenzene-d5 64.70%2-Ruorobiphenyl 60.00%Terphenyi-d14 50.00%
Phenol-d5 29.80%2-Ruorophend 38.60%2,4,6-Tribromophend 76.30%
Page2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCS ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS, INC.
SAMPLE SOURCE: Blosenski Landfill
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90__________ DATE ANALYZED: 12-14-90
SAMPLE TYPE: Water Sample________ METHOD NO.: EPA 608
ANALYST: M. Cooper__________ LAB NOTEBOOK NO.: 158, Pg. 78
CUSTOMER SAMPLE NO.: ISO-1 .OB ___ EHRT SAMPLE NO.: 30265
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.000318. Chlordane < 0.2019. Toxaphene < 3.00
Pagel flR002029
CUSTOMER SAMPLE NO.: ISO-1 .OB__________ EHRT SAMPLE NO.: 30265
20. Aroclor-1016 < 0.5021. Arodor-1221 < 0.5022. Aroclor-1232 < 0.5023. Arodor-1242 < 0.5024. Aroclor-1248 < 0.5025. Arodor-1254 < 0.5026. Arodor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - 84.7%
AR00203Q
I CO
SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: O'BRIEN & GERE ENGINEERS. INC.
AMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A________________ EHRT PROJECT NO.: 12444
DATE EXTRACTED: 12-14-90______________ DATE ANALYZED: 12-17-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 690.00
ANALYST: K. Nusekabel FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: Field Blk. #1 ______ EHRT SAMPLE NO.: 30266
LAB NOTEBOOK NO.: 166. Pg. 16____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS___________ ug/L
1. Phend < 7.252. Bis(2-Chloroethyl)Ether < 2.903. 2-Chlorophend < 2 904. 1,3-Dichlorobenzene < 8.705. 1,4-Dichlorobenzene < 8.706. Benzyl Alcohd < 4.357. 1,2-Dichlorobenzene < 8.70"8. 2-Methylphend < 4.359. Bis-(2-Chloroisopropyl)Ether < 5.8010. 4-Methylphend < 4.3511. N-Nitroso-Di-n-Propylamine < 5.8012. Hexachloroethane < 8.7013. Nitrobenzene < 4.3514. Isophorone < 2.9015. 2-Nitrophend < 5.8016. 2,4-Dimethylphend < 4.3517. Benzole Acid < 28.9918. Bis(2-Chloroethoxy)Methane < 2.9019. 2,4-Dichlorophend < 5.8020. 1,2,4-Trichlorobenzene < 8.7021. Naphthalene < 1.4522. 4-Chloroaniline < 14.4923. Hexachlorobutadiene < 17.3924. 4-Chloro-3-Methylphend < 4.3525. 2-Methylnaphthalene < 1.4526. Hexachlorocyclopentadiene < 17.3927. 2,4,5-Trichlorophend < 7.2528. 2,4,6-Trichlorophend < 7.25
Page1 flR00203l
CUSTOMER SAMPLE NO.: Field Blk. #1____________ EHRT SAMPLE NO.: 30266
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotduene3-NitroanilineAcenaphthene2,4-Dinitrophend4-NitrophendDibenzofuran2,4-DlnitrotdueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinitro-2-MethylphendN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButylphthalateRuoranthenePyreneButyl benzyiphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b) RuorantheneBenzo(k) RuorantheneBenzo(a) PyreneIndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g, h, i) Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Ruorophend2,4,6-Tribromophenol
< 4.35< 14.49< 4.35< 2.90 |< 8.70 "< 14.49< 2.90< 57.97< 28.99< 8.70< 8.70< 2.90< 8.70< 4.35< 28.99< 28.99< 4.35< 8.70< 7.25< 28.99< 2.90< 2.90< 1.45< 2.90< 2.90< 4.35 |< 14.49 *4< 4.35'< 4.35< 2.90< 2.90< 14.49< 14.49< 8.70< 14.49< 14.49< 14.49
PERCENT RECOVERY
97.30%94.20%57.40%
50.00%66.00%97.40% l
flROQ2032
Environmental Health Research and Testing, Inc.
3235 Omni Drive Cincinnati, Ohio 45245 (513) 752-2950 FAX (513) 752-2261
November 21,1990
OBG LABORATORIES, INC.ATTN: Mr. Michael Petterelli5000 Brittonfield Parkway, Suite 300P.O. Box 4942Syracuse, New York 13221
Dear Mr. Petterelli:
Please find enclosed the results of analysis for the 4 samples received on November 8,1990; andthe 25 samples received on November 9,1990.
If you have any further questions, please feel free to contact me at (513) 752-2950.
Sincerely,
Mona Risk, Ph.D.Director of Chemistry A\& 5T#|f?£&
Enclosures
NOV 26 1990OBG I_ABS, INC.SYRACUSE, N.Y.
NATIONAL OFFICES
Cincinnati, Ohio • Lexington, Kentucky • Research Triangle Park, North Carolina •Denver, Colorado • Birmingham, Alabama • Philadelphia, Pennsylvania • San Francisco, California • Miami, Florida r\ r\ O pj O O
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY:
LOCATION:
SAMPLED BY:
ORGANIZATION:
-
J
STATIONNUMBER SAMPLE LOCATION DATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONFAINERS
ANALYSISREQUIRED
MOD "Z,
bo.
-t:- i
r «)
(
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: DATE TIME _, JJeceived by Laboratory: DATE TIME-Ofc
^ <K M.r. /^uUeX P- c a, ^ 0&& LA^6l
METHOD OF SHIPMENT:P^Arhi fex nrcw, Ovt .
0 J
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-0200 SRQ02Q3l|
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill ____
WORK ORDER NO.: N/A__________ PROJECT NO.: 12307
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-09-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-I-150D EHRT SAMPLE NO.: 29358
LAB NOTEBOOK NO.: 162. Pg. 9-12_____ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride 19.765. Chlorobenzene 17.556. Chloroethane 7.537. 2-Chloroethylvinyl Ether < 0.508. Chloroform 132.279. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 49.8216. 1,2-Dichloroethane 0.8417. 1,1-Dichloroethene 14.8918. trans-1,2-Dichloroethene 137.0319. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
flR002035
CUSTOMER SAMPLE NO.: AS-I-150D _____ EHRT SAMPLE NO.: 29358
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene 1.2925. 1,1,1-Trichloroethane 117.4826. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 59.0028. Trichlorofluoromethane < 0.5029. Vinyl Chloride 13.7930. Benzene 1290.0031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____94.00%
Toluene-d8 - 99.00%
Bromofluorobenzene - 97.00%
COMPUTER SEARCH
Trichlorotrifluoroethane - Approx 46.95
flR002036
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. • MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill_________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12307
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-09-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-150D_______ EHRT SAMPLE NO.: 29359A
LAB NOTEBOOK NO.: 162. Pg. 9-12_____ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.866. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 11.709. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 3.2116. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 9.8119. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
SR002037
CUSTOMER SAMPLE NO.: AS-E-150D_______ EHRT SAMPLE NO.: 29359A
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1 -Trichloroethane 6.3326. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 3.0028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 81.6731. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - _____99.00%
Toluene-d8 - 102.00%
Bromofluorobenzene - 98.00%
SROQ2038
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLIiI
SAMPLE SOURCE: Blosenski Landfill _________________________________________________________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12307
DATE EXTRACTED: N/A___________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: ; Water Duplicate SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-150D EHRT SAMPLE NO.: 29359B
LAB NOTEBOOK NO.: 162, Pg. 9-12_____ METHOD NO.: EPA 601 &602
RESULTCOMPOUNDS ug/L
Bromodichloromethane < 0.50Bromoform < 0.50Bromomethane < 0.50Carbon Tetrachloride < 0.50Chlorobenzene 1.55Chloroethane < 0.502-Chloroethylvinyl Ether < 0.50Chloroform 10.35
9. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.9016. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 9.3019. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichlo.ropropene < 0.5022. Methyiene Chloride < 1.00
flR002039
CUSTOMER SAMPLE NO.: AS-E-150D_______ EHRT SAMPLE NO.: 29359B
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 7.1826. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 4.9828. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 80.8531. Ethylbenzene " < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
l,2-Dichloroethane-d4 - ____96.00%
Toluene-d8 - 93.00%
Bromofluorobenzene - 103.00%
AR0020W
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill__________________________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12307
DATE EXTRACTED: N/A_________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-150 EHRT SAMPLE NO.: 29360
LAB NOTEBOOK NO.: 162, Pg. 9-12_____ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 17.356. Chloroethane 7.047. 2-Chloroethylvinyl Ether < 0.508. Chloroform 128.599. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1 -Dichloroethane 47.8316. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene 14.0218. trans-1,2-Dichloroethene 130.8119. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Pagel AR0020M
CUSTOMER SAMPLE NO.: AS-l-150________ EHRT SAMPLE NO.: 29360
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene 1.2725. 1,1,1-Trichloroethane 112.9126. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 56.8328. Trichlorofluoromethane < 0.5029. Vinyl Chloride 12.5430. Benzene 1022.0031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - _____98.00%
Toluene-d8 ' - 98.00%
Bromofluorobenzene - 99.00%
fiR002Ql*2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
AMPLE SOURCE: Blosenski Landfill_______________________
WORK ORDER NO.: N/A_________________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-12-90______________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 500.00
ANALYST: K. Nusekabel____________ FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: AS-l-150___________ EHRT SAMPLE NO.: 29360
LAB NOTEBOOK NO.: 149. Pg. 83_____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1-. Phenol < 6.002. Bis(2-Chloroethyl)Ether < 4.003. 2-Chlorophenol < 4.004. 1,3-Dichlorobenzene < 12.005. 1,4-Dichlorobenzene -< 12.006. Benzyl Alcohol < 6.007. 1,2-Dichlorobenzene < 12.008. 2-Methylphenol < 6.009. Bis-(2-Chk>roisopropyl) Ether < 8.0010. 4-Methylphenol < 6.0011. N-Nitroso-Di-n-Propylamine < 8.0012. Hexachloroethane < 12.0013. Nitrobenzene < 6.0014. Isophorone < 4.0015. 2-Nitrophenol < 8.0016. 2,4-Dimethylphenol < 6.0017. Benzole Acid < 40.0018. Bis(2-Chloroethoxy)Methane < 4.0019. 2,4-Dichlorophend < 8.0020. 1,2,4-Trichlorobenzene < 12.0021. Naphthalene < 2.0022. 4-Chloroaniline < 20.0023. Hexachlorobutadiene < 24.0024. 4-Chloro-3-Methylphenol < 6.0025. 2-Methylnaphthalene < 2.0026. Hexachlorocyclopentadiene < 24.0027. 2,4,5-Trichlorophenol < 10.0028. 2,4,6-Trichlorophenol < 10.00
flR002LH3
CUSTOMER SAMPLE NO.: AS-l-150______________ EHRT SAMPLE NO.: 29360
29.30.31.32.33.34.35.36.37.38.39.40.
' 41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NrtroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroaniiineAcenaphthene2,4-Dinitrophend4-NitrophendDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-NKroaniiine4,6-Dinitro-2-MethvlphendN-Nftrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthenePyreneButyl benzylphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b)RuorantheneBenzo(k)RuorantheneBenzo(a)Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-FluorobiphenylTerphenyl-d14
Phend-d52-Fluorophend2,4,6-Tribromophenol
< 6.00< 20.00< 6.00 |< 4-00 "< 12.00< 20.00< 4.00< 80.00< 40.00< 12.00< 12.00< 4.00< 12.00< 6.00< 40.00< 40.00< 6.00< 12.00< 10.00< 40.00< 4.00< 4.00< 2.00< 4.00< 4.00 4< 6.00 ™< 20.00< 6.00< 6.00
6.92< 4.00< 20.00< 20.00< 12.00< 20.00< 20.00< 20.00
PERCENT RECOVERY
58.50%52.70%37.10%
10.00% *10.00% *18.30% 1
k A low recovery was obtained on the phend surrogates. The surrogate recovery was also very low on the matrixspike and matrix spike duplicate. The sample matrix is probably responsible for these low recoveries since itreproduces on 3 analyses of the same sample. paae 2
AR0020H
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. • MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill________________________________
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-09-90 DATE ANALYZED: 11-09-90
SAMPLE TYPE: Water Sample_______ METHOD NO.: EPA 608
ANALYST: M. Cooper_________ LAB NOTEBOOK NO.: 158. Pg. 54
CUSTOMER SAMPLE NO.: AS-l-150 EHRT SAMPLE NO.: 29360
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC . < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.0418. Chlordane < 0.2019. Toxaphene < 3.00
CUSTOMER SAMPLE NO.: AS-l-150___________ EHRT SAMPLE NO.: 29360
20. Aroclor-1016 < 0.5021. Aroclor-1221 < 0.5022. Aroclor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 < 0.5025. Aroclor-1254 < 0.5026. Aroclor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - ____99.00%
Page2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. • MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill___________________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12307
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-13-50
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-150 EHRT SAMPLE NO.: 29361
LAB NOTEBOOK NO.: 162, Pg. 9-12______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS_____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.686. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 10.259. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.9916. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 9.3319. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
CUSTOMER SAMPLE NO.: AS-E-150________ EHRT SAMPLE NO.: 29361
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1 -Trichloroethane 7.2026. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 3.4128. Trichlorofluoromethane . . < 0.5029. Vinyl Chloride < 0.5030. Benzene 82.3031. Ethylbenzene < 0.5032. Tduene 0.76
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____100.00%
Tduene-d8 - 93.00%
Bromofluorobenzene - 103.00%
Page2
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
'AMPLE SOURCE: Blosenski Landfill_________________________
WORK ORDER NO.: N/A_________________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-12-90_______________ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 1000.00
ANALYST: K. Nusekabel FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: AS-E-150 EHRT SAMPLE NO.: 29361
LAB NOTEBOOK NO.: 149, Pg. 83_____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1. Phend < 3.002. Bis(2-Chloroethyi)Ether < 2.003. 2-Chlorophend < 2.004. 1,3-Dichlorobenzene < 6.005. 1,4-Dichlorobenzene < 6.006. Benzyl Alcohol < 3.007. 1,2-Dichlorobenzene < 6.008. 2-Methylphend < 3.009. Bis-(2-Chloroisopropyl)Ether < 4.0010. 4-Methylphend < 3.0011. N-Nitroso-Di-n-Propylamine < 4.0012. Hexachloroethane < 6.0013. Nitrobenzene < 3.0014. Isophorone < 2.0015. 2-Nitrophend < 4.0016. 2,4-DImethyl phenol < 3.0017. BenzoicAcid < 20.0018. Bis(2-Chloroethoxy) Methane < 2.0019. 2,4-Dichlorophenol < 4.0020. 1,2,4-Trichlorobenzene < 6.0021. Naphthalene < 1.0022. 4-Chloroaniline < 10.0023. Hexachlorobutadiene < 12.0024. 4-Chloro-3-Methylphenol < 3.0025. 2-Methylnaphthalene < 1.0026. Hexachlorocyclopentadiene < 12.0027. 2,4,5-Trichlorophend <. 5.0028. 2,4,6-Trichlorophenbl < 5.00
Page1 ftR0020l*9
CUSTOMER SAMPLE NO.: AS-E-150_______________ EHRT SAMPLE NO.: __29361
29.30.
^ 31.B 32.
33.34.35.36.37.38.39.40.
' 41.42.43.44.45.46.47.48.49.50.51.52.
S:55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroaniiineAcenaphthene2,4-Dinitrophenol4-NltrophendDibenzofuran2,4-DinitrotdueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinitro-2-MethylphenolN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthenePyreneButyl benzylphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl) PhthalateDi-n-OctylphthalateBenzo(b)RuorantheneBenzo(k) RuorantheneBenzo(a) Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Fluorophend
^ 2,4,6-Tribromophenol
< 3.00< 10.00< 3.00< 2.00< 6.00< 10.00< 2.00< 40.00< 20.00< 6.00< 6.00< 2.00< 6.00< 3.00< 20.00< 20.00< 3.00< 6.00< 5.00< 20.00< 2.00< 2.00< 1.00< 2.00< 2.00< 3.00< 10.00< 3.00< 3.00< 2.00< 2.00< 10.00< 10.00< 6.00< 10.00< 10.00< 10.00
PERCENT RECOVERY
72.00%57.40%50.90%
10.00% *10.00% *12.20%
A low recovery was obtained on the phend surrogates due to the sample matrix.
Page2 flR002050
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill________________
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-09-90 _____ __ DATE ANALYZED: 11-09-90
SAMPLE TYPE: Water Sample_______ METHOD NO.: EPA 608
ANALYST: M. Cooper_________ LAB NOTEBOOK NO.: 158. Pg. 54
CUSTOMER SAMPLE NO.: AS-E-150 EHRT SAMPLE NO.: 29361
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.0418. Chlordane < 0.2019. Toxaphene < 3.00
Page1 flR00205l
£usSTOMER SAMPLE NO.: AS-E-150__________ EHRT SAMPLE NO.: 29361
20. Aroclor-1016 < 0.5021. Aroclor-1221 < 0.5022. Aroclor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 < 0.5025. Aroclor-1254 < 0.5026. Aroclor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - ____166.00%
flR002052
c MMirtiAorii\<_/MMiriiA i>rif\c uuruwMe rttouvcm
Lab Name: Environmental Health Research & Testing, Inc.
Customer Name: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI__________________
Project No.: 12307_________ Method No.: EPA 625_____
Customer Sample No.: AS-l-150______ EHRT No.: 29360
COMPOUNDPhenol2-Chlorophenol1 ,4-DichlorobenzeneN-Nitroso-di-n-Propylamine1 ,2,4-Trichlorobenzene4-Chloro-3-MethylphenolAcenaphthene4-Nitrophenol2,4-DinitrotoluenePentachlorophendPyrene
SPIKE ADDED(ng)200200100100100200100200100200100
SAMPLE CONC.(ug/L)0.000.000.000.000.000.000.000.000.000.000.00
MS CONC.(ug/L)16.9457.9463.3779.9562.327.2163.0678.9569.5759.4449.57
MS%REC#8.5*29.063.480.062.33.6*63.139.569.629.749.6
QC LIMITSREG.12-8927-12336-9741-11639-9823-9746-11810-8024-969-10326-127
COMPOUNDPhenol2-Chlorophenol1 ,4-DichlorobenzeneN-Nitroso-di-n-Propylamine1 ,2,4-Trichlorobenzene4-Chloro-3-MethylphenolAcenaphthene4-Nitrophend2,4-DinitrotoluenePentachlorophendPyrene
MSD CONC.(ug/L)19.2253.4456.6570.6056.725.7156.7479.3566.0360.4449.76
MSD%REC#9.6*26.7*56.770.656.72.9*56.739.766.030.249.8
MS%REC#8.5*29.063.380.062.33.6*63.139.569.629.749.6
%RPD#12.18.311.012.59.421.511.00.515.31.70.40
QCLJRPD4240283828423150385031
vllTS RECJH12-89~127-12336-9741-11639-9823-9746-11810-8024-969-10326-127
# Column to be used to flag recovery and RPD values with an asterick* Values outside of QC limits
COMMENTS:
RPD: 0:overy: 7
out of 11 outside limitsout of 22 outside limits
flR002053
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
AMPLE SOURCE: Blosenski Landfill___________________________
WORK ORDER NO.: N/A________________ EHRT PROJECT NO.: 12307
DATE EXTRACTED: 11-12-90 _______ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Blank _____ SAMPLE VOLUME: 1000.00
ANALYST: K. Nusekabel FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: N/A_________________ EHRT SAMPLE NO.: N/A
LAB NOTEBOOK NO.: 149, Pg. 83_____________ METHOD NO.: EPA 625
RESULTCOMPOUNDS__________ ug/L
1. Phend < 3.002. Bis(2-Chloroethyl)Ether < 2.003. 2-Chlorophend < 2.004. 1,3-Dichlorobenzene < 6.005. 1,4-Dichlorobenzene < 6.006. Benzyl Alcohd < 3.007. 1,2-Dichlorobenzene < 6.008. 2-Methylphend < 3.009. Bis-(2-Chloroisopropyl)Ether < 4.0010. 4-Methylphend < 3.0011. N-Nftroso-Di-n-Propylamine < 4.0012. Hexachloroethane < 6.0013. Nitrobenzene < 3.0014. Isophorone < 2.0015. 2-Nitrophend < 4.0016. 2,4-Dimethylphend < 3.0017. BenzoicAcid < 20.0018. Bis(2-Chloroethoxy)Methane < 2.0019. 2,4-Dichlorophenol < 4.0020. 1,2,4-Trichlorobenzene < 6.0021. Naphthalene < 1.0022. 4-Chloroaniline < 10.0023. Hexachlorobutadiene < 12.0024. 4-Chloro-3-Methylphenol < 3.0025. 2-Methyinaphthalene < 1.0026. Hexachlorocyclopentadiene < 12.0027. 2,4,5-Trichlorophend < 5.0028. 2,4,6-Trichlorophend < 5.00
flR00205l*
CUSTOMER SAMPLE NO.: N/A_________________ EHRT SAMPLE NO.: N/A
29.30.31.32.33.34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.53.54.55.56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotduene3-NitroanilineAcenaphthene2,4-Dinitrophend4-NitrophendDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-Nitroaniline4,6-Dinttro-2-MethylphendN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButyphthalateFluoranthenePyreneButyl benzylphthalate3,3'-Dlchlorobenz!dineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b) RuorantheneBenzo(k) RuorantheneBenzo(a)Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-FluorobiphenylTerphenyl-d14
Phenol-d52-Ruorophend2,4,6-Tribromophenol
< 3.00< 10.00< 3.00 A< 2.00 1< 6.00< 10.00< 2.00< 40.00< 20.00< 6.00< 6.00< 2.00< 6.00< 3.00< 20.00< 20.00< 3.00< 6.00< 5.00< 20.00< 2.00< 2.00< 1.00< 2.00< 2.00 M< 3.00 ^< 10.00< 3.00< 3.00< 2.00< 2.00< 10.00< 10.00< 6.00< 10.00< 10.00< 10.00
PERCENT RECOVERY
67.20%43.40%41.70%
26.60%43.90%79.50% ^
Page2 SR002055
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A PROJECT NO.: 12307 *
ANALYSIS PERFORMED: 5-Dav BOD Analysis
ANALYSIS METHOD: EPA 405.1
ANALYST: G. Stake
DATE ANALYZED: 1 1 /08-1 3/90
LAB NOTEBOOK NO.: 161, Pg. 6
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360 AS-l-150
29361 A AS-E-150
29361 B AS-E-150(Duplicate)
RESULTSmg/L
BDL
BDL
BDL
DETECTION LIMIT: < 2 mg/L
flR002056
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A
Total Suspended Solid Analysis
Std. Method 209C
M. Reddy
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360 AS-l-150
29361 AS-E-150
PROJECT NO.: 12307
--
DATE ANALYZED: 1 1 -1 2-90
LAB NOTEBOOK NO. : 1 37, Pg. 61
RESULTSmg/L
BDL
BDL
DETECTION LIMIT: < 10 mg/L
Page1 SR002057
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: QBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill______________________
WORK ORDER NO.: N/A____________ PROJECT NO.: 12307
ANALYSIS PERFORMED: Ammonia Analysis_______________________
ANALYSIS METHOD: EPA 350.1 DATE ANALYZED: 11-14-90
ANALYST:
SAMPLEEHRT NO.
29360A
29360B(Duplicate)
29361
K. Nusekabel
NO.CUSTOMER NO.
AS-l-150
AS-l-150
AS-E-150
LAB NOTEBOOK NO.: 161, Pg. 12
RESULTSmg/L
BDL
BDL
BDL
DETECTION LIMIT: < 0.10 mg/L
Page1 SROG2058
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A
ANALYSIS PERFORMED: Total Kjeldahl Nitrogen
ANALYSIS METHOD: EPA 351.2
ANALYST: K. Nusekabel
PROJECT NO.: 12307
(TKN) Analysis
DATE ANALYZED: 1 1 -21 -90
LAB NOTEBOOK NO.: 161, Pg. 15
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360A AS-l-150
29360B AS-l-150(Duplicate)
29361 AS-E-150
RESULTSmg/L
0.28
0.25
0.20
DETECTION LIMIT: < 0.12 mg/L
AROQ2059
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES,INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A PROJECT NO.: 12307
ANALYSIS PERFORMED: Phosphorus Analysis
ANALYSIS METHOD: EPA 365.2
ANALYST: M. Reddy
DATE ANALYZED: 1 1 -1 3-90
LAB NOTEBOOK NO.: 161, Pg. 10
SAMPLE NO.EHRT NO. CUSTOMER NO.
29630A AS-l-150
29360B AS-I-150(Duplicate)
29361 AS-E-150
RESULTSmg/L
BDL
BDL
BDL
Detection Limit - < 0.01 mg/L
Pagel flRQ02060
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A
Oil & Grease Analysis
EPA 41 3.1
G. Stake
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360 AS-i-150
29361 AS-E-150
PROJECT NO.: 12307
DATE ANALYZED: 1 1 -08-90
LAB NOTEBOOK NO. : 1 61 , Pg. 4
RESULTS(mg/L)
BDL
BDL
Detection Limit: < 10 mg/L
Pagel 3R00206!
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME:
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
Blosenski Landfill
N/A PROJECT NO.: 12307
TOC Analysis
EPA 9060 DATE ANALYZED: 1 1 -09-90
G. Luna LAB NOTEBOOK NO.: 135, Pg. 17
SAMPLE NO. RESULTSEHRT NO. CUSTOMER NO. mg/L
29360 AS-l-150
29361 A AS-E-150
29361 B AS-E-150(Duplicate)
BDL
BDL
BDL
Detection Limit - < 10 mg/L
flR002062
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME:
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
OBG LABORATORIES,
Blosenski Landfill
N/A
COD Analysis
EPA 41 0.4
M. Reddy
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360A AS-l-150
29360B AS-l-150(Duplicate)
29361 AS-E-150
INC. - MR. MIKE PETTERELLJ
PROJECT NO.: 12307
DATE ANALYZED: 1 1 -09-90
LAB NOTEBOOK NO.: 151 , Pg. 25
RESULTSmg/L
57.32
53.94
I101.16
DETECTION LIMIT: < 40 mg/L
Page1 flR002063
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
USTOMER NAME: OBG LABORATORIES. INC. • MR. MIKE PETTERELLIr ••- • •'•••'SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A PROJECT NO.: 12307
ANALYSIS PERFORMED: Chloride Analysis
ANALYSIS METHOD: EPA 325.1
ANALYST: K. Nusekabel
DATE ANALYZED: 1 1 -09-90
LAB NOTEBOOK NO.: 1 61 , Pg. 7
SAMPLE NO.EHRT NO. CUSTOMER NO.
BLANK N/A
29360A AS-l-150
29360B AS-l-150(Duplicate)
•361 AS-E-150
RESULTS(mg/L)
BDL
21.12
21.20
21.85
DETECTION LIMIT: < 4 mg/L
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
Detection Limit - < 5 mg/L
Pagei QR002065
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A
Sulfate Analysis
EPA 375.4
J. Burns
SAMPLE NO.EHRT NO. CUSTOMER NO.
29360 AS-l-150
29361 AS-E-150
PROJECT NO.: 12307
DATE ANALYZED: 1 1 -1 2-90
LAB NOTEBOOK NO.: 161, Pg. 9
RESULTSmg/L
66.9
69.2
U.S. EPA - CLP
COVER PflBE - INORefiNIC ANALYSES DATA PACKAGE
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: DBS.
Lab Code: W88__ Case No.: BLOSE SAS No.: 1£307_ SDB No.: 000000
SOW No. : '_____
EPA Sample No. Lab Sample ID._ASE150_ £9361_____AS1150_ 293G0A___
ASI150D 29360B
Were ICP intere 1 ement corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No N0_
Comments:OB8 LflBORftTORIES - BLOSENSKI LANDFILL DflTE OF ANALYSIS 11-12-90____ICP_S. STAKE_NB157_P623_METHOD_S010/_FURNACE_P. BARNWELL_NB154_PG63.METHOD AS706 SE7740/ CO~LD VAPOR J. RADER NB157 P623 METHOD 7470___
Release of the data contained in this hardcopy data package and in thecomputer-readable data submitted on floppy diskette has been authorized bythe Laboratory Manager or the Manager's de.signee, as verified by thefollowing signature.
Lab Manager:
Date:COVER PAGE - IN ' 7/87
flR002066
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: ENVIR. HEALTH RESEARCH TE
Code: W88 Case No. : BLOSE
-ix (soil/water): WATER
;1 (low/med): ___
slids: ___
Concentration Units (ug/L
or Before:
or After:
ments:
AS-E-150
1ICAS No.11 7429-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-21 7440-47-31 7440-48-41 7440-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-71 7782-49-21 7440-22-41 7440-23-51 7440-28-01 7440-62-21 7440-66-611
Contract: QBG
1 11 ASE150 11 1
SAS No. : 12307_ SDG No. : 000000
Lab Sample ID: 29361 ___
Date Received: 11/08/90
or nig/kg dry weight): UG/L_
1 11 Ana 1 y t e 1 Concent rat ionI 11 Aluminum 11 Ant i rnony 11 Arsenic 11 Bar i urn 11 Bery 1 1 i urn 11 Cadmium 1ICalcium 11 Chromium 11 Cobalt 11 Copper 11 Iron 1I Lead !i Magnesium!1 Manganese 11 Mercury 11 Nickel 11 Pot ass i urn 11 Se 1 en i urn 11 Silver 11 Sod i urn 11 Thai Hum 11 Vanad i urn 1IZinc 11 Cyanide 11 I
Clarity
Clarity
O fYr/U. (Jt
10.72.2
0.401.8
5.3
5.0
10.9
i i1C! Q1 11 1I U II U I1 1I U IIUI1 1IU!1 1I U I1 1I U I1 1
1IM1INRIPIFINRIPIPINRIPINRIPINRIPINRI
I I INRI0. 1
4.6IU!IUI
ICVIIP 1
1 1 INRI2. 11.9
95.5
2.4
IUIIUI1 1I U I1 1IU!
IFIPINRIPINRIP 1
I I INRI
Before :
After:
1 1 1 1
Texture:
Artifacts:
*
v<i/£ — .A LdlovO -$± djJfcJiz& Ji-uLJCt-^
FORM I - IN -7/87
AR002067
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ___________
II ASI150
Lab Name: ENVIR._HEALTH_RESEARCH_TE Contract: OBG_____ I_______
Lab Code: W88__ Case No. : BLOSE SAS No.: 1£307_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 29360A___
Level (low/wed): ___ Date Received: 11/08/90
•/• Solids: ___
Concentration Units (ug/L or rng/kg dry weight): US/L_
1ICAS No.11 7429-90-51 7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 74413-70-21 7440-47-31 7440-48-41 7440-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-71 7782-49-21 7440-22-41 7440-23-51 7440-28-01 7440-62-21 7440-66-611
Color Before:
Color After:
Comments:
1 1 1 11 Analyte IConcentrationlCI Q1 1 1 I1 Alum in urn 11 Ant i rnony 11 Arsenic 1(Barium 11 Bery 1 1 i urn 11 Cadmium 11 Calcium 11 Chromium 1(Cobalt 11 Coooer 11 Iron 11 Lead i(Magnesium!1 Manganese 1! Mercury 1INickel 1! Potassium!1 Selenium 11 Silver 11 Sod i urn 11 Thallium 11 Vanad i urn 1IZinc 11 Cyanide 11 !
Clarity
Clarity
10.7£.2
0.401.8
5.3
5.0
10.9
0. 1
4.6
2.11.9
95.5
2.4
Before:
After:
1 !IUIIUI1 II U IIUII !IUI1 1IU!1 1I U Il_l __1 1IUI __IU I1 1I U IIU!1 1IUI1 1IUI1 11 1
1 1!M I1 1INRIIP 1IF 1INRIIP 1IP 1INRIIP 1INRIIP 1INRIIP 1
__ INRIINRI
__ ICVIIP 1INRIIF 1IP 1INR!IP 1INRIIP 1INRI1 i
Texture:
Artifacts:
AS-I-150
FORM I - IN • 7/87
flR002068
U.S. EPA - CLP
Name: ENVIR. HEALTH RESEARCH
Code: W88 Case No. :
rix (soil/water): WATER
nlids for Sample: ___
Concentration Units
1 i II1 1 Control 1 1lAnalyte 1 Limit 1 1 Sample! 1 I I1 Aluminum 1 I 1
6DUPLICATES
_TE Contract
BLOSE SAS
(ug/L or mg/kg
: OBG
No. : 12307
Level
% Solids for
dry weight) :
1 1 11 1 1
(S) Cl i Duplicate (D) Cl1 1 1
1 1 !1 Antimony 1 60.0 II 10. 7000 IU II1 Arsenic 1 10.0 M1 Barium 1 1 11 Beryllium! 5. 0 1 11 Cadmium i 5. 0 1 1I Calcium 1 1 11 Chromium 1 10. 0 1 11 Cobalt 1 II1 Copper 1 25. 0 1 1I Iron 1 1 IILead 1 5. 0 ! 1IMaanesiuml 1 IIManaanesel 1 11 Mercury 1 0.2111 Nickel 1 40. 0 1 11 Pot ass i urn 1 1 I(Selenium 1 5. 0 1 11 Silver 1 10.0 1 11 Sodium 1 1 11 Thai Hum ! 10. 0 1 11 Vanad i urn 1 1 1IZinc 1 20.0 1 11 Cyanide I 1 11 1 I I
2. 2050 1 U M1 1 1
0. 4000 1 U 1 I
1.8000IUI i1 1 1
5. 3000 IUI I1 1 1
5. 0070 I U I I1 1 1
10. 9000 mi i1 1 I1 1 1
0. 1000 IUI 14. 6000 1 U 1 i
1 1 12. 1420IUI 11.9000 mi i
1 1 195. 5000 I U I I
I 1 12. 4000 I U I I
1 1 1i 1 1
1 110. 7000 IU!2. 20501 UI
1 10.4000IUI1. 80001 UI
1 - i5. 3000 1 U 1
I 15.0070IUI
1 110. 9000IUI
1 11 1
0. 1000IUI4. 6000IUI
1 I2. 1420IUI1.9000IUI
1 195. 5000 1 U 1
1 12. 4000 1 U 1
1 11 1
EPA SAMPLE NO.
1 11 ASI150D 11 1
SDG No. : 000000
(low/rned) : ___
Duplicate: ___
UG/L_
1 M l !1 1 1 I 11 RPD 1 IQI MlI 1 I 1 11 I I INRI1 1 1 IP 11 1 1 IF !1 I I INRI1 I I IP 1I I 1 IP 11 ! I INRI1 1 1 IP 11 II INR!1 1 1 IP 11 I i INRI1 1 1 IP I1 I I INRI1 I I INRI1 1 1 1 CV 11 1 1 IP 11 I i INRI1 1 1 IF 11 1 1 IP 11 II INRI1 N I P !1 I I INRI1 M IP 1! I 1 INRII I I I !
FORM VI - IN 7/87
3R002069
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: ENVIR. HEALTH RESEARCH TE Contract: OBB
Lab Code: W88__ Case No.: BLOSE SAS No.: 1£307_ SDG No.: 000000
Initial Calibration Source: SPEX
Cont i nu ing Ca 1 i brat i on Source : SPE!
Concent rat
l 11 1lAnalyte 11 11 Aluminum 11 Ant i rnony 11 Arsen i c 11 Bar i urn 11 Beryllium!1 Cad mi urn 11 Calcium 11 Chromium I1 Cobalt 1i Cop per I1 Iron 1ILead 1i Magnesium!i Manganese!1 Mercury 1INickel 11 Potassium!1 Se 1 en i urn 1(Silver 11 Sod i urn 1I Thallium tt Vanad i urn 1IZinc 1(Cyanide 11 !
1Initial Calibration 1
True Found '/.R ( 1 ) !1
1500.0 1
50.0 1I
500.0 1
500.0 11
500.0 1
r500.0 1
1500.0 !
1
i5.0 1
500.0 11
10.0 1100.0 1
1
1000.0 11
500.0 11
I
1 1
507.501 101.5147.90! 95.81
1 1476.30! 95.31490. 40 1 98. 1 1
! 1549. 00 1109. 81
! 1489.00! 97.8!
1 I483.201 96.6!
' I 11 1
5.481109.61490.701 98.11
1 110. 50 1105. 0197.101 97.11
I 1946.501 94.61
1 1494.901 99.01
1 11 I
<
ion Units: ug/L
! i 1Continuing Calibration II
True Found 5'.R(1) Found JCR(l) 1 1 MI1 1
1500.0 f
50.0 11
500.0 I
500.0 I
1500.0 1
1500.0 1
1500.0 1
1I
5.3 1500.0 1
120.0 1
100.0 I1
1000.0 11
500.0 1iI
1 1508.301101.7149.801 99.61
I 1471.801 94.41483.601 96.71
1 1548.701109.71
1 1479.801 96.01
i 1478.40! 95.71
1 11 1
5.301106.01483.20! 96.61
1 119.901 99.5196.701 96.71
1 1961.901 96.21
1 1493.701 98.71
I 11 1
1 1 iNR1 IIP1 1 IF1 1 INR1 1 IPI 1 IP1 1 INR1 1 IP1 1 INR1 1 IP1 I INRI 1 IP1 1 1 NR 11 1 INR1 1 1 CV 11 ! IP 11 I I N R I1 1 IF1 1 IP 11 1 INR1 MP I1 1 INR1 IIP 11 ! INR1 M l
(1) Control Limits: Mercury 80-1205 Other Metals 90-1105 Cyanide 85-115
FORM II (PART 1) - IN 7/87
flR002070
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: ENVIR. HEALTH RESEARCH TE Contract: OBG
Lab Code: W88__ Case No.: BLOSE SAS No.: 1£307_ SDG No. : 000000
Initial Calibration Source: SPEX______
Continuing Calibration Source: SPEX_____
Concentration Units: ug/L
1 11 1(Analyte Ii 1(Aluminum 1(Antimony 11 Arsenic 11 Bar i urn 11 Beryllium!(Cadmium 11 Calcium 11 Chromium 11 'Cobalt !(Copper 1llron 1(Lead 1(Magnesium!1 Manganese 11 Mercury 1(Nickel 11 Pot ass i urn 1(Selenium 1(Silver 11 Sod i urn 11 Thai Ii urn _lI Vanadium !(Zinc 1(Cyanide 11 1
InitTrue
12000.
1000._1000.
2000.
5000.
600.
8000.
2000.
2000.
4000.
0
0
0
0
0
0
0
0
0
0
1
ial Calibration 1Found *R ( 1 ) 1
1111176011-1 9881 102611 19191! 5299i1 5811[I1 78471I1 19781i 206511 4135i1
1.001
11
.001
.0011
.00!1
.0011
.501
I.00
1
.001
.001
.001
I
98.
98.102.
96.
106.
96.
98.
98.
103.
103.
I01
11
8!61
10!
101
191
~l1
1111
911
21I
41
1
True
112000.0 I
11
1000.0 1
1000. 0 11
2000.0 11
5000. 0 1i
600.0 i11I
3000.0 111
2000.0 11
2000. 0 11
4000.0 1
1
Continuing CalibrationFound 54R(1) Found 3CRU)
12170.
1017.1074.
1971.
5364.
609.
8090.
_2026.
2118.
4255.
1001101.
I1
001101.
001107.1
00 1 _98.1
001107.
1901101.
1II
001101.1I
001101.i
001105.
001106.
11
1 141 1
1 11 1
7! 141 1
1 I61 1
1 13! 1
1 161 1
1 11 11 1
1! 11 11 1
31 11 1
91 11 1
41 11 11 I
111 M1INRIP-INRIINRIIP IIPJINR!IPJINRIIP 1INRIIP 1INR!INRIINRIIP 1INRIINR!IP 1INRIIP 1INRIIP 1INRI1 1
(1) Control Limits: Mercury 80-1205 Other Metals 90-1105 Cyanide 85-115
FORM II (PART 1) - IN 7/87
4R002071
U.S. EPA - CLP
Lab Name: ENVIR. HEALTH
Lab Code: W88
Preparation
Preparation
i 11 i1 i1 !lAnalyte 11 I1 Aluminum iI Antimony 1! Arsenic 11 Barium I1 Beryllium!(Cadmium 1(Calcium 1(Chromium 1(Cobalt i1 Copper 11 Iron 11 Lead 1! Magnesium!1 Manganese 1i Mercury iI Nickel 11 Potassium!(Selenium 1(Silver 11 Sod i urn ((Thallium 11 Vanad i urn 1(Zinc 1(Cyanide i1 1
3BLANKS
RESEARCH TE Contract: OBG
Case No. : BLOSE SAS No. : 12307
•
SDG No. : 000000
Blank Matrix (soil/water): WATER
Blank Concentration Units (ug/L or rng/kg) : UG/L_
IInitial 1Calib. 1Blank 1(ug/L) Cl
1I 1
10.7 IUI2.2 IU!
1 I0.4 IUI1.8 IUI
I 15.3 IUI
1 15.0 IUI
1 110.9 I I
1 11 1
0.1 IUI4.6 IUI
! 12.1 IU!1.9 IU!
I i9 5 . 5 ( I
1 12. 4 IUI
1 11 I
i 11 1
Cont i nu i ng Ca 1 i brat i on 1 iBlank (ug/L) i 1
1 C 2 C 3 CM1 I
I I I I I I I10.7 I U I I I i l l2 . 2 I U ! I I i l l
i 1 I I I I I0 . 4 I U ! 1 I I I I1 . 8 I U I I I I I !
I I I I I I !5 . 3 I U I I I I I I
I I I I I I I5 . 0 I B I I I I I I
1 1 1 I I I I10.9 1 1 II 1 1 I
I I I I I I II I 1 1 1 M
0 . 1 I U I I I 1 I I4 . 6 I U I I I I I I
I I 1 1 I I I2 . 1 I U I 1 ! I l l1 . 9 I U I I I I I I
1 1 I I 1 1 !9 5 . 5 1 I I I I I I
I I I I i l l2 . 4 I U I I I 1 1 i
I I I I I I I1 I 1 I Id
1 II 1
Prepa- 1 1ration 1 1Blank C! 1 M
1 1! 1 INR
10. 700IUI IP2.200IUMF
1 i INR0. 400 1 U 1 1 P1.800IU1 IP
1 1 INR5. 300 i U 1 i P
i I INR5.010IBI IP
1 1 INR10.9001 IIP
1 1 INR1 1 INR
0.100 IUI ICV
4. 600 lUi IP1 1 INR
2. 140IUMF1.900IUI IP
1 ! INR95.5001 MP
1 1 INR2. 4001 UI IP
1 1 INR1 1 1
FORM III - IN 7/87
flR002072
U.S. EPA - CLP .
4ICP INTERFERENCE CHECK SAMPLE
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG,
b Code: W88
P ID Number: 2483
Case No. : BLOSE SAS No: 12307_
ICS Source:
SDG No. : 0000C
Concentration Units: ug/L
1 1I True 11 Sol. Sol. 11 Analyte A AB 1I 11 Alum in urn_l 500000 1(Antimony 1 1(Arsenic 1 11 Bar i urn 1 11 Beryl Ii urn 1 11 Cadmium 1 1i Calcium _ 15000001I Chromium 1 11 Cobalt 1 I1 Copper 1 11 1 ron 1 200000 11 Lead 1 I! Magnesium 1500000!! Manqanese 1 1i Mercury 1 1INickel 1 I1 Potassium! 1(Selenium 1 1I Silver 1 11 Sod i urn 1 1(Thallium 1 i1 Vanad i urn 1 1IZinc I 1
_500000 I11
5001
500110001
500000 i500150015001
200000 110001
_500000 15001
1
10001111
I1
500110001
IInitial Found 1 Final Found
Sol. Sol. 1 Sol. Sol.A AB '/.R 1 A AB *R
1_461400! 482600. 0 1 _96. 5 1 4653001
i I I !1 1 1 I1 526.01105.21 11 489.0! 97.81 1i 910.01 91.01 1
_467900 1 _485000. 0 1 _97. 0 1 _475200 1l~ 492.0! 98. 4 l~ 11 567.01113.41 i1 420.01 84.01 1
1748001 191100.0! 95.61 17620011 992.01 99.21 1
_488100I 503300.01100.71 49290011 507.01101.41 11 1 1 I1 956.01 95.61 1I I I II 1 1 II 982.01 98.2! 11 I I II I I I1 574.01114.811 2.01 0.2! 1
480500. 01 96. 111
529.01105.8490.01 98.01924.01 92.41
_486300.0I_97.3I494.0! 98.81532.01106.41402.01 80.41
11012.01101.2
_502700. 01100.5500.01100.0
1932.01 93.2
111I1
538.01107.6955.01 95.5
1 1 1 I I I I I 1
FORM IV - IN 7/87
SR002Q73
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY:
LOCATION: Uw £.<vU / 9k
SAMPLED BY:
ORGANIZATiON: D '.
STATIONNUMBER SAMPLE LOCATION DATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONTAINERS
ANALYSISREQUIRED
\. - X - ! >0 iijqfo (rriub
JU T- lift
\-IT- tOfi z- £"- 1 oo
0 »OO
1i: TO
- e - fl 4(f I V.IT
12. - e - 60 IV,\V
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: ') DATE TIMEV.o-,
Received by Laboratory: DATE TIME
COMMENTS: HL , CMA ->!~v Ux v c/ - C" 1 H^^-GlOc or
METHOD OF SHIPMENT:
OBG Laboratories, Inc., an O'Brien & Gere Limited Company5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-0200$ R Q 0 2 0 7 U
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY:
LOCATION:
SAMPLED BY:
ORGANIZATION:
STATIONNUMBER SAMPLE LOCATION DATE
COLLECTEDTIME
COLLECTEDSAMPLEMATRIX
COMP.OR GRAB
NO. OFCONTAINERS
ANALYSISREQUIRED
^- fe- to T- T I
Is- LA -A t>V, A -- Air- lOo F
/<*-
1 "™| l-fl . - 1 .IV." A , , . . A - f—— \
,1 *
\
1
\
VA 'i AS- e - / 20 6
Relinquished By: DATE TIME Received By: DATE TIME
Relinquished By: DATE TIME Received By: DATE TIME
-4-JTS:
DATE TIME Received by Laboratory: DATE TIME
COMMENt-5: » . ^ ^ <W-,JU Jyvix, '-F
.. 0''
-_
METHOD OF SHIPMENT:0
OBG Laboratories, Inc., an O'Brien & Gere Limited Company _ n . o n "7 C5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-0200 flHUUdU/3
z
CHAIN OF CUSTODY RECORD
LABORATORIES, INC.
SURVEY: &is ^ L^Jcf , \\
LOCATION: ' i« CcJK ?&STATIONNUMBER
>*
1 ——
SAMPLE LOCATION
Try- ra,w~
Relinquished By:
Relinquished By:
Relinquished By:ti n Jv ,.* ,
DATECOLLECTED
DATE
DATE
DATE
TIME'COLLECTED
•
TIME
TIME
TIME
SAMPLED BY: !K_,'r X.W /u>-- c\
ORGANIZATION^ A,,. ' '„ /» . ^J Vc?r'<^- c vrtr<~ tX.M>vi,<n>SAMPLEMATRIX
'H
COMP.OR GRAB
NO. OFCONTAINERS
(
ANALYSIS JREQUIRED
£T4 wolffeoz.
Received By: DATE TIME
Received By: DATE TIME
Received bv Laboratory: DATE TIME
COMMENTS:! \]——————^ v _ ,
-U,,
METHOD OF SHIPMENT:
OBG Laboratories, Inc., an O'Brien & Gere Limited Company /•>«-»/•5000 Brittonfield Parkway / Suite 300 / PO Box 4942 / Syracuse, NY 13221 / (315) 437-02] ) 002076
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill ____ ____
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A_________ DATE ANALYZED: 11-10-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J. Tobler ____ DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-130________ EHRT SAMPLE NO.: 29450
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS_____ uq/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 17.426. Chloroethane 8.207. 2-Chloroethylvinyl Ether < 0.508. Chloroform 114.979. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dlchlorodifluoromethane < 0.5015. 1,1-Dichloroethane 45.1516. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene 11.8318. trans-1,2-Dichloroethene 126.7819. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
8R002077
CUSTOMER SAMPLE NO.: AS-l-130________ EHRT SAMPLE NO.: 29450
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene 1.0425. 1,1,1-Trichloroethane 104.9326. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 51.3428. Trichlorofluoromethane < 0.5029. Vinyl Chloride 13.9930. Benzene 1320.0031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____100.00%
Toluene-d8 - 97.00%
Bromofluorobenzene - 103.00%
Page2 fiRQ02078
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill _____ ____
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-10-90
SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-130 EHRT SAMPLE NO.: 29451
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.446. Chloroethane < 0.507. 2-Chloroethylvinyi Ether < 0.508. Chloroform 8.209. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.3016. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 7.5519. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methyiene Chloride < 1.00
Page1 fl.R002079
CUSTOMER SAMPLE NO.: AS-E-130 EHRT SAMPLE NO.: 29451
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 4.6226. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 2.6428. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 60.7531. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____96.00%
Toluene-d8 - 95.00%
Bromofluorobenzene - 98.00%
Page2 AROU2080
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill__________________________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-10-90
SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-120 EHRT SAMPLE NO.: 29452
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 &602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 17.436. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 100.279. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 39.8216. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene 9.3518. trans-1,2-Dichloroethene 109.9719. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Paae1 8ROU208I
CUSTOMER SAMPLE NO.: AS-l-120________ EHRT SAMPLE NO.: 29452
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene 1.2825. 1,1,1-Trichloroethane 98.2226. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 49.5528. Trichlorofluoromethane < 0.5029. Vinyl Chloride 10.6130. Benzene 1294.0031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
l,2-Dichloroethane-d4 - ____101.00%
Toluene-d8 - 93.00%
Bromofluorobenzene - 102.00%
COMPUTER SEARCH
Trichlorotrifluoroethane - Approx. 26 ug/L
HR002082
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU
SAMPLE SOURCE: Blosenski Landfill___________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-10-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-120_______ EHRT SAMPLE NO.: 29453
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS_____ . ug/L
1. Bromodichloromethane < * 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.606. Chloroethane < 0.507. 2-Chloroethyivinyl Ether < 0.508. Chloroform 8.119. Chloromethane < 0.5010. Dibromochloromethane r < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.3216. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 7.6419. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
flRQ02083
CUSTOMER SAMPLE NO.: AS-E-120 EHRT SAMPLE NO.: 29453
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1 -Trichloroethane 4.9126. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 65.7131. Ethyibenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____102.00%
Toluene-d8 - 89.00%
Bromofluorobenzene - 106.00%
ftR00208U
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill __
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-15-90
SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-120D EHRT SAMPLE NO.: 29473
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.646. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 8.129. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 2.3316. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 7.4519. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Page1 SR002085
CUSTOMER SAMPLE NO.: AS-E-120D_______ EHRT SAMPLE NO.: 29473
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 5.5026. 1,1,2-Trichloroethane < . o.5027. Trichloroethene 2.7428. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 68.3331. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____98.00%
Toluene-d8 - 94.00%
Bromofluorobenzene - 105.00%
Page2 SROQ2Q86
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.SEMI-VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: . OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill___________________________
WORK ORDER NO.: N/A________________ EHRT PROJECT NO.: 12319
DATE EXTRACTED: 11-12-90 _____ DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample__________ SAMPLE VOLUME: 1000.00
ANALYST: K. Nusekabel _____ FINAL VOLUME: 1.00
CUSTOMER SAMPLE NO.: AS-E-120 EHRT SAMPLE NO.: 29453
LAB NOTEBOOK NO.: 149. Pg. 83_____________ METHOD NO.: EPA 8270
RESULTCOMPOUNDS___________ ug/L
1. Phenol < 3.002. Bis(2-Chloroethyl)Ether . < 2.003. 2-Chlorophenol < 2.004. 1,3-Dichlorobenzene < 6.005. 1,4-Dichlorobenzene < 6.006. Benzyl Alcohol < 3.007. 1,2-Dichlorobenzene < 6.008. 2-Methylphenol < 3.009. Bis-(2-Chloroisopropyl) Ether < 4.0010. 4-Methylphend < 3.0011. N-Nitroso-Di-n-Propylamine < 4.0012. Hexachloroethane < 6.0013. Nitrobenzene < 3.0014. Isophorone < 2.0015. 2-Nitrophenol < 4.0016. 2,4-Dimethylphenol < 3.0017. Benzole Acid < 20.0018. Bis(2-Chloroethoxy)Methane < 2.0019. 2,4-Dichlorophenol < 4.0020. 1,2,4-Trichlorobenzene < 6.0021. Naphthalene < 1.0022. 4-Chloroaniline < 10.0023. Hexachlorobutadiene < 12.0024. 4-Chloro-3-Methylphenol < 3.0025. 2-Methylnaphthalene < 1.0026. Hexachlorocyclopentadiene < 12.0027. 2,4,5-Trichlorophenol < 5.0028. 2,4,6-Trichlorophenol < 5.00
Page1 flR002087
CUSTOMER SAMPLE NO.: AS-E-120______________ EHRT SAMPLE NO.: 29453
29.30.31.
m 32.W 33.
34.35.36.37.38.39.40.41.42.43.44.45.46.47.48.49.50.51.52.
fe 53.^ B 54^ 55.
56.57.58.59.60.61.62.63.64.65.
2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphthene2,4-Dinrtrophenol4-N'rtrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-PhenyletherRuorene4-N'rtroaniIine4,6-Dinitro-2-MethylphenolN-Nitrosodiphenylamine4-Bromophenyl-PhenyletherHexachlorobenzenePentachlorophendPhenanthreneAnthraceneDi-n-ButyphthalateRuoranthene .PyreneButyl benzylphthalate3,3'-DichlorobenzidineBenzo(a)AnthraceneChryseneBis(2-Ethylhexyl)PhthalateDi-n-OctylphthalateBenzo(b) RuorantheneBenzo(k) RuorantheneBenzo(a) Pyrenelndeno(1 ,2,3-cd) PyreneDibenzo(a,h)AnthraceneBenzo(g,h,i)Perylene
SURROGATE COMPOUND
Nitrobenzene-d52-RuorobiphenylTerphenyl-d14
Phenol-d52-Ruorophenol2,4,6-Tribromophenol
< 3.00< 10.00< 3.00< 2.00< 6.00< 10.00< 2.00< 40.00< 20.00< 6.00< 6.00< 2.00< 6.00< 3.00< 20.00< 20.00< 3.00< 6.00< 5.00< 20.00< 2.00< 2.00< 1.00< 2.00< 2.00< 3.00< 10.00< 3.00< 3.00< 2.00< 2.00< 10.00< 10.00< 6.00< 10.00< 10.00< 10.00
PERCENT RECOVERY
68.50%58.70%56.00%
10.00% *10.00% *13.80%
* A recovery lower than 10% was obtained on surrogates due to heavy emulsion.
Page2 AR002088
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.PESTICIDES - PCB ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill_________________________
WORK ORKER NO.: N/A_____________ EHRT PROJECT NO.: 12319
DATE EXTRACTED: 11-13-90 DATE ANALYZED: 11-13-90
SAMPLE TYPE: Water Sample_______ METHOD NO.: EPA 608 .
ANALYST: M. Cooper__________ LAB NOTEBOOK NO.: 158, Pg. 56
CUSTOMER SAMPLE NO.: AS-E-120 EHRT SAMPLE NO.: 29453
RESULTCOMPOUNDS ug/L
1. Alpha-BHC < 0.00142. Beta-BHC < 0.00083. Delta-BHC < 0.00064. Gamma-BHC < 0.00065. Heptachlor < 0.00206. Aldrin < 0.00167. Heptachlor Epoxide < 0.00148. Endosulfan I < 0.00089. Dieldrin < 0.000410. 4,4'-DDE < 0.000411. Endrin < 0.000612. Endosulfan II < 0.0213. 4,4'-DDD < 0.0214. Endosulfan Sulfate < 0.000415. 4,4'-DDT < 0.001216. Methoxychlor < 0.000417. Endrin Ketone < 0.0418. Chlordane < 0.2019. Toxaphene < 3.00
Pagel 3R002089
CUSTOMER SAMPLE NO.: AS-E-120___________ EHRT SAMPLE NO.: 29453
20. Aroclor-1016 < 0.5021. Aroclor-1221 < 0.5022. Aroclor-1232 < 0.5023. Aroclor-1242 < 0.5024. Aroclor-1248 '< 0.5025. Aroclor-1254 < 0.5026. Aroclor-1260 < 0.50
SURROGATE RECOVERY
Dibutylchlorendate - ____65.30%
Page2 ARQQ209Q
U.S. EPfl - CLP
COVER PflGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: ENVIR. HEALTH RESEARCH TE Contract: OBG____
Lab Code: W88__ Case No.: BLQSE SAS No.: 1£319_ SDG No. : 000000
SOW No.: ___
EPA Sample No. Lab Sample ID.ASE120 29453___
Were ICP interelement corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No N0_
Comments:OBGJ.ABO RATORIES_-_BLOSENSKIJ.ANDFILL_DATE_OF_ANALYSIS_l1/1£/90____ICP_G.STflKE_NB15S_PG46_METHOD_6010/_FURNflCE_P.BflRNWELL_NB154_PG63____METHOD flS7060 SE7740/ COLD VflPOR J.RftDER NB157 PGS3 METHOD 7470_____
Release of the data contained in this hardcopy data package and in thecomputer-readable data submitted on floppy diskette has been authorized bythe Laboratory Manager or the Manager's designee, as verified by thefollowing signature.
Lab Manager:
Date:COVER PAGE - IN ' ' 7/87
SR00209I
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ______________
II ASE120
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG_____ I___________,
Lab Code: W88__ Case No.: BLOSE SAS No.: 12319_ SDG No. : 000000
Matrix (soil/water): WATER Lab Sample ID: 29453___
Level (low/med): _____ Date Received: 11/39/90
'/. Solids: ___
Concentration Units (ug/L or mg/kg dry weight): U6/L_
1ICAS No.11 7429-90-517440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-91 7440-70-21 7440-47-31 7440-48-41 7448-50-81 7439-89-617439-92-11 7439-95-41 7439-96-51 7439-97-61 7440-02-01 7440-09-71 7782-49-21 7440-22-41 7440-23-51 7440-28-0I 7440-62-21 7440-66-611
1 11 Ana 1 y t e 1 Concent rat i oni 11 Aluminum_!Antimony_l1 Arsenic
10.72.2
1 Barium 11 BerylliumI Cadmium1 Calcium _IChromium_1 Cobalt1 Copper1 IronILead(Magnesium1 Manganese1 MercuryINickel1 Potassium(SeleniumISilverI Sod i urnIThallium_! Vanad i um_1 Zinc1 CyanideI
0.401.8
1 1ICI QI 11 IIUIIUI1 1IU!I U I
1 1IM 11 IINRI
. IP 1IF 1INRIIP 1IP 1
1 1 - INRI5.3
5.0
I U I1 1IUI
IP 1INRIIP 1
I I INRI10.9
0.14.6
IUI1 i1 IIUIIUI
IP fINR!INRIICVIIP I
I I INRI2.11.9
IU!IUI
IF IIP I
I I INR!95.5 IUI IP 1
1 ! INRI2.4 IUI IP 1
I I INRII I I I
Color Before: _________ Clarity Before: ____ Texture:
Color After: _________ Clarity After: ____ Artifacts:
Comments:
AS--E-120
FORM I - IN 7/87
flR002092
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: DBS.
Lab Code: W8S__ Case No.: BLOSE SAS No.: 12319_ SDG No.: 000000
Initial Calibration Source: SPEX______
Continuing Calibration Source: SPEX______
Concentration Units: ug/L
i 11 1lAnalyte !1 11 Alurninum_l1 Antimony 1(Arsenic 11 Bar i urn 11 Beryl liuml'1 Cadmium 11 Calcium 11 Chromium 11 Cobalt 1! Copper 11 Iron 11 Lead 11 Magnesium I1 Manganese 11 Mercury 1INickel 11 Pot ass i urn 1ISeleniuni_l1 Silver 11 Sod i urn1 Thallium 11 Vanad i urnIZinc 11 Cyanide
1Initial Calibration 1
True Found XRCl) 11
1500.0 I50.0 I
1500.0 1
500.0 i1
__500. 0_l
1500.0 1
1500.0 i
11
5.0 1500.0 1
110.0 1
100.0 11
1000.0 11
500.0 I1
1 1507.501101.5147.901 95.81
1 - 1476.301 95.3!490. 40 1 98. 1 1
1 1_ 549.001109.81
1 1489.001 97.81
1 1483.201 96.61
1 11 1
5.481109.6!490.701 98.11
1 110.501105.0197. 101 97.11
1 i946.501 94.61
1 1494.901 99.01
1 1
i 1Continuing Calibration 1 1
True Found jtR(l) Found %R(1) 1 1 MI 1
1500.0 I50.0 I
1500.0 I
500.0 I1
__ 500. 0_l_~r500.0 1
1
500.0 1
11
5.0 1500.0 1
120.0 1100.0 1
1
1000.0 11
500.0 11
1 1508.301101.7149.801 99.61
I I471.801 94.41483.601 96.71
1 1548.701109.71
1 1479.801 96.01
1 1478.401 95.71
I 11 I
5.301106.01483.201 96.61
I 119.901 99.5196.701 96.71
1961.901 96.2
1493.701 98.7
1
1 I INR1 1 IP1 I IF1 1 INR1 1 IP1 1 IP1 I I N R I1 1 IP1 I l N R !1 1 IPi I INRI1 i IP1 MNRI1 1 INR1 1 ICV1 1 IP1 1 INR1 1 IFI 1 IP1 1 INR1 1 IP1 I INR1 1 IP1 1 INR
1 1 1 I I i ! I l l
(1) Control Limits: Mercury 80-1235 Other Metals 90-113! Cyanide 85-115
FORM II (PART 1) - IN 7/87.
SR002093
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG_
Lab Code: W88__ Case No.: BLOSE SflS No.: 12319_ SDS No. : 000303
Initial Calibration Source: SPEX_____
Continuing Calibration Source: SPEX_____
Concentration Units: ug/L
1 1lAnalyte 1I I1 Aluminum 11 Antimony_l1 Arsenic 11 Barium 11 Beryl liuml(Cadmium I(Calcium 11 Chromium 11 Cobalt i! Copper 11 Iron 1I Lead 11 Magnesium!1 Manganese 11 Mercury 1INickel 11 Pot ass i urn 1(Selenium 11 Silver 11 Sod i urn 1I Thai Hum 11 Vanad i urn 1IZinc 11 Cyanide 11 1
InitTrue
12000.0
1000. 0_1000. 0
2030. 3
5000. 0
630.3
8303. 0
2303. 3
2000. 0
4000. 3
ial CalibrationFound *R<1)I
I I I111763.331 98.3I 1 !1 11 988.001 98.81
True
112038.3 !
11
1000.8 IJ _1026. 00 1 102. 6 1 _1000. 0_l
1 1 l~~ 11 1919.301 96.31 2833.3 11 1 I I1 5299.031106.0! 5003.0 1! 1 f 11 581.501 96.91 633.3 I1 1 11 11 11 7847. 33 1 98. 11 11 11 1978.30! 98.9i 11 2065.301103.21 11 4135.031103.4i 11 1
111
8000.0 I11
2808.0 11
2000.0 i1 14000.0 1
1
1
Continuing Calibration 1Found *R(1) Found %R(1) 1 Ml
1 11 1 1
12173.001181.41 11 1
INRIIP I
I IINRI1 1 1
1017.001101.71 I1074.001107.41 1
1 11971.301 98.61 1
I I 15364.831187.31 I
.1 1 1609.901101.61 1
111
8890.081181.111
2026.081101.3I
2118.001135.9.I
4255.031106.4
111I1111111
1 1 I1 I 1
INRIPJIP-INRIIPINRIIP-INRIIP 1INRIINRINRIIP 1INRIINRIIP IINRIPINRIPINR1
(1) Control Limits: Mercury 80-120! Other Metals 98-118! Cyanide 85-115
FORM II (PART 1) - IN 7/87
U.S. EPA - CLP
3BLANKS
Lab Name: ENVIR. _HEALTH_RESEARCH_TE Contract: OBG.
Lab Code: W88__ Case No.: BLOSE SAS No.: 12319_ SDG No. : 888888
Preparation Blank Matrix (soil/water): WATER
Preparation Blank Concentration Units (ug/L or rng/kg): UG/L_
1 11 1 Initial1 1 Calib.1 I BlanklAnalyte I (ug/L)1 11 Aluminum 11 Antimony !1 Arsenic 11 Barium 11 Beryllium I1 Cadmium 11 Ca 1 c i urn 1I Chromium 11 Cobalt 11 Copper 11 Iron 11 Lead 11 Magnesium!1 Manganese 11 Mercury I(Nickel 11 Potassium!(Selenium 1(Silver 11 Sod i urn 11 Thallium 1
13.72.2
0.41.8
5.3
5.0
10.9
0.14.6
2.11.9
95.5
1111
Cl1
1 1IUIIUI1 1IUIIUI1 IIUI1 1IUI1 11 11 i1 IIU!IUI1 1IUIIUI1 Ii 1
I
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
10.72.2
8.41.8
5.3
5.8
10.9
0. 14.6
2. 11.9
95.5
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FORM III - IN 7/87
3ROG2Q95
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A_______________ DATE ANALYZED: 11-10-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J. Tobler___________ DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-100 EHRT SAMPLE NO.: 29454
LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 16.356. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 86.639. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 32.2516. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene 6.4018. trans-1,2-Dichloroethene 93.1919. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Page1 SR002096
CUSTOMER SAMPLE NO.: AS-l-100________ EHRT SAMPLE NO.: 29454
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025, 1,1,1-Trichloroethane 86.5826. 1,1,2-Trichloroethane < . 0.5027. Trichloroethene 47.6928. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 1261.0031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____96.40%
Toluene-d8 - 87.00%
Bromofluorobenzene - 109.00%
3RG02097
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill____________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-14-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-100 ___ ___ EHRT SAMPLE NO.: 29455
LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.876. Chloroethane < 0.507. 2-Chioroethylvinyl Ether < 0.508. Chloroform 9.889. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 3.1316. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 10.2219. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
flR002098
CUSTOMER SAMPLE NO.: AS-E-100_______ EHRT SAMPLE NO.: 29455
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 5.4126. 1,1,2-Trichloroethane < 0.5027. Trichloroethene < 0.5028. Trichlorofluoromethane . < 0.5029. Vinyl Chloride < 0.5030. Benzene 74.0831. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____97.00%
Toluene-d8 - ____100.00%
Bromofluorobenzene - 102.00%
Page2 3ROG2099
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES. INC. - MR. MIKE PETTERELU
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A • _______ DATE ANALYZED: 11-15-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 0.50
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-90 EHRT SAMPLE NO.: 29456
LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 &602
RESULTCOMPOUNDS____ ug/L
1. Bromodlchloromethane < 5.002. Bromoform < 5.003. Bromomethane < 5.004. Carbon Tetrachloride < 5.005. Chlorobenzene 17.206. Chloroethane < 5.007. 2-Chloroethylvinyl Ether < 5.008. Chloroform 98.109. Chloromethane < 5.0010. Dibromochloromethane < 5.0011. 1,2-Dichlorobenzene < 5.0012. 1,3-Dichlorobenzene < 5.0013. 1,4-Dichlorobenzene < 5.0014. Dichlorodifluoromethane < 5.0015. 1,1 -Dichloroethane 37.4016. 1,2-Dichloroethane < 5.0017. 1,1-Dichloroethene 9.5018. trans-1,2-Dichloroethene 110.2019. 1,2-Dichloropropane < 5.0020. cis-1,3-Dichloropropene < 5.0021. trans-1,3-Dichloropropene < 5.0022. Methylene Chloride < 10.00
SR002IOO
CUSTOMER SAMPLE NO.: AS-l-90________ EHRT SAMPLE NO.: 29456
23. 1,1,2,2-Tetrachloroethane < 5.0024. Tetrachloroethene < 5.0025. 1,1,1-Trichloroethane 131.4026. 1,1,2-Trichloroethane < 5.0027. Trichloroethene 55.5028. Trichlorofluoromethane < 5.0029. Vinyl Chloride < 5.0030. Benzene 1201.1031. Ethylbenzene < 5.0032. Toluene < 5.00
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____100.00%
Tduene-d8 - 88.00%
Bromofluorobenzene - 106.00%
Page2 3R002IOI
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill_________________________
WORK ORDER NO.: N/A__________ PROJECT NO.: 12319
DATE EXTRACTED: N/A__________ DATE ANALYZED: 11-14-90
SAMPLE TYPE: Water Sample SAMPLE VOLUME: 5.00
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-90 EHRT SAMPLE NO.: 29457
LAB NOTEBOOK NO.: 162, Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 1.966. Chloroethane < . 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 9.629. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodifluoromethane < 0.5015. 1,1-Dichloroethane 3.1216. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 9.7419. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Pagel 3RG02I02
CUSTOMER SAMPLE NO.: AS-E-90________ EHRT SAMPLE NO.: 29457
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 6.1326. 1,1,2-Trichloroethane < 0.5027. Trichloroethene 3.1128. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 81.5031. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____96.00%
Toluene-d8 - 99.00%
Bromofluorobenzene - 104.00%
Page2 3ROQ2I03
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A_____________ PROJECT NO.: 12319
DATE EXTRACTED: N/A___________ DATE ANALYZED: 11-15-90
SAMPLE TYPE: Water Sample____ SAMPLE VOLUME: 0.50
ANALYST: J.Tobler DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-l-80 EHRT SAMPLE NO.: 29458
LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS ug/L
1. Bromodichloromethane < 5.002. Bromoform < 5.003. Bromomethane < 5.004. Carbon Tetrachloride < 5.005. Chlorobenzene 17.206. Chloroethane < 5.007. 2-Chloroethylvinyl Ether < 5.008. Chloroform 95.209. Chloromethane < 5.0010. Dibromochloromethane < 5.0011. 1,2-Dichlorobenzene < 5.0012. 1,3-Dichlorobenzene < 5.0013. 1,4-Dichlorobenzene < 5.0014. Dichlorodifluoromethane < 5.0015. 1,1-Dichloroethane 36.2016. 1,2-Dichloroethane < 5.0017. 1,1-Dichloroethene < 5.0018. trans-1,2-Dichloroethene 106.6019. 1,2-Dichloropropane < 5.0020. cis-1,3-Dichloropropene < 5.0021. trans-1,3-Dichloropropene < 5.0022. Methylene Chloride < 10.00
CUSTOMER SAMPLE NO.: AS-l-80 ___ EHRT SAMPLE NO.: 29458
23. 1,1,2,2-Tetrachloroethane < 5.0024. Tetrachloroethene < 5.0025. 1,1,1-Trichloroethane 124.3026. 1,1,2-Trichloroethane < 5.0027. Trichloroethene 59.1028. Trichlorofluoromethane < 5.0029. Vinyl Chloride < 5.0030. Benzene 1267.8031. Ethylbenzene < 5.0032. Toluene < 5.00
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____102.00%
Toluene-d8 - ____85.00%
Bromofluorobenzene - 110.00%
Page2 fl R 0 0 2 I 0 5
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.VOLATILE ORGANIC ANALYSIS
CUSTOMER NAME: OBG LABORATORIES, INC. • MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill_________
WORK ORDER NO.: N/A______________ PROJECT NO.: 12319
DATE EXTRACTED: N/A___________ DATE ANALYZED: 11-14-90
SAMPLE TYPE: Water Sample_____ SAMPLE VOLUME: 5.00
ANALYST: J. ToWer DILUTION FACTOR: 1.00
CUSTOMER SAMPLE NO.: AS-E-80________ EHRT SAMPLE NO.: 29459
LAB NOTEBOOK NO.: 162. Pg. 9_______ METHOD NO.: EPA 601 & 602
RESULTCOMPOUNDS____ ug/L
1. Bromodichloromethane < 0.502. Bromoform < 0.503. Bromomethane < 0.504. Carbon Tetrachloride < 0.505. Chlorobenzene 2.436. Chloroethane < 0.507. 2-Chloroethylvinyl Ether < 0.508. Chloroform 12.069. Chloromethane < 0.5010. Dibromochloromethane < 0.5011. 1,2-Dichlorobenzene < 0.5012. 1,3-Dichlorobenzene < 0.5013. 1,4-Dichlorobenzene < 0.5014. Dichlorodrfluoromethane < 0.5015. 1,1-Dichloroethane 3.6316. 1,2-Dichloroethane < 0.5017. 1,1-Dichloroethene < 0.5018. trans-1,2-Dichloroethene 12.2219. 1,2-Dichloropropane < 0.5020. cis-1,3-Dichloropropene < 0.5021. trans-1,3-Dichloropropene < 0.5022. Methylene Chloride < 1.00
Pagel flRQQ2iQ6
CUSTOMER SAMPLE NO.: AS-E-80________ EHRT SAMPLE NO.: 29459
23. 1,1,2,2-Tetrachloroethane < 0.5024. Tetrachloroethene < 0.5025. 1,1,1-Trichloroethane 6.2926. 1,1,2-Trichloroethane < • 0.5027. Trichloroethene 3.6328. Trichlorofluoromethane < 0.5029. Vinyl Chloride < 0.5030. Benzene 94.5331. Ethylbenzene < 0.5032. Toluene < 0.50
SURROGATE STANDARDS - % RECOVERIES
1,2-Dichloroethane-d4 - ____98.00%
Toluene-d8 - 98.00%
Bromofluorobenzene - 106.00%
Page2 QROQ2IQ7
SOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lao Name: ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC._______
stomer Name: OBG LABORATORIES, INC. - MR. PETTERELLI________________
Method No.: EPA 601 & 602______ Project No.: 12319
oustomer Sample No.: AS-E-80_________ EHRT No.: 29459
COMPOUND-Dichloroethene
'i nchloroetheneRonzene
ueneunlorobenzene
AMOUNT ADDED(ng)250250250250250
SAMPLE CONC.(ug/L)03.69502.4
MS CONC.(ug/L)49.762.215654.258.2
MS%REC#99117122108112
QC LIMITSREC.59-17262-13766-14259-13960-133
^RuND1,1-DichloroetheneT-' hloroethene
nzeneToluene'orobenzene
MSD CONC.(ug/L)49.261.1153.154.557.1
MSD%REC#98115116109109
MS%REC#99117122108112
%RPD#
1250.13
QCURPD2224212121
WITSREC.59-17262-13766-14259-13960-133
-"• Column to be used to flag recovery and RPD values with an asterick
* Values outside of QC limits
RPD: _____0_____ out of ___5___ outside limitsSpike Recovery:_____0_____ out of 10 outside limits
'MMENTS:
Pagel
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE;
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A
5-Day BOD Analysis
EPA 405.1
G. Stake
SAMPLE NO.EHRT NO. CUSTOMER NO.
29458 AS-l-80
29459 AS-E-80
PROJECT NO.: 12319
DATE ANALYZED: 1 1 /09-1 4/90
LAB NOTEBOOK NO. : 161,
RESULTSmg/L
BDL
BDL
Pg.6
DETECTION LIMIT: < 2 mg/L
Pagel flRQ02l
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELU
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A
COD Analysis
EPA 41 0.4
M. Reddy
SAMPLE NO.EHRT NO. CUSTOMER NO.
29458 AS-l-80
29459 AS-E-80
PROJECT NO.: 12319
DATE ANALYZED: 11-09-90
LAB NOTEBOOK NO.: 151, Pg. 25
RESULTSmg/L
94.43
77.55
DETECTION LIMIT: < 40 mg/L
,£JR002MO
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES. INC. • MR. MIKE PETTERELLI
SAMPLE SOURCE:
WORK ORDER NO.:
ANALYSIS PERFORMED:
ANALYSIS METHOD:
ANALYST:
Blosenski Landfill
N/A PROJECT NO.:
Total Suspended Solids Analysis
Std. Method 209C DATE ANALYZED
M. Reddy LAB NOTEBOOK
SAMPLE NO.EHRT NO. CUSTOMER NO.
29458 AS-l-80
29459 AS-E-80
12319
: 11-12-90
NO.: 137, Pg.61
RESULTSmg/L
BDL
BDL
DETECTION LIMIT: < 10 mg/L
flR002il|
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
CUSTOMER NAME: OBG LABORATORIES, INC. - MR. MIKE PETTERELLI
SAMPLE SOURCE: Blosenski Landfill
WORK ORDER NO.: N/A PROJECT NO.: 12319
ANALYSIS PERFORMED: TOC Analysis
ANALYSIS METHOD: EPA 9060
ANALYST: G. Luna
DATE ANALYZED: 1 1 -09-90
LAB NOTEBOOK NO.: 135, Pg. 1 7
SAMPLE NO.EHRT NO. CUSTOMER NO.
29458A AS-l-80
29458B AS-l-80(Duplicate)
29459 AS-E-80
RESULTSmg/L
15.40
12.80
< 10 mg/L
DETECTION LIMIT: < 10 mg/L
flR002M2