phase ii environmental site assessment · 2020. 10. 18. · phase ii environmental site assessment...

Phase II Environmental Site Assessment

Sheboygan Municipal Auditorium and Armory,

516 Broughton Drive, Sheboygan, Wisconsin

U.S. EPA Brownfield Cooperative Agreement No.: BF-00E01349-0

Nicholas J. HeimStaff Geologist

Rick Binder, PG, CPG Associate

Stuart J. Gross, PGAssociate

May 22, 2015Project No. 193703239

PHASE II ENVIRONMENTAL SITE ASSESSMENT Sheboygan Municipal Auditorium and Armory, Sheboygan, Wisconsin May 22, 2015

Sheboygan Municipal Auditorium and Armory Page i Phase II ESA Project Number 193703239

TABLE OF CONTENTS

1.0 EXECUTIVE SUMMARY ............................................................................................................. 1 2.0 BACKGROUND INFORMATION .................................................................................................. 3 3.0 DESCRIPTION OF INVESTIGATION ............................................................................................. 4

3.1 SOIL BORINGS ...................................................................................................................... 4 3.2 TEMPORARY WELL INSTALLATION AND GROUNDWATER SAMPLING ............................. 4

4.0 APPLICABLE CLEAN-UP CRITERIA ........................................................................................ 5 5.0 RESULTS OF INVESTIGATION ....................................................................................................... 7

5.1 SUBSURFACE CONDITIONS ................................................................................................. 7 5.2 FIELD SCREENING RESULTS .................................................................................................. 7 5.3 SOIL SAMPLING LABORATORY ANALYTICAL RESULTS ...................................................... 7 5.4 GROUNDWATER ANALYTICAL RESULTS ............................................................................. 7

6.0 CONCLUSIONS, RECOMMENDATIONS AND LIMITATIONS ...................................................... 9 FIGURES Figure 1: Site Location and Local Topography Figure 2: Site Layout Figure 3: Soil Boring and Temporary Monitoring Well Locations

TABLES Table 1: Soil Sample Field Screening and RCRA Metals and Polynuclear Aromatic

Hydrocarbon/Semi Volatile Organic Compound Laboratory Results Table 2: Soil Sample Field Screening and Volatile Organic Compound Laboratory Results Table 3: Groundwater Quality Results APPENDICES Appendix A: Soil Boring Logs .................................................................................................. 6 pages Appendix B: Soil Borehole Abandonment Forms ............................................................... 6 pages Appendix C: Soil and Groundwater Laboratory Analytical Report ............................. 121 pages

PHASE II ENVIRONMENTAL SITE ASSESSMENT Sheboygan Municipal Auditorium and Armory, Sheboygan, Wisconsin May 22, 2015

Sheboygan Armory and Auditorium Page 1 Phase II ESA Project Number 193703239

1.0 EXECUTIVE SUMMARY

During Apr i l 2015, Stantec Consult ing Serv ices Inc. (Stantec) completed a Phase II Environmental Site Assessment (ESA) at the Sheboygan Auditorium and Armory property at 516 Broughton Drive, Sheboygan, Wisconsin (the Site or Property). The Property is 2.69 acres in size and currently contains a vacant 52,000 square-foot two-story concrete building constructed in 1941. Surrounding land use is a mix of commercial and residential properties. The Property was likely originally developed for residential and commercial use (lumberyard) prior to 1891 and used for these purposes through at least the early 1900s. In 1941, the current building, used mainly as an armory and public auditorium, was constructed at the Property. The Property was used for these purposes until recent times and is now currently vacant.

The purpose of the Phase II ESA was to further evaluate a recognized environmental condition (REC) identified during a Phase I ESA completed by Stantec in January 2015. The REC was associated with the Site’s historic use as a lumberyard. Therefore, materials commonly associated with treating lumber (e.g. semi-volatile organic compounds [SVOCs] and heavy metals) may have been used/stored at the Property. In addition, petroleum may have been used for dust suppression in lumber storage areas.

This project was performed using funding from an assessment grant for brownfield hazardous substances awarded to Sheboygan County (the County) by the United States Environmental Protection Agency (U.S. EPA) in 2014. The U.S. EPA approved the hazardous substance brownfield eligibility determination on December 3, 2014. A Site-specific Sampling and Analysis Plan (SAP) was submitted to and approved by U.S. EPA in February 2015, prior to initiation of field activities.

As part of the Phase II ESA, six soil borings were advanced at the Site with four of the borings completed as temporary groundwater monitoring wells. Soil and groundwater samples were collected from the boreholes and temporary well locations. Subsurface strata encountered in the borings generally consisted of up to six inches of topsoil underlain by silty clay/sand to boring terminus. Sandy gravel was observed below the silty clay in boring SB3 to a depth of 12 feet below grade (fbg). Saturated conditions were observed at approximately 6-7 fbg in each borehole. Stantec was able to reach targeted depths within all soil borings.

Results of the Phase II ESA indicate that polynuclear aromatic hydrocarbon (PAH), Resource Conservation and Recovery Act (RCRA) Metals, volatile organic compounds (VOCs) and SVOCs are present in soil and groundwater in some boreholes at concentrations above established standards. In general, contaminant concentrations in soil and groundwater are relatively low and do not appear to be widespread. However, it is likely that additional soil sampling may be needed to better define the extent of the SVOC/PAH contamination reported in SB4 and benzene concentrations reported in SB4 and SB6. Additional groundwater sampling may also be required to further evaluate the detection of VOCs in TW-4. Stantec recommends that a copy of this report be submitted to the Wisconsin Department of Natural Resources (WDNR) by the Property owner to maintain compliance with state statutes. Chapter 292.11 Wisconsin Statutes requires that anyone who possesses or controls a hazardous substance or who causes the discharge of a hazardous substance notify the WDNR immediately of any discharge. Further discussions could then be conducted with the WDNR to determine what additional work is necessary at the Site, if any, to address the Phase II ESA results.

The Phase II ESA was performed in accordance with generally accepted practices for the environmental consulting profession, undertaking similar studies at the same time and in the same geographical area as the work conducted by Stantec. Stantec observed the degree of care and skill that are generally exercised by the profession under similar circumstances and conditions. No other warranty is expressed or implied.

PHASE II ENVIRONMENTAL SITE ASSESSMENT Sheboygan Armory and Auditorium, Sheboygan, Wisconsin May 22, 2015


Stantec’s observations, findings and opinions should not be considered as scientific certainties, but only as opinion based on our professional judgment concerning the significance of the data gathered during the course of this investigation. Specifically, Stantec cannot represent that the Property does not contain any hazardous or toxic materials or other latent conditions beyond that observed by Stantec during the course of the investigation. Additionally, due to limitations of this investigation process and the necessary use of data furnished by others, Stantec and its subcontractors cannot assume liability if actual conditions differ from the information presented in this report.



2.0 BACKGROUND INFORMATION

During January 2015, Stantec completed a Phase I ESA under contract with the County at the request of Ms. Emily Vetting of the County to evaluate potential environmental liabilities associated with the Property. Based on the results of the Phase I ESA, the Property is 2.69 acres in size and currently contains a vacant 52,000 square-foot two-story concrete building constructed in 1941. The Property is located approximately 350 feet west of Lake Michigan and 150 feet north of the Sheboygan River. The Property is currently owned by the City of Sheboygan. Surrounding land use is a mix of commercial and residential properties. The Property was likely originally developed for residential and commercial use (lumber yard) prior to 1891 and used for these purposes through at least the early 1900s. In 1941, the current building was constructed. The Property was used for these purposes until recent times and is now currently vacant. The Site and surrounding vicinity are illustrated on Figures 1 and 2.

Based on the information gathered during the Phase I ESA, Stantec made the following findings and developed the following opinions as summarized in the Phase I ESA report dated January 20, 2015. Only those findings and opinions relevant to the Phase II ESA are listed below.

Finding 1: The Property was likely originally developed for residential and commercial use (lumberyard) prior to 1891 and used for these purposes through at least the early 1900s. In 1941, the current building, used mainly as an Armory and public auditorium was constructed at the Property. The Property was used for these purposes until recent times and is now currently vacant.

Opinion 1: The historic use of the Property as an Armory and public auditorium is not considered a REC, HREC, CREC. However, environmental concerns generally associated with lumberyards include the use and storage of petroleum products, various lubricants/solvents and wood treatment/preservative chemicals (i.e. copper, arsenic and chromium). Therefore, the historic use of the property as a lumberyard is considered a REC.



3.0 DESCRIPTION OF INVESTIGATION

3.1 SOIL BORINGS Field activities were completed in accordance to the Site-Specific Sampling and Analysis Plan (SAP; Stantec 2014) submitted to the U.S. EPA and the WDNR on February 25, 2014 and approved in March 2015 prior to initiation of site field activities. On April 9, 2015, Stantec personnel advanced six borings (SB1 through SB6) on the Property using a truck-mounted Geoprobe®. Soil samples were collected continuously from each boring from the ground surface to a maximum depth of 12 fbg. All boreholes were advanced to desired depths with no refusal. Soil boring locations are illustrated on Figure 3. Geologic logs for the soil borings are included in Appendix A.

Each two-foot soil sampling interval was divided into two aliquots; one used for field screening purposes and one used to supply materials for potential submittal to a laboratory for chemical analysis. The laboratory aliquot for each soil sample was immediately placed in laboratory provided containers, sealed and placed in a cooler with ice. The other portion of each sample was placed into plastic Ziploc® bags and used to field screen for the presence of VOCs using a photoionization detector (PID) equipped with an 11.7 electronvolt (eV) lamp. All non-disposable soil sampling equipment was washed with a detergent solution and double-rinsed with tap water before and after each soil sample was collected to prevent sample cross-contamination. The PID data for samples from each borehole are presented on Table 1 as well as included on the geologic logs presented in Appendix A.

Up to two soil samples collected from each borehole were placed in laboratory supplied containers, preserved as appropriate, placed in a sample cooler on ice and submitted under chain of custody to Test America Laboratories Inc. (Test America) of University Park, Illinois for analysis of VOCs (Method 8260B), SVOCs ( Method 8270D) and/or RCRA metals (Method 6010B and 7470A). All soil borings not completed as temporary wells were immediately abandoned following sampling by filling the boreholes with bentonite. Borehole abandonment forms are included in Appendix B.

3.2 TEMPORARY WELL INSTALLATION AND GROUNDWATER SAMPLING Four temporary wells were installed in soil borings SB1, SB2, SB3 and SB4 and designated as TW1 TW2, TW3 and TW4, respectively. The temporary wells were constructed using 1-inch inner diameter (ID), Schedule 40 polyvinyl chloride (PVC) casing and 10-foot lengths of factory-slotted PVC screen (0.010-inch slot) that were positioned to intersect the water table.

On April 9, 2015 Stantec personnel collected groundwater samples from temporary wells TW1, TW2, TW3, and TW4. Groundwater samples were poured directly into pre-cleaned sample bottles provided by Test America. The bottles were prepared with pre-measured chemical preservatives by the analytical laboratory (i.e., Hydrochloric Acid for VOC samples). Samples submitted for inorganic analyses were field filtered prior to preservation. The sample bottles were packed into a cooler with ice immediately after collection and delivered under chain-of-custody procedures directly to Test America for analysis of VOCs (Method 8260B), SVOCs ( Method 8270D) and RCRA metals (Method 6010B and 7470A).



4.0 APPLICABLE CLEAN-UP CRITERIA

Procedures for establishing soil clean-up standards applicable to sites in Wisconsin with documented soil contamination are specified in ch. NR 720 Wisconsin Administrative Code (WAC)(NR720). Significant revisions to NR720 were implemented in 2013, with an effective date of November 1, 2013.

Soil clean-up standards depend in part on current land use and zoning. I t is our understanding that the Property is current ly zoned industrial, but the planned future use of the Property is for commercial or other non-industrial land uses. Therefore, both the industrial standards and the more restrictive non-industrial classification are being used to assess clean-up criteria for the Property.

Residual contaminant levels (RCLs) are numerical soil clean-up standards that are calculated for a minimum of two exposure pathways – direct contact by humans with exposed soil, and leaching of contaminants from soil into groundwater. The clean-up standard is the lower of the RCLs calculated for a number of exposure pathways. A variety of methods may be used to calculate RCLs, subject to WDNR approval. The approach used for the Site was to use an RCL spreadsheet developed by the WDNR’s Remediation and Redevelopment Program staff for use by consultants. The spreadsheet (WDNR, 2013) is updated periodically by WDNR staff and utilizes toxicity information maintained on the U.S. EPA Regional Screening Level (RSL) website: http://www.epa.gov/reg3hwmd/risk/human/ rbconcentration_table/index.htm. As toxicity data are updated periodically for different types of contaminants, the WDNR RCL spreadsheet is similarly updated. The version used to determine RCLs for this Site is the January 2015 update.

As part of the revisions to NR720, WDNR adopted use of Background Threshold Values (BTVs) for select metals in soil whose occurrence may be attributable in whole or in part to natural occurrence in Wisconsin soil. BTVs are “non-outlier trace element maximum levels in Wisconsin surface soils” as determined through a state-wide study (USGS, 2011). BTVs were established for 16 metals including aluminum, arsenic, barium, cadmium, calcium, chromium, cobalt, copper, iron, magnesium, lead, manganese, nickel, strontium, vanadium and zinc. Probably the most significant BTV is the value of 8.0 milligrams per kilogram (mg/kg) established for arsenic. This value is significant because the RCLs calculated for the direct contact and groundwater pathways are significantly lower than this value, which in the past resulted in sites with relatively low levels of naturally occurring arsenic significantly exceeding the clean-up levels. If measured levels of arsenic or the 15 other metals for which BTVs have been established are below the BTVs, these levels can be attributed to natural occurrence without the need to perform a WDNR-approved site-specific study to determine background levels.

For samples with detections below standards, the hazard quotient, cancer risk and risk result are calculated for each sample using the WDNR’s RCL calculation spreadsheet. For an individual sample to pass, all of the following three criteria must be met: (a) the number of constituents for which there are individual exceedances must equal “0,” (b) the hazard quotient must be ≤ 1.0; (c) the cumulative cancer risk must be ≤ 1.0E-06. Criteria for which the individual samples fail, the spreadsheet notes that “This site sampling location will need either further clean-up to lower contaminant levels or the construction of a cap/cover to address the direct-contact pathway.” Public health-related groundwater quality standards are set forth by ch. NR 140 WAC (NR140). Standards are listed for substances of public health concern (defined as substances having carcinogenic, mutagenic or teratogenic properties or interactive effects) and substances of public welfare concern (defined as having a negative aesthetic value, but with little threat to human health). Two levels of standards are listed; the preventive action limit (PAL) and the enforcement standard (ES). The ES represents a concentration above which action generally must be taken to improve the quality of groundwater. The PAL represents a lower concentration (usually 10 to 20 percent of the ES) above which groundwater quality should be monitored. PAL and ES concentrations are summarized in Table 3.



WDNR vapor guidance “Addressing Vapor Intrusion at remediation and Redevelopment sites in Wisconsin”, PUB-RR-800, December 2010 includes use of Vapor Action Levels (VALs) and Vapor Risk Screening Levels (VRSLs) to evaluate potential risk due to vapor intrusion (WDNR, December 2010 and WDNR, July 2014). In general, if detected vapor concentrations are less than VRSLs, no action is needed. If detected vapor concentrations are greater than VRSLs, but less than VALs, action is recommended. If detected vapor concentrations are greater than VALs, action is required. Risk can further be assessed utilizing groundwater, soil vapor and sub-slab vapor attenuation factors, which are applied to account for each pathway.



5.0 RESULTS OF INVESTIGATION

5.1 SUBSURFACE CONDITIONS Subsurface strata encountered in the borings generally consisted of up to six inches of topsoil underlain by silty clay/sand to boring terminus. Sandy gravel material was observed below the silty clay in borings SB3 to a depth of 12 fbg. Saturated conditions were observed at a depth of approximately 6 to 7 fbg. Stantec was able to reach targeted depths within all soil borings. Soil boring logs are presented in Appendix A.

5.2 FIELD SCREENING RESULTS No elevated PID readings (greater than 1.0 instrument units [IU]) were recorded in the collected soil samples. The results of the PID screening are presented on Table 1 and also included in the soil boring logs presented in Appendix A.

5.3 SOIL SAMPLING LABORATORY ANALYTICAL RESULTS Laboratory analysis detected arsenic in concentrations in excess of the NR720 non-industrial and groundwater protection RCLs within all of the soil borings however the reported concentrations were below its respective BTV. Total Selenium was detected at concentrations in excess of the RCL for groundwater protection in soil borings SB2 at 2-4 fbg (2-4), SB3 (2-4), and SB4 (2-4). Though no BTV has been established for selenium, the reported concentrations are believed to be similar to background concentrations found in native soils throughout southeast Wisconsin. VOC analysis detected concentrations of benzene in excess of the RCL for groundwater protection in sample SB4 (2-4) and SB6 (2-4). No other RCL exceedances were present in the samples. In addition, no VOC concentrations were reported above the analytical limit of detection (LOD) in any other sample submitted for VOC analysis, except for SB2 (4-6), however the reported concentrations in this sample were below respective RCLs. Finally, SVOCS/PAH analysis detected benzo(b)flouranthene, benzo(a)pyrene and indeno(1,2,3-cd)pyrene in excess of their respective non-industrial direct contact RCLs within SB4 (2-4). In addition benzo(a)pyrene was detected above its respective non-industrial direct contact RCL within SB2 (4-6). No PAHs were reported above the analytical LOD in samples collected from SB2 (2-4), SB3 (2-4), SB4 (4-6) and SB5 (2-4). Soil laboratory analytical reports and chain-of-custody forms are presented in Appendix C. Soil laboratory results are summarized in Tables 1 and 2.

5.4 GROUNDWATER ANALYTICAL RESULTS The dissolved lead concentrations reported in TW1 and TW3 were present above the PAL. However, both results were “J” flagged by the project laboratory meaning that the reported concentration was detected between the LOD and limit of quantification and may not be statistically accurate. No other metals concentrations were reported above the analytical LOD in these samples except for barium. However, the reported barium concentrations were well below the PAL. No VOCs were reported above the analytical LOD in the groundwater samples from TW1, TW2 and TW3. The sample from TW4, did contain bromodichloromethane and chloroform at concentrations that exceeded the enforcement standard (ES). The source of these reported VOCs is not known. However, since chloroform can be present in drinking water (as a result of the chlorination of naturally occurring organic materials), it is possible that these compounds are attributed to a leaky stop box associated with the municipal water system entering the armory building that was present within 30 feet of the location of TW4. The leaky stop box has since been replaced. No SVOCs were reported above the analytical LOD in any sample. Groundwater laboratory analytical reports and chain-of-custody forms are presented in Appendix C. Groundwater laboratory results are summarized in Table 3.



5.5 VAPOR INTRUSION No vapor sampling was performed as part of this assessment. Since VOC concentrations in soil and groundwater were limited in extent and not present at concentrations that would likely prompt a threat to occupants of the current or a future building, no vapor sampling is planned at this time. However, if site conditions change or property redevelopment occurs, the potential for vapor migration and intrusion into current or future buildings should be reassessed.



6.0 CONCLUSIONS, RECOMMENDATIONS AND LIMITATIONS Results of the Phase II ESA indicate that PAHs, RCRA Metals, VOCs and/or SVOCs are present in soil and groundwater at several locations at concentrations above established standards, but that in general, contaminant concentrations are relatively low and do not appear to be widespread. However, it is likely that additional soil sampling may be needed to better define the extent of the SVOC/PAH contamination reported in SB4 and benzene concentrations reported in SB4 and SB6. Additional groundwater sampling may also be required to further evaluate the detection of VOCs in TW-4. Stantec recommends that a copy of this report be submitted to the WDNR by the Property owner to maintain compliance with state statutes. Chapter 292.11 Wisconsin Statutes requires that anyone who possesses or controls a hazardous substance or who causes the discharge of a hazardous substance notify the WDNR immediately of any discharge. Further discussions could then be conducted with the WDNR to determine what additional work is necessary at the Site, if any, to address the Phase II ESA results.

The Phase II ESA was performed in accordance with generally accepted practices for the environmental consulting profession, undertaking similar studies at the same time and in the same geographical area as the work conducted by Stantec. Stantec observed the degree of care and skill that are generally exercised by the profession under similar circumstances and conditions. No other warranty is expressed or implied.

Stantec’s observations, findings and opinions should not be considered as scientific certainties, but only as opinion based on our professional judgment concerning the significance of the data gathered during the course of this investigation. Specifically, Stantec cannot represent that the Property does not contain any hazardous or toxic materials or other latent conditions beyond that observed by Stantec during the course of the investigation. Additionally, due to limitations of this investigation process and the necessary use of data furnished by others, Stantec and its subcontractors cannot assume liability if actual conditions differ from the information presented in this report.


FIGURES

Project Location

Figure No.

Title

Client/Project

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MOSEL

SHEBOYGAN

SHEBOYGANFALLS

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1

Site Location andLocal Topography

193703239T15N, R23E, S23C of SheboyganSheboygan Co., WI

Prepared by AJS on 2015-05-15Technical Review by XXX on 2015-XX-XX

Independent Review by XXX on 2015-XX-XX

LegendUSA Topo Maps

Coordinate System: NAD 1983 HARN WISCRS Fond duLac County FeetData Sources Include: StantecOrthophotography: USGS Topo Quad 7.5

Disclaimer: Stantec assumes no responsibility for datasupplied in electronic format. The recipient accepts fullresponsibility for verifying the accuracy and completenessof the data. The recipient releases Stantec, its officers,employees, consultants and agents, from any and all claimsarising in any way from the content or provision of the data.

Sheboygan ArmorySheboygan, WisconsinProject: 193703239

Site Location

Project Location

Figure No.

Title

Client/Project

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SHEBOYGAN

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Site Layout

193703239T15N, R23E, S23C. of Sheboygan,Sheboygan Co., WI



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Armory Building

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Soil Boring and TemporaryMonitoring Well Locations

193703239T15N, R23E, S23C. of Sheboygan,Sheboygan Co., WI



Legend

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Sheboygan ArmorySheboygan, WisconsinProject # 193703239


TABLES

V:\1937\active\193703239\05_report_deliv\deliverables\reports\Sheboygan Armory Site\Phase II ESA\Table 1 - Metals and PAH, Soil Sheboygan Armory.xlsx 5/7/2015

Table 1 Soil Sample Field Screening and RCRA Metals and Polynuclear Aromatic Hydrocarbon Laboratory Results, Sheboygan Armory Site, Sheboygan, Wisconsin

Date

Dept

h(fe

et b

elow

gra

de)

PID

Resp

onse

(iui

)

Description

Tota

l Ars

enic

Tota

l Bar

ium

Tota

l Cad

miu

m

Tota

l Chr

omiu

m

Tota

l Lea

d

Tota

l Mer

cury

Tota

l Sel

eniu

m

Tota

l Silv

er

Ace

naph

then

e

Ant

hrac

ene

Benz

o(a)

an

thra

cene

Benz

o(g,

h,i)

pery

lene

Benz

o(b)

flu

oran

then

e

Benz

o(k)

flu

oran

then

e

Benz

o(a)

pyr

ene

Bis(

2-et

hylh

exyl

) ph

thal

ate

Chr

ysen

e

Fluor

anth

ene

Fluor

ene

Inde

no(1

,2,3

-cd)

py

rene

1-M

ethy

l na

phth

alen

e

2-M

ethy

l na

phth

alen

e

Nap

htha

lene

Phen

anth

rene

Pyre

ne

Industrial 8* [2.39] 100,000 803 NE 800 3.13 5,110 5110 33,000,000 100,000,000 2,110 NE 2,110 21,100 211 123,000 211,000 22,000,000 22,000,000 2,110 53,100 368,000 26,000 115,000 16,500,000Non-Industrial 8* [0.613] 15,300 70.0 NE 400 3.13 391 391 3,440,000 17,200,000 148 NE 148 1,480 15 34,700 14,800 2,290,000 2,290,000 148 15,600 229,000 5,150 115,000 1,720,000

8* [0.584] 364* [164.8] 1* [0.752] 360,000 52* [27] 0.208 0.52 0.8497 NE 196,744.2 NE NE 479.3 NE 470 NE 144.6 88,817.9 14,814.8 NE NE NE 658.7 NE 54,472.5

8 364 1 44 52 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE

SB1 (2-4) 04/09/15 2-4 <1 Silty Sand 0.84 "J" 8.6 <0.057 4.4 3.4 0.028 <0.49 <0.12 <4.7 <6.0 13 "J" 14 "J" 17 "J" <11 13 "J" <66 14 "J" 21 "J" <5.1 9.7 "J" <8.8 <6.6 <5.5 8.6 "J" 20 "J"

SB1 (6-8) 04/09/15 6-8 <1 Silty Sand - - - - - - - - 15 "J" 49 89 44 89 30 "J" 71 NA 77 190 17 "J" 35 "J" <9.4 <7.0 <5.9 160 170

SB2 (2-4) 04/09/15 2-4 <1 Silty Sand 2.0 45 <0.066 15 7.8 0.0090 "J" <0.56 <0.13 <5.0 <6.3 <5.1 <12 <8.1 <11 <7.3 <69 <10 <7.0 <5.3 <9.8 <9.2 <6.9 <5.8 <5.3 <7.5

SB2 (4-6) 04/09/15 4-6 <1 Silty Sand - - - - - - - - <6.5 <6.0 31 "J" 20 "J" 36 "J" 14 "J" 26 "J" NA 34 "J" 55 <5.1 <9.3 28 "J" 33 "J" 24 "J" 45 50

SB3 (2-4) 04/09/15 2-4 <1 Silty Clay 2.1 58 <0.061 17 7.6 0.026 0.69 <0.12 <6.6 <6.1 <4.9 <12 <7.9 <11 <7.1 <67 <9.9 <6.8 <5.1 <9.5 <8.9 <6.7 <5.6 <5.1 <7.2

SB3 (6-8) 04/09/15 6-8 <1 Sandy Gravel - - - - - - - - <4.4 <5.6 7.3 "J" <11 <7.2 <9.9 <6.5 NA <9.1 7.4 "J" <4.7 <8.7 <8.2 <6.2 <5.2 <4.7 7.7 "J"

SB4 (2-4) 04/09/15 2-4 <1 Silty Sand 0.90 "J" 19 <0.059 6.8 13 0.024 0.73 "J" <0.12 19 "J" 13 "J" 110 170 250 89 160 100 "J" 110 82 <4.9 160 60 72 57 54 150

SB4 (4-6) 04/09/15 6-8 <1 Silty Sand - - - - - - - - <4.4 <5.6 <4.5 <11 <7.2 <9.9 <6.5 NA <9.1 <6.2 <4.7 <8.7 <8.2 <6.2 <5.1 <4.7 <6.6

SB5 (2-4) 04/09/15 2-4 <1 Silty Clay 1.0 33 <0.057 11 4.5 0.015 "J" <0.49 <0.12 <4.9 <6.2 <5.0 <12 <8.0 <11 <7.2 <68 <10 <6.9 <5.2 <9.6 <9.1 <6.8 <5.7 <5.2 <7.4

SB6 (2-4) 04/09/15 2-4 <1 Silty Clay 2.4 45 <0.057 15 15 0.039 <0.49 <0.12 <5.1 11 "J" 44 25 "J" 89 56 <7.4 87 "J" 62 95 <5.4 18 "J" 150 170 130 120 99

Notes: WDNR soil RCL Summary table (January 2015) used to establish RCLs for groundwater protection and direct contact.

<x = compound not detected to a detection limit of x - = not laboratory analyzed

XX* [XXX] = standard in bold are background threshold values (BTVs) being utilized for the purpose of evaulation under ch. NR700 WAC. The established WAC RCL is noted in brackets. XXX = exceeds WDNR Industrial RCL for direct contact riskXXX = exceeds WDNR Non-Industrial RCL for direct contact riskXXX = exceeds WDNR RCL for protection of groundwater and/or BTVNE = not established by Wisconsin Administrative Code (Wis. Adm. Code) or WDNR Soil RCL Summary TableNA = not analyzed (Samples were either analyzed using Method 8270 or 8270D)* = The WDNR has determined state-wide soil background threshholed values (February 2013).

Therefore, reported values less than BTWs are not considered a direct contact or groundwater pathway concern with respect to site releases requiring further remediation action. However, the detection could represent a personal health risk if detected above health based standards.

"J" = analyte detected between the limit of detection and limit of quantificationiui = instrument units as isobutylene

RCL = residual contaminant levelNote: = For the purpose of this evaluation under ch. NR 700, background threshold values are being considered as representative of background conditions.

However, constituent concentrations less than background threshold values may represent a potential health risk if concentrations are greater than health-based standards.

Background Threshold Value

WDNR RCL for Groundwater Protection

Semi Volatile Organic Compounds/Polynuclear Aromatic Hydrocarbon Laboratory Result (microgram per kilogram)Metals (milligram per kilogram)Bo

reho

leN

umbe

r

WDNR Direct Contact RCL

V:\1937\active\193703239\05_report_deliv\deliverables\reports\Sheboygan Armory Site\Phase II ESA\Table 2 - VOCs, Soil Sheboygan Armory.xlsx 5/6/2015

Table 2 Soil Sample Field Screening and Volatile Organic Compounds Laboratory Results, Sheboygan Armory Site, Sheboygan, Wisconsin

Date

Dept

h(fe

et b

elow

gra

de)

PID

Resp

onse

(iui

)

Description

1,2,

4-

Trim

ethy

lben

zene

Benz

ene

Ethy

lben

zene

Nap

thal

ene

Toul

ene

Xyle

nes,

Tot

al

Industrial 219,000 7,410 37,000 26,000 818,000 258,000

Non-Industrial 89,800 1,490 7,470 5,150 818,000 258,000

1,379.3 5.1 1,570 658.7 1,107.2 3,940

SB1 (2-4) 04/09/15 2-4 <1 Silty Sand <12 <4.4 <7.4 <29 <6.8 <4.0

SB1 (6-8) 04/09/15 6-8 <1 Silty Sand <15 <5.1 <8.7 <34 <8.0 <4.7

SB2 (2-4) 04/09/15 2-4 <1 Silty Sand <15 <5.1 <8.7 <34 <7.9 <4.7

SB2 (4-6) 04/09/15 4-6 <1 Silty Sand <13 <4.7 <7.9 <31 16 <4.3

SB3 (2-4) 04/09/15 2-4 <1 Silty Clay <14 <5.0 <8.4 <33 <7.7 <4.6

SB3 (6-8) 04/09/15 6-8 <1 Sandy Gravel <12 <4.2 <7.1 <28 <6.5 <3.8

SB4 (2-4) 04/09/15 2-4 <1 Silty Sand 71 "J" 38 34 190 280 330

SB4 (4-6) 04/09/15 6-8 <1 Silty Sand <13 <4.5 <7.6 <30 <6.9 <4.1

SB5 (2-4) 04/09/15 2-4 <1 Silty Clay <14 <4.9 <8.4 <33 <7.7 <4.6

SB6 (2-4) 04/09/15 2-4 <1 Silty Clay <14 24 17 74 "J" 150 150

Notes: WDNR soil RCL Summary table (June 2013) used to establish RCLs for groundwater protection and direct contact.

<x = compound not detected to a detection limit of x

NE = not established by Wisconsin Administrative Code (Wis. Adm. Code) or WDNR Soil RCL Summary Table

"J"

iui = instruments units as isobutylene

RCL = residual contaminant level

WDNR RCL for Groundwater Protection**

WDNR Direct Contact RCL

= analyte detected between limit of detection and limit of quantification

Bore

hole

Num

ber

Volatile Organic Compounds Laboratory Result (microgram per kilogram)

Table 3 Groundwater Quality Results, Sheboygan Armory Site, Sheboygan, Wisconsin

Ars

enic

Bar

ium

Cad

miu

m

Ch

rom

ium

Lead

Mer

cury

Sele

niu

m

Silv

er

Bro

mod

ich

loro

met

han

e

Ch

loro

form

Dib

rom

och

loro

met

han

e

1 400 0.5 10 1.5 0.2 10 10 0.06 0.6 6

10 2,000 5 100 15 2 50 50 0.6 6 60

TW1 04/09/15 <3.8 50 <0.94 <2.4 4.6 "J" <0.061 <4.6 <1.3 <0.17 <0.20 <0.32

TW2 04/09/15 NA NA NA NA NA NA NA NA <0.17 <0.20 <0.32

TW3 04/09/15 <3.8 58 <0.94 <2.4 3.0 "J" <0.061 <4.6 <1.3 <0.17 <0.20 <0.32

TW4 04/09/15 NA NA NA NA NA NA NA NA 3.6 15 0.98 "J"

NE = not established by Wisconsin Administrative Code (Wis. Adm. Code)NA = not analyzed <x = compound not detected to a detection limit of xJ = analyte detected between the limit of detection and the limit of quantitation

N/a = well was dry, no sample collectedXXX = exceeds NR 140, Wis. Adm. Code prevention action limit (PAL)XXX = exceeds NR 140, Wis. Adm. Code enforcement standard (ES)

NR 140, Wis. Adm. Code ES

VOCs (micrograms per liter)

Sample Location

DateSampled

RCRA Metals (micrograms per liter)

NR 140, Wis. Adm. Code PAL


APPENDICES


APPENDIX A – SOIL BORING LOGS


APPENDIX B – SOIL BOREHOLE ABANDONMENT FORMS


APPENDIX C – SOIL AND GROUNDWATER LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY FORM

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200

TestAmerica Job ID: 500-94669-2Client Project/Site: Muni. Aud & Armory 193703239 Task 3.0.2

For:Stantec Consulting Corporation/Bonestroo12075 Corporate ParkwaySuite 200Mequon, Wisconsin 53092

Attn: Stu Gross

Authorized for release by:4/24/2015 4:45:55 PMBonnie Stadelmann, Senior Project [email protected]

Designee for

Sandie Fredrick, Project Manager II(920)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Stantec Consulting Corporation/BonestrooProject/Site: Muni. Aud & Armory 193703239 Task 3.0.2

TestAmerica Job ID: 500-94669-2

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

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Case NarrativeClient: Stantec Consulting Corporation/Bonestroo TestAmerica Job ID: 500-94669-2

Project/Site: Muni. Aud & Armory 193703239 Task 3.0.2

Job ID: 500-94669-2

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-94669-2

Comments

No additional comments.

Receipt

The samples were received on 4/15/2015 10:15 AM; the samples arrived in good condition, properly preserved and, where required, on

ice. The temperatures of the 2 coolers at receipt time were 3.1º C and 4.2º C.

GC/MS VOA

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC/MS Semi VOA

Method(s) 8270D: The following sample was diluted due to the nature of the sample matrix: TW3 (500-94669-15). Elevated reporting

limits (RLs) are provided.

Method(s) 8270D: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation

batch 500-283982 recovered outside control limits (20%) for the following analytes: 2,2'-oxybis[1-chloropropane] at 25%;

3,3'-Dichlorobenzidine at 23%; Bis(2-chloroethoxy)methane at 23%; and Bis(2-chloroethyl)ether at 23%. All % recoveries were within

limits. No further action was required.TW1 (500-94669-13), TW2 (500-94669-14), TW3 (500-94669-15), TW4 (500-94669-16) and TW1 FD

(500-94669-18)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals


Organic Prep


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Detection SummaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Client Sample ID: TW1 Lab Sample ID: 500-94669-13

Barium

RL

0.010 mg/L

MDL

0.0022

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total

Recoverable

10.050 6010B

Lead 0.0050 mg/L0.0025 Total

Recoverable

10.0046 J 6010B


No Detections.


Barium

RL

0.010 mg/L

MDL

0.0022


Total

Recoverable

10.058 6010B


Recoverable

10.0030 J 6010B


Bromodichloromethane

RL

1.0 ug/L

MDL

0.17


Total/NA13.6 8260B

Chloroform 1.0 ug/L0.20 Total/NA115 8260B

Dibromochloromethane 1.0 ug/L0.32 Total/NA10.98 J 8260B

Client Sample ID: Trip Blank Lab Sample ID: 500-94669-17

No Detections.

Client Sample ID: TW1 FD Lab Sample ID: 500-94669-18

Barium

RL

0.010 mg/L

MDL

0.0022


Total

Recoverable

10.050 6010B


Recoverable

10.0062 6010B

Selenium 0.010 mg/L0.0046 Total

Recoverable

10.0050 J 6010B

TestAmerica Chicago

This Detection Summary does not include radiochemical test results.

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Method SummaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL CHI

SW8468270D Semivolatile Organic Compounds (GC/MS) TAL CHI

SW8466010B Metals (ICP) TAL CHI

SW8467470A Mercury (CVAA) TAL CHI

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

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Sample SummaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

500-94669-13 TW1 Water 04/09/15 10:50 04/15/15 10:15

500-94669-14 TW2 Water 04/09/15 12:25 04/15/15 10:15

500-94669-15 TW3 Water 04/09/15 10:00 04/15/15 10:15

500-94669-16 TW4 Water 04/09/15 13:30 04/15/15 10:15

500-94669-17 Trip Blank Water 04/09/15 00:00 04/15/15 10:15

500-94669-18 TW1 FD Water 04/09/15 11:00 04/15/15 10:15

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Client Sample ResultsTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Lab Sample ID: 500-94669-13Client Sample ID: TW1Matrix: WaterDate Collected: 04/09/15 10:50

Date Received: 04/15/15 10:15

Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL

1,1,1,2-Tetrachloroethane <0.25 1.0 0.25 ug/L 04/22/15 05:13 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 0.20 ug/L 04/22/15 05:13 11,1,1-Trichloroethane <0.20

1.0 0.23 ug/L 04/22/15 05:13 11,1,2,2-Tetrachloroethane <0.23


1.0 0.19 ug/L 04/22/15 05:13 11,1-Dichloroethane <0.19

1.0 0.31 ug/L 04/22/15 05:13 11,1-Dichloroethene <0.31

1.0 0.34 ug/L 04/22/15 05:13 11,1-Dichloropropene <0.34

1.0 0.24 ug/L 04/22/15 05:13 11,2,3-Trichlorobenzene <0.24

1.0 0.45 ug/L 04/22/15 05:13 11,2,3-Trichloropropane <0.45


1.0 0.14 ug/L 04/22/15 05:13 11,2,4-Trimethylbenzene <0.14

2.0 0.87 ug/L 04/22/15 05:13 11,2-Dibromo-3-Chloropropane <0.87

1.0 0.36 ug/L 04/22/15 05:13 11,2-Dibromoethane <0.36

1.0 0.27 ug/L 04/22/15 05:13 11,2-Dichlorobenzene <0.27


1.0 0.20 ug/L 04/22/15 05:13 11,2-Dichloropropane <0.20






1.0 0.21 ug/L 04/22/15 05:13 12-Chlorotoluene <0.21


0.50 0.074 ug/L 04/22/15 05:13 1Benzene <0.074

1.0 0.25 ug/L 04/22/15 05:13 1Bromobenzene <0.25

1.0 0.40 ug/L 04/22/15 05:13 1Bromochloromethane <0.40

1.0 0.17 ug/L 04/22/15 05:13 1Bromodichloromethane <0.17

1.0 0.28 ug/L 04/22/15 05:13 1Bromoform <0.28

1.0 0.31 ug/L 04/22/15 05:13 1Bromomethane <0.31

1.0 0.26 ug/L 04/22/15 05:13 1Carbon tetrachloride <0.26

1.0 0.14 ug/L 04/22/15 05:13 1Chlorobenzene <0.14

1.0 0.34 ug/L 04/22/15 05:13 1Chloroethane <0.34

1.0 0.20 ug/L 04/22/15 05:13 1Chloroform <0.20

1.0 0.18 ug/L 04/22/15 05:13 1Chloromethane <0.18

1.0 0.12 ug/L 04/22/15 05:13 1cis-1,2-Dichloroethene <0.12

1.0 0.18 ug/L 04/22/15 05:13 1cis-1,3-Dichloropropene <0.18

1.0 0.32 ug/L 04/22/15 05:13 1Dibromochloromethane <0.32

1.0 0.33 ug/L 04/22/15 05:13 1Dibromomethane <0.33

1.0 0.20 ug/L 04/22/15 05:13 1Dichlorodifluoromethane <0.20

0.50 0.13 ug/L 04/22/15 05:13 1Ethylbenzene <0.13

1.0 0.26 ug/L 04/22/15 05:13 1Hexachlorobutadiene <0.26

1.0 0.15 ug/L 04/22/15 05:13 1Isopropyl ether <0.15

1.0 0.14 ug/L 04/22/15 05:13 1Isopropylbenzene <0.14

1.0 0.24 ug/L 04/22/15 05:13 1Methyl tert-butyl ether <0.24

5.0 0.68 ug/L 04/22/15 05:13 1Methylene Chloride <0.68

1.0 0.16 ug/L 04/22/15 05:13 1Naphthalene <0.16

1.0 0.13 ug/L 04/22/15 05:13 1n-Butylbenzene <0.13

1.0 0.13 ug/L 04/22/15 05:13 1N-Propylbenzene <0.13

1.0 0.17 ug/L 04/22/15 05:13 1p-Isopropyltoluene <0.17

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL

sec-Butylbenzene <0.15 1.0 0.15 ug/L 04/22/15 05:13 1


1.0 0.10 ug/L 04/22/15 05:13 1Styrene <0.10

1.0 0.14 ug/L 04/22/15 05:13 1tert-Butylbenzene <0.14

1.0 0.17 ug/L 04/22/15 05:13 1Tetrachloroethene <0.17

0.50 0.11 ug/L 04/22/15 05:13 1Toluene <0.11

1.0 0.25 ug/L 04/22/15 05:13 1trans-1,2-Dichloroethene <0.25

1.0 0.21 ug/L 04/22/15 05:13 1trans-1,3-Dichloropropene <0.21

0.50 0.19 ug/L 04/22/15 05:13 1Trichloroethene <0.19

1.0 0.19 ug/L 04/22/15 05:13 1Trichlorofluoromethane <0.19

0.50 0.10 ug/L 04/22/15 05:13 1Vinyl chloride <0.10

1.0 0.068 ug/L 04/22/15 05:13 1Xylenes, Total <0.068

1,2-Dichloroethane-d4 (Surr) 97 75 - 125 04/22/15 05:13 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 82 04/22/15 05:13 175 - 120

Dibromofluoromethane 100 04/22/15 05:13 175 - 120

Toluene-d8 (Surr) 96 04/22/15 05:13 175 - 120

Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL

1,2,4-Trichlorobenzene <0.19 1.6 0.19 ug/L 04/15/15 16:41 04/16/15 16:39 1


1.6 0.19 ug/L 04/15/15 16:41 04/16/15 16:39 11,2-Dichlorobenzene <0.19



0.79 0.24 ug/L 04/15/15 16:41 04/16/15 16:39 11-Methylnaphthalene <0.24

1.6 0.30 ug/L 04/15/15 16:41 04/16/15 16:39 12,2'-oxybis[1-chloropropane] <0.30 *

7.9 2.0 ug/L 04/15/15 16:41 04/16/15 16:39 12,4,5-Trichlorophenol <2.0


7.9 2.1 ug/L 04/15/15 16:41 04/16/15 16:39 12,4-Dichlorophenol <2.1

7.9 1.4 ug/L 04/15/15 16:41 04/16/15 16:39 12,4-Dimethylphenol <1.4

16 6.8 ug/L 04/15/15 16:41 04/16/15 16:39 12,4-Dinitrophenol <6.8

0.79 0.19 ug/L 04/15/15 16:41 04/16/15 16:39 12,4-Dinitrotoluene <0.19


1.6 0.19 ug/L 04/15/15 16:41 04/16/15 16:39 12-Chloronaphthalene <0.19

4.0 0.44 ug/L 04/15/15 16:41 04/16/15 16:39 12-Chlorophenol <0.44


1.6 0.24 ug/L 04/15/15 16:41 04/16/15 16:39 12-Methylphenol <0.24

4.0 1.0 ug/L 04/15/15 16:41 04/16/15 16:39 12-Nitroaniline <1.0

7.9 2.0 ug/L 04/15/15 16:41 04/16/15 16:39 12-Nitrophenol <2.0

1.6 0.35 ug/L 04/15/15 16:41 04/16/15 16:39 13 & 4 Methylphenol <0.35

4.0 1.4 ug/L 04/15/15 16:41 04/16/15 16:39 13,3'-Dichlorobenzidine <1.4 *


16 4.7 ug/L 04/15/15 16:41 04/16/15 16:39 14,6-Dinitro-2-methylphenol <4.7

4.0 0.43 ug/L 04/15/15 16:41 04/16/15 16:39 14-Bromophenyl phenyl ether <0.43

7.9 1.8 ug/L 04/15/15 16:41 04/16/15 16:39 14-Chloro-3-methylphenol <1.8

7.9 1.6 ug/L 04/15/15 16:41 04/16/15 16:39 14-Chloroaniline <1.6

4.0 0.50 ug/L 04/15/15 16:41 04/16/15 16:39 14-Chlorophenyl phenyl ether <0.50


16 5.9 ug/L 04/15/15 16:41 04/16/15 16:39 14-Nitrophenol <5.9

0.79 0.24 ug/L 04/15/15 16:41 04/16/15 16:39 1Acenaphthene <0.24

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Acenaphthylene <0.21 0.79 0.21 ug/L 04/15/15 16:41 04/16/15 16:39 1


0.79 0.26 ug/L 04/15/15 16:41 04/16/15 16:39 1Anthracene <0.26

0.16 0.045 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzo[a]anthracene <0.045

0.16 0.078 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzo[a]pyrene <0.078

0.16 0.064 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzo[b]fluoranthene <0.064

0.79 0.30 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzo[g,h,i]perylene <0.30

0.16 0.051 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzo[k]fluoranthene <0.051

16 4.6 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzoic acid <4.6

16 4.8 ug/L 04/15/15 16:41 04/16/15 16:39 1Benzyl alcohol <4.8

1.6 0.22 ug/L 04/15/15 16:41 04/16/15 16:39 1Bis(2-chloroethoxy)methane <0.22 *

1.6 0.23 ug/L 04/15/15 16:41 04/16/15 16:39 1Bis(2-chloroethyl)ether <0.23 *

7.9 1.4 ug/L 04/15/15 16:41 04/16/15 16:39 1Bis(2-ethylhexyl) phthalate <1.4

1.6 0.38 ug/L 04/15/15 16:41 04/16/15 16:39 1Butyl benzyl phthalate <0.38

4.0 0.28 ug/L 04/15/15 16:41 04/16/15 16:39 1Carbazole <0.28

0.40 0.054 ug/L 04/15/15 16:41 04/16/15 16:39 1Chrysene <0.054

0.24 0.040 ug/L 04/15/15 16:41 04/16/15 16:39 1Dibenz(a,h)anthracene <0.040

1.6 0.21 ug/L 04/15/15 16:41 04/16/15 16:39 1Dibenzofuran <0.21

1.6 0.29 ug/L 04/15/15 16:41 04/16/15 16:39 1Diethyl phthalate <0.29

1.6 0.25 ug/L 04/15/15 16:41 04/16/15 16:39 1Dimethyl phthalate <0.25

4.0 0.58 ug/L 04/15/15 16:41 04/16/15 16:39 1Di-n-butyl phthalate <0.58

7.9 0.83 ug/L 04/15/15 16:41 04/16/15 16:39 1Di-n-octyl phthalate <0.83

0.79 0.36 ug/L 04/15/15 16:41 04/16/15 16:39 1Fluoranthene <0.36

0.79 0.19 ug/L 04/15/15 16:41 04/16/15 16:39 1Fluorene <0.19

0.40 0.063 ug/L 04/15/15 16:41 04/16/15 16:39 1Hexachlorobenzene <0.063

4.0 0.41 ug/L 04/15/15 16:41 04/16/15 16:39 1Hexachlorobutadiene <0.41

16 5.0 ug/L 04/15/15 16:41 04/16/15 16:39 1Hexachlorocyclopentadiene <5.0

4.0 0.47 ug/L 04/15/15 16:41 04/16/15 16:39 1Hexachloroethane <0.47

0.16 0.059 ug/L 04/15/15 16:41 04/16/15 16:39 1Indeno[1,2,3-cd]pyrene <0.059

1.6 0.30 ug/L 04/15/15 16:41 04/16/15 16:39 1Isophorone <0.30

0.79 0.24 ug/L 04/15/15 16:41 04/16/15 16:39 1Naphthalene <0.24

0.79 0.35 ug/L 04/15/15 16:41 04/16/15 16:39 1Nitrobenzene <0.35

0.40 0.12 ug/L 04/15/15 16:41 04/16/15 16:39 1N-Nitrosodi-n-propylamine <0.12

0.79 0.29 ug/L 04/15/15 16:41 04/16/15 16:39 1N-Nitrosodiphenylamine <0.29

16 3.1 ug/L 04/15/15 16:41 04/16/15 16:39 1Pentachlorophenol <3.1

0.79 0.24 ug/L 04/15/15 16:41 04/16/15 16:39 1Phenanthrene <0.24

4.0 0.53 ug/L 04/15/15 16:41 04/16/15 16:39 1Phenol <0.53

0.79 0.34 ug/L 04/15/15 16:41 04/16/15 16:39 1Pyrene <0.34

2,4,6-Tribromophenol (Surr) 100 53 - 150 04/15/15 16:41 04/16/15 16:39 1


2-Fluorobiphenyl 91 04/15/15 16:41 04/16/15 16:39 141 - 132

2-Fluorophenol (Surr) 65 04/15/15 16:41 04/16/15 16:39 132 - 110

Nitrobenzene-d5 (Surr) 88 04/15/15 16:41 04/16/15 16:39 147 - 134

Phenol-d5 (Surr) 45 04/15/15 16:41 04/16/15 16:39 125 - 100

Terphenyl-d14 (Surr) 115 04/15/15 16:41 04/16/15 16:39 159 - 150

Method: 6010B - Metals (ICP) - Total RecoverableRL MDL

Arsenic <0.0038 0.010 0.0038 mg/L 04/15/15 15:30 04/17/15 04:27 1


0.010 0.0022 mg/L 04/15/15 15:30 04/17/15 04:27 1Barium 0.050

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Method: 6010B - Metals (ICP) - Total Recoverable (Continued)RL MDL

Cadmium <0.00094 0.0020 0.00094 mg/L 04/15/15 15:30 04/17/15 04:27 1


0.010 0.0024 mg/L 04/15/15 15:30 04/17/15 04:27 1Chromium <0.0024

0.0050 0.0025 mg/L 04/15/15 15:30 04/17/15 04:27 1Lead 0.0046 J

0.010 0.0046 mg/L 04/15/15 15:30 04/17/15 04:27 1Selenium <0.0046

0.0050 0.0013 mg/L 04/15/15 15:30 04/17/15 04:27 1Silver <0.0013

Method: 7470A - Mercury (CVAA)RL MDL

Mercury <0.061 0.20 0.061 ug/L 04/16/15 12:00 04/17/15 12:36 1





























0.50 0.074 ug/L 04/22/15 05:41 1Benzene <0.074




1.0 0.28 ug/L 04/22/15 05:41 1Bromoform <0.28





1.0 0.20 ug/L 04/22/15 05:41 1Chloroform <0.20


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cis-1,2-Dichloroethene <0.12 1.0 0.12 ug/L 04/22/15 05:41 1












1.0 0.16 ug/L 04/22/15 05:41 1Naphthalene <0.16




1.0 0.15 ug/L 04/22/15 05:41 1sec-Butylbenzene <0.15

1.0 0.10 ug/L 04/22/15 05:41 1Styrene <0.10



0.50 0.11 ug/L 04/22/15 05:41 1Toluene <0.11











Toluene-d8 (Surr) 97 04/22/15 05:41 175 - 120


















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2-Methylnaphthalene <0.049 0.38 0.049 ug/L 04/15/15 16:41 04/16/15 17:08 1




7.6 1.9 ug/L 04/15/15 16:41 04/16/15 17:08 12-Nitrophenol <1.9










15 5.6 ug/L 04/15/15 16:41 04/16/15 17:08 14-Nitrophenol <5.6


0.76 0.20 ug/L 04/15/15 16:41 04/16/15 17:08 1Acenaphthylene <0.20

0.76 0.25 ug/L 04/15/15 16:41 04/16/15 17:08 1Anthracene <0.25






15 4.4 ug/L 04/15/15 16:41 04/16/15 17:08 1Benzoic acid <4.4






3.8 0.27 ug/L 04/15/15 16:41 04/16/15 17:08 1Carbazole <0.27

0.38 0.052 ug/L 04/15/15 16:41 04/16/15 17:08 1Chrysene <0.052








0.76 0.18 ug/L 04/15/15 16:41 04/16/15 17:08 1Fluorene <0.18






1.5 0.28 ug/L 04/15/15 16:41 04/16/15 17:08 1Isophorone <0.28

0.76 0.23 ug/L 04/15/15 16:41 04/16/15 17:08 1Naphthalene <0.23





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Phenanthrene <0.23 0.76 0.23 ug/L 04/15/15 16:41 04/16/15 17:08 1


3.8 0.51 ug/L 04/15/15 16:41 04/16/15 17:08 1Phenol <0.51

0.76 0.32 ug/L 04/15/15 16:41 04/16/15 17:08 1Pyrene <0.32



2-Fluorobiphenyl 95 04/15/15 16:41 04/16/15 17:08 141 - 132



Phenol-d5 (Surr) 47 04/15/15 16:41 04/16/15 17:08 125 - 100

Terphenyl-d14 (Surr) 115 04/15/15 16:41 04/16/15 17:08 159 - 150




























0.50 0.074 ug/L 04/22/15 06:08 1Benzene <0.074




1.0 0.28 ug/L 04/22/15 06:08 1Bromoform <0.28





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Chloroform <0.20 1.0 0.20 ug/L 04/22/15 06:08 1














1.0 0.16 ug/L 04/22/15 06:08 1Naphthalene <0.16





1.0 0.10 ug/L 04/22/15 06:08 1Styrene <0.10



0.50 0.11 ug/L 04/22/15 06:08 1Toluene <0.11











Toluene-d8 (Surr) 95 04/22/15 06:08 175 - 120









37 9.6 ug/L 04/15/15 16:41 04/17/15 12:18 52,4,5-Trichlorophenol <9.6

19 2.7 ug/L 04/15/15 16:41 04/17/15 12:18 52,4,6-Trichlorophenol <2.7

37 9.7 ug/L 04/15/15 16:41 04/17/15 12:18 52,4-Dichlorophenol <9.7

37 6.7 ug/L 04/15/15 16:41 04/17/15 12:18 52,4-Dimethylphenol <6.7

75 32 ug/L 04/15/15 16:41 04/17/15 12:18 52,4-Dinitrophenol <32



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2-Chloronaphthalene <0.88 7.5 0.88 ug/L 04/15/15 16:41 04/17/15 12:18 5


19 2.1 ug/L 04/15/15 16:41 04/17/15 12:18 52-Chlorophenol <2.1



19 4.8 ug/L 04/15/15 16:41 04/17/15 12:18 52-Nitroaniline <4.8

37 9.3 ug/L 04/15/15 16:41 04/17/15 12:18 52-Nitrophenol <9.3


19 6.4 ug/L 04/15/15 16:41 04/17/15 12:18 53,3'-Dichlorobenzidine <6.4 *


75 22 ug/L 04/15/15 16:41 04/17/15 12:18 54,6-Dinitro-2-methylphenol <22

19 2.0 ug/L 04/15/15 16:41 04/17/15 12:18 54-Bromophenyl phenyl ether <2.0

37 8.6 ug/L 04/15/15 16:41 04/17/15 12:18 54-Chloro-3-methylphenol <8.6

37 7.5 ug/L 04/15/15 16:41 04/17/15 12:18 54-Chloroaniline <7.5

19 2.4 ug/L 04/15/15 16:41 04/17/15 12:18 54-Chlorophenyl phenyl ether <2.4


75 28 ug/L 04/15/15 16:41 04/17/15 12:18 54-Nitrophenol <28



3.7 1.2 ug/L 04/15/15 16:41 04/17/15 12:18 5Anthracene <1.2






75 22 ug/L 04/15/15 16:41 04/17/15 12:18 5Benzoic acid <22

75 23 ug/L 04/15/15 16:41 04/17/15 12:18 5Benzyl alcohol <23



37 6.4 ug/L 04/15/15 16:41 04/17/15 12:18 5Bis(2-ethylhexyl) phthalate <6.4


19 1.3 ug/L 04/15/15 16:41 04/17/15 12:18 5Carbazole <1.3

1.9 0.25 ug/L 04/15/15 16:41 04/17/15 12:18 5Chrysene <0.25





19 2.7 ug/L 04/15/15 16:41 04/17/15 12:18 5Di-n-butyl phthalate <2.7

37 3.9 ug/L 04/15/15 16:41 04/17/15 12:18 5Di-n-octyl phthalate <3.9


3.7 0.91 ug/L 04/15/15 16:41 04/17/15 12:18 5Fluorene <0.91


19 1.9 ug/L 04/15/15 16:41 04/17/15 12:18 5Hexachlorobutadiene <1.9

75 24 ug/L 04/15/15 16:41 04/17/15 12:18 5Hexachlorocyclopentadiene <24

19 2.2 ug/L 04/15/15 16:41 04/17/15 12:18 5Hexachloroethane <2.2


7.5 1.4 ug/L 04/15/15 16:41 04/17/15 12:18 5Isophorone <1.4

3.7 1.2 ug/L 04/15/15 16:41 04/17/15 12:18 5Naphthalene <1.2



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N-Nitrosodiphenylamine <1.4 3.7 1.4 ug/L 04/15/15 16:41 04/17/15 12:18 5


75 15 ug/L 04/15/15 16:41 04/17/15 12:18 5Pentachlorophenol <15


19 2.5 ug/L 04/15/15 16:41 04/17/15 12:18 5Phenol <2.5

3.7 1.6 ug/L 04/15/15 16:41 04/17/15 12:18 5Pyrene <1.6



2-Fluorobiphenyl 107 04/15/15 16:41 04/17/15 12:18 541 - 132



Phenol-d5 (Surr) 25 04/15/15 16:41 04/17/15 12:18 525 - 100

Terphenyl-d14 (Surr) 108 04/15/15 16:41 04/17/15 12:18 559 - 150


Arsenic <0.0038 0.010 0.0038 mg/L 04/15/15 15:30 04/17/15 04:59 1


0.010 0.0022 mg/L 04/15/15 15:30 04/17/15 04:59 1Barium 0.058

0.0020 0.00094 mg/L 04/15/15 15:30 04/17/15 04:59 1Cadmium <0.00094

0.010 0.0024 mg/L 04/15/15 15:30 04/17/15 04:59 1Chromium <0.0024

0.0050 0.0025 mg/L 04/15/15 15:30 04/17/15 04:59 1Lead 0.0030 J

0.010 0.0046 mg/L 04/15/15 15:30 04/17/15 04:59 1Selenium <0.0046

0.0050 0.0013 mg/L 04/15/15 15:30 04/17/15 04:59 1Silver <0.0013


Mercury <0.061 0.20 0.061 ug/L 04/16/15 12:00 04/17/15 12:38 1






















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1,3,5-Trimethylbenzene <0.18 1.0 0.18 ug/L 04/22/15 06:35 1








0.50 0.074 ug/L 04/22/15 06:35 1Benzene <0.074



1.0 0.17 ug/L 04/22/15 06:35 1Bromodichloromethane 3.6

1.0 0.28 ug/L 04/22/15 06:35 1Bromoform <0.28





1.0 0.20 ug/L 04/22/15 06:35 1Chloroform 15




1.0 0.32 ug/L 04/22/15 06:35 1Dibromochloromethane 0.98 J









1.0 0.16 ug/L 04/22/15 06:35 1Naphthalene <0.16





1.0 0.10 ug/L 04/22/15 06:35 1Styrene <0.10



0.50 0.11 ug/L 04/22/15 06:35 1Toluene <0.11











Toluene-d8 (Surr) 95 04/22/15 06:35 175 - 120

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7.4 1.9 ug/L 04/15/15 16:41 04/16/15 18:07 12-Nitrophenol <1.9










15 5.5 ug/L 04/15/15 16:41 04/16/15 18:07 14-Nitrophenol <5.5



0.74 0.25 ug/L 04/15/15 16:41 04/16/15 18:07 1Anthracene <0.25






15 4.3 ug/L 04/15/15 16:41 04/16/15 18:07 1Benzoic acid <4.3






3.7 0.26 ug/L 04/15/15 16:41 04/16/15 18:07 1Carbazole <0.26

0.37 0.051 ug/L 04/15/15 16:41 04/16/15 18:07 1Chrysene <0.051





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Di-n-butyl phthalate <0.54 3.7 0.54 ug/L 04/15/15 16:41 04/16/15 18:07 1




0.74 0.18 ug/L 04/15/15 16:41 04/16/15 18:07 1Fluorene <0.18






1.5 0.28 ug/L 04/15/15 16:41 04/16/15 18:07 1Isophorone <0.28

0.74 0.23 ug/L 04/15/15 16:41 04/16/15 18:07 1Naphthalene <0.23






3.7 0.50 ug/L 04/15/15 16:41 04/16/15 18:07 1Phenol <0.50

0.74 0.32 ug/L 04/15/15 16:41 04/16/15 18:07 1Pyrene <0.32



2-Fluorobiphenyl 90 04/15/15 16:41 04/16/15 18:07 141 - 132



Phenol-d5 (Surr) 42 04/15/15 16:41 04/16/15 18:07 125 - 100

Terphenyl-d14 (Surr) 116 04/15/15 16:41 04/16/15 18:07 159 - 150

Lab Sample ID: 500-94669-17Client Sample ID: Trip BlankMatrix: WaterDate Collected: 04/09/15 00:00





















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Lab Sample ID: 500-94669-17Client Sample ID: Trip BlankMatrix: WaterDate Collected: 04/09/15 00:00



1,3-Dichlorobenzene <0.15 1.0 0.15 ug/L 04/22/15 00:39 1







0.50 0.074 ug/L 04/22/15 00:39 1Benzene <0.074




1.0 0.28 ug/L 04/22/15 00:39 1Bromoform <0.28





1.0 0.20 ug/L 04/22/15 00:39 1Chloroform <0.20













1.0 0.16 ug/L 04/22/15 00:39 1Naphthalene <0.16





1.0 0.10 ug/L 04/22/15 00:39 1Styrene <0.10



0.50 0.11 ug/L 04/22/15 00:39 1Toluene <0.11











Toluene-d8 (Surr) 97 04/22/15 00:39 175 - 120

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Lab Sample ID: 500-94669-18Client Sample ID: TW1 FDMatrix: WaterDate Collected: 04/09/15 11:00



























0.50 0.074 ug/L 04/22/15 07:03 1Benzene <0.074




1.0 0.28 ug/L 04/22/15 07:03 1Bromoform <0.28





1.0 0.20 ug/L 04/22/15 07:03 1Chloroform <0.20













1.0 0.16 ug/L 04/22/15 07:03 1Naphthalene <0.16




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sec-Butylbenzene <0.15 1.0 0.15 ug/L 04/22/15 07:03 1


1.0 0.10 ug/L 04/22/15 07:03 1Styrene <0.10



0.50 0.11 ug/L 04/22/15 07:03 1Toluene <0.11











Toluene-d8 (Surr) 94 04/22/15 07:03 175 - 120





















8.0 2.0 ug/L 04/15/15 16:41 04/16/15 18:36 12-Nitrophenol <2.0










16 5.9 ug/L 04/15/15 16:41 04/16/15 18:36 14-Nitrophenol <5.9


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Acenaphthylene <0.21 0.80 0.21 ug/L 04/15/15 16:41 04/16/15 18:36 1


0.80 0.27 ug/L 04/15/15 16:41 04/16/15 18:36 1Anthracene <0.27






16 4.6 ug/L 04/15/15 16:41 04/16/15 18:36 1Benzoic acid <4.6






4.0 0.28 ug/L 04/15/15 16:41 04/16/15 18:36 1Carbazole <0.28

0.40 0.054 ug/L 04/15/15 16:41 04/16/15 18:36 1Chrysene <0.054








0.80 0.19 ug/L 04/15/15 16:41 04/16/15 18:36 1Fluorene <0.19






1.6 0.30 ug/L 04/15/15 16:41 04/16/15 18:36 1Isophorone <0.30

0.80 0.25 ug/L 04/15/15 16:41 04/16/15 18:36 1Naphthalene <0.25






4.0 0.54 ug/L 04/15/15 16:41 04/16/15 18:36 1Phenol <0.54

0.80 0.34 ug/L 04/15/15 16:41 04/16/15 18:36 1Pyrene <0.34



2-Fluorobiphenyl 92 04/15/15 16:41 04/16/15 18:36 141 - 132



Phenol-d5 (Surr) 47 04/15/15 16:41 04/16/15 18:36 125 - 100

Terphenyl-d14 (Surr) 112 04/15/15 16:41 04/16/15 18:36 159 - 150


Arsenic <0.0038 0.010 0.0038 mg/L 04/15/15 15:30 04/17/15 05:03 1


0.010 0.0022 mg/L 04/15/15 15:30 04/17/15 05:03 1Barium 0.050

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Method: 6010B - Metals (ICP) - Total Recoverable (Continued)RL MDL

Cadmium <0.00094 0.0020 0.00094 mg/L 04/15/15 15:30 04/17/15 05:03 1


0.010 0.0024 mg/L 04/15/15 15:30 04/17/15 05:03 1Chromium <0.0024

0.0050 0.0025 mg/L 04/15/15 15:30 04/17/15 05:03 1Lead 0.0062

0.010 0.0046 mg/L 04/15/15 15:30 04/17/15 05:03 1Selenium 0.0050 J

0.0050 0.0013 mg/L 04/15/15 15:30 04/17/15 05:03 1Silver <0.0013


Mercury <0.061 0.20 0.061 ug/L 04/16/15 12:00 04/17/15 12:40 1


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Definitions/GlossaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Qualifiers

GC/MS VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

GC/MS Semi VOA


* RPD of the LCS and LCSD exceeds the control limits

Qualifier


Metals



Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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QC Association SummaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


GC/MS VOA

Analysis Batch: 284724

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B500-94669-13 TW1 Total/NA




Water 8260B500-94669-17 Trip Blank Total/NA

Water 8260B500-94669-18 TW1 FD Total/NA

Water 8260BLCS 500-284724/4 Lab Control Sample Total/NA

Water 8260BMB 500-284724/28 Method Blank Total/NA

GC/MS Semi VOA

Prep Batch: 283982


Water 3510C500-94669-13 TW1 Total/NA




Water 3510C500-94669-18 TW1 FD Total/NA

Water 3510CLCS 500-283982/2-A Lab Control Sample Total/NA

Water 3510CLCSD 500-283982/3-A Lab Control Sample Dup Total/NA

Water 3510CMB 500-283982/1-A Method Blank Total/NA



Water 8270D 283982500-94669-13 TW1 Total/NA



Water 8270D 283982500-94669-18 TW1 FD Total/NA

Water 8270D 283982LCS 500-283982/2-A Lab Control Sample Total/NA

Water 8270D 283982LCSD 500-283982/3-A Lab Control Sample Dup Total/NA

Water 8270D 283982MB 500-283982/1-A Method Blank Total/NA




Metals

Prep Batch: 283993


Water 3005A500-94669-13 TW1 Total Recoverable

Water 3005A500-94669-13 DU TW1 Total Recoverable

Water 3005A500-94669-13 MS TW1 Total Recoverable

Water 3005A500-94669-13 MSD TW1 Total Recoverable

Water 3005A500-94669-15 TW3 Total Recoverable

Water 3005A500-94669-18 TW1 FD Total Recoverable

Water 3005ALCS 500-283993/2-A Lab Control Sample Total Recoverable

Water 3005AMB 500-283993/1-A Method Blank Total Recoverable

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Metals (Continued)

Prep Batch: 284159


Water 7470A500-94669-13 TW1 Total/NA

Water 7470A500-94669-15 TW3 Total/NA

Water 7470A500-94669-18 TW1 FD Total/NA

Water 7470ALCS 500-284159/13-A Lab Control Sample Total/NA

Water 7470AMB 500-284159/12-A Method Blank Total/NA



Water 6010B 283993500-94669-13 TW1 Total Recoverable

Water 6010B 283993500-94669-13 DU TW1 Total Recoverable

Water 6010B 283993500-94669-13 MS TW1 Total Recoverable

Water 6010B 283993500-94669-13 MSD TW1 Total Recoverable

Water 6010B 283993500-94669-15 TW3 Total Recoverable

Water 6010B 283993500-94669-18 TW1 FD Total Recoverable

Water 6010B 283993LCS 500-283993/2-A Lab Control Sample Total Recoverable

Water 6010B 283993MB 500-283993/1-A Method Blank Total Recoverable



Water 7470A 284159500-94669-13 TW1 Total/NA

Water 7470A 284159500-94669-15 TW3 Total/NA

Water 7470A 284159500-94669-18 TW1 FD Total/NA

Water 7470A 284159LCS 500-284159/13-A Lab Control Sample Total/NA

Water 7470A 284159MB 500-284159/12-A Method Blank Total/NA

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Surrogate SummaryTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE BFB DBFM TOL

97 82 100 96500-94669-13

Percent Surrogate Recovery (Acceptance Limits)

TW1

111 85 109 97500-94669-14 TW2

98 84 103 95500-94669-15 TW3

97 84 99 95500-94669-16 TW4

104 86 107 97500-94669-17 Trip Blank

100 83 100 94500-94669-18 TW1 FD

98 93 98 93LCS 500-284724/4 Lab Control Sample

100 84 100 95MB 500-284724/28 Method Blank

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (53-150) (41-132) (32-110) (47-134) (25-100) (59-150)

TBP FBP 2FP NBZ PHL TPH

100 91 65 88 45 115500-94669-13


TW1

98 95 65 4790 115500-94669-14 TW2

137 107 74 2561 108500-94669-15 TW3

100 90 61 4287 116500-94669-16 TW4

97 92 65 4788 112500-94669-18 TW1 FD

107 84 73 6189 112LCS 500-283982/2-A Lab Control Sample

107 79 96 5380 106LCSD 500-283982/3-A Lab Control Sample Dup

93 84 63 4882 107MB 500-283982/1-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol (Surr)

FBP = 2-Fluorobiphenyl

2FP = 2-Fluorophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPH = Terphenyl-d14 (Surr)

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QC Sample ResultsTestAmerica Job ID: 500-94669-2Client: Stantec Consulting Corporation/Bonestroo


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 500-284724/28

Matrix: Water Prep Type: Total/NA


RL MDL


MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

<0.20 0.201.0 ug/L 04/22/15 00:11 11,1,1-Trichloroethane

<0.23 0.231.0 ug/L 04/22/15 00:11 11,1,2,2-Tetrachloroethane

<0.28 0.281.0 ug/L 04/22/15 00:11 11,1,2-Trichloroethane

<0.19 0.191.0 ug/L 04/22/15 00:11 11,1-Dichloroethane

<0.31 0.311.0 ug/L 04/22/15 00:11 11,1-Dichloroethene

<0.34 0.341.0 ug/L 04/22/15 00:11 11,1-Dichloropropene

<0.24 0.241.0 ug/L 04/22/15 00:11 11,2,3-Trichlorobenzene

<0.45 0.451.0 ug/L 04/22/15 00:11 11,2,3-Trichloropropane

<0.31 0.311.0 ug/L 04/22/15 00:11 11,2,4-Trichlorobenzene

<0.14 0.141.0 ug/L 04/22/15 00:11 11,2,4-Trimethylbenzene

<0.87 0.872.0 ug/L 04/22/15 00:11 11,2-Dibromo-3-Chloropropane

<0.36 0.361.0 ug/L 04/22/15 00:11 11,2-Dibromoethane

<0.27 0.271.0 ug/L 04/22/15 00:11 11,2-Dichlorobenzene

<0.28 0.281.0 ug/L 04/22/15 00:11 11,2-Dichloroethane

<0.20 0.201.0 ug/L 04/22/15 00:11 11,2-Dichloropropane

<0.18 0.181.0 ug/L 04/22/15 00:11 11,3,5-Trimethylbenzene





<0.21 0.211.0 ug/L 04/22/15 00:11 12-Chlorotoluene

<0.20 0.201.0 ug/L 04/22/15 00:11 14-Chlorotoluene

<0.074 0.0740.50 ug/L 04/22/15 00:11 1Benzene

<0.25 0.251.0 ug/L 04/22/15 00:11 1Bromobenzene

<0.40 0.401.0 ug/L 04/22/15 00:11 1Bromochloromethane

<0.17 0.171.0 ug/L 04/22/15 00:11 1Bromodichloromethane

<0.28 0.281.0 ug/L 04/22/15 00:11 1Bromoform

<0.31 0.311.0 ug/L 04/22/15 00:11 1Bromomethane

<0.26 0.261.0 ug/L 04/22/15 00:11 1Carbon tetrachloride

<0.14 0.141.0 ug/L 04/22/15 00:11 1Chlorobenzene

<0.34 0.341.0 ug/L 04/22/15 00:11 1Chloroethane

<0.20 0.201.0 ug/L 04/22/15 00:11 1Chloroform

<0.18 0.181.0 ug/L 04/22/15 00:11 1Chloromethane

<0.12 0.121.0 ug/L 04/22/15 00:11 1cis-1,2-Dichloroethene

<0.18 0.181.0 ug/L 04/22/15 00:11 1cis-1,3-Dichloropropene

<0.32 0.321.0 ug/L 04/22/15 00:11 1Dibromochloromethane

<0.33 0.331.0 ug/L 04/22/15 00:11 1Dibromomethane

<0.20 0.201.0 ug/L 04/22/15 00:11 1Dichlorodifluoromethane

<0.13 0.130.50 ug/L 04/22/15 00:11 1Ethylbenzene

<0.26 0.261.0 ug/L 04/22/15 00:11 1Hexachlorobutadiene

<0.15 0.151.0 ug/L 04/22/15 00:11 1Isopropyl ether

<0.14 0.141.0 ug/L 04/22/15 00:11 1Isopropylbenzene

<0.24 0.241.0 ug/L 04/22/15 00:11 1Methyl tert-butyl ether

<0.68 0.685.0 ug/L 04/22/15 00:11 1Methylene Chloride

1.05 0.161.0 ug/L 04/22/15 00:11 1Naphthalene

<0.13 0.131.0 ug/L 04/22/15 00:11 1n-Butylbenzene

<0.13 0.131.0 ug/L 04/22/15 00:11 1N-Propylbenzene

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)




RL MDL

p-Isopropyltoluene <0.17 1.0 0.17 ug/L 04/22/15 00:11 1

MB MB


<0.15 0.151.0 ug/L 04/22/15 00:11 1sec-Butylbenzene

<0.10 0.101.0 ug/L 04/22/15 00:11 1Styrene

<0.14 0.141.0 ug/L 04/22/15 00:11 1tert-Butylbenzene

<0.17 0.171.0 ug/L 04/22/15 00:11 1Tetrachloroethene

<0.11 0.110.50 ug/L 04/22/15 00:11 1Toluene

<0.25 0.251.0 ug/L 04/22/15 00:11 1trans-1,2-Dichloroethene

<0.21 0.211.0 ug/L 04/22/15 00:11 1trans-1,3-Dichloropropene

<0.19 0.190.50 ug/L 04/22/15 00:11 1Trichloroethene

<0.19 0.191.0 ug/L 04/22/15 00:11 1Trichlorofluoromethane

<0.10 0.100.50 ug/L 04/22/15 00:11 1Vinyl chloride

<0.068 0.0681.0 ug/L 04/22/15 00:11 1Xylenes, Total


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

84 04/22/15 00:11 14-Bromofluorobenzene (Surr) 75 - 120

100 04/22/15 00:11 1Dibromofluoromethane 75 - 120

95 04/22/15 00:11 1Toluene-d8 (Surr) 75 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-284724/4



1,1,1,2-Tetrachloroethane 50.0 58.3 ug/L 117 75 - 122

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,1-Trichloroethane 50.0 53.1 ug/L 106 72 - 130

1,1,2,2-Tetrachloroethane 50.0 52.8 ug/L 106 72 - 130

1,1,2-Trichloroethane 50.0 55.8 ug/L 112 75 - 120

1,1-Dichloroethane 50.0 50.0 ug/L 100 75 - 120

1,1-Dichloroethene 50.0 48.8 ug/L 98 69 - 120

1,1-Dichloropropene 50.0 50.7 ug/L 101 75 - 130

1,2,3-Trichlorobenzene 50.0 52.0 ug/L 104 69 - 131

1,2,3-Trichloropropane 50.0 51.0 ug/L 102 65 - 132


1,2,4-Trimethylbenzene 50.0 51.2 ug/L 102 75 - 121

1,2-Dibromo-3-Chloropropane 50.0 48.4 ug/L 97 62 - 130

1,2-Dibromoethane 50.0 56.9 ug/L 114 78 - 122

1,2-Dichlorobenzene 50.0 53.1 ug/L 106 75 - 120

1,2-Dichloroethane 50.0 54.0 ug/L 108 69 - 130

1,2-Dichloropropane 50.0 51.8 ug/L 104 75 - 120

1,3,5-Trimethylbenzene 50.0 51.6 ug/L 103 75 - 121





2-Chlorotoluene 50.0 52.0 ug/L 104 75 - 120

4-Chlorotoluene 50.0 51.8 ug/L 104 75 - 120

Benzene 50.0 49.0 ug/L 98 75 - 120

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Bromobenzene 50.0 55.9 ug/L 112 75 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bromochloromethane 50.0 55.3 ug/L 111 76 - 120

Bromodichloromethane 50.0 56.9 ug/L 114 77 - 121

Bromoform 50.0 56.7 ug/L 113 68 - 126

Bromomethane 50.0 66.3 ug/L 133 45 - 169

Carbon tetrachloride 50.0 53.6 ug/L 107 70 - 130

Chlorobenzene 50.0 54.5 ug/L 109 75 - 120

Chloroethane 50.0 58.7 ug/L 117 58 - 147

Chloroform 50.0 53.3 ug/L 107 76 - 120

Chloromethane 50.0 45.6 ug/L 91 63 - 133

cis-1,2-Dichloroethene 50.0 50.1 ug/L 100 75 - 120

cis-1,3-Dichloropropene 50.0 52.8 ug/L 106 78 - 130

Dibromochloromethane 50.0 58.0 ug/L 116 71 - 126

Dibromomethane 50.0 52.3 ug/L 105 75 - 120

Dichlorodifluoromethane 50.0 52.2 ug/L 104 41 - 146

Ethylbenzene 50.0 55.6 ug/L 111 75 - 120

Hexachlorobutadiene 50.0 52.4 ug/L 105 71 - 131

Isopropylbenzene 50.0 52.4 ug/L 105 75 - 121

Methyl tert-butyl ether 50.0 48.2 ug/L 96 75 - 130

Methylene Chloride 50.0 50.4 ug/L 101 73 - 130

Naphthalene 50.0 55.0 ug/L 110 69 - 135

n-Butylbenzene 50.0 50.1 ug/L 100 75 - 121

N-Propylbenzene 50.0 52.0 ug/L 104 75 - 120

p-Isopropyltoluene 50.0 54.2 ug/L 108 75 - 121

sec-Butylbenzene 50.0 51.6 ug/L 103 75 - 120

Styrene 50.0 53.6 ug/L 107 75 - 120

tert-Butylbenzene 50.0 53.3 ug/L 107 75 - 123

Tetrachloroethene 50.0 53.1 ug/L 106 75 - 120

Toluene 50.0 51.1 ug/L 102 75 - 120

trans-1,2-Dichloroethene 50.0 49.2 ug/L 98 77 - 120

trans-1,3-Dichloropropene 50.0 53.2 ug/L 106 74 - 130

Trichloroethene 50.0 53.7 ug/L 107 75 - 120

Trichlorofluoromethane 50.0 50.6 ug/L 101 71 - 130

Vinyl chloride 50.0 46.2 ug/L 92 72 - 123

Xylenes, Total 100 107 ug/L 107 75 - 120

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

98

LCS LCS

Qualifier Limits%Recovery

934-Bromofluorobenzene (Surr) 75 - 120

98Dibromofluoromethane 75 - 120

93Toluene-d8 (Surr) 75 - 120

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Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 500-283982/1-A


Analysis Batch: 284092 Prep Batch: 283982

RL MDL


MB MB


<0.20 0.201.6 ug/L 04/15/15 16:41 04/16/15 13:43 11,2-Dichlorobenzene



<0.24 0.240.80 ug/L 04/15/15 16:41 04/16/15 13:43 11-Methylnaphthalene

<0.30 0.301.6 ug/L 04/15/15 16:41 04/16/15 13:43 12,2'-oxybis[1-chloropropane]

<2.1 2.18.0 ug/L 04/15/15 16:41 04/16/15 13:43 12,4,5-Trichlorophenol

<0.57 0.574.0 ug/L 04/15/15 16:41 04/16/15 13:43 12,4,6-Trichlorophenol

<2.1 2.18.0 ug/L 04/15/15 16:41 04/16/15 13:43 12,4-Dichlorophenol

<1.4 1.48.0 ug/L 04/15/15 16:41 04/16/15 13:43 12,4-Dimethylphenol

<6.9 6.916 ug/L 04/15/15 16:41 04/16/15 13:43 12,4-Dinitrophenol

<0.20 0.200.80 ug/L 04/15/15 16:41 04/16/15 13:43 12,4-Dinitrotoluene

<0.059 0.0590.40 ug/L 04/15/15 16:41 04/16/15 13:43 12,6-Dinitrotoluene

<0.19 0.191.6 ug/L 04/15/15 16:41 04/16/15 13:43 12-Chloronaphthalene

<0.45 0.454.0 ug/L 04/15/15 16:41 04/16/15 13:43 12-Chlorophenol

<0.052 0.0520.40 ug/L 04/15/15 16:41 04/16/15 13:43 12-Methylnaphthalene

<0.24 0.241.6 ug/L 04/15/15 16:41 04/16/15 13:43 12-Methylphenol

<1.0 1.04.0 ug/L 04/15/15 16:41 04/16/15 13:43 12-Nitroaniline

<2.0 2.08.0 ug/L 04/15/15 16:41 04/16/15 13:43 12-Nitrophenol

<0.36 0.361.6 ug/L 04/15/15 16:41 04/16/15 13:43 13 & 4 Methylphenol

<1.4 1.44.0 ug/L 04/15/15 16:41 04/16/15 13:43 13,3'-Dichlorobenzidine


<4.7 4.716 ug/L 04/15/15 16:41 04/16/15 13:43 14,6-Dinitro-2-methylphenol

<0.43 0.434.0 ug/L 04/15/15 16:41 04/16/15 13:43 14-Bromophenyl phenyl ether

<1.8 1.88.0 ug/L 04/15/15 16:41 04/16/15 13:43 14-Chloro-3-methylphenol

<1.6 1.68.0 ug/L 04/15/15 16:41 04/16/15 13:43 14-Chloroaniline

<0.51 0.514.0 ug/L 04/15/15 16:41 04/16/15 13:43 14-Chlorophenyl phenyl ether


<5.9 5.916 ug/L 04/15/15 16:41 04/16/15 13:43 14-Nitrophenol

<0.25 0.250.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Acenaphthene

<0.21 0.210.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Acenaphthylene

<0.27 0.270.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Anthracene

<0.045 0.0450.16 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzo[a]anthracene

<0.079 0.0790.16 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzo[a]pyrene

<0.065 0.0650.16 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzo[b]fluoranthene

<0.30 0.300.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzo[g,h,i]perylene

<0.051 0.0510.16 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzo[k]fluoranthene

<4.6 4.616 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzoic acid

<4.8 4.816 ug/L 04/15/15 16:41 04/16/15 13:43 1Benzyl alcohol

<0.23 0.231.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Bis(2-chloroethoxy)methane

<0.23 0.231.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Bis(2-chloroethyl)ether

<1.4 1.48.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Bis(2-ethylhexyl) phthalate

<0.38 0.381.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Butyl benzyl phthalate

<0.28 0.284.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Carbazole

<0.055 0.0550.40 ug/L 04/15/15 16:41 04/16/15 13:43 1Chrysene

<0.041 0.0410.24 ug/L 04/15/15 16:41 04/16/15 13:43 1Dibenz(a,h)anthracene

<0.21 0.211.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Dibenzofuran

<0.29 0.291.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Diethyl phthalate

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)




RL MDL

Dimethyl phthalate <0.25 1.6 0.25 ug/L 04/15/15 16:41 04/16/15 13:43 1

MB MB


<0.58 0.584.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Di-n-butyl phthalate

<0.84 0.848.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Di-n-octyl phthalate

<0.36 0.360.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Fluoranthene

<0.20 0.200.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Fluorene

<0.064 0.0640.40 ug/L 04/15/15 16:41 04/16/15 13:43 1Hexachlorobenzene

<0.41 0.414.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Hexachlorobutadiene

<5.1 5.116 ug/L 04/15/15 16:41 04/16/15 13:43 1Hexachlorocyclopentadiene

<0.48 0.484.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Hexachloroethane

<0.060 0.0600.16 ug/L 04/15/15 16:41 04/16/15 13:43 1Indeno[1,2,3-cd]pyrene

<0.30 0.301.6 ug/L 04/15/15 16:41 04/16/15 13:43 1Isophorone

0.372 J 0.250.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Naphthalene

<0.36 0.360.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Nitrobenzene

<0.12 0.120.40 ug/L 04/15/15 16:41 04/16/15 13:43 1N-Nitrosodi-n-propylamine

<0.30 0.300.80 ug/L 04/15/15 16:41 04/16/15 13:43 1N-Nitrosodiphenylamine

<3.2 3.216 ug/L 04/15/15 16:41 04/16/15 13:43 1Pentachlorophenol

<0.24 0.240.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Phenanthrene

<0.54 0.544.0 ug/L 04/15/15 16:41 04/16/15 13:43 1Phenol

<0.34 0.340.80 ug/L 04/15/15 16:41 04/16/15 13:43 1Pyrene

2,4,6-Tribromophenol (Surr) 93 53 - 150 04/16/15 13:43 1

MB MB

Surrogate

04/15/15 16:41

Dil FacPrepared AnalyzedQualifier Limits%Recovery

84 04/15/15 16:41 04/16/15 13:43 12-Fluorobiphenyl 41 - 132

63 04/15/15 16:41 04/16/15 13:43 12-Fluorophenol (Surr) 32 - 110

82 04/15/15 16:41 04/16/15 13:43 1Nitrobenzene-d5 (Surr) 47 - 134

48 04/15/15 16:41 04/16/15 13:43 1Phenol-d5 (Surr) 25 - 100

107 04/15/15 16:41 04/16/15 13:43 1Terphenyl-d14 (Surr) 59 - 150

Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-283982/2-A




Analyte

LCS LCS


Spike

Added

%Rec.

Limits




1-Methylnaphthalene 32.0 18.7 ug/L 59 35 - 111

2,2'-oxybis[1-chloropropane] 32.0 26.4 ug/L 83 24 - 115

2,4,5-Trichlorophenol 32.0 33.4 ug/L 104 59 - 132

2,4,6-Trichlorophenol 32.0 32.0 ug/L 100 61 - 125

2,4-Dichlorophenol 32.0 31.1 ug/L 97 61 - 122

2,4-Dimethylphenol 32.0 26.4 ug/L 82 49 - 117

2,4-Dinitrophenol 64.0 74.2 ug/L 116 47 - 161

2,4-Dinitrotoluene 32.0 34.3 ug/L 107 71 - 127

2,6-Dinitrotoluene 32.0 33.6 ug/L 105 67 - 124

2-Chloronaphthalene 32.0 24.1 ug/L 75 40 - 114

2-Chlorophenol 32.0 26.1 ug/L 82 57 - 108

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2-Methylnaphthalene 32.0 19.3 ug/L 60 35 - 113

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

2-Methylphenol 32.0 27.7 ug/L 87 54 - 109

2-Nitroaniline 32.0 32.1 ug/L 100 59 - 129

2-Nitrophenol 32.0 29.1 ug/L 91 62 - 117

3 & 4 Methylphenol 32.0 30.0 ug/L 94 54 - 107

3,3'-Dichlorobenzidine 32.0 32.7 ug/L 102 49 - 127


4,6-Dinitro-2-methylphenol 64.0 65.4 ug/L 102 66 - 143

4-Bromophenyl phenyl ether 32.0 29.7 ug/L 93 61 - 123

4-Chloro-3-methylphenol 32.0 21.4 ug/L 67 64 - 129

4-Chloroaniline 32.0 21.9 ug/L 68 15 - 141

4-Chlorophenyl phenyl ether 32.0 29.7 ug/L 93 58 - 120


4-Nitrophenol 64.0 51.1 ug/L 80 35 - 112

Acenaphthene 32.0 24.6 ug/L 77 41 - 120

Acenaphthylene 32.0 27.0 ug/L 84 47 - 112

Anthracene 32.0 26.7 ug/L 83 56 - 124

Benzo[a]anthracene 32.0 30.0 ug/L 94 60 - 122

Benzo[a]pyrene 32.0 28.6 ug/L 89 66 - 116

Benzo[b]fluoranthene 32.0 29.2 ug/L 91 66 - 120

Benzo[g,h,i]perylene 32.0 29.5 ug/L 92 42 - 164

Benzo[k]fluoranthene 32.0 28.7 ug/L 90 52 - 123

Benzoic acid 32.0 25.1 ug/L 78 18 - 91

Benzyl alcohol 32.0 30.1 ug/L 94 52 - 119

Bis(2-chloroethoxy)methane 32.0 32.2 ug/L 101 57 - 115

Bis(2-chloroethyl)ether 32.0 24.8 ug/L 77 50 - 105

Bis(2-ethylhexyl) phthalate 32.0 32.0 ug/L 100 69 - 123

Butyl benzyl phthalate 32.0 32.1 ug/L 100 69 - 123

Carbazole 32.0 30.3 ug/L 95 63 - 135

Chrysene 32.0 30.4 ug/L 95 59 - 126

Dibenz(a,h)anthracene 32.0 29.9 ug/L 93 53 - 149

Dibenzofuran 32.0 28.9 ug/L 90 54 - 120

Diethyl phthalate 32.0 33.5 ug/L 105 54 - 140

Dimethyl phthalate 32.0 32.8 ug/L 103 60 - 130

Di-n-butyl phthalate 32.0 30.6 ug/L 96 64 - 125

Di-n-octyl phthalate 32.0 31.7 ug/L 99 62 - 132

Fluoranthene 32.0 29.1 ug/L 91 68 - 114

Fluorene 32.0 27.5 ug/L 86 50 - 125

Hexachlorobenzene 32.0 28.0 ug/L 88 59 - 122

Hexachlorobutadiene 32.0 18.9 ug/L 59 25 - 104

Hexachlorocyclopentadiene 32.0 19.8 ug/L 62 14 - 106

Hexachloroethane 32.0 17.6 ug/L 55 25 - 96

Indeno[1,2,3-cd]pyrene 32.0 29.4 ug/L 92 53 - 151

Isophorone 32.0 32.0 ug/L 100 61 - 112

Naphthalene 32.0 21.4 ug/L 67 41 - 106

Nitrobenzene 32.0 26.9 ug/L 84 52 - 112

N-Nitrosodi-n-propylamine 32.0 28.6 ug/L 90 47 - 113

N-Nitrosodiphenylamine 64.0 52.5 ug/L 82 50 - 117

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Pentachlorophenol 64.0 58.4 ug/L 91 55 - 129

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Phenanthrene 32.0 27.2 ug/L 85 55 - 126

Phenol 32.0 20.4 ug/L 64 34 - 89

Pyrene 32.0 30.0 ug/L 94 62 - 118

2,4,6-Tribromophenol (Surr) 53 - 150

Surrogate

107

LCS LCS


842-Fluorobiphenyl 41 - 132

732-Fluorophenol (Surr) 32 - 110

89Nitrobenzene-d5 (Surr) 47 - 134

61Phenol-d5 (Surr) 25 - 100

112Terphenyl-d14 (Surr) 59 - 150

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-283982/3-A



1,2,4-Trichlorobenzene 32.0 20.1 ug/L 63 36 - 98 4 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

1,2-Dichlorobenzene 32.0 18.2 ug/L 57 36 - 96 8 20



1-Methylnaphthalene 32.0 21.6 ug/L 67 35 - 111 14 20

2,2'-oxybis[1-chloropropane] 32.0 20.5 * ug/L 64 24 - 115 25 20

2,4,5-Trichlorophenol 32.0 31.8 ug/L 99 59 - 132 5 20

2,4,6-Trichlorophenol 32.0 29.0 ug/L 91 61 - 125 10 20

2,4-Dichlorophenol 32.0 27.1 ug/L 85 61 - 122 14 20

2,4-Dimethylphenol 32.0 23.1 ug/L 72 49 - 117 13 20

2,4-Dinitrophenol 64.0 67.3 ug/L 105 47 - 161 10 20

2,4-Dinitrotoluene 32.0 29.9 ug/L 93 71 - 127 14 20

2,6-Dinitrotoluene 32.0 29.9 ug/L 93 67 - 124 12 20

2-Chloronaphthalene 32.0 22.9 ug/L 72 40 - 114 5 20

2-Chlorophenol 32.0 23.2 ug/L 73 57 - 108 12 20

2-Methylnaphthalene 32.0 21.7 ug/L 68 35 - 113 12 20

2-Methylphenol 32.0 24.6 ug/L 77 54 - 109 12 20

2-Nitroaniline 32.0 28.5 ug/L 89 59 - 129 12 20

2-Nitrophenol 32.0 24.8 ug/L 77 62 - 117 16 20

3 & 4 Methylphenol 32.0 25.3 ug/L 79 54 - 107 17 20

3,3'-Dichlorobenzidine 32.0 25.9 * ug/L 81 49 - 127 23 20


4,6-Dinitro-2-methylphenol 64.0 57.6 ug/L 90 66 - 143 13 20

4-Bromophenyl phenyl ether 32.0 25.9 ug/L 81 61 - 123 14 20

4-Chloro-3-methylphenol 32.0 26.0 ug/L 81 64 - 129 19 20

4-Chloroaniline 32.0 24.5 ug/L 77 15 - 141 11 20

4-Chlorophenyl phenyl ether 32.0 28.3 ug/L 88 58 - 120 5 20


4-Nitrophenol 64.0 50.8 ug/L 79 35 - 112 1 20

Acenaphthene 32.0 22.4 ug/L 70 41 - 120 9 20

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Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-283982/3-A



Acenaphthylene 32.0 24.7 ug/L 77 47 - 112 9 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Anthracene 32.0 24.0 ug/L 75 56 - 124 11 20

Benzo[a]anthracene 32.0 26.9 ug/L 84 60 - 122 11 20

Benzo[a]pyrene 32.0 26.2 ug/L 82 66 - 116 9 20

Benzo[b]fluoranthene 32.0 27.0 ug/L 84 66 - 120 8 20

Benzo[g,h,i]perylene 32.0 27.3 ug/L 85 42 - 164 8 20

Benzo[k]fluoranthene 32.0 26.2 ug/L 82 52 - 123 9 20

Benzoic acid 32.0 21.6 ug/L 68 18 - 91 15 20

Benzyl alcohol 32.0 26.7 ug/L 83 52 - 119 12 20

Bis(2-chloroethoxy)methane 32.0 25.5 * ug/L 80 57 - 115 23 20

Bis(2-chloroethyl)ether 32.0 19.7 * ug/L 61 50 - 105 23 20

Bis(2-ethylhexyl) phthalate 32.0 29.0 ug/L 91 69 - 123 10 20

Butyl benzyl phthalate 32.0 28.5 ug/L 89 69 - 123 12 20

Carbazole 32.0 26.9 ug/L 84 63 - 135 12 20

Chrysene 32.0 26.8 ug/L 84 59 - 126 13 20

Dibenz(a,h)anthracene 32.0 27.9 ug/L 87 53 - 149 7 20

Dibenzofuran 32.0 26.5 ug/L 83 54 - 120 9 20

Diethyl phthalate 32.0 30.2 ug/L 94 54 - 140 10 20

Dimethyl phthalate 32.0 30.2 ug/L 94 60 - 130 8 20

Di-n-butyl phthalate 32.0 27.7 ug/L 86 64 - 125 10 20

Di-n-octyl phthalate 32.0 29.4 ug/L 92 62 - 132 8 20

Fluoranthene 32.0 26.2 ug/L 82 68 - 114 10 20

Fluorene 32.0 26.6 ug/L 83 50 - 125 3 20

Hexachlorobenzene 32.0 25.5 ug/L 80 59 - 122 9 20

Hexachlorobutadiene 32.0 19.2 ug/L 60 25 - 104 1 20

Hexachlorocyclopentadiene 32.0 17.9 ug/L 56 14 - 106 10 20

Hexachloroethane 32.0 16.3 ug/L 51 25 - 96 8 20

Indeno[1,2,3-cd]pyrene 32.0 26.3 ug/L 82 53 - 151 11 20

Isophorone 32.0 27.4 ug/L 86 61 - 112 16 20

Naphthalene 32.0 21.0 ug/L 66 41 - 106 2 20

Nitrobenzene 32.0 23.6 ug/L 74 52 - 112 13 20

N-Nitrosodi-n-propylamine 32.0 26.1 ug/L 82 47 - 113 9 20

N-Nitrosodiphenylamine 64.0 47.7 ug/L 75 50 - 117 10 20

Pentachlorophenol 64.0 52.3 ug/L 82 55 - 129 11 20

Phenanthrene 32.0 24.4 ug/L 76 55 - 126 11 20

Phenol 32.0 16.9 ug/L 53 34 - 89 19 20

Pyrene 32.0 26.3 ug/L 82 62 - 118 13 20


Surrogate

107

LCSD LCSD







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Method: 6010B - Metals (ICP)


Matrix: Water Prep Type: Total Recoverable


RL MDL

Arsenic <0.0038 0.010 0.0038 mg/L 04/15/15 15:30 04/17/15 04:12 1

MB MB


<0.0022 0.00220.010 mg/L 04/15/15 15:30 04/17/15 04:12 1Barium

<0.00094 0.000940.0020 mg/L 04/15/15 15:30 04/17/15 04:12 1Cadmium

<0.0024 0.00240.010 mg/L 04/15/15 15:30 04/17/15 04:12 1Chromium

<0.0025 0.00250.0050 mg/L 04/15/15 15:30 04/17/15 04:12 1Lead

<0.0046 0.00460.010 mg/L 04/15/15 15:30 04/17/15 04:12 1Selenium

<0.0013 0.00130.0050 mg/L 04/15/15 15:30 04/17/15 04:12 1Silver




Arsenic 0.100 0.103 mg/L 103 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 0.500 0.521 mg/L 104 80 - 120

Cadmium 0.0500 0.0518 mg/L 104 80 - 120

Chromium 0.200 0.206 mg/L 103 80 - 120

Lead 0.100 0.105 mg/L 105 80 - 120

Selenium 0.100 0.0945 mg/L 94 80 - 120

Silver 0.0500 0.0522 mg/L 104 80 - 120

Client Sample ID: TW1Lab Sample ID: 500-94669-13 MS



Arsenic <0.0038 0.100 0.108 mg/L 108 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.050 0.500 0.552 mg/L 100 75 - 125

Cadmium <0.00094 0.0500 0.0535 mg/L 107 75 - 125

Chromium <0.0024 0.200 0.208 mg/L 104 75 - 125

Lead 0.0046 J 0.100 0.117 mg/L 113 75 - 125

Selenium <0.0046 0.100 0.103 mg/L 103 75 - 125

Silver <0.0013 0.0500 0.0553 mg/L 111 75 - 125

Client Sample ID: TW1Lab Sample ID: 500-94669-13 MSD



Arsenic <0.0038 0.100 0.105 mg/L 105 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 0.050 0.500 0.562 mg/L 102 75 - 125 2 20

Cadmium <0.00094 0.0500 0.0523 mg/L 105 75 - 125 2 20

Chromium <0.0024 0.200 0.201 mg/L 100 75 - 125 4 20

Lead 0.0046 J 0.100 0.112 mg/L 107 75 - 125 5 20

Selenium <0.0046 0.100 0.0988 mg/L 99 75 - 125 4 20

Silver <0.0013 0.0500 0.0534 mg/L 107 75 - 125 3 20

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Method: 6010B - Metals (ICP) (Continued)

Client Sample ID: TW1Lab Sample ID: 500-94669-13 DU



Arsenic <0.0038 <0.0038 mg/L NC 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Barium 0.050 0.0490 mg/L 2 20

Cadmium <0.00094 <0.00094 mg/L NC 20

Chromium <0.0024 <0.0024 mg/L NC 20

Lead 0.0046 J 0.00454 J mg/L 2 20

Selenium <0.0046 0.00562 J mg/L NC 20

Silver <0.0013 <0.0013 mg/L NC 20

Method: 7470A - Mercury (CVAA)




RL MDL

Mercury <0.061 0.20 0.061 ug/L 04/16/15 12:00 04/17/15 11:47 1

MB MB





Mercury 2.00 1.78 ug/L 89 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Lab ChronicleClient: Stantec Consulting Corporation/Bonestroo TestAmerica Job ID: 500-94669-2


Client Sample ID: TW1 Lab Sample ID: 500-94669-13Matrix: WaterDate Collected: 04/09/15 10:50


Analysis 8260B 04/22/15 05:13 EMA1 284724 TAL CHI

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3510C 283982 04/15/15 16:41 JP1 TAL CHITotal/NA

Analysis 8270D 1 284092 04/16/15 16:39 KDL TAL CHITotal/NA

Prep 3005A 283993 04/15/15 15:30 PJH TAL CHITotal Recoverable

Analysis 6010B 1 284243 04/17/15 04:27 PJ1 TAL CHITotal Recoverable

Prep 7470A 284159 04/16/15 12:00 RLL TAL CHITotal/NA

Analysis 7470A 1 284374 04/17/15 12:36 RLL TAL CHITotal/NA




Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



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Client Sample ID: Trip Blank Lab Sample ID: 500-94669-17Matrix: WaterDate Collected: 04/09/15 00:00



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: TW1 FD Lab Sample ID: 500-94669-18Matrix: WaterDate Collected: 04/09/15 11:00



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









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Certification SummaryClient: Stantec Consulting Corporation/Bonestroo TestAmerica Job ID: 500-94669-2


Laboratory: TestAmerica ChicagoThe certifications listed below are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Wisconsin 9995800105State Program 08-31-15

TestAmerica Chicago

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of 43 4/24/2015

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Login Sample Receipt Checklist

Client: Stantec Consulting Corporation/Bonestroo Job Number: 500-94669-2

Login Number: 94669

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice. 4.2,3.1

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200

TestAmerica Job ID: 500-94669-1Client Project/Site: Muni. Aud & Armory 193703239 Task 3.0.2

For:Stantec Consulting Corporation/Bonestroo12075 Corporate ParkwaySuite 200Mequon, Wisconsin 53092

Attn: Stu Gross

Authorized for release by:4/24/2015 4:44:50 PMBonnie Stadelmann, Senior Project [email protected]

Designee for

Sandie Fredrick, Project Manager II(920)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Stantec Consulting Corporation/BonestrooProject/Site: Muni. Aud & Armory 193703239 Task 3.0.2

TestAmerica Job ID: 500-94669-1

Page 2 of 78TestAmerica Chicago

4/24/2015

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78

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Case NarrativeClient: Stantec Consulting Corporation/Bonestroo TestAmerica Job ID: 500-94669-1


Job ID: 500-94669-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-94669-1

Comments

No additional comments.

Receipt

The samples were received on 4/15/2015 10:15 AM; the samples arrived in good condition, properly preserved and, where required, on

ice. The temperatures of the 2 coolers at receipt time were 3.1º C and 4.2º C.

GC/MS VOA

Method(s) 8260B: The prepation batch laboratory control sample (LCS) for prep batch 284058 recovered outside control limits for 23

compounds. These analytes were biased high in the preparation LCS, were within limits in the analytical batch LCS, MS and MSD and

were not detected in the associated samples; therefore, the data has been reported.


GC/MS Semi VOA

Method(s) 8270D: The following samples: SB1 FD (500-94669-3), SB2 (2-4) (500-94669-4) and SB3 (6-8) (500-94669-7) had one

surrogate outside limits. No further action was required.

Method(s) 8270D: The following sample contained one acid surrogate and one base/neutral surrogate outside acceptance limits: SB6

(2-4) (500-94669-11). The laboratory's SOP allows one acid and one base/neutral surrogate to be outside acceptance limits; therefore,

re-extraction was not performed. These results have been reported and qualified.

Method(s) 8270D: 500-94669-1 MS and -1 MSD had Terphenyl-d14 outside of limits, biased high. All other surrogates for this MS/MSD

were within limits. No further action was required.SB1 (2-4) (500-94669-1)

Method(s) 8270D: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that

one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 4 analytes to recover outside criteria for this

method when a full list spike is utilized. The LCS associated with batch 500-284633 had 2 known poor performing analytes outside

control limits: Benzoic Acid at 0% (10%-100%) and Hexachlorocyclopentadiene at 2% (10%-134%) therefore, corrective action was not

performed. These results have been reported and qualified. SB1 (2-4) (500-94669-1), SB1 (6-8) (500-94669-2), SB1 FD (500-94669-3),

SB2 (2-4) (500-94669-4), SB2 (4-6) (500-94669-5), SB3 (2-4) (500-94669-6), SB3 (6-8) (500-94669-7), SB4 (2-4) (500-94669-8), SB4 (4-6)

(500-94669-9), SB5 (2-4) (500-94669-10) and SB6 (2-4) (500-94669-11)


Metals


Organic Prep



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Client Sample ID: SB1 (2-4) Lab Sample ID: 500-94669-1

☼Benzo[a]anthracene

RL

36 ug/Kg

MDL

4.8


Total/NA1J13 8270D

☼Benzo[a]pyrene 36 ug/Kg7.0 Total/NA113 J 8270D

☼Benzo[b]fluoranthene 36 ug/Kg7.8 Total/NA117 J 8270D

☼Benzo[g,h,i]perylene 36 ug/Kg12 Total/NA114 J 8270D

☼Chrysene 36 ug/Kg9.8 Total/NA114 J 8270D

☼Fluoranthene 36 ug/Kg6.7 Total/NA121 J F1 8270D

☼Indeno[1,2,3-cd]pyrene 36 ug/Kg9.3 Total/NA19.7 J 8270D

☼Phenanthrene 36 ug/Kg5.0 Total/NA18.6 J F1 8270D

☼Pyrene 36 ug/Kg7.1 Total/NA120 J F1 F2 8270D

☼Arsenic 0.99 mg/Kg0.46 Total/NA10.84 J 6010B

☼Barium 0.99 mg/Kg0.18 Total/NA18.6 6010B

☼Chromium 0.99 mg/Kg0.17 Total/NA14.4 6010B

☼Lead 0.49 mg/Kg0.25 Total/NA13.4 6010B

☼Mercury 0.018 mg/Kg0.0062 Total/NA10.028 7471A


☼Acenaphthene

RL

38 ug/Kg

MDL

6.9


Total/NA1J15 8270D

☼Anthracene 38 ug/Kg6.4 Total/NA149 8270D

☼Benzo[a]anthracene 38 ug/Kg5.2 Total/NA189 8270D

☼Benzo[a]pyrene 38 ug/Kg7.4 Total/NA171 8270D

☼Benzo[b]fluoranthene 38 ug/Kg8.3 Total/NA189 8270D

☼Benzo[g,h,i]perylene 38 ug/Kg12 Total/NA144 8270D

☼Benzo[k]fluoranthene 38 ug/Kg11 Total/NA130 J 8270D

☼Chrysene 38 ug/Kg10 Total/NA177 8270D

☼Fluoranthene 38 ug/Kg7.1 Total/NA1190 8270D

☼Fluorene 38 ug/Kg5.4 Total/NA117 J 8270D

☼Indeno[1,2,3-cd]pyrene 38 ug/Kg9.9 Total/NA135 J 8270D

☼Phenanthrene 38 ug/Kg5.3 Total/NA1160 8270D

☼Pyrene 38 ug/Kg7.6 Total/NA1170 8270D

Client Sample ID: SB1 FD Lab Sample ID: 500-94669-3


RL

36 ug/Kg

MDL

4.9


Total/NA1J23 8270D


☼Benzo[b]fluoranthene 36 ug/Kg7.9 Total/NA122 J 8270D




☼Phenanthrene 36 ug/Kg5.1 Total/NA116 J 8270D



☼Barium 1.1 mg/Kg0.20 Total/NA127 6010B



☼Selenium 1.1 mg/Kg0.54 Total/NA11.1 6010B


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☼Arsenic

RL

1.1 mg/Kg

MDL

0.53


Total/NA12.0 6010B


☼Chromium 1.1 mg/Kg0.20 Total/NA115 6010B


☼Mercury 0.017 mg/Kg0.0060 Total/NA10.0090 J 7471A


☼Toluene

RL

16 ug/Kg

MDL

7.2


Total/NA50*16 8260B

☼1-Methylnaphthalene 36 ug/Kg8.8 Total/NA128 J 8270D

☼2-Methylnaphthalene 36 ug/Kg6.6 Total/NA133 J 8270D

☼Benzo[a]anthracene 36 ug/Kg4.8 Total/NA131 J 8270D




☼Benzo[k]fluoranthene 36 ug/Kg11 Total/NA114 J 8270D



☼Naphthalene 36 ug/Kg5.5 Total/NA124 J 8270D




☼Arsenic

RL

1.0 mg/Kg

MDL

0.48


Total/NA12.1 6010B




☼Selenium 1.0 mg/Kg0.52 Total/NA10.69 J 6010B




RL

33 ug/Kg

MDL

4.5


Total/NA1J7.3 8270D

☼Fluoranthene 33 ug/Kg6.2 Total/NA17.4 J 8270D

☼Pyrene 33 ug/Kg6.7 Total/NA17.7 J 8270D


☼1,2,4-Trimethylbenzene

RL

110 ug/Kg

MDL

12


Total/NA50J71 8260B

☼Benzene 14 ug/Kg4.3 Total/NA5038 8260B

☼Ethylbenzene 14 ug/Kg7.2 Total/NA5034 * 8260B

☼Naphthalene 110 ug/Kg28 Total/NA50190 8260B

☼Toluene 14 ug/Kg6.6 Total/NA50280 * 8260B

☼Xylenes, Total 29 ug/Kg3.9 Total/NA50330 8260B

☼1-Methylnaphthalene 35 ug/Kg8.5 Total/NA160 8270D

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Client Sample ID: SB4 (2-4) (Continued) Lab Sample ID: 500-94669-8

☼2-Methylnaphthalene

RL

35 ug/Kg

MDL

6.4


Total/NA172 8270D

☼Acenaphthylene 35 ug/Kg4.6 Total/NA119 J 8270D

☼Anthracene 35 ug/Kg5.8 Total/NA113 J 8270D


☼Benzo[a]pyrene 35 ug/Kg6.8 Total/NA1160 8270D


☼Benzo[g,h,i]perylene 35 ug/Kg11 Total/NA1170 8270D

☼Benzo[k]fluoranthene 35 ug/Kg10 Total/NA189 8270D

☼Bis(2-ethylhexyl) phthalate 180 ug/Kg64 Total/NA1100 J 8270D

☼Chrysene 35 ug/Kg9.5 Total/NA1110 8270D


☼Indeno[1,2,3-cd]pyrene 35 ug/Kg9.0 Total/NA1160 8270D

☼Naphthalene 35 ug/Kg5.4 Total/NA157 8270D






☼Lead 0.51 mg/Kg0.25 Total/NA113 6010B

☼Selenium 1.0 mg/Kg0.50 Total/NA10.73 J 6010B



No Detections.


☼Arsenic

RL

0.99 mg/Kg

MDL

0.46


Total/NA11.0 6010B




☼Mercury 0.018 mg/Kg0.0064 Total/NA10.015 J 7471A


☼Benzene

RL

17 ug/Kg

MDL

5.0


Total/NA5024 8260B

☼Ethylbenzene 17 ug/Kg8.5 Total/NA5017 * 8260B

☼Naphthalene 130 ug/Kg33 Total/NA5074 J 8260B

☼Toluene 17 ug/Kg7.8 Total/NA50150 * 8260B

☼Xylenes, Total 34 ug/Kg4.6 Total/NA50150 8260B



☼Anthracene 38 ug/Kg6.4 Total/NA111 J 8270D




☼Benzo[k]fluoranthene 38 ug/Kg11 Total/NA156 8270D

☼Bis(2-ethylhexyl) phthalate 190 ug/Kg70 Total/NA187 J 8270D

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Client Sample ID: SB6 (2-4) (Continued) Lab Sample ID: 500-94669-11

☼Chrysene

RL

38 ug/Kg

MDL

10


Total/NA162 8270D



☼Naphthalene 38 ug/Kg5.9 Total/NA1130 8270D



☼Arsenic 1.0 mg/Kg0.47 Total/NA12.4 6010B



☼Lead 0.51 mg/Kg0.25 Total/NA115 6010B


Client Sample ID: Trip Blank Lab Sample ID: 500-94669-12

No Detections.

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Method SummaryTestAmerica Job ID: 500-94669-1Client: Stantec Consulting Corporation/Bonestroo


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL CHI

SW8468270D Semivolatile Organic Compounds (GC/MS) TAL CHI

SW8466010B Metals (ICP) TAL CHI

SW8467471A Mercury (CVAA) TAL CHI

EPAMoisture Percent Moisture TAL CHI

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.



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Sample SummaryTestAmerica Job ID: 500-94669-1Client: Stantec Consulting Corporation/Bonestroo


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

500-94669-1 SB1 (2-4) Solid 04/09/15 10:12 04/15/15 10:15

500-94669-2 SB1 (6-8) Solid 04/09/15 10:30 04/15/15 10:15

500-94669-3 SB1 FD Solid 04/09/15 10:15 04/15/15 10:15

500-94669-4 SB2 (2-4) Solid 04/09/15 11:51 04/15/15 10:15

500-94669-5 SB2 (4-6) Solid 04/09/15 11:54 04/15/15 10:15

500-94669-6 SB3 (2-4) Solid 04/09/15 09:36 04/15/15 10:15

500-94669-7 SB3 (6-8) Solid 04/09/15 09:38 04/15/15 10:15

500-94669-8 SB4 (2-4) Solid 04/09/15 12:46 04/15/15 10:15

500-94669-9 SB4 (4-6) Solid 04/09/15 12:48 04/15/15 10:15

500-94669-10 SB5 (2-4) Solid 04/09/15 11:26 04/15/15 10:15

500-94669-11 SB6 (2-4) Solid 04/09/15 13:26 04/15/15 10:15

500-94669-12 Trip Blank Solid 04/09/15 00:00 04/15/15 10:15

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Lab Sample ID: 500-94669-1Client Sample ID: SB1 (2-4)Matrix: SolidDate Collected: 04/09/15 10:12

Percent Solids: 91.9Date Received: 04/15/15 10:15


1,1,1,2-Tetrachloroethane <20 * 120 20 ug/Kg ☼ 04/09/15 10:12 04/20/15 16:01 50


59 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1,1-Trichloroethane <12 *

59 14 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1,2,2-Tetrachloroethane <14

59 16 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1,2-Trichloroethane <16

59 11 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1-Dichloroethane <11 *

59 18 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1-Dichloroethene <18

59 20 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,1-Dichloropropene <20

120 21 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2,3-Trichlorobenzene <21

120 34 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2,3-Trichloropropane <34


120 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2,4-Trimethylbenzene <12

120 51 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2-Dibromo-3-Chloropropane <51

120 19 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2-Dibromoethane <19 *

120 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2-Dichlorobenzene <12

59 17 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2-Dichloroethane <17

59 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,2-Dichloropropane <12 *



59 7.9 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼1,3-Dichloropropane <7.9


59 19 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼2,2-Dichloropropane <19

59 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼2-Chlorotoluene <12


15 4.4 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Benzene <4.4

120 25 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Bromobenzene <25

120 22 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Bromochloromethane <22 *

120 20 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Bromodichloromethane <20 *

120 26 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Bromoform <26

120 40 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Bromomethane <40

59 15 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Carbon tetrachloride <15 *

59 8.4 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Chlorobenzene <8.4

120 26 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Chloroethane <26

59 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Chloroform <12 *

120 27 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Chloromethane <27

59 7.3 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼cis-1,2-Dichloroethene <7.3 *

59 11 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼cis-1,3-Dichloropropene <11

120 20 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Dibromochloromethane <20

120 28 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Dibromomethane <28 *

120 30 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Dichlorodifluoromethane <30

15 7.4 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Ethylbenzene <7.4 *

120 20 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Hexachlorobutadiene <20

120 8.7 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Isopropyl ether <8.7

120 15 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Isopropylbenzene <15

120 25 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Methyl tert-butyl ether <25

300 40 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Methylene Chloride <40

120 29 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Naphthalene <29

59 7.6 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼n-Butylbenzene <7.6

120 10 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼N-Propylbenzene <10

120 11 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼p-Isopropyltoluene <11

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sec-Butylbenzene <9.1 59 9.1 ug/Kg ☼ 04/09/15 10:12 04/20/15 16:01 50


59 5.8 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Styrene <5.8 *

59 8.0 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼tert-Butylbenzene <8.0

59 9.9 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Tetrachloroethene <9.9 *

15 6.8 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Toluene <6.8 *

59 15 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼trans-1,2-Dichloroethene <15

59 12 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼trans-1,3-Dichloropropene <12

30 11 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Trichloroethene <11 *

120 24 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Trichlorofluoromethane <24

15 6.1 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Vinyl chloride <6.1

30 4.0 ug/Kg 04/09/15 10:12 04/20/15 16:01 50☼Xylenes, Total <4.0

1,2-Dichloroethane-d4 (Surr) 99 75 - 125 04/09/15 10:12 04/20/15 16:01 50


4-Bromofluorobenzene (Surr) 85 04/09/15 10:12 04/20/15 16:01 5075 - 120

Dibromofluoromethane 99 04/09/15 10:12 04/20/15 16:01 5075 - 120

Toluene-d8 (Surr) 93 04/09/15 10:12 04/20/15 16:01 5075 - 120


1,2,4-Trichlorobenzene <39 F1 180 39 ug/Kg ☼ 04/20/15 16:14 04/23/15 14:39 1


180 43 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼1,2-Dichlorobenzene <43 F1



36 8.8 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼1-Methylnaphthalene <8.8 F1

180 42 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,2'-oxybis[1-chloropropane] <42

360 82 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,4,5-Trichlorophenol <82


360 85 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,4-Dichlorophenol <85 F1

360 140 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,4-Dimethylphenol <140 F1

730 630 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,4-Dinitrophenol <630 F1

180 57 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,4-Dinitrotoluene <57 F1

180 71 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2,6-Dinitrotoluene <71 F1

180 40 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Chloronaphthalene <40 F1

180 61 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Chlorophenol <61 F1

36 6.6 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Methylnaphthalene <6.6

180 58 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Methylphenol <58

180 48 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Nitroaniline <48 F1

360 85 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼2-Nitrophenol <85 F1

180 60 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼3 & 4 Methylphenol <60 F1

180 50 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼3,3'-Dichlorobenzidine <50 F1

360 110 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼3-Nitroaniline <110

360 290 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4,6-Dinitro-2-methylphenol <290 F1

180 47 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4-Bromophenyl phenyl ether <47

360 120 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4-Chloro-3-methylphenol <120 F1

730 170 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4-Chloroaniline <170

180 42 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4-Chlorophenyl phenyl ether <42


730 340 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼4-Nitrophenol <340

36 6.5 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Acenaphthene <6.5

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Acenaphthylene <4.7 F1 36 4.7 ug/Kg ☼ 04/20/15 16:14 04/23/15 14:39 1


36 6.0 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Anthracene <6.0 F1

36 4.8 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzo[a]anthracene 13 J

36 7.0 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzo[a]pyrene 13 J

36 7.8 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzo[b]fluoranthene 17 J

36 12 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzo[g,h,i]perylene 14 J

36 11 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzo[k]fluoranthene <11

1800 400 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzoic acid <400 * F1

360 110 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Benzyl alcohol <110 F1 F2

180 37 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Bis(2-chloroethoxy)methane <37 F1

180 54 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Bis(2-chloroethyl)ether <54 F1

180 66 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Bis(2-ethylhexyl) phthalate <66 F2

180 68 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Butyl benzyl phthalate <68 F1 F2

180 93 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Carbazole <93 F1

36 9.8 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Chrysene 14 J

36 7.0 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Dibenz(a,h)anthracene <7.0

180 42 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Dibenzofuran <42

180 61 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Diethyl phthalate <61

180 47 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Dimethyl phthalate <47

180 55 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Di-n-butyl phthalate <55

180 59 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Di-n-octyl phthalate <59 F1 F2

36 6.7 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Fluoranthene 21 J F1

36 5.1 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Fluorene <5.1

73 8.3 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Hexachlorobenzene <8.3


730 210 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Hexachlorocyclopentadiene <210 F1 *

180 55 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Hexachloroethane <55 F1

36 9.3 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Indeno[1,2,3-cd]pyrene 9.7 J

180 40 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Isophorone <40 F1

36 5.5 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Naphthalene <5.5 F1

36 9.0 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Nitrobenzene <9.0 F1

180 44 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼N-Nitrosodi-n-propylamine <44 F1

180 42 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼N-Nitrosodiphenylamine <42

730 580 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Pentachlorophenol <580

36 5.0 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Phenanthrene 8.6 J F1

180 80 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Phenol <80 F1

36 7.1 ug/Kg 04/20/15 16:14 04/23/15 14:39 1☼Pyrene 20 J F1 F2



2-Fluorobiphenyl 50 04/20/15 16:14 04/23/15 14:39 125 - 119



Phenol-d5 (Surr) 34 04/20/15 16:14 04/23/15 14:39 131 - 110

Terphenyl-d14 (Surr) 71 04/20/15 16:14 04/23/15 14:39 136 - 134

Method: 6010B - Metals (ICP)RL MDL

Arsenic 0.84 J 0.99 0.46 mg/Kg ☼ 04/17/15 08:50 04/19/15 02:49 1


0.99 0.18 mg/Kg 04/17/15 08:50 04/19/15 02:49 1☼Barium 8.6

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Method: 6010B - Metals (ICP) (Continued)RL MDL

Cadmium <0.057 0.20 0.057 mg/Kg ☼ 04/17/15 08:50 04/19/15 02:49 1


0.99 0.17 mg/Kg 04/17/15 08:50 04/19/15 02:49 1☼Chromium 4.4

0.49 0.25 mg/Kg 04/17/15 08:50 04/19/15 02:49 1☼Lead 3.4

0.99 0.49 mg/Kg 04/17/15 08:50 04/19/15 02:49 1☼Selenium <0.49

0.49 0.12 mg/Kg 04/17/15 08:50 04/19/15 02:49 1☼Silver <0.12


Mercury 0.028 0.018 0.0062 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:00 1





























17 5.1 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Benzene <5.1




140 31 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Bromoform <31





69 14 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Chloroform <14 *


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cis-1,2-Dichloroethene <8.5 * 69 8.5 ug/Kg ☼ 04/09/15 10:30 04/20/15 16:29 50








140 10 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Isopropyl ether <10








69 11 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼sec-Butylbenzene <11

69 6.9 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Styrene <6.9 *


69 12 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Tetrachloroethene <12 *

17 8.0 ug/Kg 04/09/15 10:30 04/20/15 16:29 50☼Toluene <8.0 *











Toluene-d8 (Surr) 95 04/09/15 10:30 04/20/15 16:29 5075 - 120


1-Methylnaphthalene <9.4 38 9.4 ug/Kg ☼ 04/20/15 16:14 04/23/15 15:00 1



38 6.9 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Acenaphthene 15 J

38 5.1 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Acenaphthylene <5.1

38 6.4 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Anthracene 49

38 5.2 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Benzo[a]anthracene 89

38 7.4 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Benzo[a]pyrene 71

38 8.3 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Benzo[b]fluoranthene 89

38 12 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Benzo[g,h,i]perylene 44

38 11 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Benzo[k]fluoranthene 30 J

38 10 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Chrysene 77


38 7.1 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Fluoranthene 190

38 5.4 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Fluorene 17 J

38 9.9 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Indeno[1,2,3-cd]pyrene 35 J

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Naphthalene <5.9 38 5.9 ug/Kg ☼ 04/20/15 16:14 04/23/15 15:00 1


38 5.3 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Phenanthrene 160

38 7.6 ug/Kg 04/20/15 16:14 04/23/15 15:00 1☼Pyrene 170

2-Fluorobiphenyl 47 25 - 119 04/20/15 16:14 04/23/15 15:00 1



Terphenyl-d14 (Surr) 70 04/20/15 16:14 04/23/15 15:00 136 - 134

Lab Sample ID: 500-94669-3Client Sample ID: SB1 FDMatrix: SolidDate Collected: 04/09/15 10:15



























16 4.6 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼Benzene <4.6




120 27 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼Bromoform <27





62 13 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼Chloroform <13 *



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cis-1,3-Dichloropropene <11 62 11 ug/Kg ☼ 04/09/15 10:15 04/20/15 16:56 50















62 9.6 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼sec-Butylbenzene <9.6

62 6.1 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼Styrene <6.1 *



16 7.2 ug/Kg 04/09/15 10:15 04/20/15 16:56 50☼Toluene <7.2 *











Toluene-d8 (Surr) 95 04/09/15 10:15 04/20/15 16:56 5075 - 120


1,2,4-Trichlorobenzene <39 180 39 ug/Kg ☼ 04/20/15 16:14 04/23/15 15:20 1









360 86 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2,4-Dichlorophenol <86

360 140 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2,4-Dimethylphenol <140

730 640 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2,4-Dinitrophenol <640

180 58 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2,4-Dinitrotoluene <58


180 40 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2-Chloronaphthalene <40

180 62 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼2-Chlorophenol <62


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2-Methylphenol <58 180 58 ug/Kg ☼ 04/20/15 16:14 04/23/15 15:20 1




180 61 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼3 & 4 Methylphenol <61

180 51 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼3,3'-Dichlorobenzidine <51


360 290 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼4,6-Dinitro-2-methylphenol <290


360 120 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼4-Chloro-3-methylphenol <120







36 6.1 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Anthracene <6.1



36 7.9 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Benzo[b]fluoranthene 22 J

36 12 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Benzo[g,h,i]perylene <12


1800 410 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Benzoic acid <410 *

360 110 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Benzyl alcohol <110

180 37 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Bis(2-chloroethoxy)methane <37

180 55 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Bis(2-chloroethyl)ether <55

180 66 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Bis(2-ethylhexyl) phthalate <66

180 69 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Butyl benzyl phthalate <69

180 94 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Carbazole <94

36 9.9 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Chrysene 19 J






180 59 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Di-n-octyl phthalate <59


36 5.1 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Fluorene <5.1



730 210 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Hexachlorocyclopentadiene <210 *

180 55 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Hexachloroethane <55


180 41 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Isophorone <41

36 5.6 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Naphthalene <5.6

36 9.1 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Nitrobenzene <9.1

180 44 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼N-Nitrosodi-n-propylamine <44



36 5.1 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Phenanthrene 16 J

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Phenol <81 180 81 ug/Kg ☼ 04/20/15 16:14 04/23/15 15:20 1


36 7.2 ug/Kg 04/20/15 16:14 04/23/15 15:20 1☼Pyrene 36

2,4,6-Tribromophenol (Surr) 30 X 35 - 137 04/20/15 16:14 04/23/15 15:20 1


2-Fluorobiphenyl 54 04/20/15 16:14 04/23/15 15:20 125 - 119



Phenol-d5 (Surr) 38 04/20/15 16:14 04/23/15 15:20 131 - 110

Terphenyl-d14 (Surr) 69 04/20/15 16:14 04/23/15 15:20 136 - 134


Arsenic 1.0 J 1.1 0.50 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:13 1


1.1 0.20 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Barium 27

0.22 0.063 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Cadmium <0.063

1.1 0.19 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Chromium 9.7

0.54 0.27 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Lead 5.4

1.1 0.54 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Selenium 1.1

0.54 0.13 mg/Kg 04/17/15 08:50 04/19/15 03:13 1☼Silver <0.13


Mercury 0.042 0.019 0.0065 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:02 1

























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1,4-Dichlorobenzene <12 140 12 ug/Kg ☼ 04/09/15 11:51 04/20/15 17:24 50





17 5.1 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Benzene <5.1




140 30 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Bromoform <30





69 14 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Chloroform <14 *









140 10 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Isopropyl ether <10









69 6.8 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Styrene <6.8 *



17 7.9 ug/Kg 04/09/15 11:51 04/20/15 17:24 50☼Toluene <7.9 *











Toluene-d8 (Surr) 95 04/09/15 11:51 04/20/15 17:24 5075 - 120

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37 6.3 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Anthracene <6.3

37 5.1 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Benzo[a]anthracene <5.1

37 7.3 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Benzo[a]pyrene <7.3

37 8.1 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Benzo[b]fluoranthene <8.1









190 97 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Carbazole <97

37 10 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Chrysene <10





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Di-n-butyl phthalate <57 190 57 ug/Kg ☼ 04/20/15 16:14 04/23/15 04:58 1



37 7.0 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Fluoranthene <7.0

37 5.3 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Fluorene <5.3





37 9.8 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Indeno[1,2,3-cd]pyrene <9.8

190 42 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Isophorone <42






37 5.3 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Phenanthrene <5.3

190 84 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Phenol <84

37 7.5 ug/Kg 04/20/15 16:14 04/23/15 04:58 1☼Pyrene <7.5



2-Fluorobiphenyl 49 04/20/15 16:14 04/23/15 04:58 125 - 119



Phenol-d5 (Surr) 49 04/20/15 16:14 04/23/15 04:58 131 - 110

Terphenyl-d14 (Surr) 72 04/20/15 16:14 04/23/15 04:58 136 - 134


Arsenic 2.0 1.1 0.53 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:17 1


1.1 0.21 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Barium 45

0.23 0.066 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Cadmium <0.066

1.1 0.20 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Chromium 15

0.57 0.28 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Lead 7.8

1.1 0.56 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Selenium <0.56

0.57 0.13 mg/Kg 04/17/15 08:50 04/19/15 03:17 1☼Silver <0.13


Mercury 0.0090 J 0.017 0.0060 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:04 1









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1,1,2-Trichloroethane <18 63 18 ug/Kg ☼ 04/09/15 11:54 04/20/15 17:51 50





















16 4.7 ug/Kg 04/09/15 11:54 04/20/15 17:51 50☼Benzene <4.7




130 28 ug/Kg 04/09/15 11:54 04/20/15 17:51 50☼Bromoform <28





63 13 ug/Kg 04/09/15 11:54 04/20/15 17:51 50☼Chloroform <13 *


















63 6.2 ug/Kg 04/09/15 11:54 04/20/15 17:51 50☼Styrene <6.2 *


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Tetrachloroethene <10 * 63 10 ug/Kg ☼ 04/09/15 11:54 04/20/15 17:51 50


16 7.2 ug/Kg 04/09/15 11:54 04/20/15 17:51 50☼Toluene 16 *











Toluene-d8 (Surr) 96 04/09/15 11:54 04/20/15 17:51 5075 - 120


1-Methylnaphthalene 28 J 36 8.8 ug/Kg ☼ 04/20/15 16:14 04/23/15 05:19 1


36 6.6 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼2-Methylnaphthalene 33 J



36 6.0 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Anthracene <6.0





36 11 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Benzo[k]fluoranthene 14 J

36 9.8 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Chrysene 34 J



36 5.1 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Fluorene <5.1


36 5.5 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Naphthalene 24 J


36 7.2 ug/Kg 04/20/15 16:14 04/23/15 05:19 1☼Pyrene 50

2-Fluorobiphenyl 43 25 - 119 04/20/15 16:14 04/23/15 05:19 1



Terphenyl-d14 (Surr) 65 04/20/15 16:14 04/23/15 05:19 136 - 134








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1,1,2-Trichloroethane <19 67 19 ug/Kg ☼ 04/09/15 09:36 04/20/15 18:18 50





















17 5.0 ug/Kg 04/09/15 09:36 04/20/15 18:18 50☼Benzene <5.0




130 29 ug/Kg 04/09/15 09:36 04/20/15 18:18 50☼Bromoform <29





67 14 ug/Kg 04/09/15 09:36 04/20/15 18:18 50☼Chloroform <14 *


















67 6.6 ug/Kg 04/09/15 09:36 04/20/15 18:18 50☼Styrene <6.6 *


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Tetrachloroethene <11 * 67 11 ug/Kg ☼ 04/09/15 09:36 04/20/15 18:18 50


17 7.7 ug/Kg 04/09/15 09:36 04/20/15 18:18 50☼Toluene <7.7 *











Toluene-d8 (Surr) 96 04/09/15 09:36 04/20/15 18:18 5075 - 120


































36 6.1 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Anthracene <6.1


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Benzo[a]pyrene <7.1 36 7.1 ug/Kg ☼ 04/20/15 16:14 04/23/15 07:21 1











180 94 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Carbazole <94

36 9.9 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Chrysene <9.9








36 5.1 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Fluorene <5.1






180 41 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Isophorone <41







180 81 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Phenol <81

36 7.2 ug/Kg 04/20/15 16:14 04/23/15 07:21 1☼Pyrene <7.2



2-Fluorobiphenyl 48 04/20/15 16:14 04/23/15 07:21 125 - 119



Phenol-d5 (Surr) 36 04/20/15 16:14 04/23/15 07:21 131 - 110

Terphenyl-d14 (Surr) 108 04/20/15 16:14 04/23/15 07:21 136 - 134


Arsenic 2.1 1.0 0.48 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:22 1


1.0 0.19 mg/Kg 04/17/15 08:50 04/19/15 03:22 1☼Barium 58

0.21 0.061 mg/Kg 04/17/15 08:50 04/19/15 03:22 1☼Cadmium <0.061

1.0 0.18 mg/Kg 04/17/15 08:50 04/19/15 03:22 1☼Chromium 17

0.52 0.26 mg/Kg 04/17/15 08:50 04/19/15 03:22 1☼Lead 7.6

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Method: 6010B - Metals (ICP) (Continued)RL MDL

Selenium 0.69 J 1.0 0.52 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:22 1


0.52 0.12 mg/Kg 04/17/15 08:50 04/19/15 03:22 1☼Silver <0.12


Mercury 0.026 0.018 0.0062 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:10 1

























110 9.8 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼1,4-Dichlorobenzene <9.8




14 4.2 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼Benzene <4.2




110 25 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼Bromoform <25





56 12 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼Chloroform <12 *





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Dibromomethane <27 * 110 27 ug/Kg ☼ 04/09/15 09:38 04/20/15 18:46 50











110 9.8 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼N-Propylbenzene <9.8



56 5.5 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼Styrene <5.5 *



14 6.5 ug/Kg 04/09/15 09:38 04/20/15 18:46 50☼Toluene <6.5 *











Toluene-d8 (Surr) 95 04/09/15 09:38 04/20/15 18:46 5075 - 120







33 5.6 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Anthracene <5.6

33 4.5 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Benzo[a]anthracene 7.3 J




33 9.9 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Benzo[k]fluoranthene <9.9

33 9.1 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Chrysene <9.1


33 6.2 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Fluoranthene 7.4 J

33 4.7 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Fluorene <4.7




33 6.7 ug/Kg 04/20/15 16:14 04/23/15 15:40 1☼Pyrene 7.7 J

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2-Fluorobiphenyl 33 25 - 119 04/20/15 16:14 04/23/15 15:40 1


Nitrobenzene-d5 (Surr) 23 X 04/20/15 16:14 04/23/15 15:40 125 - 115

Terphenyl-d14 (Surr) 52 04/20/15 16:14 04/23/15 15:40 136 - 134















110 12 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼1,2,4-Trimethylbenzene 71 J













14 4.3 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Benzene 38




110 25 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Bromoform <25





57 12 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Chloroform <12 *







14 7.2 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Ethylbenzene 34 *

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Hexachlorobutadiene <20 110 20 ug/Kg ☼ 04/09/15 12:46 04/20/15 19:13 50






110 28 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Naphthalene 190





57 5.7 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Styrene <5.7 *



14 6.6 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Toluene 280 *






29 3.9 ug/Kg 04/09/15 12:46 04/20/15 19:13 50☼Xylenes, Total 330





Toluene-d8 (Surr) 95 04/09/15 12:46 04/20/15 19:13 5075 - 120







35 8.5 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼1-Methylnaphthalene 60

















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3-Nitroaniline <110 350 110 ug/Kg ☼ 04/20/15 16:14 04/23/15 16:01 1










35 4.6 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Acenaphthylene 19 J

35 5.8 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Anthracene 13 J


35 6.8 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Benzo[a]pyrene 160


35 11 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Benzo[g,h,i]perylene 170

35 10 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Benzo[k]fluoranthene 89





180 64 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Bis(2-ethylhexyl) phthalate 100 J


180 90 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Carbazole <90

35 9.5 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Chrysene 110








35 4.9 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Fluorene <4.9





35 9.0 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Indeno[1,2,3-cd]pyrene 160

180 39 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Isophorone <39

35 5.4 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Naphthalene 57






180 78 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Phenol <78

35 6.9 ug/Kg 04/20/15 16:14 04/23/15 16:01 1☼Pyrene 150



2-Fluorobiphenyl 62 04/20/15 16:14 04/23/15 16:01 125 - 119

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2-Fluorophenol (Surr) 55 25 - 110 04/20/15 16:14 04/23/15 16:01 1



Phenol-d5 (Surr) 36 04/20/15 16:14 04/23/15 16:01 131 - 110

Terphenyl-d14 (Surr) 120 04/20/15 16:14 04/23/15 16:01 136 - 134


Arsenic 0.90 J 1.0 0.47 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:34 1


1.0 0.19 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Barium 19

0.20 0.059 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Cadmium <0.059

1.0 0.18 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Chromium 6.8

0.51 0.25 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Lead 13

1.0 0.50 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Selenium 0.73 J

0.51 0.12 mg/Kg 04/17/15 08:50 04/19/15 03:34 1☼Silver <0.12


Mercury 0.024 0.018 0.0063 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:12 1





























15 4.5 ug/Kg 04/09/15 12:48 04/20/15 19:41 50☼Benzene <4.5


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Bromochloromethane <23 * 120 23 ug/Kg ☼ 04/09/15 12:48 04/20/15 19:41 50



120 26 ug/Kg 04/09/15 12:48 04/20/15 19:41 50☼Bromoform <26





60 12 ug/Kg 04/09/15 12:48 04/20/15 19:41 50☼Chloroform <12 *


















60 5.9 ug/Kg 04/09/15 12:48 04/20/15 19:41 50☼Styrene <5.9 *



15 6.9 ug/Kg 04/09/15 12:48 04/20/15 19:41 50☼Toluene <6.9 *











Toluene-d8 (Surr) 95 04/09/15 12:48 04/20/15 19:41 5075 - 120







33 5.6 ug/Kg 04/20/15 16:14 04/23/15 05:39 1☼Anthracene <5.6


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Benzo[a]pyrene <6.5 33 6.5 ug/Kg ☼ 04/20/15 16:14 04/23/15 05:39 1




33 9.9 ug/Kg 04/20/15 16:14 04/23/15 05:39 1☼Benzo[k]fluoranthene <9.9

33 9.1 ug/Kg 04/20/15 16:14 04/23/15 05:39 1☼Chrysene <9.1



33 4.7 ug/Kg 04/20/15 16:14 04/23/15 05:39 1☼Fluorene <4.7




33 6.6 ug/Kg 04/20/15 16:14 04/23/15 05:39 1☼Pyrene <6.6

2-Fluorobiphenyl 53 25 - 119 04/20/15 16:14 04/23/15 05:39 1



Terphenyl-d14 (Surr) 89 04/20/15 16:14 04/23/15 05:39 136 - 134




























17 4.9 ug/Kg 04/09/15 11:26 04/20/15 20:08 50☼Benzene <4.9



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Bromodichloromethane <23 * 130 23 ug/Kg ☼ 04/09/15 11:26 04/20/15 20:08 50


130 29 ug/Kg 04/09/15 11:26 04/20/15 20:08 50☼Bromoform <29





67 14 ug/Kg 04/09/15 11:26 04/20/15 20:08 50☼Chloroform <14 *


















67 6.6 ug/Kg 04/09/15 11:26 04/20/15 20:08 50☼Styrene <6.6 *



17 7.7 ug/Kg 04/09/15 11:26 04/20/15 20:08 50☼Toluene <7.7 *











Toluene-d8 (Surr) 95 04/09/15 11:26 04/20/15 20:08 5075 - 120










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2,4,6-Trichlorophenol <130 370 130 ug/Kg ☼ 04/20/15 16:14 04/23/15 06:00 1

























37 6.2 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Anthracene <6.2












190 96 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Carbazole <96

37 10 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Chrysene <10








37 5.2 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Fluorene <5.2




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Hexachloroethane <57 190 57 ug/Kg ☼ 04/20/15 16:14 04/23/15 06:00 1



190 42 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Isophorone <42







190 83 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Phenol <83

37 7.4 ug/Kg 04/20/15 16:14 04/23/15 06:00 1☼Pyrene <7.4



2-Fluorobiphenyl 56 04/20/15 16:14 04/23/15 06:00 125 - 119



Phenol-d5 (Surr) 42 04/20/15 16:14 04/23/15 06:00 131 - 110

Terphenyl-d14 (Surr) 82 04/20/15 16:14 04/23/15 06:00 136 - 134


Arsenic 1.0 0.99 0.46 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:39 1


0.99 0.18 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Barium 33

0.20 0.057 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Cadmium <0.057

0.99 0.17 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Chromium 11

0.50 0.25 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Lead 4.5

0.99 0.49 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Selenium <0.49

0.50 0.12 mg/Kg 04/17/15 08:50 04/19/15 03:39 1☼Silver <0.12


Mercury 0.015 J 0.018 0.0064 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:14 1
















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1,2,4-Trimethylbenzene <14 130 14 ug/Kg ☼ 04/09/15 13:26 04/20/15 20:36 50














17 5.0 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Benzene 24




130 30 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Bromoform <30





67 14 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Chloroform <14 *







17 8.5 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Ethylbenzene 17 *






130 33 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Naphthalene 74 J





67 6.7 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Styrene <6.7 *



17 7.8 ug/Kg 04/09/15 13:26 04/20/15 20:36 50☼Toluene 150 *






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Xylenes, Total 150 34 4.6 ug/Kg ☼ 04/09/15 13:26 04/20/15 20:36 50






Toluene-d8 (Surr) 96 04/09/15 13:26 04/20/15 20:36 5075 - 120


































38 6.4 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Anthracene 11 J





38 11 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Benzo[k]fluoranthene 56




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Bis(2-chloroethyl)ether <57 190 57 ug/Kg ☼ 04/20/15 16:14 04/23/15 07:01 1


190 70 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Bis(2-ethylhexyl) phthalate 87 J


190 99 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Carbazole <99

38 10 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Chrysene 62








38 5.4 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Fluorene <5.4






190 43 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Isophorone <43

38 5.9 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Naphthalene 130






190 85 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Phenol <85

38 7.6 ug/Kg 04/20/15 16:14 04/23/15 07:01 1☼Pyrene 99



2-Fluorobiphenyl 30 04/20/15 16:14 04/23/15 07:01 125 - 119


Nitrobenzene-d5 (Surr) 21 X 04/20/15 16:14 04/23/15 07:01 125 - 115

Phenol-d5 (Surr) 31 04/20/15 16:14 04/23/15 07:01 131 - 110

Terphenyl-d14 (Surr) 63 04/20/15 16:14 04/23/15 07:01 136 - 134


Arsenic 2.4 1.0 0.47 mg/Kg ☼ 04/17/15 08:50 04/19/15 03:44 1


1.0 0.19 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Barium 45

0.20 0.059 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Cadmium <0.059

1.0 0.18 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Chromium 15

0.51 0.25 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Lead 15

1.0 0.51 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Selenium <0.51

0.51 0.12 mg/Kg 04/17/15 08:50 04/19/15 03:44 1☼Silver <0.12


Mercury 0.039 0.018 0.0063 mg/Kg ☼ 04/17/15 12:00 04/20/15 10:16 1


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Lab Sample ID: 500-94669-12Client Sample ID: Trip BlankMatrix: SolidDate Collected: 04/09/15 00:00



1,1,1,2-Tetrachloroethane <17 * 100 17 ug/Kg 04/09/15 00:00 04/20/15 14:12 50


50 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1,1-Trichloroethane <10 *

50 12 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1,2,2-Tetrachloroethane <12

50 14 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1,2-Trichloroethane <14

50 9.3 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1-Dichloroethane <9.3 *

50 15 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1-Dichloroethene <15

50 17 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,1-Dichloropropene <17

100 18 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2,3-Trichlorobenzene <18

100 29 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2,3-Trichloropropane <29

100 19 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2,4-Trichlorobenzene <19

100 11 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2,4-Trimethylbenzene <11

100 44 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2-Dibromo-3-Chloropropane <44

100 16 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2-Dibromoethane <16 *

100 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2-Dichlorobenzene <10

50 14 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2-Dichloroethane <14

50 9.8 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,2-Dichloropropane <9.8 *

100 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,3,5-Trimethylbenzene <10

100 13 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,3-Dichlorobenzene <13

50 6.7 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,3-Dichloropropane <6.7

100 8.7 ug/Kg 04/09/15 00:00 04/20/15 14:12 501,4-Dichlorobenzene <8.7

50 16 ug/Kg 04/09/15 00:00 04/20/15 14:12 502,2-Dichloropropane <16

50 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 502-Chlorotoluene <10

50 9.9 ug/Kg 04/09/15 00:00 04/20/15 14:12 504-Chlorotoluene <9.9

13 3.7 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Benzene <3.7

100 21 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Bromobenzene <21

100 19 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Bromochloromethane <19 *

100 17 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Bromodichloromethane <17 *

100 22 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Bromoform <22

100 34 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Bromomethane <34

50 13 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Carbon tetrachloride <13 *

50 7.2 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Chlorobenzene <7.2

100 22 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Chloroethane <22

50 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Chloroform <10 *

100 23 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Chloromethane <23

50 6.2 ug/Kg 04/09/15 00:00 04/20/15 14:12 50cis-1,2-Dichloroethene <6.2 *

50 8.9 ug/Kg 04/09/15 00:00 04/20/15 14:12 50cis-1,3-Dichloropropene <8.9

100 17 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Dibromochloromethane <17

100 24 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Dibromomethane <24 *

100 26 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Dichlorodifluoromethane <26

13 6.3 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Ethylbenzene <6.3 *

100 17 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Hexachlorobutadiene <17

100 7.4 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Isopropyl ether <7.4

100 13 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Isopropylbenzene <13

100 22 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Methyl tert-butyl ether <22

250 34 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Methylene Chloride <34

100 25 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Naphthalene <25

50 6.5 ug/Kg 04/09/15 00:00 04/20/15 14:12 50n-Butylbenzene <6.5

100 8.8 ug/Kg 04/09/15 00:00 04/20/15 14:12 50N-Propylbenzene <8.8

100 9.3 ug/Kg 04/09/15 00:00 04/20/15 14:12 50p-Isopropyltoluene <9.3

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Lab Sample ID: 500-94669-12Client Sample ID: Trip BlankMatrix: SolidDate Collected: 04/09/15 00:00



sec-Butylbenzene <7.7 50 7.7 ug/Kg 04/09/15 00:00 04/20/15 14:12 50


50 4.9 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Styrene <4.9 *

50 6.8 ug/Kg 04/09/15 00:00 04/20/15 14:12 50tert-Butylbenzene <6.8

50 8.4 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Tetrachloroethene <8.4 *

13 5.8 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Toluene <5.8 *

50 13 ug/Kg 04/09/15 00:00 04/20/15 14:12 50trans-1,2-Dichloroethene <13

50 10 ug/Kg 04/09/15 00:00 04/20/15 14:12 50trans-1,3-Dichloropropene <10

25 9.3 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Trichloroethene <9.3 *

100 21 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Trichlorofluoromethane <21

13 5.2 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Vinyl chloride <5.2

25 3.4 ug/Kg 04/09/15 00:00 04/20/15 14:12 50Xylenes, Total <3.4





Toluene-d8 (Surr) 96 04/09/15 00:00 04/20/15 14:12 5075 - 120

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Definitions/GlossaryTestAmerica Job ID: 500-94669-1Client: Stantec Consulting Corporation/Bonestroo


Qualifiers

GC/MS VOA


* LCS or LCSD is outside acceptance limits.

Qualifier


GC/MS Semi VOA


F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier


* LCS or LCSD is outside acceptance limits.

F2 MS/MSD RPD exceeds control limits

E Result exceeded calibration range.

X Surrogate is outside control limits

Metals



Qualifier

F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the

absolute difference is less than the RL.

F3 Duplicate RPD exceeds the control limit

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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GC/MS VOA

Prep Batch: 284058


Solid 5035500-94669-1 SB1 (2-4) Total/NA

Solid 5035500-94669-1 MS SB1 (2-4) Total/NA

Solid 5035500-94669-1 MSD SB1 (2-4) Total/NA

Solid 5035500-94669-2 SB1 (6-8) Total/NA

Solid 5035500-94669-3 SB1 FD Total/NA

Solid 5035500-94669-4 SB2 (2-4) Total/NA

Solid 5035500-94669-5 SB2 (4-6) Total/NA

Solid 5035500-94669-6 SB3 (2-4) Total/NA

Solid 5035500-94669-7 SB3 (6-8) Total/NA

Solid 5035500-94669-8 SB4 (2-4) Total/NA

Solid 5035500-94669-9 SB4 (4-6) Total/NA

Solid 5035500-94669-10 SB5 (2-4) Total/NA

Solid 5035500-94669-11 SB6 (2-4) Total/NA

Solid 5035500-94669-12 Trip Blank Total/NA

Solid 5035LB3 500-284058/20-A Method Blank Total/NA

Solid 5035LCS 500-284058/21-A Lab Control Sample Total/NA



Solid 8260B 284058LB3 500-284058/20-A Method Blank Total/NA

Solid 8260BLCS 500-284358/4 Lab Control Sample Total/NA

Solid 8260BMB 500-284358/7 Method Blank Total/NA



Solid 8260B 284058500-94669-1 SB1 (2-4) Total/NA

Solid 8260B 284058500-94669-1 MS SB1 (2-4) Total/NA

Solid 8260B 284058500-94669-1 MSD SB1 (2-4) Total/NA


Solid 8260B 284058500-94669-3 SB1 FD Total/NA









Solid 8260B 284058500-94669-12 Trip Blank Total/NA

Solid 8260B 284058LCS 500-284058/21-A Lab Control Sample Total/NA

Solid 8260BLCS 500-284574/4 Lab Control Sample Total/NA

Solid 8260BMB 500-284574/7 Method Blank Total/NA

GC/MS Semi VOA

Prep Batch: 284633


Solid 3541500-94669-1 SB1 (2-4) Total/NA

Solid 3541500-94669-1 MS SB1 (2-4) Total/NA

Solid 3541500-94669-1 MSD SB1 (2-4) Total/NA

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GC/MS Semi VOA (Continued)

Prep Batch: 284633 (Continued)


Solid 3541500-94669-2 SB1 (6-8) Total/NA

Solid 3541500-94669-3 SB1 FD Total/NA

Solid 3541500-94669-4 SB2 (2-4) Total/NA

Solid 3541500-94669-5 SB2 (4-6) Total/NA

Solid 3541500-94669-6 SB3 (2-4) Total/NA

Solid 3541500-94669-7 SB3 (6-8) Total/NA

Solid 3541500-94669-8 SB4 (2-4) Total/NA

Solid 3541500-94669-9 SB4 (4-6) Total/NA

Solid 3541500-94669-10 SB5 (2-4) Total/NA

Solid 3541500-94669-11 SB6 (2-4) Total/NA

Solid 3541LCS 500-284633/2-A Lab Control Sample Total/NA

Solid 3541MB 500-284633/1-A Method Blank Total/NA



Solid 8270D 284633LCS 500-284633/2-A Lab Control Sample Total/NA

Solid 8270D 284633MB 500-284633/1-A Method Blank Total/NA



Solid 8270D 284633500-94669-4 SB2 (2-4) Total/NA









Solid 8270D 284633500-94669-1 MS SB1 (2-4) Total/NA

Solid 8270D 284633500-94669-1 MSD SB1 (2-4) Total/NA


Solid 8270D 284633500-94669-3 SB1 FD Total/NA



Metals

Prep Batch: 284279


Solid 3050B500-94669-1 SB1 (2-4) Total/NA

Solid 3050B500-94669-1 DU SB1 (2-4) Total/NA

Solid 3050B500-94669-1 MS SB1 (2-4) Total/NA

Solid 3050B500-94669-1 MSD SB1 (2-4) Total/NA

Solid 3050B500-94669-3 SB1 FD Total/NA





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Metals (Continued)

Prep Batch: 284279 (Continued)



Solid 3050BLCS 500-284279/2-A Lab Control Sample Total/NA

Solid 3050BMB 500-284279/1-A Method Blank Total/NA

Prep Batch: 284308


Solid 7471A500-94669-1 SB1 (2-4) Total/NA

Solid 7471A500-94669-3 SB1 FD Total/NA






Solid 7471ALCS 500-284308/13-A Lab Control Sample Total/NA

Solid 7471AMB 500-284308/12-A Method Blank Total/NA




Solid 6010B 284279500-94669-1 DU SB1 (2-4) Total/NA

Solid 6010B 284279500-94669-1 MS SB1 (2-4) Total/NA

Solid 6010B 284279500-94669-1 MSD SB1 (2-4) Total/NA

Solid 6010B 284279500-94669-3 SB1 FD Total/NA






Solid 6010B 284279LCS 500-284279/2-A Lab Control Sample Total/NA

Solid 6010B 284279MB 500-284279/1-A Method Blank Total/NA



Solid 7471A 284308500-94669-1 SB1 (2-4) Total/NA

Solid 7471A 284308500-94669-3 SB1 FD Total/NA






Solid 7471A 284308LCS 500-284308/13-A Lab Control Sample Total/NA

Solid 7471A 284308MB 500-284308/12-A Method Blank Total/NA

General Chemistry



Solid Moisture500-94669-1 SB1 (2-4) Total/NA


Solid Moisture500-94669-3 SB1 FD Total/NA

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General Chemistry (Continued)

Analysis Batch: 283935 (Continued)










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Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE BFB DBFM TOL

99 85 99 93500-94669-1


SB1 (2-4)

110 94 105 94500-94669-1 MS SB1 (2-4)

97 91 98 93500-94669-1 MSD SB1 (2-4)

98 86 98 95500-94669-2 SB1 (6-8)

99 86 101 95500-94669-3 SB1 FD

105 87 102 95500-94669-4 SB2 (2-4)

100 84 101 96500-94669-5 SB2 (4-6)

100 86 101 96500-94669-6 SB3 (2-4)

103 86 103 95500-94669-7 SB3 (6-8)

97 85 96 95500-94669-8 SB4 (2-4)

101 86 100 95500-94669-9 SB4 (4-6)

100 86 101 95500-94669-10 SB5 (2-4)

101 86 101 96500-94669-11 SB6 (2-4)

98 87 100 96500-94669-12 Trip Blank

103 85 103 95LB3 500-284058/20-A Method Blank

96 90 98 94LCS 500-284058/21-A Lab Control Sample



99 87 102 95MB 500-284358/7 Method Blank

95 86 96 94MB 500-284574/7 Method Blank

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (35-137) (25-119) (25-110) (25-115) (31-110) (36-134)

TBP FBP 2FP NBZ PHL TPH

40 50 38 33 34 71500-94669-1


SB1 (2-4)

68 51 37 3733 252 X500-94669-1 MS SB1 (2-4)

54 48 37 3735 156 X500-94669-1 MSD SB1 (2-4)

47 28 70500-94669-2 SB1 (6-8)

30 X 54 45 3838 69500-94669-3 SB1 FD

24 X 49 53 4942 72500-94669-4 SB2 (2-4)

43 33 65500-94669-5 SB2 (4-6)

46 48 43 3630 108500-94669-6 SB3 (2-4)

33 23 X 52500-94669-7 SB3 (6-8)

56 62 55 3646 120500-94669-8 SB4 (2-4)

53 39 89500-94669-9 SB4 (4-6)

45 56 48 4237 82500-94669-10 SB5 (2-4)

30 X 30 36 3121 X 63500-94669-11 SB6 (2-4)

88 81 74 6868 92LCS 500-284633/2-A Lab Control Sample

60 81 74 5652 100MB 500-284633/1-A Method Blank

Surrogate Legend

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TBP = 2,4,6-Tribromophenol (Surr)

FBP = 2-Fluorobiphenyl

2FP = 2-Fluorophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPH = Terphenyl-d14 (Surr)

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Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: LB3 500-284058/20-A

Matrix: Solid Prep Type: Total/NA


RL MDL

1,1,1,2-Tetrachloroethane <17 100 17 ug/Kg 04/16/15 07:30 04/17/15 16:54 50

LB3 LB3


<10 1050 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1,1-Trichloroethane

<12 1250 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1,2,2-Tetrachloroethane

<14 1450 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1,2-Trichloroethane

<9.3 9.350 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1-Dichloroethane

<15 1550 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1-Dichloroethene

<17 1750 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,1-Dichloropropene

<18 18100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2,3-Trichlorobenzene

<29 29100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2,3-Trichloropropane

<19 19100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2,4-Trichlorobenzene

<11 11100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2,4-Trimethylbenzene

<44 44100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2-Dibromo-3-Chloropropane

<16 16100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2-Dibromoethane

<10 10100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2-Dichlorobenzene

<14 1450 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2-Dichloroethane

<9.8 9.850 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,2-Dichloropropane

<10 10100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,3,5-Trimethylbenzene


<6.7 6.750 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,3-Dichloropropane

<8.7 8.7100 ug/Kg 04/16/15 07:30 04/17/15 16:54 501,4-Dichlorobenzene

<16 1650 ug/Kg 04/16/15 07:30 04/17/15 16:54 502,2-Dichloropropane

<10 1050 ug/Kg 04/16/15 07:30 04/17/15 16:54 502-Chlorotoluene

<9.9 9.950 ug/Kg 04/16/15 07:30 04/17/15 16:54 504-Chlorotoluene

<3.7 3.713 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Benzene

<21 21100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Bromobenzene

<19 19100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Bromochloromethane

<17 17100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Bromodichloromethane

<22 22100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Bromoform

<34 34100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Bromomethane

<13 1350 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Carbon tetrachloride

<7.2 7.250 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Chlorobenzene

<22 22100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Chloroethane

<10 1050 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Chloroform

<23 23100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Chloromethane

<6.2 6.250 ug/Kg 04/16/15 07:30 04/17/15 16:54 50cis-1,2-Dichloroethene

<8.9 8.950 ug/Kg 04/16/15 07:30 04/17/15 16:54 50cis-1,3-Dichloropropene

<17 17100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Dibromochloromethane

<24 24100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Dibromomethane

<26 26100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Dichlorodifluoromethane

<6.3 6.313 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Ethylbenzene

<17 17100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Hexachlorobutadiene

<7.4 7.4100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Isopropyl ether

<13 13100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Isopropylbenzene

<22 22100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Methyl tert-butyl ether

<34 34250 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Methylene Chloride

<25 25100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Naphthalene

<6.5 6.550 ug/Kg 04/16/15 07:30 04/17/15 16:54 50n-Butylbenzene

<8.8 8.8100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50N-Propylbenzene

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Client Sample ID: Method BlankLab Sample ID: LB3 500-284058/20-A



RL MDL

p-Isopropyltoluene <9.3 100 9.3 ug/Kg 04/16/15 07:30 04/17/15 16:54 50

LB3 LB3


<7.7 7.750 ug/Kg 04/16/15 07:30 04/17/15 16:54 50sec-Butylbenzene

<4.9 4.950 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Styrene

<6.8 6.850 ug/Kg 04/16/15 07:30 04/17/15 16:54 50tert-Butylbenzene

<8.4 8.450 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Tetrachloroethene

<5.8 5.813 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Toluene

<13 1350 ug/Kg 04/16/15 07:30 04/17/15 16:54 50trans-1,2-Dichloroethene

<10 1050 ug/Kg 04/16/15 07:30 04/17/15 16:54 50trans-1,3-Dichloropropene

<9.3 9.325 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Trichloroethene

<21 21100 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Trichlorofluoromethane

<5.2 5.213 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Vinyl chloride

<3.4 3.425 ug/Kg 04/16/15 07:30 04/17/15 16:54 50Xylenes, Total


LB3 LB3

Surrogate

04/16/15 07:30


85 04/16/15 07:30 04/17/15 16:54 504-Bromofluorobenzene (Surr) 75 - 120

103 04/16/15 07:30 04/17/15 16:54 50Dibromofluoromethane 75 - 120

95 04/16/15 07:30 04/17/15 16:54 50Toluene-d8 (Surr) 75 - 120




1,1,1,2-Tetrachloroethane 2500 3180 * ug/Kg 127 75 - 122

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1,1-Trichloroethane 2500 3280 * ug/Kg 131 72 - 130

1,1,2,2-Tetrachloroethane 2500 2550 ug/Kg 102 72 - 130

1,1,2-Trichloroethane 2500 3000 ug/Kg 120 75 - 120

1,1-Dichloroethane 2500 3030 * ug/Kg 121 75 - 120

1,1-Dichloroethene 2500 2970 ug/Kg 119 69 - 120

1,1-Dichloropropene 2500 3140 ug/Kg 126 75 - 130

1,2,3-Trichlorobenzene 2500 2710 ug/Kg 108 69 - 131

1,2,3-Trichloropropane 2500 2510 ug/Kg 100 65 - 132


1,2,4-Trimethylbenzene 2500 2790 ug/Kg 111 75 - 121

1,2-Dibromo-3-Chloropropane 2500 2420 ug/Kg 97 62 - 130

1,2-Dibromoethane 2500 3060 * ug/Kg 123 78 - 122

1,2-Dichlorobenzene 2500 2800 ug/Kg 112 75 - 120

1,2-Dichloroethane 2500 3120 ug/Kg 125 69 - 130

1,2-Dichloropropane 2500 3040 * ug/Kg 121 75 - 120

1,3,5-Trimethylbenzene 2500 2800 ug/Kg 112 75 - 121


1,3-Dichloropropane 2500 3000 ug/Kg 120 77 - 124


2,2-Dichloropropane 2500 3050 ug/Kg 122 65 - 132

2-Chlorotoluene 2500 2740 ug/Kg 110 75 - 120

4-Chlorotoluene 2500 2800 ug/Kg 112 75 - 120

Benzene 2500 2960 ug/Kg 118 75 - 120

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Bromobenzene 2500 2770 ug/Kg 111 75 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bromochloromethane 2500 3220 * ug/Kg 129 76 - 120

Bromodichloromethane 2500 3170 * ug/Kg 127 77 - 121

Bromoform 2500 2920 ug/Kg 117 68 - 126

Bromomethane 2500 3550 ug/Kg 142 45 - 169

Carbon tetrachloride 2500 3260 * ug/Kg 131 70 - 130

Chlorobenzene 2500 2990 ug/Kg 120 75 - 120

Chloroethane 2500 3100 ug/Kg 124 58 - 147

Chloroform 2500 3170 * ug/Kg 127 76 - 120

Chloromethane 2500 2140 ug/Kg 86 63 - 133

cis-1,2-Dichloroethene 2500 3060 * ug/Kg 122 75 - 120

cis-1,3-Dichloropropene 2500 3030 ug/Kg 121 78 - 130

Dibromochloromethane 2500 3070 ug/Kg 123 71 - 126

Dibromomethane 2500 3020 * ug/Kg 121 75 - 120

Dichlorodifluoromethane 2500 1840 ug/Kg 73 41 - 146

Ethylbenzene 2500 3160 * ug/Kg 126 75 - 120

Hexachlorobutadiene 2500 2980 ug/Kg 119 71 - 131

Isopropylbenzene 2500 2790 ug/Kg 112 75 - 121

Methyl tert-butyl ether 2500 2830 ug/Kg 113 75 - 130

Methylene Chloride 2500 3000 ug/Kg 120 73 - 130

Naphthalene 2500 2610 ug/Kg 104 69 - 135

n-Butylbenzene 2500 2880 ug/Kg 115 75 - 121

N-Propylbenzene 2500 2810 ug/Kg 113 75 - 120

p-Isopropyltoluene 2500 2890 ug/Kg 116 75 - 121

sec-Butylbenzene 2500 2840 ug/Kg 114 75 - 120

Styrene 2500 3010 * ug/Kg 121 75 - 120

tert-Butylbenzene 2500 2970 ug/Kg 119 75 - 123

Tetrachloroethene 2500 3160 * ug/Kg 126 75 - 120

Toluene 2500 3030 * ug/Kg 121 75 - 120

trans-1,2-Dichloroethene 2500 2970 ug/Kg 119 77 - 120

trans-1,3-Dichloropropene 2500 2930 ug/Kg 117 74 - 130

Trichloroethene 2500 3270 * ug/Kg 131 75 - 120

Trichlorofluoromethane 2500 2880 ug/Kg 115 71 - 130

Vinyl chloride 2500 2370 ug/Kg 95 72 - 123

Xylenes, Total 5000 5990 ug/Kg 120 75 - 120


Surrogate

96

LCS LCS





Client Sample ID: SB1 (2-4)Lab Sample ID: 500-94669-1 MS



1,1,1,2-Tetrachloroethane <20 * 2950 3190 ug/Kg 108 75 - 122☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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1,1,1-Trichloroethane <12 * 2950 2690 ug/Kg 91 72 - 130☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,1,2,2-Tetrachloroethane <14 2950 3140 ug/Kg 107 72 - 130☼

1,1,2-Trichloroethane <16 2950 3260 ug/Kg 111 75 - 120☼

1,1-Dichloroethane <11 * 2950 2680 ug/Kg 91 75 - 120☼

1,1-Dichloroethene <18 2950 2250 ug/Kg 76 69 - 120☼

1,1-Dichloropropene <20 2950 2490 ug/Kg 85 75 - 130☼

1,2,3-Trichlorobenzene <21 2950 2770 ug/Kg 94 69 - 131☼

1,2,3-Trichloropropane <34 2950 3070 ug/Kg 104 65 - 132☼

1,2,4-Trichlorobenzene <22 2950 2670 ug/Kg 91 73 - 130☼

1,2,4-Trimethylbenzene <12 2950 2590 ug/Kg 88 75 - 121☼

1,2-Dibromo-3-Chloropropane <51 2950 3000 ug/Kg 102 62 - 130☼

1,2-Dibromoethane <19 * 2950 3360 ug/Kg 114 78 - 122☼

1,2-Dichlorobenzene <12 2950 2930 ug/Kg 99 75 - 120☼

1,2-Dichloroethane <17 2950 3320 ug/Kg 112 69 - 130☼

1,2-Dichloropropane <12 * 2950 2960 ug/Kg 100 75 - 120☼

1,3,5-Trimethylbenzene <12 2950 2580 ug/Kg 88 75 - 121☼


1,3-Dichloropropane <7.9 2950 3210 ug/Kg 109 77 - 124☼


2,2-Dichloropropane <19 2950 2490 ug/Kg 84 65 - 132☼

2-Chlorotoluene <12 2950 2690 ug/Kg 91 75 - 120☼

4-Chlorotoluene <12 2950 2690 ug/Kg 91 75 - 120☼

Benzene <4.4 2950 2610 ug/Kg 88 75 - 120☼

Bromobenzene <25 2950 2950 ug/Kg 100 75 - 120☼

Bromochloromethane <22 * 2950 3270 ug/Kg 111 76 - 120☼

Bromodichloromethane <20 * 2950 3290 ug/Kg 111 77 - 121☼

Bromoform <26 2950 3360 ug/Kg 114 68 - 126☼

Bromomethane <40 2950 3060 ug/Kg 104 45 - 169☼

Carbon tetrachloride <15 * 2950 2600 ug/Kg 88 70 - 130☼

Chlorobenzene <8.4 2950 2850 ug/Kg 97 75 - 120☼

Chloroethane <26 2950 3470 ug/Kg 118 58 - 147☼

Chloroform <12 * 2950 3010 ug/Kg 102 76 - 120☼

Chloromethane <27 2950 2150 ug/Kg 73 63 - 133☼

cis-1,2-Dichloroethene <7.3 * 2950 2770 ug/Kg 94 75 - 120☼

cis-1,3-Dichloropropene <11 2950 3030 ug/Kg 103 78 - 130☼

Dibromochloromethane <20 2950 3310 ug/Kg 112 71 - 126☼

Dibromomethane <28 * 2950 3270 ug/Kg 111 75 - 120☼

Dichlorodifluoromethane <30 2950 2390 ug/Kg 81 41 - 146☼

Ethylbenzene <7.4 * 2950 2840 ug/Kg 96 75 - 120☼

Hexachlorobutadiene <20 2950 2500 ug/Kg 85 71 - 131☼

Isopropylbenzene <15 2950 2560 ug/Kg 87 75 - 121☼

Methyl tert-butyl ether <25 2950 3050 ug/Kg 103 75 - 130☼

Methylene Chloride <40 2950 2950 ug/Kg 100 73 - 130☼

Naphthalene <29 2950 2930 ug/Kg 99 69 - 135☼

n-Butylbenzene <7.6 2950 2410 ug/Kg 82 75 - 121☼

N-Propylbenzene <10 2950 2560 ug/Kg 87 75 - 120☼

p-Isopropyltoluene <11 2950 2700 ug/Kg 91 75 - 121☼

sec-Butylbenzene <9.1 2950 2470 ug/Kg 84 75 - 120☼

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Styrene <5.8 * 2950 2920 ug/Kg 99 75 - 120☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

tert-Butylbenzene <8.0 2950 2580 ug/Kg 88 75 - 123☼

Tetrachloroethene <9.9 * 2950 2580 ug/Kg 87 75 - 120☼

Toluene <6.8 * 2950 2760 ug/Kg 94 75 - 120☼

trans-1,2-Dichloroethene <15 2950 2500 ug/Kg 85 77 - 120☼

trans-1,3-Dichloropropene <12 2950 2990 ug/Kg 101 74 - 130☼

Trichloroethene <11 * 2950 2780 ug/Kg 94 75 - 120☼

Trichlorofluoromethane <24 2950 2580 ug/Kg 87 71 - 130☼

Vinyl chloride <6.1 2950 2190 ug/Kg 74 72 - 123☼

Xylenes, Total <4.0 5900 5530 ug/Kg 94 75 - 120☼


Surrogate

110

MS MS





Client Sample ID: SB1 (2-4)Lab Sample ID: 500-94669-1 MSD



1,1,1,2-Tetrachloroethane <20 * 2950 3020 ug/Kg 102 75 - 122 6 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,1,1-Trichloroethane <12 * 2950 2770 ug/Kg 94 72 - 130 3 30☼

1,1,2,2-Tetrachloroethane <14 2950 2740 ug/Kg 93 72 - 130 14 30☼

1,1,2-Trichloroethane <16 2950 2880 ug/Kg 98 75 - 120 12 30☼

1,1-Dichloroethane <11 * 2950 2680 ug/Kg 91 75 - 120 0 30☼

1,1-Dichloroethene <18 2950 2390 ug/Kg 81 69 - 120 6 30☼

1,1-Dichloropropene <20 2950 2620 ug/Kg 89 75 - 130 5 30☼

1,2,3-Trichlorobenzene <21 2950 2730 ug/Kg 93 69 - 131 1 30☼

1,2,3-Trichloropropane <34 2950 2700 ug/Kg 91 65 - 132 13 30☼

1,2,4-Trichlorobenzene <22 2950 2680 ug/Kg 91 73 - 130 0 30☼

1,2,4-Trimethylbenzene <12 2950 2680 ug/Kg 91 75 - 121 4 30☼

1,2-Dibromo-3-Chloropropane <51 2950 2680 ug/Kg 91 62 - 130 11 30☼

1,2-Dibromoethane <19 * 2950 2970 ug/Kg 101 78 - 122 12 30☼

1,2-Dichlorobenzene <12 2950 2840 ug/Kg 96 75 - 120 3 30☼

1,2-Dichloroethane <17 2950 2900 ug/Kg 98 69 - 130 13 30☼

1,2-Dichloropropane <12 * 2950 2700 ug/Kg 91 75 - 120 9 30☼

1,3,5-Trimethylbenzene <12 2950 2680 ug/Kg 91 75 - 121 4 30☼


1,3-Dichloropropane <7.9 2950 2880 ug/Kg 98 77 - 124 11 30☼


2,2-Dichloropropane <19 2950 2530 ug/Kg 86 65 - 132 2 30☼

2-Chlorotoluene <12 2950 2730 ug/Kg 93 75 - 120 2 30☼

4-Chlorotoluene <12 2950 2730 ug/Kg 92 75 - 120 1 30☼

Benzene <4.4 2950 2610 ug/Kg 88 75 - 120 0 30☼

Bromobenzene <25 2950 2910 ug/Kg 99 75 - 120 2 30☼

Bromochloromethane <22 * 2950 2880 ug/Kg 98 76 - 120 13 30☼

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Bromodichloromethane <20 * 2950 2890 ug/Kg 98 77 - 121 13 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Bromoform <26 2950 3000 ug/Kg 102 68 - 126 11 30☼

Bromomethane <40 2950 3210 ug/Kg 109 45 - 169 5 30☼

Carbon tetrachloride <15 * 2950 2760 ug/Kg 93 70 - 130 6 30☼

Chlorobenzene <8.4 2950 2830 ug/Kg 96 75 - 120 1 30☼

Chloroethane <26 2950 3080 ug/Kg 104 58 - 147 12 30☼

Chloroform <12 * 2950 2850 ug/Kg 97 76 - 120 6 30☼

Chloromethane <27 2950 2460 ug/Kg 83 63 - 133 13 30☼

cis-1,2-Dichloroethene <7.3 * 2950 2710 ug/Kg 92 75 - 120 2 30☼

cis-1,3-Dichloropropene <11 2950 2740 ug/Kg 93 78 - 130 10 30☼

Dibromochloromethane <20 2950 2970 ug/Kg 101 71 - 126 11 30☼

Dibromomethane <28 * 2950 2780 ug/Kg 94 75 - 120 16 30☼

Dichlorodifluoromethane <30 2950 2590 ug/Kg 88 41 - 146 8 30☼

Ethylbenzene <7.4 * 2950 2890 ug/Kg 98 75 - 120 2 30☼

Hexachlorobutadiene <20 2950 2700 ug/Kg 91 71 - 131 8 30☼

Isopropylbenzene <15 2950 2720 ug/Kg 92 75 - 121 6 30☼

Methyl tert-butyl ether <25 2950 2560 ug/Kg 87 75 - 130 17 30☼

Methylene Chloride <40 2950 2730 ug/Kg 92 73 - 130 8 30☼

Naphthalene <29 2950 2770 ug/Kg 94 69 - 135 6 30☼

n-Butylbenzene <7.6 2950 2620 ug/Kg 89 75 - 121 9 30☼

N-Propylbenzene <10 2950 2700 ug/Kg 91 75 - 120 5 30☼

p-Isopropyltoluene <11 2950 2810 ug/Kg 95 75 - 121 4 30☼

sec-Butylbenzene <9.1 2950 2660 ug/Kg 90 75 - 120 7 30☼

Styrene <5.8 * 2950 2850 ug/Kg 97 75 - 120 2 30☼

tert-Butylbenzene <8.0 2950 2770 ug/Kg 94 75 - 123 7 30☼

Tetrachloroethene <9.9 * 2950 2760 ug/Kg 94 75 - 120 7 30☼

Toluene <6.8 * 2950 2690 ug/Kg 91 75 - 120 3 30☼

trans-1,2-Dichloroethene <15 2950 2600 ug/Kg 88 77 - 120 4 30☼

trans-1,3-Dichloropropene <12 2950 2730 ug/Kg 93 74 - 130 9 30☼

Trichloroethene <11 * 2950 2820 ug/Kg 95 75 - 120 1 30☼

Trichlorofluoromethane <24 2950 2740 ug/Kg 93 71 - 130 6 30☼

Vinyl chloride <6.1 2950 2460 ug/Kg 83 72 - 123 12 30☼

Xylenes, Total <4.0 5900 5630 ug/Kg 95 75 - 120 2 30☼


Surrogate

97

MSD MSD








RL MDL

1,1,1,2-Tetrachloroethane <0.35 2.0 0.35 ug/Kg 04/17/15 16:26 1

MB MB


<0.20 0.201.0 ug/Kg 04/17/15 16:26 11,1,1-Trichloroethane

<0.23 0.231.0 ug/Kg 04/17/15 16:26 11,1,2,2-Tetrachloroethane

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1,1,2-Trichloroethane <0.28 1.0 0.28 ug/Kg 04/17/15 16:26 1

MB MB


<0.19 0.191.0 ug/Kg 04/17/15 16:26 11,1-Dichloroethane

<0.31 0.311.0 ug/Kg 04/17/15 16:26 11,1-Dichloroethene

<0.34 0.341.0 ug/Kg 04/17/15 16:26 11,1-Dichloropropene

<0.35 0.352.0 ug/Kg 04/17/15 16:26 11,2,3-Trichlorobenzene

<0.57 0.572.0 ug/Kg 04/17/15 16:26 11,2,3-Trichloropropane


<0.21 0.212.0 ug/Kg 04/17/15 16:26 11,2,4-Trimethylbenzene

<0.87 0.872.0 ug/Kg 04/17/15 16:26 11,2-Dibromo-3-Chloropropane

<0.31 0.312.0 ug/Kg 04/17/15 16:26 11,2-Dibromoethane

<0.21 0.212.0 ug/Kg 04/17/15 16:26 11,2-Dichlorobenzene


<0.20 0.201.0 ug/Kg 04/17/15 16:26 11,2-Dichloropropane






<0.21 0.211.0 ug/Kg 04/17/15 16:26 12-Chlorotoluene


<0.074 0.0740.25 ug/Kg 04/17/15 16:26 1Benzene

<0.43 0.432.0 ug/Kg 04/17/15 16:26 1Bromobenzene

<0.38 0.382.0 ug/Kg 04/17/15 16:26 1Bromochloromethane

<0.34 0.342.0 ug/Kg 04/17/15 16:26 1Bromodichloromethane

<0.44 0.442.0 ug/Kg 04/17/15 16:26 1Bromoform

<0.68 0.682.0 ug/Kg 04/17/15 16:26 1Bromomethane

<0.26 0.261.0 ug/Kg 04/17/15 16:26 1Carbon tetrachloride

<0.14 0.141.0 ug/Kg 04/17/15 16:26 1Chlorobenzene

<0.44 0.442.0 ug/Kg 04/17/15 16:26 1Chloroethane

<0.21 0.211.0 ug/Kg 04/17/15 16:26 1Chloroform

<0.46 0.462.0 ug/Kg 04/17/15 16:26 1Chloromethane

<0.12 0.121.0 ug/Kg 04/17/15 16:26 1cis-1,2-Dichloroethene

<0.18 0.181.0 ug/Kg 04/17/15 16:26 1cis-1,3-Dichloropropene

<0.35 0.352.0 ug/Kg 04/17/15 16:26 1Dibromochloromethane

<0.48 0.482.0 ug/Kg 04/17/15 16:26 1Dibromomethane

<0.51 0.512.0 ug/Kg 04/17/15 16:26 1Dichlorodifluoromethane

<0.13 0.130.25 ug/Kg 04/17/15 16:26 1Ethylbenzene

<0.35 0.352.0 ug/Kg 04/17/15 16:26 1Hexachlorobutadiene

<0.15 0.152.0 ug/Kg 04/17/15 16:26 1Isopropyl ether

<0.25 0.252.0 ug/Kg 04/17/15 16:26 1Isopropylbenzene

<0.43 0.432.0 ug/Kg 04/17/15 16:26 1Methyl tert-butyl ether

<0.68 0.685.0 ug/Kg 04/17/15 16:26 1Methylene Chloride

<0.49 0.492.0 ug/Kg 04/17/15 16:26 1Naphthalene

<0.13 0.131.0 ug/Kg 04/17/15 16:26 1n-Butylbenzene

<0.18 0.182.0 ug/Kg 04/17/15 16:26 1N-Propylbenzene

<0.19 0.192.0 ug/Kg 04/17/15 16:26 1p-Isopropyltoluene

<0.15 0.151.0 ug/Kg 04/17/15 16:26 1sec-Butylbenzene

<0.099 0.0991.0 ug/Kg 04/17/15 16:26 1Styrene

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tert-Butylbenzene <0.14 1.0 0.14 ug/Kg 04/17/15 16:26 1

MB MB


<0.17 0.171.0 ug/Kg 04/17/15 16:26 1Tetrachloroethene

<0.12 0.120.25 ug/Kg 04/17/15 16:26 1Toluene

<0.25 0.251.0 ug/Kg 04/17/15 16:26 1trans-1,2-Dichloroethene

<0.21 0.211.0 ug/Kg 04/17/15 16:26 1trans-1,3-Dichloropropene

<0.19 0.190.50 ug/Kg 04/17/15 16:26 1Trichloroethene

<0.42 0.422.0 ug/Kg 04/17/15 16:26 1Trichlorofluoromethane

<0.10 0.100.25 ug/Kg 04/17/15 16:26 1Vinyl chloride

<0.068 0.0680.50 ug/Kg 04/17/15 16:26 1Xylenes, Total


MB MB




95 04/17/15 16:26 1Toluene-d8 (Surr) 75 - 120




1,1,1,2-Tetrachloroethane 50.0 52.6 ug/Kg 105 75 - 122

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1,1-Trichloroethane 50.0 48.8 ug/Kg 98 72 - 130



1,1-Dichloroethane 50.0 46.0 ug/Kg 92 75 - 120

1,1-Dichloroethene 50.0 44.2 ug/Kg 88 69 - 120

1,1-Dichloropropene 50.0 46.5 ug/Kg 93 75 - 130

1,2,3-Trichlorobenzene 50.0 49.9 ug/Kg 100 69 - 131

1,2,3-Trichloropropane 50.0 49.5 ug/Kg 99 65 - 132


1,2,4-Trimethylbenzene 50.0 46.0 ug/Kg 92 75 - 121

1,2-Dibromo-3-Chloropropane 50.0 51.1 ug/Kg 102 62 - 130

1,2-Dibromoethane 50.0 53.4 ug/Kg 107 78 - 122

1,2-Dichlorobenzene 50.0 49.8 ug/Kg 100 75 - 120


1,2-Dichloropropane 50.0 47.8 ug/Kg 96 75 - 120






2-Chlorotoluene 50.0 47.0 ug/Kg 94 75 - 120


Benzene 50.0 45.3 ug/Kg 91 75 - 120

Bromobenzene 50.0 51.7 ug/Kg 103 75 - 120

Bromochloromethane 50.0 53.2 ug/Kg 106 76 - 120

Bromodichloromethane 50.0 52.2 ug/Kg 104 77 - 121

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Bromoform 50.0 53.3 ug/Kg 107 68 - 126

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bromomethane 50.0 57.1 ug/Kg 114 45 - 169

Carbon tetrachloride 50.0 48.6 ug/Kg 97 70 - 130

Chlorobenzene 50.0 48.3 ug/Kg 97 75 - 120

Chloroethane 50.0 54.2 ug/Kg 108 58 - 147

Chloroform 50.0 50.2 ug/Kg 100 76 - 120

Chloromethane 50.0 37.5 ug/Kg 75 63 - 133

cis-1,2-Dichloroethene 50.0 47.7 ug/Kg 95 75 - 120

cis-1,3-Dichloropropene 50.0 49.1 ug/Kg 98 78 - 130

Dibromochloromethane 50.0 54.0 ug/Kg 108 71 - 126

Dibromomethane 50.0 49.8 ug/Kg 100 75 - 120

Dichlorodifluoromethane 50.0 40.8 ug/Kg 82 41 - 146

Ethylbenzene 50.0 49.7 ug/Kg 99 75 - 120

Hexachlorobutadiene 50.0 46.1 ug/Kg 92 71 - 131

Isopropylbenzene 50.0 46.8 ug/Kg 94 75 - 121

Methyl tert-butyl ether 50.0 48.8 ug/Kg 98 75 - 130

Methylene Chloride 50.0 54.8 ug/Kg 110 73 - 130

Naphthalene 50.0 50.9 ug/Kg 102 69 - 135

n-Butylbenzene 50.0 45.2 ug/Kg 90 75 - 121

N-Propylbenzene 50.0 46.1 ug/Kg 92 75 - 120

p-Isopropyltoluene 50.0 48.1 ug/Kg 96 75 - 121

sec-Butylbenzene 50.0 45.4 ug/Kg 91 75 - 120

Styrene 50.0 48.6 ug/Kg 97 75 - 120

tert-Butylbenzene 50.0 47.1 ug/Kg 94 75 - 123

Tetrachloroethene 50.0 47.1 ug/Kg 94 75 - 120

Toluene 50.0 46.7 ug/Kg 93 75 - 120

trans-1,2-Dichloroethene 50.0 45.5 ug/Kg 91 77 - 120

trans-1,3-Dichloropropene 50.0 48.3 ug/Kg 97 74 - 130

Trichloroethene 50.0 49.4 ug/Kg 99 75 - 120

Trichlorofluoromethane 50.0 45.6 ug/Kg 91 71 - 130

Vinyl chloride 50.0 40.6 ug/Kg 81 72 - 123

Xylenes, Total 100 95.7 ug/Kg 96 75 - 120


Surrogate

100

LCS LCS








RL MDL

1,1,1,2-Tetrachloroethane <0.35 2.0 0.35 ug/Kg 04/20/15 13:44 1

MB MB



<0.23 0.231.0 ug/Kg 04/20/15 13:44 11,1,2,2-Tetrachloroethane


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1,1-Dichloroethane <0.19 1.0 0.19 ug/Kg 04/20/15 13:44 1

MB MB


<0.31 0.311.0 ug/Kg 04/20/15 13:44 11,1-Dichloroethene

<0.34 0.341.0 ug/Kg 04/20/15 13:44 11,1-Dichloropropene


<0.57 0.572.0 ug/Kg 04/20/15 13:44 11,2,3-Trichloropropane



<0.87 0.872.0 ug/Kg 04/20/15 13:44 11,2-Dibromo-3-Chloropropane

<0.31 0.312.0 ug/Kg 04/20/15 13:44 11,2-Dibromoethane











<0.074 0.0740.25 ug/Kg 04/20/15 13:44 1Benzene

<0.43 0.432.0 ug/Kg 04/20/15 13:44 1Bromobenzene

<0.38 0.382.0 ug/Kg 04/20/15 13:44 1Bromochloromethane

<0.34 0.342.0 ug/Kg 04/20/15 13:44 1Bromodichloromethane

<0.44 0.442.0 ug/Kg 04/20/15 13:44 1Bromoform

<0.68 0.682.0 ug/Kg 04/20/15 13:44 1Bromomethane

<0.26 0.261.0 ug/Kg 04/20/15 13:44 1Carbon tetrachloride

<0.14 0.141.0 ug/Kg 04/20/15 13:44 1Chlorobenzene

<0.44 0.442.0 ug/Kg 04/20/15 13:44 1Chloroethane

<0.21 0.211.0 ug/Kg 04/20/15 13:44 1Chloroform

<0.46 0.462.0 ug/Kg 04/20/15 13:44 1Chloromethane

<0.12 0.121.0 ug/Kg 04/20/15 13:44 1cis-1,2-Dichloroethene

<0.18 0.181.0 ug/Kg 04/20/15 13:44 1cis-1,3-Dichloropropene

<0.35 0.352.0 ug/Kg 04/20/15 13:44 1Dibromochloromethane

<0.48 0.482.0 ug/Kg 04/20/15 13:44 1Dibromomethane

<0.51 0.512.0 ug/Kg 04/20/15 13:44 1Dichlorodifluoromethane

<0.13 0.130.25 ug/Kg 04/20/15 13:44 1Ethylbenzene

<0.35 0.352.0 ug/Kg 04/20/15 13:44 1Hexachlorobutadiene

<0.15 0.152.0 ug/Kg 04/20/15 13:44 1Isopropyl ether

<0.25 0.252.0 ug/Kg 04/20/15 13:44 1Isopropylbenzene

<0.43 0.432.0 ug/Kg 04/20/15 13:44 1Methyl tert-butyl ether

<0.68 0.685.0 ug/Kg 04/20/15 13:44 1Methylene Chloride

<0.49 0.492.0 ug/Kg 04/20/15 13:44 1Naphthalene

<0.13 0.131.0 ug/Kg 04/20/15 13:44 1n-Butylbenzene

<0.18 0.182.0 ug/Kg 04/20/15 13:44 1N-Propylbenzene

<0.19 0.192.0 ug/Kg 04/20/15 13:44 1p-Isopropyltoluene

<0.15 0.151.0 ug/Kg 04/20/15 13:44 1sec-Butylbenzene

<0.099 0.0991.0 ug/Kg 04/20/15 13:44 1Styrene

<0.14 0.141.0 ug/Kg 04/20/15 13:44 1tert-Butylbenzene

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Tetrachloroethene <0.17 1.0 0.17 ug/Kg 04/20/15 13:44 1

MB MB


<0.12 0.120.25 ug/Kg 04/20/15 13:44 1Toluene

<0.25 0.251.0 ug/Kg 04/20/15 13:44 1trans-1,2-Dichloroethene

<0.21 0.211.0 ug/Kg 04/20/15 13:44 1trans-1,3-Dichloropropene

<0.19 0.190.50 ug/Kg 04/20/15 13:44 1Trichloroethene

<0.42 0.422.0 ug/Kg 04/20/15 13:44 1Trichlorofluoromethane

<0.10 0.100.25 ug/Kg 04/20/15 13:44 1Vinyl chloride

<0.068 0.0680.50 ug/Kg 04/20/15 13:44 1Xylenes, Total


MB MB




94 04/20/15 13:44 1Toluene-d8 (Surr) 75 - 120





Analyte

LCS LCS


Spike

Added

%Rec.

Limits





1,1-Dichloroethene 50.0 42.5 ug/Kg 85 69 - 120

1,1-Dichloropropene 50.0 46.1 ug/Kg 92 75 - 130


1,2,3-Trichloropropane 50.0 46.4 ug/Kg 93 65 - 132



1,2-Dibromo-3-Chloropropane 50.0 45.0 ug/Kg 90 62 - 130

1,2-Dibromoethane 50.0 50.7 ug/Kg 101 78 - 122











Benzene 50.0 44.1 ug/Kg 88 75 - 120

Bromobenzene 50.0 49.0 ug/Kg 98 75 - 120

Bromochloromethane 50.0 51.4 ug/Kg 103 76 - 120

Bromodichloromethane 50.0 50.4 ug/Kg 101 77 - 121

Bromoform 50.0 49.7 ug/Kg 99 68 - 126

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Bromomethane 50.0 62.6 ug/Kg 125 45 - 169

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Carbon tetrachloride 50.0 48.1 ug/Kg 96 70 - 130

Chlorobenzene 50.0 47.7 ug/Kg 95 75 - 120

Chloroethane 50.0 58.3 ug/Kg 117 58 - 147

Chloroform 50.0 48.9 ug/Kg 98 76 - 120

Chloromethane 50.0 45.1 ug/Kg 90 63 - 133

cis-1,2-Dichloroethene 50.0 46.9 ug/Kg 94 75 - 120

cis-1,3-Dichloropropene 50.0 48.3 ug/Kg 97 78 - 130

Dibromochloromethane 50.0 51.2 ug/Kg 102 71 - 126

Dibromomethane 50.0 47.8 ug/Kg 96 75 - 120

Dichlorodifluoromethane 50.0 50.7 ug/Kg 101 41 - 146

Ethylbenzene 50.0 48.5 ug/Kg 97 75 - 120

Hexachlorobutadiene 50.0 48.0 ug/Kg 96 71 - 131

Isopropylbenzene 50.0 46.0 ug/Kg 92 75 - 121

Methyl tert-butyl ether 50.0 45.6 ug/Kg 91 75 - 130

Methylene Chloride 50.0 47.5 ug/Kg 95 73 - 130

Naphthalene 50.0 46.3 ug/Kg 93 69 - 135

n-Butylbenzene 50.0 45.8 ug/Kg 92 75 - 121

N-Propylbenzene 50.0 45.9 ug/Kg 92 75 - 120

p-Isopropyltoluene 50.0 47.5 ug/Kg 95 75 - 121

sec-Butylbenzene 50.0 45.1 ug/Kg 90 75 - 120

Styrene 50.0 47.4 ug/Kg 95 75 - 120

tert-Butylbenzene 50.0 47.7 ug/Kg 95 75 - 123

Tetrachloroethene 50.0 48.0 ug/Kg 96 75 - 120

Toluene 50.0 46.1 ug/Kg 92 75 - 120

trans-1,2-Dichloroethene 50.0 43.9 ug/Kg 88 77 - 120

trans-1,3-Dichloropropene 50.0 47.3 ug/Kg 95 74 - 130

Trichloroethene 50.0 48.9 ug/Kg 98 75 - 120

Trichlorofluoromethane 50.0 48.3 ug/Kg 97 71 - 130

Vinyl chloride 50.0 46.3 ug/Kg 93 72 - 123

Xylenes, Total 100 93.7 ug/Kg 94 75 - 120


Surrogate

96

LCS LCS





Method: 8270D - Semivolatile Organic Compounds (GC/MS)




RL MDL

1,2,4-Trichlorobenzene <36 170 36 ug/Kg 04/20/15 16:14 04/21/15 12:02 1

MB MB




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1,4-Dichlorobenzene <43 170 43 ug/Kg 04/20/15 16:14 04/21/15 12:02 1

MB MB


<8.1 8.133 ug/Kg 04/20/15 16:14 04/21/15 12:02 11-Methylnaphthalene

<39 39170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,2'-oxybis[1-chloropropane]

<76 76330 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4,5-Trichlorophenol

<110 110330 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4,6-Trichlorophenol

<79 79330 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4-Dichlorophenol

<130 130330 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4-Dimethylphenol

<590 590670 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4-Dinitrophenol

<53 53170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,4-Dinitrotoluene

<65 65170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12,6-Dinitrotoluene

<37 37170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Chloronaphthalene

<57 57170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Chlorophenol

<6.1 6.133 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Methylnaphthalene

<53 53170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Methylphenol

<45 45170 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Nitroaniline

<79 79330 ug/Kg 04/20/15 16:14 04/21/15 12:02 12-Nitrophenol

<55 55170 ug/Kg 04/20/15 16:14 04/21/15 12:02 13 & 4 Methylphenol

<47 47170 ug/Kg 04/20/15 16:14 04/21/15 12:02 13,3'-Dichlorobenzidine


<270 270330 ug/Kg 04/20/15 16:14 04/21/15 12:02 14,6-Dinitro-2-methylphenol

<44 44170 ug/Kg 04/20/15 16:14 04/21/15 12:02 14-Bromophenyl phenyl ether

<110 110330 ug/Kg 04/20/15 16:14 04/21/15 12:02 14-Chloro-3-methylphenol

<160 160670 ug/Kg 04/20/15 16:14 04/21/15 12:02 14-Chloroaniline

<39 39170 ug/Kg 04/20/15 16:14 04/21/15 12:02 14-Chlorophenyl phenyl ether


<320 320670 ug/Kg 04/20/15 16:14 04/21/15 12:02 14-Nitrophenol

<6.0 6.033 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Acenaphthene

<4.4 4.433 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Acenaphthylene

<5.6 5.633 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Anthracene

<4.5 4.533 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzo[a]anthracene

<6.4 6.433 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzo[a]pyrene

<7.2 7.233 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzo[b]fluoranthene

<11 1133 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzo[g,h,i]perylene

<9.8 9.833 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzo[k]fluoranthene

<370 3701700 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzoic acid

<100 100330 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Benzyl alcohol

<34 34170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Bis(2-chloroethoxy)methane

<50 50170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Bis(2-chloroethyl)ether

<61 61170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Bis(2-ethylhexyl) phthalate

<63 63170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Butyl benzyl phthalate

<86 86170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Carbazole

<9.1 9.133 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Chrysene

<6.4 6.433 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Dibenz(a,h)anthracene

<39 39170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Dibenzofuran

<56 56170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Diethyl phthalate

<43 43170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Dimethyl phthalate

<51 51170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Di-n-butyl phthalate

<54 54170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Di-n-octyl phthalate

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RL MDL

Fluoranthene <6.2 33 6.2 ug/Kg 04/20/15 16:14 04/21/15 12:02 1

MB MB


<4.7 4.733 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Fluorene

<7.7 7.767 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Hexachlorobenzene

<52 52170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Hexachlorobutadiene

<190 190670 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Hexachlorocyclopentadiene

<51 51170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Hexachloroethane

<8.6 8.633 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Indeno[1,2,3-cd]pyrene

<37 37170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Isophorone

<5.1 5.133 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Naphthalene

<8.3 8.333 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Nitrobenzene

<41 41170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1N-Nitrosodi-n-propylamine

<39 39170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1N-Nitrosodiphenylamine

<530 530670 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Pentachlorophenol

<4.6 4.633 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Phenanthrene

<74 74170 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Phenol

<6.6 6.633 ug/Kg 04/20/15 16:14 04/21/15 12:02 1Pyrene

2,4,6-Tribromophenol (Surr) 60 35 - 137 04/21/15 12:02 1

MB MB

Surrogate

04/20/15 16:14


81 04/20/15 16:14 04/21/15 12:02 12-Fluorobiphenyl 25 - 119

74 04/20/15 16:14 04/21/15 12:02 12-Fluorophenol (Surr) 25 - 110

52 04/20/15 16:14 04/21/15 12:02 1Nitrobenzene-d5 (Surr) 25 - 115

56 04/20/15 16:14 04/21/15 12:02 1Phenol-d5 (Surr) 31 - 110

100 04/20/15 16:14 04/21/15 12:02 1Terphenyl-d14 (Surr) 36 - 134





Analyte

LCS LCS


Spike

Added

%Rec.

Limits




1-Methylnaphthalene 1330 1050 ug/Kg 79 50 - 110

2,2'-oxybis[1-chloropropane] 1330 1130 ug/Kg 84 32 - 117

2,4,5-Trichlorophenol 1330 1170 ug/Kg 88 49 - 123

2,4,6-Trichlorophenol 1330 1150 ug/Kg 86 43 - 127

2,4-Dichlorophenol 1330 1040 ug/Kg 78 54 - 118

2,4-Dimethylphenol 1330 1000 ug/Kg 75 50 - 125

2,4-Dinitrophenol 2670 653 J ug/Kg 24 10 - 110

2,4-Dinitrotoluene 1330 1260 ug/Kg 94 55 - 123

2,6-Dinitrotoluene 1330 1180 ug/Kg 89 54 - 121

2-Chloronaphthalene 1330 1110 ug/Kg 83 51 - 113

2-Chlorophenol 1330 1000 ug/Kg 75 50 - 118

2-Methylnaphthalene 1330 1080 ug/Kg 81 49 - 110

2-Methylphenol 1330 1070 ug/Kg 80 48 - 120

2-Nitroaniline 1330 1100 ug/Kg 83 51 - 124

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2-Nitrophenol 1330 1000 ug/Kg 75 42 - 129

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

3 & 4 Methylphenol 1330 1020 ug/Kg 76 48 - 122

3,3'-Dichlorobenzidine 1330 932 ug/Kg 70 35 - 113


4,6-Dinitro-2-methylphenol 2670 962 ug/Kg 36 10 - 110

4-Bromophenyl phenyl ether 1330 1090 ug/Kg 82 55 - 122

4-Chloro-3-methylphenol 1330 1020 ug/Kg 76 56 - 117

4-Chloroaniline 1330 845 ug/Kg 63 23 - 114

4-Chlorophenyl phenyl ether 1330 1180 ug/Kg 89 54 - 120


4-Nitrophenol 2670 2500 ug/Kg 94 25 - 143

Acenaphthene 1330 1120 ug/Kg 84 47 - 110

Acenaphthylene 1330 1110 ug/Kg 84 51 - 113

Anthracene 1330 1090 ug/Kg 82 53 - 121

Benzo[a]anthracene 1330 1100 ug/Kg 83 52 - 113

Benzo[a]pyrene 1330 1080 ug/Kg 81 52 - 110

Benzo[b]fluoranthene 1330 1030 ug/Kg 77 49 - 118

Benzo[g,h,i]perylene 1330 1130 ug/Kg 85 53 - 115

Benzo[k]fluoranthene 1330 1140 ug/Kg 86 46 - 115

Benzoic acid 1330 <370 * ug/Kg 0 10 - 100

Benzyl alcohol 1330 1050 ug/Kg 79 40 - 110

Bis(2-chloroethoxy)methane 1330 896 ug/Kg 67 50 - 110

Bis(2-chloroethyl)ether 1330 923 ug/Kg 69 41 - 112

Bis(2-ethylhexyl) phthalate 1330 1080 ug/Kg 81 52 - 129

Butyl benzyl phthalate 1330 1060 ug/Kg 79 54 - 126

Carbazole 1330 1050 ug/Kg 79 56 - 123

Chrysene 1330 1120 ug/Kg 84 51 - 112

Dibenz(a,h)anthracene 1330 1140 ug/Kg 85 48 - 113

Dibenzofuran 1330 1170 ug/Kg 88 52 - 115

Diethyl phthalate 1330 1180 ug/Kg 89 47 - 129

Dimethyl phthalate 1330 1170 ug/Kg 88 55 - 116

Di-n-butyl phthalate 1330 1040 ug/Kg 78 53 - 121

Di-n-octyl phthalate 1330 1060 ug/Kg 79 44 - 137

Fluoranthene 1330 1090 ug/Kg 82 53 - 122

Fluorene 1330 1170 ug/Kg 88 51 - 119

Hexachlorobenzene 1330 1100 ug/Kg 82 55 - 121

Hexachlorobutadiene 1330 1030 ug/Kg 77 45 - 119

Hexachlorocyclopentadiene 1330 <190 * ug/Kg 2 10 - 134

Hexachloroethane 1330 920 ug/Kg 69 42 - 111

Indeno[1,2,3-cd]pyrene 1330 1140 ug/Kg 85 49 - 113

Isophorone 1330 908 ug/Kg 68 46 - 110

Naphthalene 1330 994 ug/Kg 75 49 - 110

Nitrobenzene 1330 933 ug/Kg 70 49 - 110

N-Nitrosodi-n-propylamine 1330 951 ug/Kg 71 44 - 112

N-Nitrosodiphenylamine 2670 2150 ug/Kg 81 48 - 113

Pentachlorophenol 2670 1780 ug/Kg 67 10 - 152

Phenanthrene 1330 1050 ug/Kg 79 54 - 120

Phenol 1330 986 ug/Kg 74 50 - 117

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Pyrene 1330 1090 ug/Kg 82 54 - 119

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

88

LCS LCS










1,2,4-Trichlorobenzene <39 F1 1400 630 F1 ug/Kg 45 48 - 113☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,2-Dichlorobenzene <43 F1 1400 510 F1 ug/Kg 36 48 - 110☼



1-Methylnaphthalene <8.8 F1 1400 718 ug/Kg 51 50 - 110☼

2,2'-oxybis[1-chloropropane] <42 1400 675 ug/Kg 48 32 - 117☼

2,4,5-Trichlorophenol <82 1400 780 ug/Kg 56 49 - 123☼

2,4,6-Trichlorophenol <120 1400 843 ug/Kg 60 43 - 127☼

2,4-Dichlorophenol <85 F1 1400 738 F1 ug/Kg 53 54 - 118☼

2,4-Dimethylphenol <140 F1 1400 692 F1 ug/Kg 49 50 - 125☼

2,4-Dinitrophenol <630 F1 2810 <620 F1 ug/Kg 0 10 - 110☼

2,4-Dinitrotoluene <57 F1 1400 622 F1 ug/Kg 44 55 - 123☼

2,6-Dinitrotoluene <71 F1 1400 715 F1 ug/Kg 51 54 - 121☼

2-Chloronaphthalene <40 F1 1400 746 ug/Kg 53 51 - 113☼

2-Chlorophenol <61 F1 1400 584 F1 ug/Kg 42 50 - 118☼

2-Methylnaphthalene <6.6 1400 728 ug/Kg 52 49 - 110☼

2-Methylphenol <58 1400 697 ug/Kg 50 48 - 120☼

2-Nitroaniline <48 F1 1400 740 ug/Kg 53 51 - 124☼

2-Nitrophenol <85 F1 1400 444 F1 ug/Kg 32 42 - 129☼

3 & 4 Methylphenol <60 F1 1400 669 ug/Kg 48 48 - 122☼

3,3'-Dichlorobenzidine <50 F1 1400 463 F1 ug/Kg 33 35 - 113☼

3-Nitroaniline <110 1400 691 ug/Kg 49 43 - 113☼

4,6-Dinitro-2-methylphenol <290 F1 2810 <280 F1 ug/Kg 0 10 - 110☼

4-Bromophenyl phenyl ether <47 1400 1140 ug/Kg 81 55 - 122☼

4-Chloro-3-methylphenol <120 F1 1400 778 F1 ug/Kg 55 56 - 117☼

4-Chloroaniline <170 1400 399 J ug/Kg 28 23 - 114☼

4-Chlorophenyl phenyl ether <42 1400 908 ug/Kg 65 54 - 120☼

4-Nitroaniline <150 1400 462 ug/Kg 33 31 - 135☼

4-Nitrophenol <340 2810 1730 ug/Kg 62 25 - 143☼

Acenaphthene <6.5 1400 773 ug/Kg 55 47 - 110☼

Acenaphthylene <4.7 F1 1400 737 ug/Kg 52 51 - 113☼

Anthracene <6.0 F1 1400 804 ug/Kg 57 53 - 121☼

Benzo[a]anthracene 13 J 1400 861 ug/Kg 60 52 - 113☼

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Benzo[a]pyrene 13 J 1400 826 ug/Kg 58 52 - 110☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Benzo[b]fluoranthene 17 J 1400 780 ug/Kg 54 49 - 118☼

Benzo[g,h,i]perylene 14 J 1400 954 ug/Kg 67 53 - 115☼

Benzo[k]fluoranthene <11 1400 847 ug/Kg 60 46 - 115☼

Benzoic acid <400 * F1 1400 630 J ug/Kg 45 10 - 100☼

Benzyl alcohol <110 F1 F2 1400 520 F1 ug/Kg 37 40 - 110☼

Bis(2-chloroethoxy)methane <37 F1 1400 510 F1 ug/Kg 36 50 - 110☼

Bis(2-chloroethyl)ether <54 F1 1400 578 ug/Kg 41 41 - 112☼

Bis(2-ethylhexyl) phthalate <66 F2 1400 1590 ug/Kg 113 52 - 129☼

Butyl benzyl phthalate <68 F1 F2 1400 1850 F1 ug/Kg 132 54 - 126☼

Carbazole <93 F1 1400 590 F1 ug/Kg 42 56 - 123☼

Chrysene 14 J 1400 925 ug/Kg 65 51 - 112☼

Dibenz(a,h)anthracene <7.0 1400 941 ug/Kg 67 48 - 113☼

Dibenzofuran <42 1400 798 ug/Kg 57 52 - 115☼

Diethyl phthalate <61 1400 862 ug/Kg 61 47 - 129☼

Dimethyl phthalate <47 1400 863 ug/Kg 61 55 - 116☼

Di-n-butyl phthalate <55 1400 871 ug/Kg 62 53 - 121☼

Di-n-octyl phthalate <59 F1 F2 1400 83.2 J F1 ug/Kg 6 44 - 137☼

Fluoranthene 21 J F1 1400 393 F1 ug/Kg 26 53 - 122☼

Fluorene <5.1 1400 792 ug/Kg 56 51 - 119☼

Hexachlorobenzene <8.3 1400 1030 ug/Kg 73 55 - 121☼

Hexachlorobutadiene <57 1400 627 ug/Kg 45 45 - 119☼

Hexachlorocyclopentadiene <210 F1 * 1400 <200 F1 ug/Kg 0 10 - 134☼

Hexachloroethane <55 F1 1400 <53 F1 ug/Kg 0 42 - 111☼

Indeno[1,2,3-cd]pyrene 9.7 J 1400 944 ug/Kg 67 49 - 113☼

Isophorone <40 F1 1400 530 F1 ug/Kg 38 46 - 110☼

Naphthalene <5.5 F1 1400 583 F1 ug/Kg 41 49 - 110☼

Nitrobenzene <9.0 F1 1400 467 F1 ug/Kg 33 49 - 110☼

N-Nitrosodi-n-propylamine <44 F1 1400 498 F1 ug/Kg 35 44 - 112☼

N-Nitrosodiphenylamine <42 2810 2140 ug/Kg 76 48 - 113☼

Pentachlorophenol <580 2810 864 ug/Kg 31 10 - 152☼

Phenanthrene 8.6 J F1 1400 822 ug/Kg 58 54 - 120☼

Phenol <80 F1 1400 608 F1 ug/Kg 43 50 - 117☼

Pyrene 20 J F1 F2 1400 2800 E F1 ug/Kg 198 54 - 119☼


Surrogate

68

MS MS






252 XTerphenyl-d14 (Surr) 36 - 134

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1,2,4-Trichlorobenzene <39 F1 1420 660 F1 ug/Kg 47 48 - 113 5 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,2-Dichlorobenzene <43 F1 1420 533 F1 ug/Kg 38 48 - 110 4 30☼



1-Methylnaphthalene <8.8 F1 1420 698 F1 ug/Kg 49 50 - 110 3 30☼

2,2'-oxybis[1-chloropropane] <42 1420 678 ug/Kg 48 32 - 117 0 30☼

2,4,5-Trichlorophenol <82 1420 710 ug/Kg 50 49 - 123 9 30☼

2,4,6-Trichlorophenol <120 1420 743 ug/Kg 52 43 - 127 13 30☼

2,4-Dichlorophenol <85 F1 1420 690 F1 ug/Kg 49 54 - 118 7 30☼

2,4-Dimethylphenol <140 F1 1420 618 F1 ug/Kg 44 50 - 125 11 30☼

2,4-Dinitrophenol <630 F1 2830 <620 F1 ug/Kg 0 10 - 110 NC 30☼

2,4-Dinitrotoluene <57 F1 1420 585 F1 ug/Kg 41 55 - 123 6 30☼

2,6-Dinitrotoluene <71 F1 1420 624 F1 ug/Kg 44 54 - 121 14 30☼

2-Chloronaphthalene <40 F1 1420 699 F1 ug/Kg 49 51 - 113 7 30☼

2-Chlorophenol <61 F1 1420 591 F1 ug/Kg 42 50 - 118 1 30☼

2-Methylnaphthalene <6.6 1420 707 ug/Kg 50 49 - 110 3 30☼

2-Methylphenol <58 1420 730 ug/Kg 52 48 - 120 5 30☼

2-Nitroaniline <48 F1 1420 668 F1 ug/Kg 47 51 - 124 10 30☼

2-Nitrophenol <85 F1 1420 448 F1 ug/Kg 32 42 - 129 1 30☼

3 & 4 Methylphenol <60 F1 1420 587 F1 ug/Kg 41 48 - 122 13 30☼

3,3'-Dichlorobenzidine <50 F1 1420 511 ug/Kg 36 35 - 113 10 30☼

3-Nitroaniline <110 1420 612 ug/Kg 43 43 - 113 12 30☼

4,6-Dinitro-2-methylphenol <290 F1 2830 <280 F1 ug/Kg 0 10 - 110 NC 30☼

4-Bromophenyl phenyl ether <47 1420 923 ug/Kg 65 55 - 122 21 30☼

4-Chloro-3-methylphenol <120 F1 1420 675 F1 ug/Kg 48 56 - 117 14 30☼

4-Chloroaniline <170 1420 422 J ug/Kg 30 23 - 114 6 30☼

4-Chlorophenyl phenyl ether <42 1420 820 ug/Kg 58 54 - 120 10 30☼

4-Nitroaniline <150 1420 509 ug/Kg 36 31 - 135 10 30☼

4-Nitrophenol <340 2830 1740 ug/Kg 61 25 - 143 0 30☼

Acenaphthene <6.5 1420 702 ug/Kg 50 47 - 110 10 30☼

Acenaphthylene <4.7 F1 1420 684 F1 ug/Kg 48 51 - 113 7 30☼

Anthracene <6.0 F1 1420 707 F1 ug/Kg 50 53 - 121 13 30☼

Benzo[a]anthracene 13 J 1420 763 ug/Kg 53 52 - 113 12 30☼

Benzo[a]pyrene 13 J 1420 784 ug/Kg 54 52 - 110 5 30☼

Benzo[b]fluoranthene 17 J 1420 717 ug/Kg 49 49 - 118 8 30☼

Benzo[g,h,i]perylene 14 J 1420 833 ug/Kg 58 53 - 115 14 30☼

Benzo[k]fluoranthene <11 1420 887 ug/Kg 63 46 - 115 5 30☼

Benzoic acid <400 * F1 1420 <400 F1 ug/Kg 0 10 - 100 NC 30☼

Benzyl alcohol <110 F1 F2 1420 1210 F2 ug/Kg 86 40 - 110 80 30☼

Bis(2-chloroethoxy)methane <37 F1 1420 500 F1 ug/Kg 35 50 - 110 2 30☼

Bis(2-chloroethyl)ether <54 F1 1420 494 F1 ug/Kg 35 41 - 112 16 30☼

Bis(2-ethylhexyl) phthalate <66 F2 1420 1140 F2 ug/Kg 80 52 - 129 33 30☼

Butyl benzyl phthalate <68 F1 F2 1420 1350 F2 ug/Kg 95 54 - 126 32 30☼

Carbazole <93 F1 1420 581 F1 ug/Kg 41 56 - 123 2 30☼

Chrysene 14 J 1420 764 ug/Kg 53 51 - 112 19 30☼

Dibenz(a,h)anthracene <7.0 1420 836 ug/Kg 59 48 - 113 12 30☼

Dibenzofuran <42 1420 745 ug/Kg 53 52 - 115 7 30☼

Diethyl phthalate <61 1420 791 ug/Kg 56 47 - 129 9 30☼

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Dimethyl phthalate <47 1420 789 ug/Kg 56 55 - 116 9 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Di-n-butyl phthalate <55 1420 756 ug/Kg 53 53 - 121 14 30☼

Di-n-octyl phthalate <59 F1 F2 1420 148 J F1 F2 ug/Kg 10 44 - 137 56 30☼

Fluoranthene 21 J F1 1420 448 F1 ug/Kg 30 53 - 122 13 30☼

Fluorene <5.1 1420 722 ug/Kg 51 51 - 119 9 30☼

Hexachlorobenzene <8.3 1420 837 ug/Kg 59 55 - 121 21 30☼

Hexachlorobutadiene <57 1420 637 ug/Kg 45 45 - 119 1 30☼

Hexachlorocyclopentadiene <210 F1 * 1420 <200 F1 ug/Kg 0 10 - 134 NC 30☼

Hexachloroethane <55 F1 1420 <54 F1 ug/Kg 0 42 - 111 NC 30☼

Indeno[1,2,3-cd]pyrene 9.7 J 1420 805 ug/Kg 56 49 - 113 16 30☼

Isophorone <40 F1 1420 471 F1 ug/Kg 33 46 - 110 12 30☼

Naphthalene <5.5 F1 1420 585 F1 ug/Kg 41 49 - 110 0 30☼

Nitrobenzene <9.0 F1 1420 479 F1 ug/Kg 34 49 - 110 2 30☼

N-Nitrosodi-n-propylamine <44 F1 1420 499 F1 ug/Kg 35 44 - 112 0 30☼

N-Nitrosodiphenylamine <42 2830 1710 ug/Kg 60 48 - 113 23 30☼

Pentachlorophenol <580 2830 865 ug/Kg 31 10 - 152 0 30☼

Phenanthrene 8.6 J F1 1420 688 F1 ug/Kg 48 54 - 120 18 30☼

Phenol <80 F1 1420 586 F1 ug/Kg 41 50 - 117 4 30☼

Pyrene 20 J F1 F2 1420 1740 F1 F2 ug/Kg 121 54 - 119 47 30☼


Surrogate

54

MSD MSD






156 XTerphenyl-d14 (Surr) 36 - 134

Method: 6010B - Metals (ICP)




RL MDL

Arsenic <0.46 1.0 0.46 mg/Kg 04/17/15 08:50 04/19/15 02:41 1

MB MB


<0.18 0.181.0 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Barium

<0.058 0.0580.20 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Cadmium

<0.17 0.171.0 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Chromium

<0.25 0.250.50 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Lead

<0.50 0.501.0 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Selenium

<0.12 0.120.50 mg/Kg 04/17/15 08:50 04/19/15 02:41 1Silver

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Method: 6010B - Metals (ICP) (Continued)




Arsenic 10.0 10.0 mg/Kg 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 200 193 mg/Kg 96 80 - 120

Cadmium 5.00 4.85 mg/Kg 97 80 - 120

Chromium 20.0 19.1 mg/Kg 95 80 - 120

Lead 10.0 9.94 mg/Kg 99 80 - 120

Selenium 10.0 8.75 mg/Kg 87 80 - 120

Silver 5.00 4.81 mg/Kg 96 80 - 120




Arsenic 0.84 J 10.5 10.6 mg/Kg 94 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 8.6 209 199 mg/Kg 91 75 - 125☼

Cadmium <0.057 5.24 4.96 mg/Kg 95 75 - 125☼

Chromium 4.4 20.9 24.6 mg/Kg 97 75 - 125☼

Lead 3.4 10.5 14.7 mg/Kg 107 75 - 125☼

Selenium <0.49 10.5 9.17 mg/Kg 88 75 - 125☼

Silver <0.12 5.24 4.79 mg/Kg 91 75 - 125☼




Arsenic 0.84 J 10.3 10.2 mg/Kg 91 75 - 125 5 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 8.6 205 198 mg/Kg 92 75 - 125 1 20☼

Cadmium <0.057 5.13 4.88 mg/Kg 95 75 - 125 2 20☼

Chromium 4.4 20.5 24.1 mg/Kg 96 75 - 125 2 20☼

Lead 3.4 10.3 15.9 mg/Kg 121 75 - 125 8 20☼

Selenium <0.49 10.3 9.00 mg/Kg 88 75 - 125 2 20☼

Silver <0.12 5.13 4.78 mg/Kg 93 75 - 125 0 20☼

Client Sample ID: SB1 (2-4)Lab Sample ID: 500-94669-1 DU



Arsenic 0.84 J 0.526 J F5 mg/Kg 45 20☼

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Barium 8.6 8.42 mg/Kg 3 20☼

Cadmium <0.057 <0.058 mg/Kg NC 20☼

Chromium 4.4 7.87 F3 mg/Kg 56 20☼

Lead 3.4 3.46 mg/Kg 1 20☼

Selenium <0.49 <0.50 mg/Kg NC 20☼

Silver <0.12 <0.12 mg/Kg NC 20☼

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Method: 7471A - Mercury (CVAA)




RL MDL

Mercury <0.0058 0.017 0.0058 mg/Kg 04/17/15 12:00 04/20/15 09:22 1

MB MB





Mercury 0.167 0.173 mg/Kg 103 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Client Sample ID: SB1 (2-4) Lab Sample ID: 500-94669-1Matrix: SolidDate Collected: 04/09/15 10:12


Prep 5035 04/09/15 10:12 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260B 50 284574 04/20/15 16:01 EMA TAL CHITotal/NA

Prep 3541 284633 04/20/15 16:14 DEA TAL CHITotal/NA


Prep 3050B 284279 04/17/15 08:50 JLC TAL CHITotal/NA

Analysis 6010B 1 284462 04/19/15 02:49 PJ1 TAL CHITotal/NA



Analysis Moisture 1 283935 04/15/15 13:32 LWN TAL CHITotal/NA



Prep 5035 04/09/15 10:30 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA





Client Sample ID: SB1 FD Lab Sample ID: 500-94669-3Matrix: SolidDate Collected: 04/09/15 10:15


Prep 5035 04/09/15 10:15 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 04/09/15 11:51 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


TestAmerica Chicago

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Prep 3541 04/20/15 16:14 DEA284633 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Prep 5035 04/09/15 11:54 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA







Prep 5035 04/09/15 09:36 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 04/09/15 09:38 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




TestAmerica Chicago

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Analysis Moisture 04/15/15 13:32 LWN1 283935 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035 04/09/15 12:46 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 04/09/15 12:48 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA







Prep 5035 04/09/15 11:26 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









TestAmerica Chicago

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Prep 5035 04/09/15 13:26 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Client Sample ID: Trip Blank Lab Sample ID: 500-94669-12Matrix: SolidDate Collected: 04/09/15 00:00


Prep 5035 04/09/15 00:00 WRE284058 TAL CHI

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




TestAmerica Chicago

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Certification SummaryClient: Stantec Consulting Corporation/Bonestroo TestAmerica Job ID: 500-94669-1


Laboratory: TestAmerica ChicagoUnless otherwise noted, all analytes for this laboratory were covered under each certification below.

Authority Program EPA Region Certification ID Expiration Date

Wisconsin 9995800105State Program 08-31-15

Analysis Method Prep Method Matrix Analyte

The following analytes are included in this report, but certification is not offered by the governing authority:

Moisture Solid Percent Moisture

Moisture Solid Percent Solids

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Login Sample Receipt Checklist

Client: Stantec Consulting Corporation/Bonestroo Job Number: 500-94669-1

Login Number: 94669

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice. 4.2,3.1

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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phase ii environmental site assessment · 2020. 10. 18. · phase ii environmental site assessment...

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