' T McKesson Corporation One Post Street San Francisco, CA 94104 608.848.4134 Tel

Jean Mescher Director, Environmental Services

US I:PA RI-CORDSCKNTFR RKGION S

494726

MCKESSON Empowering Healthcare

Via Federal Express

December 8, 2005

Mr. Michael A. Gifford (RPM/OSC) Remedial Response Branch, Region 5 U.S. Environmental Protection Agency 77 W. Jackson Boulevard, SE-4J Chicago, IL 60604

Subject: Monthly Progress Report - November 2005 XXKem Site, Toledo, Ohio

Dear Mr. Gifford:

Pursuant to Section VI.2.6 of the Administrative Order by Consent in this matter, enclosed is Safety-Kleen Envirosystems Company's monthly progress report.

If you have any questions regarding this monthly progress report, please do not hesitate to contact me at (608) 848-4134.

/A. Mescher rbject Coordinator

Enclosure

Copy: Tim Christman, GEPA Sherry L. Estes, USEPA (via Federal Express) Paul Jayko, GEPA Jane Montgomery, Schiff, et. al. David Leffler, City of Toledo Frank Robinson, McKesson (w/o enclosure)

- • ' Cousins Waste Control Corporation - PSC

Memo Toe JeanMescher

Prom Michael Graf

12rt)5/2005

RK XXKEM 84*' Monthly Report >1

XXKEM 84tli Monthly Rsport - NovMnber 2005

Dear Jean,

DuringNovember2005, no LES operations have occurred at the XXKEM site in Toiedo, Ohio. Cousins Waste Corrtrol (CWCC) performed tasks to supplement the LES abandonment and well installation. Fluid samples collected from existing well PX-42 and new wells PX-58 and 59 were analyzed tiy Brighton Analytical of Brighton Michigan; the laboratory reports are attached. In addition, all wastes generated during October 2005 were taken off-site for dispr^; the Hazardous Waste Manifests will be included in next months report. Also, Mannik & Smith surveyed the new well casings and secondly containment discharge line near the southern boundary of the landfill; the results of the sun/ey are attached.

Plans for December 2005 include removal of the fiac tank.

If you have any questions, please call.

Sincerely.

Michael Graf

Attachments; Brighton Analytical Laboratory Reports Mannik & Smith Survey Results

1701 E. Matzinger Road Toledo. Ohio 43612 {419)726-1500

THg MANNIK & SMITH QROUF, INC. laOQ Indian Wood CIrola

Maumae. Ohio 43837-4088 (411)091-2322

PAX (419)891-1996

JM CiJS^^—s4it.ktk\Lif

OAUJULMHIBy

OP

npT.

OMIGiaOBV lun

PoaWfFaxNota 7871

OoAtlpt. Co: '

nWMl ^hw«#

rtMf FIX*

H mi'ii

Loi4h Bpil

N tm i ^ »—

mt)/* 519.K

^on»h)r M p%-3<i y/N ^nu

cr fkp FiC' tf/tfV.

/^mid

7^/foPFVC. ffOTG^ lU.

c

V)

o

E •<

L

s'ev.'fihir

liML} JS .^iClt 6^ ^ ^

CffiL-pOUflMoh A u .

^& C9f S<ic. It H %mj^ m Q'*IIIA.O4^

American Environmental Group Ltd.

P;..

December 5,2005 ^ .

Cousins Waste Control, Inc. BBC/PSC ' ^ ; 1701 East Matzinger Road Toledo, OH 43612

Attn.: Mike Graf

SubJ.r Repair Work at Landfill Toledo, Ohio

Dear Mr. Graf,

Per our conversations concerning the r^r worit performed October 26"" and October 28"*, 2005 at the Cousins Landfill in Toledo, Ohio. AEGL certifies that all woric was performed to industry standards, AEGL further certifies that all seams made were made to industry standards and all seams were non-destructively tested and passed.

If you require further information, please contact me at 330-659-5930.

Sincerely, American Environmental Group, Ltd.

3600 Brecksville Rd, Suite 100. Richfield, OH 44286 • Pk 330-659-5930. Fx: 330-659-5931

xoo/zoolB ivxNaiNmiiANa Nvoitiaiiv icssssaoccT xvd 9S:OT NOM SOOZ/SO/ZT

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04764

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX58 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

[>CB/Pesticlde Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

i-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Kldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005

VRO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

^RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

KRO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005

^R0 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

^RO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

^RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

IRQ 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

^RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\R0 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

)-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

1,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005

1,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005

1,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005

^ieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

mdosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005

indosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005

Endosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005

mdrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

mdrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005

mdrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005

5-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

5-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

leptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005

3eptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005

Pagel

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612

BA Report Number: 83603 BA Sample ID: BK04764

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX58 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

texabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005

vtethoxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005

vtirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Toxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005

'CB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005

$eml-Volatile Analysis Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005

JN A liquid (extraction) Extracted 3510/3550 LS 10/31/2005

Volatile Analysis \cetone Not detected ug/L 500 SW846 8260 JH 11/03/2005

\crylonitrile Not detected ug/L 20 SW846 8260 JH 11/03/2005

Jenzene 94 ug/L 20 SW846 8260 JH 11/03/2005

3romochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Jromodichloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

3romoform Not detected ug/L 20 SW846 8260 JH 11/03/2005

3romomethane(Methyl Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005

l-Butanone (MEK.) Not detected ug/L 100 SW846 8260 JH 11/03/2005.

2arbon disulfide Not detected ug/L 100 SW846 8260 JH 11/03/2005

Tarbon t^rachloride Not detected ug/L 20 SW846 8260 JH 11/03/2005

2hlorobenzene 22 ug/L 20 SW846 8260 JH 11/03/2005

rhloroethanc 97 ug/L 20 SW846 8260 JH 11/03/2005

rhloroform Not detected ug/L 20 SW846 8260 JH 11/03/2005

rhloromethane(Methyl Chloride) Not detected ug/L 20 SW846 8260 JH 11/03/2005

;is-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

:is-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dibromo-3-Chloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005

3ibromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dibromoethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

3ibromomethane(Methylene Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Page 2

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone; (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Rqx)rtDate: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04764

Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: PO#63602D70

Sample ID: PX58 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

l3-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,4-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Qichlorodifluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Diethyl ether Not detected ug/L 200 SW846 8260 JH 11/03/2005

Ethyl benzene 510 ug/L 20 SW846 8260 JH 11/03/2005

Hexachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

>-Hexanone(Methyl Butyl Ketone) Not detected ug/L 100 SW846 8260 JH 11/03/2005

isopropylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

\tethyl iodide(Iodomethane) Not detected ug/L 20 SW846 8260 JH 11/03/2005

Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 100 SW846 8260 JH 11/03/2005

t-Methyl-2-pentanonc(MIBK) Not detected ug/L 100 SW846 8260 JH 11/03/2005

vtethylene chloride Not detected ug/L 100 SW846 8260 JH 11/03/2005

1-Methylnaphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005

^Japhthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005

i-Butylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1-Propylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

styrene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,1,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,2,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

r etrachloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Toluene 46 ug/L 20 SW846 8260 JH 11/03/2005

rans-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

rans-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005

rans-1,4-Dichloro-2-butene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2,3-Trichlorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005

1,2,4-Trichlorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005

1,1,1-Trichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,2-T richloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Page 3

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX; (810) 229-8650

Sample E>ate: 10/28/2005 Submit Date: 10/28/2005

Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04764

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX58 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

rrichloroefliene Not detected ug/L 20 SW846 8260 JH 11/03/2005 rrichlorofluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trimethylbenzene 44 ug/L 20 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,3,5-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 Vinyl chloride 61 ug/L 20 SW846 8260 JH 11/03/2005

Xylenes(total) 1800 ug/L 60 SW846 8260 JH 11/03/2005

DL=Reported detection limit for analytical method requested. Some compounds Released by: require special analytical methods to achieve MDEQ designated target detection limits (TDL). Date:

Elevated volatile dl due to sample matrix.

1

Page 4

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzlnger Road Toledo, OH 43612

BA Report Number: 83603 BA Sample ID: BK04765

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX59 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

PCB/Pesticide Analysis

i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

i-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

\ldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005

\RO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\R0 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005

\RO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\RO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\RO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

\R0 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

)-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

1,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005

1,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005

1,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Dieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005

3ndosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005

3ndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005

3ndrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Bndrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Sndrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005

j-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

;-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

rleptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005

rleptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005

-lexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Page 1

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number. 83603 BA Sample ID: BK0476S

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX59 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

y4eflioxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005

ttirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Poxt^ene Not detected ug/L 0.1 EPA 608 BY 11/02/2005

X!B/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005

Semi-Volatile Analysis

Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005

3NA liquid (extraction) Extracted 3510/3550 LS 10/31/2005

i/olatile Analysis

\cetone Not detected ug/L 500 SW846 8260 JH 11/03/2005

\ctylonitrile Not detected ug/L 20 SW846 8260 JH 11/03/2005

Benzene 92 ug/L 20 SW846 8260 JH 11/03/2005

Bromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Bromodichloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Bromoform Not detected ug/L 20 SW846 8260 JH 11/03/2005

Bromomethane(Methyl Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005

t-Butanone (MEK) Not detected ug/L 100 SW846 8260 JH 11/03/2005

2arbon disulfide Not detected ug/L 100 SW846 8260 JH 11/03/2005

2arbon tetrachloride Not detected ug/L 20 SW846 8260 JH 11/03/2005

Dhlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Dhloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Chloroform Not detected ug/L 20 SW846 8260 JH 11/03/2005

Chloromethane(Methyl Chloride) Not detected ug/L 20 SW846 8260 JH 11/03/2005

:is-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

:is-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dibromo-3-Chloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005

Oibromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dibromoethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

[)ibromomethane(Methylene Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,3-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Page 2

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date; 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04765

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number; P0#63602070

Sample ID: PXS9 leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

1,4-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Dichlorodifluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1 -Dich loroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2-Dichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005

diethyl ether Not detected ug/L 200 SW846 8260 JH 11/03/2005

ithyl benzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

^exachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

l-Hexanonc(Methyl Butyl Ketone) Not detected ug/L 100 SW846 8260 JH 11/03/2005

sopropylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Methyl iodide(Iodomethane) Not detected ug/L 20 SW846 8260 JH 11/03/2005

Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 100 SW846 8260 JH 11/03/2005

t-Methyl-2-pentanone(MlBK) Not detected ug/L 100 SW846 8260 JH 11/03/2005

\4ethylene chloride Not detected ug/L 100 SW846 8260 JH 11/03/2005

1-Methylnaphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005

*4aphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005

i-Butylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

i-Propylbcnzene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Styrene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,1,2-T etrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,2,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

relrachloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Toluoie 30 ug/L 20 SW846 8260 JH 11/03/2005

Tans-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

rans-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005

xans-l ,4-Dichloro-2-butene Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,2,3-T richloro benzene Not detected ug/L 100 SW846 8260 JH 11/03/2005

1,2,4-T rich lorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005

1,1,1-Trich loroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

1,1,2-T richloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005

rrichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005

Page 3

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005

Submit Date: 10/28/2005

Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number: 83603

BA Sample ID: BK04765

Project Name: Cousins Waste Control/XXKEM WV Abandonment

Project Number: P0#63602070 Sample ID: PXS91eachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

Trichlorofluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-T rimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,3,5-T rimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 Vinyl chloride Not detected ug/L 20 SW846 8260 JH 11/03/2005 Xylenes(total) Not detected ug/L 60 SW846 8260 JH 11/03/2005

DL=Reported detection limit for analytical method requested. Some compounds Released by: require special analytical methods to achieve MDEQ designated target detection limits (TDL). Date:

Elevated volatile dl due to sample matrix.

Page 4 •4

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612

BA Report Number: 83603 BA Sample ID: BK04766

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0«63602070

Sample ID: PX42 leachate & LNAPL

Parameters Results Units DL Method Reference Analyst Analysis

Date

PCB/Pesticide Analysis

i-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005

i-Chlordane Not detected ug/L 0.08 EPA 608 BY 11/02/2005

\Idrin Not detected ug/L 0.04 EPA 608 BY 11/02/2005

\RO 1016 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

\RO 1221 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

ytO 1232 Not detected ug/L 1.6 EPA 608 BY 11/02/2005

\RO 1242 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

\RO 1248 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

\R0 1254 11 ug/L 0.80 EPA 608 BY 11/02/2005

\RO 1260 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

\RO 1262 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

\RO 1268 Not detected ug/L 0.80 EPA 608 BY 11/02/2005

5-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005

3P-6(PBB) Not detected ug/L 0.04 EPA 608 BY 11/02/2005

1-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005

1,4-DDD Not detected ug/L 0.08 EPA 608 BY 11/02/2005

1,4-DDE Not detected ug/L 0.08 EPA 608 BY 11/02/2005

1,4-DDT Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Dieldrin Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Endosulfan I Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Endosulfan II Not detected ug/L 0.12 EPA 608 BY 11/02/2005

Endosulfan sulfate Not detected ug/L 0.20 EPA 608 BY 11/02/2005

indrin Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Endrin aldehyde Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Endrin ketone Not detected ug/L 0.08 EPA 608 BY 11/02/2005

j-BHC(Lindane) Not detected ug/L 0.04 EPA 608 BY 11/02/2005

;-Chlordane Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Hleptachlor Not detected ug/L 0.04 EPA 608 BY 11/02/2005

Heptachlor epoxide Not detected ug/L 0.04 EPA 608 BY 11/02/2005

hiexabromobenzene Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Page I

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04766

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX42 leachate & LNAPL

Parameters Results Units DL Method Reference Analyst Analysis

Date

Methoxychlor Not detected ug/L 0.20 EPA 608 BY 11/02/2005

Mirex Not detected ug/L 0.08 EPA 608 BY 11/02/2005

Total PCB 11 ug/L 0.80 EPA 608 BY 11/02/2005

Toxaphene Not detected ug/L 0.40 EPA 608 BY 11/02/2005

PCB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005

Semi-Volatile Analysis Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005

BNA liquid (extraction) Extracted 3510/3550 LS 10/31/2005

Volatile Analysis Acetone Not detected ug/L 50 SW846 8260 JH 11/03/2005

Acrylonitrile Not detected ug/L 2 SW846 8260 JH 11/03/2005

Benzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromochioromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromodichloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromoform Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromomethane(Methyl Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005

2-Butanone (MEK) Not detected ug/L 10 SW846 8260 JH 11/03/2005

Carbon disulfide Not detected ug/L 10 SW846 8260 JH 11/03/2005

Carbon tetrachloride Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloroform Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloromethane(Methyl Chloride) Not detected ug/L 2 SW846 8260 JH 11/03/2005

cis-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

:is-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005

l,2-Dibromo-3-Chloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Dibromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dibromoethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Dibromomethane(Methylene Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Page 2

1 4

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04766

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: PX42 leachate & LNAPL

Parameters Results Units DL Method Reference Analyst Analysis

Date

1,3-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,4-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Dichlorodifluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1-Dichioroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Diethyl ether Not detected ug/L 20 SW846 8260 JH 11/03/2005

Ethyl benzene 180 ug/L 2 SW846 8260 JH 11/03/2005

Hexachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Z-Hexanone(Methyl Butyl Ketone) Not detected ug/L 10 SW846 8260 JH 11/03/2005

Isopropyibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Methyl iodide(Iodomethane) Not detected ug/L 2 SW846 8260 JH 11/03/2005

Methyl(tert)butyl ether(MTBE) Not detected ug/L 10 SW846 8260 JH 11/03/2005

t-Methyl-2-pentanone(MIBK) Not detected ug/L 10 SW846 8260 JH 11/03/2005

Methylene chloride Not detected ug/L 10 SW846 8260 JH 11/03/2005

Z-Methylnaphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005

Naphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005

ri-Butylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

i-Propylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Styrene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1,1,2-T etrachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1,2,2-Tetrachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Tetrachloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Toluene 30 ug/L 2 SW846 8260 JH 11/03/2005

xans-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

xans-l ,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005

;rans-1,4-Dichloro-2-butene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2,3-Trichlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005

1,2,4-T richlorobenzaie Not detected ug/L 10 SW846 8260 JH 11/03/2005

1,1,1-Trichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1,2-Trichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Page 3

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone; (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005

Report Date: 11/07/2005

To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number: 83603

BA Sample ID: BK04766

Project Name: Cousins Waste Control/XXKEM WV Abandonment

Project Number: P0#63602070

Sample ID: PX42 leachate & LNAPL

Parameters Results Units DL Method Reference Analyst Analysis

Date

Trichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005 Trichlorofluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005 1,2,3-Trimethylbenzene 65 ug/L 2 SW846 8260 JH 11/03/2005 1,2,4-T rimethy Ibenzene 70 ug/L 2 SW846 8260 JH 11/03/2005 1,3,5-T rimethy Ibenzene 24 ug/L 2 SW846 8260 JH 11/03/2005 Vinyl chloride Not detected ug/L 2 SW846 8260 JH 11/03/2005 Xylenes(total) 1400 ug/L 6 SW846 8260 JH 11/03/2005

DL=Reported detection limit for analytical method requested. Some compounds require special analytical methods to achieve MDEQ designated target detection limits (TDL).

Elevated PCB/pesticide dl due to sample matrix. Elevated volatile dl due to sample matrix.

Released by:

Date:

Page 4

;i

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 RqjortDate: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04767

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P(M63602070

Sample ID: Dupl leachate

Parameters Results Units DL Mediod Reference Analyst Analysis

Date

PCB/Pesticide Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

a-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

4ldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005

4RO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005

\RO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

4RO 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005 b-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

BP-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

t,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005

t,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005

t,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Dieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endosulfan I Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Bndosul&n II Not detected ug/L 0.03 EPA 608 BY 11/02/2005

Bndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005

Endrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Bndrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005

;-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

j-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Heptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005

Heptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005

Flexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Page 1

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005

Submit Date: 10/28/2005

Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04767

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: PO#636D2070

Sample ID: Dnpl leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

VIettioxychlor Not detected ug/L 0.05 EPA 608 BY 11/02A2005

Mirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Foxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005

PCB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005

Senii-Volatik Analysis

Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005

SNA liquid (extraction) Extracted 3510/3550 LS 10/31/2005

Volatile Analysis

\cetone Not detected ug/L 50 SW846 8260 JH 11/03/2005

4ctylonitrile Not detected ug/L 2 SW846 8260 JH 11/03/2005

Benzene 78 ug/L 2 SW846 8260 JH 11/03/2005

Bromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromodichloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromoform Not detected ug/L 2 SW846 8260 JH 11/03/2005

Bromomethane(Methyl Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005

t-Butanone (MEK) Not detected ug/L 10 SW846 8260 JH 11/03/2005

Carbon disulfide Not detected ug/L 10 SW846 8260 JH 11/03/2005

Carbon tetrachloride Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloroform Not detected ug/L 2 SW846 8260 JH 11/03/2005

Chloromethane(MethyI Chloride) Not detected ug/L 2 SW846 8260 JH 11/03/2005

:is-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

:is-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005

[ ,2-Dibromo-3-Chloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Dibromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dibromoethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

3ibromomethane(Methylene Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,3-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Page 2

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number; 83603 BA Sample ID: BK04767

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: Dnpl ieacbate

Parameters Results Units DL Method Reference Analyst Analysis

Date

1,4-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

3ichlorodifluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1-Dichioroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2-Dichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005

diethyl ether Not detected ug/L 20 SW846 8260 JH 11/03/2005

ithyl benzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

3exachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

J-Hexanone(Methyl Butyl Ketone) Not detected ug/L 10 SW846 8260 JH 11/03/2005

sopropy 1 ben zene Not detected ug/L 2 SW846 8260 JH 11/03/2005

diethyl iodide(Iodomethane) Not detected ug/L 2 SW846 8260 JH 11/03/2005

Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 10 SW846 8260 JH 11/03/2005

l-Methyl-2-pentanone{MlBK) Not detected ug/L 10 SW846 8260 JH 11/03/2005

Vlethylene chloride Not detected ug/L 10 SW846 8260 JH 11/03/2005

J-Methylnaphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005

Naphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005

i-Butylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

i-Propylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Styrene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1,1,2-T etrachioroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

[, 1,2,2-T etrachioroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

Tetrachloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Toluene 23 ug/L 2 SW846 8260 JH 11/03/2005

rans-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

rans-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005

rans-1,4-Dichioro-2-butene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2,3-T richlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005

1,2,4-T richlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005

1,1,1 -T richloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,1,2-T richloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

frichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Page 3

Brighton Analytical, LX.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810)229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005

Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04767

Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: Dnpl leachate

Parameters Results Units DL Method Reference Analyst Analysis

Date

frichlorofluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2,3-Trich loropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2,3-T rimethy Ibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,2,4-T rimethy Ibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

1,3,5-Trimethylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005

Vinyl chloride Not detected ug/L 2 SW846 8260 JH 11/03/2005

Xylcnes(total) Not detected ug/L 6 SW846 8260 JH 11/03/2005

[)L=Reported detection limit for analytical method requested. Some compounds Released by: •equire special analytical methods to achieve MDEQ designated target detection imits (TDL). Date:

alevated volatile dl due to sample matrix.

Page 4

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810)229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005

RqaortDate: 11/07/2005

To: Cousins Waste Control Corp.

1701-1801 Matzinger Road

Toledo, OH 43612

BA Report Numben 83603 BA Sample ID: BK04768

Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: Trip Blank

Parameters Results Units DL Method Reference Analyst Analysis

Date

PCB/Pesticide Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

j-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Aldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005

ARO 1016 Not detected Ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005

ARO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

ARO 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005

IvBHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005

M-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005

t,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005

»,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Oieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Bndosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005

Bndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005

Bndrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Endrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005

;-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005

{-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005

deptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005

deptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005

dexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Page 1

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date; 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number 83603 BA Sample ID: BK04768

Project Name: Consins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: Trip Blank

Parameters Results Units DL Method Reference Analyst Analysis

Date

Vlethoxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005

^irex Not detected ug/L 0.02 EPA 608 BY 11/02/2005

Foxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005

iHTB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005

Semi-Volatile Analysis

Dimethylaniiine Not detected ug/L 10 EPA 625 RG 11/02/2005

3NA liquid (extraction) Extracted 3510/3550 LS 10/31/2005

i^olatile Analysis

\cetone Not detected ug/L 25 SW846 8260 JH 11/03/2005

\crylonitrile Not detected ug/L 1 SW846 8260 JH 11/03/2005

Benzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Bromochloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

3romodichloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Jromoform Not detected ug/L 1 SW846 8260 JH 11/03/2005

3romomethane(Methyl Bromide) Not detected ug/L 1 SW846 8260 JH 11/03/2005

1-Butanone (MEK) Not detected ug/L SW846 8260 JH 11/03/2005

Zlarbon disulfide Not detected ug/L SW846 8260 JH 11/03/2005

Darbon tetrachloride Not detected ug/L 1 SW846 8260 JH 11/03/2005

Dhlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

"hloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Chloroform Not detected ug/L 1 SW846 8260 JH 11/03/2005

Chloromethane(Methyl Chloride) Not detected ug/L 1 SW846 8260 JH 11/03/2005

:is-1,2-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005

:is- 1,3-Dichloropropene Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2-Dibromo-3-Chloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Dibromochloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2-Dibromoethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Z)ibromomethane(Methylene Bromide) Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,3-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Page 2

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612

BA Report Number. 83603 BA Sample ID: BK04768

Project Name: Consins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070

Parameters Results

Sample ID: Trip Blank

Units DL Method Reference Aruilyst Analysis

Date

1,4-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Dichlorodlfluoromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,1-Dichloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2-Dichloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,1-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2-Dichloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Diethyl ether Not detected ug/L 10 SW846 8260 JH 11/03/2005

Ethyl benzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Hexachioroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

2-Hexanone(Methyl Butyl Ketone) Not detected ug/L 5 SW846 8260 JH 11/03/2005

Isopropylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Methyl iodide(Iodomethane) Not detected ug/L 1 SW846 8260 JH 11/03/2005

Methyl(tert)butyl ether(MTBE) Not detected ug/L 5 SW846 8260 JH 11/03/2005

4-Methyl-2-pentanone(MIBK) Not detected ug/L SW846 8260 JH 11/03/2005

Methylene chloride Not detected ug/L SW846 8260 JH 11/03/2005

2-Methylnaphthalene Not detected ug/L 5 SW846 8260 JH 11/03/2005

Naphthalene Not detected ug/L 5 SW846 8260 JH 11/03/2005

n-Butylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

n-Propylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Styrene Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,1,1,2-T etrachloroethan e Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,1,2,2-Tetrachloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

FeU^hloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Toluene Not detected ug/L 1 SW846 8260 JH 11/03/2005

rans-1,2-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005

trans-1,3-Dichloropropene Not detected ug/L 1 SW846 8260 JH 11/03/2005

trans-1,4-Dichloro-2-butene Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,2,3-Trichlorobenzene Not detected ug/L 5 SW846 8260 JH 11/03/2005

1,2,4-T rich lorobenzene Not detected ug/L SW846 8260 JH 11/03/2005

1,1,1 -T richloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

1,1,2-T richloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005

Trichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005

Pages

Brighton Analytical, L.L.C. 2105 Pless Drive

Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650

Sample Date: 10/28/200S Submit Date: 10/28/2005 Report Date: 11/07/2005

To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612

BA Report Number; 83603 BA Sample ID: BK04768

Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070

Sample ID: Trip Blank

Parameters Results Units DL Method Reference Analyst Analysis

Date

rrichlorofluoromcthane Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,3-T rimethy Ibenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,3,5-T rimethy Ibenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 ^inyl chloride Not detected ug/L 1 SW846 8260 JH 11/03/2005 Xylcnes(total) Not detected ug/L 3 SW846 8260 JH 11/03/2005

DL=Reported detection limit for analytical method requested. Some compounds Released by: 'equire special analytical methods to achieve MDEQ designated target detection imits (TDL). Date:

Page 4

-u . : I

Brighton Analytical, L.L.C. | 2105 Pless Drive

Brighton, Michigan 48116 I jM Phone: (810) 229-7575 FAX: (810) 229-8650 |

To: Cousins Waste Control Corp. Sample Date: 10/28/2005 1701-1801 Matzinger Road Submit Date: 10/28/2005 Toledo, OH 43612 Report Date: 11/07/2005

BA Report Numben 83603 Project Name: Cousins Waste ControI/XXKEM WV Abandonment BA Sample ID: BK04768 Project Number: P0#63602070

Sample ID: Trip Blank

Analysis Parameters Results Units DL Method Reference Analyst D^te

Page 5