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December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 1 of 106
0800597 Ogden Railyard (US EPA Region 8)
Source Procedure ID Procedure Name Citation
1668
200.7
2216-90
3510C
7470A
7471A
8015B
8015B MOD
3010-A
3050-B
3510-B
3550-B
unknown
unknown
unknown
unknown
Unknown
Unknown
Unknown
Unknown
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis fy FLAA or ICPSpectrometry
Acid Digestion of Sediments, Sludges, and Soils forMetals Analysis by FLAA/ICP or GFAA/ICPMS
Separatory Funnel Extraction, Liquid-Liquid
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
0800597
0800597
0800597
0800597
0800597
0800597
0800597
0800597
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 2 of 106
1119USBR Bureau of Reclamation
Source Procedure ID Procedure Name Citation
200.7-T Total Metals Preparation for EPA 200.2 USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 3 of 106
11DELMOD Delaware River Basin Commission
Source Procedure ID Procedure Name Citation
9230-C-2
200.2
Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation
Preparation for Water, Soil, or Waste Samples
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
APHA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 4 of 106
11NPSWRD National Park Service
Source Procedure ID Procedure Name Citation
GLKN_ACLS
GLKN_CAT
GLKN_CHLA
GLKN_DOC
GLKN_NH4-N
GLKN_NOX-N
GLKN_SIO2
Alk, Cl, & SO4
Cations (Ca, Na, Mg, K)
Chlorophyll a
Dissolved Organic Carbon
Ammonium-N
Nitrate+Nitrite-N
SiO2
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 5 of 106
11NPSWRD National Park Service
Source Procedure ID Procedure Name Citation
GLKN_TP/TN
GLKN_TSS
GRCA_ALPHA-BETA
NGPN_TSS_TDS
NPS_INVERTS
NPS_WHATMAN_GF
OZAR_PREP_CHL
OZAR_PREP_TN
OZAR_PREP_TP
SEDSIEVELT2MM
Total phosphorus/total nitrogen
Total Suspended Solids
Evaporation to Dryness on a Planchet
Total Suspended and Dissolved Solids
Invertebrate Counting Procedures
Whatman GF/F Filtration
Preparing Suspended Chlorophyll a Samples forAnalysis
Processing Total Nitrogen Samples
Processing Total Phosphorus Samples
Sediment Sieved to <2mm
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
GLKN_0000002 - Magdalene, S., D.R. Engstrom, and J. Elias, 2007,Great Lakes Inventory & Monitoring Network Large Rivers Water QualityMonitoring Protocol: Standard Operation Procedure #7: ProcessingWater Samples and Analytical Laboratory Requirements, National ParkService, Great Lakes Network, 11p
Monroe, S.A., R.C. Antweiler, R.J. Hart, H.E. Taylor, M. Truini, J.R.Rihs, and T.J. Felger, 2005, Chemical Characteristics of Ground-WaterDischarge along the South Rim of Grand Canyon in Grand CanyonNational Park, Arizona, 2000-2001, U.S. Geological Survey, S.I.Report2004-5146
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1999, Rapid Bioassessment Protocols for Wadeable Streamsand Rivers: Periphyton, Benthic Macroinvertebrates, and Fish, 2nd ed,USEPA, EPA 841/B-99-002
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
OZAR_0000001 - Ozark National Scenic Riverways, August 25, 2005,Standard Operating Procedures for Water Quality Monitoring-OzarkNational Scenic Riverways, Ozark National Scenic Riverways, 50 pages
OZAR_0000001 - Ozark National Scenic Riverways, August 25, 2005,Standard Operating Procedures for Water Quality Monitoring-OzarkNational Scenic Riverways, Ozark National Scenic Riverways, 50 pages
OZAR_0000001 - Ozark National Scenic Riverways, August 25, 2005,Standard Operating Procedures for Water Quality Monitoring-OzarkNational Scenic Riverways, Ozark National Scenic Riverways, 50 pages
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
11NPSWRD
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 6 of 106
11NPSWRD National Park Service
Source Procedure ID Procedure Name Citation
SEDSIEVELT63UM
SHIL_GRUB_1UM
WRST_MAC_SCPREP
3030-B
200.2
3050-B
Sediment Sieved to <63 micrometers
Prefiltered w/Glass Fiber Filter, Effective Retention of> 1um
Hecht Specific Conductance Lab Prep for McCarthy,AK
Preliminary Filtration of Metals Samples
Preparation for Water, Soil, or Waste Samples
Acid Digestion of Sediments, Sludges, and Soils forMetals Analysis by FLAA/ICP or GFAA/ICPMS
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
WRST_MAC_HEC - Hecht, B. and E. LaChapelle, 1999, Hydrologic andHydrogeologic Factors Affecting Aquifer Protection, McCarthy Area,Alaska. Geotechnical Report for Alaska Department for EnvironmentalConservation. Grant C9000652-94-0. Report prepared for The McCarthyArea Council, Glennallen, Alaska., Balance Hydrologics, Inc., 90 pages
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
11NPSWRD
11NPSWRD
11NPSWRD
APHA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 7 of 106
1CTDPHBM Connecticut Department of Public Health
Source Procedure ID Procedure Name Citation
ASTM D6503 ENTEROLERT American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (II), American Society for Testingand Materials, Vol 11.02
1CTDPHBM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 8 of 106
21CAOCSD Orange County Sanitation District California
Source Procedure ID Procedure Name Citation
LPROC001 organics USEPA, 1982, Test Method for the Determination of PolychlorinatedBiphenyls in Transformer Fluid and Waste Oils, USEPA, EPA 600/4-81-045
21CAOCSD
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 9 of 106
21COL001 Colorado Dept. of Public Health & Environment
Source Procedure ID Procedure Name Citation
200.2 Preparation for Water, Soil, or Waste Samples USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 10 of 106
21DCBAWQ District of Columbia Dept of Health, Water Quality Division
Source Procedure ID Procedure Name Citation
LSP-001
LSP-002
LSP-003
LSP-004
Filtration of water samples, 0.45
Preparation of biological samples for inorganicchemical analysis
Manual digestion with persulfate for polyphosphatesand phosphorus compounds
Filtration of water samples, particle retention =1.6um
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
21DCBAWQ
21DCBAWQ
21DCBAWQ
21DCBAWQ
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 11 of 106
21FLACEP Alachua County Environmental Protection Department (Florida)
Source Procedure ID Procedure Name Citation
351.2
365.2/365.3
FIELD_FLTRD
FILTRATION
3005-A
351.2
Phosphorus- Total
Field Filtered
Filtration
Total Recoverable and Dissolved Prep for FLAA, ICP
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21FLACEP
21FLACEP
21FLACEP
21FLACEP
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 12 of 106
21FLAVON Avon Park Air Force Range - 18 ASOG DET 1 OL A/CEV
Source Procedure ID Procedure Name Citation
EPA 351.2 11
SM 10200 H 1
SM 4500-P B 5
Acid digestion by block digestor
Pigment extraction
Persulfate digestion
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
21FLAVON
21FLAVON
21FLAVON
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 13 of 106
21FLBFA FL Dept. of Environmental Protection
Source Procedure ID Procedure Name Citation
DIG-TKN-TP
DIG-TP-LOW
DIG-TKN-TP
Preparation method for TKN and TP
Preparation method for low-level phosphorus
Preparation method for TKN and Total Phosphorus
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
21FLBFA
21FLBFA
21FLCMP
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 14 of 106
21FLBRA Biological Research Associates (Florida)
Source Procedure ID Procedure Name Citation
10200-H
GENPREP
200.7-T
200.8-T
Chlorophyll a prep
General Preparation related to Analytical procedure
Total Metals Preparation for EPA 200.2
Total Metals Preparation for EPA 200.8
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21FLBRA
21FLBRA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 15 of 106
21FLBREV Brevard County Stormwater Utility Department (Florida)
Source Procedure ID Procedure Name Citation
10200-H
160.2
351.2
365.4
SW846-3005A
Chlorophyll a
TSS
TKN
Total Phosphorus
Metals
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
21FLBREV
21FLBREV
21FLBREV
21FLBREV
21FLBREV
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 16 of 106
21FLBROW Broward Co Dept of Natural Resource Protection (Florida)
Source Procedure ID Procedure Name Citation
P001
P002
P003
P004
Bacti Prep
Chlorophyll Extraction
EPA 600
MIBK EXTRACTION
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1996, Method 1637: Determination of Trace Elements inAmbient Waters by Chelation Preconcentration with GFAA., USEPA,EPA 821/R-96-004
21FLBROW
21FLBROW
21FLBROW
21FLBROW
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 17 of 106
21FLCEN Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
10200-H
1631
200.2
Prep chlorophyll and pheophytin
Mercury
Preparation for Water, Soil, or Waste Samples
Lou, Ley, 2002, Volume Name, Department of Environmental ProtectionCentral District, v.1
USEPA, 1999, Method 1631, rev B: Mercury in Water by Oxication,Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry.,USEPA, EPA 821/R-99-005
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
21FLCEN
21FLCEN
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 18 of 106
21FLCMP FL Dept. of Environmental Protection
Source Procedure ID Procedure Name Citation
351.2
DIG-TKN-TP
351.2
365.4
LAB
TKN Sample Preparation Procedure
Preparation method for TKN and Total Phosphorus
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Phosphorus, Total (as P)
Methodology for Chemical Analysis
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
21FLCMP
21FLCMP
21FLFTM
21FLFTM
21FLPNS
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 19 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
2310-B
3030-B
3030-C
3030-D
3030-E
3030-F
3030-G
3030-H
3030-I
3030-J
Acidity, hot peroxide preparation
Preliminary Filtration of Metals Samples
Treatment for Acid-Extractable Metals
Preliminary Digestion for Metal Samples
Nitric Acid Digestion of Metals
Nitric and Hydrochloric Acid Digestion
Nitric and Sulfuric Acid Digestion
Nitric and Perchloric Acid Digestion
Nitric, Perchloric and Hydrofluoric Acid
Dry Ashing of Metals Samples
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 20 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
4500-CN(B)
4500-CN-B
4500-F-B
4500-NH3(B)
4500-NH3-B
4500-S2(B)
4500-S2(C)
4500-S2-C
5520-E
9213-D-3
Preliminary Treatment of Cyanide Samples
Preliminary Treatment of Samples in WaterContaining Cyanide
Preliminary Distillation for Water Samples ContainingFluoride
Preliminary Distillation Step
Preliminary Distillation for Ammonia in Water
Separation of Soluble and Insoluble Sulfides
Pretreatment to Remove Interfering Substances orConcentrate Sulfide
Pretreatment to Remove Interfering Substances or toConcentrate the Sulfide in Water by Wet Chemistry
Extraction of Oil and Grease for Sludge
Natural Bathing Beach, Sample Preparation forEscherichia coli Determination
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 21 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
9215-A-5
9215-C-3
9215-D-3
9230-C-2
1310-A
1311
1311-HG
1311-MT
1311-V
1625P
200.2
Heterotrophic Plate Count, General SamplePreparation
Heterotrophic Plate Count, Spread Plate MethodSample Preparation
Heterotrophic Plate Count, Membrane Filter MethodSample Preparation
Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation
Extraction Procedure Toxicity Test Method andStructural Integrity Test
TCLP Preparation for Semivolatiles
TCLP Preparation for Mercury
TCLP Preparation for Metals
TCLP Preparation ZHE
BNA (isotopic dilution) Preparation
Preparation for Water, Soil, or Waste Samples
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
APHA
APHA
APHA
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 22 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
200.2-M
200.7-T
200.8-CR
200.8-T
3005-A
3010-A
3015
3015-M
3020-A
3040
Total Recoverable Metals Digestion
Total Metals Preparation for EPA 200.2
Clean Room Preparation for EPA 200.8
Total Metals Preparation for EPA 200.8
Total Recoverable and Dissolved Prep for FLAA, ICP
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis fy FLAA or ICPSpectrometry
Microwave Assisted Acid Digestion of AqueousSamples and Extracts
Aqueous Sample Prep for Total Metals (modified)Suspended Solids, ICP,GFAA,ICP-MS
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis by GFAA Spectroscopy
Oily Waste Prep for Soluble Metals by AA and ICP
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 23 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
3040-A
3050-A
3050-B
3051
3510-B
3510-C
3520-B
3520-C
3540-B
3540-C
Dissolution Procedure for Oils, Greases, and Waxes
Acid Digestion of Sediments, Sludges, and Soils
Acid Digestion of Sediments, Sludges, and Soils forMetals Analysis by FLAA/ICP or GFAA/ICPMS
Microwave Assisted Acid Digestion of Sediments,Sludges, Soils, and Oils
Separatory Funnel Extraction, Liquid-Liquid
Separatory Funnel Liquid-Liquid Estraction
Continuous Liquid-Liquid Extraction for Organics
Continuous Liquid-Liquid Extraction for Organics
Soxhlet Extraction for Nonvolatile and SemivolatileOrganic Compounds from Solids, Solid SamplesOnly
Soxhlet Extraction for Nonvolatile and SemivolatileOrganics from Soils, Sludges, and Wastes
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 24 of 106
21FLDADE Dade Environmental Resource Management (Florida)
Source Procedure ID Procedure Name Citation
3550-A
3550-B
3580-A
3585
50.6
5030-A
548.1-P
549.1-P
8150-P
P-010-1
SFSAS_FT_PREP
Ultrasonic Extraction of Nonvolatile and SemivolatileOrganic Compounds form Soils, Sludges, andWastes
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
Waste Dilution
Waste Dilution
Phase Separation and Aliquotting
Sample Preparation and Extraction for VolatileOrganic Analysis by Purge-and Trap
Endothall Preparation
Diquat and Paraquat Preparation
Herbicide Preparation Portion of 8150
Preparation for Pesticides/PCB in Water/Soil
Fish Tissue Preparation Technique
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 19--, CLP SOW for Inorganics Analysis-IHC01_3, USEPA,IHC01_3
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 25 of 106
21FLEECO Lee County (Florida)
Source Procedure ID Procedure Name Citation
3030-E Nitric Acid Digestion of Metals American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 26 of 106
21FLFMRI Florida Fish & Wildlife C C / Marine Research Institute
Source Procedure ID Procedure Name Citation
PROC 1 Field Hydrolab Sample Procedures ORG-01 - U.S. Environmental Protection Agency, 2001, NationalCoastal Assessment Field Operations Manual, USEPA, Unknown
21FLFMRI
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 27 of 106
21FLFTM Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
DIG-TKN-TP
245.1
351.2
365.1
365.4
DIG-TKN-TP-2
GC-002
LC-006
LC-006-A
Preparation method for TKN and Total Phosphorus
Mercury Analysis
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Total Phosphorus in Water
Preparation for Phosphorus, Total (as P)
Preparation method for TKN and Total Phosphorus
DEP SOP-GC-002
DEP SOP-LC-006
DEP SOP-LC-006 (A)
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
21FLCMP
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 28 of 106
21FLFTM Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
LC-011-A
LC-011-B
LC-021
PK-SETTLE
SOP-AB02_1
SOP-AB04
SOP-AB05
SOP-AB10_1
SOP-AB11
DEP SOP-LC-011 (A)
DEP SOP-LC-011 (B)
DEP SOP-LC-021
Pheophytin preparation analysis
Phytoplankton Identification - Diatom
Phytoplankton Identification - Wet Taxa
DEP Phytoplankton Preparation - Wet Taxa
DEP-SOP-0/001
Proceedure for Phytoplankton Sample Receipt andSample Handling for Taxonomic Analysis
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
DEP-CHEM - Florida DEP Laboratory Chemistry Section, Amended 6-8-04, Florida DEP Laboratory Standard Operating Procedures for theChemistry Section, Florida DEP Laboratory, Chapter 62-160
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
21FLFTM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 29 of 106
21FLFTM Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
SOP-BB01
SOP-BB02
SOP-TA08_010804
W-M-DIGEST
200.2
200.7-T
3050-A
3550-B
Preparation for Bacterial Analysis
Preparation for Chlorophyll-A (Monochromatic) &Pheophytin-A (Monochromatic)
Preparation for Algal Growth Potential
ICP Metals Digestion
Preparation for Water, Soil, or Waste Samples
Total Metals Preparation for EPA 200.2
Acid Digestion of Sediments, Sludges, and Soils
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21FLFTM
21FLFTM
21FLFTM
21FLFTM
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 30 of 106
21FLGFWF Florida Fish and Wildlife Conservation Commission
Source Procedure ID Procedure Name Citation
4500-P-B(1)
4500-P-B(5)
3030-B
3030-E
4500-NH3(B)
Preliminary filtration for orthophosphorus 0.45ummembrane filter
Persulfate digestion for total phosphorus
Preliminary Filtration of Metals Samples
Nitric Acid Digestion of Metals
Preliminary Distillation Step
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
21FLGFWF
21FLGFWF
APHA
APHA
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 31 of 106
21FLGW FL Dept. of Environmental Protection
Source Procedure ID Procedure Name Citation
351.2
365.4
SOP-BB02
351.2 SEDIMENT
365.1
365.4 SEDIMENT
MERCURY
ORGANIC EXT
SOP-AB02_1
SOP-AB11
SOP-BB02
SOP-TA08_01-04
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Phosphorus, Total (as P)
Preparation for Chlorophyll-A (Monochromatic) &Pheophytin-A (Monochromatic)
Preparation of samples for total kjeldahl nitrogenanalysis
Preparation for Total Phosphorus in Water
Preparation of samples for total phoshorus analysis
Preparation of solid and liquid matrices for mercuryanalysis
Extraction of non-volatile and semi-volatile organiccompounds from soils, sludges, wastes
Preparation of Periphyton Diatoms
Proceedure for Phytoplankton Sample Receipt andSample Handling for Taxonomic Analysis
Proceedure for Phytoplankton Sample Filtering
Proceedure for Algal Growth Potential
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
21FLFTM
21FLFTM
21FLFTM
21FLGW
21FLGW
21FLGW
21FLGW
21FLGW
21FLGW
21FLGW
21FLGW
21FLGW
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 32 of 106
21FLGW FL Dept. of Environmental Protection
Source Procedure ID Procedure Name Citation
TOTAL DIGESTION
200.2
TOTAL TOTAL DIGESTION
Preparation for Water, Soil, or Waste Samples
Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
21FLGW
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 33 of 106
21FLHILL Hillsborough County Environmental (Florida)
Source Procedure ID Procedure Name Citation
3030-E Nitric Acid Digestion of Metals American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 34 of 106
21FLLCPC Lake County Water Resource Management (Florida)
Source Procedure ID Procedure Name Citation
GENPREP General Preparation LAKE COUNTY WATER RESOURCE LAB, 2001, LAKE COUNTYWATER RESOURCE MANAGEMENT QUALITY SYSTEMS MANUAL,LAKE COUNTY WATER RESOURCE MANAGEMENT, ALL PAGES
21FLLCPC
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 35 of 106
21FLLEON Leon County Public Works (Florida)
Source Procedure ID Procedure Name Citation
3510-C Separatory Funnel Liquid-Liquid Estraction USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 36 of 106
21FLLOX Loxahatchee River District (Florida)
Source Procedure ID Procedure Name Citation
200.2 Preparation for Water, Soil, or Waste Samples USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 37 of 106
21FLMANA Manatee County Environmental Management Dept (Florida)
Source Procedure ID Procedure Name Citation
GENERIC General Listing of Field and Lab AnalyticalProcedures for Manatee County
Greg Blanchard, 2002, General Listing of Field and LaboratoryAnalytical Procedures for Manatee County, Manatee County, 1
21FLMANA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 38 of 106
21FLMCGL McGlynn Laboratories, Inc
Source Procedure ID Procedure Name Citation
10200-H Chlorophyll a-b-c Determination American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
21FLMCGL
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 39 of 106
21FLNAPL City of Naples (Florida)
Source Procedure ID Procedure Name Citation
3010-A
GEN PREP
Acid digestion of aqueous samples and extracts fortotal metals
General preparation method
USEPA, 2000, Estuarine and Coastal Marine Waters: Bioassessmentand Biocriteria Technical Guidance., USEPA, EPA 822/B-00-024
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
21FLNAPL
21FLNAPL
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 40 of 106
21FLNWFD Northwest Florida Water District
Source Procedure ID Procedure Name Citation
200.2 Preparation for Water, Soil, or Waste Samples USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 41 of 106
21FLORAN Orange County Environmental Protection (Florida)
Source Procedure ID Procedure Name Citation
3020A
EPA100.1
EPA110.2
EPA120.1
EPA130.1
EPA150.1
EPA160.1
EPA160.2
EPA160.3
EPA160.4
EPA170.1
EPA180.1
EPA200.7
EPA210.2
Metals Prep
Depth, Secchi disk depth
True Color
Specific Conductance
Harness by titration
pH
Volatile Solids
Total Suspended Solids
Total Solids
Dissolved Solids
Temperature, water
Turbidity
ICAP Metals
Beryllium
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 42 of 106
21FLORAN Orange County Environmental Protection (Florida)
Source Procedure ID Procedure Name Citation
EPA213.2
EPA239.2
EPA245.1
EPA270.2
EPA272.2
EPA279.2
EPA310.1
EPA325.3
EPA350.1
EPA351.2
EPA353.2
EPA360.2
EPA365.1
EPA375.4
Cadmium
Lead
Mercury
Selenium
Silver
Thallium
Alkalinity
Chloride
Ammonia, unionized
Nitrogen, Kjeldahl
Nitrogen Suite
Dissolved Oxygen
Phosphorus Suite
Sulfate
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 43 of 106
21FLORAN Orange County Environmental Protection (Florida)
Source Procedure ID Procedure Name Citation
EPA405.1
EPA410.4
EPA500.1
EPD100.1
GEN PREP
SM10200H
SM2120B
SM2310B
SM2320B
SM2340B
SM2340C
SM3113B
SM6010B
SM9222B
SM9222D
Biochemical Oxygen Demand
Chemical Oxygen Demand
Nitrogen, organic
Depth, secchi disk depth
General Preperation corresponding to Lab Methods
Chlorophyll Suite
Color
Acidity as CaCO3
Alkalinity, Total
Hardness, Ca, Mg
Harness, Ca, Mg
Metals Prep
Metals Prep Procedure
Total Coliform
Total Fecal Coliform
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
21FLORAN
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 44 of 106
21FLORAN Orange County Environmental Protection (Florida)
Source Procedure ID Procedure Name Citation
SM9230C Fecal Strep USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
21FLORAN
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 45 of 106
21FLORL Orlando Streets Drainage Stormwater Utility Bureau(Florida)
Source Procedure ID Procedure Name Citation
GEN PREP General Prep Method Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21FLORL
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 46 of 106
21FLPCSW PROJECT COAST - Southwest Florida Water Management District
Source Procedure ID Procedure Name Citation
PROJECT COAST Project Coast Field and Lab Analytical Procedures PASCO - Frazer, T.K., S.K. Notestein, J.A. Hale, M.V. Hoyer, D.E.Canfield, 2003, Water Quality Characteristics of the Nearshore GulfCoast Waters Adjacent to Pasco County, Florida, Southwest FloridaWater Management District, Methods Pg. 5
21FLPCSW
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 47 of 106
21FLPDEM Pinellas County Dept. of Environmental Management (Florida)
Source Procedure ID Procedure Name Citation
3005A
GEN PREP
LSP 001
Metals
General Preparation
Filtration of water samples, 0.45 micron
Pinellas County Department of Environmental Management, 1998, 1998Comprehensive Quality Assurance Plan, Pinellas County Department ofEnvironmental Management, 1
DEP-QA-001/92, 1992, Florida Department of Environmental ProtectionQA-001/92, DEP, Page 1of 3
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
21FLPDEM
21FLPDEM
21FLPDEM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 48 of 106
21FLPNS Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
351.2
365.4
200.2
3050
351.2
BIO
DIG-TKN-TP
LAB
SOP-BB02
SOP-HG-020
3050-B
3540-B
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Phosphorus, Total (as P)
Metals EPA Method 200.1
ICP Mass Spec for Metals in Sediment
351.2 (March 1983) TKN Prep
Methodology for Bacteria and Biological OxygenDemand
Preparation Method for TKN and TP
Methodology for Chemical Analysis
Preparation for Phytoplankton chlorophyll-a andphaeophytin by spectrophotometry
Mercury in Sediment
Acid Digestion of Sediments, Sludges, and Soils forMetals Analysis by FLAA/ICP or GFAA/ICPMS
Soxhlet Extraction for Nonvolatile and SemivolatileOrganic Compounds from Solids, Solid SamplesOnly
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP, UNK, USEPA - Modified, Central Lab, Unknown, unk
USEPA, 1990, Method 6020 CLP-M: Inductively Coupled Plasma-MassSpectrometry., USEPA, O1A0007861
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
FDEP, UNK, USEPA - Modified, Central Lab, Unknown, unk
FDEP, UNK, USEPA - Modified, Central Lab, Unknown, unk
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21FLFTM
21FLFTM
21FLPNS
21FLPNS
21FLPNS
21FLPNS
21FLPNS
21FLPNS
21FLPNS
21FLPNS
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 49 of 106
21FLPNS Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
3540-C
3550-B
Soxhlet Extraction for Nonvolatile and SemivolatileOrganics from Soils, Sludges, and Wastes
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 50 of 106
21FLPOLK Polk County Water Resources (Florida)
Source Procedure ID Procedure Name Citation
9230-C-2
LSP-01
3030-B
3030-D
3030-E
4500-NH3-B
9230-C-2
200.2
200.2-M
200.7-T
200.8-T
MT_PREP1
Enterococci (MF)
Nutrients
Preliminary Filtration of Metals Samples
Preliminary Digestion for Metal Samples
Nitric Acid Digestion of Metals
Preliminary Distillation for Ammonia in Water
Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Total Metals Preparation for EPA 200.2
Total Metals Preparation for EPA 200.8
Preparation of Metals Samples in Water
DEP Methods, 1992, DEP Standard Methods, DEP, ALL
DEP Methods, 1992, DEP Standard Methods, DEP, ALL
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
21FLPOLK
21FLPOLK
APHA
APHA
APHA
APHA
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 51 of 106
21FLSARA Sarasota County Environmental Services (Florida)
Source Procedure ID Procedure Name Citation
351.2
365.4
LSP-1
LSP-2
NO PREP
Nitrogen, Kjeldahl
Phosphorus Suite
Lab Procedure
Filtration
Lab Sample Prep (No Prep)
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
2 - Mote Marine Laboratory, 2006, Sarasota County, Ambient MonitoringProgram, 1998 to present., Mote Marine Laboratory, NA
2 - Mote Marine Laboratory, 2006, Sarasota County, Ambient MonitoringProgram, 1998 to present., Mote Marine Laboratory, NA
2 - Mote Marine Laboratory, 2006, Sarasota County, Ambient MonitoringProgram, 1998 to present., Mote Marine Laboratory, NA
21FLSARA
21FLSARA
21FLSARA
21FLSARA
21FLSARA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 52 of 106
21FLSEM Seminole County (Florida)
Source Procedure ID Procedure Name Citation
GEN PREP Standard Preperation Methods Used by HarborBranch
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21FLSEM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 53 of 106
21FLSFWM South Florida Water Management District
Source Procedure ID Procedure Name Citation
AZODIPH
BNA-SF
CARBALK
DIPHENYLHYDRA
ETHYL
GAMMA
GEC
GROSS
HAL1000
HAL1099
LP-1
MALE
METHYL
MFILT
SFWMD: Azobenzene/1-2-Diphenylhydrazine
LAB TEST: W-BNA-SF
SFWMD: Carbonate Alkalinity (CaCO3)
/1,2- Diphenylhydrazine
Ethyl
Gamma Count
Gross Error Count
Gross
SFWMD: Halowax 1000
SFWMD: Halowax 1099
LAB PREPARATION PROCEDURE
Male
Methyl
Membrane Filtrate
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 54 of 106
21FLSFWM South Florida Water Management District
Source Procedure ID Procedure Name Citation
NET
NITRODIPHE
ORGCOMP
SOMATIC
T60D
TITRATION
TRIBEN
UNSPECIFIED
VOC-SF
XIL1
XYL2
200.2
MT_PREP1
Net
SFWMD: N-Nitrosodiphenylamine/Diphenylamin
SFWMD: In Organic Compounds
Somatic
SFWMD: Temperature = 60 Deg C
Alkalinity by Titration
SFWMD: Trifluralin/Benfluralin
Unspecified BHC
LAB TEST: W-VOC-SF
SFWMD: Xylene
SFWMD: Xylenes (Total)
Preparation for Water, Soil, or Waste Samples
Preparation of Metals Samples in Water
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
21FLSFWM
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 55 of 106
21FLSJWM St. Johns Water Management District
Source Procedure ID Procedure Name Citation
ACID DIGEST
EPA 200.7
EPA 200.8
EPA 315.2
EPA 351.2
EPA 365.2
EPA 365.3
EPA 395.3
EPA 415.1
EPA METAL
EPA METALS
EPA3010
METHOD
NONE
SM 10200H
TP/TKN PREP
Acid Digest
EPA 200.8
EPA 200.8
EPA 315.2
EPA 351.2
EPA 365.2
EPA 365.3
EPA 395.3
EPA 415.1
EPA METAL
EPA METALS
EPA3010
METHOD
NONE
SM 10200H
TP/TKN Prep
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
Unknown, 19--, SJRWMD standard preparation methods, none, Vol--
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
21FLSJWM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 56 of 106
21FLTBW Tampa Bay Water
Source Procedure ID Procedure Name Citation
CHLA Chlorophyll Preparation American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
21FLTBW
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 57 of 106
21FLTPA Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
SOP-2 Standard Methods Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21FLTPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 58 of 106
21FLVEMD Volusa County Environmental Health Lab (Florida)
Source Procedure ID Procedure Name Citation
SOP-2
SOP-3
SOP-4
SOP-5
Determination of Ammonia Nitrogen by Semi-Automated Colorimetry
Determination of Total Kjeldahl Nitrogen by Semi-Automated Colorimetry
Determination of Nitrate-Nitrite Nitrogen byAutomated Colorimetry
Determination of Phosphorus by Semi-AutomatedColorimetry
USEPA, 1993, Methods for the Determination of Inorganic Substancesin Environmental Samples, USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination of Inorganic Substancesin Environmental Samples, USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination of Inorganic Substancesin Environmental Samples, USEPA, EPA 600/R-93-100
USEPA, 1993, Methods for the Determination of Inorganic Substancesin Environmental Samples, USEPA, EPA 600/R-93-100
21FLVEMD
21FLVEMD
21FLVEMD
21FLVEMD
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 59 of 106
21FLWPB Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
351.2
365.4
245.6
3050
351.2 MAR 83
3550B
365.4 (SED)
DEPSED SOP-003
DEPSED SOP-008
DEPSED SOP-012
DEPSED SOP-015
DEPSED SOP-019
DEPSED SOP-021
SOP-GC-002
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Phosphorus, Total (as P)
Fish Tissue Preparation Central Lab Tallahassee
Metals in Sediments
Preparation for Ammonia and TKN
Sediment
Preparation for Phosphorus, Total as P
Ammonia automated phenate method
chlorophyll determination
nitrate-nitrite determination
Preparation for Reactive Orthophosphate
total kjeldahl nitrogen
total phosphorus
Preparation for pesticides in water
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
FDEP Central Lab, 1999, FDEP SOP1, FDEP Central Lab, 1-1000
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
21FLFTM
21FLFTM
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
21FLWPB
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 60 of 106
21FLWPB Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
SOP-HG-020
200.2
3510-B
Mercury in Sediments
Preparation for Water, Soil, or Waste Samples
Separatory Funnel Extraction, Liquid-Liquid
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21FLWPB
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 61 of 106
21FLWQA Florida Department of Environmental Protection
Source Procedure ID Procedure Name Citation
351.2
365.4
SOP-BB02
DEP-SOP-BB02
DEP-SOP-NU-048
Preparation for Ammonia+Organic Nitrogen, Total(as N)
Preparation for Phosphorus, Total (as P)
Preparation for Chlorophyll-A (Monochromatic) &Pheophytin-A (Monochromatic)
Phytoplankton Sample Filtering for Chlorophyll aAnalysis
Preparation of Waters and Sediments for Nitrogenand Phosphorus Analysis; based on EPA methods351.2 and 365.4
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
FDEP-SOP - FDEP Envirionmental Assessment Section, Feb. 1, 2004,Department of Environmental Protection Standard OperatingProcedures for Field Activities DEP-SPO-001/01, Florida Department ofEnvironmental Protection, Feb.1, 2004 Revision
Florida DEP Central Laboratory, 19-, FDEP, Unknown, Unkown
Florida DEP Central Laboratory, 19-, FDEP, Unknown, Unkown
21FLFTM
21FLFTM
21FLFTM
21FLWQA
21FLWQA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 62 of 106
21GUAM Guam Environmental Protection Agency
Source Procedure ID Procedure Name Citation
GUAM-S01 Guam EPA Legacy Sample Preparation Procedures Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21GUAM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 63 of 106
21IOWA Iowa Dept. of Natural Resources
Source Procedure ID Procedure Name Citation
3510-B
3550-B
8150-P
Separatory Funnel Extraction, Liquid-Liquid
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
Herbicide Preparation Portion of 8150
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 64 of 106
21NEB001 Nebraska Dept. of Environmental Quality
Source Procedure ID Procedure Name Citation
CHLOROPHYLL A
3030-G
1311
1311-HG
1311-MT
1311-V
200.2
200.2-M
200.7-T
200.8-T
3005-A
Chlorophyll A preparation for analysis. Filtering
Nitric and Sulfuric Acid Digestion
TCLP Preparation for Semivolatiles
TCLP Preparation for Mercury
TCLP Preparation for Metals
TCLP Preparation ZHE
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Total Metals Preparation for EPA 200.2
Total Metals Preparation for EPA 200.8
Total Recoverable and Dissolved Prep for FLAA, ICP
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21NEB001
APHA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 65 of 106
21NEB001 Nebraska Dept. of Environmental Quality
Source Procedure ID Procedure Name Citation
3015
3040
3051
3510-B
3510-C
3540-B
3540-C
3550-A
3550-B
3580-A
Microwave Assisted Acid Digestion of AqueousSamples and Extracts
Oily Waste Prep for Soluble Metals by AA and ICP
Microwave Assisted Acid Digestion of Sediments,Sludges, Soils, and Oils
Separatory Funnel Extraction, Liquid-Liquid
Separatory Funnel Liquid-Liquid Estraction
Soxhlet Extraction for Nonvolatile and SemivolatileOrganic Compounds from Solids, Solid SamplesOnly
Soxhlet Extraction for Nonvolatile and SemivolatileOrganics from Soils, Sludges, and Wastes
Ultrasonic Extraction of Nonvolatile and SemivolatileOrganic Compounds form Soils, Sludges, andWastes
Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)
Waste Dilution
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 66 of 106
21NEB001 Nebraska Dept. of Environmental Quality
Source Procedure ID Procedure Name Citation
3585
50.6
5030-A
MT_PREP1
MT_PREP2
MT_PREP3
P-010-1
PAH-010
PCB-007
R-003-1
SFSAS_S_PREP
Waste Dilution
Phase Separation and Aliquotting
Sample Preparation and Extraction for VolatileOrganic Analysis by Purge-and Trap
Preparation of Metals Samples in Water
Preparation of Metals Samples in Soils
Sample Preparation Using Microwave Digestion
Preparation for Pesticides/PCB in Water/Soil
Preparation of Samples for PAH Analysis
Preparation of Samples for PCB Analysis
Preparation of Soil for Radiological Analysis
Sediment Preparation Technique
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 19--, CLP SOW for Inorganics Analysis-IHC01_3, USEPA,IHC01_3
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 67 of 106
21NJDEP1 NJ Department of Environmental Protection
Source Procedure ID Procedure Name Citation
350.2
351.3
365.2
4500-N
4500-CN(B)
4500-F-B
200.2-M
Ammonia (as N) Distillation
Kjeldahl Nitrogen (as N) Digestion and Distillation
Phoshporus (as P) Persulrate Digestion
Persulfate Method (proposed)
Preliminary Treatment of Cyanide Samples
Preliminary Distillation for Water Samples ContainingFluoride
Total Recoverable Metals Digestion
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
American Public Health Association, 199X, Stardard Methods for theExamination of Water and Wastewater, American Public HealthAssociation, 19th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
21NJDEP1
21NJDEP1
21NJDEP1
21NJDEP1
APHA
APHA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 68 of 106
21NYDECA NYS Dept. of EnCon, Division of Water
Source Procedure ID Procedure Name Citation
RIBS-BSED
RIBS-WCOL
RIBS-WCOL-FLT
RIBS Bottom Sediment Sample Collection
RIBS Water Column Sample Collection
RIBS Filtered Water Column Sample Collection
J.A.Myers, etal., 2000, Program Plan for Statewide Waters MonitoringProgram, NYSDEC, 47 pgs (plus append)
J.A.Myers, etal., 2000, Program Plan for Statewide Waters MonitoringProgram, NYSDEC, 47 pgs (plus append)
J.A.Myers, etal., 2000, Program Plan for Statewide Waters MonitoringProgram, NYSDEC, 47 pgs (plus append)
21NYDECA
21NYDECA
21NYDECA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 69 of 106
21SC60WQ SC Dept. of Health & Environmental Control
Source Procedure ID Procedure Name Citation
D3976 Std. Practice for Prep. of Sediment Samples forChemical Analysis
American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (II), American Society for Testingand Materials, Vol 11.02
ASTM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 70 of 106
21SCSANT Santee Cooper - South Carolina Public Service Authority
Source Procedure ID Procedure Name Citation
BACTERIA
CHPYL A
METAL
NUTRIENTS
SOLIDS
Bacteria Analysis Procedure
Chlorophyll a analysis
Metals Analysis Procedures
Nutrients Analysis Procedures
Total Dissolved Solids / Total Dissolved Solids
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
21SCSANT
21SCSANT
21SCSANT
21SCSANT
21SCSANT
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 71 of 106
21SDAK01 SD Dept of Environmental & Natural Resources
Source Procedure ID Procedure Name Citation
515TDS
CATION-ANION %
SAR
TDS
VISUAL
WRAP
Total Dissolved Solids
Cation-Anion Balance
SAR
TDS
VISUAL
Water Resources Assistance Program Procedure
USEPA, 1979, Methods for Analysis of Water., USEPA, EPA 600/4-79-020
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
21SDAK01
21SDAK01
21SDAK01
21SDAK01
21SDAK01
21SDAK01
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 72 of 106
21VASWCB Virginia Department of Environmental Quality (VADEQ)
Source Procedure ID Procedure Name Citation
D3987
3020-A
Shake Extraction of Solid Waste and Water
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis by GFAA Spectroscopy
American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (II), American Society for Testingand Materials, Vol 11.02
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
ASTM
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 73 of 106
22LAGWTR Louisiana Dept of Environmental Quality
Source Procedure ID Procedure Name Citation
BMP-FLD
HG-106
METAL-1
METAL-2
NUTRNT-1
PEST/PCB
PEST/PCB-2
SVOC-1
SVOC-2
VOC-1
VOC-2
WQ-1
Field Measurements
Merecury in Water (106)
Total Metals in Water
Total Metals in Water (106)
Nutrients in Water
Pesticides/PCB's in Water (8270C)
Pesticides/PCB's in Water (106)
SVOC's in Water (8270C)
SVOC's in Water (106)
VOC's in Water (8260B)
VOC's in Water (106)
Water Quality Parameters Prep
Baseline Monitoring Project, 1999, Baseline Monitoring Project, QualityAssurance Project Plan, LDEQ, 198pp
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1984, Guidelines Establishing Test Procedures for the Analysisof Pollutants Under the Clean Water Act, USEPA, 40CFR136
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1984, Guidelines Establishing Test Procedures for the Analysisof Pollutants Under the Clean Water Act, USEPA, 40CFR136
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1984, Guidelines Establishing Test Procedures for the Analysisof Pollutants Under the Clean Water Act, USEPA, 40CFR136
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
22LAGWTR
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 74 of 106
31DELRBC Delaware River Basin Commission
Source Procedure ID Procedure Name Citation
MT_PREP1
P-010-1
PAH-010
PCB-007
Preparation of Metals Samples in Water
Preparation for Pesticides/PCB in Water/Soil
Preparation of Samples for PAH Analysis
Preparation of Samples for PCB Analysis
USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 75 of 106
31ORWUNT Ohio River Sanitation Commission
Source Procedure ID Procedure Name Citation
200.2
245.1
3500CR D
9213D
9222D
Digestion, ICP, ICPMS
Mercury Digestion
Chromium Hexavalent
E. Coli
Fecal Coliform
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020
31ORWUNT
31ORWUNT
31ORWUNT
31ORWUNT
31ORWUNT
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 76 of 106
BUNKER Bunker Hill Mining and Metallurgical Complex
Source Procedure ID Procedure Name Citation
UNKNOWN
200.2
UNKNOWN
Preparation for Water, Soil, or Waste Samples
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
BUNKER
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 77 of 106
COE/ISU Des Moines River - Corp of Engineers (IOWA)
Source Procedure ID Procedure Name Citation
3030-E Nitric Acid Digestion of Metals American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 78 of 106
EMAP-CS Environmental Monitoring and Assessment Program
Source Procedure ID Procedure Name Citation
90%ACEX
ASE
ASTM1993
CHLA-NCA
EMAP-E
EPA 160.2
EPA245.5
EPA3051
EPA3052
EPA3052/3050B
Chlorophyll a filter suspended in 10ml of 90 %acetone until frozen
Accelerated Solvent Extraction
Standard guide for conducting 10-day static sedimenttoxicity tests w/marine organisms
Pigment extraction from filter with 90% acetone
Methods in EMAP 1995 Laboratory Methods Manual
Water sample filtered for TSS
Mercury in sediment (cold vapor with permanganatedigestion)
Strong acid microwave method
Microwave assisted acid digestion of siliceous andorganically based matrices
Microwave/hot plate assisted acid digestion ofsiliceous and organically based matrices
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
U.S. Environmental Protection Agency, 2001, EMAP-National CoastalAssessment Quality Assurance Project Plan 2001-2004, USEPA,NHEERL Gulf Ecology Division, Gulf Breeze, FL, 202 p
ASTM, 1993, Standard guide for conducting 10-day static sedimenttoxicity tests with marine and estuarine amphipods. E1367-92. In:Annual Book of ASTM Standards. Vol. 11.04. Philadelphia, PA, ASTM,pp. 1138-1163
J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 NutrientCollections/Chemistry Metadata, U.S. Environmental Protection Agency,10 p
U.S. EPA, 1995, EMAP: Laboratory Methods Manual-Estuaries, Volume1: Biological and Physical Analyses, Environmental Protection Agency,Office of Research and Development, Narragansett, RI, 128 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 79 of 106
EMAP-CS Environmental Monitoring and Assessment Program
Source Procedure ID Procedure Name Citation
HF/HNO3
HG-NCA
HNO3/HCL
HSGAS
MASE
MET-NCA
MGNO3
NA
NOTREC
NR
NUT-NCA
Total digestion using HF/HNO3 in an open beaker ona hot plate
Cold vapor AA for Hg (persulfate acid digestion)
Microwave digestion using HNO3/HCl in a closedteflon-lined pressure vessel
React sediment w/ hydrochloric acid; trap theevolved hydrogen sulfide gas
Microwave assisted solvent extraction
Sediment dried and completely digested innitric/hydrofluoric acids
Magnesium Nitrate addition w/ hydrochloric aciddigestion
Not analyzed
Procedure not recorded
Not relevant
Filtration operation using a 0.7 micron glass-fiberfilter
C. Strobel, 1996, EMAP-Estuaries 1993 Virginian Province SedimentChemistry Metadata, U.S. Environmental Protection Agency, 15 p
J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 SedimentChemistry Metadata, U.S. Environmental Protection Agency, 16 p
C. Strobel, 1996, EMAP-Estuaries 1993 Virginian Province SedimentChemistry Metadata, U.S. Environmental Protection Agency, 15 p
C. Strobel, 1996, EMAP-Estuaries 1993 Virginian Province SedimentChemistry Metadata, U.S. Environmental Protection Agency, 15 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 SedimentChemistry Metadata, U.S. Environmental Protection Agency, 16 p
State of California, 1986, Procedures for analysis of selenium andarsenic in fish and wildlife tissues with emphasis on quality control, Stateof California, Department of Fish and Game, Lab. Rpt 86-3
U.S. Environmental Protection Agency, 2001, EMAP-National CoastalAssessment Quality Assurance Project Plan 2001-2004, USEPA,NHEERL Gulf Ecology Division, Gulf Breeze, FL, 202 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
U.S. Environmental Protection Agency, 2001, EMAP-National CoastalAssessment Quality Assurance Project Plan 2001-2004, USEPA,NHEERL Gulf Ecology Division, Gulf Breeze, FL, 202 p
J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 NutrientCollections/Chemistry Metadata, U.S. Environmental Protection Agency,10 p
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 80 of 106
EMAP-CS Environmental Monitoring and Assessment Program
Source Procedure ID Procedure Name Citation
ORG-NCA
PSEP86
SE
SE(VP)
SM2540D
SM4500NH3
SM4500NO3
SM4500P
SOXHLET
TAAII
National Status and Trends Organic Methods
PSEP86: Sediment grain size
Solvent extraction
Soxhlet extraction and extract drying, concentrationand clean-up
SM2540D: EMAP-West CA 1999-2000 for TSS
SM4500NH3: EMAP-West CA 1999-2000 for NH4-Nand NO3-N
SM4500NO3: EMAP-West CA 1999-2000 for NO2
SM4500P: EMAP-West CA 1999-2000 for PO4
Soxhlet solvent extraction
Lab sample prep procedures for using a TechniconAutoAnalyzer II
Lauenstein, G. G. and A. Y. Cantillo (eds.), 1993, Sampling andanalytical methods of the National Status and Trends Program NationalBenthic Surveillance and Mussel Watch Projects 1984-1992:Comprehensive descriptions of trace organic analytical methods,Volume IV NOAA Technical Memorandum NOS ORCA 71, SilverSpring, MD., NOAA, Silver Spring, MD, 182 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
C. Strobel, 1996, EMAP-Estuaries 1993 Virginian Province SedimentChemistry Metadata, U.S. Environmental Protection Agency, 15 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
EMAP-CS
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 81 of 106
EMAP-CS Environmental Monitoring and Assessment Program
Source Procedure ID Procedure Name Citation
TOX-NCA
TSS-NCA
V-EPA245.5
3010-A
3020-A
Sediment toxicity test laboratory set-up
Water sample filtered
Method variation of EPA245.5 developed by VarianAnalytical Instruments
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis fy FLAA or ICPSpectrometry
Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis by GFAA Spectroscopy
U.S. EPA, 1995, EMAP: Laboratory Methods Manual-Estuaries, Volume1: Biological and Physical Analyses, Environmental Protection Agency,Office of Research and Development, Narragansett, RI, 128 p
J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 NutrientCollections/Chemistry Metadata, U.S. Environmental Protection Agency,10 p
Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
EMAP-CS
EMAP-CS
EMAP-CS
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 82 of 106
FWCLOCAL Florida Fish and Wildlife Conservation Commission (Florida)
Source Procedure ID Procedure Name Citation
4500-P-B(1)
4500-P-B(5)
3030-B
3030-E
4500-NH3(B)
4500-P-B(1)
4500-P-B(5)
Preliminary filtration for orthophosphorus 0.45ummembrane filter
Persulfate digestion for total phosphorus
Preliminary Filtration of Metals Samples
Nitric Acid Digestion of Metals
Preliminary Distillation Step
Preliminary filtration for othrhophosphorus 0.45ummembrane filter
Persulfate digestion for total phosphorus
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
21FLGFWF
21FLGFWF
APHA
APHA
APHA
FWCLOCAL
FWCLOCAL
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 83 of 106
HI301H City and county of Honolulu
Source Procedure ID Procedure Name Citation
3030-B
3030-E
NITRIC-PEROXIDE
PERSULF DIG
SPE
SPE-SGT
1625P
200.2
200.2-M
200.8-CR
Preliminary Filtration of Metals Samples
Nitric Acid Digestion of Metals
nitric acid and peroxide digestion for As and Se
Persulfate Digestion for Total Nitrogen
Solid Phase Extraction
solid phase extraction followed by fog removal by sgtcolumn
BNA (isotopic dilution) Preparation
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Clean Room Preparation for EPA 200.8
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
APHA
APHA
HI301H
HI301H
HI301H
HI301H
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 84 of 106
IL_EPA Illinois EPA
Source Procedure ID Procedure Name Citation
FIELD
LAB
ANALYZED IN FIELD
ANALYZED IN LAB
IEPA FIELD - Illinois EPA, 1994, Illinois EPA field methods manual,Illinois EPA, Sections B and H
IEPA LAB - Illinois EPA, 1993, IEPA Lab Methods Manual, Illinois EPA, Volumes 1 and 2
IL_EPA
IL_EPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 85 of 106
LAKELAND City of Lakeland (Florida)
Source Procedure ID Procedure Name Citation
2120 C
2540 C
2540 D
3111 B
3111 D
3113 B
4500-NH3-G
9222-B
9222-D
CHLA 4.3.1
EPA 310.1
Color in Water by Specrophotometry
FilterableTDS residues
Nonfilterable TSS Residues
CA/MG/FE/CD/ZN
ALUMINUM
Cr/aS/Pb/Se/Ag/Cu
AMMONIA IN WATER USING AUTOMATEDPHENOTE METHOD
Total Coliform analysis
Fecal Coliform Analysis
CHLOROPHYL A ANALYSIS
Alkalinity by Titration
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 86 of 106
LAKELAND City of Lakeland (Florida)
Source Procedure ID Procedure Name Citation
EPA 350.1
EPA 353.2
EPA 365.1
EPA 365.4
EPA6.4
NITROGEN
AMMONIA NITROGEN BY COLORIMETRY
NITRATE NITRITE NITROGEN BY COLORIMETRY
PHOSPHORUS BY COLORIMETRY
TOTAL PHOSPHORUS AFTER DIGESTION BLOCK
EPA Macroinvert Field & Lab methods for evaluatingBiological integrity of Surface Waters
TOTAL NITROGEN
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, 2000, Methods for the Determination of Organic and InorganicCompounds in Drinking Water, vol 1., USEPA, 815/R-00-014
USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008
USEPA, Donald J. Klemm, Philip A. Lewis, Florence Fulk, and James M.Lazorchak, 1990, Macroinvertebrate Field and Laboratory Methods forEvaluating the Biological Integrity of Surface Waters, USEPA,Environmental Monitoring Systems Laboratory- Cincinnati, Office ofResearch and Development, 600/4-90/030
City of Lakeland, 1999, Total Nitrogen, City of Lakeland, 1
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
LAKELAND
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 87 of 106
MDEDAT01 Maryland Dept. of the Environment Dredging Ambient Data
Source Procedure ID Procedure Name Citation
CBL001 Sample preparation of biotic tissue used byChesapeake Biological Laboratory - yr01
Jay C. Means, October 1982, "Data on Trace Organic Contaminants inWater, Sediments and the Biota". Assessment of the EnvironmentalImpacts of Construction and Operation of the Hart and Miller IslandsContainment Facility, 1981 - 1982, Chesapeake Research Consortium,VII, pp. 210-272
MDEDAT01
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 88 of 106
MDEDAT09 Maryland Dept. of the Environment Risk Assessment Data
Source Procedure ID Procedure Name Citation
200.7-T
P-010-1
PAH-010
PCB-007
SFSAS_FT_PREP
Total Metals Preparation for EPA 200.2
Preparation for Pesticides/PCB in Water/Soil
Preparation of Samples for PAH Analysis
Preparation of Samples for PCB Analysis
Fish Tissue Preparation Technique
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
USEPA
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 89 of 106
MDEQ-WQ Montana DEQ - Water Quality Division
Source Procedure ID Procedure Name Citation
4500-N-C
4500-P-B
TPN-4500-N-C
200.2
200.2-M
3051
3550-A
Persulfate Digestion
Sulfuric Acid and Persulfate Digestion SamplePreparation
Persulfate Nitrogen Method
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Microwave Assisted Acid Digestion of Sediments,Sludges, Soils, and Oils
Ultrasonic Extraction of Nonvolatile and SemivolatileOrganic Compounds form Soils, Sludges, andWastes
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
MDEQ-WQ
MDEQ-WQ
MDEQ-WQ
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 90 of 106
MNPCA1 Minnesota Pollution Control Agency
Source Procedure ID Procedure Name Citation
FLT CHL A Filtration of sample prior to lab delivery forchlorophyll analysis
Minnesota Pollution Control Agency Quality Assurance Program, 2000,www.pca.state.mn.us/programs/qa_p.html, Minnesota Pollution ControlAgency, all pages
MNPCA1
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 91 of 106
MONT-DEQ Montana Department of Environmental Quality
Source Procedure ID Procedure Name Citation
TPN-4500-N-C
3050-A
Persulfate Nitrogen Method
Acid Digestion of Sediments, Sludges, and Soils
American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
MONT-DEQ
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 92 of 106
MTWTRSHD Montana Watershed Data
Source Procedure ID Procedure Name Citation
200.2
200.2-M
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 93 of 106
MWRDSTOR Metropolitan Water Reclamation District of Greater Chicago
Source Procedure ID Procedure Name Citation
200.2 Preparation for Water, Soil, or Waste Samples USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 94 of 106
R2-LAB New York
Source Procedure ID Procedure Name Citation
D4638 Preparation of Biological Samples for InorganicChemical Analysis
American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (I), American Society for Testingand Materials, Vol 11.01
ASTM
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 95 of 106
R4ATHENS EPA Region 4 Athens Lab (Georgia)
Source Procedure ID Procedure Name Citation
103C
107C
245.1
245.5
300.0
3520C
3545
5030B
5035
ILM04.1
OLM04.2
200.2
103C
107C
245.1
245.5
300.0
3520C
3545
5030B
5035
ILM04.1
OLM04.2
Preparation for Water, Soil, or Waste Samples
ASB103C_MOD1 - USEPA, Region 4, Unknown, ASB103C, Mod 1.0,USEPA, Region 4, All
ASB107C - USEPA, Region 4, 2002, ASB107C,Nov 2002, USEPA,Region 4, All
245.1_REV3 - USEPA, Region 4, 1994, 245.1 Rev 3.0, May 1994,USEPA Region 4, All
245.5_REV2.3 - USEPA, Region 4, 1991, 245.5,Rev 2.3, Apr 1991,USEPA, Region 4, All
300.0_REV2.1 - USEPA, Region 4, 1993, 300.0 Rev 2.1, Aug 1993,Mod 1.0 Sep 2000, USEPA, Region 4, All
3520C_REV3 - USEPA, Region 4, 1996, 3520C Rev 3, Dec 1996, Mod1.0, USEPA, Region 4, All
3545_REV0 - USEPA, Region 4, 1996, 3545 Rev 0, Dec 1996, USEPA,Region 4, All
5030B_REV2 - USEPA, Region 4, 1996, 5030B Rev 2, Dec 1996,USEPA, Region 4, All
5035_REV0 - USEPA, Region 4, 1996, 5035 Rev 0, Dec 1996, USEPA,Region 4, All
ILM04.1 - USEPA, Region 4, Unknown, ILM04.1, USEPA, Region 4, All
OLM04.2 - USEPA, Region 4, Unknown, OLM04.2, USEPA, Region 4,All
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
R4ATHENS
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 96 of 106
SDWRAP SD Dept of Environmental & Natural Resources
Source Procedure ID Procedure Name Citation
SECCHI DISK SECCHI DISK TRANSPARENCY SDWRAP SOP - Watershed Assessment Team, June 2003, StandardOperating Procedure for Field Samplers Volume 1, State of SouthDakota, Voume 1
SDWRAP
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 97 of 106
SHELLYAB Shell Chemical Yabucoa (Puerto Rico)
Source Procedure ID Procedure Name Citation
3541
AQUA REGIA
HF DIGEST
3541
Aqua Regia Digest
HF DIGEST
6 - http://www.epa.gov/epaoswer/hazwaste/test/pdfs/8082.pdf, 1996,http://www.epa.gov/epaoswer/hazwaste/test/pdfs/8082.pdf,http://www.epa.gov/epaoswer/hazwaste/test/pdfs/8082.pdf, 8082-3
7 - http://www.cdc.gov/niosh/nmam/pdfs/7301.pdf, 2004, ELEMENTS byICP(Aqua Regia Ashing) - 7301, NIOSH Manual of Analytical Methods(NMAM), Fourth Edition, pp 8
8 - Government Geoscience Information Policy Advisory Committee(GGIPAC), 2004, AUSTRALIAN REQUIREMENTS FOR THESUBMISSION OF DIGITAL EXPLORATION DATA, GovernmentGeoscience Information Policy Advisory Committee (GGIPAC), pp 43
SHELLYAB
SHELLYAB
SHELLYAB
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 98 of 106
SRMTAKNY St. Regis Mohawk Tribe (New York)
Source Procedure ID Procedure Name Citation
PCB-007
SFSAS_FT_PREP
SFSAS_S_PREP
Preparation of Samples for PCB Analysis
Fish Tissue Preparation Technique
Sediment Preparation Technique
USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 99 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
3030-C
3030-D
% SOLIDS
A.12
A.18.1
A.18.2
A.18.4
A.18.8
A.18.8.1
A.18.9.1
A.19.1
Treatment for Acid-Extractable Metals
Preliminary Digestion for Metal Samples
Percent Solids
Total Hardness - State of Tennessee EnvironmentalLaboratories
Ammonia - State of Tennessee EnvironmentalLaboratories
Ammonia, sediment
NO3 & NO2 - State of Tennessee EnvironmentalLaboratories
Total Kjeldahl Nitrogen - State of TennesseeEnvironmental Laboratories
Total Kjeldahl Nitrogen, sediment
Total Phosphate - State of Tennessee EnvironmentalLaboratories
Oil and grease, sediment
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
APHA
APHA
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 100 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
A.19.2
A.2
A.23.1
A.24.2
A.24.3
A.3
A.6
A.9
EPA 200.7
EPA 200.9
EPA 202.1
TPH Total Petroleum Hydrocarbons - sediment
BOD, 5-day - State of Tennessee EnvironmentalLaboratories
Total Phenols, sediment
Suspended Residue - State of TennesseeEnvironmental Laboratories
Dissolved Residue - State of TennesseeEnvironmental Laboratories
Boron, sediment
Low COD - State of Tennessee EnvironmentalLaboratories
Cyanide - State of Tennessee EnvironmentalLaboratories
Lithium
Metals - EPA
Aluminum by FLAA
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 101 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
EPA 206.2
EPA 208.1
EPA 213.1
EPA 215.1
EPA 218.1
EPA 219.1
EPA 220.1
EPA 236.1
EPA 236.2
EPA 239.1
EPA 242.1
Arsenic sediment
Barium, sediment
Cadmium, sediment
Calcium, sediment
Chromium, sediment
Cobalt, sediment
Copper, sediment
Iron
Iron sediment
Lead, sediment
Magnesium, sediment
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
USEPA, 1991, Methods for the Determination of Metals inEnvironmental Samples, USEPA, EPA 600/4-91-010
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 102 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
EPA 243.1
EPA 243.2
EPA 245.1
EPA 245.5
EPA 249.1
EPA 249.2
EPA 258.1
EPA 270.3
EPA 272.1
EPA 273.1
EPA 289.1
Manganese
Manganese sediment
Mercury - EPA
Mercury, sediment
Nickel, sediment
Nickel by GFAA
Potassium
Selenium
Silver
Sodium, sediment
Zinc
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 103 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
EPA 289.2
EPA 375.4
MS
MS+ECD
PARTSIZE
R.1.3
R.6
SM 9000
SM 9222-D
SM 9230-B
Zinc sediment
Sulfate by Turbidimetric Determination
Mass spec for extractable organics
Mass spec & electron capture for extractableorganics
Particle Size Distribution of Sediment
Gross Alpha & Beta, State of TennesseeEnvironmental Laboratory Services
Gamma Radionuclides, State of TennesseeEnvironmental Laboratories
E. Coli, Enterococcus - Standard Methods 9000
Fecal Coliform - Membrane filter procedure
Fecal Strep
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
TDECDOE
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 104 of 106
TDECDOE Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
TOC
200.2
200.2-M
200.7-T
200.8-T
EPA 9060 Total Organic Carbon (TOC)
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Total Metals Preparation for EPA 200.2
Total Metals Preparation for EPA 200.8
Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
TDECDOE
USEPA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 105 of 106
TDECWPC Tennessee Department of Environment and Conservation
Source Procedure ID Procedure Name Citation
3030-C
3030-D
4500-NH3-B
200.2
200.2-M
200.7-T
Treatment for Acid-Extractable Metals
Preliminary Digestion for Metal Samples
Preliminary Distillation for Ammonia in Water
Preparation for Water, Soil, or Waste Samples
Total Recoverable Metals Digestion
Total Metals Preparation for EPA 200.2
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III
APHA
APHA
APHA
USEPA
USEPA
USEPA
December 14, 2007 09:23:58Lab Sample Preparation Procedures
Page 106 of 106
USVIST Government US Virgin Islands
Source Procedure ID Procedure Name Citation
9230-C-2 Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation
American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition
APHA