introduction to the hplc chemstation - chemical analysis ...· •he structure of the chemstation

Download Introduction to the HPLC ChemStation - Chemical Analysis ...· •he structure of the ChemStation

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  • Introduction to the HPLC ChemStation

  • 2

    In This Section, We Will Discuss:

    The structure of the ChemStation Software.

    How to use the ChemStation Configuration Editor.

    How to open the ChemStation .

    ChemStation Explorer and Views.

    Preferences.

    How to set up user access levels.

    How to use the Scheduler.

    How to maintain the computer system.

  • 3

    Directory Structure of ChemStation Software

    Instrument #

    Spectral Libraries

    Report Templates

    UV Spectra UV Signal

    Chromatograms

    Logbook for Run

    DEFAULT.D

    ACQRES.REG DAD1.UV DAD1A.CH GLPSAVE.REG LCDIAG.REG RUN.LOG SAMPLE.MAC

    005-0101.D

    DEMO

    DATA METHODS SEQUENCE TEMP VERIFY

    1 BACKUP Core REPSTYLE SPECLIBS

    Chem32

    C:

    SINGLE.B

    Master Methods

    Sequence Templates

  • 4

    Sequence Data Structure

    Sequence Container (Folder)

    Subdirectory sequencetemplatename year-month-day hour-minute-second

    C:\Chem32\1\DATA\03-15-06\CLASSSEQUENCE 2006-03-15 10-46-09

    Copy of Sequence Template

    Copy of Master Method

    Acquired Data

    Batch file for Batch Review

    Sequence Logbook

  • 5

    File Naming Conventions

    Forbidden characters for filenames:

    . / \ : []| + ; , ? = * < >@#%

    Type

    Max

    Input

    Length

    Auto

    AppendExample

    DataFile Name 38 .D Demodad.d

    DataFile Name using prefix & counter 15 .D longname000001.d

    Method 40 .M def_lc.m

    Sequence 40 .S def_lc.s

    Hypersequence 40 .HYP def_lc.hyp

    Batch 40 .B batch.b

    Libraries 40 .UVL demodad.uvl

    Customized Report Template 40 .FRP areapct.frp

    Datafile subdirectory 40 demo

    Data sequence subdirectory 40 demo

    Sequence Data Container Name 40 test_date_time

    Revision

    B.01

    and

    higher

    Note: Revisions A.0X files are limited to eight characters.

  • 6

    The HPLC ChemStation Software

    Add Instruments

    Schedule ChemStation Tasks

    Access Instrument

    and Software

  • 7

    ChemStation

    6890 Series

    GC

    System

    HEWLET

    TPACKAR

    D7673B

    AUTOMATIC

    SAMPLER

    STAR

    T

    STO

    P

    FAUL

    T

    RU

    N

    READ

    Y

    35900E8453

    6890 System1100/1200

    System

    ChemStation

    Existing LAN Backbone

    LAN Configuration with Existing Network

  • 8

    Instrument Configuration

    Select Instrument Type Select LAN and Add IP Address

  • 9

    Default paths for data

    files, methods, and

    sequences.

    Configure Paths

  • 10

    Configure Custom Colors

  • 11

    Configuration - When Entering the ChemStation

  • 12

    Method and Run Control View

    Sampling

    Diagram

    System

    Diagram

    Online Plot

    Navigation Pane

    ChemStation Explorer

    Navigation Buttons

  • 13

    ChemStation Explorer Views

  • 14

    ChemStation Views ViewsMethod and Run Control

    Data Analysis

    Report Layout

    Verification (OQ/PV)

    Diagnosis

    Full menu or Short menu

    Change

    Views

  • 15

    Navigation Pane Customization

  • 16

    View Preferences Allows you to configure the contents of theChemStation Explorer

    Specifies naming convention for sequence

    data containers

    Specifies how signals are loaded

  • 17

    Change Access Level

    Manager Level - Access to all

    capabilities.

    Operator Level - Cannot edit

    and save a method.

  • 18

    Access from:

    View menu

    Start, All Programs,

    Agilent ChemStation

    ChemStation Scheduler

  • 19

    Delete temporary files on a regular basis. Use Clean Disk for Windows 2000 and XP.

    Use Checkdisk to find and correct errors on the disk.

    Defragment the hard drive.

    Use Virus detection software.

    Create an Emergency Repair disk.

    Maintaining the Computer System

    Accessories

    Right-click drive letter

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