gc section - allpump.co.kr · copyright 2004 alltech associates, inc. ®™ ™™™-™...

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

329328

328

GC SectionGC Columns .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..328-384

Introduction .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..329-330

Capillary Columns, Alltech .. .. .. .. .. .. .. ..331-352

Custom Columns .. .. .. .. .. .. .. .. .. .. .. .. .. 331

Heliflex® .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..332-349

Econo-Cap™ .. .. .. .. .. .. .. .. .. .. .. .. .. ..333-341

EPA Methods Guide .. .. .. .. .. .. .. .. .. ..350-352

Capillary Columns, Other .. .. .. .. .. .. .. ..353-364

Astec, Agilent/J&W, SGE, Quadrex®

Packed Columns .. .. .. .. .. .. .. .. .. .. .. .. ..365-384

Packed Columns .. .. .. .. .. .. .. .. .. .. ..365-367

Custom Packings .. .. .. .. .. .. .. .. .. .. ..368-371

Empty Columns & Supports .. .. .. .. ..372-384

GC Accessories .. .. .. .. .. .. .. .. .. .. .. ..385-443

Capillary Accessories .. .. .. .. .. .. .. .. .. ..385-387

Packed Accessories .. .. .. .. .. .. .. .. .. .. ..388-389

Gas Management

Gas Flow .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..390-397

Purifiers .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..398-409

Pressure Regulators .. .. .. .. .. .. .. .. .. .. .. 410

Gas Sampling .. .. .. .. .. .. .. .. .. .. .. .. ..411-414

Ferrules .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..415-416

Fittings & Tubing .. .. .. .. .. .. .. .. .. .. .. .. ..417-426

Injection Liners & Accessories .. .. .. .. .. ..427-429

Kits .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. 430

Septa .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..431-436

Tools & Organizers .. .. .. .. .. .. .. .. .. .. .. ..437-438

Valves .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..439-443

GC Instruments .. .. .. .. .. .. .. .. .. .. .. .. ..444-460

GC Systems & Data Collection .. .. .. .. .. ..444-450

Gas Generators

Hydrogen .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..451-453

Air .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..454-455

Nitrogen .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. ..456-458

Air Compressors .. .. .. .. .. .. .. .. .. .. ..459-460

Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

329

Alltech Capillary Columns

Helifl ex® Capillary Column Line• High performance individually tested columns• Choice of 5" or 7" rugged cage • Most complete selection of phases• Custom columns available to suit your specifi c

application

Helifl ex® Capillary Columns are manufactured from the highest quality polyimide coated synthetic fused silica. They are mounted on a rugged wear-resistant cage. Each Helifl ex® Column is individually tested to guarantee column performance and comes with a test chromatogram, instruction manual, capillary end caps, and a free ceramic column cutter.

Note: Column nuts and ferrules are not included. If the column you need is not available in our standard offering, request a custom Helifl ex® Column made to your individual specifi cations.

Econo-Cap™ Capillary Column Line• Best value in capillary columns anywhere• Batch tested to dramatically reduce price• Ideal for aggressive applications• Available in the most popular phases

We’ve taken our most popular capillary columns and perfected the manufacturing procedure to the point that reproducibility is assured. This allows us to test these columns in batches instead of individually, while still offering an unconditional guarantee. Batch testing signifi cantly reduces cost in production without sacrifi cing quality.

Each Econo-Cap™ Capillary Column comes with a copy of the batch test results, an instruction manual, and capillary end caps. If you are not completely satisfi ed with the quality of your Econo-Cap™ Capillary Column it will be replaced at no charge.

Note: Column nuts and ferrules are not included.

Capillary Columns IntroductionC O L U M N S

What do I need to consider when selecting a GC column?

• Internal diameter - Selection is based on sample concentration and instrumentation. Narrow bore(0.1mm-0.2mm) are ideal for MS, and wide bore (.53mm) are ideal for purge and trap applications.

• Film thickness - Film thickness has a direct affect on retention of the compound. A thicker fi lm thickness retains the compound longer, and a thinner fi lm decreases retention.

• Column Length - The column length affects both the resolution and the rate of analysis. A longer column provides better resolution, but doubling the column length will double the time of analysis(isothermal conditions).

• Stationary Phase - The most important consideration is the stationary phase; this is dependent upon the polarity of the compound, property of the column, and standard methods referenced,

- All Alltech columns are presented with their USP designations to help you easilymake a selection.

- The GC Application section (p. 522-556) offers proven methods for analysis.Seewww.alltechweb.com for a complete listing.

- Questions on stationary phase selection? Call Technical Service; we are ready toassist you with your application questions.

Best value in capillary columns anywhereBest value in capillary columns anywhere

Alltech Capillary Column Families

5382

Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech office or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

330 331

Capillary Column Phase Cross ReferenceUse the chart below to cross reference manufacturers’ stationary phases as well as USP method designations to

Alltech equivalent columns. Slight variations in selectivity may result between different manufacturers’ columns.

Alltech Standard Phase Cross Reference

Standard Phase Cross Reference

COMPOSITION ALLTECHUSP

DESIGNATION SIMILIAR PHASES

100% Dimethylpolysiloxane AT™-1ms G1, G2, G38

DB™-1ms, HP™-1ms, Rtx-1ms, CP-Sil,5CB low Bleed/ms

100% Dimethylpolysiloxane AT™-1ht, AT™-1,EC™-1

G1, G2, G38

007-1, CP-Sil 5CB, DB™-1, DB-1ht,HP™-1,HP- 101,

OV™-1, RSL™-150,RSL-160, Rtx™-1, SE-30™, SPB™-1,SPB-Sulfur,ULTRA™-1, SP-2100, BP-1, DC-200, PE-1, ZB-1

5% Phenyl equivalentPolysilphenylene-Siloxane

AT™-5ms DB™-5ms, Rtx™-5Sil ms, BPX-5, 007-5ms, HP™-5ms

(5% Phenyl)- 95% methylpolysiloxane

AT™-5,EC™-5

G27,G36

007-2, CP-Sil 8CB, DB™-5, D™B-5.625, DB™-5ht, HP™-5,HP™-5ms, OV™-5, PTE-5, PTE-5QTM, PAS-5, RSL-200,Rtx™-5,Rtx™-5ms, SAC-5, SE-54, SPB-5, ULTRA-2, XTI-5, SE-52, BP-5, PE-2, ZB-5

(20% Phenyl)- 80% methylpolysiloxane

AT™-20,EC™-20

G28,G32

007-7, Rtx™-20, SPB-20, VOCOL, PE-7

(35 Phenyl)-65% Methylpolysiloxane

AT™-35msAT™-35

G42 DB-35ms, Rtx-35, SPB-35, SUP-HERB, MDN-35, BPX-35

007-11, DB™-35, DB™-35ms, HP™-35, RSL-300, Rtx™-35,SPB-35, SPB-608, OV™-11, PE-35, Sup-Herb

(50 Phenyl)-50% methylpolysiloxane

AT™-50msAT™-50htAT™-50

G3 DB –17ms, H5-50+, Rtx-50, SP-2250, SPB-50, SPB-17, BPX-50

DB-17ht, Rtx-65TG, BPX-50, CP-TAB-CB,

007-17, DB-17, DB-17ht, HP™-17, HP™-50+, Rtx™-50SP-50, SP-2250, SPB-50, CP Sil 24CB, PE-17, ZB-50

(6% Cyanopropylphenyl)-94% methylpolysiloxane

AT™-624AT™-1301

G43 007-1301, DB™-624, DB™-1301, HP™-1301, HP™-624,

Rtx™-1301, Rtx™-624, SPB-1301, SPB-624, 007-624, ZB-624(14% Cyanopropylphenyl)-86% methylpolysiloxane

AT™-1701 007-1701, CP-Sil 19CB, DB-1701, HP™-1701, OV™-1701,PAS-1701, Rtx™-1701, SPB-1701, BP-10, ZB-1701

Trifluoropropylmethyl polysiloxane

AT™-210 G6 DB™-210, RSL-400, Rtx™-200, OV™-202, OV™-210,OV™-215, QF-1, SP-2401

(50% Cyanopropylphenyl)-50% methylpolysiloxane

AT™-225 G7 007-225, CP-Sil43CB, DB™-225, HP™-225, OV™-225,RSL-500,Rtx™-225, BP-225, PE-225

(50% Cyanopropyl)-50% methylpolysiloxane

AT™-SILAR G5 DB™-23, 007-23, PE-23, Rtx™-2330, SP 2330

poly(80% bis cyanopropyl)-20% cyanoproylphenyl siloxane

AT™-SILAR-90 G8 DB-23, CP-Sil84, Rtx-2330, SP-2330

poly(biscyanopropylsiloxane)

AT™-SILAR-100 G5 CP-Sil88, Rtx-2330, SP-2340

Polyethyleneglycol AT™-WAXmsAT™-WAXAT™-AquaWaxEC™-WAX

G14,G15

G16,G20,

G39

DB-WAX, Rtx-WAX, SUPELCOWAX-10

007-CW, Carbowax® 20M, CP-Wax 52CB, DB™-WAXetr,

DB™-WAX, Rtx™-WAX, HP-20M, HP™-Wax, Innowax™,

Omegawax, Stabilwax®, SUPELCOWAX®-10, SUPEROX® II, BP-20, ZB-WAX

PolyethyleneglycolAcid Modified

AT™-1000,EC™-1000,AT™-AquaWax-DA

G25,G35

007-FFAP, CP-Wax 58CB, DB™-FFAP, HP™-FFAP, Nukol™,OV™-351, SP-1000, Stabilwax-DA, SUPEROX-FA, BP-21

PolyethyleneglycolBase Modified

AT™-CAM Stabilwax®-DB, CAM, Carbowax® Amine, CP Wax 51

PONA Analysis AT™-Petro 007-1-100-0.5F, CP-Sil PONA CB, DB™-Petro100, Petrocol DH, PONA, Ttx-1PONA, HP-PONA

ASTM Method 2887 AT™-2887 007-1-10V-1.0F, DB™-2887, Petrocol 2887, Petrocol EX2887, Rtx-2887, Sim-Dist-CB

ASTM Method 3710 AT™-3710 Petrocol 3710

Capillary Columns IntroductionC O L U M N S


330 331

• A wide selection of stationary phases• Lengths from 1 to 105 meters• Wide selection of i.d. tubing• Every column individually tested

Custom Capillary Column Instructions 1. Stationary Phase: Choose a Phase in

"Table 1: Custom Phase."2. Length & Internal Diameter: Choose any length (1 to 105 meters) and internal diameter (0.10mm to 0.53mm) from in "Table 2: Custom Dimensions."3. Film Thickness: Choose a film thickness; 0.01µm tolerance.4. See Coiling and Guard Information for additional options.5. Call Customer Service and they will confirm your order and provide exact prices.

Alltech Specialty Columns Cross Reference

ALLTECH HELIFLEX® CUSTOM CAPILLARY COLUMNSLENGTH I.D. DESCRIPTION PART NO. PRICE

1-5m 0.10mm Specify Phase & Film 9710010.18mm Specify Phase & Film 9710050.25mm Specify Phase & Film 9720100.32mm Specify Phase & Film 9730100.45mm Specify Phase & Film 9740100.53mm Specify Phase & Film 975010



31-60m 0.18mm Specify Phase & Film 9710500.25mm Specify Phase & Film 9720600.32mm Specify Phase & Film 9730600.45mm Specify Phase & Film 9740600.53mm Specify Phase & Film 975060

61-105m 0.25mm Specify Phase & Film 9721050.32mm Specify Phase & Film 9731050.45mm Specify Phase & Film 9741050.53mm Specify Phase & Film 975105

Custom CapillaryAll other Dimensions not specified 970123

CUSTOM COILINGDESCRIPTION PART NO. PRICE

Custom Capillary on 4" Cage 970124Custom Capillary on 5" Cage 970125

Custom Capillary Column with Integral GuardCUSTOM CAPILLARY COLUMN WITH INTEGRAL GUARD

DESCRIPTION PART NO. PRICE

Custom 0.25mm i.d. w/Integral 5m Guard C-5400Custom 0.32mm i.d. w/Integral 5m Guard C-5500Custom 0.53mm i.d. w/Integral 5m Guard C-5600

Specialty Phases Cross ReferenceEPA Method 608 AT™-Pesticide 007-608, DB™-608, HP™-608, SPB-608EPA Method 502.2 AT™-502.2 007-624, 007-502, DB-502.2, DB™-VRX, HP™-624,

HP™-VOC,MST-502.2, MXT-624, MXT-Volatiles, OV-624, Rtx-502.2,Rtx™-624,

Rtx™-Volatiles, VOCOLSulfur Analysis AT™-Sulfur SPB-1 SULFURFAME Analysis AT™-FAME FAMEWAX, OmegaWAX


Phases Available for Custom Capillary ColumnsAquawax Dexsil® 400 OV™-17Aquawax-DA Dexsil® 410 OV™-1701AT™-1 Di (2ethylhexyl OV™-25AT™-5 phthalate OV™-61AT™-20 Diisodecyl

phthalateOV™-73

AT™-35 FFAP OV™-101AT™-1000 Hi-Eff®-1AP OV™-105AT™-1301 Hi-Eff®-1BP OV™-210AT™-1701 Hi-Eff®-2AP OV™-351AT™-WAX Hi-Eff®-2BP PolyvinylpyrrolidoneAT™-Amine Hi-Eff®-3AP QF-1Apiezon® phases Hi-Eff®-3BP Reoplex®400Apolane®-87 Hi-Eff®-4BP SE-30Butanediol succinate Hi-Eff®-8BP Squalane(Craig’s polyester) Hi-Eff®-10BP Superox-FACarbowax® phases Igepal CO-880 XE-60DC-550 OV™-1Dexsil® 300 OV™-11

C O L U M N S

Custom Capillary Coiling

Table 2: Custom Dimensions

Table 1: Custom Phases

Alltech Custom Capillary Columns

Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc. Contact your Alltech offi ce or distributor for current or local prices.© Copyright 2004 Alltech Associates, Inc.

332 333

Helifl ex® AT™-1ms• Guaranteed low bleed characteristics• Specifi cally designed for mass spec analysis• Highly inert• Similar to DB-1ms, HP-1ms, Rtx-1ms, CP-Sil 5 CB Low

Bleed/MS, MDN-1.

AT™-1ms is a line of high-performance low bleed non-polar columns designed specifi cally for use with mass spectrometers. They are ideal for pharmaceutical, environmental, petrochemical, and food and fragrance analysis, or any GC/MS analysis requiring a 100% dimethylpolysiloxane-type polarity capillary column.

Helifl ex® AT™-1htShorten your analysis time with high temperature/low bleed columns

• Faster analysis time for high boiling compounds• Better peak detection at lower concentrations• Individually bleed tested at 380ºC• Similar to 007-1, CP-Sil 5CB, DBTM-1, DB-1ht, HPTM-

1, HP-101,OVTM-1,RSLTM-150, RSL-160, RtxTM-1, SE-30TM, SPBTM-1, SPB-Sulfur,ULTRATM-1, SP-2100, BP-1, DC-200, PE-1, ZB-1

HELIFLEX AT™-1MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.25µm -60/360°C 158800.32mm 0.25µm -60/360°C 15882

30m 0.25mm 0.10µm -60/360°C 158840.25mm 0.25µm -60/360°C 158970.25mm 0.25µm -60/360°C 15735*0.32mm 0.10µm -60/360°C 159220.32mm 0.25µm -60/360°C 159380.32mm 0.25µm -60/360°C 15739*

60m 0.25mm 0.25µm -60/360°C 159410.32mm 0.25µm -60/360°C 15944

Figure 1 - AT™-1ms Low Bleed

Column: Helifl ex® AT™-1ms, 30m x 0.25mm x 0.25µm (Part No. 15897) Temp: 135°C (20 min hold) to 320°C (10 min hold) at 20°C/min Carrier Gas: Helium at 0.65mL/min (23.1cm/sec) Detector: FID

��

�

�

�

�

�

�

��

�

� ��

1. 2-Ethylhexanoic Acid 2. 4-Chlorophenol 3. 1,7-Heptanediol 4. n-Tridecane 5. 1-Undecanol 6. n-Tetradecane 7. Dicyclohexylamine 8. Acenaphthylene 9. n-Pentadecane

*Equipped with uncoated 5m integral guard column. Total column length is35 meters.

C O L U M N S


HELIFLEX® AT™-1HT GC CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.1µm -60 - 380/400°C 1636730m 0.25mm 0.1µm -60 - 380/400°C 1636860m 0.25mm 0.1µm -60 - 380/400°C 16369

Column: Helifl ex® AT™-1ht, 30m x 0.25mm x 0.10µm (Part No. 16368)Column Temp: 125ºC (hold 25 min) to 380ºC at 20ºC/minCarrier Gas: Helium at 26.3cm/secDetector: FID at 390ºC

QC Test Chromatogram - Bleed Profi le

0

1

2

3

45

67

3.4 pA

5 10 15 20 25 30 35 40 45 50 Min.

3. 4-Chlorophenol 4. n-Pentadecane 5. Fluorene 6. Anthracene 7. n-Heptadecane

1. 1-Undecanol 2. Dicyclohexylamine

Specifi cationsPhase: 100% DimethylpolysiloxanePolarity: Non-polarMax. Temp.: 340/360°CUSP Designation: G1, G2, G38Ideal for: Mass Spec Analysis for Environmental, PAH, CLP

Pesticides, Steroids and Drugs

Specifi cationsPhase: 100% DimethylpolysiloxanePolarity: Non-polarMax. Temp.: 380/400°CUSP Designation: G1, G2, G38Ideal for: High Boiling Compounds Waxes, Crude Oils, and

Trigylcerides

2578 2634

For more Capillary GC Applications, See the GC Applications Section p522-556.

To view Alltech's complete chromatogram library, visit www.chromatography.com

Shorten your analysis time with high Shorten your analysis time with high


332 333

Specifi cationsPhase: 100% DimethylpolysiloxanePolarity: Non-polar General Purpose ColumnUSP Designation: G1, G2, G38Ideal for: General Purpose

Helifl ex® AT™-1• Excellent general purpose columns• Similar to DB™-1, Rtx™-1, SPB™-1, SPB-Sulfur, SP™-

2100, HP™-1, HP™-101, ULTRA™-1, BP™-1, CP-Sil™-5-CB, 007™-1, OV™-1, SE™-30, DC™-200, RSL™-150, RSL-160, PE-1, ZB-1

HELIFLEX® AT™-1 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

10m 0.25mm 0.20µm -60/350°C 9325100.25mm 0.25µm -60/350°C 137520.25mm 0.10µm -60/350°C 168660.32mm 0.10µm -60/350°C 168680.32mm 0.25µm -60/350°C 137550.32mm 0.30µm -60/350°C 9332100.53mm 0.25µm -60/350°C 168400.53mm 1.20µm -60/350°C 9351100.53mm 2.65µm -60/300°C 168490.53mm 5.00µm -60/300°C 16842

15m 0.25mm 0.10µm -60/350°C 136490.25mm 0.20µm -60/350°C 9325150.25mm 0.25µm -60/350°C 137530.25mm 1.00µm -60/350°C 136530.32mm 0.10µm -60/350°C 136730.32mm 0.25µm -60/350°C 137570.32mm 0.30µm -60/350°C 9332150.32mm 1.00µm -60/350°C 136980.32mm 3.00µm -60/350°C 137010.32mm 5.00µm -60/300°C 168360.53mm 0.15µm -60/350°C 139450.53mm 0.25µm -60/350°C 141940.53mm 0.50µm -60/350°C 140300.53mm 1.00µm -60/350°C 135050.53mm 1.20µm -60/350°C 9351150.53mm 1.50µm -60/330°C 139050.53mm 2.65µm -60/300°C 168750.53mm 3.00µm -60/300°C 138930.53mm 5.00µm -60/300°C 16851

25m 0.25mm 0.20µm -60/350°C 9325250.32mm 0.30µm -60/350°C 9332250.53mm 1.20µm -60/350°C 935125

30m 0.25mm 0.10µm -60/350°C 136630.25mm 0.20µm -60/350°C 9325300.25mm 0.25µm -60/350°C 136380.25mm 1.00µm -60/350°C 136390.32mm 0.10µm -60/350°C 136990.32mm 0.25µm -60/350°C 136400.32mm 0.30µm -60/350°C 9332300.32mm 1.00µm -60/350°C 136410.32mm 3.00µm -60/300°C 137020.32mm 5.00µm -60/300°C 168380.53mm 0.50µm -60/350°C 140380.53mm 1.00µm -60/350°C 135150.53mm 1.20µm -60/350°C 9351300.53mm 1.50µm -60/330°C 13908

HELIFLEX® AT™-1™ CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE





HELIFLEX® AT™-1 CAPILLARY COLUMNS ON 5" CAGELENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.25µm -60/350°C 1375350.32mm 0.25µm -60/350°C 1375750.32mm 1.00µm -60/350°C 1369850.53mm 1.00µm -60/350°C 1350550.53mm 1.50µm -60/350°C 139055


C O L U M N S


ECONO-CAP™ EC™-1 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO.10m 0.53mm 2.65µm -60/350°C 1967815m 0.53mm 1.00µm -60/350°C 19662

0.45mm 1.00µm -60/350°C 196420.53mm 1.20µm -60/350°C 19650

30m 0.25mm 0.25µm -60/350°C 196520.32mm 0.25µm -60/350°C 196510.32mm 1.00µm -60/350°C 196600.45mm 1.00µm -60/350°C 196440.53mm 1.00µm -60/350°C 196640.53mm 1.20µm -60/350°C 19656

ECONO-CAP™ EC™-1 CAPILLARY COLUMNS, SIX PACKLENGTH I.D. FILM TEMP. LIMITS PART NO.30m 0.25mm .25µm -60/350°C 19652630m 0.32mm .25µm -60/350°C 19651630m 0.53mm 1.20µm -60/350°C 196566

Econo Cap™ EC-1• Batch tested to dramatically reduce price

PART NO. PRICE

PART NO. PRICE

Batch tested to dramatically reduce priceBatch tested to dramatically reduce price


334 335

Helifl ex® AT™-5ms• Similar to DB™-5ms, Rtx®-5 Sil ms,

HP™-5TA, BPX-5, 007-5ms

HELIFLEX® AT™-5MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.25µm -60-325/350°C 1580130m 0.25mm 0.10µm -60-325/350°C 15806

0.25mm 0.25µm -60-325/350°C 158070.25mm 0.25µm -60-325/350°C 15881*0.25mm 0.50µm -60-325/350°C 158080.25mm 0.50µm -60-325/350°C 15889*0.25mm 1.00µm -60-325/350°C 158090.32mm 0.10µm -60-325/350°C 158930.32mm 0.25µm -60-325/350°C 158940.32mm 0.25µm -60-325/350°C 15883*0.32mm 1.00µm -60-325/350°C 15895

60m 0.25mm 0.10µm -60-325/350°C 158790.25mm 0.25µm -60-325/350°C 158910.25mm 1.00µm -60-325/350°C 158920.32mm 0.25µm -60-325/350°C 15896



15m 0.25mm 0.10µm -60/300°C 137050.25mm 0.20µm -60/300°C 9525150.25mm 0.25µm -60/350°C 137580.25mm 1.00µm -60/350°C 137060.32mm 0.10µm -60/350°C 137090.32mm 0.25µm -60/350°C 138870.32mm 0.30µm -60/350°C 9532150.32mm 1.00µm -60/350°C 137100.53mm 0.25µm -60/350°C 141960.53mm 0.50µm -60/300°C 140390.53mm 1.00µm -60/350°C 135690.53mm 1.20µm -60/350°C 9551150.53mm 1.50µm -60/330°C 139060.53mm 3.00µm -60/300°C 138940.53mm 5.00µm -60/300°C 13896




Organophosphorus Pesticides

Column: Helifl ex® AT™-5ms, 30m x 0.25mm x 0.25µm (Part No. 15807)Temp: 120°C (3min hold) to 285°C at 5°C/min (4min hold) Carrier Gas: Helium, 26 cm/secDetector: MSD

4 8 12 16 20 24 28 32 36 40 Min.

1

2

3

46

5

7

89

10

11

12

13

1415

16

1718

16. EPN 17. Leptophos 18. Azinphos-ethyl

1. TEPP 2. Sulfotepp 3. Monocrotophos 4. Dimethoate 5. Dioxathion 6. Terbufos 7. Phosphamidon 8. Malathion 9. Parathion 10. cis-Chlorfenvinphos 11. trans-Chlorfenvinphos 12. Ethion

13. Famphur 14. Carbophenothion 15. Phosmet

*With 5 meter Integral Guard Columns. Total length of column is 35 meters.

The AT™-5ms capillaries are ideal for environmental, pharmaceutical, and petrochemical analysis, or anyGC/MS analysis requiring a 5% phenyl-type polarity capillary column.

Alltech Capillary ColumnsC O L U M N S

Specifi cationsPhase: (5% Phenyl)-95% MethoxpolysiloxanePolarity: Non-polarUSP Designation: G27, G36Ideal for: Mass Spec Analysis-General Application

Specifi cationsPhase: (5% Phenyl)-95% MethylpolysiloxanePolarity: Non-polarMax. Temp.: 380/400°CUSP Designation: G27, G36Ideal for: General Applications

Helifl ex® AT™-5• Excellent general purpose columns• Similar to DB™-5, Rtx®-5, SPB™-5, HP™-5, ULTRA™-2,

BP™-5, CP-Sil™-8-CB, 007™-2, OV™-5, SE™-52, SE-54, RSL™-200, ZB-5

2469


334 335

HELIFLEX® AT™-5 CAPILLARY COLUMNS ON 5" CAGELENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE



Econo-Cap EC™-20• Batch tested to dramatically reduce price

HELIFLEX® AT™-5 CAPILLARY COLUMNS (CONTINUED)LENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

60m 0.25mm 0.10um -60/350°C 137080.25mm 0.20µm -60/350°C 9525600.25mm 0.25µm -60/350°C 136760.25mm 1.00µm -60/350°C 136770.32mm 0.10µm -60/350°C 137120.32mm 0.25µm -60/350°C 136780.32mm 0.30µm -60/350°C 9532600.32mm 1.00µm -60/350°C 136790.53mm 0.50µm -60/350°C 138990.53mm 1.00µm -60/350°C 140760.53mm 1.20µm -60/350°C 138200.53mm 1.50µm -60/330°C 139310.53mm 3.00µm -60/350°C 139030.53mm 5.00µm -60/300°C 13829



10m 0.53mm 1.20µm -20/320°C 1393615m 0.25mm 0.25µm -20/320°C 13838

0.32mm 0.25µm -20/320°C 138490.53mm 1.20µm -20/320°C 139190.53mm 1.00µm -20/300°C 13880

25m 0.53mm 1.20µm -20/320°C 1393430m 0.25mm 0.25µm -20/320°C 13857


50m 0.53mm 1.20µm -20/320°C 1394460m 0.25mm 0.25µm -20/320°C 13868


ECONO-CAP™ EC™-20 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO.15m 0.45mm 1.00µm -20/300°C 19670

0.53mm 1.00µm -20/300°C 196870.53mm 1.20µm -20/300°C 19673


Helifl ex® AT™-20• Unique polarity between non-polar and mid-range.• Similar to 007™-7, Rtx®-20, SPB-20, VOCOL, PE-7

C O L U M N S


ECONO-CAP™ EC™-5 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO.15m 0.45mm 1.00µm -60/350°C 19661

0.53mm 1.00µm -60/350°C 196680.53mm 1.20µm -60/350°C 19645


ECONO-CAP™ EC™-5 CAPILLARY COLUMNS, SIX PACKLENGTH I.D. FILM TEMP. LIMITS PART NO.15m 0.25mm 0.25µm -60/350°C 1964930m 0.25mm 0.25µm -60/350°C 196476

0.32mm 0.25µm -60/350°C 1964660.53mm 1.20µm -60/350°C 196576

For a complete listing of Alltech Helifl ex® Capillary Columns, request data sheet 19650 PS.

Specifi cationsPhase: (20% Phenyl)-80% MethylpolysiloxanePolarity: Intermediate PolarityUSP Designation: G28, G32Ideal for: Volatile compounds and Solvents

Econo-Cap EC™-5 • Batch tested to dramatically reduce price

PART NO. PRICE

PART NO. PRICE

Batch tested to dramatically reduce priceBatch tested to dramatically reduce price

PART NO. PRICE


336

Helifl ex® AT™-35• Ideal column for conformational analysis• Similar to DB™-35, DB™-35ms, Rtx®-35,BP™X35, SPB™-

35, SPB-608, tHP™-35, 007™-11, OV™-11, RSL™-300, PE-35, Sup-Herb, ZB-35

AT™-35 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

10m 0.25mm 0.25µm -20/320°C 196130.32mm 0.10µm -20/350°C 168720.32mm 0.25µm -20/300°C 137590.53mm 0.10µm -20/350°C 168610.53mm 0.20µm -20/280°C 168650.53mm 1.20µm -20/300°C 9651100.53mm 2.65µm -20/280°C 16877

15m 0.25mm 0.25µm -20/320°C 139430.25mm 0.50µm -20/320°C 137130.32mm 0.15µm -20/280°C 137140.32mm 0.25µm -20/320°C 137600.32mm 0.50µm -20/320°C 130910.53mm 1.00µm -20/300°C 141290.53mm 1.20µm -20/300°C 965115


30m 0.25mm 0.15µm -20/320°C 134320.25mm 0.20µm -20/300°C 9625300.25mm 0.25µm -20/320°C 136420.25mm 0.50µm -20/320°C 136430.25mm 1.00µm -20/300°C 137960.32mm 0.15µm -20/320°C 137160.32mm 0.25µm -20/320°C 136440.32mm 0.50µm -20/320°C 136450.53mm 0.50µm -20/320°C 137970.53mm 1.00µm -20/300°C 140010.53mm 1.20µm -20/300°C 9651300.53mm 2.65µm -20/280°C 16878

50m 0.25mm 0.20µm -20/320°C 9625500.32mm 0.30µm -20/320°C 963250


Helifl ex® AT™-35ms• Guaranteed low bleed• Specifi cally designed for mass spec analysis• Similar to DB-35ms, Rtx-35, SPB-35, SUP-HERB,

MDN-35, BPX-35

Alltech Capillary ColumnsC O L U M N S

AT™ -35MS CAPILLARY COLUMNLENGTH I.D. FILM TEMP. LIMIT PART NO. PRICE

15m 0.25mm 0.25µm -40°/ 340°C 1258830m 0.25mm 0.25µm -40°/ 340°C 1258960m 0.25mm 0.25µm -40°/ 340°C 12590

Column: Helifl ex® AT™-35, 25m x 0.25mm x 0.20µm (Part No. 962525) Temp: 310°C Carrier: Hydrogen at 40 cm/sec Detector: FID

0 1 2 3 4 5 6 Min.

13

2

4

Tocopherols

1 . d-δ-Tocopherol 2 . d-β-Tocopherol 3 . d-γ-Tocopherol 4 . d-α-Tocopherol

1273

Specifi cationsPhase: (35% Phenyl)-65% MethylpolysiloxanePolarity: Intermediate PolarityUSP Designation: G42Ideal for: Pesticides, Herbicides, Drugs, Aromatics

Specifi cationsPhase: (35% Phenyl)-65% MethylpolysiloxanePolarity: Intermediate PolarityUSP Designation: G42Ideal for: Pesticides, Herbicides, Drugs, Aromatics

For more Capillary GC Applications, See the GC Applications Section p522-556.


337

G C C O L U M N S


Specifi cationsPhase: (50% Phenyl)-MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: G3Ideal For: Mass Spec Applications

AT™-50MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.25µm -40°/340°C 1259830m 0.25mm 0.25µm -40°/340°C 1259960m 0.25mm 0.25µm -40°/340°C 1260015m 0.32mm 0.25µm -40°/340°C 1260130m 0.32mm 0.25µm -40°/340°C 12636

Helifl ex® AT™-50ms• Designed to provide low MS bleed• Similar to DB™-17ms, H5-50+, Rtx®-50, SP-2250, SPB-50, SPB-17, BPX™-50

Helifl ex® AT™-50ht• Specially tested for bleed at 340°C• Higher temperatures mean faster analysis• Similar to DB™-17ht, Rtx®-65TG, BPX-50, CP-TAB-CB

Specifi cationsPhase: (50% Phenyl)-MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: G3Ideal For: High Boiling Compounds

AT™-50HT CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.15µm -40°/340°C 1263530m 0.25mm 0.15µm -40°/340°C 1259215m 0.32mm 0.15µm -40°/340°C 1259330m 0.32mm 0.15µm -40°/340°C 1259460m 0.32mm 0.15µm -40°/340°C 1259515m 0.53mm 0.15µm -40°/340°C 1259630m 0.53mm 0.15µm -40°/340°C 12597

Helifl ex® AT™-50• General purpose column• Similar to DB™-17, DB™-17ht, Rtx®-50, BPX-50,

SPB-50, SP-2250, HP™-50+, HP™-17, 007™-17, OV™-17, CP Sil 24CB, PE-17, ZB-50

Specifi cationsPhase: (50% Phenyl)-MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: G3Ideal For: Pesticides, Herbicides, Phthalate Esters, Free

Phenols, and Basic Drugs

AT™-50 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.25µm 40/325°C 138370.32mm 0.25µm 40/325°C 138560.53mm 1.00µm 40/280°C 13876

30m 0.25mm 0.25µm 40/325°C 138390.32mm 0.25µm 40/325°C 138580.53mm 0.50µm 40/300°C 139910.53mm 1.00µm 40/280°C 13878

Helifl ex® AT™-1301• Unique polarity makes it ideal for a range of

applications• Similar to BP™624, DB™-1301, Rtx®-1301, Rtx®-624,

HP™-1301,HP™-624, DB™-624, 007™-624, 007™-1301, SPB-1301, SPB-624, ZB-624

Specifi cationsPhase: (6% Cyanopropylpenyl)-MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: G43Ideal For: Volatile Organics, Pharmaceuticals, and

EPA Method 612



To view Alltech’s complete chromatogram library, visit www.chromatography.com

For Capillary GC Applications, see the GC Applications Section, pages 522-556.


338 339

2105

Column: Helifl ex® AT™-1701, 30m x 0.32mm x 0.25µm (Part No. 13690)Temp: 50°C (10 min hold) to 120°C at 10°C/minCarrier Gas: Helium at 35cm/secDetector: ECD

1. Monochloroacetic Acid2. Monobromoacetic Acid3. Dalapon4. Dichloroacetic Acid5. Trichloroacetic Acid6. Bromochloroacetic Acid7. Dibromoacetic Acid

0

1

23

45

6

7

2 4 6 8 10 12 14 16 18 Min.

G C C O L U M N S


Helifl ex® AT™-1701 • Similar to DB™-1701, OV™-1701, SPB™-1701, Rtx®-1701,

007™-1701, PAS-1701, CP-Sil 19CB, HP™-1701, BP-10, ZB-1701

Helifl ex® AT™-210 • Similar to DB™- 210, Rtx®-200, OV™- 202, OV™-210,

OV™-215, QF-1, SP-2401, RSL-400

Specifi cationsPhase: Trifl uoropropyl MethylpolysiloxanePolarity: PolarUSP Code: G6Ideal For: Ketones, Aldehydes, Silanes, Glycols, Nitro

Aromatics, Herbicides, and Method 8140 and 609

Specifi cationsPhase: (14% Cyanopropylphenyl)-86% MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: n/aIdeal For: Pesticides, PCB’s, Drugs, Herbicides, and TMS

Sugars


10m 0.25mm 0.20µm 45/260°C 9825100.53mm 1.20µm 45/240°C 985110

15m 0.25mm 0.25µm 45/260°C 138850.25mm 0.20µm 45/260°C 9825150.25mm 0.50µm 45/260°C 137220.32mm 0.15µm 45/260°C 137240.32mm 0.25µm 45/260°C 138880.53mm 1.00µm 45/240°C 131270.53mm 1.20µm 45/240°C 985115

25m 0.53mm 1.20µm 45/240°C 98512530m 0.25mm 0.25µm 45/260°C 13763

0.25mm 0.50µm 45/260°C 137230.32mm 0.15µm 45/260°C 137260.32mm 0.25µm 45/260°C 138400.32mm 0.50µm 45/260°C 137270.53mm 1.00µm 45/240°C 131360.53mm 1.20µm 45/240°C 985130

60m 0.25mm 0.25µm 45/260°C 137670.32mm 0.30µm 45/260°C 983260

AT™-1701 CAPILLARY COLUMNS ON 5" CAGELENGTH I.D. FILM TEMP. RANGE PART NO. PRICE




10m 0.25mm 0.20µm -20/280°C 9425100.53mm 1.20µm -20/280°C 945110

15m 0.25mm 0.25µm -20/280°C 138810.25mm 1.00µm -20/280°C 137180.32mm 0.25µm -20/280°C 137620.32mm 1.00µm -20/280°C 137200.53mm 0.50µm -20/280°C 140460.53mm 1.00µm -20/280°C 140740.25mm 0.20µm -20/280°C 9425150.32mm 0.15µm -20/280°C 137190.53mm 1.20µm -20/280°C 945115


30m 0.25mm 0.15µm -20/280°C 134170.25mm 0.25µm -20/280°C 136860.25mm 1.00µm -20/280°C 136870.32mm 0.25µm -20/280°C 136900.32mm 0.25µm -20/280°C 13106*0.32mm 1.00µm -20/280°C 136910.53mm 0.50µm -20/280°C 141050.53mm 1.00µm -20/280°C 137950.53mm 1.20µm -20/280°C 13830

50m 0.25mm 0.20µm -20/280°C 9425500.32mm 0.30µm -20/280°C 943250

60m 0.25mm 0.15µm -20/280°C 134040.25mm 0.25µm -20/280°C 136880.25mm 1.00µm -20/280°C 136890.32mm 0.15µm -20/280°C 134340.32mm 0.25µm -20/280°C 136920.32mm 1.00µm -20/280°C 136930.53mm 0.50µm -20/280°C 141070.53mm 1.00µm -20/280°C 14131

*10 meter integral guard column.

EPA Method 552.1: Haloacetic Acids



338 339

G C C O L U M N S


Helifl ex® AT™-WAX • Similar to DB™-WAX, DB™-WAXetr, Rtx®-WAX,

Stabilwax®, Carbowax® 20M, Supelcowax®-10, Innowax™, HP™-20M, HP™-Wax, BP™-20, CP-Wax-52-CB, 007™-CW, Superox® II, OmegaWAX™, ZB-WAX™

Specifi cationsPhase: 100% Polyethylene GlycolPolarity: PolarUSP Code: G14, G15, G16, G39Ideal For: FAMEs, Polar Solvents, BTEX, Flavor and Fragrances,

Glycols, Alcohols, and Aromatics

AT™-WAX CAPILLARY COLUMNS CONTINUEDLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.32mm 2.50µm 40/260°C 1373720.53mm 0.50µm 40/260°C 141090.53mm 1.00µm 40/260°C 139040.53mm 1.20µm 40/260°C 99511520.53mm 150µm 40/250°C 132150.53mm 2.50µm 40/250°C 168810.53mm 5.00µm 40/250°C 16883


30m 0.25mm 0.15µm 40/280°C 134180.25mm 0.20µm 40/280°C 99253020.25mm 0.25µm 40/280°C 1364620.25mm 0.50µm 40/260°C 1364720.32mm 0.25µm 40/280°C 1364820.32mm 0.30µm 40/280°C 99323020.32mm 0.50µm 40/260°C 1365220.32mm 1.00µm 40/260°C 1373820.53mm 0.50µm 40/260°C 141110.53mm 1.00µm 40/260°C 139070.53mm 1.20µm 40/260°C 99513020.53mm 1.50µm 40/260°C 131090.53mm 2.00µm 40/250°C 161620.53mm 2.50µm 40/250°C 168850.53mm 5.00µm 40/250°C 16887


60m 0.25mm 0.20µm 40/280°C 99256020.25mm 0.25µm 40/280°C 1369420.25mm 0.50µm 40/260°C 139160.32mm 0.25µm 40/280°C 1369620.32mm 0.30µm 40/280°C 99326020.32mm 0.50µm 40/260°C 1369720.53mm 0.50µm 40/260°C 139010.53mm 1.00µm 40/260°C 139290.53mm 1.20µm 40/260°C 138500.53mm 1.50µm 40/260°C 13243

Helifl ex® AT™-WAXms• Designed to provide low MS bleed• Similar to DB™-WAX, Rtx®-WAX,

Supelcowax®-10

Specifi cationsPhase: 100% Polyethylene GlycolPolarity: PolarUSP Code: G14, G15, G16, G39Ideal For: Mass Spec Analysis

AT™-WAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE



60m 0.25mm 0.25µm 40/260°C 126050.32mm 0.25µm 40/260°C 12608

AT™-WAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


15m 0.25mm 0.15µm 40/280°C 134330.25mm 0.20µm 40/280°C 99251520.25mm 0.25µm 40/280°C 137770.25mm 0.50µm 40/260°C 1373020.25mm 1.00µm 40/260°C 1373120.32mm 0.25µm 40/280°C 137790.32mm 0.30µm 40/280°C 99321520.32mm 0.50µm 40/260°C 1373520.32mm 1.00µm 40/260°C 137362

AT™-WAX CAPILLARY COLUMNS ON 5" CAGELENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.25µm 40/280°C 1377550.32mm 0.25µm 40/280°C 1377850.32mm 1.00µm 40/260°C 13736250.53mm 1.00µm 40/260°C 1390450.53mm 1.20µm 40/260°C 99511525



340 341

0

1

2

34

5

6

2 4 6 8 10 Min.

2528

Column: Helifl ex® AT™-AquaWax-DA, 30m x 0.25mm x 0.25µm (Part No. 14537) Temp: 180°C Carrier Gas: Helium at 22cm/sec Detector: FID

1. Propionic Acid 2. Butyric Acid 3. Valeric Acid 4. Caproic Acid 5. Heptanoic Acid 6. Caprylic Acid

G C C O L U M N S


Helifl ex® AT™-AquaWax • Designed and tested for aqueous injections• Similar to DB™-Wax, DB™-Waxer, Rtx®-WAX, Stabilwax®,

HP™-Wax, HP™-20M, HP™-INNOwax, ZB-Wax and Supelcowax 10

Helifl ex® AT™-AquaWax-DA

• Designed and tested for aqueous injections• Eliminates the need for derivatization of acidic

organic compounds • Similar to DB™-FFAP, Stabilwax™, HP™-FFAP-DA,

ZB-FFAP, SPB-1000 and Nukol™

Specifi cationsPhase: 100% Polyethylene GlycolPolarity: PolarUSP Code: n/aIdeal For: Food and Beverage Analysis

AT™-AQUAWAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.25mm 0.25µm 40/260°C 124370.32mm 0.25µm 40/260°C 12439

60m 0.25mm 0.25µm 40/260°C 124470.32mm 0.25µm 40/260°C 12449

Specifi cationsPhase: 100% Polyethylene Glycol - Nitroterephthal Acid

Modifi ed

Polarity: Polar USP Code: n/aIdeal For: Analysis of Acidic Organic Compounds and Free

Fatty Acids

AT™-AQUAWAX-DA CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


60m 0.25mm 0.25µm 40/250°C 145470.32mm 0.25µm 40/250°C 14549

Econo-Cap™ EC™-WAX • Batch tested to dramatically

reduce price• For phase specifi cations, see Helifl ex® AT™ version

EC™-WAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE



For more information on the Econo-Cap™ Capillary Line, refer to page 329.

EC™-WAX SIX-PACK CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


Free Fatty Acids


AT AT™™ version version


340 341

G C C O L U M N S


Helifl ex® AT™-1000 • Similar to DB™-FFAP, Stabilwax®-DA, SPB™-1000,

Nukol™, HP™-FFAP, BP™-21, CP-Wax™-58-CB, 007™-FFAP, OV™-351, FFAP, SUPEROX®-FA, ZB-FFAP

Helifl ex® AT™-CAM• Eliminates need for derivitazation• Similar to Stabilwax™-DB, Carbowax® Amine, CAM,

CP-WAX 51

Helifl ex® AT™-FAME• Similar to FAMEWAX™ and OmegaWAX™

Specifi cationsPhase: 100% Polyethylene Glycol - Acid Modifi edPolarity: High PolarityUSP Code: G25, G35Ideal For: Free Fatty Acids



15m 0.25mm 0.20µm 40/250°C 9725150.25mm 0.25µm 40/250°C 137820.32mm 0.25µm 40/250°C 138860.32mm 0.30µm 40/250°C 9732150.53mm 1.00µm 40/250°C 138730.53mm 1.20µm 40/250°C 975115


30m 0.25mm 0.20µm 40/250°C 9725300.25mm 0.25µm 40/250°C 137830.32mm 0.25µm 40/250°C 137850.32mm 0.30µm 40/250°C 9732300.53mm 1.00µm 40/250°C 138770.53mm 1.20µm 40/250°C 9751300.53mm 2.0µm 40/250°C 13017

50m 0.25mm 0.20µm 40/250°C 9725500.32mm 0.30µm 40/250°C 973250

60m 0.25mm 0.20µm 40/250°C 9725600.25mm 0.25µm 40/250°C 137840.32mm 0.25µm 40/250°C 137860.32mm 0.30µm 40/250°C 9732600.32mm 1.00µm 40/250°C 132760.53mm 1.00µm 40/250°C 13879

Specifi cationsPhase: 100% Polyethylene Glycol-Base Modifi edPolarity: High PolarityUSP Code: G25, G35Ideal For: Basic Compounds, Amines

AT™-CAM CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


Specifi cationsPhase: Stable Bonded Polyethylene GlycolPolarity: High PolarityUSP Code: G25, G35Ideal For: Fatty Acid Methyl Esters

AT™-FAME CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.25mm 0.25µm 40/280°C 124360.32mm 0.25µm 40/280°C 12438

Econo-Cap™ EC™-1000 • Batch tested to dramatically

reduce price• For phase specifi cations, see Helifl ex® AT™ version

EC™-1000 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE



For more information on the Econo-Cap™ Capillary Line, refer to page 329.

EC™-1000 SIX-PACK CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


AT AT™™ version version


342 343

0 2 4 6 8 10 12 14 16 Min.

12

34

5

7

6 1233

1. Benzene 2. Toluene 3. Chlorobenzene 4. Ethylbenzene 5. 1,3-Dichlorobenzene 6. 1,4-Dichlorobenzene 7. 1,2-Dichlorobenzene

Column: Helifl ex® AT™-624, 30m x 0.32mm x 1.80µm (Part No. 13756 )Temp: 90°C (7 min hold) to 180°C at 10°C/minCarrier Gas: Helium at 1.1mL/minDetector: FID

G C C O L U M N S


Helifl ex® AT™-624• Specially tested for EPA Method 624• Similar to DB™-1301, Rtx®-1301, Rtx®-624, HP™-1301,

HP™-624, DB™-624, 007™-624, 007™-1301, SPB-1301, SPB-624, ZB-624

Specifi cationsPhase: 6% Cyanopropylphenyl-94% MethylpolysiloxanePolarity: Intermediate PolarityUSP Code: G43Ideal For: EPA Methods 524, 601, 602, 624, 8240 and 8260

and Solvent Analysis


30m 0.25mm 1.40µm -20/260°C 137540.32mm 1.80µm -20/260°C 137560.32mm 3.00µm -20/260°C 137800.53mm 3.00µm -20/260°C 16889


75m 0.53mm 3.00µm -20/260°C 13937

Helifl ex® AT™-225• Similar to DB™-225, HP™-225, Rtx®-225, OV™-225,

RSL-500, 007™-225, CP-Sil 43CB, BP™-225, PE-225

Helifl ex® AT™-Silar• Similar to DB™-23, 007™-23, PE-23, Rtx™-2330, SP-

2330

Specifi cationsPhase: (50% Cyanopropyl)-50% MethylpolysiloxanePolarity: High PolarityUSP Code: G5Ideal For: cis/trans Fatty Acids Methyl Esters

AT™-SILAR CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


Specifi cationsPhase: (50% Cyanopropylphenyl)-50% MethylpolysiloxanePolarity: Mid to High PolarityUSP Code: G19Ideal For: Carbohydrates and Solvents



25m 0.25mm 0.20µm 40/240°C 9125250.53mm 1.20µm 40/220°C 915125




EPA Method 602 - Purgeable Aromatics


342 343

2678

1. C14:0 2. C16:0 3. C16:1 4. C18:1 5. C18:2 6. C18:3 7. C18:3

Column: Helifl ex® AT™-Silar-90, 30m x 0.25mm x 0.20µm (Part No. 24019) Temp: 200°C Carrier Gas: Helium at 20cm/sec Detector: FID

8. C20:1 9. C20:3 10. C20:4 11. C20:5 12. C20:5 13. C22:4 14. C22:5 15. C22:6

2679

1. C14:0 2. C16:0 3. C18:0 4. C18:1 5. C18:2

Column: Helifl ex® AT™-Silar-100, 30m x 0.25mm x 0.20µm (Part No. 24022) Temp: 190°C Carrier Gas: Helium at 20cm/sec Detector: FID

6. C20:0 7. C20:1 8. C18:3 9. C22:0 10. C22:1

0

1

2

36

7

8

910

4 5

2 4 6 8 10 12 Min.0

1

2

4 5 10

3

6

78

9

1112

1314

2 4 6 8 10 12 14 16 18 20 22 24 26 Min.

G C C O L U M N S


Helifl ex® AT™-Silar-90• Designed and tested for FAME• Similar to DB™-23, CP-Sil84,

Rtx®-2330, SP-2330

Specifi cationsPhase: Poly (90% bis Cyanopropyl)-10%

Cyanopropyphenyl Siloxane

Polarity: High PolarityUSP Code: G8Ideal For: Analysis of FAMEs

SILAR-90 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.20µm 0/250°C 126270.32mm 0.20µm 0/250°C 12629

30m 0.25mm 0.20µm 0/250°C 126280.32mm 0.20µm 0/250°C 12630

Helifl ex® AT™-Silar-100• Ideal for high and low temperature

separation of samples containing geometric isomers of FAMEs

• Similar to CO-Sil88, Rtx®-2330, SP-2340

Specifi cationsPhase: Poly bis CyanopropylPolarity: High Polarity AvailableUSP Code: G8Ideal For: cis/trans Isomers of FAMEs, Dioxins and Furans

SILAR-100 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.20µm 0/250°C 126310.32mm 0.20µm 0/250°C 12633

30m 0.25mm 0.20µm 0/250°C 126320.32mm 0.20µm 0/250°C 12634

Fatty Acid Methyl Esters Fatty Acid Methyl Esters in Rapeseed Oil

Tips for Helifl ex® AT™-Silar-90 and Silar-100

Silar-90 and Silar-100 are more susceptible to damage by oxygen, moisture, and HCL than other silicone phases. Avoid solvents

such as water and methanol when using on-column injection techniques. Columns should not be rinsed.




344 345

13. Glutamic Acid 14. Lysine 15. Tyrosine 16. Arginine 17. Histidine 18. Tryptophan

0

12 34

56

78

10 20 30 40 50 Min.

1288

1. S-Mephenytoin 2. R-Mephenytoin 3. S-3-Methyl-5-Isopropyl-5- Phenylhydantoin 4. R-3-Methyl-5-Isopropyl-5- Phenylhydantoin 5. S-5-Phenyl-5-Ethylhydantoin 6. R-5-Phenyl-5-Ethylhydantoin 7. S-5-Phenyl-5-Propylhydantoin 8. R-5-Phenyl-5-Propylhydantoin

Column: Helifl ex® Chirasil-Val®, 25m x 0.32mm x 0.20µm (Part No. 13630) Temp: 165°C Carrier Gas: Helium at 1.1mL/min Detector: FID

1241

Column: Helifl ex® AT™-Amino Acid, 25m x 0.53mm x 1.20µm (Part No. 16864)Temp: 80°C (2 min hold) to 230°C at 4°C/min Carrier Gas: Helium at 10mL/minDetector: FID

1. Alanine 2. Glycine 3. Valine 4. Threonine 5. Serine 6. Leucine

��

�

�

�

�

��

�

�

��

��

��

��

��

��

��

��

7. Isoleucine 8. Proline 9. Cystine 10. Methionine 11. Aspartic Acid 12. Phenylalanine

G C C O L U M N S


Helifl ex® Chirasil-Val® • Cross-linked for thermal stability• Ideal for the determination of the optical purity

of amino acids and the extent of ra ce m iza tion in peptide synthesis

Specifi cationsPhase: ProprietaryPolarity: Intermediate - Chiral SeparationsUSP Code: n/aIdeal For: Optical Enantiomers

CHIRASIL-VAL® CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

20m 0.53mm 0.60µm 40/220°C 1685025m 0.25mm 0.16µm 40/220°C 13636

0.32mm 0.20µm 40/220°C 136300.32mm 0.20µm 40/220°C 13631

Test KitsTest Mixture*, 250µL 19268Derivatization Kit** for Making Pentafl uoropropyl Isopropyl Esters

18093

*TFA Isopropyl Esters of 5 Amino Acids**Contains 12.5 mL Acetyl Chloride, 20mL PFPA, and 50mL 2-Propanol

Helifl ex® AT™-Amino Acid• Separates all 20 essential amino acids

Specifi cationsPhase: ProprietaryPolarity: IntermediateUSP Code: n/aIdeal For: Amino Acids

AT™-AMINO ACID CAPILLARY COLUMNLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

25m 0.53mm 1.20µm -20/350°C 16864

R,S-Anticonvulsants



N(O,S)-Heptafl uorobutyl-isobutyl Esters of Amino Acids from Soy Protein Hydrolysate


344 345

1. Methylenedioxy- methamphetamine ( MDMA) 2. Benzocaine 3. Meperidine 4. Phencyclidine ( PCP) 5. Caffeine 6. Procaine 7. Mepivacaine 8. Methadone 9. Atropine 10. Cocaine 11. Oxazepam 12. Codeine 13. Diazepam

Column: Helifl ex® Drug Two, 30m x 0.25mm x 0.25µm (Part No. 13746)

Temp: 230°C to 250°C at 5°C/minCarrier Gas: Helium at 0.64mL/minDetector: FID

0042

� � ��

�

��

�

��

�

�

�

��

��

��

��

G C C O L U M N S


Drug Analysis Capillaries• No derivatization of sample necessary• Specially tested for drugs

Drug One is a non-polar column that will elute drugs in the same order as an OV™-1 or OV™-101 packed column. Drug Two is a moderately polar column that will give a retention order similar to OV-17. Drug Three is a special phase for mu lat ed for the analysis of anticonvulsants.

Helifl ex® USP 467 Capillary Kits

• Tested for organic volatile impurities• Kits for Method I and V for Metod 467• Guard columns plus connector

USP Method 467 deals with the determination of organic volatile impurities in pharmaceuticals, which results from sol vents commonly used in the manufacturing process.

Method I Kit contains:

AT™-5, (USP G27) 30m x 0.53mm x 5.00µm; 5 x Universal FSOT Connectors; and 5 x 5m Deactivated Guard Columns (0.53mm i.d.).

Method V Kit contains:

AT™-624, (USP G43) 30m x 0.53mm x 3.00µm; 5 x Universal FSOT Con nec tors; and 5 x 5m Deactivated Guard Columns (0.53mm i.d.).

Specifi cationsPhase: ProprietaryPolarity: Drug I - Non-Polar, Drug 2 - Intermediate Polarity,

Drug 3 - PolarTemp. Range: 330°C Isothermal/350°C ProgrammedUSP Code: n/aIdeal For: Drug Analysis

DRUG CAPILLARY COLUMNSLENGTH COATING I.D. FILM PART NO. PRICE

10m Drug One 0.53mm 1.20µm 16844Drug Two 0.53mm 1.20µm 16845Drug Three 0.53mm 1.20µm 16847

30m Drug One 0.25mm 0.25µm 13745Drug Two 0.25mm 0.25µm 13746Drug One 0.32mm 0.25µm 13748Drug Two 0.32mm 0.25µm 13750

USP CAPILLARY KITSDESCRIPTION PART NO. PRICE

Capillary KitsUSP 467/Method I Capillary Kit 13963USP 467/Method V Capillary Kit 13971Replacement ComponentsAT™-5, 30m x 0.53mm x 5.0µm 16859AT™-624, 30m x 0.53mm x 3.0µm 16889Universal FSOT Connectors, 5/pk 20400Deactivated Guard Columns, 5m x 0.53mm, 5/pk 13990

Drug Mixture

Specifi cationsPhase: (5% Phenyl)-95% MethylpolysiloxanePolarity: Non-PolarTemp. Range: -60/350°C USP Code: G27Ideal For: Drug Analysis

Specifi cationsPhase: (6% Cyanopropylphenyl)-94% MethylpolysiloxanePolarity: IntermediateTemp. Range: 20/260°C USP Code: G43Ideal For: Drug Analysis



For more information on Pharmaceutical analysis, request brochure #470.


346 347

1569

Column: Helifl ex® AT™-Pesticide, 30m x 0.25mm x 0.25µm (Part No. 13662)Temp: 190°C to 240°C at 3°C/minCarrier Gas: Helium at 0.65mL/minDetector: ECD

5. Heptachlor 6. Aldrin 7. Heptachlor Epoxide 8. Endosulfan I 9. p,p'-DDE 10. Dieldrin 11. Endrin 12. p,p’-DDD 13. Endosulfan II 14. p,p’-DDT 15. Endrin Aldehyde 16. Endosulfan Sulfate

1. α-BHC 2. γ-BHC 3. β-BHC 4. δ-BHC

0 4 8 12 16 20 Min.

1615

14

13 1211

1098

7

6

5

4

1

2

3

2064

1. Vinyl Chloride 2. 1,1-Dichloroethene 3. 2-Butanone 4. Chloroform 5. Carbon Tetrachloride 6. Benzene + 1,2-Dichloroethene 7. Trichloroethene 8. Tetrachloroethene 9. Chlorobenzene 10. 1, 4-Dichlorobenzene

Column: Helifl ex® AT™-502.2, 30m x 0.53mm x 3.00µm (Part No. 13792)Temp: 40°C (10min hold) to 120°C at 4°C/minCarrier Gas: Helium at 22cm/secDetector: FID

0

1

2

3

45

6

7

8

9

10

3 6 9 12 15 18 21 24 Min.

G C C O L U M N S


Helifl ex® AT™-Pesticide• Unique selectivity for pesticide confi rmation• Pretested with pesticide mix

Helifl ex® AT™-502.2• Separates early eluting gases at above ambient

temperature• Useful for volatile organics analysis, including EPA

Methods 502.2, 524.2, 8260

AT™-PESTICIDE CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

20m 0.53mm 0.60µm 40/240°C 1684630m 0.25mm 0.25µm 40/240°C 13662

0.32mm 0.25µm 40/240°C 137440.53mm 0.60µm 40/240°C 13969

AT™-502.2 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.25mm 1.40µm 270°C 137870.32mm 1.80µm 270°C 137890.53mm 3.00µm 270°C 13792


105m 0.32mm 1.80µm 270°C 137910.53mm 3.00µm 270°C 13794

Chlorinated Pesticides TCLP Volatiles Mix

Specifi cationsPhase: ProprietaryPolarity: Intermediate USP Code: n/aIdeal For: Chlorinated Pesticides, PCBs

Specifi cationsPhase: ProprietaryPolarity: Intermediate USP Code: n/aIdeal For: Volatile Organics and EPA Methods 502.2, 524.2,

and 8260



Need Sample Prep for Your Pesticide Analysis?Florisil®-PR is pretested specifi cally chlorinated pesticides, see page 16


346 347

G C C O L U M N S


Helifl ex® AT™-2887• For simulated distillation of petroleum products

Helifl ex® AT™-Sulfur• Designed for the analysis of volatile sulfur-containing

compounds in pe tro leum distillates

Helifl ex® AT™-Amine• Separates underivatized amines with no tailing

Helifl ex® AT™-3710• For boiling range of gasoline samples

Helifl ex® AT™-Petro• For high resolution of complex hydrocarbon mixtures

AT™-2887 CAPILLARY COLUMNLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

10m 0.53mm 1.20µm 350°C 13947Test Mix for AT™-2887 41719

AT™-SULFUR CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.32mm 4.00µm -20/350°C 14029

AT™-3710 CAPILLARY COLUMNLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.53mm 5.00µm 300°C 13949Test Mix for AT™-3710 41718

AT™-AMINE CAPILLARY COLUMNSLENGTH I.D. FILM MAX. TEMP. PART NO. PRICE



AT™-PETRO CAPILLARY COLUMNLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

100m 0.25mm 0.50µm 350°C 13948

Specifi cationsPhase: 100% MethylpolysiloxanePolarity: Non PolarUSP Code: n/aIdeal For: Petroleum Distillation

Specifi cationsPhase: 100% MethylpolysiloxanePolarity: Non PolarUSP Code: n/aIdeal For: Volatile Sulfur Compounds

Specifi cationsPhase: 100% MethylpolysiloxanePolarity: Non PolarUSP Code: n/aIdeal For: Boiling Point of Gasoline

Specifi cationsPhase: Proprietary - Non bondedPolarity: IntermediateUSP Code: n/aIdeal For: Amino Acids

Specifi cationsPhase: 100% MethylpolysiloxanePolarity: Non PolarUSP Code: n/aIdeal For: hydrocarbon Mixtures

For more information about Petrochemical analysis, request brochure #478.




348 349

1821

1. Methane 2. CF2Cl2 ( Freon®-12) 3. Ethylene Oxide

Column: Helifl ex® AT™-Q, 30m x 0.53mm (Part No. 13939)Temp: 180°C Carrier Gas: Helium at 4mL/minDetector: FID

1

23

0 1 2 3 Min.

1764

Column: Helifl ex® AT™-Alumina, 50m x 0.53mm (Part No. 13926)Temp: 100°CCarrier Gas: Helium at 7.1mL/minDetector: FID

1. Methane 2. Ethane 3. Ethene 4. Propane 5. Propene

6. Isobutane 7. Butene 8. Acetylene 9. trans-2-Butene 10. 1-Butene 11. cis-2-Butene 12. Isopentane 13. Pentane 14. 1,3-Butadiene 15. Propyne

��

��

��

��

��

�

��

��

G C C O L U M N S


PLOT ColumnsThese PLOT (Porous Layer Open Tubular) columns can be used in capillary instruments, or in packed column

instruments with a simple adapter kit, and are suitable for use with any detector appropriate for your application (FID, TCD, MSD, etc.).

Helifl ex® AT™-Q• Porous divinylbenzene polymer• Similar to GS-Q, PoraPLOT Q, PoraPLOT Q-HT,

Rt-QPLOT, SupelQPLOT, HP-Q PLOT

Helifl ex® AT™-Alumina• Faster and more effi cient than packed alumina

columns, with increased sensitivity• Similar to GS-Alumina, Rt-Alumina™, HP PLOT S, HP

PLOT M, Aluminum Oxide

Specifi cationsPhase: Porous Divinylbenzene PolymerUSP Code: n/aIdeal For: Many gases and light hydrocarbons, and other

applications currently using packed porous polymer columns

AT™-Q CAPILLARY COLUMNSLENGTH I.D. TEMP. RANGE PART NO. PRICE

30m 0.53mm -60/250°C 139390.32mm -60/250°C 13950

Specifi cationsPhase: AluminaUSP Code: n/aIdeal For: Light hydrocarbon analysis, separation of C1-C4

saturated and unsaturated hydrocarbons

AT™-ALUMINA CAPILLARY COLUMNSLENGTH I.D. TEMP. RANGE PART NO. PRICE

30m 0.53mm -60/200°C 1389250m 0.53mm -60/200°C 13926

Chlorofl uorocarbons and Ethylene Oxide Light Hydrocarbons



Need to use 0.53 Columns in a Packed Column Instrument?Use Alltech’s 0.53mm Conversion Kit. Kit includes deactivated injector and detector adapter, fi ttings, and instructions.

0.53MM CONVERSION KITSDESCRIPTION LENGTH PART NO. PRICE

Direct Injection kits for 1/4" Ports 6" 5818Expansion Liner Kit for 1/4" Ports 6" 5836


348 349

1823

1. Sulfur Hexafl uoride 2. Oxygen 3. Nitrogen

Column: Helifl ex® AT™-Mole Sieve, 30m x 0.53mm (Part No. 13940)Temp: 50°C Carrier Gas: Helium at 4.6mL/minDetector: TCD

1

3

2

0 2 4 6 Min.

1902

1. Methylene Chloride 2. m-Xylene 3. p-Xylene 4. Isopropylbenzene 5. Chlorobenzene 6. n-Propylbenzene 7. tert-Butylbenzene 8. sec-Butylbenzene 9. 2-Chlorotoluene 10. 4-Chlorotoluene 11. 1,3-Dichlorobenzene 12. 1,4-Dichlorobenzene 13. 1,2-Dichlorobenzene

Column: Carbograph™ VOC, 30m x 0.25mm (Part No. 1773)Temp: 50°C (2min) to 200°C at 20°C/min Carrier Gas: Helium at 55cm/secDetector: FID at 230°CInjector: 230°C

0 8 Min.642

109

87

6

5

432

1

12

1113

G C C O L U M N S


Specifi cationsPhase: Molecular Sieve 5AUSP Code: n/aIdeal For: Separates permanent gases, noble gases, SF6,

nitrogen, oxygen, carbon monoxide and methane resolved in less than 5 minutes

AT™-MOLE SIEVE CAPILLARY COLUMNSLENGTH I.D. TEMP. RANGE PART NO. PRICE

30m 0.53mm -60/300°C 13940

Specifi cationsPhase: Carbon GraphitizedUSP Code: n/aIdeal For: Volatile organics, and medium boiling

hydrocarbons and solvents

CARBOGRAPH™ CAPILLARY COLUMNSLENGTH I.D. TEMP. RANGE PART NO. PRICE

30m 0.53mm 240°C 17720.25mm 240°C 1773

Helifl ex® AT™-Mole Sieve• Similar to Molesieve 5A, GS-Molesieve, PLT-5A,

Rt-Msieve™ 5A, Mol Sieve 5A PLOT, HP™ PLOT/Molesieve, CP-Molesieve 5A

Carbograph™ VOC• The effi ciency of a capillary with the selectivity of

graphitized carbon• Mixed adsorption/partition mechanism provides

unique selectivity



For more information about Petrochemical analysis, request brochure #478.

Sulfur Hexafl uoride Volatile Organic Compounds


350 351

G C C O L U M N S


ALLTECH GUIDE TO CAPILLARY COLUMNS FOR ENVIRONMENTAL ANALYSISMETHOD DESCRIPTION AND RECOMMENDED COLUMNS COMMENTS PART NO. PRICE

501.3 – Trihalomethanes in Drinking WaterHeliflex® AT™-624, 30m x 0.53mm x 3.00µm 16889502.1 – Volatile Halogenated Organics by Purge and Trap GC/ELCDHeliflex® AT™-624, 30m x 0.53mm x 3.00µm Subambient 16889Heliflex® AT™-624, 60m x 0.53mm x 3.00µm Ambient 13800502.2 – Volatile Organics in Water by Purge and Trap GC/PID/ELCDHeliflex® AT™-502.2, 105m x 0.53mm x 3.00µm 13794Heliflex® AT™-624, 60m x 0.53mm x 3.00µm 13800DB™-624, 75mx 0.53mm x 3.00µm 125-1374504 – DBE and DBCP by Microextraction GC/ECDDX-3, 30m x 0.32mm x 0.25µm 123-6332Econo-Cap™ EC™-1, 30m x 0.32mm x 1.00µm (Inexpensive, Batch QC’ed Column) 19660505 – Organohalide Pesticides and PCBs by Microextraction and GC/ECDHeliflex® AT™-1, 30m x 0.32mm x 1.00µm Primary Column 13641DX-3, 30m x 0.32mm x 0.25µm Alternate Column 123-6332506 – Phthalate and Adipate Esters in Water (GC/PID)Heliflex® AT™-1, 30m x 0.32mm x 0.25µm 13640Heliflex® AT™-5, 30m x 0.32mm x 0.25µm 13658507 – Nitrogen and Phosphorus Containing Pesticides by GC/NPDHeliflex® AT™-5, 30m x 0.25mm x 0.25µm Primary Column 13656Econo-Cap™ EC™-5, 30m x 0.25mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19647Heliflex® AT™-1701, 30m x 0.25mm x 0.25µm Confirmation Column 13686508 – Chlorinated Pesticides by GC/ECDHeliflex® AT™-5, 30m x 0.25mm x 0.25µm Primary Column 13656Econo-Cap™ EC™-5, 30m x 0.25mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19647Heliflex® AT™-1701, 30m x 0.25mm x 0.25µm Alternate Column 13686Heliflex® AT™-Pesticide, 30m x 0.32mm x 0.25µm 13744Heliflex® AT™-Pesticide, 30m x 0.25mm x 0.25µm 13662513 – 2,3,7,8 Tetrachlorodibenzo-p-DioxinDB-Dioxin, 60m x 0.25mm x 0.15µm 122-2461DB-Dioxin, 60m x 0.32mm x 0.15µm 123-2461515.1 – Chlorinated Acids by GC/ECDHeliflex® AT™-5, 30m x 0.25mm x 0.25µm Primary Column 13656Econo-Cap™ EC™-5 Econo-Cap, 30m x 0.25mm x 0.25µm (Inexpensive, batch QC’ed column) 19647Heliflex® AT™-1701, 30m x 0.25mm x 0.25µm Confirmation Column 13686524.2 – Purgeables by Purge and Trap GC/MSHeliflex® AT™-624, 30m x 0.53mm x 3.00µm Subambient (10°C) 16889Heliflex® AT™-624, 60m x 0.53mm x 3.00µm Ambient 13800Heliflex® AT™-5, 30m x 0.32mm x 1.00µm Subambient, Cryofocusing 13659Heliflex® AT™-5, 30m x 0.25mm x 1.00µm Subambient, Cryofocusing 13657525 – Organic Compounds in Water by Liquid-Solid Extraction and Capillary GC/MSHeliflex® AT™-5ms, 30m x 0.32mm x 0.25µm 15894Heliflex® AT™-5ms, 30m x 0.25mm x 0.25µm 15807548 – Endothall in Drinking WaterHeliflex® AT™-1, 30m x 0.25mm x 0.25µm 13638Heliflex® AT™-5, 30m x 0.25mm x 0.25µm 13656551 – Chlorination Disinfection Byproducts and Chlorinated Solvents in Drinking Water Heliflex® AT™-1, 30m x 0.32mm x 1.00µm 13641Heliflex® AT™-210, 30m x 0.32mm x 0.50µm 13727 Econo-Cap™ EC™-1, 30m x 0.32mm x 1.00µm (Inexpensive, Batch QC’ed Column) 19660552.1 – Haloacetic Acids in Drinking WaterHeliflex® AT™-1701, 30m x 0.32mm x 0.25µm 13690Heliflex® AT™-210, 30m x 0.32mm x 0.50µm 13727556.1 – Carbonyl Compounds in Drinking WaterHeliflex® AT™-5, 10m x 0.10mm x 0.10µm Fast GC 14438Heliflex® AT™-1701, 10m x 0.10mm x 0.10µm Fast GC 14439

Alltech Column Guide to EPA Methods


350 351

G C C O L U M N S


ALLTECH GUIDE TO CAPILLARY COLUMNS FOR ENVIRONMENTAL ANALYSIS CONTINUEDMETHOD DESCRIPTION AND RECOMMENDED COLUMNS COMMENTS PART NO. PRICE

601 – Purgeable Halocarbons by Purge and Trap ELCDHeliflex® AT™-624, 30m x 0.53mm x 3.00µm Subambient 16889Heliflex® AT™-624, 60m x 0.53mm x 3.00µm Ambient 13800602 – Purgeable Aromatics by Purge and Trap GC/PIDHeliflex® AT™-624, 30m x 0.53mm x 3.00µm 16889Heliflex® AT™-WAX, 30m x 0.53mm x 2.50µm Plus xylenes 16885Econo-Cap™ EC™-WAX, 30m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19659603 – Acrolein and Acrylonitrile by GC/FIDHeliflex® AT™-624, 30m x 0.53mm x 3.00µm 16889604 – Phenols by GC/FID and GC/ECDHeliflex® AT™-5, 30m x 0.53mm x 1.20µm 955130Econo-Cap™ EC™-5, 30m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19657Heliflex® AT™-5, 30m x 0.32mm x 0.25µm 13658Econo-Cap™ EC™-5, 30m x 0.32mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19646Heliflex® AT™-5, 30m x 0.25mm x 0.25µm 13656Econo-Cap™ EC™-5, 30m x 0.25mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19647606 – Phthalate Esters by GC/ECDHeliflex® AT™-5, 15m x 0.53mm x 1.20µm 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19645607 – NitrosaminesHeliflex® AT™-5, 15m x 0.53mm x 1.20µm 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19645608 – Organochlorine Pesticides and PCBs by GC/ECDHeliflex® AT™-Pesticide, 20m x 0.53mm x 0.60µm 16846Heliflex® AT™-Pesticide, 30m x 0.32mm x 0.25µm 13744Heliflex® AT™-Pesticide, 30m x 0.25mm x 0.25µm 13662609 – Nitroaromatics and Isophorone by GC/FID and GC/ECDHeliflex® AT™-5, 15m x 0.53mm x 1.20µm (Capillary GC) 955115610 – Polynuclear Aromatic Hydrocarbons by GC/FID Heliflex® AT™-5, 30m x 0.53mm x 1.20µm 955130Econo-Cap™ EC™-5, 30m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19657Heliflex® AT™-5, 30m x 0.32mm x 0.25µm 13658610 – Polynuclear Aromatic Hydrocarbons by HPLC and GC/FIDHeliflex® AT™-5, 30m x 0.32mm x 0.25µm 13658Econo-Cap™ EC™-5, 30m x 0.32mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19646Heliflex® AT™-5, 30m x 0.25mm x 0.25µm 13656Econo-Cap™ EC™-5, 30m x 0.25mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19647611 – Haloethers by GC/HSDHeliflex® AT™-5, 15m x 0.53mm x 1.20µm 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19645612 – Chlorinated Hydrocarbons by GC/ECDHeliflex® AT™-5, 15m x 0.53mm x 1.20µm 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19645613 – 2,3,7,8-Tetrachlorodibenzo-p-Dioxin by GC/MSDB™-Dioxin, 60m x 0.25mm x 0.25µm 122-2462615 – Chlorinated Herbicides by GC/ECD/ELCDHeliflex® AT™-1, 30m x 0.32mm x 0.25µm 13640Econo-Cap™ EC™-1, 30m x 0.32mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19651619 – Triazine HerbicidesHeliflex® AT™-50, 30m x 0.53mm x 1.00µm 13878624 – Purgeables by Purge and Trap GC/MSHeliflex® AT™-624, 30m x 0.53mm x 3.00µm Subambient (10°C) 16889Heliflex® AT™-624, 60m x 0.53mm x 3.00µm Ambient 13800Heliflex® AT™-5, 30m x 0.32mm x 1.00µm Subambient, Cryofocusing 13659Heliflex® AT™-5, 30m x 0.25mm x 1.00µm Subambient, Cryofocusing 13657625 – Base/Neutral and Acids by GC/MS See Method 8270 — —680 – Pesticides and PCB’s in Water and Soil/Sediment by GC/MSHeliflex® AT™-5ms, 30m x 0.32mm x 0.25µm 158948011- EDB and DBCP by Microextraction Using GCHeliflex® AT™-1, 30m x 0.32mm x 0.25µm 13640


352 353

G C C O L U M N S


ALLTECH GUIDE TO CAPILLARY COLUMNS FOR ENVIRONMENTAL ANALYSIS CONTINUEDMETHOD DESCRIPTION AND RECOMMENDED COLUMNS COMMENTS PART NO. PRICE

8015 – Nonhalogenated Volatile OrganicsHeliflex® AT™-WAX, 30m x 0.53mm x 1.00µm 13907Heliflex® AT™-5, 30m x 0.53mm x 1.50µm 139098021 – Halogenated Volatiles Using GC/PID/ELCDHeliflex® AT™-20, 60m x 0.53mm x 1.20µm 139338032 – Acrylamide by GC/ECDHeliflex® AT™-1000, 15m x 0.53mm x 1.20µm 9751158033 – Acetonitrile by GC/NPDHeliflex® AT™-WAX, 15m x 0.53mm x 1.00µm 139048041 – Phenols by GC/FID/(ECD)Heliflex® AT™-5, 30m x 0.53mm x 1.50µm 13909Heliflex® AT™-1701, 30m x 0.53mm x 1.00µm 137958070 – NitrosaminesHeliflex® AT™-5, 15m x 0.53mm x 1.20µm 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 196458081 – Organochlorine Pesticides by GC/ECDHeliflex® AT™-5, 30m x 0.25mm x 1.00µm 13657Heliflex® AT™-35, 30m x 0.25mm x 1.00µm 13796Heliflex® AT™-35, 30m x 0.53mm x 0.50µm 13797Heliflex® AT™-1701, 30m x 0.53mm x 1.00µm 13795Heliflex® AT™-5, 30m x 0.53mm x 1.50µm 13909Heliflex® AT™-Pesticide, 30m x 0.53mm x 0.60µm 139698082 – Polychlorinated Biphenyls (PCBs) by GC/ECD or GC/ELCDHeliflex® AT™-5, 30m x 0.25mm x 1.00µm 13657Heliflex® AT™-35, 30m x 0.25mm x 1.00µm 13796Heliflex® AT™-35, 30m x 0.53mm x 0.50µm 13797Heliflex® AT™-1701, 30m x 0.53mm x 1.00µm 13795Heliflex® AT™-5, 30m x 0.53mm x 1.50µm 13909Heliflex® AT™-Pesticide, 30m x 0.53mm x 0.60µm 139698091 – Nitroaromatics and Cyclic Ketones by GC/ECD or GC/NPDHeliflex® AT™-5, 30m x 0.53mm x 1.50µm 13909Heliflex® AT™-1701, 30m x 0.53mm x 1.00µm 137958100 – Polynuclear Aromatic Hydrocarbons by GC/FID Heliflex® AT™-5, 30m x 0.53mm x 1.20µm 955130Econo-Cap™ EC™-5, 30m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 19657Heliflex® AT™-5, 30m x 0.32mm x 0.25µm 13658Econo-Cap™ EC™-5, 30m x 0.32mm x 0.25µm (Inexpensive, Batch QC’ed Column) 19646Heliflex® AT™-5, 30m x 0.25mm x 0.25µm 13656Econo-Cap™ EC™-5, 30m x 0.25mm x 0.25µm (Inexpensive, Batch QC’ed Column) 196478111 – Haloethers by GC/ECDHeliflex® AT™-5, 30m x 0.53mm x 1.50µm 13909Heliflex® AT™-1701, 30m x 0.53mm x 1.20µm 138308141 – Organophosphorus Pesticides by GC/NPD/FPD/ELCDHeliflex® AT™-210, 15m x 0.53mm x 1.20µm Column 1 985115Heliflex® AT™-5, 15m x 0.53mm x 1.20µm Column 2 955115Econo-Cap™ EC™-5, 15m x 0.53mm x 1.20µm (Inexpensive, Batch QC’ed Column) 196458151 – Chlorinated Herbicides by GC/ECD Using Methylation and Pentafluorobenzylation DerivatizationHeliflex® AT™-5, 30m x 0.25mm x 0.25µm 13656Heliflex® AT™-5, 30m x 0.32mm x 1.00µm 13659Heliflex® AT™-35, 30m x 0.25mm x 0.25µm 13642Heliflex® AT™-1701, 30m x 0.25mm x 0.25µm 13686Heliflex® AT™-1701, 30m x 0.53mm x 1.00µm 13795Heliflex® AT™-Pesticide, 30m x 0.53mm x 0.60µm 139698260 – Volatile Organics by GC/MS: Capillary Column TechniqueHeliflex® AT™-624, 30m x 0.53mm x 3.00µm Subambient (10°C) 16889Heliflex® AT™-624, 60m x 0.53mm x 3.00µm Ambient 13800Heliflex® AT™-5, 30m x 0.32mm x 1.00µm Subambient, Cryofocusing 13659Heliflex® AT™-5, 30m x 0.25mm x 1.00µm Subambient, Cryofocusing 13657Heliflex® AT™-502.2, 60m x 0.53mm x 3.00µm Ambient 13793Heliflex® AT™-502.2, 105m x 0.53mm x 3.00µm Ambient 13794


352 353

G C C O L U M N S

Astec Capillary Columns

Chiraldex™ Capillary GC Columns

TABLE 1 – GENERAL CLASSES OF COMPOUNDS SEPARATED ON CHIRALDEX™ CAPILLARY COLUMNS

Chiraldex™ A-PH: Smaller linear and saturated amines, alcohols, carboxylic acids, and epoxidesChiraldex™ B-PH: Most structural types of compounds including linear and cyclic amines and alcohols, carboxylic acids, lactones, amino

alcohols, sugars, bicyclics, epoxides, haloalkanes and moreChiraldex™ G-PH: Cyclic and bicyclic diols and other larger compounds including steroids and carbohydratesChiraldex™ A-DA: Smaller cyclic amines, alcohols, and epoxides (Inquire regarding availability)Chiraldex™ B-DA: Nitrogen heterocyclics, heterocyclics, some bicyclics, and epoxides, lactones, aromatic amines, sugars, amino acid

derivativesChiraldex™ G-DA: Aromatic amines containing 2 or more rings, large cyclic diols, some heterocyclics, multi-ring compounds or compounds

with bulky substituentsChiraldex™ A-TA: Smaller alcohols, amino alcohols, amino alkanes, and diolsChiraldex™ B-TA: Broad range alkyl alcohols, halo acid esters, amino alkanes, halocycloalkanes, certain lactones, diols, alkyl halides, furan

and pyran derivativesChiraldex™ G-TA: >350 pairs chiral alcohols, diols, polyols, hydrocarbons, lactones, amine alcohols, halocarboxylic acid esters, homologous

series, furan and pyran derivatives, epoxides, glycidyl analogs and haloepihydrinsChiraldex™ G-PN: Epoxides, higher alcohols >C4, lactonesChiraldex™ G-BP: Amino acids, certain primary amines and furansChiraldex™ G-DM: Selectivity similar to PM and PH, but with shorter retention times, and greater resolution. Especially applicable to

aliphatic, olefenic and aromatic enantiomersChiraldex™ B-PM: Acids, alcohols, barbitals, diols, epoxides, esters, hydrocarbons, ketones, lactones, and terpenesChiraldex™ B-DM: Selectivity similar to PM and PH, but with shorter retention times, and greater resolution. Especially applicable to

aliphatic, olefenic and aromatic enantiomersChiraldex™ B-DP: Aromatic and aliphatic amines and some aliphatic and aromatic estersChiraldex™ G-DP: Aromatic and aliphatic amines and some aliphatic and aromatic esters

• Resolve aromatic and nonaromatic enantiomers• Pure cyclodextrin derivative coating• No racemization of chiral stationary phase at

elevated temperatures

Chiraldex™ capillaries are based on derivatized cyclodextrins, which are chiral in nature formed by the α-1,4 linkage of glucose units into toroidal shaped structures. The enzyme cyclodextrin glucosyl transferance (CGT) cleaves partially digested starch and links the glucose units into predominantly three forms, referred to as alpha, beta, and gamma; 6, 7 and 8 glucose units respectively. These cyclodextrins are thermally stable, highly crystalline and virtually insoluble in most organic solvents. Using the three forms of cyclodextrin, Astec has manufactured derivatives that exhibit properties allowing them to be used as GC phases. They are:

- Permethylated Hydroxypropyl (PH)

- Dialkylated (DA)

- Trifl uoroacetylated (TA)

- Propionylated (PN)

- Butyrylated (BP)

- Permethylated (PM)

- Dimethylated (DM)

- Dipropionyl (DP)

The prefi x A, B, G describes the cyclodextrins alpha, beta, and gamma respectively. The suffi x describes the nature of the derivatization i.e., G-TA refers to Gamma Trifl uororacetylated phase.

The most striking characteristic of these phases is that they separate nonaromatic enantiomers including saturated alcohols, amines, carboxylic acids, epoxides, diols, polyols, cyclic, bicyclic, heterocyclic compounds, lactones, amino alcohols, amino acids, halohydrocarbons, α-halocarboxylic esters, pyrans and furans. Little functionality is required for chiral recognition (Table 1). Also, there can be reversals of elution order from one series to the next as well as from one cavity size (beta) to another (gamma). The acylating reagent also can contribute to stereo-selectivity.

Need more information about Chiral Chromatography?

CHIRAL BOOKSDESCRIPTION PART NO. PRICE

Chiral Chromatography 5350Chiral Separation Techniques: A Practical Approach

5433

For more information on Chiraldex Capillary GC Columns, request document 4711.


354 355

G C C O L U M N S

Astec Capillary Columns

CHIRALDEX™ CAPILLARY COLUMNSPHASE LENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

A-DA 10m 0.25mm 0.125µm 200/220°C 410420m 0.25mm 0.125µm 200/220°C 410730m 0.25mm 0.125µm 200/220°C 410940m 0.25mm 0.125µm 200/220°C 439950m 0.25mm 0.125µm 200/220°C 4614

B-DA 10m 0.25mm 0.125µm 200/220°C 411120m 0.25mm 0.125µm 200/220°C 411330m 0.25mm 0.125µm 200/220°C 411540m 0.25mm 0.125µm 200/220°C 440150m 0.25mm 0.125µm 200/220°C 4626

G-DA 10m 0.25mm 0.125µm 200/220°C 411720m 0.25mm 0.125µm 200/220°C 411930m 0.25mm 0.125µm 200/220°C 412140m 0.25mm 0.125µm 200/220°C 440350m 0.25mm 0.125µm 200/220°C 4627

G-PN 10m 0.25mm 0.125µm 200/220°C 466020m 0.25mm 0.125µm 200/220°C 466430m 0.25mm 0.125µm 200/220°C 466840m 0.25mm 0.125µm 200/220°C 467250m 0.25mm 0.125µm 200/220°C 4676

G-BP 10m 0.25mm 0.125µm 200/220°C 466220m 0.25mm 0.125µm 200/220°C 468030m 0.25mm 0.125µm 200/220°C 467040m 0.25mm 0.125µm 200/220°C 467450m 0.25mm 0.125µm 200/220°C 4678

G-DM 10m 0.25mm 0.25µm 230/250°C 555020m 0.25mm 0.25µm 230/250°C 555130m 0.25mm 0.25µm 230/250°C 555240m 0.25mm 0.25µm 230/250°C 559950m 0.25mm 0.25µm 230/250°C 5688

B-DM 10m 0.25mm 0.25µm 230/250°C 471820m 0.25mm 0.25µm 230/250°C 471930m 0.25mm 0.25µm 230/250°C 472740m 0.25mm 0.25µm 230/250°C 472850m 0.25mm 0.25µm 230/250°C 4729

B-DP 10m 0.25mm 0.125µm 200/220°C 4115920m 0.25mm 0.125µm 200/220°C 4116030m 0.25mm 0.125µm 200/220°C 4119340m 0.25mm 0.125µm 200/220°C 4116550m 0.25mm 0.125µm 200/220°C 41166

G-DP 10m 0.25mm 0.125µm 200/220°C 4117320m 0.25mm 0.125µm 200/220°C 4117430m 0.25mm 0.125µm 200/220°C 4117540m 0.25mm 0.125µm 200/220°C 4117650m 0.25mm 0.125µm 200/220°C 41177

Chiraldex™ GC KitsChiraldex™ 3 column kits include 1 each of any three

columns of the same i.d. and length at an economical price. We recommend as a starter kit for the broadest range of applications a Chiraldex™-30 Kit including 1 each of B-DA, BDM, G-TA. Please note that Chiraldex™ B-PM is not included in the Chiraldex™ kits.

CHIRALDEX™ GC KITSPHASE LENGTH I.D. PART NO. PRICE

Chiraldex-10 Kit 10m 0.25mm 4207Chiraldex-20 Kit 20m 0.25mm 4209Chiraldex-30 Kit 30m 0.25mm 4211Chiraldex-40 Kit 40m 0.25mm 4608Chiraldex-50 Kit 50m 0.25mm 4634

CHIRALDEX™ CAPILLARY COLUMNSPHASE LENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

B-PM 30m 0.25mm 0.25µm 230/250°C 471150m 0.25mm 0.25µm 230/250°C 4713

A-TA 10m 0.25mm 0.125µm 180/180°C 412320m 0.25mm 0.125µm 180/180°C 412530m 0.25mm 0.125µm 180/180°C 412740m 0.25mm 0.125µm 180/180°C 440550m 0.25mm 0.125µm 180/180°C 4635

B-TA 10m 0.25mm 0.125µm 180/180°C 412920m 0.25mm 0.125µm 180/180°C 413130m 0.25mm 0.125µm 180/180°C 413340m 0.25mm 0.125µm 180/180°C 440750m 0.25mm 0.125µm 180/180°C 4637

G-TA 10m 0.25mm 0.125µm 180/180°C 413520m 0.25mm 0.125µm 180/180°C 413730m 0.25mm 0.125µm 180/180°C 413940m 0.25mm 0.125µm 180/180°C 440950m 0.25mm 0.125µm 180/180°C 4639

A-PH 10m 0.25mm 0.125µm 200/220°C 407320m 0.25mm 0.125µm 200/220°C 408830m 0.25mm 0.125µm 200/220°C 408940m 0.25mm 0.125µm 200/220°C 439350m 0.25mm 0.125µm 200/220°C 4197

B-PH 10m 0.25mm 0.125µm 200/220°C 409020m 0.25mm 0.125µm 200/220°C 409230m 0.25mm 0.125µm 200/220°C 409440m 0.25mm 0.125µm 200/220°C 439550m 0.25mm 0.125µm 200/220°C 4199

G-PH 10m 0.25mm 0.125µm 200/220°C 409620m 0.25mm 0.125µm 200/220°C 409830m 0.25mm 0.125µm 200/220°C 410140m 0.25mm 0.125µm 200/220°C 439750m 0.25mm 0.125µm 200/220°C 4202

Need more information about Chiral Chromatography?

CHIRAL BOOKSDESCRIPTION PART NO. PRICE

Chiral Chromatography 5350Chiral Separation Techniques: A Practical Approach

5433


354 355

G C C O L U M N S

Agilent/J&W Capillary Columns

DB™-1 and DB™-1ht • 100% Methyl Silicone • Similar to AT™-1, OV™-1, OV™-101, SE™-30, SP™-2100,

CP-Sil-5, Rtx®-1, DC-200, UCW-982, SF-96

Dimethylpolysiloxane is the most non-polar siloxane stationary phase available for GC. In general, less polar stationary phases have greater thermal stability, therefore, lower bleed than the more polar phases. DB™-1 exhibits excellent thermal stability and low bleed levels.

DB™-1 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

5m 0.53mm 2.65µm -60-260/280°C 125-100B0.53mm 5.00µm -60-260/280°C 125-1005

10m 0.18mm 0.40µm -60-325/350°C 121-101312m 0.20mm 0.33µm -60-325/350°C 128-101215m 0.25mm 0.25µm -60-325/350°C 122-1012

0.25mm 1.00µm -60-325/350°C 122-10130.32mm 0.10µm -60-325/350°C 123-10110.32mm 0.50µm -60-325/350°C 123-101E0.32mm 1.00µm -60-325/350°C 123-10130.32mm 5.00µm -60-325/350°C 123-10150.45mm 2.55µm -60-260/280°C 124-10140.53mm 0.15µm -60-300/360°C 125-10110.53mm 0.50µm -60-300/320°C 125-10170.53mm 1.00µm -60-300/320°C 125-101J0.53mm 1.50µm -60-300/320°C 125-10120.53mm 3.00µm -60-260/280°C 125-10140.53mm 5.00µm -60-260/280°C 125-1015

20m 0.10mm 0.40µm -60-325/350°C 127-10230.40µm 0.18µm -60-325/350°C 121-10220.40µm 0.40µm -60-325/350°C 121-1023

25m 0.20mm 0.33µm -60-325/350°C 128-10220.25µm 0.25µm -60-325/350°C 122-10220.32µm 0.52µm -60-325/350°C 123-1026

30m 0.25mm 0.10µm -60-325/350°C 122-10310.25mm 0.25µm -60-325/350°C 122-10320.25mm 0.50µm -60-325/350°C 122-103E0.25mm 1.00µm -60-325/350°C 122-10330.32mm 0.10µm -60-325/350°C 123-10310.32mm 0.25µm -60-325/350°C 123-10320.32mm 0.50µm -60-325/350°C 123-103E0.32mm 1.00µm -60-325/350°C 123-10330.32mm 3.00µm -60-280/300°C 123-10340.32mm 5.00µm -60-280/300°C 123-10350.45mm 1.27µm -60-300/320°C 124-10320.53mm 0.50µm -60-300/320°C 125-10370.53mm 1.00µm -60-300/320°C 125-103J0.53mm 1.50µm -60-300/320°C 125-10320.53mm 2.65µm -60-260/280°C 125-103B0.53mm 3.00µm -60-260/280°C 125-10340.53mm 5.00µm -60-260/280°C 125-1035

Alltech offers the more popular Agilent/J&W columns in the next few pages, but Alltech is a complete line supplier of all of Agilent/J&W columns. Request datasheet 126-1012D for a listing of over 1100 products manufactured by Agilent/J&W available through Alltech. The datasheet is also available on the Alltech web site.

DB™-1 CAPILLARY COLUMNS CONTINUEDLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

50m 0.25mm 0.25µm -60-325/350°C 122-105260m 0.25mm 0.25µm -60-325/350°C 122-1062

0.25mm 0.50µm -60-325/350°C 122-106E0.25mm 1.00µm -60-325/350°C 122-10630.32mm 0.25µm -60-325/350°C 123-10620.32mm 0.50µm -60-325/350°C 123-106E0.32mm 1.00µm -60-325/350°C 123-10630.32mm 3.00µm -60-280/300°C 123-10640.32mm 5.00µm -60-280/300°C 123-10650.53mm 1.00µm -60-300/320°C 125-106J

100m 0.25mm 0.50µm -60-325/350°C 122-10AE

DB™-1HT CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.10µm -60-400°C 122-11110.32mm 0.10µm -60-400°C 122-1111

30m 0.25mm 0.10µm -60-400°C 122-1131

Alltech is a full line Agilent/J&W distributor. Call Alltech Technical Support for more information and a complete list of Agilent/J&W columns.

DB™-1msJ&W Scientifi c developed DB™-1ms to extend their

family of low bleed capillary columns designed for use with mass spectrometers to the very non-polar end of the polarity scale. Designed to match the polarity of the regular DB™-1, you can use these columns for any application requiring a non-polar capillary with very low bleed and excellent inertness.


12m 0.20mm 0.33µm -60-340/360°C 128-01120.32mm 0.25µm -60-340/360°C 123-0112

25m 0.20mm 0.33µm -60-340/360°C 128-012230m 0.25mm 0.10µm -60-340/360°C 122-0131

0.25mm 0.25µm -60-340/360°C 122-013260m 0.25mm 0.25µm -60-340/360°C 122-0162


356 357

G C C O L U M N S


DB™-5 and DB™-5ht • 5% Phenyl, 95% Methyl Silicone• Similar to SE-54, AT™-5, CP-Sil-8, Dexsil® 300, DC-

200, Rtx®-5, Fluorolube, OV-73, DC-560, OV™-3

DB™-5ms Low bleed and very low chemical activity make this

new column ideal for GC/MS use. Although based on an entirely new polymer system and fabrication process, DB™-5ms is engineered to behave just like a DB-5 column so current methods can be used.


10m 0.10mm 0.40µm -60-325/350°C 127-50130.18mm 0.40µm -60-325/350°C 121-50130.53mm 5.00µm -60-260/280°C 125-50H5

15m 0.25mm 0.10µm -60-325/350°C 122-50110.25mm 0.25µm -60-325/350°C 122-50120.25mm 0.50µm -60-325/350°C 122-501E0.25mm 1.00µm -60-325/350°C 122-50130.32mm 0.10µm -60-325/350°C 123-50110.32mm 0.25µm -60-325/350°C 123-50120.32mm 1.00µm -60-325/350°C 123-50130.53mm 0.50µm -60-300/320°C 125-50170.53mm 1.00µm -60-300/320°C 125-501J0.53mm 1.50µm -60-300/320°C 125-5012

20m 0.10mm 0.40µm -60-325/350°C 127-50230.18mm 0.40µm -60-325/350°C 121-5023

30m 0.25mm 0.10µm -60-325/350°C 122-50310.25mm 0.25µm -60-325/350°C 122-50320.25mm 0.50µm -60-325/350°C 122-503E0.25mm 1.00µm -60-325/350°C 122-50330.32mm 0.25µm -60-325/350°C 123-50320.32mm 0.50µm -60-325/350°C 123-503E0.32mm 1.00µm -60-325/350°C 123-50330.53mm 0.50µm -60-300/320°C 125-50370.53mm 0.88µm -60-300/320°C 125-503D0.53mm 1.00µm -60-300/320°C 125-503J0.53mm 1.50µm -60-300/320°C 125-50320.53mm 2.65µm -60-260/280°C 125-503B0.53mm 5.00µm -60-260/280°C 125-5035

50m 0.25mm 0.25µm -60-325/350°C 122-50520.32mm 0.25µm -60-325/350°C 123-50520.32mm 1.00µm -60-325/350°C 123-5053

60m 0.25mm 0.10µm -60-325/350°C 122-50610.25mm 0.25µm -60-325/350°C 122-50620.25mm 0.50µm -60-325/350°C 122-506E0.25mm 1.00µm -60-325/350°C 122-50630.32mm 0.10µm -60-325/350°C 123-50610.32mm 0.25µm -60-325/350°C 123-50620.32mm 0.50µm -60-325/350°C 123-506E0.32mm 1.00µm -60-325/350°C 123-50630.53mm 1.50µm -60-300/320°C 125-5062

DB™-5MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

12m 0.20mm 0.33µm -60-325/350°C 128-551215m 0.25mm 0.10µm -60-325/350°C 122-5511

0.25mm 0.25µm -60-325/350°C 122-55120.25mm 0.50µm -60-325/350°C 122-55160.25mm 1.00µm -60-325/350°C 122-55130.32mm 0.10µm -60-325/350°C 123-55110.32mm 0.25µm -60-325/350°C 123-55120.32mm 1.00µm -60-325/350°C 123-55130.53mm 0.50µm -60-300/320°C 125-55170.53mm 1.50µm -60-300/320°C 125-5512

20m 0.18mm 0.18µm -60-325/350°C 121-552225m 0.20mm 0.33µm -60-325/350°C 128-5522

0.25mm 0.25µm -60-325/350°C 122-55220.25mm 0.40µm -60-325/350°C 122-552A0.32mm 0.52µm -60-325/350°C 123-5526

30m 0.25mm 0.10µm -60-325/350°C 122-55310.25mm 0.25µm -60-325/350°C 122-55320.25mm 0.50µm -60-325/350°C 122-55360.25mm 1.00µm -60-325/350°C 122-55330.32mm 0.10µm -60-325/350°C 123-55310.32mm 0.25µm -60-325/350°C 123-55320.32mm 0.50µm -60-325/350°C 123-55360.32mm 1.00µm -60-325/350°C 123-55330.53mm 0.50µm -60-300/320°C 125-55370.53mm 1.00µm -60-300/320°C 125-553J0.53mm 1.50µm -60-300/320°C 125-5532

40m 0.18mm 0.18µm -60-325/350°C 121-554250m 0.20mm 0.33µm -60-325/350°C 128-5552

0.25mm 0.25µm -60-325/350°C 122-55520.32mm 0.25µm -60-325/350°C 123-5552

60m 0.25mm 0.10µm -60-325/350°C 122-55610.25mm 0.25µm -60-325/350°C 122-55620.25mm 1.00µm -60-325/350°C 122-55630.32mm 0.10µm -60-325/350°C 123-55610.32mm 0.25µm -60-325/350°C 123-55620.32mm 1.00µm -60-325/350°C 123-5563

*DB-5ms ITD (Ion Trap tested).


15m 0.25mm 0.10µm -60-400°C 122-57110.32mm 0.10µm -60-400°C 123-5711

30m 0.25mm 0.10µm -60-400°C 122-57310.32mm 0.10µm -60-400°C 123-5731


356 357

G C C O L U M N S


DB™-35 • 35% Phenyl, 65% Methyl Silicone• Similar to AT™-35, Rtx™-35 and SPB™-35

DB™-17 and DB™-17ht • 50% Phenyl, 50% Methyl Silicone• Similar to AT™-50, OV™-17, SP-2250, OV™-11, DC-710,

OV™-22, OV™-25, Rtx®-50

DB™-35ms • Very low bleed

DB™-1701 • 14% Cyanopropyl Phenyl Silicone• Similar to AT™-1701, OV™-1701 and Rtx®-1701

DB™-17ms • Very low bleed• Ideal for MS work


15m 0.53mm 1.00µm 40-260/280°C 125-191230m 0.25mm 0.25µm 40-300/320°C 122-1932

0.32mm 0.25µm 40-300/320°C 123-19320.53mm 0.50µm 40-280/300°C 125-19370.53mm 1.00µm 40-260/280°C 125-1932


15m 0.25mm 0.25µm 50-340/360°C 122-38120.32mm 0.25µm 50-340/360°C 123-3812

30m 0.25mm 0.15µm 50-340/360°C 122-38310.25mm 0.25µm 50-340/360°C 122-38320.32mm 0.25µm 50-340/360°C 123-38320.53mm 1.00µm 50-320/360°C 125-3832

60m 0.25mm 0.25µm 50-340/360°C 122-3862


10m 0.18mm 0.40µm -20-280/300°C 121-071315m 0.25mm 0.25µm -20-280/300°C 122-0712

0.25mm 1.00µm -20-280/300°C 122-07130.32mm 0.25µm -20-280/300°C 123-07120.32mm 1.00µm -20-280/300°C 123-07130.53mm 0.50µm -20-260/280°C 125-07170.53mm 1.00µm -20-260/280°C 125-0712

30m 0.25mm 0.15µm -20-280/300°C 122-07310.25mm 0.25µm -20-280/300°C 122-07320.25mm 1.00µm -20-280/300°C 122-07330.32mm 0.25µm -20-280/300°C 123-07320.32mm 1.00µm -20-280/300°C 123-07330.53mm 0.50µm -20-260/280°C 125-07370.53mm 1.00µm -20-260/280°C 125-0732

50m 0.32mm 1.00µm -20-280/300°C 123-075360m 0.25mm 0.15µm -20-280/300°C 122-0761

0.25mm 0.25µm -20-280/300°C 122-07620.25mm 1.00µm -20-280/300°C 122-07630.32mm 0.25µm -20-280/300°C 123-07620.32mm 1.00µm -20-280/300°C 123-0763


5m 0.53mm 2.00µm 40-280/300°C 125-170415m 0.25mm 0.15µm 40-280/300°C 122-1711

0.25mm 0.25µm 40-280/300°C 122-17120.32mm 0.25µm 40-280/300°C 123-17120.32mm 0.50µm 40-280/300°C 123-17130.53mm 1.00µm 40-260/280°C 125-17120.53mm 1.50µm 40-260/280°C 125-1713

20m 0.10mm 0.10µm 40-280/300°C 127-17220.10mm 0.20µm 40-280/300°C 127-17230.18mm 0.30µm 40-280/300°C 121-1723

30m 0.25mm 0.15µm 40-280/300°C 122-17310.25mm 0.25µm 40-280/300°C 122-17320.25mm 0.50µm 40-280/300°C 122-17330.32mm 0.15µm 40-280/300°C 123-17310.32mm 0.25µm 40-280/300°C 123-17320.32mm 0.50µm 40-280/300°C 123-17330.53mm 0.50µm 40-280/300°C 125-17370.53mm 1.00µm 40-260/280°C 125-1732



15m 0.25mm 0.15µm 40-340/365°C 122-18110.32mm 0.15µm 40-340/365°C 123-1811

30m 0.25mm 0.15µm 40-340/365°C 122-18310.32mm 0.15µm 40-340/365°C 123-1831

60m 0.32mm 0.15µm 40-340/365°C 123-1861



20m 0.18mm 0.18µm 40-320/340°C 121-472230m 0.25mm 0.15µm 40-320/340°C 122-4731

0.25mm 0.25µm 40-320/340°C 122-47320.32mm 0.15µm 40-320/340°C 123-47310.32mm 0.25µm 40-320/340°C 123-4732

60m 0.25mm 0.25um 40-320/340°C 122-4762


358 359

G C C O L U M N S


DB™-210 • 50% Trifl uoropropyl, 50% Methyl Silicone• Similar to AT™-210, OV™-210, SP-2401



30m 0.25mm 0.25µm 45-240/260°C 122-02320.32mm 0.15µm 45-240/260°C 123-02310.32mm 0.25µm 45-240/260°C 123-02320.32mm 0.50µm 45-240/260°C 123-02330.53mm 1.00µm 45-220/240°C 125-0232

DB™-225 • 50% Cyanopropylmethyl, 50% Methylphenyl Silicone• Similar to AT™-225, OV™-225, HP™-225, Rtx®-225




DB™-225ms • Very low bleed• Ideal for MS work


15m 0.25mm 0.25µm 40-260°C 122-29120.32mm 0.25µm 40-260°C 123-2912

30m 0.25mm 0.25µm 40-260°C 122-29320.32mm 0.25µm 40-260°C 123-2932

60m 0.25mm 0.25µm 40-260°C 122-2962

DB™-XLB • Exceptionally low bleed -certifi ed for MS• Extended temperature limit of 360°C

DB™-XLB CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

12m 0.20mm 0.33µm 30-340/360°C 128-121215m 0.25mm 0.25µm 30-340/360°C 122-1212

0.25mm 0.10µm 30-340/360°C 122-12110.25mm 1.00µm 30-340/360°C 122-12130.32mm 0.25µm 30-340/360°C 123-12120.53mm 1.50µm 30-320/340°C 125-1212

20m 0.18mm 0.18µm 30-340/360°C 121-122225m 0.20mm 0.33µm 30-340/360°C 128-122230m 0.25mm 0.10µm 30-340/360°C 122-1231

0.25mm 0.25µm 30-340/360°C 122-12320.25mm 0.25µm 30-340/360°C 122-4232*0.25mm 1.00µm 30-340/360°C 122-12330.25mm 0.50µm 30-340/360°C 122-12360.32mm 0.25µm 30-340/360°C 123-12320.53mm 1.50µm 30-320/340°C 125-1232

60m 0.25mm 0.25µm 30-340/360°C 122-12620.32mm 0.25µm 30-340/360°C 123-1262

*DB-XLB ITD (Ion Trap Tested).

DURAWAX® • DX-3 is specifi ed by the EPA in Methods 504 and 505

DURAWAX® CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

DX-115m 0.25mm 0.25µm 50-250/270°C 122-611230m 0.32mm 1.00µm 50-250/270°C 123-6133DX-315m 0.25mm 0.25µm 50-250/270°C 122-631230m 0.25mm 0.25µm 50-250/270°C 122-633230m 0.32mm 0.25µm 50-250/270°C 123-6332DX-415m 0.25mm 0.25µm 50-250/270°C 122-641260m 0.32mm 0.25µm 50-250/270°C 123-6462

DB™-1301 • 6% Cyanopropyl Phenyl Silicone• Unique retention characteristics



30m 0.25mm 0.25µm -20-280/300°C 122-13320.25mm 1.00µm -20-280/300°C 122-13330.32mm 0.25µm -20-280/300°C 123-13320.32mm 1.00µm -20-280/300°C 123-13330.53mm 1.00µm -20-260/280°C 125-1332

60m 0.25mm 0.25µm -20-280/300°C 122-13620.32mm 0.25µm -20-280/300°C 123-1362

Alltech is a full line Agilent/J&W distributor. Call Alltech Technical Support for more information and a complete list of Agilent/J&W columns.


358 359

G C C O L U M N S


DB™-WAX • Polyethylene Glycol• Similar to Carbowax® 20M, AT™-WAX, SUPEROX®,

Stabilwax™, Supelcowax® 10, HP™-20M

DB™-WAXetr • Polyethylene Glycol• Similar to Carbowax® 20M, Supelcowax® 10,

Stabilwax™, HP™-Innowax• Extended temperature range

DB™-WAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE


15m 0.25mm 0.25µm 20-250/260°C 122-70120.25mm 0.50µm 20-250/260°C 122-70130.32mm 0.25µm 20-250/260°C 123-70120.32mm 0.50µm 20-250/260°C 123-70130.53mm 0.50µm 20-230/240°C 125-70170.53mm 1.00µm 20-230/240°C 125-7012


30m 0.25mm 0.25µm 20-250/260°C 122-70320.25mm 0.50µm 20-250/260°C 122-70330.32mm 0.25µm 20-250/260°C 123-70320.32mm 0.50µm 20-250/260°C 123-70330.53mm 0.50µm 20-230/240°C 125-70370.53mm 1.00µm 20-230/240°C 125-7032


DB™-WAXETR CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE




DB™-FFAP • Esterified Polyethylene Glycol • Similar to FFAP, AT™-1000, SP™-1000, SUPEROX™ FA,

Stabilwax™ DA, HP™-FFAP

DB™-FFAP CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

15m 0.25mm 0.25µm 40-250°C 122-32120.32mm 0.25µm 40-250°C 123-32120.53mm 1.00µm 40-250°C 125-3212

30m 0.25mm 0.25µm 40-250°C 122-32320.25mm 0.50µm 40-250°C 122-32330.32mm 0.25µm 40-250°C 123-32320.53mm 1.00µm 40-250°C 125-32320.53mm 1.50µm 40-250°C 125-3233

DB™-23 • 50% Cyanopropyl Silicone• Similar to Rtx®-2330, SP™-2330

DB™-Dioxin • Designed specifically for the analysis of dioxins and

furans• Separates 2,3,7,8-TCDD and 2,3,7,8-TCDF from all

other isomers in one run




60m 0.25mm 0.25µm 40-250/260°C 122-23620.32mm 0.25µm 40-250/260°C 123-2362

DB™-DIOXIN CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE



360

G C C O L U M N S


DB™-VRX, DB™-502.2 • For EPA Method 502.2

DB™-VRX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.25mm 1.40µm -10/260°C 122-15340.32mm 1.80µm -10/260°C 123-15340.45mm 2.55µm -10/260°C 124-1534

60m 0.25mm 1.40µm -10/260°C 122-15640.32mm 1.80µm -10/260°C 123-1564

75m 0.45mm 2.55µm -10/260°C 124-1574

DB™-502.2 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

105m 0.53mm 3.00µm 0-260/280°C 125-14A4

DB™-5.625 • For the Analysis of Base-Neutral/Acid Extractables• Additional QC Using US EPA Protocols• Similar to PTE™-5, XTI™-5, Ultra™-2

DB™-5.625 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

30m 0.25mm 0.25µm -60-325/350°C 122-56310.25mm 0.50µm -60-325/350°C 122-56320.25mm 1.00µm -60-325/350°C 122-56330.32mm 0.25µm -60-325/350°C 123-56310.32mm 0.50µm -60-325/350°C 123-56320.32mm 1.00µm -60-325/350°C 123-5633

DB™-Petro 50 and 100• Detailed analysis of petroleum products• Designed for PONA, PIANO, and PNA Analyses• Similar to Petrocol DH, HP™-PONA, SPB™-1, Rtx®-1

DB™-PETRO CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

50m 0.20mm 0.50µm -60-325/350°C 128-10560.25mm 0.50µm -60-325/350°C 122-10A6

DB-HT SIM DIS• For extended temperature simulated distillation• 430°C upper temperature limit• Rugged stainless steel

DB™-HT SIM DIS CAPILLARY COLUMNLENGTH I.D. FILM TEMP. RANGE PART NO. PRICE

5m 0.53mm 0.15µm -60-400°C 145-1001

DB™-608 • Specialty columns for the analysis of pesticides and

PCB’s• Similar to SPB™-608


15m 0.53mm 0.83µm 40-260/280°C 125-171030m 0.25mm 0.25µm 40-280/300°C 122-6832

0.32mm 0.50µm 40-280/300°C 123-17300.45mm 0.42µm 40-260/280°C 124-68370.45mm 0.70µm 40-260/280°C 124-17300.53mm 0.50µm 40-260/280°C 125-68370.53mm 0.83µm 40-260/280°C 125-1730

DB™-624 • Specialty columns for the analysis of volatile

halocarbons & purgeable aromatics• Similar to VOCOL™, Rtx®-Volatiles


20m 0.18mm 1.00µm -20-260°C 121-132425m 0.20mm 1.12µm -20-260°C 128-132430m 0.25mm 1.40µm -20-260°C 122-1334

0.32mm 1.80µm -20-260°C 123-13340.45mm 2.55µm -20-260°C 124-13340.53mm 3.00µm -20-260°C 125-1334

60m 0.25mm 1.40µm -20-260°C 122-13640.32mm 1.80µm -20-260°C 123-13640.53mm 3.00µm -20-260°C 125-1364

75m 0.45mm 2.55µm -20-260°C 124-13740.53mm 3.00µm -20-260°C 125-1374

Alltech is a full line Agilent/J&W distributor. Call Alltech Technical Support for more information and a complete list of Agilent/J&W Columns. Request datasheet 126-1012D or go to www.alltechWEB.com

To view applications performed on J&W Capillary Columns, go to www.chromatography.com


361

G C C O L U M N S


GS-CarbonPLOT™

GS-Q

HP-PLOT Molesieve

GS-Alumina and GS-Alumina/KCL

DB-ALC1™ and DB-ALC2™

• For blood alcohol analysis

Cyclodex-B™ Chiral • Permethylated β-Cyclodextrin

CycloSil-B™ Chiral • Silane modified β-Cyclodextrin in DB-1701 matrix

GS-GasPro™ GS-CARBONPLOT™ CAPILLARY COLUMNS

LENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.32mm 1.50µm -60-350/360°C 113-31120.53mm 3.00µm -60-350/360°C 115-3113


60m 0.32mm 1.50µm -60-350/360°C 113-3162

GS-Q CAPILLARY COLUMNSLENGTH I.D. TEMP. LIMITS PART NO. PRICE

10m 0.53mm -60-250°C 115-34H215m 0.32mm -60-250°C 113-3412

0.53mm -60-250°C 115-341225m 0.32mm -60-250°C 113-3422

0.53mm -60-250°C 115-342230m 0.32mm -60-250°C 113-3432

0.53mm -60-250°C 115-3432

HP-PLOT MOLESIEVE CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.32mm 12.00µm -60/300°C 19091P-M530.32mm 25.00µm -60/300°C 19091P-MS70.53mm 25.00µm -60/300°C 19095P-MS50.53mm 50.00µm -60/300°C 19095P-MS9

30m 0.32mm 12.00µm -60/300°C 19091P-MS40.32mm 25.00µm -60/300°C 19019P-MS80.53mm 25.00µm -60/300°C 19095P-MS60.53mm 50.00µm -60/300°C 19095P-MS0

*Lower temperatures may be used depending on the sample.

GS-ALUMINA CAPILLARY COLUMNSLENGTH I.D. TEMP. LIMITS PART NO. PRICE

GS-Alumina30m 0.53mm -60*-200°C 115-353250m 0.53mm -60*-200°C 115-3552GS-Alumina KCL Column30m 0.53mm -60*-200°C 115-333250m 0.53mm -60*-200°C 115-3352*Lower temperatures may be used depending on the sample.

GS-GASPRO™ CAPILLARY COLUMNSLENGTH I.D. TEMP. LIMITS PART NO. PRICE

5m 0.32mm -80/260°C 113-430215m 0.32mm -80/260°C 113-431230m 0.32mm -80/260°C 113-433260m 0.32mm -80/260°C 113-4362

CYCLOSIL-B CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

30m 0.25mm 0.25µm 10-250°C 112-66320.32mm 0.25µm 10-250°C 113-6632

CYCLODEX-B CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

30m 0.25mm 0.25µm 50-230/250°C 112-25320.32mm 0.25µm 50-230/250°C 113-2532

60m 0.25mm 0.25µm 50-230/250°C 112-2562

DB-ALC1™ & ALC2™ CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

DB-ALC1™

30m 0.32mm 1.8µm 20-260/280°C 123-913430m 0.53mm 3.0µm 20-260/280°C 125-9134DB-ALC2™

30m 0.32mm 1.2µm 20-260/280°C 123-923430m 0.53mm 2.0µm 20-260/280°C 125-9234


362 363

1871 1. Phenol 2. 2-Chlorophenol 3. 2,4-Dinitrophenol 4. 2-Nitrophenol 5. 2,4-Dichlorophenol 6. 4-Chloro-3-methylphenol 7. 2,4,6-Trichlorophenol 8. 2,4-Dinitrophenol 9. 4-Nitrophenol 10. 2-Methyl-4,6-dinitrophenol 11. Pentachlorphenol

Column: SGE BPX-5, 25m x 0.32mm x 0.50µm (Part No. 52318) Temp: 125°C to 250°C (5min hold) at 15°C/min Carrier Gas: Hydrogen at 1.4mL/minDetector: FID

1

2

3

4

5

6

7

8

910

11

0 12 Min.1 2 3 4 5 6 7 8 9 10 11

G C C O L U M N S

SGE Capillary Columns

BPX Capillary Columns

Specifi cationsPHASE PHASE COMPOSITION

BPX1-SimD 100% MethylpolysiloxaneBPX5 5% Phenyl, 95% MethylpolysiloxaneBPX35 35% Phenyl, 65% MethylpolysiloxaneBPX50 50% Phenyl, 50% MethylpolysiloxaneBPX70 70% Cyanopropyl

• Extended temperature range• Low bleed ideal for GC/MS applications

SGE uses silphenylene-siloxane chemistry to manufacture BPX stationary phases, resulting in extremely low bleed, thermally stable capillary columns.

This is a partial listing of SGE Capillary Columns available from Alltech. For a complete listing request datasheet 54800. This datasheet is also available on our website.

BPX1-SIMD CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

5m 0.53mm 0.1µm 430°C 54800*10m 0.53mm 0.9µm 400°C 54801**

0.53mm 2.65µm 370°C 54802***Aluminum Clad. **Polyimide Clad

BPX5 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.25µm -40 to 360/370°C 541030.25mm 1.00µm -40 to 360/370°C 541210.32mm 0.25µm -40 to 360/370°C 541440.32mm 1.00µm -40 to 360/370°C 541520.53mm 1.00µm -40 to 360/370°C 541470.53mm 3.00µm -40 to 350/360°C 54159

30m 0.25mm 0.25µm -40 to 360/370°C 541010.25mm 0.50µm -40 to 360/370°C 5410250.25mm 1.00µm -40 to 360/370°C 541220.32mm 0.25µm -40 to 360/370°C 541450.32mm 0.50µm -40 to 360/370°C 5412050.32mm 1.00µm -40 to 360/370°C 541530.53mm 0.50µm -40 to 360/370°C 5413450.53mm 1.00µm -40 to 360/370°C 541480.53mm 1.50µm -40 to 360/370°C 5413480.53mm 3.00µm -40 to 350/360°C 54160

60m 0.25mm 0.25µm -40 to 360/370°C 541020.25mm 1.00µm -40 to 360/370°C 541230.32mm 0.25µm -40 to 360/370°C 541460.32mm 1.00µm -40 to 360/370°C 541540.53mm 1.00µm -40 to 360/370°C 54158


15m 0.25mm 0.25µm 0 to 360/370°C 547000.25mm 1.00µm 0 to 360/370°C 547030.32mm 0.25µm 0 to 360/370°C 547230.32mm 1.00µm 0 to 360/370°C 547160.53mm 0.50µm 0 to 360/370°C 547340.53mm 1.00µm 0 to 360/370°C 54736

BPX35 CAPILLARY COLUMNS (CONTINUED)LENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

30m 0.25mm 0.25µm 0 to 360/370°C 547010.25mm 0.50µm 0 to 360/370°C 5470250.25mm 1.00µm 0 to 360/370°C 547040.32mm 0.25µm 0 to 360/370°C 547240.32mm 0.50µm 0 to 360/370°C 5471580.32mm 1.00µm 0 to 360/370°C 547170.53mm 0.50µm 0 to 360/370°C 547350.53mm 1.00µm 0 to 360/370°C 54737

60m 0.25mm 0.25µm 0 to 360/370°C 547020.25mm 1.00µm 0 to 360/370°C 547050.32mm 0.25µm 0 to 360/370°C 54725





15m 0.25mm 0.25µm 50 to 260/290°C 546210.53mm 0.50µm 50 to 260/290°C 54619



120m 0.25mm 0.25µm 50 to 260/290°C 54624

EPA Method 625 - Phenols


362 363

G C C O L U M N S

SGE and Quadrex® Capillary Columns

Quadrex® Capillary ColumnsAluminum Clad Silica

• Quadrex® high temperature capillaries• Rapid heat transfer

SpecificationsPHASE PHASE COMPOSITION

1HT 100% Methyl Silicone5HT 5% Phenyl, 95% Methyl Silicone50HT 50% Phenyl, 50% Methyl Silicone65HT 65% Phenyl, 35% Methyl Silicone

BTR-CW — Oxygen Resistant Carbowax® • Enhanced oxygen resistance for longer column

lifetimes• Increased thermal stability

1, 5, 50, 65HT ALUMINUM CLAD CAPILLARIESLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

1HT10m 0.25mm 0.10µm 420/440°C 1696015m 0.25mm 0.10µm 420/440°C 1696125m 0.25mm 0.10µm 420/440°C 169625HT10m 0.25mm 0.10µm 420/440°C 1696315m 0.25mm 0.10µm 420/440°C 1696425m 0.25mm 0.10µm 420/440°C 1696550HT25m 0.25mm 0.10µm 370/390°C 16968065HT10m 0.25mm 0.10µm 370/390°C 1697015m 0.25mm 0.10µm 370/390°C 1697125m 0.25mm 0.10µm 370/390°C 16972

BTR-CW CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

15m 0.25mm 0.25µm 20/280˚C 432020.32mm 0.25µm 20/280˚C 432100.53mm 1.0µm 20/280˚C 43216

30m 0.25mm 0.25µm 20/280˚C 432000.32mm 0.25µm 20/280˚C 432120.53mm 1.0µm 20/280˚C 43204

SolGel-WAX Capillary Columns• Highest temperature polyethylene glycol column • Maximum temperature 300°C• Ideal for: essential oils, food additives, industrial

solvents, unreacted latex monomers, mixtures of aromatic hydrocarbons (e.g. BTEX), FAMEs, and mixtures of alcohols, esters, aldehydes, and ketones

SolGeL-WAX is a bonded polyethylene glycol stationary phase. It is unique technology because the phase is encapsulated in synthetic glass (SolGeL material) and the whole matrix is itself bonded to the surface of the fused silica. This process leads to a very inert high-temperature column.

SolGel 1-ms Capillary Columns• MS-grade capillary columns• Maximum temperature 380°C• Ideal for: essential oils, pharmaceuticals, food

additives, industrial solvents, and hydrocarbons

SolGeL-1ms is a low bleed bonded polydimethylsiloxane (100% methyl) stationary phase encapsulated in synthetic glass (SolGeL material) and the whole matrix is itself bonded to the surface of the fused silica capillary. The anchoring of the matrix to the glass surface using this unique technology leads to a very inert, high-temperature column.

SOLGEL-1MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE



SOLGEL-WAX CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE



SolGel Capillary Columns• Unique technology encapsulates phase in synthetic

glass• Greater inertness and thermal stability than “coated”

phases


364 365

G C C O L U M N S

Quadrex® Capillary Columns

Quadrex® 007

This is a partial listing of Quadrex® products available from Alltech. Quadrex® manufactures a broad range of capillary columns. Please contact Technical Support for more information.

QUADREX® 007-1 CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

30m 0.25mm 0.10µm 325°C 425020.25mm 0.25µm 325°C 425040.25mm 0.50µm 325°C 425060.25mm 1.00µm 325°C 425080.32mm 0.25µm 325°C 425520.32mm 0.50µm 325°C 425530.32mm 1.00µm 325°C 425540.32mm 5.00µm 300°C 425560.53mm 1.00µm 325°C 425740.53mm 3.00µm 300°C 425750.53mm 5.00µm 300°C 42576

60m 0.25mm 0.10µm 325°C 425160.25mm 0.25µm 325°C 425180.25mm 0.50µm 325°C 425220.25mm 1.00µm 325°C 425240.32mm 0.25µm 325°C 425590.32mm 0.50µm 325°C 425600.32mm 1.00µm 325°C 425610.32mm 3.00µm 300°C 425620.53mm 1.00µm 325°C 425790.53mm 3.00µm 300°C 425800.53mm 5.00µm 300°C 42581

QUADREX® 007-5MS CAPILLARY COLUMNSLENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE



60m 0.25mm 0.25µm 325/350°C 400650.32mm 0.25µm 325/350°C 40059

QUADREX® 007-CW CAPILLARY COLUMNS*LENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE

30m 0.25mm 0.25µm 260°C 426360.32mm 0.25µm 260°C 426400.32mm 0.50µm 260°C 426410.53mm 1.00µm 260°C 426440.53mm 3.00µm 240°C 42645

60m 0.25mm 0.25µm 260°C 426380.25mm 0.50µm 260°C 426390.32mm 0.25µm 260°C 426420.32mm 0.50µm 260°C 426430.53mm 1.0µm 260°C 426460.53mm 3.0µm 240°C 42647

*Polyethylene Glycol.

QUADREX® 007-FFAP CAPILLARY COLUMNS**LENGTH I.D. FILM TEMP. LIMITS PART NO. PRICE



**Nitroterephthalic Acid Modifi ed Polyethylene Glycol

Specifi cationsPHASE PHASE COMPOSITION

007-1 Dimethylpolysiloxane, non-polar007-5ms Silphenylene, polysiloxane, non-polar007-CW Polyethylene glycol (PEG,) polar007-FFAP Nitroterephthalic acid modifi ed polyethylene

glycol/siloxane, polar

Quadrex® 007-1 Capillary Columns• Ideal for general purpose: hydrocarbons, solvents,

waxes, pharmaceuticals, fl avors, etc.

Quadrex® 007-FFAP Capillary Columns• Ideal for alcohols, aldehydes, ketones, acids

Quadrex® 007-CW Capillary Columns• Ideal for alcohols, free acids, essential oils, solvents,

aromatics, BTEX, fl avors and fragrances

Quadrex® 007-5ms Capillary Columns• Ideal for low bleed characteristics for GC/MS use:

hydrocarbonsm solvents, waxes, etc.


364 365

3980

1059 1. Air and Carbon Monoxide (Inner Column) 2. Methane (Inner Column) 3. Carbon Dioxide (Inner Column) 4. Oxygen (Outer Column) 5. Nitrogen (Outer Column) 6. Methane (Outer Column) 7. Carbon Monoxide (Outer Column)

Column: CTR I (Part No. 8700)Outer Column: 6ft x 1/4" Packed with Activated Molecular SieveInner Column: 6ft x 1/8" Packed with Porous Polymer MixtureTemp: AmbientCarrier Gas: Helium at 65mL/minDetector: TCD

123

4

5

6 7

0 1 2 3 4 5 6 7 8 9 Min.

1060

Column: CTR III, 6ft x 1/4" SS (Part No. 8725)Outer Column: 6ft x 1/4" Packed with Activated Molecular SieveInner Column: 6ft x 1/8" Packed with Molecular Sieve and Oxy AdsorbentTemp: AmbientCarrier Gas: Helium at 70mL/minDetector: TCD

0 2 4 6 8 10 12 Min.

1

2 3 4 1. Argon (Inner Column) 2. Nitrogen (Inner Column) 3. Oxygen + Argon (Outer Column) 4. Nitrogen (Outer Column)

G C C O L U M N S

Packed Columns

CTR Concentric Columns — For Gas Analysis• CRT I is ideal for separating O2, N2, CH4, CO, CO2 at

ambient conditions• CRT III is ideal for argon analysis in the presence of

O2

• Useful where two separate chromatographic runs are required to analyze one sample

• Individually tested

A CTR column is essentially a column within a column. This permits you to use two different packings for the analysis of your sample. The diagram shows the construction of the CTR column. Cut-away view of CTR column

CTR I - Oxygen, Nitrogen, Methane, Carbon Monoxide and Carbon Dioxide

Until the CTR, no single column operating at room temperature has been designed to permit, in one analysis, all these components in air. The analysis is usually accomplished by separate runs or with expensive valves. The CTR I accomplishes this separation in less than nine minutes.

Calibration Gas for CTR I Column – This special mixture is useful for calibrating Part No. 8700 CTR I columns. It contains approximately 15% CO2 + 7% CO + 7% O2 + 4.5% CH4 with the balance N2. It is supplied in a 4L push button can with a needle applicator.

CTR III Argon Analysis Column

The CTR III is special designed for the separation of argon in the presence of oxygen. The outer column contains a special adsorbent that removes oxygen allowing the elution of argon and nitrogen. The inner column allows the combined elution of a peak containing oxygen and argon and later nitrogen. This separation is accomplished at ambient temperatures in ten minutes.

CTR I - Air, CO, CH4, CO2, O2, N2

CTR I COLUMN DESCRIPTION TEMP. LIMITS PART NO. PRICE

CTR I Column 275°C 8700Calibration Gas for CTR I — 9799

CTR III COLUMN DESCRIPTION TEMP. LIMITS PART NO. PRICE

CTR III Argon Analysis Column 275°C 8725Additional FittingsTube End Connector, 1/4" to 1/8" Tube 14169

CTR III - Argon in Air

For more GC Applications, see the GC Applications Section, pages 522-556.

Outer 1/4" o.d. Tube ContainingColumn Packing B

Inner 1/8" o.d. Tube ContainingColumn Packing A


366 367

G C C O L U M N S

Packed Columns

POPULAR GC PACKED COLUMNSPACKING DESCRIPTION DIMENSIONS* PART NO. PRICE

Alumina F-1, 60/80 5' x 1/8" SS Tubing 5664PC 1% AT™-1000 on Carbograph 1, 60/80 144041% AT™-1000 on Carbograph 1, 60/80 24' x 1/8" SS Tubing 1446810% AT™-1000 on Chromosorb W-AW, 80/100 12001PC 0.10% AT™-1000 on Graphpac-GC, 80/100 8542PC 10% Carbowax® 1500 on Chromosorb T, 40/60 144796.6% Carbowax® 20M on Carbograph 1 AW, 80/100 10' x 1/8" SS Tubing 144735.0% Carbowax® 20M on Chromosorb W-HP, 80/100 1448210% Carbowax® 20M on Chromosorb W-AW, 80/100 12005PC 10% Carbowax® 20M on Chromosorb W-HP, 80/100 12106PC 6.6% Carbowax® 20M on Graphpac GB, 80/120 10' x 1/8" SS Tubing 144720.20% Carbowax® 1500 on Graphpac-GC, 80/100 8546PC Carbosphere®, 60/80 5680PC Carbosphere®, 80/100 10' x 1/8" SS Tubing 56821PC Carbosphere®, 80/100 5682PC Chemipack C18, 80/100 2768PC Chromosorb® 101, 80/100 2406PC Chromosorb® 102, 80/100 2409PC Chromosorb® 107, 80/100 2424PC Chromosorb® 107, 80/100 6' x 1/8" TFE Tubing 9783 Chromosorb® 750, 80/100 4' x 1/8" SS Tubing 1448030% DC-200 (500cstks) on Chromosorb® P-AW, 60/80 1448130% DC-200 (500cstks) on Chromosorb® P-AW, 60/80 8' x 1/8" SS Tubing 12713PC 10% FFAP on Chromosorb® W-AW, 80/100 8434PC Gas Chrom® 220, 80/100 2484PC Gas Chrom® 254, 80/100 2486PC Gas Chom® MP-1, 100/120 30' x 1/8" SS Tubing 4945PC HayeSep® A, 80/100 14484HayeSep® A, 120/140 40' x 1/8" SS Tubing 28211 HayeSep® B, 80/100 14485HayeSep® D, 80/100 14487HayeSep® D, 100/120 3' x 1/8" SS Tubing 14486HayeSep® D, 100/120 20' x 1/8" Ni Tubing 27082PC HayeSep® D, 100/120 30' x 1/8" SS Tubing 27083PC HayeSep® D, 100/120 10' x 1/8" SS Tubing 28301PC HayeSep® DB, 100/120 30' x 1/8" SS Tubing 2836PC HayeSep® Dip, 100/120 9' x 1/8" SS Tubing 2833PC HayeSep® N, 80/100 14488HayeSep® Q, 60/80 14490HayeSep® Q, 80/100 8' x 11/8" SS Tubing 28010PC HayeSep® Q, 80/100 2801PC HayeSep® Q, 100/120 14489HayeSep® P, 60/80 8' x 1/8" SS Tubing 2803PC HayeSep® P, 80/100 2804PC HayeSep® R, 80/100 2807PC HayeSep® S, 100/120 2811PC HayeSep® T, 60/80 3' x 1/8" SS Tubing 14491HayeSep® T, 80/100 2813PC HayeSep® T, 100/120 5' x 1/8" SS Tubing 2814PC *6' x 1/8" stainless steel unless otherwise specified.

Popular GC Packed ColumnsPopular Packed Column Ordering Instructions:1. Choose the part no. for your column from pages 366-367.2. Specify make and model of GC.*3. If your column is not listed, see page 372 for custom columns.*If no coiling instructions are provided, we will supply in a nominal 6" coil.

These columns are 6' x 1/8" o.d. 304 premium grade, precleaned stainless steel (unless otherwise indicated). Each column is made with preconditioned, pretested packing and comes complete with fittings, packing quality control chromatogram, column tags, and conditioning instructions.


366 367

G C C O L U M N S

Packed Columns

POPULAR GC PACKED COLUMNS**PACKING DESCRIPTION DIMENSIONS* PART NO. PRICE

5% Krytox® 143 AC on Graphpac, GB 60/80 10' x 1/8" SS Tubing 85222 Molecular Sieve 5A (Washed), 60/80 14494Molecular Sieve 5A (Washed), 80/100 5605PC Molecular Sieve 5A (Washed), 80/100 10' x 1/8" SS Tubing 14495Molecular Sieve 13X (Washed), 60/80 5' x 1/8" SS Tubing 57730PC Molecular Sieve 13X (Washed), 80/100 3' x 1/8" SS Tubing 14492Molecular Sieve 13X (Washed), 80/100 5773PC Molecular Sieve 13X (Washed), 80/100 10' x 1/8" SS Tubing 144933% OV-1 on Chromosorb W-HP, 80/100 12716PC 10% OV™-101 on Chromosorb P-AW, 80/100 4' x 1/8" SS Tubing 1447710% OV™-101 on Chromosorb P-AW, 80/100 1447820% OV™-101 on Chromosorb P-AW, 80/100 144693% OV™-101 on Chromosorb W-HP, 80/100 12019PC 3% OV™-101 on Chromosorb W-HP, 100/120 12700PC 20% OV™-101 on Chromosorb W-HP, 80/100 1447010% OV™-101 on Chromosorb W-HP, 80/100 12703PC 3% OV™-17 on Chromosorb W-HP, 100/120 12017PC 3% OV™-17 on Chromosorb W-HP, 80/100 12719PC 0.19% Picric Acid on Graphpac-GC, 80/100 7' x 1/8" SS Tubing 85501PC Porapak® N, 80/100 3' x 1/8" SS Tubing 14497Porapak® N, 80/100 2716PC Porapak® N, 80/100 12' x 1/8" SS Tubing 14498Porapak® N, 100/120 3' x 1/8" SS Tubing 14496Porapak® P, 80/100 14499Porapak® PS, 80/100 10' x 1/8" SS Tubing 14506Porapak® PS, 100/120 3' x 1/8" SS Tubing 14500Porapak® Q, 50/80 4' x 1/8" SS Tubing 14508Porapak® Q, 50/80 2700PC Porapak® Q, 80/100 3' x 1/8" SS Tubing 14519Porapak® Q, 80/100 12' x 1/8" SS Tubing 27012PC Porapak® Q, 80/100 2701PC Porapak® Q, 100/120 2702PC Porapak® QS, 80/100 2719PC Porapak® R, 80/100 2707PC Porapak® S, 50/80 7' x 1/8" SS Tubing 2709PC Porapak® S, 80/100 2710PC Porapak® T, 80/100 2713PC 5% SE-30 on Chromosorb® W-HP, 80/100 12025PC 10% SE-30 on Chromosorb® W-HP, 80/100 12423PC Silica Gel Grade 12, 60/80 8' x 1/8" SS Tubing 14523Silica Gel Grade 12, 60/80 18' x 1/8" SS Tubing 5651PC Silica Gel Grade 12, 80/100 8' x 1/8" SS Tubing 1453010% Silar® 10C on Chromosorb® W-HP, 100/120 12430PC 20% Squalane on Chromosorb® P-AW, 80/100 3' x 1/8" SS Tubing 1447115% Squalane on Chromosorb® P-AW-DMCS, 80/100 8' x 1/8" SS Tubing 5327PC Sulfur Gas Column 36' x 1/8" TFE Tubing 9779 Super Q, 80/100 2735PC 18" of Super Q, 80/100 30" x 1/8" TFE Tubing 9781 Tenax® TA, 60/80 4' x 1/8" SS Tubing 14538Tenax® TA, 60/80 4900PC Tenax® TA, 80/100 4901PC Tenax® GR, 60/80 4937PC Unibeads® 1S, 60/80 2752PC Unibeads® 2S, 60/80 2760PC Unibeads® 3S, 60/80 14541Unibeads® 3S, 80/100 14542VZN-1 , 60/80 23' x 1/8" SS Tubing 84623PC 10% Silicone UCW-98 on Chromosorb® W-HP, 80/100 8493PC 1% TCEP on Carbograph® 1, 80/120 4' x 1/8" SS Tubing 14474*6' x 1/8" stainless steel unless otherwise specified.

**To order, use the part number shown and specify the instrument for which it should be coiled.


368 369

G C C O L U M N S

Packed Columns

Alltech Pretested GC PackingsPretested packings are guaranteed and supplied

with a test chromatogram. Preconditioning service is available for 20g or 25g of packing. The packing is heated at 25°C below the upper temperature limit for 3 hours with a flow of oxygen-free nitrogen.

PRECONDITIONING SERVICESDESCRIPTION PART NO. PRICE

Packing Preconditioning Service(per 20-25 grams). Specify Pretested GC Packing Part Number.

C-14000

PRETESTED GC PACKINGSPACKING DESCRIPTION TEMP. LIMITS QTY. PART NO. PRICE

Alumina F-1, 60/80 300°C 100g 56641% AT™-1000 on Carbograph 1, 60/80 250°C 15g 173310% AT™-1000 on Chromosorb W-AW, 80/100 250°C 20G 120010.10% AT™-1000 on Graphpac GC, 80/100 225°C 15g 854210% Carbowax® 1500 on Chromosorb T, 40/60 175°C 20g 161466.6% Carbowax® 20M on Carbograph 1-AW, 80/120 660/225°C 15g 17315.0% Carbowax® 20M on Chromosorb W-HP, 80/100 660/225°C 20g 161475.0% Carbowax® 20M on Chromosorb T, 40/60 660/225°C 25g 841610.0% Carbowax® 20M on Chromosorb W-AW, 80/100 660/225°C 20g 1200510.0% Carbowax® 20M on Chromosorb W-HP, 80/100 660/225°C 20g 121064% Carbowax® 20M + 0.8% KOH on Graphpac GB, 60/80 220°C 15g 85196.6% Carbowax® 20m on Graphpac GB, 80/120 175°C 15g 161480.2% Carbowax® 1500 on Graphpac GC, 80/100 175°C 15g 8546Carbosphere®, 60/80 400°C 5g 5680Carbosphere®, 80/100 400°C 5g 5682Chemipack C18, 80/100 320°C 15mL 2768Chromosorb® 101, 80/100 275/325°C 25g 16149Chromosorb® 102, 80/100 250/300°C 25g 16150Chromosorb® 107, 80/100 250/275°C 25g 16151Chromosorb® 750, 80/100 250/275°C 25g 1615230% DC-200 (500 cstk) on Chromosorb® P-AW, 60/80 0/200°C 25g 1271310% FFAP on Chromosorb® W-AW, 80/100 50/250°C 25g 843428% AT-223 + 4% KOH on Gas Chrom® R, 80/100 200°C 25g 49259Gas Chrom® 220, 80/100 250°C 25g 2484Gas Chrom® 254, 80/100 275°C 25g 2486Gas Chrom® MP-1, 100/120 50/250°C 25g 16153HayeSep® A, 80/100 165°C 15g 16154HayeSep® A, 120/140 165°C 15g 16155HayeSep® B, 80/100 190°C 15g 16156HayeSep® D, 80/100 290°C 15g 16157


368 369

G C C O L U M N S

Packed Columns

PRETESTED GC PACKINGS CONTINUEDPACKING DESCRIPTION TEMP. LIMITS QTY. PART NO. PRICE

HayeSep® D, 100/120 290°C 15g 16166HayeSep® DB, 100/120 290°C 15g 16169HayeSep® Dip, 100/120 290°C 15g 16170HayeSep® N, 80/100 165°C 15g 16172HayeSep® Q, 60/80 275°C 15g 16196HayeSep® Q, 80/100 275°C 15g 16197HayeSep® Q, 100/120 275°C 15g 16198HayeSep® P, 60/80 250°C 15g 16199HayeSep® P, 80/100 250°C 15g 16210HayeSep® R, 80/100 250°C 15g 16211HayeSep® S, 100/120 250°C 15g 16212HayeSep® T, 60/80 165°C 15g 16213HayeSep® T, 80/100 165°C 15g 16214HayeSep® T, 100/120 165°C 15g 162155% Krytox® 143AC on Graphpac® GB, 60/80 175°C 15g 8522Molecular Sieve 5A (washed), 60/80 350°C 50g 5604Molecular Sieve 5A (washed), 80/100 350°C 50g 5605Molecular Sieve 13X (washed), 60/80 350°C 50g 57730Molecular Sieve 13X (washed), 80/100 350°C 50g 577323% OV™-1 on Chromosorb® W-HP, 80/100 100/350°C 20g 1271610% OV™-101 on Chromosorb® P-AW, 80/100 100/350°C 20g 1621620% OV™-101 on Chromosorb® P-AW, 80/100 350°C 20g 162173% OV™-101 on Chromosorb® W-HP, 80/100 350°C 20g 120193% OV™-101 on Chromosorb® W-HP, 100/120 350°C 20g 1270020% OV™-101 on Chromosorb® P-AW, 80/100 350°C 20g 1621810% OV™-101 on Chromosorb® W-HP, 80/100 350°C 20g 127033% OV™-17 on Chromosorb® W-HP, 100/120 350°C 20g 120173% OV™-17 on Chromosorb® W-HP, 80/100 350°C 20g 127190.19% Picric Acid on Graphpac® GC, 80/100 120°C 15g 8550Porapak® N, 80/100 190°C 15g 16219Porapak® N, 100/120 190°C 15g 16220Porapak® P, 80/100 250°C 15g 16221Porapak® PS, 80/100 250°C 15g 16223Porapak® PS, 100/120 250°C 15g 16224Porapak® Q. 50/80 250°C 15g 16225Porapak® Q, 80/100 250°C 15g 16226Porapak® Q, 100/120 250°C 15g 16228Porapak® QS, 80/100 250°C 15g 16229Porapak® R, 80/100 250°C 15g 16230Porapak® S, 50/80 250°C 15g 16231Porapak® S, 80/100 250°C 15g 16232Porapak® T, 80/100 190°C 15g 16233Silica Gel Grade 12, 60/80 350°C 100g 5651Silica Gel Grade 12, 80/100 350°C 100g 565320% Squalane on Chromosorb® P-AW, 80/100 140°C 20g 1623515% Squalane on Chromosorb® P-AW-DCMS, 80/100 140°C 20g 16236Super Q, 80/100 250°C 10g 2735Tenax® TA, 60/80 350°C 10g 04916Tenax® TA, 80/100 350°C 10g 04917Tenax® GR, 60/80 350°C 10g 4937Unibeads® 1S, 60/80 200°C 25g 2752Unibeads® 2S, 60/80 200°C 25g 2760Unibeads® 3S, 60/80 200°C 25g 2764Unibeads® 3S, 80/100 200°C 25g 2766VZN-1, 60/80 50°C 10g 84621% TCEP on Carbograph® 1, 80/120 180°C 15g 16270


370 371

G C C O L U M N S

Packed Columns

Custom Coated Packings

TABLE 1 - BASE PRICE FOR CUSTOM COATED PACKINGS

SOLID SUPPORT20 GRAMSPART NO. PRICE

50 GRAMSPART NO. PRICE

100 GRAMS PART NO. PRICE

Chromosorb® G, W (HP) C-3004 C-3036 C-3068Chromosorb® G, W, or P (NAW, AW, DMCS) C-3006 C-3038 C-3070Chromosorb® T C-3008 C-3040 C-3072Chromosorb® 101-108 C-2031 C-2032 —Chromosorb® 750 C-3012 C-3044 C-3076Gas Chrom® S C-3018 C-3050 C-3082Gas Chrom® R C-3020 C-3052 C-3084Gas Chrom® 220, 254 C-3022 C-3054 C-3086Graphpac™ GC & GB (15 grams), Carbograph™ C-2200 — —Porapak® C-2041 C-2042 —Tenax® or HayeSep® (15 grams) C-3028 — —

TABLE 3 - GC STATIONARY PHASES

DESCRIPTION SOLVENTTEMP. LIMITS

°C USP CODE QTY. PART NO. PRICE

Apiezon® L C 50/300 — 25g 5017bis-(2-Ethoxyethyl) Adipate (BEEA) C 150 — 25g 5046Carbowax® 400 C 20/100 G20 100g 5051Carbowax® 20M C 60/225 G16 10g 5264DC-200, 350cstk (Methyl) C 20/250 — 100g 5251Dexsil® 300GC C 50/400 G33 1g 5092FFAP C 50/250 G35 20g 5156Hi-Eff®-1BP (Diethyleneglycol Succinate)[1] C 20/200 G4 25g 09505Igepal® CO-630 M 30/200 — 50g 5175OV™-1 (Methyl Gum) C 100/350 G2 10g 5293OV™-17 (50% Phenyl) A 20/350 G3 20g 5301OV™-101 (Methyl Fluid) C 20/350 G1 20g 5309OV™-275 (Dicyanoallyl) C 250+ — 5g 5314QF-1 (50% Trifluoropropyl) EA 20/250 — 25g 5269SE-30 (Methyl Gum) C 75/300 — 100g 5271Sebaconitrile C 150 — 20g 5244Silar® 5CP (50% Cyanopropyl Phenyl Silicone)[2] C 50/250 G7 10g 5246Silar® 9CP (90% Cyanopropyl Phenyl Silicone) C 50/250 G8 5g 08269Silar® 10C (100% Cyanopropyl Silicone)[3] C 50/250 G5 5g 5250Tetrahydroxyethylethylene Diamine (THEED) M 125 — 25g 5347[1] U.S. Patent #3,239,997, [2] U.S. Patent #3,960,521; [3] U.S.Patent #4,063,911

C=Chloroform; M=Methanol; MC=Methylene Chloride; W=Water; EA=Ethyl Acetate; A=Acetone; T=Toluene

Stationary Phases

Table 2 - Maximum Stationary Phase Loading for Solid SupportsMAX. % LOAD SUPPORTED MATERIAL MAX. % LOAD SUPPORTED MATERIAL MAX. % LOAD SUPPORTED MATERIAL

5% Chromosorb® G 12% Chromosorb® 750 2% Porapak®

15% Chromosorb® W 15% Gas Chrom® S, A, P, Z & Q 2% Super Q25% Chromosorb® A 30% Gas Chrom® R 12% T-Port-F30% Chromosorb® P 2% Gas Chrom® 220 & 254 2% HayeSep12% Chromosorb® T 0.5% Glass Beads 2% Tenax2% Chromosorb® 101-108 8% Graphpac™, Carbograph™ 15% Supelcoport

Custom Coated Packing Ordering Instructions:1. Choose your solid support from Table 1.2. Specify mesh range.3. Choose the stationary phase from Table 3 or 4. It is possible to

coat up to 3 stationary phases on one support).4. Specify % loading for each stationary phase. Note maximum %

loading guidelines for each support in Table 2.

Before ordering a custom coated packing, please check the list of stock pretested packings on p368-369 (called "Pretested" on these pages. You may find the packing you need in stock and at a savings.


370 371

G C C O L U M N S

Packed Columns

ADDITIONAL CHARGES FOR CUSTOM COATED PACKINGSDESCRIPTION PART NO. PRICE

Multiple Stationary Phases (per phase)Expensive Stationary Phases: Add the cost of the stationary phase used to base price

C-2000

Acetone Washing C-2700

Additional Stationary Phases for Custom Packings and Columns

Table 4 - Stationary PhasesAT™-1000 bis-(2-Ethoxyethyl) Sebacate (BEES) OV®-225Apiezon® H Glycerin OV®-330Apiezon® J Halocarbon 25-55 Grease OV®-351Apiezon® K Halocarbon Oil 14-25 Poly-A® 103Apiezon® N Hexadecanol Poly-A® 135BBBT Hi-Eff™ 1AP (Diethyleneglycol Adipate) Poly-I® 110Bentone 34 Hi-Eff™ 2AP (Ethyleneglycol Adipate) Poly-S® 176BHXBT Hi-Eff™ 2BP (Ethyleneglycol Succinate) Polyox 600MBMBT Hi-Eff™ 3BP (Neopentylglycol Succinate) PolyvinylpyrrolidoneBMEA Hi-Eff™ 3CP (Neopentylglycol Sebacate) Reoplex 400Carbowax® 540 Hi Eff™ 8AP (Cyclohexanedimethanol Adipate) SE-52Carbowax® 600 Hi-Eff™ 10BP (Phenyldiethanolamine Succinate) SE-54Carbowax® 1000 Igepal® CO-880 SF-96Carbowax® 1450 Igepal® CO-990 SorbitolCarbowax® 20M-TPA Kel-F® Oil No. 3 SPAN 80Castorwax Kel-F® Oil No. 10 SqualaneCS-10 Kel-F® Wax SUPEROX® 4N,N-bis-(2-Cyanoethyl) formamide (BCEF) Krytox 143AD SUPEROX® 20MDC-200 (500cstk) LAC 3-R-728 TCEPEDC-410 LAC 4-R-886 TCEPDC-550 LAC 5-R-737 β,β-ThiodipropionitrileDC-702 Lexan (Polycarbonate Resin) Triton® X-100Di-n-butyl Maleate Neopentylglycol Succinate Triton® X-305Didecyl Phthalate Octyldecyl Adipate TWEEN 80Di(2-ethylhexyl) Sebacate OV®-3 UC L-45Di(2-ethylhexyl) Phthalate OV®-7 UCON 50-HB-280-XDiglycerol OV®-17 Vinyl UCON 75-H-90,000Diisodecyl Phthalate OV®-22 UCON LB-135Dimethyl Sulfolane OV®-25 UCON LB-1715Dinonyl Phthalate OV®-73 UCON LB-550XECNSS-M OV®-105 UCON LB-1800-XEGSS-X OV®-202 UC W-98Ethofat 60-25 OV®-210 Versamide® 900

OV®-215 Versilube F-50

Contact Alltech Tech Support:

Email: [email protected] Online: www.alltechWEB.com

Need Technical Assistance?


372 373

2483 24852484

2486 24882487

2489 24912490

�

�

�

�

�

�

�

�

�

�

�

�

�

�

�

�

� �

�

� �

�

�

�

�

�

�

�

�

�

��

�

�

�

�

��

��

G C C O L U M N S

Packed Columns

Custom Packed Metal and PTFE ColumnsBefore ordering a custom packed GC column, consult the list of popular packed columns on page 366-367 to see

if the column you need is there. Each column comes complete with brass nuts and brass ferrules. For assistance or a quote, please contact Alltech Technical Support.

Coiling Schematics

Figure 1 Figure 3Figure 2



Certain expensive stationary phases and packings may require a surcharge. Be sure to state coiling instructions.

Custom metal and PTFE columns - ordering instructionsSpecify Coiling

1) Instrument Make and Model: ______________________

2) Confi guration Number: (see coiling schematics) ______

3) Dimensions: A= ______ in/mm (circle one)

B= ______ in/mm (circle one)

C= ______ in/mm (circle one)

D= ______ in/mm (circle one)

E= ______ in/mm (circle one)

F= ______ in/mm (circle one)

X= ______ in/mm (circle one)

4) Column Length: ______ ft/m (circle one)

5) Column i.d.: ______ in/mm (circle one)

6) Column o.d.: ______ in/mm (circle one)

7) Tubing Material: (circle one)Stainless Steel AT-Steel Nickel PTFE

TFE-Coated SS Aluminum Copper

8) Solid Support: ______ Mesh Size: ______

Specify PackingChoose either a Pretested Packing (p368-369) or create your own custom (refer to p370-371) by specifying information below:

9) Stationary Phase A: ______ % Loading: ______

Stationary Phase B*: ______ % Loading: ______

Stationary Phase C*: ______ % Loading: ______

10) Mirror Image:______ Please check if a mirror image is required.

11) Injection Port Design: (circle one)on-column not on-column

12) Stainless Steel Fittings:______ Please check if stainless steel fi ttings are required

(PN: C-14010N)

13) Preconditioning:______ Please check if column preconditioning is required

(PN: C-14005)

14) Other Special Instructions: (please be specifi c) ________________________________________________

________________________________________________

________________________________________________

*Additional charge applies to dual & triple coated packings (Part No. C-14020).

CUSTOM PACKED COLUMNSDESCRIPTION PART NO. PRICE

Custom Packed Columns (Specify all information from Table 1)

C-5000

Empty ColumnsEmpty Column with Fittings and Ferrules C-5100Additional Charges (per Column)Preconditioned Column C-14005Stainless Steel Fittings C-14010NDual and Triple Coated Packings C-14020


372 373

0043

5290

2513

4691

2514

4695

��

��

��

��

��

��

��

��

��

G C C O L U M N S

Packed Columns

SPECIAL SERVICES FOR GLASS COLUMNSDESCRIPTION PART NO. PRICE

Stainless Steel Fittings (Per Column) C-14010NPreconditioned Packing (Per Column) C-14005

Key to Configurations for Glass Columns

Deactiglas® Glass Columns• Silane treated for inertness• Precision bore glass for reproducibility• Brass fittings and vespel/graphite ferrules included• Available packed or empty

Alltech GC Columns are fabricated from precision-bore (2mm ±0.05mm or 4mm ±0.1mm i.d.) glass. All columns are 1/4" o.d. unless otherwise specified. Columns longer than 2 meters may have joints. Several additional services such as stainless steel fittings and preconditioning of the packing are available. Certain expensive stationary phases and packings may require a surcharge.

Due to space limitations we are not able to list all of the different manufacturers columns in our catalog. However, they are still available and can be specified at time of order placement. If you do not see your instrument on the following pages, please call Customer Service.

DEACTIGLAS® GLASS GC COLUMNSCHROMATOGRAPH CONFIGURATION LENGTH I.D. PACKED PART NO. PRICE EMPTY PART NO. PRICE

Hewlett Packard 5830, 5840, 5985On-Column InjectionA1 - 10.72" (272mm) 3ft 2mm 131122 131121A2 - 7.18" (182mm) 6ft 2mm C6067 6067S = 6" (152mm) 6ft 4mm C6076 6076

Not On-Column InjectionA1 - 8.95" (227mm) 3ft 2mm C6564 6564A2 - 9.25" (235mm) 6ft 2mm C6568 6568S = 6" (152mm) 6ft 4mm C6572 6572

On-Column InjectionA1 - 10.72" (272mm) 6ft 2mm C6055 6055A2 - 7.18" (182mm) 6ft 4mm C6061 6061S = 9" (229mm)

Not On-Column InjectionA1 - 8.95" (227mm) 6ft 2mm C6578 6578A2 - 9.25" (235mm) 6ft 4mm C6580 6580S = 9" (229mm)

Deactiglas® Column Ordering Instructions:1. Choose column configuration part no. below.2. Choose either a pretested packing (p368-369) or create a custom

packing (refer to p370-371) by specifying information below:Stationary Phase A % LoadingStationary Phase B % LoadingStationary Phase C % Loading


374 375

2515

4692

4693

2531

2530

G C C O L U M N S

Packed Columns

DEACTIGLAS® GLASS GC COLUMNS CONTINUEDCHROMATOGRAPH CONFIGURATION LENGTH I.D. PACKED PART NO. PRICE EMPTY PART NO. PRICE

Hewlett Packard 5880, 5890, 5987, 6890* 3ft 2mm 130962 1309613ft 4mm 130972 1309714ft 2mm C6082 6082

Confi guration A 4ft 4mm C6085 6085On-Column Injection 6ft 2mm C6087 6087A1 = 11.02" (280mm) 6ft 4mm C6089 6089A2 = 9.05" (230mm) 2m 2mm C6336 6336S = 9" (229mm) 2m 4mm C6343 6343FID 8ft 2mm C6347 6347

1.8m 3mm C6346 634610ft 2mm C6091 609110ft 4mm 131552 131551

6ft 22mm C6368 6368Confi guration B 6ft 4mm C6391 6391On-Column Injection 2m 2mm C6393 6393A1 = 11.02" (280mm) 2m 4mm C6396 6396A2 = 7.09" (180mm) 8ft 2mm C6413 6413S = 9" (229mm) 1.8m 3mm C6346 6346TCD 10ft 2mm C6431 6431

10ft 4mm C6435 6435

3ft 2mm C6427 64273ft 4mm C6433 6433

Confi guration C 4ft 2mm C6436 6436Not On-Column Injection 4ft 4mm C6440 6440A1 & A2 = 9.05" (230mm) 6ft 2mm C6442 6442S = 9" (229mm) 6ft 4mm C6445 6445All Detectors 2m 2mm C6447 6447Use with Liner or 2m 4mm C6449 6449Disposable Insert 8ft 2mm C6452 6452

2.4m 2mm C6454 645410ft 2mm C6456 645610ft 4mm C6460 6460

Perkin Elmer 115, 300, 900, 910, 990, F30, 2000, 2100, 3920, Sigma Series 2ft 2mm 132442 1324413ft 2mm 131432 1314313ft 4mm 131442 1314411m 2mm C6437 64374ft 2mm C6148 6148

Not On-Column Injection 4ft 4mm C6150 6150A1 = 9" (229mm) 6ft 2mm C6152 6152A2 = 9" (229mm) 6ft 4mm C6154 6154S = 8.75" (222mm) 2m 2mm C6439 6439

2m 4mm C6441 64418ft 2mm C6443 6443

2.4m 2mm C6446 644610ft 2mm C6105 610512ft 2mm C6448 6448

3ft 2mm C6451 64511m 2mm C6453 6453

On-Column Injection 6ft 2mm C6149 6149A1 = 12.62" (321mm) 6ft 4mm C6151 6151A2 = 7.09" (180mm) 2m 2mm C6455 6455S = 8.75" (222mm) 2m 4mm C6458 6458

2.4m 2mm C6462 646210ft 2mm C6106 6106

For explanation of A1, A2, and S, refer to key on Page 373.© Copyright 2004 Alltech Associates, Inc.© Copyright 2004 Alltech Associates, Inc.


374 375

2538

2539

2537

2534A

2534B

2549

G C C O L U M N S

Packed Columns


Perkin Elmer 8300, 8400, 8700 Series, 9000 Series, Autosystem3ft 2mm C6464 6464

Not On-Column Injection 1m 2mm C6466 6466A1 = 6.75" (171mm) 6ft 2mm C6479 6479A2 = 6.75" (171mm) 6ft 4mm C6482 6482S = 6.5" (165mm) 2m 2mm C6468 6468

2m 4mm C6584 65842.4m 2mm C6471 6471

3ft 2mm C6474 6474On-Column Injection 1m 2mm C6477 6477A1 = 12" (305mm) 4ft 2mm C6243 6243A2 = 6.75" (171mm) 4ft 4mm C6245 6245S = 6.5" (165mm) 6ft 2mm C6247 6247

6ft 4mm C6249 62492m 2mm C6484 6484

Shimadzu 4BF, 4BM, 4CM, 4MG, 6A, 6AM, 7AG (No Fittings Included) A1 = 13.2" (335mm) 1.7m 3mm C6509 6509A2 = 11.1" (282mm) 2m 2mm* C6349 6349S = 1.57" (40mm) 2m 3mm C6485 64855mm o.d. Tubing 2m 4mm* C6359 6359

2.5m 3mm C6515 6515Shimadzu 8A, RIA, GC-8A8IF (No Fittings Included)

1m 3mm C6489 6489A1 = 9" (229mm) 1.5m 2.6mm C6598 6598A2 = 9" (229mm) 1.5m 3mm C6658 6658S = 6" (152mm) 2m 2mm* C6281 628115mm o.d. Tubing 2m 2.6mm C6673 6673

2m 3mm C6493 64932m 4mm* C6334 6334

Shimadzu 7A, 9A, 12A, 14A, 14B, 15A, 16A (No Fittings Included)1m 2.6mm C6487 64871m 3mm C6497 6497

1.7m 2.6mm C6491 6491A1 = 10.69" (272mm) 1.7m 3mm C6495 6495A2 = 12.81" (327mm) 2m 2mm* C6337 6337S = 1.57" (40mm) 2m 2.6mm C6498 64985mm o.d. Tubing 2m 3mm C6499 6499

2m 4mm* C6367 63672.4m 2.6mm C6501 65012.4m 3mm C6505 6505

Varian 3300, 34003ft 2mm C6558 6558

Injector B to Detector B 4ft 2mm C6261 6261A1 = 9.5" (241mm) 4ft 4mm C6263 6263A2 = 8.1" (206mm) 6ft 2mm C6265 6265S = 6.82" (173mm) 6ft 4mm C6283 6283FID 2m 2mm C6340 6340

2m 4mm C6342 6342* 1/4" o.d. Column tapered to 5mm o.d. x 2.6mm i.d. ends.

For explanation of A1, A2, and S, refer to Page 373.


376 377

Column PackingDeactiglas®

ColumnInlet Liner

2mm i.d. Column

4mm i.d. ColumnGlass Wool

0050C

0050A

G C C O L U M N S

Packed Columns

For explanation of A1, A2, and S, refer to Page 373.


Varian 3300, 3400,3600, 3700, 4400, 4600, 6000 Vista Series 3ft 2mm 131662 1316613ft 4mm 131672 1316711m 2mm C6306 63061m 4mm C6308 6308

Injector A to Detector A 4ft 2mm C6189 6189A1 = 9.5" (241mm) 4ft 4mm C6190 6190A2 = 8.1" (206mm) 6ft 2mm C6191 6191S = 5.5" (140mm) 6ft 4mm C6192 6192FID 2m 2mm C6310 6310

2m 4mm C6312 63122.4m 2mm C6560 656010ft 2mm C6197 619710ft 4mm 131692 1316914m 2mm C6314 63144m 4mm C6316 6316

Varian Universal Columns 3300, 3400, 3600, 3700, 4400, 4600, 6000 Vista Series3ft 2mm C6562 65626ft 2mm C6206 6206

A1 = 9.5" (241mm) 6ft 4mm C6208 6208A2 = 2.25" (57mm) 2m 2mm C6356 6356S = N/A 2m 4mm C6358 6358FID, TCD, ECD 4m 2mm C6360 6360

4m 4mm C6366 6366

ADAPTER KITDESCRIPTION PART NO. PRICE

Universal Adapter Kit 6210

Hi-EFF® Pre-Columns• Extend column life• Reduce sample clean-up• Perform reaction chromatography• Perform subtraction chromatography

To order a Hi-EFF® Pre-Column, state catalog number and, if packed, describe the packing (% load, phase, support and mesh). Glass and glass-lined SS and columns are deactivated at no charge.

HI-EFF® PRE-COLUMNS

DESCRIPTION LENGTH QTY.PACKED

PART NO. PRICEEMPTY

PART NO. PRICE

1/8" SS 6" 6 5900 59101/4" Glass w/Guide 6" 6 5902 59121/8" Glass-Lined SS 6" 3 5904 59141/8" Bottom-Drilled SS Union

— ea — 5920

1/4" Bottom-Drilled SS Union

— ea — 5921

Deactiglas® Column Inlet Liners

• Prolong the life of your glass columns• Silane-treated for inertness• Available for 2mm or 4mm i.d. columns• Inserts directly into the end of your column

DEACTIGLAS® COLUMN INLET LINERSDESCRIPTION QTY. PART NO. PRICE

For 2mm i.d. Columns 10 6301For 2mm i.d. Columns 50 6302For 4mm i.d. Columns 10 6303For 4mm i.d. Columns 50 6304Glass Wool Inserter/Remover 2 6292

Universal Glass Column Adapters are available for the Varian 3000 and Varian 3700/VISTA Series. Please contact Customer Service for part numbers and prices.


376 377

G C C O L U M N S

Packed Columns

Chromosorb® Diatomite Supports

Specifications

CHROMOSORB®

SERIES TYPESURFACEAREA

PACKEDDENSITY

RECOMMENDEDLIQUID PHASE

LOAD

A Flux-calcined 2.7m2/g 0.48g/cc 25%G Flux-calcined 0.5m2/g 0.58g/cc 5%P Calcined 4.0m2/g 0.47g/cc 30%W Flux-calcined 1.0m2/g 0.24g/cc 15%

750 Flux-calcined 0.75m2/g 0.40g/cc 12%

Chromosorb® Treatment SpecificationsABBREVIATION TREATMENTS

NAW Untreated (non-acid washed)AW Acid washed (HCL is used) DMCS Dimethyldichlorosilane (silanized)HP High performance QC'd (acid washed, silanized,

flux-calcined)

CHROMOSORB® DIATOMITE SUPPORTSDESCRIPTION QTY. PART NO. PRICE

Chromosorb® A-NAW20/30 454g 243145/60 454g 243260/80 454g 2433Chromosorb® G-NAW45/60 225g 2372160/80 225g 2373180/100 225g 23741100/120 225g 23751120/140 225g 23761Chromosorb® G-AW45/60 225g 2382160/80 225g 2383180/100 225g 23841100/120 225g 23851Chromosorb® G-AW-DMCS45/60 225g 2392160/80 225g 2393180/100 225g 23941100/120 225g 23951120/140 225g 23961Chromosorb® G-HP60/80 225g 239680/100 225g 2397100/120 225g 2398120/140 225g 2444

Chromosorb® A, G, P and W are available in both untreated and treated forms, as well as in a choice of various mesh ranges.

CHROMOSORB® DIATOMITE SUPPORTS CONTINUEDDESCRIPTION QTY. PART NO. PRICE

Chromosorb® P-NAW30/60 454g 230445/60 454g 230560/80 454g 230680/100 454g 2307100/120 454g 2308Chromosorb® P-AW30/60 454g 231445/60 454g 231560/80 454g 231680/100 454g 2317100/120 454g 2318Chromosorb® P-AW-DMCS45/60 454g 232360/80 454g 232480/100 454g 2325100/120 454g 2326Chromosorb® W-NAW30/60 150g 2333145/60 150g 2334160/80 150g 2335180/100 150g 23361100/120 150g 23371120/140 150g 23381Chromosorb® W-AW30/60 150g 2345145/60 150g 2346160/80 150g 2347180/100 150g 23481100/120 150g 23491Chromosorb® W-AW-DMCS45/60 150g 2358160/80 150g 2359180/100 150g 23601100/120 150g 23611Chromosorb® W-HP60/80 150g 2440180/100 150g 23651100/120 150g 23661120/140 150g 24421

CHROMOSORB® 750DESCRIPTION QTY. PART NO. PRICE

60/80 100g 239980/100 100g 2400100/120 100g 2401

Chromosorb® 750• Designed specifically for biomedical and pesticide

analyses

Chromosorb® 750 is the most inert and highly efficient support material in the series. This support material is acid-washed, DMCS treated, and carefully screened.


378 379

G C C O L U M N S

Packed Columns

Gas Chrom®

Gas Chrom® S is white diatomaceous earth that is screened and is non acid washed. Use as a filtering agent or trapping material.

Gas Chrom® R is red diatomaceous earth that is screened and water washed to neutrality.

Gas Chrom® Porous Polymers 220 and 254 are low in residual monomers and contaminants, condition faster and have lower column bleed.

GAS CHROM®

DESCRIPTION QTY. PART NO. PRICE

Gas Chrom® S80/100 100g 03010Gas Chrom® R40/60 100g 495660/80 100g 496680/100 100g 4976Gas Chrom® Porous Polymer 220, 80/100 25g 2484254, 80/100 25g 2486Stock Packed Columns6ft x 1/8" SS Column with Gas Chrom® Porous Polymer 220, 80/100

ea 2484PC

6ft x 1/8" SS Column with Gas Chrom® Porous Polymer 254, 80/100

ea 2486PC

T-Port-F

T-Port-F is a screened tetrafluoroethylene support useful for analysis of very polar compounds. It has a density of about 0.5g/cc with a maximum temperature limit of 150°C.

Chromosorb® T

Chromosorb® T is a support material made from PTFE and is useful for the analysis of polar compounds such as water, hydrazine, sulfur dioxide, etc.

Chromosorb® T melts at 327°C, starts to decompose at 290°C, and fuses together under prolonged use at 250°C. The density is 0.42g/cc. The surface area is 7-8m2/g and maximum loading capacity is 12%. When packing, chill the material below 19°C.

Activated Alumina

Activated alumina is useful for the analysis of light hydrocarbons. Unsaturated hydrocarbons are retained longer than saturated ones. Grade F-6 is an indicating alumina which turns from blue to pink upon adsorption of water. The maximum temperature limit is 300°C.

Glass Beads

Glass beads can be loaded up to 0.5 wt. % before becoming tacky. Two types are available: untreated (regular) or dimethyldichlorosilane (DMCS)-treated.

SpecificationsGAS CHROM® 254 GAS CHROM® 220

Pore Size: 3000nm 10nmSurface Area: 1000m2/g 450m2/gEquivalents: Porapak® P Porapak® Q

GLASS BEADSDESCRIPTION QTY. PART NO. PRICE

Regular, 60/80 mesh 125g 5420Regular, 80/100 mesh 125g 5422Regular, 100/120 mesh 125g 5424DMCS Treated, 60/80 mesh 125g 5426DMCS Treated, 80/100 mesh 125g 5428DMCS Treated, 100/120 mesh 125g 5430

ACTIVATED ALUMINADESCRIPTION QTY. PART NO. PRICE

Grade F-140/60 100g 566260/80 100g 566480/100 100g 5666100/120 100g 5668Grade F-68/14 100g 05561Stock Packed Column5ft x 1/8" SS Packed with Alumina Grade F-1, 60/80

Ea 5664PC

CHROMOSORB® TDESCRIPTION QTY. PART NO. PRICE

30/60 225g 2437140/60 225g 24381

T-PORT-FDESCRIPTION QTY. PART NO. PRICE

30/60 50g 244760/80 50g 244880/100 50g 2449

GC Supports


378 379

G C C O L U M N S

Packed Columns

Silica Gel

Silica Gel is used for the analysis of fixed gases and light hydrocarbons. It is also useful for dehydration of gases and liquids.

Grade 42 Indicating Silica Gel changes from blue to pink as it becomes saturated with water. It conforms to MIL-D-3716 Type IV Grade H. It will absorb water up to about 40% by weight. The maximum temperature limit is 350°C.

Chemipack® C18

Chemipack® C18 is a chemically bonded GC packing. Because it is bonded, it has high thermal stability, zero bleed and stability to water. These properties make it ideal for GC/MS or high sensitivity GC with any detector. The functional group bonded to the silica is octadecyl.

Carbosphere™ - Carbon Molecular Sieve

Carbosphere™ exhibits properties similar to molecular sieves. It has a surface area of about 1000m2/g with a pore size of about 13Å. Carbosphere™ separates oxygen, nitrogen, methane, carbon monoxide, and carbon dioxide in the same run. It also separates air, carbon dioxide, and the C1-C2 hydrocarbons. At ambient temperatures, hydrogen will elute before oxygen.

Carbosphere™ resolves trace amounts of methane and acetylene in ethylene and even trace amounts of methane, acetylene, and ethylene in ethane. The carbon molecular sieves also separate oxides of nitrogen and sulfur. Because Carbosphere™ is very nonretentive for water, rapid separations of organics, such as formaldehyde and methanol in water are possible.

It is important to remove every trace of oxygen from the carrier gas used on Carbosphere™ columns. This is essential if you are doing trace analysis or using temperatures above 200°C. Alltech’s Oxy-Trap™ and Indicating Oxy-Trap™ are ideal for removal of oxygen from carrier gas. Carbosphere™ can be affected by contaminants in the air and in carrier gas. Store under pure nitrogen or argon gas.

Unibeads® S

The Unibeads® S series consists of spherical porous silica beads. Unibeads® 2S are comparable to Porasil® A. Unibeads® 3S are similar to Porasil® B. The smaller the pore size, the greater the retention for hydrocarbons.

SILICA GEL

DESCRIPTION100 GRAMSPART NO. PRICE

1KGPART NO. PRICE

Grade 1240/60 5650 0553260/80 5651 0553380/100 5653 05534100/120 5655 05535Grade 1535/60 5648 05545Indicating Silica Gel, Grade 426/16 05559 05560Stock Packed Column18ft x 1/8" SS Packed with Silica Gel, 60/80, ea

5651PC

CHEMIPACK®


Chemipack® C18, 80/100, 320°C 15mL 2768Stock Packed Column6ft x 1/8" SS Packed with Chemipack® C18, 80/100, 320°C

ea 2768PC

UNIBEADS® SDESCRIPTION QTY. PART NO. PRICE

1S, 60/80, 22A 25g 27521S, 80/100, 22A 25g 27582S, 60/80, 60A 25g 27602S, 80/100, 60A 25g 27623S, 60/80, 100A 25g 27643S, 80/100, 100A 25g 2766Stock Packed Column6ft x 1/8" SS Packed with Unibeads® 1S, 60/80

ea 2752PC

6ft x 1/8" SS Packed with Unibeads® 2S, 60/80

ea 2760PC

CARBOSPHERE™


60/80 5g 568080/100 5g 5682Stock Packed Columns6ft x 1/8" SS Packed with Carbosphere™, 60/80

ea 5680PC

6ft x 1/8" SS Packed with Carbosphere™, 80/100

ea 5682PC

10ft x 1/8" SS Packed with Carbosphere™, 80/100

ea 56821PC


380 381

G C C O L U M N S

Packed Columns

Molecular Sieves• For drying applications

Molecular sieves are synthetic alkali metal alumino-silicates with various cations. They are used for the separation of fixed gases and drying of liquid or gas streams. They can be reactivated by heating at 250°C for 12 hours; 300°C for 4 hours; or 350°C for 2 hours.

Molindicator®

Molindicator® is a moisture-indicating molecular sieve. At full activity, it is bright blue in color. The blue color will turn to buff as water is adsorbed.

Washed Molecular Sieves• For chromatography applications

The usual gas chromatographic grades of molecular sieves have a fine dust adhering to each particle which cannot be removed simply by careful sieving. This dust is responsible for poorer separations and higher pressure drops than molecular sieves which are essentially dust-free.

The washed molecular sieves offered here have been carefully cleaned of dust particles by washing with distilled water. The cleaned product is then activated and sealed in glass jars. Molecular Sieves are typically reactivated at a temperature of 300°C for four hours.

MOLECULAR SIEVES

DESCRIPTION100 GRAMSPART NO. PRICE

1KGPART NO. PRICE

Molecular Sieve 3A1/8" Pellets 05252 052531/16" Pellets 05254 0525540/60 05306 0529560/80 05307 0529880/100 05308 05301100/120 05309 05304Molecular Sieve 4A8/12 Beads 05256 052571/8" Pellets 05258 052591/16" Pellets 05260 0526140/60 5620 0534560/80 5622 0534880/100 5624 05351100/120 5625 05355Molecular Sieve 5A1/8" Pellets 05264 052651/16" Pellets 5633 0526740/60 5626 0532760/80 5328 0533080/100 5630 05333100/120 5632 05336Molecular Sieve 13X8/12 Beads 05268 052691/8" Pellets 05270 052711/16" Pellets 05272 0527340/60 5634 0549360/80 5636 0549680/100 5638 05499100/120 5640 05502

MOLINDICATOR®


8/12 100g 055521000g 05553

WASHED MOLECULAR SIEVES


Washed Molecular Sieve 5A40/60 50g 560260/80 50g 560480/100 50g 5605100/120 50g 5606Washed Molecular Sieve 13X40/60 50g 5772860/80 50g 5773080/100 50g 57732100/120 50g 57734Stock Packed Columns6ft x 1/8" SS Packed with 80/100 Washed 5A

ea 5605PC

6ft x 1/8" SS Packed with 80/100 Washed 13X

ea 5773PC

5ft x 1/8" SS Packed with 60/80 Washed 13X

ea 57730PC

GC Supports

Need more information on Gas Chromatography?

GC BOOKDESCRIPTION PART NO. PRICE

Modern Practice of Gas Chromatography 1166


380 381

G C C O L U M N S

Packed Columns

CARBOGRAPH™


UncoatedCarbograph™ 1-TD, 20/40, >500°C 15g 1740Carbograph™ 1, 60/80, >500°C 10g 1722Carbograph™ 1 80/120, >500°C 10g 1724Carbograph™ 2-TD, 20/40, >500°C 15g 1745Carbograph™ 2, 60/80, >500°C 10g 1726Carbograph™ 2, 80/100, >500°C 10g 1728Carbograph™ 1-SC, 40/60, 225°C 10g 1734Coated1% AT™-1000 on Carbograph™ 1 60/80, 225°C 15g 17330.1% AT™-1000 on Carbograph™ 2 80/100, 225°C 15g 17374% Carbowax® 20M on Carbograph™ 1 DA 80/120, 200°C

15g 17271

0.2% Carbowax® 1500 on Carbograph™ 2 60/80, 175°C

15g 1725

0.2% Carbowax® 1500 on Carbograph™ 2 80/100, 175°C

15g 1720

5% Carbowax® 20M on Carbograph™ 1 AW 80/120, 225°C

15g 1729

6.6% Carbowax® 20M on Carbograph™ 1 AW 80/120, 225°C

15g 1731

4% Carbowax® 20M + 0.8% KOH on Carbograph™ 1 60/80, 220°C

15g 1735

0.19% Picric Acid on Carbograph™ 2 80/100, 120°C

15g 1736

0.8% THEED on Carbograph™ 2 80/100, 125°C 15g 1942

Carbograph™

Graphitized Carbon Blacks• High speed analysis• Extremely hydrophobic - ideal for aqueous injections

Equivalent to the Carbopack packings. Carbograph™ packings can be modified with a stationary phase giving them unique selectivities.

Carbograph™ 1

Equivalent to Carbopack™ B. It has a surface area of 100m2/g. Carbograph™ 1-TD has a coarse mesh of 20/40 which is suitable for thermal desorption work. Maximum temperature 500°C.

Carbograph™ 1SC

Similar to Carbopack™ BHT, specifically for the separation of sulfur compounds. It has a mesh of 40/60, and a maximum temperature of 225°C.

Carbograph™ 2

Equivalent to Carbopack™ C. It has a specific surface of 10m2/g for the separation of volatile organic compounds. Carbograph™ 2-TD has a coarse mesh of 20/40 which is suitable for thermal desorption work. Maximum temperature 500°C.

GRAPHPAC™


Graphpac™-GC0.1% Alltech AT™-1000, 225°C, 80/100 15g 85420.2% Carbowax® 1500, 175°C, 80/100 15g 85460.19% Picric Acid, 120°C, 80/100 15g 85500.8% THEED, 125°C, 80/100 15g 8552Uncoated, 60/80 15g 8536 Uncoated, 80/100 15g 8538Custom – Specify Phase and % Loading 15g C-2200Graphpac™-GB1% Alltech AT™-1000, 225°C, 60/80 15g 85174% Carbowax® 20M + 0.8% KOH Amines, 220°C, 60/80

15g 8519

Uncoated, 60/80 15g 8513Uncoated, Acid Washed, 60/80 15g 8533Custom – Specify Phase, Mesh, and % Loading

15g C-2200

Custom, Acid Washed – Specify Phase, Mesh, and % Loading

15g C-2300

Stock Packed Columns6ft x 1/8" SS Packed with 0.1% AT™-1000, 225°C, 80/100

ea 8542PC

6ft x 1/8" SS Packed with 0.2% Carbowax® 1500, 175°C, 80/100

ea 8546PC

7ft x 1/8" SS Packed with 0.19% Picric Acid, 120°C 80/100

ea 85501PC

10ft x 1/8" SS Packed with 5% Krytox® 143C, 60/80

ea 85222

Graphpac™-GC and -GB• Graphitized carbon• Inert, non-specific surface• Unique separation properties• Optimized phase loading• Hydrophobic – ideal for aqueous injections

Graphpac™-GC has an average surface area of 10-13m2/g, while Graphpac™-GB has a larger surface area of 100-110m2/g. Both types interact with samples almost completely by non-specific adsorption. Which results in unique separations not achievable with fused silica open tubular (FSOT) capillary columns. Alcohols, hydrocarbons, and acids are separated in series according to carbon number.

The carbons possess partitioning capabilities as uncoated packings, use stationary phases to modify the selectivity of these carbons.


382 383

G C C O L U M N S

Packed Columns

Tenax®-TA (GC) • Stable baseline after conditioning • Short retention times • Low affi nity for water • Maximum temperature limit is 350°C

Tenax®-TA is a porous polymer that is based on 2,6-Diphenyl-p-phenylene Oxide. It has replaced Tenax®-GC. Tenax®-TA can be used as a packing and as a trapping material. Both the EPA and NIOSH specify the use of Tenax® in their standard methods. Tenax® is particularly useful for the analysis of high boiling com pounds such as alcohols, poly eth yl ene glycols, diols, phe nols, monoamines and diamines, eth a no lamines, al de hydes, ketones and chlorinated aromatics.

Tenax®-GR• Superior properties as trapping material• Maximum temperature limit is 350°C

Tenax®-GR contains 23% graphitized carbon as an integral part of the material. This is not an admixture; the graphitized carbon is co-precipitated with the Tenax® polymer. The resulting material gives higher break-through volumes for most materials, yet is less water retentive than Tenax®-TA. When using this material for packing GC columns, better peak sym me try is observed. Surface area is 24.1m2/g.

Specifi cationsSpecifi c Surface Area: 35m2/gPore Volume: 2.4g/ccAverage Pore Size: 200nmDensity: 0.25g/cc

Conditioning

We highly recommend that Tenax®, like all other porous poly mers, be preconditioned before being packed into GC col umns. This removes most of the shrinkage

of the polymer and min i miz es the need for further conditioning. Tenax® can be expected to shrink further in use.

TENAX®-TA (GC)DESCRIPTION QTY. PART NO. PRICE

20/35 10g 0491420/35 100g 04914120/35 500g 04914220/35 1000g 04914335/60 10g 0491535/60 100g 04915135/60 500g 04915235/60 1000g 04915360/80 10g 0491660/80 100g 04916160/80 500g 04916260/80 1000g 04916380/100 10g 0491780/100 100g 04917180/100 500g 04917280/100 1000g 049173Pretreated Tenax® -TACleaned by Solvent Extraction C-4196Stocked Packed Columns6ft x 1/8" SS Packed with Tenax®-TA Porous Polymer, 60/80

ea 4900PC

6ft x 1/8" SS Packed with Tenax®-TA Porous Polymer, 80/100

ea 4901PC

Tenax®-TA - Membranes, 47mm 10 4943

TENAX®-GRDESCRIPTION QTY. PART NO. PRICE

20/35 10g 493320/35 100g 4933120/35 500g 4933220/35 1000g 4933335/60 10g 493535/60 100g 4935135/60 500g 4935235/60 1000g 4935360/80 10g 493760/80 100g 4937160/80 500g 4937260/80 1000g 4937380/100 10g 493980/100 100g 4939180/100 500g 4939280/100 1000g 49393Stocked Packed Columns6ft x 1/8" SS Packed with Tenax®-GR Porous Polymer, 60/80

ea 4937PC

For additional information on Tenax® products, request datasheets 04914 and 4943.


382 383

G C C O L U M N S

Packed Columns

HAYESEP®


HayeSep® A60/80, 165°C 75cc 281880/100, 165°C 75cc 2819100/120, 165°C 75cc 282020/140, 165°C 75cc 2821HayeSep® B60/80, 190°C 75cc 282280/100, 190°C 75cc 2823100/120, 190°C 75cc 2824HayeSep® C60/80, 250°C 75cc 282580/100, 250°C 75cc 2826100/120, 250°C 75cc 2827HayeSep® D60/80, 290°C 75cc 282880/100, 290°C 75cc 2829100/120, 290°C 75cc 2830

HAYESEP® CONTINUEDDESCRIPTION QTY. PART NO. PRICE

HayeSep® DB60/80, 290°C 75cc 283480/100, 290°C 75cc 2835100/120, 290°C 75cc 2836HayeSep® DIP

60/80, 290°C 75cc 283180/100, 290°C 75cc 2832100/120, 290°C 75cc 2833HayeSep® N60/80, 165°C 75cc 281580/100, 165°C 75cc 2816100/120, 165°C 75cc 2817HayeSep® P60/80, 250°C 75cc 280380/100, 250°C 75cc 2804100/120, 250°C 75cc 2805HayeSep® Q60/80, 275°C 75cc 280080/100, 275°C 75cc 2801100/120, 275°C 75cc 2802HayeSep® R60/80, 250°C 75cc 280680/100, 250°C 75cc 2807100/120, 250°C 75cc 2808HayeSep® S60/80, 250°C 75cc 280980/100, 250°C 75cc 2810100/120, 250°C 75cc 2811HayeSep® T60/80, 165°C 75cc 281280/100, 165°C 75cc 2813100/120, 165°C 75cc 2814Stock Packed Columns40ft x 1/8" SS Packed with HayeSep® A, 120/140, 165°C

ea 28211

10ft x 1/8" SS Packed with HayeSep® D, 100/120, 290°C

ea 28301PC

20ft x 1/8" NI Packed with HayeSep® D, 100/120, 290°C

ea 27082PC

30ft x 1/8" SS Packed with HayeSep® D, 100/120, 290°C

ea 27083PC

30ft x 1/8" SS Packed with HayeSep® DB, 100/120, 290°C

ea 2836PC

9ft x 1/8" SS HayeSep® DIP, 100/120, 290°C

ea 2833PC

8ft x 1/8" SS Packed with HayeSep® P, 60/80, 250°C

ea 2803PC

6ft x 1/8" SS Packed with HayeSep® P, 80/100, 250°C

75cc 2804PC

6ft x 1/8" SS Packed with HayeSep® Q, 80/100, 275°C

ea 2801PC

8ft x 1/8" SS Packed with HayeSep® Q, 80/100, 275°C

ea 28010PC

6ft x 1/8" SS Packed with HayeSep® R, 80/100, 250°C

ea 2807PC

6ft x 1/8" SS Packed with HayeSep® S, 100/120, 250°C

ea 2811PC

6ft x 1/8" SS Packed with HayeSep® T, 80/100, 165°C

ea 2813PC

5ft x 1/8" SS Packed with HayeSep® T, 100/120, 165°C

ea 2814PC

HayeSep® • Pre-purified porous polymers for GC• Less bleed and shrinkage than other porous polymers• Cleaned and conditioned to 200°C (165°C for N & T)

HayeSep® polymers were developed to solve room temperature separation of N2, O2, Ar and CO; ppm H2O in the presence of HCl, Cl2 etc. with HayeSep® R; and many others. The HayeSep® D series better separates the fixed gases to the C2 hydrocarbons.

Specifications

HAYESEP® SERIES POLYMER COMPOSITION

SURFACE AREA

(M2/G) POLARITY

Q DVB* 582 Non-polarP DVB*/Styrene 165 Slightly PolarR DVB*/N-Vinyl-2-

pyrrolidinone344 Moderately Polar

S DVB*/4-Vinyl-pyridine 583 Moderately PolarT EGDM** 250 Very PolarN DVB*/EGDM** 405 Very PolarA DVB*/EGDM** (high

purity)526 Moderately Polar

B DVB*/Polyethyleneimine 608 Very PolarC DVB*/Acrylonitrile 442 Moderately PolarD DVB* (high purity) 795 Non-Polar

* Divinylbenzene. ** Ethyleneglycoldimethacrylate.

Table 1 – Retention Time (in minutes)AIR CH4 CO2 C2H2 C2H4 C2H6 H2O

DIP 0.9 1.7 3.1 5.4 5.8 8.3 9.0D 0.9 1.7 3.1 5.8 6.1 8.4 8.6DOX 1.0 1.8 3.2 5.9 6.3 8.5 8.3DB 0.9 1.6 3.1 6.1 6.6 8.7 8.1

†Retention data based on 10ft x 1/8" SS at 45°C, 30mL/min.

Comparison of HayeSep® “D” Formulations†


384

G C C O L U M N S

Packed Columns

PORAPAK®


Porapak® Q50/80, 250°C 26g 270080/100, 250°C 26g 2701100/120, 250°C 26g 2702Super Q80/100 10g 2735Super Q Stock Packed Column6ft x 1/8" SS Packed with Super Q Polymer, 80/100

ea 2735PC

30" x 1/8" TFE Packed with 18" of Super Q Polymer, 80/100

ea 9781

Porapak® P50/80, 250°C 20g 270380/100, 250°C 20g 2704100/120, 250°C 20g 2705Porapak® R50/80, 250°C 24g 270680/100, 250°C 24g 2707100/120, 250°C 24g 2708Porapak® S50/80, 250°C 26g 270980/100, 250°C 26g 2710100/120, 250°C 26g 2711Porapak® T50/80, 190°C 31g 271280/100, 190°C 31g 2713100/120, 190°C 31g 2714Porapak® N50/80, 190°C 29g 271580/100, 190°C 29g 2716100/120, 190°C 29g 2717Porapak® QS50/80, 250°C 26g 271880/100, 250°C 26g 2719100/120, 250°C 26g 2720Porapak® PS50/80, 250°C 20g 272180/100, 250°C 20g 2722100/120, 250°C 20g 2723Acetone Washing Service† per bottle C-2700†Specify bulk packing part no. in addition to acetone washing part no.

Century Series Chromosorb®

Century Series Chromosorb® porous polymers have a rigid structure and distinct pore size. They are packed into columns in the normal manner and do not require a liquid coating. We recommend preconditioning all porous polymers before packing columns.

Porapak® Porapak® GC packings are cross-linked polymers which

can be used directly in GC columns without a stationary phase coating. Acetone washing of Porapaks® improves performance.

SpecificationsCHROMOSORB®

SERIES POLYMER COMPOSITIONSURFACE AREA

(M2/G) POLARITY

101 DVB*/Styrene >50 Non-Polar102 DVB*/Styrene 300-400 Slightly Polar103 Cross-linked

Polystyrene**15-25 Non-Polar

105 Polyaromatic 600-700 Mod. Polar106 Cross-linked Polystyrene 700-800 Non-Polar107 Cross-linked Acrylic Ester 400-500 Polar108 Cross-linked Acrylic 100-200 Polar

*Divinylbenzene. **The surface is Basic.

SpecificationsPORAPAK®

SERIES POLYMER COMPOSITIONSURFACE AREA

(M2/G) POLARITY

Q DVB*/Ethylvinylbenzene 500-600 Slightly PolarSuper Q Modified Q

P DVB*/Styrene 100-200 Non-PolarR DVB*/Vinyl pyrrolidinone 450-600 Mod. PolarS DVB*/Vinyl pyridine 300-450 Mod. PolarT EGDM** 225-350 PolarN DVB*/Vinyl pyrrolidinone 250-350 Very Polar

* Divinylbenzene, ** Ethyleneglycoldimethacrylate

CHROMOSORB®


Chromosorb® 10160/80, 275/325°C 50g 240580/100, 275/325°C 50g 2406100/120, 275/325°C 50g 2407Chromosorb® 10260/80 250/300°C 50g 240880/100, 250/300°C 50g 2409100/120, 250/300°C 50g 2410Chromosorb® 10360/80, 250/300°C 50g 241180/100, 250/300°C 50g 2412100/120, 250/300°C 50g 2413Chromosorb® 10560/80, 250/275°C 50g 241780/100, 250/275°C 50g 2418100/120, 250/275°C 50g 2419Chromosorb® 106,60/80, 250/275°C 50g 242080/100, 250/275°C 50g 2421100/120, 250/275°C 50g 2422Chromosorb® 10760/80, 250/275°C 50g 242380/100, 250/275°C 50g 2424100/120, 250/275°C 50g 2425Chromosorb® 10860/80, 250/275°C 50g 2426 80/100, 250/275°C 50g 2427100/120, 250/275°C 50g 2428Preconditioning Service† per bottle C-14030†Specify bulk packing part no. and preconditioning service part no.

gc section - allpump.co.kr · copyright 2004 alltech associates, inc. ®™ ™™™-™...

Documents