crescent chemical co., inc

1
FREE 900-PAGE CRESCENT CATALOG of over 8500 Riedel-deHaën LABORATORY CHEMICALS Reagents for analysis Solvents Products for synthesis • Products tor chromatography • Industrial chemicals FREE SPECIALTY BROCHURE ON HYDRANAL • The new Pyridine-free Karl Fischer reagent — is now available. • Greater accuracy and end point stability. Rapid titration speed 35 pages of technical data in brochure I Working together so you can do more! Crescent Chemical, distributor of Riedel-de Haën's enormous inventory, offers you these valuable publications ABSOLUTELY FREE! To receive them, return the ' reply form now, or call (515) 348-0333. Crescent Chemical Co., Inc. 1324 Motor Parkway · Hauppauge, NY 11788 Please send the following: Ζ 900-PAGE CRESCENT CATALOG of Riedel-de Haën laboratory chemicals Ζ HYDRANAL* -Eugen Scholz Reagent for the determination of water according to Karl Fischer The areas I am most interested in are: Ζ Analytical chemistry ζ Fluorine/bromine Ζ Chromatography chemistry Reagents and lab Ζ Karl Fischer analysis chemicals ζ Residue analysis Ζ Microscopy ζ Research NAME Letters Dr. Perry also claims that I was wrong in referring to the lack of some basic discussions. For example, I men- tioned that the retention index is not explained, and his answer is that it is discussed in four pages. However, no- where is its meaning explained, that it corresponds to the carbon number (X 100) of a hypothetical η -paraffin with the same retention characteristics. Also, while the fundamental equation is treated in detail, the conclusions are not drawn. For example, in pp 43-53, the variation in liquid loading is dis- cussed historically but is not related at all to the last term of equation 4.8. If the capacity factor (k) is small, ways must be found to increase it, while if k is large, one tries to reduce it. Such a discussion is much more important than showing how equations are rear- ranged, moving a term from the right- hand side to the other or vice versa, which is elementary mathematics. Dr. Perry complains that I did not mention some features that are "sin- gular to this book" such as an elabo- rate treatment of open tubular col- umns or of fused-silica columns. But these are self-evident in a general book on gas chromatography pub- lished in 1981. Would you praise a book dealing with basic mathematics because it also discusses multiplica- tion? I could continue and present a re- buttal of each point in Dr. Perry's let- ter; however, I feel that this is unnec- essary. Rather, permit me to make a general statement. A book review is not promotional material extolling the virtues of the particular book. Rather it represents the personal opinion of the reviewer who is selected by the editor of the journal because of his familiarity with the topics. Also, a review is not a sci- entific paper in which every statement must be explained and proven. The author may or may not agree with the reviewer. However, the author can be sure that the reviewer had good rea- sons for every statement in the review, even if he did not elaborate in detail; after all, only summary conclusions can be given in 500-600 words. In my review of Dr. Perry's book I characterized it as a useful general text for GC training courses and ex- pressed my opinion that, in spite of a number of shortcomings, it fills many of the requirements for a serious, modern general textbook on gas chro- matography. There is nothing I can add to this opinion. L. S. Ettre Norwalk, Conn. |^/AREX .. . where innovation is the way to the future Producers of: Innovative Analytical Instruments 1 Chromatography 1 Spectroscopy Data Handling Special Products 1 Accessories For information contact: VAREX Corporation 11600 Nebel Street Rockville, MD 20852. USA (301) 984-7760 TWX: 710-828-9816 COMPANY ADDRESS CITY STATE ZIP M M V M M M M M H M M M M I M M M I CIRCLE 37 ON READER SERVICE CARD CIRCLE 218 ON READER SERVICE CARD 424 A · ANALYTICAL CHEMISTRY, VOL. 54, NO. 3, MARCH 1982 VAREX

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Page 1: Crescent Chemical Co., Inc

FREE

900-PAGE CRESCENT CATALOG

of over 8500 Riedel-deHaën

LABORATORY CHEMICALS

• Reagents for analysis • Solvents • Products for synthesis • Products tor chromatography • Industrial chemicals

FREE SPECIALTY BROCHURE ON HYDRANAL • The new Pyridine-free

Karl Fischer reagent — is now available.

• Greater accuracy and end point stability.

Rapid titration speed 35 pages of technical data in brochure

I Working together so you can do more! Crescent Chemical, distributor of Riedel-de Haën's enormous inventory, offers you these valuable publications ABSOLUTELY FREE!

To receive them, return the ' reply form now, or call (515) 348-0333.

Crescent Chemical Co., Inc. 1324 Motor Parkway · Hauppauge, NY 11788

Please send the following: Ζ 900-PAGE CRESCENT CATALOG of

Riedel-de Haën laboratory chemicals

Ζ HYDRANAL* -Eugen Scholz Reagent for the determination of water according to Karl Fischer

The areas I am most interested in are: Ζ Analytical chemistry ζ Fluorine/bromine Ζ Chromatography chemistry — Reagents and lab Ζ Karl Fischer analysis

chemicals ζ Residue analysis Ζ Microscopy ζ Research

NAME

Letters

Dr. Perry also claims that I was wrong in referring to the lack of some basic discussions. For example, I men­tioned that the retention index is not explained, and his answer is that it is discussed in four pages. However, no­where is its meaning explained, that it corresponds to the carbon number (X 100) of a hypothetical η -paraffin with the same retention characteristics. Also, while the fundamental equation is treated in detail, the conclusions are not drawn. For example, in pp 43-53, the variation in liquid loading is dis­cussed historically but is not related at all to the last term of equation 4.8. If the capacity factor (k) is small, ways must be found to increase it, while if k is large, one tries to reduce it. Such a discussion is much more important than showing how equations are rear­ranged, moving a term from the right-hand side to the other or vice versa, which is elementary mathematics.

Dr. Perry complains that I did not mention some features that are "sin­gular to this book" such as an elabo­rate treatment of open tubular col­umns or of fused-silica columns. But these are self-evident in a general book on gas chromatography pub­lished in 1981. Would you praise a book dealing with basic mathematics because it also discusses multiplica­tion?

I could continue and present a re­buttal of each point in Dr. Perry's let­ter; however, I feel that this is unnec­essary. Rather, permit me to make a general statement.

A book review is not promotional material extolling the virtues of the particular book. Rather it represents the personal opinion of the reviewer who is selected by the editor of the journal because of his familiarity with the topics. Also, a review is not a sci­entific paper in which every statement must be explained and proven. The author may or may not agree with the reviewer. However, the author can be sure that the reviewer had good rea­sons for every statement in the review, even if he did not elaborate in detail; after all, only summary conclusions can be given in 500-600 words.

In my review of Dr. Perry's book I characterized it as a useful general text for GC training courses and ex­pressed my opinion that, in spite of a number of shortcomings, it fills many of the requirements for a serious, modern general textbook on gas chro­matography. There is nothing I can add to this opinion.

L. S. E t t r e Norwalk, Conn.

|^/AREX

.. . where innovation is the way to the future

Producers of:

Innovative Analytical Instruments

1 Chromatography 1 Spectroscopy

• Data Handling

• Special Products 1 Accessories

For information contact:

VAREX Corporation 11600 Nebel Street Rockville, MD 20852. USA (301) 984-7760 TWX: 710-828-9816

COMPANY

ADDRESS

CITY

STATE ZIP

• M M V M M M M M H M M M M I M M M I CIRCLE 37 ON READER SERVICE CARD CIRCLE 218 ON READER SERVICE CARD

424 A · ANALYTICAL CHEMISTRY, VOL. 54, NO. 3, MARCH 1982

VAREX