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St. Patrick’s Day Eggs: A Factorial Eggspearmint (experiment) By Cheryl A Kilroy 5/5/2010

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St. Patrick’s Day Eggs:A Factorial Eggspearmint

(experiment)By Cheryl A Kilroy

5/5/2010

Outline• Introduction•Objective •Design Description

Procedure•Data Analysis•Conclusion •Recommendations

Objective

Determine which combination of levels of factors maximizes shade of green when dyeing eggs.

Design Description

•2 ^ 4 factorial design•Response •Factors (Refer to handout)•Experimental Unit•Blocks•Randomization (Refer to

handout)

Design Description

• Egg Organization (refer to handout)• Dyeing Procedures = egg organization + run order (eliminated need for blocks)• Solution organization like an excel

spreadsheet• Controlled Variables

Procedure

•Prepare eggs•Prepare solutions•Dye Eggs following dyeing procedures

•Measure shade of eggs 2 hours after removing from solution

Data Analysis of all Effects

1-1

10.8

10.4

10.0

9.6

9.21-1

1-1

10.8

10.4

10.0

9.6

9.21-1

EggType

Mean

EggTemp

VinegarLevel SoakTime

Factorial Plot - Main Effects

Data Analysis of all Effects

1-1 1-1

11

10

9

11

10

9

11

10

9

1-1

11

10

9

1-1

EggType

EggTemp

VinegarLevel

SoakTime

-11

EggType

-11

EggTemp

-11

VinegarLevel

-11

SoakTime

Interaction Plots - Main Effects

Data Analysis of all Effects

AD

ACD

ABC

ABD

AC

BCD

AB

B

BC

ABCD

A

C

BD

CD

D

1.41.21.00.80.60.40.20.0

Term

Effect

1.384

A EggTypeB EggTempC VinegarLevelD SoakTime

Factor Name

Pareto Chart of the Effects(response is Y, Alpha = 0.20)

Lenth's PSE = 0.9375

Data Analysis of all Effects

2.52.01.51.00.50.0

98

95

90

85

80

70

60

50

403020100

Absolute Effect

Perc

ent

A EggTypeB EggTempC VinegarLevelD SoakTime

Factor Name

Not SignificantSignificant

Effect Type

Half Normal Plot of the Effects(response is Y, Alpha = 0.20)

Lenth's PSE = 0.9375

Data Analysis – Next Step

•Because the two way interaction of BD is as close to significant as effect C, run an analysis including effects A, B, C, D and two way interactions BC, CD, BD to preserve hierarchy.

Data Analysis (A, B, C, D, BD, BD, CD)

1.00.50.0-0.5-1.0-1.5

99

95

90

80

70

605040

30

20

10

5

1

Residual

Perc

ent

Normal Probability Plot(response is Y)

Data Analysis (A, B, C, D, BD, BD, CD)

1312111098

1.0

0.5

0.0

-0.5

-1.0

Fitted Value

Resi

dual

Versus Fits(response is Y)

Data Analysis (A, B, C, D, BD, BD, CD)

1.00.50.0-0.5-1.0

1.0

0.5

0.0

-0.5

-1.0

VinegarLevel

Resi

dual

Residuals Versus VinegarLevel(response is Y)

Data Analysis (A, B, C, D, BD, BD, CD)

1.00.50.0-0.5-1.0

1.0

0.5

0.0

-0.5

-1.0

SoakTime

Resi

dual

Residuals Versus SoakTime(response is Y)

Data Analysis (A, B, C, D, BD, BD, CD)

Output

Data Analysis (A, C, D, CD)

Normality was not an issue

(graph lost)

Data Analysis (A, C, D, CD)

12111098

2.0

1.5

1.0

0.5

0.0

-0.5

-1.0

-1.5

Y

Resi

dual

Residuals Versus Y(response is Y)

Data Analysis (A, C, D, CD)

Log Y

0.100.050.00-0.05-0.10

99

95

90

80

70

605040

30

20

10

5

1

Residual

Perc

ent

Normal Probability Plot(response is LOG (Y))

Data Analysis (A, C, D, CD)

Log Y

1.1001.0751.0501.0251.0000.9750.950

0.08

0.06

0.04

0.02

0.00

-0.02

-0.04

-0.06

-0.08

Fitted Value

Resi

dual

Versus Fits(response is LOG (Y))

Data Analysis (A, C, D, CD)

Log Y

1.00.50.0-0.5-1.0

0.08

0.06

0.04

0.02

0.00

-0.02

-0.04

-0.06

-0.08

VinegarLevel

Resi

dual

Residuals Versus VinegarLevel(response is LOG (Y))

Data Analysis (A, C, D, CD)

Log Y

1.00.50.0-0.5-1.0

0.08

0.06

0.04

0.02

0.00

-0.02

-0.04

-0.06

-0.08

SoakTime

Residual

Residuals Versus SoakTime(response is LOG (Y))

Data Analysis (A, C, D, CD)

Log Y

Output

A Contour Plot

Soak

Vin

egar

1.00.50.0-0.5-1.0

1.0

0.5

0.0

-0.5

-1.0

> – – – – < 8

8 99 10

10 1111 12

12

Y

Contour Plot of Y vs Vinegar, Soak

Conclusion

To get a deep dark green eggs:•Soak large white room

temperature raw eggs in a solution of ½ cup room temperature water, ¼ teaspoon food coloring, and 4 teaspoons of vinegar for 7 minutes

Recommendations

• Use 20 drops of food coloring• Use machinery to conduct

experiment and measure shade of green

• Change temperature levels• Add factors• Start dyeing eggs for St. Patrick’s

Day and holidays in general