ab302502 - records collections · mcdp 87, and # 15536 sdgs mcdp 80 and ccboo. the validation for...

CaRPORATIONEnvironmental Services

Public Ledger BuildingIndependence Square6th and Chestnut StreetsSuite 872Philadelphia, PA 19106

Telephone: 215-440-7340Fax: 215-440-7346

July 17, 1991

HAND DELIVERY

Ms. Christine ChulickU.S. Environmental Protection Agency841 Chestnut BuildingPhiladelphia, PA 19107

RE: Data Validation ReportsSaegertown SiteWork Assignment No. C03045

Dear Ms. Chulick:

Enclosed are copies of the data summary forms for case # 15741 SDGs MCBB99 andMCDP 87, and # 15536 SDGs MCDP 80 and CCBOO. The validation for these cases hasbeen completed and sent to Diann Sims in Region HI Central Laboratory. Also enclosedare copies of a completed case #15741 SDG CAU93 which was approved by Region HICentral Laboratory for distribution.

Should you have any questions, please do not hesitate to call me at (215) 440-7340.

Sincerely,

Camille Costa JE.Project Manager

cc: Mr. Robert E. Stecik, Dynamac, Philadelphia Operations (letter only)Ms. Donna McGowan, EPA, Regional Project Officer (letter only)

Enclosure

AB302502

Corporate Headquarters: The Dynamac Building, 2275 Research Boulevard, Suite 500, Rockville, MD 20850-3268

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02518"2 •i HIo MIH- aMl 0H- ft" f• A

Date : June 14, 1991

Subject : Organic Data Validation Case 15741,SDG:CAU93Site: Saegertown Industrial r t

From : Ting-Ting Chang, Darline F. Terrell'Data Reviewer, Project Manager

To: :Diann SimsEPA Region III TES Contract Coordinator

Overview

Case 15741, SDG CAU93 contained two (2) soil samples and six (6)water samples for full organic analyses, and two (2) water samplesfor volatile analysis only. All these samples were analyzedthrough the Contract Laboratory Program Routine AnalyticalServices.

summary

All compounds were successfully analyzed. Areas of concern withrespect to usability are listed according to the seriousness of theproblem.

Ma-1 or Problems

2-butanone in all the water samples would not have beendetected even if this compound were present in the samples.The reported detection limits for this compound has beenqualified as unreliable (R) due to the very poor instrumentresponse factors (0.023 and 0.024).

Minor Issues

Estimate (J) the positive results and (UJ) all the non-detected sample results for both BNA and pesticide/PCB data insamples CAU97 and CAU98 due to the sample extraction holdingtime were exceeded for two days.

AR302519

Low level blank contaminations affected the reported resultsfor the following compounds in the samples indicated. Theywere all qualified "B".

Compound SamplesMethylene Chloride All samplesAcetone CAU97, CAU98Bis(2-Ethylhexyl)Phthalate All Samples

The following TICs were crossed off of the TIC forms : Unknownat retention time 4.81 and 22.83, Sulfur, Unknown Hydrocarbonat retention time 6.23, Hexane (DOT 8CI9CI), and 1,1,2-Trichloro-l,2,2-Trifluoroethane. The above mentioned TICs werealso detected in the associated blanks.

The TICs which were not blank contaminations were flagged "J"(estimated) to reflect the quantitative error inherent in theanalysis of compounds without corresponding calibrationstandards.

Notes

All other compounds with a HJ" qualifier were detected attrace levels.

All data was reviewed according to the National FunctionalGuildlines for evaluating Organic Analyses. The text of thisreport addresses only those problems affecting usability.

Attachments:

1. Glossary of data qualifier codes.2. Data Summary. This includes:

a) All positive results for the target analytes withqualifier codes, if applicable.b) All unusable detection limits (qualified NRM).

3. Appendix A - Results as reported by the laboratory for alltarget analytes (no corrections were made during datavalidation).

4. Appendix B - Results of all tentatively identified compounds(TIC) which have been corrected to exclude method artifactsand laboratory contaminants.

5. Appendix C - DPO report addresses laboratory compliance tothe statement of work.

6. Appendix D - Support Documentation includes details tosupport the statements in this report.

7. Appendix E - Telephone log.

AR3025

Attachment 1Data Qualifier Codes

SR302521

Glossary of Data Qualifier Codes (Organic)

Codes Relating to Identification(Confidence concerning presence or absence of compounds):

U = Not detected. The associated number indicatesapproximate sample concentrations necessary to bedetected.

(NO CODE) - Confirmed identification.

B — Not detected substantially above the level reported inlaboratory or field blanks.

R = Unreliable results. Analyte may or may not be presentin the sample. Supporting data necessary to confirmresults.

Codes Related to Ouantitation(can be used for both positive results and sample quantitationlimit):

J = Analyte Present. Reported value may not be accurate orprecise.

K = Analyte present. Reported value may be biased high.Actual value is expected to be lower.

L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.

UJ = Not detected. Quantitation limit may be inaccurate orimprecise.

UL » Not detected. Quantitation limits is probably higher.

Other Codes

Q - No analytical result.

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Appendix ALaboratory Results of all Target Analytes

A83G2536

1A EPA S A M P L E NOV O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

I CAUS3Lab Name: NET C o n t r a c t : 63090031 I

Lab Code: NET Case No.: 15741 S A S N o . : S D G N o . : C A U 9 3

M a t r i x : (soil/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3700

L e v e l : (low/med) LOW Date Received: 1/24/31

% Moisture: not dec. 100. Date A n a l y z e d : 1/29/91

Column: (pack/cap) CAP D i l u t i o n Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3-------Ch1orometbane ____74-83-9-------Bromomet hane______75-01-4-------Vinyl chloride____75-00-3-------Ch1oroe thane______75-03-2-------Methylene chloride,67 - 64 - 1 -- -- - --Acetone __________75-15-0-------Carbon d i s u l f i d e__75-35-4-------1 , l - D i c h 1 o r o e t h e n e _7 5 - 3 4 - 3 - - - - - - - 1 , 1 - D i c h l o r o e t h a n e

540-5'3-0-------l,2-Dich1oroethene (total) __S7-66-3-------Ch1orofor m__________________

107-06-2-------1 , 2 - D i c h l o r o e t h a n e__________78-93-3-------2-8u tan one_________________7 1 - 5 5 - l s - - - - - - - l , l , l - T r i c h l o r o e t h a n e _____56-23-5-------Carbon t e t r a c h l o r i de_______108-05-4-------Vinyl acetate _____________75-27-4-------8romodi chloromethane_______78-87-5-------l,2-Oichloropropane _______

10061-Ql-5-------ci s - 1 , 3 - D i c h l o r o p r o p e n e79-01 - 6-------Trichloroethene _______

124-48-1-------Oi bromochloromethane_79-00-5-------1,1,2-Tri c h l o r o e t h a n e71-43-2-------Benzene ____________

10061-02-6-------trans-l ,3-Di c h l o r o p r o p e n e -75-25 - 2 - - -----Bromoform

108-10-l-------4-Methyl-2-pen tan one_____531-78-6-------2-Hex an one_______________127-18-4-------Tetrachloroethene _______79-34-5-------1,1,2,2-Tetrachloroethane108-88-3-------To1uene _________________108-90-7-------Ch1orobenzene __________100-4l-4-------Etny1benzene_____________100-42-5-------Styrene

10. |U10. |U10. |U10. j U11 . I B10. | U5 . I U5. |U5. |U5. |U5. |U5. |U

10. | U5. |U5. |U10. |U5. |U5. |U5. |U1. | J5. |U5. |U5. |U5. '|U5. |U10. | U10. |U5. |U5. |U

5. |U5. |U* w w ^ w «•* ^ v r i w i c ^ v <-* * \ •*• |

1330-20-7-------Xy1ene (total)_____________| 5. |U | C J

1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________

II CAUS4

Lab Name: NET C o n t r a c t : 68090031 I

Lab Code: NET Case No.: 15741 3AS No.: SOG No.: CAU93



Level: (low/med) LOW Date Received: 1/24/91

% M o i s t u r e : not dec. 100. Date A n a l y z e d : 1/29/91



74-87-3---74-83-9---75-01-4---75-00-3----? er n Q •? »

67-64-1 ---75-15-0---75-35-4---75-34-3---

540-59-0---67-66-3---107-06-2---

71-55-6---56-23-5---108-05-4---75-27-4---/ O O / v

10061-01-5---79-01 -6---

124-48-1 ---79-00-5---71-43-2---

10061-02-6---75-25-2---

108-10-1 ---O 7 i / O O127-13-4---79-34-5---

108-88-3---108-90-7---100-41-4---100-42-5---

1330-20-7---

----Chl oromethane----Bromomethane- - - - V i n y l c h l o r i d e----Chl oroethane- - --Me t hy 1 ene c h l o r i d e----Acetone----Carbon d i s u l f i d e----1 , 1-Dichloroethene----1 , 1 - D i c h l o r o e t h a n e- --- 1 , 2 -Di c hi oroet hen e (total) __----Chl orofo rm----1 , 2 - O i c h l o r o e t h a n e----2-8utanone----1 , 1 , 1 - T r i c h l o r o e t h a n e----Carbon t e t r a c h 1 o r i de- - - - V i n y l acetate- -- -8 r omodi chl oromethane----1 , 2 - O i c h l o r o p r o p a n e- - - -c i s - 1 , 3 - Oi c h 1 o r op r open e ____----Trichloroethene----Di bromochl oromethane----1 , 1 ,2-Trichl oroethane----Benzene- - - - t r ans- 1 , 3 - Oi c h 1 o r op r opene __- -- -8 r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachloroethene- - - - 1 , 1 , 2 , 2 -Te t r achl o r oet hane __----Toluene----Chl orobenzene----Ethyl benzene----Styrene----Xy 1 ene (total )

10.10.10.10.10.10.5 .5 .5 .5 .5 .5 .10.5 .5 .10.5 .5 .

. 5 .1 .5 .5 .5 .5 .5 .10.10.5 .

AB3C5 .5.5.5 .

1

I|U|U|U|UI B|U|U|U|U|U|U|U|U|U|U|U|U|U|U1 J|U|U[U|U|U|U|U|U

1 538|U|U|U|U1

37

1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

I CAU95Lab Name: NET $ C o n t r a c t : 68090031 I___

Lab Code: NET Case No.: 15741 3AS No.: SDG No.: CAU93


Sample wt/vol: 5.0 (g/mt.) ML Lab F i l e ID: F3704

Level: (low/med) LOW Date Re c e i v e d : 1/24/91

% M o i s t u r e : not dec. 100. Date Analyzed: 1/29/91



74-87-3-------Chloromethane ____74-83-9-------Br omomethane______75-01-4-------Vinyl chloride____75-00-3-------Chloroe thane______75-03-2-------Methylene chloride,67-64-1-------Acetone __________75-15-0-------Carbon disulfide__75-35-4-------1,l-0ichloroethene_7 5 - 3 4 - 3 - - - - - - - 1 , 1 - O i c h l o r o e t h a n e

540-59-0-------1,2-Dichloroethene (total)__67-66-3-------Chlorof orm__________________

107-06-2-------1 ,2-Dichloroethan e_________78-33-3-------2-Butanone__________________71-55-6-------1 , 1 , 1 - T r i c h l o r o e t h a n e ______56-23-5-------Carbon t e t r a c h l o r i de_______108-05-4-------Vinyl acetate _____________75-27-4-------Bromodi chl orome thane________78-87-5-------l,2-Dichloropropane ________

10061 -01-5-------cis-1,3-Dichloropropene79-01 - 6-----~-Trichl oroethene _____

1 24-43-1-------Di bromochl oromethane_79-00-5-------1,1,2-Trichloroethane7 1-43-2-------Benzene ______ ___

10061-02-6-------trans-l ,3-Di chloropropene __75 - 25 - 2 --- - ---Bromoform _______________

108-10-1-------4-Methyl -2-pentan one_____59 1-73-&-------2-Hexanone______________127-13-4-------Tetrachloroethene _______79-34-5-------1 , 1,2,2-Tetrachloroethane

•To 1uene1 08-90-7-------Ch1orobenzene100-41-4-------Ethyl benzene__100-42-5-------Styrene ______

1330-20-7-------Xy1ene (total).

10. |U10. JU10. JU10. |U12. | B10. | U5. |U5. |U5. |U5. |U5. |U5. |U10. | U5. |U5 . | U10. |U5. |U5 . |U5. |U5. |U5. |U5. |U5. |U5. |U5 . U10. U10, U5. U5. U

5 . U5 . |U5. U

1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

I ———;I CAU96 j

Lab Name: NET C o n t r a c t : 68030031 |__________ \\

Lab Code: NET Case No.: 15741 S A S N o . : S D G N o . : C A U 9 3

M a t r i x : ( s o i l / w a t e r ) WATER Lab Sample ID:



% M o i s t u r e : not dec. 100. Date Analyzed: 1/29/91


CONCENTRATION UNITS:CAS NO. • COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3----74-83-9----75-01-4----75-00-3----75-09-2----67-64- 1 - - - -75-15-0----75-35-4----75-34-3----

540-53-0----67-66-3----

107-06-2----78-93-3----71-55-6----56-23-5----

1 U O U 3 *+

75-27-4----78-37-5----

10061 -01 -5----79-01-6----

124-43-1----79-00-5----71-43-2----

10061-02-6----75-25-2----

108-10-1 ----C Q 1 7 Q _ C - _ _ -

127-18-4----79-34-5----

i U w w w O

I U o a U /100-41 -4----100-42-5----

1330-20-7----

- --Ch 1 oromethane---Bromomethane---Vinyl c h loride---Chloroethane---Methylene c h l o r i d e---Acetone---Carbon d i s u l f i d e---1 , 1 - D i c h l o r o e t h e n e---1 , 1 - O i c h l o r o e t h a n e- - - 1 , 2 -Di c hi o r oe t hen e (total) __---Chloroform---1 , 2 - D i c h l o r o e t h a n e---2-8utanone---1 , 1 , 1-Trichl oroethane---Carbon t e t rachl o r i de- - - V i n y l acetate- --Bromodi chl o r ome thane---1 , 2-Oichloropropane- - -e i s-1 ,3-Oi chl oropropene---Trichloroethene- - - Oi b r omoc hi o r ome thane---1 , 1 ,2-Trichl oroethane---Benzene- - - t r ans- 1 , 3 -Oi c hi o r op r op ene __- - - 8 r omof o rm---4-Methyl -2-oentanone---2-Hexanone---Tetrachloroethene---!-, 1,2,2- Tetrachloroethane __---Toluene---Chlorobenzene---Ethylbenzene---Styrene---Xy 1 ene (tota 1 )

110. U10. U10. U10. U14. B10. U5. U5. |U5 . U5. U5 . U5. U

10. U5 . U5. JU10. |U5. U5 . U5. U5. U5 . U5 . U5. U5 . U5 . U

10. U10. U5. |U

A5R3Cl|5l4i5'. |u5. |U5 . U

1A EPA SAMPLE NO,VOLATILE ORGANICS A N A L Y S I S DATA SHEET

| CAU97Lab Name: NET C o n t r a c t : 68D90031 I

Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU33

M a t r i x : (soil/water) SOIL Lab Sample ID:

Sample wt/vol: 5.1 (g/mL) G Lab F i l e ID: F3724



Column: (pack/cap) CAP D i l u t i o n Factor? 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3----7 A O "* Q

75-01-4----75-00-3----75-03-2----67-64- i - - - -75-15-0----75-35-4----75-34-3----

540-53-0----67-66-3----

107-06-2----/ O J O J71 C C C.

56-23-5----108-05-4----75-27-4----78-87-5----

10061-01-5----73-01-6----

124-48-1----79-00-5----71-43-2---

10061-02-6----75-25-2----108-10-1---591-78-6---127-18-4---79-34-5---

108-90-7---100-41-4---100-42-5---

1330-20-7---1

---Chl oromethane• - - - 8 r omome thane• - - - V i n y l c h l o r i d e•---Chl oroethane- - - -Me t hy 1 ene c h l o r i d e•---Acetone•---Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e•---1 , 2-Di chl oroethene (total) __•---Chl orofo rm•---1 , 2-Di chl oroethane•---2-Butanone----1 , 1 , 1-Trichl oroethane•---Carbon te t rachl o r i de•---Vinyl acetate

•---1 , 2-Oichloropropane•---ci s-1.3-Dichloropropene•---Tri chl oroethene•---Di br omoc hi oromethane•---1 , 1 ,2-Trichl oroethane----Benzene• --- t r an s- 1 , 3 -Di c hi o r op r opene __- - -- B r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachl oroethene- --- 1 , 1 , 2 , 2 -Te t r ac h 1 o roe t hane __----To! uene----Chl orobenzene----Ethyl benzene----Styrene- - - - X y l e n e (total)

15. U15. U15. U15. U9. B18. B8. U8. U8. U8. U3. U8. U

15 . U8. U8. U

15. U3. U8. U8. U8. U8. U8. U8. U8. |U3. |U

15 . |U15. |U8. |U8. |U

A|;30|?5l»l8. (U8. | U

1 8. |U1

95

1A EPA S A M P L E NOV O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________

\ CAU38Lab Name: NET C o n t r a c t : 68090031 I

Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93







74-87-3----74-83-9----75-01 -4----75-00-3----75-03-2----67-64-1----75-15-0----75-35-4----7 c _ - 3 4 _ 3 - _ _ .' J V ** J

540-59-0----67-66-3----

107-06-2----/ O J J J

71-55-6----5f 1 *^ C6-23-5----108-05-4----75-27-4----/ o O / 3

10061-01-5----73-01-6----

124-43-1----79-00-5----71-43-2----

10061 -02-6----T C * ff *575-25-2----

108-10-1----b3l~/o"b"*""127-13-4----7<9_-54_c.__.1 J sP ** -J

iuo o o J1 U O J U /

100-41-4----100-42-5----

1330-20-7----

----Chl oromethane----Bromomethane- - - - V i n y l c h l o r i d e----Chloroethane- -- -Me t hy 1 ene c h l o r i d e----Acetone•---Carbon d i s u l f i d e----1 , 1 - D i c h l o r o e t h e n e•---1 , 1-Dichloroethane- - -- 1 , 2 -Oi c hi or o e t hen e (total) __- - - - C h l o r o f o r m•---1 , 2 - D i c h l o r o e t h a n e• ---2-Butanone•---1 , 1 , 1 - T r i c h l oroethane----Carbon t e t r achl o r i de•---Vinyl acetate•---Bromodi chl oromethane----1 , 2 - D i c h l o r o p r o p a n e• - - -c i s - 1 , 3 - Di c h 1 o r op r open e ____•---Tri chl oroethene•---Di bromochl oromethane----1 , 1 ,2-Trichl oroethane•---Benzene• -- - t r an s - 1 , 3 - Di c h 1 o r op r op en e __• -- - 8 r omof o rm----4-Methyl -2-pentanone•---2-Hexanone•---Tetrachl oroethene• - -- 1 , 1 , 2 , 2 -Te t r ac hi o r oe t hane __• - - -To 1 uene•---Chlorobenzene•---Ethylbenzene- - - - S t y r e n e•---Xy 1 ene (total )

12.12 .12.12 .7.

1 1 .6.6 •6.6.6.6.

12.6.6.

12.6.6.6.6.6.6.6.6.6.

12.12.6.

6.6.6.3.

UUUUBBJUUUUUUUUUUUUUUUUUuuuuu

*5«,2UuJ

Ul

IA EPA S A M P L E NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET _____________^

II CAU99

Lab Name: NET Contract: 68090031 I


M a t r i x : (soil/water) WATER Lao Sample ID:

Sample wt/vol: 5.0 (g/mL) ML Lab F i l e 10: F3706





74-37-3----/*»"*O.53

75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----

540-53-0----67-66-3----

107-06-2----73-93-3----71-55-6----5C. - -" -5 -. C _ _ _ .

108-05-4----75-27-4----/ o - o / — 0

10061-01-5----73-01-6---

1 24-43-1----79-00-5----71 _ 4 - 5 _ - > _ - _/I *+ '^ la,

i U U O l U l . O

75-25-2---108-10-1---531-73-6---127-13-4---73-34-5---

i U O s ? t 3 j108-30-7---100-41-4---100-42-5---

1330-20-7---

• ---Ch 1 oromethane•---Bromomethane• - - - V i n y l c h l o r i d e•---Chl oroethane• ---Me t hy 1 ene c h l o r i d e•---Acetone•---Carbon d i s u l f i d e•---1 , 1 - O i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n s•---1 , 2-Di c h l o r o e t h e n e (total ) __•---Chl oroform•---1 , 2 - D i c h l o r o e t h a n e•---2-Sutanone•---1 , 1 , 1 - T r i c h l oroethane•---Carbon t et r achl o r i de- - - - V i n y l acetate- - --B r omodi chl oromethane----1 , 2-Oichloropropane- -- -c i s - 1 1 3 -Oi c h I o r op r open e ____----Tri chl oroethene----Oi br omoch lor orne thane----1 . 1 ,2-Trichl oroethane•---Benzene- - -- t r ans- 1 , 3 -Di c h 1 o r op r op ene __- - - - 8 r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachloroethene- --- 1 , 1 , 2 , 2 -Te t r ac hi o r oe t hane __- -- -To 1 uen e----Chl orobenzene----Ethylbenzene----Styrene- - - - X y l e n e (total)

10.10.10.10.14.12 .5 .5 .5 .5 .5.5 .10.5 .5.10.5 .5 .5 .5 .5 .5 .5.5.5 .10.10.5 .

^R3<5 .5.5.5 .

UUUuB

UUUUuUuuuu|Uuu|U|U|U|U|U|Uu|U

ii-si^|U|U|U|U1

1A EPA SAMPLE NO.VOLATILE ORGANICS ANA L Y S I S DATA SHEET

I 1I CC612 |

Lab Name: NET ' C o n t r a c t : S8DS0031 I___ i

Lab Cod*: NET Case No.: 15741 SAS No.: SDG No.: CAU33





Column: (pack/cap) CAP D i l u t i o n F a c t o r : 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

I74-87-3-------Chloromethane74-83-3-------Br omome thane75-01-4-------Vinyl chloride____75-00-3-------Chloroethane______75-09-2-------Methylene chloride,67-64-1-------Acetone ___________75-15-0-------Carbon disulfide__7 5 - 3 5 - 4 - - - - - - - 1 , 1 - D i c h l o r o e t h e n e

10. |U10. |U10. JU10. | U10. | B10. | U5. JU5. |U

75-34-3-------1 , 1-Di chl oroethane__________| 5. |U540-53-0-------1 ,2-Dichloroethene (total)__| 5. |U67-66-3-------Ch 1 oroform_________________| 5- I U

107-06-2-------1 , 2-Di chl oroethane_________| 5. |U10. | U5 . |U5. |U10. |U5. |U5 . | U5. |U5. |U5. |U5. |U5. |U5. |U .5. |U10. |U4. | J5. |U5. |U

73-93-3-------2-Bu tanone___________7 1 - 5 5 - 6 - - - - - - - l , l , l - T r i c h l o r o e t h a n e56-23-5-------Carbon tetrachlori de_

103-05-4-------Vinyl acetate _______75-27-4-------8r omodi chloromet hane_78-87-5-------1,2-Dichloropropane _

10061-01-5-------ci s-1,3-Oichloropropene79-01 -6-------Triohloroethene _______

124-48-l-------Dib romochlo r omet hane_79-00-5-------1,1,2-Trichloroethane7 1-43-2 -------Benzene __________________

10061-02-6-------trans-l ,3-Di chloropropene __75 - 25 - 2 -------8romoform _________________108-10-l-------4-Methyl-2-pentanone_______591-78-6-------2-Hexanone_________________127-18-4-------Tetrachloroethene _________79-34-5-------1,1,2,2-Tetrachloroethane __108-33-3 -------To 1uene ___________________108-90-7-------Ch1orobenzene _____________100-41-4-------Ethyl benzene_______________100-42-5-------Styrene ___________________

1330-20-7-------Xylene (total)_____________

5. |U5. |U5. IU

144

IA EPA S A M P L E NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

| CCB13Lab Name: NET C o n t r a c t : 68D30031 I




Lev e l : (low/med) LOW Date Received: 1/24/31

% Moisture: not dec. 100. Date Analyzed: 1/23/31



74-87-3----74-33-3----75-01-4----7 5 - UU - J - - -75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----

540-53-0----67-66-3----

107-06-2----78-93-3----71 -55-6----56-23-5----108-05-4----75-27-4----

10061-01-5----73-01-6----

124-48-1----73-00-5----71-43-2----

10061-02-6---75-25-2----

108-10-1---531-78-6---127-18-4---73-34-5---l u o o o oI U <3 j \J f100-41-4---

| 100-42-5---| 1330-20-7---1

•---Chloromethane• - - - B r omome thane•---Vinyl c h l o r i d e•---Chl oroethane• -- -Me t hy 1 ene c h l o r i d e•---Acetone----Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e•--- 1 , 2-Di c hi or oethene (total) __•---Chloroform•---1 ,2-Dichloroethane•---2-Butanone•---1 , 1 , 1-Trichl oroethane•---Carbon te t r a chl o r i de- - - - V i n y l acetate- - - - B r omodi chl oromethane----1 , 2-Di chl oropropane•- --c i s- 1 , 3 -Di ch 1 orop r open e ____----Tri chl oroethene•---Di bromochl oromethane•---1 , 1 ,2-Trichl oroethane----Benzene-- -- t r ans - 1 , 3-Oi c hi o ropr opene __- ---B r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachl oroethene- - -- 1 , 1 , 2 , 2 -Te t r achl o r oe t hane __-- --To 1 uene----Chl orobenzene----Ethyl benzene----Styrene----Xy 1 ene ( tota 1 )

101010101210555555

10551055555555510to55

si555

1. |U. |U. |U. |U• 18• |U

|U. |U• |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U- |U. |U. !U. |U. |U• |U. |U. |U

30$5 if 5. |U• |U. |U

1

1A ERA S A M P L E NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET _____________

II CC814

Lab Name: NET C o n t r a c t : 68090031 |_____________

L a b C o a e : N E T Case No.: 15741 SAS No.: S D G N o . : C A U 3 3

M a t r i x : (soil/water) WATER Lab S a m p l e ID:


L e v e l : (low/med) LOW Date R e c e i v e d : 1/24/91




74-87-3----74-83-9----75-01-4---75-00-3----75-03-2----67-64-1 ---75-15-0----75-35-4---75-34-3----

540-59-0----67-66-3----

107-06-2----' O ™" J sj J

71 C C r"1-55-6----56-23-5----108-05-4----75-27-4----o o / D

10061-01-5----73-01 -6----

124-43-1----79-00-5----71 -43-2----

10061-02-6----75-25-2----108-10- 1 - - - -

127-13-4----73-34-5----

I U 8 3 U /100-41 -4----100-42-5----

1330-20-7----1

- - - - C h l oromethane- -- - 8 r omome thane- - - - V i n y l c h l o r i d e- - - - C h l oroethane• - - -Me t hy 1 ene c h l o r i d e----Acetone----Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e• - - - 1 , 2 - D i c h l o r o e t h e n e (total) __•---Chlorofo rm----1 , 2 - D i c h l o r o e t h a n e•---2-Butanone•---1 , 1 , 1 - T r i c h l oroethane•---Carbon t e t r a c h l o r i d e•---Vinyl acetate

•---1 , 2-Di chl oropropane• - - -c i s - 1 , 3 -Oi c h 1 o r op ropen e ___•---Trichloroethene•---Oi bromochl oromethane•---1 , 1 ,2-Trichl oroethane•---Benzene• - - - t r an s- 1 , 3 -Di ch 1 o r op r op ene __• -- -B r omof o rm•---4-Methyl -2-pentanone•---2-Hexanone•---Tetrachl oroethene• -- - 1 , 1 , 2 , 2 -Te t r ac h 1 o r oe t hane __•---Toluene•---Chl orobenzene•---Ethylbenzene•---Styrene•---Xy 1 ene (tota 1 )

10.10.10.10.12.10.5 .5 .5 .5 .5.5 .

10.5,5 .10.5 .5.5.5.5 .5.5 .5.5 .10.10.5.

ftilSG5.5.5.5.

11

u lu tu l8 Iu l

U |u lu 1u lu iu lu lu iu 1u iu iu lu iu lu lu lu 1^en*^djDHOju !u Iu lu li

179

18 EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

I CAU93Lab Name: NET C o n t r a c t : 68090031 I


M a t r i v : (soil/water) WATER Lab Sample ID:

Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8561


% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/31

E x t r a c t i o n : (SepF/Cont/Sone) CONT Date A n a l y z e d : 2/ 7/91

GPC C l e a n u p : (Y/N) N PH: .0 D i l u t i o n Factor: 1.00


1 1 i-44-4----9C C "7 O

541 -73-1----106-46-7----100-51-6----35-50-1 ----95-48-7----103-60-1 ----106-44-5----621 -64-7----

/ - / _ ~ i - - - -

O J O O

O O '3 J

105-67-9----65-35-0----

1 1 1 - 31-1----

120-32- 1 ----31-20-3----106-47-8----37-63-3----53-50-7----31-57-6----77-47-4----83-06-2----35-35-4---31-58-7----38-74-4---

131-1 1 - 3 - - - -203-36-8---S06-20-2---

1---Phenol•---bi s(2-Chl oroethyl )ether ____---2-Chl orophenol

• - - - 1 ,3-Dichlorobenzene---1 , 4-Di chl orobenzene•---Benzyl a l c o h o l---1 , 2-Di chl orobensene---2-Methyl phenol---bi s(2-chloroi sopropyl )ether._,_4_Ma,thyl phenol- - -N -N i troso-di - n - p r o p y l ami n e __•---Hexachl oroethane- - -N i trobenzene•---Isophorone---2-Ni trophenol•---2, 4-Dimethyl phenol•---Benzoic acid•---bi s ( 2-Chloroethoxy)met hane __•---2 , 4-Oi chl orophenol•---1,2,4-Trichlorobenzene•---Naphtha! ene----4-Chl oroani 1 i ne•---Hexachl orobutadi ene- - - -4- Chl or o-3 -me t hy 1 pheno 1 ____- - - - 2 - M e t h y l n a p h t h a l e n e- - --He xachl o r ocy c 1 open t adi ene __- - - - 2 , 4 , 6 - T r i c h l o r o p h e n o l----2.4,5-Trichl orophenol- - - - 2 - C h 1 o r o n a D h t h a 1 e n e- - - - 2 - N i troani 1 i ne- - - - D i m e t h y l p h t h a l a t e- - - - A c e n a p h t h y l ene- - - - 2 . 6 - D i n i t r o t o l u e n e

10.10.10.10.10.10.10 .'10.10.10 .10 .10.10 .10.10.10.50.10.10.10.10.10.10 .10.10.10.10.50.

10.10.10.

1|U|U|U|U|U|U|U|U|UI1-1|U|U|U|U|U|U|U|U|U|U|U|U

|U|U|U|U|U

fl25^^|U|U|U1

286

1C EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________

I I| CAU93 |

Lab Name: NET C o n t r a c t : S8D90031 | ______________ i





% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91


GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND Og/L or ug/Kg) UG/L Q

99-09-2---->J 3 £ J

51 -28-5----100-02-7----132-64-3----1 2 1 - 1 4 - 2 - - - -

7005-72-3----36-73-7----

100-01-6----534-52-1----86-30-6----

101 -55-3----

37-36-5----85-01-8----

120-12-7----84-74-2----

206-44-0----129-00-0----35-63-7----31 -34- 1 ----56-55-3----

218-01-3----1 17-81-7----1 1 7-fid-fi----

207-08-9---50-32-8----

193-39-5---53-70-3----

191-24-2----

- - - 3 - N i t r o a n i l i n e•---Acenaohthene---2 , 4-Oi ni trophenol

• ---4-Ni trophenol- - -Di benz of u r an- - - 2 , 4 - D i n i t r o t o l u e n e---Di e t h y l p h t h a l ate---4-Chl orophenyl - p h e n y l erthe r __- - - F l uorene---4-Ni troani 1 i ne---4, 6-Di ni t r o - 2 - m e t h y l p h e n o l __

• - - -N -N i t r o sodi p hen y 1 ami ne (1) __

•---Hexachl orobenzene---Pentachl orophenol•---Phenanthrene•---Anthracene•---Di - n - b u t y l p h t h a l a t e•---Fl uoranthene•---Pyrene•---Butyl benzy! ph t h a l ate----3,3'-Dichlorobenzidine•---Benzo(a')anthracene----Chrysene•---bi s(2-Ethylhexyl ) p h t h a 1 a t e __----Oi -n-octyl p h t h a l ate•---Benzo(b)fluoranthene•---Benzo(k)fluoranthene•---Benzo(a)oyrene- - - - I n d e n o f l ,2.3-cd)pyrene----Dibenzfa.h)anthracene- ---Benzo (g . h . i ) per y 1 ene

50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10 .10.20.10.10.4.10.10.10.10a rlO*?*10.10.

1 1|U 1

|U ||U !|U |

|U i|U i

|U I|U i

iu' i|U 1|U ||U ||U |

|U ||U I|U 1IM 1|U ||U i1 BJ ||U 1|U 1|U

|U1 1____ 237(1) - Cannot be separated from d i p h e n y 1 amine

FORM I SV-2 1/37 Rev.

IB EPA SAMPLE NOSEMIVOLATILE ORGANICS A N A L Y S I S DATA SHEET ______________

I| CAU94

Lab Name: NET C o n t r a c t : 68D30031 I

Lab Code: NET Case No.: 15741 • SAS No.: SOG No.: CAUS3


Sample w t / v o l : 1000.0 (g/rnL) ML Lab F i l e ID: 08564



E x t r a c t i o n : (SepF/Cont/Sonc ) CONT Date A n a l y z e d : 2/ 7/91



108-95-2----1 l l -44-4----

541 -73-1----106-46-7----100-51-6----35-50- 1 ----95-43-7----

108-60- 1 ----106-44-5----621 -64-7----67-72-1----93-95-3----/ O J J 1

08" /3-D----105-67-3----65-85-0----

1 1 1 - 3 1 - 1 - - - -120-S3-2----120-32- 1----91 -20-3----106-47-8----

53-50-7----31 -57-6----77-47-4----

35-35-4----31-53-7----88-74-4----

131-1 1-3----203-36-8----606-20-2----

i---Phenol i- --bi s ( 2 -Chl oroet hy 1 ) e the r _____---2-Chl orophenol---1 , 3-Oi chl orobenzene---1 ,4-Oichlorobenzene---Benzyl alcohol- - - 1 , 2 - D i c h l o r o b e n z e n e- - - 2 - M e t h y l phenol- - - b i s(2-chl oroi s o p r o p y l )ether---4-Methyl phenol

---Hexachl oroethane---Ni trobenzene---Isophorone---2-Ni trophenol•---2.4-Oimethyl phenol•---Benzoic a c i d•---bi s(2-Chloroethoxy)met hane __•---2,4-Oichlorophenol•---1 . 2.4-Tri chl orobenzene•---Naphthalene•---4-Chloroani 1 ine•---Hexachl o r o b u t a d i ene• - - - 4 - Ch 1 o r o - 3 -me t hy 1 pheno 1 _____•--- 2 - M e t h y l n a p h t h a l ene•---He'xachl orocycl opentadi ene _•---2.4,6-Trichlorophenol•---2 , 4.5-Tri chl orophenol•---2-Chl oronaphthal ene•---2-Ni troani 1 i ne•---Dimethylphthal ate•---Acenaohthyl ene•---2, 6-Di ni trotol uene

10.10 .10.10.10.10 .10 .10.10.10.10.10 .10.10.10.10.50.10.10 .10.10.10.10.10.10.10.10.50.

$8310.10.10.

1'-' 1

'u |

u |

|U1FORM I SV- 1 1 /S7

1C EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________

I| CAU94

Lab Name: NET C o n t r a c t : 68D30031

Lab Cod*: NET Case No.: 15741 SAS No.: SDG No.: CAU33«


Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e 10: OS564



E x t r a c t i o n : ( S e p F/C o n t /S on c ) CONT Date A n a l y z e d : Z/ 7/91

GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n F a c t o r ; 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 0

39-09-2----o ~> -j c j5 1-28-5----100-02-7----132-64-9----1 2 1 - 1 4 - 2 - - - -84-66-2----

7005-72-3----86-73-7----

100-01-6----5 3 4 - 5 2 - 1 - - - -3f "j f*\ C6-JO-6----101 -55-3----i t o / ** I

/ O O J

3 - l J l O120-12-7----34-74-2----

206-44-0----129-00-0----35-63-7----91-94-1----56-55-3----

218-01 -9----117-81-7----1 17-84-0----205-99-2----C U / U O J50-32-8----

193-39-5----53-70-3----

191 -24-2----

- - - 3 - N i t r o a n i 1 i ne•---Acenaphthene---2 , 4-Di ni trophenol•---4-Ni trophenol---Di benzofuran---2 , 4-Di ni t r o t o l uene---Di e t h y l p h t h a l a t e---4-Chlorophenyl -phenyl ether---Fl uorene---4-Ni t r o a n i 1 i ne---4 , 6-Di ni t r o - 2 - m e t h y l phenol __- - -N -N i t r o sod i p hen y 1 ami ne (1) __- - - 4- B r omophen y 1 - p hen y 1 e t he r __---Hexachl orobenzene---Pentachl orophenol---Phenanthrene---Anthracene•---Di -n-butyl phthal ate---Fl uoranthene•---Pyrene---Butyl benzyl p h t h a l ate•---3,3'-Dichlorobenzidine---Benzo(a)anthracene

• - - -Ch r y sen e- - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e __•---Di - n - o c t y l p h t h a l ate---Benzo(b)fl uoranthene•---Benzo(k)fluoranthene•---Benzo(a)pyrene•---Indenofl.2.3-cd')pyrene•---Oibenz(ath")anthracene•---8enzo(q.h.i "Jperylene

50 .10 .50.50.10.10.10 .10 .10 .50.50.10.10.10.50.10.10.10.10.10.10.20.10 .10.8.10.10.10.10.

10.

1I'J|U|U|U|U|U|UIUm|U|UI'J|U|U|UI'J|U|UI'J|UI'JI'J|U|U| BJI'J|U|U|U

q§25^|U1

(1) - Cannot be separated from d i p h e n y 1 amine

FORM I SV-2 1/37 Rev

18 EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________'

II C A U 9 S

Lab Name: NET C o n t r a c t : 68090031 |_________


M a t r i x : (soil/water) WATER Lao Sample ID:

Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08565



E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/91



11 1-44-4----j O O / O

541-73-1 ----106-46-7----100-51 -6----95-50- 1 ----35-48-7----103-60-1 ----106-44-5----621-64-7----67-72-1 ----90 o c ^

38-75-5----105-67-3----o D o O U

1 1 1 - 9 1 - 1 - - - •120-33-2----120-82-1----31-20-3----106-47-8---87-63-3----59-50-7---31 -57-6----77-47-4----33-06-2----35-35-4---91-58-7----33-74-4---

131-1 1 - 3 - - - -

606-20-2----

• ---Phenol |•---bis(2-Chloroethyl.) ether ___•---2-Chl orophenol•---1 ,3-Dichlorobenzene---1 , 4-Di chl orobenzene•---Benzyl alcohol•---1 , 2 - D i o h l o r o b enzene• - - - 2 - M e t h y l phenol---bi s(2-chl oroi sopropyl )ether

- - - -4-Me t hy 1 phenol- - - N - N i troso-di - n - p r o p y l a m i ne _•---Hexachl oroethane•---Ni trobenzene• -- - I sophor one•---2-Ni trophenol•---2,4-Oi met hy 1 phenol•---Benzoic acid•---bi s(2-Chloroethoxy)rnet hane __•---2,4-Dichlorophenol•---1 , 2,4-Tri chl orobenzene----Naphtha! ene•---4-Ch!oroanil ine•---Hexachl orobutadi ene----4- Chl or o-3 -methyl phenol• - - - 2 - M e t h y l n a p h t h a l ene--- -Hexachl o rocyc 1 open tadi ene __----2, 4,6-Tri chl orophenol----2.4,5-Trichlorophenol• - - - 2 - C h l o r o n a p h t h a l e n e•---2-Ni troani 1 i ne• - - - D i m e t h y l p h t h a l ate- - - - A c e n a p h t h y l ene----2 . 6-Di ni trotol uene

10.10.10.10.10 .10.10.10 .10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.

50.10.10.10.

1|U|U|U|U|UItJ|U|UI'J|U|U|U|U|U|UI'J|U|U 1|U 1|UI'J 1I'J|U 1I'J|U ||U|U3^25^

I

|U|U|U|U1

IC EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET _______________'

I_ | CAU96Lab Name: NET C o n t r a c t : 63090031 I



Sample wt/vol : 1000.0 (g/mL) ML Lab F i l e ID: D8565

L e v e l : (low/med) LOW ' Date Received:. 1/24/91

% M o i s t u r e : not dec. 100. dec. 0. Date Extracted: 1/23/31




93-09-2-------3-N1 t r o a n i 1 i ne____83-32-9-------Acenapht hene______51-28-5-------2,4-Dinitrophenol

1 00-02-7-------4-Nitropheno1 ____132-64-9-------Di benzofu ran______1 2 1 - 1 4 - 2 - - - - - - - 2 , 4 - O i n i t r o t o l u e n e _84-66-2-------Di et h y l p h t h a l a t e__

7005-72-3-------4-Chlorophenyl-phenylethe r__86-73-7-------F1uoren e___________________

100-01-6-------4-Ni t r o a n i 1 i n e_____________534-52-l-------4,6-Dinitro-2-methylphenol__36-30-6-------N-Nitrosodipheny1amine (1)__

101-5 5 - 3 - - - - - - - 4 - B r o m o p h e n y l - p h e n y l e t h e r __113-74-l-------Hexachlorobenzene _________87-36-5-------Pentachlorophenol _________85-01-8-------Phenant hrene_______________120-12-7-------Anthracene_________________84-74-2-------Di-n-butylphthalate _______

206-44-0-------Fluoran thene_______________1 29-00-0-------Pyrene_____________________35-68-7-------Butylbenzylphthala te_______91-34-l-------3,3'-Oichlorobenzidi ne______56-55-3-------6enzo(a)anthracen e_________213-01-3-------Chrysene___________________M7-81-7-------bis(2-Ethylhexyl)phthalat e__117-84-0-------Di-n-octylphthalate _______205-99-2-------Benzo(b)fluoranthen e_______207-08-3-------Benzo(k)fluoranthen e_______50-32-8-------Benzo(a)py rene_____________193-39-5-------Indeno(1,2,3-cd)pyrene_____53-70-3-------Dibenz(a,h)anthracene ______131-24-2-------Benzo(g,h,i)perylene_______

50. |U10. |U50. |U50. |U10. |U10. |U10. |U10. |U10. |U50. |U50. |U10. |U10. |U10. |U50. |U10. ID10. |U10. I U10. |U10. |U10. |U20. |U10. |U10. |U3 . I BJ10. |U10. |U10. IU

10. |U10. |U

o «j(1) - Cannot be separated from d i p h e n y l a m i n e


IB EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________

I| CAU97

Lab Name: NET Contract: 63D90031 I



Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: D8574


% M o i s t u r e : not dec. ,34. dec. 0. Date Extracted: 2/ 1/91

E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/ 8/91

GPC Cleanup: (Y/N) Y pH: 6.7 D i l u t i o n Factor: 1.00


i U O j 3 L1 l 1-44-4-9C —— C 7 a. O ——D-D / - o -

541 -73-1-106-46-7-100-51 -6-35-50-1-95-43-7-103-60- 1 -106-44-5-621 -64-7-67-72-1-O - IT O ~ -> ~

/ O 3 5 I

'jo / J -3

105-67-3-/- c o c _ n _b D o O u

1 1 1 - 9 1 - 1 -1 *> t"l —— Q "5 a. *> ——1 * _ U O - » - .

120-32-1-91-20-3-106-47-8-37-63-3-59-50-7-31-57-6-77-47-4-a Q - n c - '-s o - u b iSe Q C A

91 C O - "7 —l o o /38-74-4-

1 3 1 - 1 1-3-i U o j O o

606-20-2-

1------Phenol |------bi s(2-Chloroethyl )ether------2-Chl orophenol------1 ,3-Dichlorobenzene------ 1 , 4-Di chl orobenzene- - - - - - B e n z y l a l c o h o l_ _ _ _ _ _ 1 , 2-Dichlorobenzene- - - - - - 2 - M e t h y l p h e n o l- - - - - _ t ) i 3 ( 2 - c h l o r o i s o p r o p y l ) e t h e r_ _ - - - _ 4 _ M f t t | n y l phenol------N-Ni troso-di - n - p r o p y l a m i ne __------Hexachl oroethane------Ni trobenzene------Isophorone------2-Ni trophenol------2, 4-Dimethyl phenol------ Benz o i c a c i d------bi s(2-Chloroethoxy)met hane __------ 2 , 4-Di chl orophenol------ 1 , 2,4-Tri chl orobenzene_ _ . _ _ _ N a p h t h a l ene- - - - - - 4 - C h l o r o a n i l ine------Hexachl o r o b u t a d i ene_---__4_Ch'Ioro_3-me(:hyTpheno-|------2-Methyl naphtha! ene------Hexachl orocycl opentadi ene _------2. 4. 6-Trich! orophenol------2, 4, 5-Trichl orophenol------2-Chl oronaphthal ene------2-Ni troani 1 i ne- - - - - - O i m e t h y l p h t h a l ate------Acenaphthy! ene_ _ - . _ - 2 , 6 - O i n i t r o t o l u e n e

1000.1000.1000.1000.1000.1000.1000 .1000.1000.1000 .1000.1000.1000.1000.1000.1000.4900 .1000.1000.1000.1000.1000.1000.1000.1000.1000.1000.

i!ol33o4900.1000.1000.1000.

uuuuuuuuuuuuuuuuuu'JI'Juu|UI UI'Juu

$553uuuu

o D o

1C EPA SAMPLE NOSEMIVOLATILE ORGANICS A N A L Y S I S DATA SHEET ___________

I ~I CAU97

Lao Name: NET C o n t r a c t : 6 8 D 9 0 0 3 1 | ______

Lab C o d e : N £ T Case No.: 15741 SAS No.: S D G N o . : C A U 9 3

M a t r i x : (soil/water) SOIL Lab S a m p l e ID:

Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: 08574

Level : (low/med) LOW Date Received: 1/24/91

% M o i s t u r e : not dec. 34. dec. 0. Date Extracted: 2/ 1/91

E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/31

GPC Cl e a n u p : (Y/N)Y pH: 6.7 D i l u t i o n Factor: 1.00


99-09-2-----5 O t J

51-28-5----100-02-7----132-64-3----121 - 1 4 - 2 - - - -84-66-2----

7005-72-3----86-73-7----

100-01-6----534-52- 1 - - - -86-30-6----

101 -55-3----1 18-74-1----O / O O v

35-01-8----l _ ij i - /34-74-2----

206-44-0----123-00-0----

3 b o /3 1 -94- 1 ---•56-55-3----

21 3-01-9---1 17-81-7---1 17-34-0---->Q 5 _qq _ 2 - - -207-03-3---50-32-8---

193-39-5---53-70-3---1Q1.74-2---

•---3-Ni troani 1 i ne- ---Acenaphthene•---2 , 4-Oi ni trophenol•---4-Ni trophenol•---Oi benzofuran•---2, 4 - O i n i trotol uene• - - - D i e t h y l p h t h a l a t e- - - - 4 - C h l o r o p h e n y l - p h e n y l e t h e r __•---Fl uorene•---4-Ni troani 1 i ne•---4 , 6-Di ni tro-2-methyl phenol __• - --N -Ni t r o sodi p hen y 1 ami n e (1) __• - - -4- 8 r omophen y 1 -pheny 1 e t he r __•---Hexachl orobenzene•---Pentachl orophenol----Phenanthrene•---Anthracene----Di -n-butyl p h t h a l ate•---F! uoranthene•---Pyrene----Butylbenzy! p h t h a l ate----3,3'-Oichlorobenzidine•---Benzo(a)anthracene•---Chrysene----bi s ( 2 - E t h y l h e x y l )phthalat e __----Di - n - o c t y l p h t h a l a t e• - - - B e n z o C b ^ f l uoranthene----Benzofk If 1 uoranthene- - --Benzo (a)pyrene----Indeno(l .2.3-cd)pyrene----Dibenz(afh")anthracene- - - - B e n z o ( g . h . i 1 p e r y 1 e n e

4900.1000.4300.4300 .1000.1000.1000.1000.130.

4300.4900.1000.1000.1000.4900.1400 .380.330.

2200 .1400 .1000.2000.850.870.460.1000.680.720.7 WDf* <35W «1000.260.

1 1

IU |I'J 1

1 J 1|U |IU iIU i

IU |IU |1 11 J 11 J 11 11 1IU |I'J 11 J 11 J 11 BJ |IU |1 J 1

3 55(4

1 1(1) - Cannot be separated from d i p h e n y 1 amine

F O R M I S V - 2

359

18 EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________

I C A U9 8Lab Name: NET C o n t r a c t : 63D90031 | _ _ _ _ _ _ _ _ _ |

Lab Code: NET Case No.: 15741 . SAS No.: SDG No.: CAU93

M a t r i x : ( s o i l / w a t e r ) SOIL Lab Sample ID:

Sample w t / v o l : 30.1 (g/mL) G Lab F i l e ID: 03577


% M o i s t u r e : not dec. 22. dec. 0. Date E x t r a c t e d : 2/ 1/91


GPC Clean up: (Y/N) Y pH: 6.9 D i l u t i o n Factor: 1.00

CONCENTRATION UNITS:CA3 NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

In o c c "5 _» -.

1 1 1-44-4----3C C "7 O . .

541 -73-1----106-46-7----100-51 -6----95-50-1 ----95-48-7----

108-60-1----106-44-5----621 -64-7----O / / i. I

7O C & 1

38-75-5----105-67-3----65-35-0----

X i i J i, i

120-32-1----91-20-3----106-47-8----87-68-3----59-50-7----91-57-6----77-47-4----

35-95-4----j I O O /38-74-4----

1 3 1 - 1 1-3----208-96-3----606-20-2----

- - -Phenol• ---bi s(2-Chl oroethyl )ether ___---2-Chl orophenol---1 ,3-Dichlorobenzene---1 ,4-Dichlorobenzene---Benzyl a l c o h o l--- 1 , 2-Di chl orobenzene

• - --2 -Me thy 1 phen ol---bi s(2~chl oroi s o p r o p y l )ether---4-Methyl phenol---N-Ni troso-di - n - p r o p y l a m i ne __•---Hexachl oroethane---Ni trobenzene

• - - - I sopho r one•---2-Ni trophenol•---2,4-Oimethylphenol•---Benzoic acid•---bi s(2-Chloroethoxy)met hane __•---2 , 4-Di chl orophenol•---1 ,2,4-Trichloroben_ene•---Naphtha! ene•---4-Chloroani 1 ine•---Hexachl orobutadi ene-----4-Chloro-3-methyl phenol•---2-Methylnaphthal ene- - - -He x ac hi o r oc y c 1 open t a di ene __•---2,4.6-Trichlorophenol• ---2 . 4 . 5-Tri chl orophenol•---2-Chl o r o n a p h t h a l ene----2-Ni troani 1 i ne• - - - D i m e t h y l p h t h a l a t e•---Acenaphthyl ene• - - - 2 , 6 - D i n i t r o t o l u e n e

860.860.860.860.360.860 .860.360 .860 .860.860 .860.860.860.360.360.

4200.360.860.360 .360.860.860.860.860.360.860 .

4200.360.360 .360.

1u 1u lu 1u lU Iu 1u lu 1u iu 1u lu lu iu 1u 1u lu lu lu lu 1u l

I'J 1u 1I'J

IU |uu l

1^25^uuuu

£54J4

c n R M T c y - i

!C EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

I '| CAU98



M a t r i x : ( s o i l / w a t e r ) SOIL L a b S a m p l e I D :

Sample w t / v o l : 30.1 (g/mL) G Lab F i l e ID: D8577


% M o i s t u r e : not dec. 22. dec. 0. Date E x t r a c t e d : 2/ 1/31


GPC C l e a n u p : (Y/N) Y pH: 6.3 D i l u t i o n F actor: 1.00


93-03-2-------3-Ni troani 1 ine_83-32-9-------Acenaphthene__51-28-5-------2,4-Dinitrophenol

100-02-7-------4-Nitropheno1 ____132-64-9-------Di benzofu ran______12 1 - 1 4 - 2 - - - - - - - 2 , 4 - D i n i t r o t o l u e n e ,34-66-2-------Di ethyl p h t h a l a te__

7 0 0 5 - 7 2 - 3 - - - - - - - 4 - C h 1 o r o p h e n y 1 - p h e n y l e t h e r _36-73 - 7---- ---Fl uorene _________________

100-01-6-------4-Ni troani 1 i n e____________53 4 - 5 2 - l - - - - - - - 4 , 6 - O i n i t r o - 2 - m e t h y l p h e n o l .8 6 - 3 0 - 6 - - - - - - - N - N i t r o s o d i p h e n y l a m i n e (1).

101 -55-3-------4-Bromophenyl - p h e n y l e t h e r118-74- 1 - - - - - - - H e x a c h l orobenz ene ________87-S6-5-------Pentachloroph«nol _______35-01-8-------Phenant hr ene_____

•Anthracene84-74-2-------Oi-n-butyl p h t h a l a t e

206-44-0-------F1 uoran thene________123-00-0-------Pyrene_____________35-68-7-------Butyl benzyl p h t h a l a te__9 1 - 9 4 - l - - - - - - - 3 , 3 ' - O i c h l o r o b e n z i d i n e _56-55-3-------Benzo(a)anthracen e____

•Chrysene_l l 7 - 8 1 - 7 - - - - - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e .117-34-0-------Di-n-octyl p h t h a l a t e ______205-99-2-------Benzo(b)fluoranthen e______

•8enzo(k)f!uoranthene_50-32-8-------Ben_o(a)pyren e________

193-39-5-------Indeno(1,2,3-cd)pyrene.53-70-3-------Dibenz(a,h)anthracene

131-24-2-------Benzo(g,h,i)perylen e__

4200.250.

4200.4200.160.860.860.860.360.4200 .4200.860 .860.860 .

4200.2400.370 .860.

4600.3300 .360 .1700.1700.1500.310.360

1300.1500

J

BJu

560.860. |U360. | J 4:5

(1) - Cannot be separated from d i p h e n y l a m i n e

FORM I SV-2 1/87 Rev.

18 EPA SAMPLE N'.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET

I CAU93Lab Name: NET C o n t r a c t : 68090031 I

Lab Code: NET Case No.: 1574] SAS No.: S O G N o . : C A U 3 3


Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e ID: D8566




GPC C l e a n up: (Y/N)N pH: .0 D i l u t i o n Factor: 1.00


l U O - J O t1 l l -44-4----9r- c •— Q

541 -73-1----106-46-7----100-51-6----95-50-1----95-43-7----108-60- 1----106-44-5----621 -64-7----67-72- 1 ----G -^ O K .. __3 O 3 D - J "

/ O O J 1

83-75-5----105-67-9----65-35-0----

1 1 1 -91-1---.120-83-2----L h. U O i. 1

31-20-3----106-47-8----87-68-3----53-50-7---31-57-6----77-47-4---88-06-2----95-95-4---91-58-7----38-74-4----

13 1 - 1 1-3----_.Uo3b-o"~"'606-20-2----

---Phenol•---bi s (2-Chloroethyl )ether---2-Chl orophenol

•---1 ,3-Dichlorobenzene---1 , 4-Oi chl orobenzene•---Benzyl a l c o h o l- - - 1 , 2-Oi chl orobenrene

• - - - 2 - M e t h y l phenol---bi s(2-chloroi s o p r o p y l ) e t h* r

• ---4-Methyl phenol

•---Hexachl oroethane•---Ni trobenzene•---Isophorone•---2-Ni trophenol• ---2. 4-Dime thy! phenol•---Benzoic acid•---bi s(2-Chloroethoxy)methan e __•---2 , 4-Di chl orophenol----1,2,4-Trichlorobenzene----Naphtha! ene

•---Hexachl orobutadi en<?- - - - 4 -Chl o r o - 3 -me t h y ! p h en o 1 _______• - - - 2 - M e t h y l n a p h t h a l ene----Hexachl orocycl opentadi ene __•---2,4,6-Trichloropheno!----2.4.5-Trichl orophenol•---2-Chl o r o n a p h t h a l ene----2-Ni troani 1 i ne- - - - D i m e t h y l p h t h a l ate- - - - A c e n a p h t h y l ene----2. 6-Di ni t r o t o l uene

10.10.10.10 .10.10.10.10.10.10.10.10 .10.10.10.10.50.10.10.10 .10 .10.10.10.10.10.10.D'Mu

50.10 .10.10.

1|U|UIU1 u|U1 uI U1 'JIU1 u|U1 uIUI'J|UI'JIU|UI UI'J|U|UIUI'J|U|U

ifessIU|UI UIU1

443

IC EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________

I ~I CAU99

Lab Name: NET C o n t r a c t : S3D30031 I

Lab Code: NET Case No.: 15741 SAS No.: S O G N o . : C A U 9 3

M a t r i x : ( s o i l / w a t e r ) WATER L a b Sample I D :

Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e ID: 08566






99-09-2----83-32-3----51-28-5----

100-02-7----132-64-3----1 2 1 - 1 4 - 2 - - - -

7005-72-3----86-73-7----100-01 -6----534-52- 1 ----36-30-6----

1f\ 1 C C •*»OI -55-^----

87-36-5----O U l o

120-12-7----84-74-2----

206-44-0----123-00-0----

31-34-1----56-55-3----

117-31-7----1 1 7-84-0----

L U / U O j

U -5 C OIQ •_. "5 O C

53-70-3----131 -24-2----

1- - - 3 - N i t r o a n i l i n e |

• - - - Ac enap h t hen e |- - - 2 , 4 - Di n i t r op hen o 1 |

• - - -4 -N i t r o pheno 1 |- - - D i b e n z o f u r a n |

• - - - 2 , 4 -Di n i t r o t o 1 uen e 1- - -Di e thy 1 ph t ha 1 a te 1---4-Chloropheny! - p h e n y l e t h e r __ |- - - F l u o r e n e |

---4, 6-Di ni t r o - 2 - m e t h y l phenol __ |• - - -N -N i t r o sodi p hen y 1 ami ne (1) __ |- - -4- B r omophen y 1 -phen y 1 e t he r __ |•---Hexachl orobenzene 1- - - Pen tac h 1 o r op henol 1•---Phenanthrene |---Anthracene 1

• - - -Oi -n-bu t y 1 ph t ha 1 a t e |- - - Fl uo r an t hen e |•---Pyrene 1•---Butyl benzyl p h t h a l ate 1•---3,3'-Dichlorobenzidine 1- - -Benzo ( a ) an t h r acen e 1•---Chrysene |---bi s ( 2 - £ t h y l h e x y l ) p h t h a l ate _ |

- - - - Di -n -oc t y 1 ph t ha 1 a t e 1• - - - Be nz o ( b ) f 1 uo r an t h en e 1• - - - Ben z o ( k ) f 1 uo r an t hen e |• - - - Benzo ( a ) py r ene 1• - - - I n deno ( 1 , 2 . 3 -cd 1 p y r ene 1• - - -Di benz ( a . h 1 an t h r acene 1•-- -Benzo (g . h . i ) per y 1 ene J

1 -

150. |

. 10. |50. |50. |10. |10. |10. |10. '110. |50. |50. |10. |10. |10. |50. |10. |10. |10. |10. |.0. |10. |20. |10. |10. |3. |10.10.10.

ft 8-3010.10.10.

uuuuuuuuuuU'uuuuuuuuuuuuuBOuuuuuu

11111111ii11i111I111111111i1

>58i1i

(1) - Cannot be separated from d i p h e n y l a m i n e

FORM I SV-2 1/3

18 EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SnEET ___________

l" "——I C CB12

Lab Name: NET C o n t r a c t : b3D30031 I

Lab Code: NET Case No.: 1 5 7 4 1 . SAS No.; S D G N o . : C A U 3 3

M a t r i x : ( s o i l / w a t e r ) WATER L a b Sample I D :

Sample *t/vo1: 1000.0 (g/mL) ML Lab F i l e ID: D8553






1/1 f*t Q _ *5

1 1 1 -44-4----J 3 O / O

541-73-1----106-46-7----100-51 -&----95-50-1----95-48-7----

108-60-1 ----106-44-5----621-64-7----67-72- 1 ----38-95-3----"7O CO 1

83-75-5----105-67-9----65-35-0----

1 1 1 - 9 1 - 1 ----120-83-2----120-82- 1----91-20-3----106-47-3----

53-50-7----31-57-6----77-47-4---88-06-2----35-95-4---91-58-7----88-74-4---

1 3 1 - 1 1-3---

606-20-2----

---Phenol• ---bi s ( 2-Chl or oe thy 1 ) et he r ___---2-Chl orophenol•---1 , 3-Oichlorobenzene---1 ,4-Dichlorobenzene•---Benzyl alcohol---1 , 2-Di ch! orobenzene•---2-Methyl phenol---bi s(2-chloroi sopropyl )ether•---4-Methylpheno!- - -N -N i troso-di -n-propyl ami ne __•---Hexachl oroethane•---Ni trobenzene• - - - I sophor one•---2-Ni trophenol• ---2 , 4-Dimethyl pheno 1•---Benzoic acid----bi s(2-Chloroethoxy)methan e __•---2, 4-Di chlorophenol•---1 , 2,4-Trichl orobenzene•---Naphthalene----4-Chloroani ! ine•---Hexachl orobutadi ene-- --4-Chl o ro-3 -me thy 1 pheno 1 ____•---2-Methylnaphthalene- - - -He x ac h 1 or oc y c 1 open t a di en e __• --- 2 , 4 , 6 -Tr i chl or ophenol- - - - 2 , 4,5-Tri chl orophenol----2-Chl oronaphtha! ene•---2-Ni troani 1 i ne• - - -Di met h y l p h t h a l a t e----Acenaphthylene•---2,6-Dinitrotoluene

10.10.10.10.10.10.10.10.10. •10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.

10.10.10.

1IUIUIUI'J|UI U|U|U|UI'J|UI'JIU|U|UI UI U|U|UIUIU|UIU|U|UI U|U|U

Dtijss;|U|UI U1

472

FORM I SV-1 1/37 R*v.

1C EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________

II CC81Z

L a b N a m e : N E T C o n t r a c t : 6809003! I

Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 3 3t


Sample \* t / v o 1 : 1000.0 (g/mL) ML Lab F i l e ID: D8559


% M o i s t u r e : not dec. 100. dec. 0. Date Ex t r a c t e d : 1/28/91




39-09-2----O -3 O t 7

i w O 3

100-02-7----1 32-64-9----1 2 1 - 1 4 - 2 - - - -34-66-2----

7005-72-3----86-73-7----

100-01-6----534-52-1----36-30-6----

101-55-3----1 13-74-1 ----87-36-5----85-01-3----

120-12-7----34-74-2----

206-44-0----123-00-0----85-68-7----3 1 -34-1 ----56-55-3----

218-01-3----117-81-7----117-84-0----205-99-2----207-03-9----50-32-3----

193-39-5----53-70-3----

i q i _ ? 4 _ 2 - - -

- - - 3 -N i troani 1 i ne

---2. 4-Oini trophenol---4-Ni trophenol---Di benzofuran- - - 2 , 4-Di ni trotol uene- - - D i e t h y l p h t h a l a t e- - - 4 - C h l o r o p h e n y l -phenyl ethe r __--- F l uorene•---4-Ni troani 1 i ne- - - 4 , 6 - D i n i t r o - 2 -met hy 1 phenol __

• - - -N -N i t r o sodi p heny 1 ami ne (1) __- - - 4 - B r omophen y 1 - phen y 1 e t he r __•---Hexachl orobenzene---Pentachlorophenol•---Phenanthrene---Anthracene•---Di - n - b u t y l p h t h a ! a t e•---Fl uoranthene•---Pyrene• ---Butyl benzyl p h t h a l ate•---3.3'-Oichlorobenzidine•---Benzo(a)anthracene- - - -Ch r y sen e- - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e __----Di -n-octy!phthalate•---Benzo(b)fluoranthene•---Benzo(k)fluoranthene•---Benzo(a)oyrene----Indeno(l .2,3-cd)pyrene----Dibenz(a.h)anthracene----Benzo(q.h.i)perylene

50. |U10. |U50. |U50. |U10. |U10. | U10. |U10. | U10. |U50. | U50 . |U10 . | U10 . |U10. |U50. U10. U10. U10. U10. U10. U10. U20. U10. |U10. U3 . 8010. U10. U10. Uwsq?5^10. U10. |U 473_____________ _ _ _______i__i


FORM I SV-2 1/37 R e v .

IS EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________^

II C C B 1 3








GPC C l e a n u p : (Y/N)N pH: .0 D i l u t i o n Factor: 1.00


1r"^ O Q C O

1 l 1-44-4----35-57-8----

541 -73- 1----106-46-7----100-51 -6----95-50-1----O H - O /----

l U O O U i - - — -

106-44-5----621 -64-7----67-72- 1 ----

/ O w - f l

O O / 3 J

105-67-9----65-35-0----

1 1 1 - 3 1 -1----120-33-2----120-82-1----91-20-3----106-47-8----87-63-3----59-50-7----91-57-6----77-47-4----o O 1J D -,9C Q C A

i "DO /----

38-74-4----1 3 1 - 1 1 -3----— u o j b o606-20-2----

---Phenol---bi s( 2-Chl oroe thy! ) e the r ____---2-Chl oropheno!---1 , 3-Di chl orobenzene---1 , 4-Oi chl orobenzene---Benzyl alcohol---1 , 2 - D i c h l o r o b e n z e n e---2-Methyl phenol---bi s(2-chloroi sopropyl )ether---4-Methyl phenol- - -N -N i troso-di - n - p r o p y l a m i ne __---Hexachl oroethane---Ni trobenzene- -- I sophor one- --2-Ni trophenol---2,4-Dimethy! phenol---Benzoic acid---bi s(2-Chloroethoxy)methan e __---2,4-Oichlorophenol---1 ,2,4-Trichl orobenzene---Naphthalene---4-Chloroani ! ine---Hexachl orobutadi ene- - - 4 - Chl o r o -3 -me t h y 1 p heno 1 ____- - - 2 - M e t h y l n a p h t h a l e n e- --He xachl or oc y c 1 open tadi ene __---2.4,6-Trichlorophenol---2,4,5-Trichlorophenol---2-Chl oronaphthal ene---2-Ni troani 1 i ne- - - D i m e t h y l p h t h a l a t e---Acenaphthyl ene- - - 2 . 6 - D i n i t r o t o l u e n e

10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.

50.10.10.10.

1 1|U ||U | IU | M|U | W|U |IU |IU |1- 1IU |I'J 1IU ||U ||U |IU |IU |IU ||U ||U |IU ||U ||U ||U ||U |IU |IU ||U I

3$>56|! AI" i ™|U ||U |1 1

1C EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________

II CC813


Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 9 3




% Moisture: not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91


GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00


99-09-2---33-32-9---51-23-5---100-02-7---132-64-9---121-14-2---84-66-2---

7005-72-3---86-73-7---100-01 -6---534-52-1---36-30-6---

101-55-3---i i O / ** A

87-86-5---

120-12-7---84-74-2---206-44-0---129-00-0---85-68-7- —91-94-1---56-55-3---

218-01 -9---117-31-7---117-84-0---205-99-2---207-03-9---50-32-8---

53-70-3---191-24-2---

1

----3-Ni t r o a n i 1 i ne- ---Acenaphthene- - - - 2 , 4 - D i n i t r o p h e n o l----4-Ni trophenol- - - - D i benzofuran----2,4-Dini trotoluene- ---Di ethyl phtha! ate----4-Chlorophenyl -phenyl ethe r __----Fl uorene----4-Ni troani 1 i ne

- - - -N -N i t r o sod i p hen y 1 ami n e (1) __- - - - 4- B r omophen y 1 -pheny 1 e t he r __----Hexachl orobenzene----Pentachl orophenol----Phenanthrene----Anthracene----.Di - n - b u t y l p h t h a l a t e----Fl uoranthene- ---Py r ene----Butyl benzyl phthal ate----3 , 3 '-Oi chl orobenz i di ne----Benzo(a)anthraoene- - --Ch r y sene- - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l ate __----Di -n-octy!phthalate----Benzo(b)fluoranthene- - - - B e n z o f k l f l u o r a n t h e n e----Benzo(a)pyrene----Indeno( 1 .2.3-cd)pyrene----Oi benz(afh)anthracene- - - - 8 e n z o ( g . h . i ) p e r y ! e n e

50.10.50.50.10.10.10.10.10.50.50 .10 .10 .10.50.10.10.10.10.10.10.20.10.10.2 .10.to.

10*.10.10.

1|UIU|U|UIU|U|U|U|U|U|U|UIU|U|U|U|UI U|U|U|UIU|U|U| 80|U|U

|U|U|U1

497


FORM I SV-2 1/87 R e v .

10 EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET

I CAU93Lab Name: NET C o n t r a c t : 68D90031 I



Sample wt/vol: 1000. (g/mL)ML Lab F i l e ID: F20A2018


% M o i s t u r e : not dec.100. dec. 0. Date E x t r a c t e d : 1/29/31

E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date A n a l y z e d : 2/20/31


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/- or ug/Kg) UG/L Q

313-84-6-----ALPHA-BHC313-85-7-----8ETA-BHC319-86-8-----DELTA-BHC53-89 -9-----GAMMA-BHC76-44-3-----HEPTACHLOR

309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE359-38-3-----ENDOSULFAN I60-57- 1 - - - - - O I E L D R I N72-S5-9-----4,4'-OOE72-20-8-----ENDRIN

33213-65-9-----ENDOSULFAN I I72-54-S-----4,4'-DDO

1031-07-3-----ENDOSULFAN SULFATE50-29-3-----4,4'-OOT72-43-5-----METHOXYCHLOR

53494-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE

12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111141-16-5-----AROCLOR-123253463-21-9-----AROCLOR-124212672-23-6-----AROCLOR-124811097-69-1-----AROCLOR-125411096-82-5-----AROCLOR-1260

.050 |U

.050 | U

.050 |U

.050 |U

.050 |U

.050 |U

.050 |U

.050 |U

.100 |U

.100 |U

.100 |U

.100 | U

. 100 |U

. 100 |U

.100 |U.50 | U

. 100 |U.50 |U.50 | U1.0 | U.50 |U.50 |U.50 |U.50 | U.50 |U1.0 |U1.0 |U

AR302563

FORM I PEST 1/87 Rev

10 ' EPA SAMPLE NO.PESTICIDE ORGANICS A N A L Y S I S DATA SHEET ______________

I| CAU94


Lab Code: NET Case No.: 15741 * SAS No.: SDG No.: CAU93




% Moisture: not dec.100. dec. 0. Date E x t r a c t e d : 1/29/31



CONCENTRATION UNITS:CAS NO. COMPOUND C-g/L or ug/Kg) UG/L Q

319-84-6-----ALPHA-8HC313-35-7-----8ETA-8HC319-86-8-----DELTA-8HC58-33-9-----GAMMA-BHC76-44-8-----HEPTACHLOR

303-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-93-3-----ENDOSULFAN I60-57-1-----DIELDRIN72-5S-9-----4,4 '-ODE72-20-8-----ENDRIN

33213-65-3-----ENDOSULFAN II72-S4-8-----4,4'-OOD

1031-07-3-----ENOOSULFAN SULFATE50-29-3-----4,4'-ODT72-43-5-----METHOXYCHLOR

53494-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLOROANE8001-35-2-----TOXAPHENE

12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111 141-16-5-----AROCLOR-123253469-21-9-----AROCLOR-124212672-29-6-----AROCLOR-12481 1097-63-1-----AROCLOR-12541 1096-82-5-----AROCLOR-1260

050 |U050 |U050 |U050 |U050 |U050 |U050 |U050 | U100 |U100 1 U100 |U100 |U100 |U100 |U100 |U.50 | U100 |U.50 | U.50 | U1.0 |U.50 |U.50 |U.50 | U.50 |U.50 |UI . 0 | U1.0 IU

AR30256«»646



I CAU96Lab Name: NET Co n t r a c t : 68D90031 |

Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 3 3•


Sample w t / v o l : 1000. (g/mL)ML Lab F ^ l e ID: F20A2023


% M o i s t u r e : not dec.100. dec. 0. Date E x t r a c t e d : 1/29/91




313-84-6-----ALPHA-BHC319-85-7-----BETA-BHC319-86-8-----DELTA-BHC58-89-9-----GAMMA-BHC76-44-8-----HEPTACHLOR

309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-33-3-----ENOOSULFAN I60-57-1-----DIELDRIN72-55-9-----4,4'-DDE72-20-8-----ENDRIN

33213-S5-3-----ENOOSULFAN I I72-54-S-----4,4 '-ODD

1031-07-8-----ENDOSULFAN SULFATE50-23-3-----4,4'-ODT72-43-5-----METHOXYCHLOR

53494-70-5-----ENDRIN KETONE5103-71-9-----ALPHA-CHLOROANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE

12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111141-16-5-----AROCLOR-123253463-21-3-----AROCLOR-124212672-23-6-----AROCLOR-124811037-63-1-----AROCLOR-12541 1036-82-5-----AROCLOR-1260

.050

.050

.050

. 050

.050

.050

.050

.050

. 100

. 100

. 100

. 100

. 100

. 100

. 100.50

. 100.50.501 .0.50.50.50.50.501 .01 .0

8R3G256565



I CAU37Lab Name: NET Contract: 68030031 I



Sample wt/vol: 30. (g/mL) G Lab F i l e ID: F20A2027

L e v e l : (!ow/med) LOW Date Received: 1/24/91

% Mo i s t u r e : not dec. 37. dec. 0. Date E x t r a c t e d : 2/ 1/91

E x t r a c t i o n : (SepF/Cont/Sone) SONC Date Analyzed: 2/21/91



319-84-6-----ALPHA-8HC319-85-7-----BETA-8HC319-86-8-----DELTA-BHC58-39-9-----GAMMA-BHC76-44-8-----HEPTACHLOR

309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-93-8-----ENOOSULFAN I60-57-1-----OIELDRIN72-55-9-----4,4'-OOE72-20-8-----ENORIN

33213-65-9-----ENOOSULFAN I I72-54-S-----4,4'-DDD

1031-07-S-----ENDOSULFAN SULFATE50-23-3-----4,4'-ODT72-43-5-----METHOXYCHLOR

53434-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLOROANE8001-35-2-----TOXAPHENE

12674-11-2-----AROCLOR-101611104-28-2-----AROCLOR-122111141-16-5-----AROCLOR-123253469-21-9-----AROCLOR-124212672-29-6-----AROCLOR-124811097-69-1-----AROCLOR-125411096-82-5-----AROCLOR-1260

25. |U25. |ll25. |U25. |U25. |U25. |U25. |U25. |U50. | U50. |U50. |U50. |U50. |U50. |U50. |U

250. |U50. |U50. | U

250. |U500. |U250. |U250. |U250. |U250. |U250. |U500. |U500. ' IU

65G

FORM I PEST 1/37 Rev.

ID EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET __

I| CAU98




Sample wt/vol: 30. (g/mL) G Lab F i l e ID: F20A2030


*o M o i s t u r e : not dec. 22. dec. 0. Date Extracted: 2/ 1/31

E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/21/91



1 7 O * * O

319-35-7--I T J S b o

76-44-8--303-00-2--

1024-57-3--j D .i-TO o60-57-1--/4"D5"72-20-8--

3 _ 1 3 - b b ?72-54-8--

1031-07-8--50-29-3--72-43-5--

53494-70-5--5103-71-9--5103-74-2--3001 -35-2--

12674-1 1-2--1 1 104-23-2--1 1 141-16-5--53469-21-9--12672-23-6--1 1097-69-1--1 1036-82-5--

-. _ -. A 1 D U A — B U /*

8C T __ - D U C

---DELTA-BHC---GAMMA-BHC- - - u c o T A r u i no---ALDRIN— — _-LJCDTA/~lJ( f\D IT D A Y T F\ C

---ENOOSULFAN I---01 ELDRIN---4,4'-DOE---ENORIN---ENDOSULFAN I I---4, 4'-DDD---ENDOSULFAN SULFATE---4, 4'-OOT

M_TT*LJAVV/*UI rtO

---ENDRIN KETONE---ALPHA-CHLORDANE-- -GAMMA -CHLORD AN E---TOXAPHENE---AROCLOR-1016---AROCLOR-1221---AROCLOR-1232---AROCLOR-1242---AROCLOR-1248---AROCLOR-1254---AROCLOR-1260

21 .21 .21 .2 1_ 4 •

21 .21 .21 .") 141 .H JL •

41 .41 .*+ 4 .41 .41 .

210.41 .

210.210.410.^ i n

210.210.210.210.410.410.

1IUI UIUI UIUI UIUI U|UI'JIUI'JIU|U|UIUIUI'J|UIUI'J|UI'JI'JI'JI'JIU1


• 10 EPA SAMPLE NOPESTICIDE ORGANICS ANALYSIS DATA SHEET

I CAU99Name: NET C o n t r a c t : 63D90031 I

_ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93

M a t r i x : (soil/water) WATER Lab Sample 10:

Sample w f / v o l : 1000. (g/mL)ML ' Lab F i l e ID: F20A2024


* M o i s t u r e : not dec.100. dec. 0. Date Extracted: 1/29/91

E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date Analyzed: 2/21/91



319-84-6---3 i J <5 O /

.$ l j 3 b o

76-44-8---303-00-2--

1024-57-3---? v ? ./ Q O

60-57-1---72-55-9---72-20-8---

^ J w l - 5 Ov J

72-54-3---1031-07-3---

50-29-3---72-43-5--.

53434-70-5---5103-71-9---5103-74-2---3001-35-2---

iCO/4* l l « *

1 1 104-23-2---1 1 1 4 1 - 1 6-5---53463-21 -9---12672-29-6---11097-63-1--11096-32-5---

MLrnnon**.C 1 n B n v_,

•--OELTA-BHC---GAMMA-BHC

Her i H v^ n — v ~---ALDRIN•--HEPTACHLOR EPOXIDE---ENDOSULFAN I---DI ELDRIN---4,4 '-DDE---ENDRIN•--ENDOSULFAN II•--4,4'-OOD•--ENDOSULFAN SULFATE• - -4 4 ' - DOT** | •* V \ti \

MC "— 'LJ— t V V — 'LJI f\C r

•--ENORIN KETONE•--ALPHA-CHLORDANE•--GAMMA-CHLORDANE•--TOXAPHENE•--AROCLOR-1016---AROCLOR-1221•--AROCLOR-1232---AROCLOR-1242•--AROCLOR-1248---AROCLOR-1254•--AROCLOR-1260

.050

.050

.050

.050

.050

. 050

.050

.050

. 100

. 100

. 100

. 100

. 100

. 100

. 100.50

. 100.50R A. 5 0

1 .0

.50

.50

.50

.50

.501 .01 .0 ,

1IUIUIUIUIUIUIUI'JI'uI'-1I UIU !I'J|UIU|U|UI U|U|UI'JIUIUIU|UI'J|U1

AR302568C,,6b

10 EPA SAMPLE NOP E S T I C I D E ORGANICS A N A L Y S I S DATA SHEET _____________

II CC812


Lab Code: NET Case No.: 1 5 7 4 1 * SAS No.; S D G N o . : C A U S 3


Sample w t / v o l : 1000. (g/mL)ML Lab F i l e ID: F20A2016


*• M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/29/91

E x t r a c t i o n : (SepF/Cont/Sone) SEPF Date A n a l y z e d : 2/20/91



313-84-6--3 L ? >i y l» j o o oD 0 O 33

76-44-8--303-00-2- -

1024-57-3--D 3 3 . 5 O

60-57-1--"7 T C P O

72-20-8--33213-65-3--

72-54-3--1031-07-8--

50-23-3--72-43-5--

53434-70-5--5 103 -71 -9--5103-74-2--3001-35-2--

12674-1 1-2--11 104-23-2--1 1 141-16-5--53463-2 1-3--l _ _ O / t _ . t ; 7 O

1 1037-69-1--11 09 6-8 2 -5--

- _ _ A 1 DLJA-QUr

8C T A — D U CC 1 n " Dn (~-

---DELTA-BHC---GAMMA-BHC

C r \ rt V* — 1 L w — \

---ALDRINt _ r i n V _ . n L U K t, r U A 1 U t

---ENDOSULFAN I---DI ELDRIN---4, 4'-DDE---ENDRIN---ENDOSULFAN I I---4, 4'-DDD---ENDOSULFAN SULFATE---4,4'-DOT

tut C T t_l rt V V /^ t_l 1 /~\ D

---ENDRIN KETONE---ALPHA -CHLORD AN E---GAMMA-CHLORDANE---TOXAPHENE---AROCLOR-1016---AROCLOR-1221---AROCLOR-1232---AROCLOR-1242---AROCLOR-1248---AROCLOR-1 254---AROCLOR-1260

.050

.050

.050

.050

.050

.050

.050

.050

. 100

. 100

. 100

. 100

. 100

. 100

. 100.50

. 100.50.501 .0.50.50.50.50.501 .01 .0

1I UIUIUI UI'JI UI UIUI UI'JI UI UIUI UI UI'J|UI'JIUIUIUIUIUI'JIU|UIU1

RR302569


ID £PA SAMPLE NO.PESTICIDE ORGANICS A N A L Y S I S DATA SHEET

| CCB13•_ab Name: NET Contract: 68D30031 |________

_ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33•M a t r i x : (soil/water) WATER Lab Sample ID:



* Moisture: not dee.100. dec. 0. Date E x t r a c t e d : 1/29/91


GPC Cleanup: (Y/N) N • >pH: .0 D i l u t i o n Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND fug/L or ug/Kg) UG/L Q

313-84-6-----ALPHA-8HC313-85-7-----8ETA-BHC319-86-8-----DELTA-BHC58-89-9-----GAMMA-BHC76-44-8-----HEPTACHLOR

309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIOE959-93-3-----ENOOSULFAN I60-57-1-----OIELDRIN72-5S-9-----4,4'-DDE72-20-3-----ENORIN

33213-65-9-----ENDOSULFAN II72-54-S-----4,4'-ODD

1031-07-8-----ENDOSULFAN SULFATE50-29-3-----4,4'-DDT72-43-5-----METHOXYCHLOR

53494-70-5-----ENDRIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE12674-11-2-----AROCLOR-101611 104-28-2-----AROCLOR-122111 141-16-5-----AROCLOR-123253463-21-9-----AROCLOR-124212672-29-6-----AROCLOR-12481 1097-69-1-----AROCLOR-125411 096-82-5-----AROCLOR-1260

,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U, 100 |U, 100 | U, 100 |U, 100 |U, 100 |U, 100 |U,100 |U.50 |U

, 100 |U.50 | U.50 |U1.0 |U.50 |U.50 |U.50 |U.50 |U.50 |U1.0, |U1.0 |U

8R30257Q677


Appendix BTIC Results

AR302571

SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ________________

TENTATIVELY IDENTIFIED COMPOUNDS | ~—————————"I CAU93



Matrix: (soil/water) WATER Lab Sample ID:



* Moisture: not dec. 100. Date Analyzed: 1/29/91


CONCENTRATION UNITS:Number TICs found: 3 (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 76-13-12. 110-54-33. - -4.S.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

COMPOUND NAME

Ethan*, 1 , 1 , 2-t H ehl or o-l , 2 ,Hexane (DOT) (8CI9C I )UNKNOWN

-

-,

RT

4.326.24

22.85

-

EST. CONC.

90.5.10.

———— H D Q fl 9 fA n o u d H

Q

JJJ

L "7 9

21FORM I VOA-TIC 1/87 Rev.

IE EPA SAMPLE NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET ________________

TENTATIVELY I D E N T I F I E D COMPOUNDS |I CAU94

Lab Name: NET Contract: 68D90031 I _____________








CAS NUMBER

1. 76-13-12. - -3. - -4.5.6.7.8 .9.10.11 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

1COMPOUND NAME • | RT

E-t liana t 1 , l.-.-,r.t-f-ic.h-V«ro- r , 2 . \ 4" . 3 0UNKNOWN HYDROCARBON 1 6.22UttKfTCWN 1 22.86

111111I11I1111I111111111I111

EST. CONC..............

90.7. -10. '

1 R n • 0 f> <"» r- -i1 A n 0 U c <j* /l

Q 1L.»-••r i

u J ..— <

3 — 43=138

FORM I VOA-T1C 1/87 Rev.

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS | ~~———————I CAU95

Lab Name: NET Contract: 68090031 |

Lab Code: NET Case No.: 1574', SAS No.: SDG No.: CAU93


Sample *t/vol: 5.0 (g/mL) ML Lab F i l e ID: F3704

Level: (low/med) LOW Date Received: 1/24/9*


Column: (pack/cap) CAP Dilution Factor: 1.00

CONCENTRATION UNITS:Number TICs found: 3 C-g/- or ug/Kg) UG/L

CAS NUMBER

1. - -2. - -3. 76-13-14.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.k30.'

COMPOUND NAME

UNKNOWN HYDROCARBONUNKNOWNETHANE, 1 , 1 ,2-TRICHLORO-l ,2,2

RT

6.2322.874.31

.

-

. EST. CONC.

7.5.90.

ft D tj n *> rr«H3025i

Q

JJJ

"7 f7^___________ 56

FORM I VOA-TIC 1/87 Rev.

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS | ~I CAU96



Matrix.'(soil/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 (g/ml.) ML Lab File ID: F3705





CAS NUMBER

1. 110-54-32. 76-13-13.

(4.5-6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.

•io.•

COMPOUND NAME

Hexane (DOT) (8C I 9C I )ETHANE, 1,1 ,2-TRICHLORO-l ,2,2

-

RT

6.244.31

.

EST. CONC.

8.80.

QK3021

Q

Jj

-i -i t r*D7b— i7'


IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

TENTATIVELY IDENTIFIED COMPOUNDS |I CAU97

Lab Name: NET Contract: 68090031 |







CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/KG

CAS NUMBER

1 . - -2.3.4.5.6.7.8.9.10.11 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

COMPOUND NAME.. ———— ..... ———————————————

RT

22.72

EST. CONC.———— . ———— ..

10T.

. _ ~ ~A R 3 Q £ 5

Q

*j '__ ji

i^h (i ,___..!i •


1E EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET __________

TENTATIVELY I D E N T I F I E D COMPOUNDS ———I CAU98

Lab Name: NET Contract: 68D90031 |



Sample wt/vol: 5.3 (g/mL) G Lab Fil e ID: F3725



Column: (pack/cap) CAP Di l u t i o n Factor: 1.00

CONCENTRATION UNITS:Number TICs found: 0 C-g/L or ug/Kg) UG/KG

CAS NUMBER

1 .2 .

k 3 .1 4.

5 .6.7.8 .9 .10.1 1 .12.13.14.15 .16.17.18.19.20.21 .22 .23.24 .25 .26.27.28.

' 30.

COMPOUND NAME RT EST. CONC.

_H'R3Q__5 i

i1 Q1

.^7

FORM I VOA-TIC 1/87 Rev

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: NET Contract: 68D90031


Matrix: (soil/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 (g/mL) ML Lab File 10: F3706





CAS NUMBER

1. 110-54-32. -3.4.5.6.7.8.9.10.11 .12.13.14.IS .16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

Hexane ( DOT) C8C I 9C I )UNKNOWN

r*

RT--------

6.2222.85

EST. CONC.

6.6.

•

s p o n 9 i~

Q

JJ

5 7 8

— T7.1 c.FORM I VOA-TIC 1/87 Rev

IE EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET _____ __________

TENTATIVELY IDENTIFIED COMPOUNDS | "I CCB12

Lab Name: NET Contract: 68D90031 ____





* Moisture: not dec. 100. Date Analyzed: 1/29/91



CAS NUMBER

1. - -^2 .

k 3'1 4'^ 5.6.7.8 .9 .to.11 .12.13 .14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.

,29.MO.

COMPOUND NAME

nrjifN.nh.tt" — — "' " ~~~"~

1ii

RT

22.86

_EST. CONC.

. 1 U-T*-«

-

-

fi n i n n A h J U _. u

QL-a-?«1—9 ——— 1

"?O/ J

.145FORM I VOA-TIC 1/87 Rev.

1E EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______

TENTATIVELY IDENTIFIED COMPOUNDS |I CCB13

Lab Name: NET Contract: 68D90031 |







CONCENTRATION UNITS:Number TICs found: 3 (ug/- or ug/Kg) UG/L

CAS NUMBER

1. 76-13-12. 110-54-33. - -4.5.6.7.8.9.10.1 1 .12 .13.14.15.16.17.18.19 .20.21 .22.23 .24 .25.26.27.28.29.30.

COMPOUND NAME

i-T44AN rn".T 72 - f FrrCHTOfTO' - 172 ! ,llennfl (POT) en-fr.-9e.-3 —— ' -UNKNOWN

RT

4.3T—— ••&-. 2-3 -

22.85

EST. CONC.——— ————————

• - 2ocr: —10%

._ . .

5 R 0 2 5

Q—— i--T--~ j.. j— (

RO 1l


.. *. v-.>- • .-it-'1'' •

Matrix: (901 ' /ir»ater) K*TER ... Sampl« ID:

Sampl» v»t/vol: 5,0 (9/wL) ML Lab F i * « 10; F3$»9

L e v e l ; (low/nr.«d) LOW D.t» R««»iv«_: :/24/91

% Hoi*t-r»: n«fc -•«. JOO. 0«t» Ana'y.s-; J/2V3I

Caljmn: (pi«l«/oap) CAP D i l u t i o n Factoi ; l . 00

CONCENTRATION UNITS:Numb«r TIC* r'ognd: 1 (uf/- or vig/Kg) U6/L

1j CA, MUMiEft

| 1. 7&-J3-11 2-1 3., -.1 5.r 6.' 7 .• 9.1 9.1 10.1 It.1 !_.f 13.1 14.1 IS.| 16.1 17.i 18.1 IS.I 20.i 21.; 22.1 23. .,1 24.1 25. ... ,.1 26.1 27.| 28. •1 29.1 30.1

1CCI^OUNO NAME

Elnan*, 1 , 1 , 2-fcr i chl pro -J , 2 ,

,„ ,, ... .,„.„., , .-

._

RT

-.3!

- ........

FST. CONC.

40.

»

—————————— ft

J

Ri_•»-••

k f* C*

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Name: NET Contract: 68D90031 I___





% Moisture: not dec. 100. dee. 0. Date Extracted: 1/28/91

E x t r a c t i o n : (SepF/Cont/Sone) CONT Date Analyzed: 2/ 7/91



CAS NUMBER

1 -2.3.4.5 .6.7.8.9.10.1 1 .12 .13.14.15 .16.17.18.19.20.21 .22.23 .24.25.26.27.28.29.30.

ICOMPOUND NAME

, ——————————— , —— .,,,..»..,.RT EST. CONC.

— AR3025£

iQ 1

_A—— 1

,

if — i|_, |l1 __ _i\

FORM I SV-TIC 1/87 Rev

IF EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____ __________


Lab Name: NET Contract: 68090031 I






Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91



1CAS NUMBER

1 1. 10544-50-0

1 3'r 4.5 .6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.

^27.28.29.| 30.1

COMPOUND NAME

SULFUR

y

RT--------22.76

•

EST. CONC.

10.

dKliOX

Q

BJ

i B .5

FORM I SV-TIC 1 /87 Rev.

IF EPA SAMPLE NO.SEMIVOLAT1LE ORGANICS ANALYSIS DATA SHEET _________

TENTATIVELY IDENTIFIED COMPOUNDS |~| CAU96

Lab Name: NET Contract: 68D9003 1 I





X Moisture: not dec. 100. d«c. 0. Date Extracted: 1/28/91

E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91



CAS NUMBER

1 .2.3.4.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

COMPOUND NAME RT

, ,

EST. CONC.

- -

riH:«i25

0

ai*—O •}«-• -J

FORM I SV-TIC 1/87 Rev.

1F EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALY S I S DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS |—————————————"| CAU97

'ab Name: NET Contract: 68D90031 ___




Level: (1ow/med) LOW Date Received: 1/24/91

% Moisture: not dec. 34. dec. 0. Date Extracted: Z/ .1/91

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/91



CAS NUMBER

1. - -2. 10544-50-03. - -4. - -5. - -6. - -7. - -8.9.10.11 .12.13.14.15.16.17.18.19. •20.21 .22.23.24.25.26.27.28.23.30.

COMPOUND NAME

tffl KNOWN ————SULFURUNKNOWN HYDROCARBONUNKNOWN AROMATICUNKNOWNUNKNOWNUNKNOWN

RT

4.7322.8126.4327.5832.2532.3235.69

EST. CONC..............

r~ -•- Am>A>~ -400<T;1000.400.800.600.400.400.

flp onnr- r,j-« 1 1 v> y c ,5 d *j

Qv-jjjjjj

FORM I SV-TIC 1/87 Rev

1F EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS | ~————'I CAU98


Lab Code: NET Case No..1 15741 SAS No.: SDG No.: CAU93



Le v e l : (low/med) LOW Date Received: 1/24/91

\ Moisture: not dec. 22. dec. 0. Date Extracted: 2/ 1/91

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/91

GPC Cleanup: (Y/N) Y pH: 6.9 Dilution Factor: 1.00


CAS NUMBER

1. - -2. - -3. 10544-50-04. 2381-21-75. - -6. - -7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

COMPOUND NAME

•tfN-KNOWW-'UNKNOWNSULFURPYRENE. 1-METHYLUNKNOWN AROMATICUNKNOWN

RT

f~- 4.8622.1422.8224.0527.5929.07

.. . ..

EST. CONC.-------------—— 3000.—

300.500.500.500.400.

&R302J

Q.....J -"*"JJJJJ

L a -5c_»b ,4

FORM I SV-TIC 1/87 Rev,

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET __________•

TENTATIVELY I D E N T I F I E D COMPOUNDS | — — — — —I CAU99

b Name: NET Contract: 68D90031 I









CAS NUMBER

1 .2.

i J:5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23 .24.25.26.27.28.29.30.

COMPOUND NAME RT—— ————

EST. CONC.

.

0

q •?u / ^, Iik Q

FORM I SV-TIC 1/87 Rev,

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET "* SAMPLE N0-TENTATIVELY IDENTIFIED COMPOUNDS - ———————— ———— -

Lab Nam*: NET Contract: 68D90031

Lab Code: NET Case No.: 15741 SAS No.: SOG N o > .

M a t r i x : (soil/water) WATER Lab Sflmple ID;

Sample wt/vol: 1000.0 (g/mL) ML Lab Fn. IQ. 0855g

L«v«l : (low/med) LOW n . ...Date Received: 1/24/91

* Moisture: not dec. 100. dec 0 n.* - .' u' Date Extracted: 1/28/91


GPC Cleanup: (Y/N)N pH: .0 Di1ution Factor: , . 00

_, . -.._, . CONCENTRATION UNITS:Number TICs found: 1 (ug/_ Q_ Ug/Kg3

CAS NUMBER

1. 10544-50-02.3.4.5.6.7 8 .9.10.11.12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.

COMPOUND NAME

3ULTU* ———————————————— ..--.- 4

RT

— - £ -«p-*-*~

-

-

*

EST. CONC.

———— • • - ——— 8 —— , ,

——— frfr£K

Q

_EJ— ..

}9Cq.<_.C»u CI1 ^

t)4fI 174

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY I D E N T I F I E D COMPOUNDS | — — — —I CCB13

Lab Name: NET Contract: 68090031 |__________






E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91


CONCENTRATION UNITS:Number TICs found: 0 (-g/- or ug/Kg) UG/L

«

CAS NUMBER

M:* 3.4.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.

k 27.^28.

30.

COMPOUND NAME RT EST. CONC.

a H :i ii _> 5

Q

1 1 i

ay498

1


Appendix CDPO Report

AR30259Q

ORGANIC REGIONAL DATA ASSZSSMtNT

CASE NO. ( > f wLABORATORY ,,A/ T

SOG • CA<*. 3j>saw*DPf> ACTION _ „ FY1

DATA ASSE:

1. HOLDING TIMES2. GC/MS TUNE/INSTR. PERFORM.3. CALIBRATIONS4. BLANKS5. SURROGATES6. MATRIX SPOCE/DU?

7. OTHER OjCS. INTERNAL STANDARDS9. COMPOUND IDENTIFICATION10. SYSTEM PERFORMANCE11. OVERALL ASSESSMENT

0 * Diet had so probl«ffi*/or quaJLfi«d dueM « Dita quaJifrd dot to otjor problem.Z • D»a unacctpabi*.X • Probtoott, bos do ao( i/Tiet daa.

Ar-nrtN rrewft .S.,?1 "* --- 4-*s* u.-**«

lf_T". /Vf-* - **tL0,- cJ Jf l , /d^

. sm i-t -rz»6/NO. OF SAJU LES/MATRIX /d /

. REVIEWER (IF NOT

. REVIEWER'S NAME

. COMPLETION DATE

5SVTENT SUMVAiy

VOA 8NA

0 Q__0 05. /0' g)r0 j2 _-d- J-—^ f.n nd rj0 0-M— JL-

to minor probtems.

xt*#** -> •A'' A **

i-i_j_->-« <^— / l.vr-,-£it .fa

TV JffJ ^ -

W*ti~~, friCJ)C5D) w A-i J-f /'J'«I A>X*«-rJL . Ccrvt,.

^j/.r/

PEST OTHER

a _ /.^^- /v^_ __vc)a£a6 / •2 __ / __

5~- jsy jO«-_ T! /<K*L _**e ) pk+ll+jLA0 0 "

AREAS OF CONCERN:

ftB30259i

NOTABLE PERFORMANCE:

Appendix DSupport Doc-mentation

AR302592

6AVOLATILE ORGANICS I N I T I A L C A L I B R A T I O N DATA


Lab Code: NET Case No.: 15741 SAS No.: SDG No.:

Instrument ID: 7002F C a l i b r a t i o n Date(s): 1/25/91 1/25/91

Matri x: (soi I/water ) WATER Level :( 1 ov^/med ): LOW Col umn : (pac k /cap ) CAP

Min RRF for SPCC(#) - .300 (0.250 for Bromoform) Max %RSO for CCC(») - 30.OX

LAB F I L E ID: RRF020- F3663 RRF050- F3664RRF100- F3665 RRF150- F3666 RRF200- F3667

1COMPOUND |RRF020

Chl o romet hane * .609B r omome t hane 1 .879Vin y l chloride * .813Chloroethane 1 .540

LMethvlene chloride I 1.505•Acetone 1 .293'Carbon d i s u l f i d e 1 2.4911 . 1 - Di chl oroethene * 1.0201 . 1 -Di chl oroethane * 1.5451 , 2 - Di chl oroet hene (total)_| 1.270Chloroform »2.4521 . 2-Di chl oroethane | 1.3582-8utanone 1 .0171 , 1 , 1 -Tri chl or oethane _____ | .384Carbon te t rach.1 or i de j .363V i n y l acetate 1 .127B r omodi ch 1 o romet hane | .4981 . 2- Di chl or oor ooane • .255c i s- 1 , 3 -Di chl o ropropene __ | .360Trichloroethene 1 .376Di b r omochl oromethane | .5141 , 1 , 2-Tri chl oroethane ____ | .287Benzene 1 . 6 3 1t rans- 1 , 3 -Di chl oropropene _| .295Bromoform * .3664-Me thy! - 2-pen tanone 1 .2582-Hexanone | .172Te t r achl o roethene 1 .4221,1,2,2-Tetrachloroethane _* .619Toluene * .591

kChlorobenzene * .841^Ethvl benzene * .368|Styrene 1 .807IXylene (total) 1 .436

Toluene-d8 1 .880| Br omof 1 uor oben zene | .4761 , 2-Di chl oroethane-d4 ____ | 1.178

RRF050

.6361 .033.825.578

1 .340.202

2.7001 .0431.6121 .3062.5711 .471.022.437.41 1.241.561.287.411.407.592.325.689.346.449.300.206.445.698.628.905.396.857.463

1 .023.554

1 .334

RRF100

.6681 .245.878.636

1 .396.215

3 . 1241 . 1731 .7811 . 4232 . 7491 . 617.028.518.493.367.647.332.483.460.685.370.783.429.556.358.252.511.829.717

1 .042. 446.963.528

1 . 144. 619

1 . 435

RRF150

.5921 .219.781.593

1 .257.206

2.8891 .0831 .6191 .2992.4501 .460.027.499.476.399.629.319.467.440.681.358.747.424.549.367.255.494.815.687

1 .009.431.928.512

RRF200

.5421. 131.718.563

1.205.200

2.7931.0491 .5481 .2422. 2961 .410.027.492.471.417.619.317.470.431.675.349. 736.431.554.354.249.481.800.686.970m.500

RRF

.6091 . 101.803.582

1 .341.223

2.7991 .0741 . 6211 .3082.5041.4fi-t.024.466. 443.310.591.302.438.423.630.338.717.385.495.327.227.471.752.862.953

;°283M88

1.118 1.083 1.049.616| .596| .572

1.323 1.250 1.304

* 1RSD |

7.8*13. 6|7.3*6.2|8.8|17.8|8.3|5. 6*5 . 9*5.3)6. 7*6.6|

18.9|11 .8 j

10.3|10.3*

7.6|CT>

1 7 . 2ff*~14.4^16.2|7.7|

12.1*7.7*8.5*

P7.7*6.9|7.7|

-4-3&I_. w vjl10.0|10.4|7.41

7AVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: NET Contract: 68D90031t


Instrument ID: 7002F C a l i b r a t i o n Date: 1/29/91 Time: 9:54

Lab F i l e ID: F3694 Init. Calib. Oate(s): 1/25/91 1/25/91

Matrix:(soi1/water) WATER Level :(1ow/med): LOW Column:(pack/cap) CAP

Min RRF50 for SPCC(*) - .300 (0.250 for Bromoform) Max %0 for CCC(») - 25.0%

COMPOUND

C h 1 o r ome thaneB r omomet han eV i n y l c h l o r i deChl oroethaneMethylene c h l o r i d eAcet oneCarbon di su 1 f i de1 ,1-Dichloroethene1 . 1-Di chloroethane1 , 2-Di chl or oethene (totalChl orofo rm1 ,2-Dichloroethane2-8utanone1 ,1 , 1-TrichloroethaneCarbon te t r ac hi o r i deV i n y l acetateB r omod i ch 1 o romet hane1 ,2-Dichloroprooanec i s - 1 , 3 -Di c hi o r opr opene __Tri chl oroet h-eneDi bromochl o romet hane1 ,1.2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneB romof orm4 -Methyl -2- pen tanone2-HexanoneTetrac hi or oethene1,1,2,2-TetrachloroethaneTo! uen eChl o robenz eneEthylbenzeneS ty r eneXyl ene (total)

To! uene-d8Bromof luorobenzene1 , 2-Di chl oroethane-d4

11

*1

1111**

*i11111*

~l1t1

*111

_****11

1111

RRF

. 6091 . 101. 803.582

1 . 341. 223

2. 7991 .0741 . 6211 .3082.5041 . 463. 024. 466. 443. 310. 591. 302. 438. 423. 630. 338. 717. 385. 495.327. 227.471. 752. 662.953. 414. 894. 488

1 .049. 572

1 . 304

RRF50

.6891 .144.988.678

1 .609.227

3.0941 .1641 .7611 .3812.6331 .4750_T].436.403.240.559.302.429.409.578.317.701.361.441.301.213.452.679.627.896.399.834.460

1 . 100.587

| 1.391

1%D |

113.1*3.8 |

23. 1 •16.4 |20.0 |1.8 |

10.5 |8.4 »8.6 *5.6 |5.2 ».8 |

5.8 |6.5 |3.1 |

22.6 |5.5 |. 1 •

2.2 |3.1 |8.2 |6.2 |2.3 |6.2 |

10.9 *8.0 |6.0 |3.9 |9.8 *5.3 »6. 1 *3.7 *6.8 I5 •#Dl'.,,,J4ty4.9 |2.6 |6.7 |

1

FORM VI I VOA 1787 Rev

IA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________

I| VBLKW1





Level: (low/med) LOW Date Received: O/ O/ 0




74-87-3----

75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----

3 H \J J J W

67-66-3----107-06-2----

71-55-6----56-23-5----108-05-4----75-27-4----78-87-5----

10061-01-5----/ j U 1 O

124-48-1----79-00-5----71-43-2----

10061-02-6----75-25-2----

108-10-1----

127-18-4----79-34-5----l U o o o *I U O j U /100-41-4----100-42-5----

1330-20-7----

---Chl oromethane- --8r omome thane---Vinyl chloride---Chl oroethane---Methylene chloride---Acetone---Carbon disulfide---1 , 1-Dichloroethene---1 , 1-Dichloroethane--- 1 , 2-Di chl or oethene (total) __---Chloroform---1 ,2-Dichloroethane---2 -8u tanone---1 , 1 , 1 -Tri chl oroethane---Carbon tet rachl or i de---Vinyl acetate---Bromodi chl or ome thane•---1 , 2-Di chl oropropane• ---ci s-1 , 3 -Di chl or op r opene ___ _•---Trichloroethene•---Di br omochl o romet hane•---1 , 1 , 2-Tri chl oroethane• ---B«nzene- --t r ans- 1 , 3-Di chl or opr opene __

• - - -B r omof orm•---4-Methyl -2-pentanone•---2-Hexanone•---Tetrachloroethene•---1,1,2,2-Tetrachloroethane __• - --To 1 uene•---Chl orobenzene•---Ethylbenzene•---St y rene•---Xylene (total)

10.10.10.10.. .8.

10-T-5.5.5 .5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.

iftR5.5.5.

UUUuuuuuuuuuuuuuuuuuuuuuuuu

$25uuu

1

35228


TENTATIVELY IDENTIFIED COMPOUNDS I| VBLKW1

Lab Name: NET Contract: 68D90031 |_________








CAS NUMBER

1 . - -2.3.4.5.6.7.8.9.10.11 .12.13.14.15.16.17.18.19 .20.21.22.23.24.25 .26.27.28.29.30.

COMPOUND NAME

UNKNOWN

RT

22.83

EST. CONC.———————————

7.

flH3iJ/__«

Q

J

——

jrc ——in!

___ J


I* EPA SAMPLE NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET ______________

II V B L K S 1

Lab Name: NET C o n t r a c t : 68D90031 I___________








74-87-3----74-83-9----75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----

75-34-3----540-59-0----67-66-3----

107-06-2----/ O J -J J

71-55-6----5f 1 *} S6-23-5----108-05-4----75-27-4----/ O O / 3

10061-01-5----79-01-6 —— -

124-48-1----79-00-5----71-43-2----

10061-02-6----~T f? 1C •*}75-25- 2- ---U o —I U l

O3 I — / e — o127-18-4----79-34-5----

i U O J w /

100-41-4----100-42-5----

1330-20-7----

• ---Chl oromethane- - - - B r omome thane•---Vinyl chloride•---Chl oroethane• ---Me thy I ene chloride•---Acetone•---Carbon disulfide•---I , l-Dichloroethene•---I , l - D i c h l o r o e t h a n e•--- I , 2 -Di c hi oroethene (total) __•---Chloroform•---I , 2-Dichloroethane•---2-Butanone•---I , I , l - T r i c h l oroethane•---Carbon te t r achl or i de• ---Vi nyl acetate• ---8 r omodi chl o romet hane•---I , 2-Dichloropropane• -- -c i s - I , 3 -Di c h I or op ropen e ______•---Trichloroethene• - --Di bromochl o romet hane•---I , I ,2-Trichl oroethane• ---Benzene• - -- 1 r ans- I , 3-Di c hi or opr opene __• - --Br omof o rm•---4-Methyl -2-pentanone• ---2 - Hexanone•---Tetrachl oroethene•---1,1,2,2-Tetrachloroethane __• - - -To 1 uene• ---Ch 1 or obenzene•---Ethyl benz ene•---Styrene•---Xylene (total)

10.10.10.10.2.

31 .5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.1 .

10.5.5.

• 5.5.5.

1|U|UI'J|U1 J1|U|U|U|U|U|U|U|UIUIUIUIU|U|U|U|U|U|U|U1 J|U|U|U^Ift^R^Jjydu^|UIU|U1 1

245


TENTATIVELY IDENTIFIED COMPOUNDS || VBL K S 1

Lab Name: NET Contract: 68D90031 j______________






Column: (pack/cap) CAP D i l u t i o n Factor! 1.00

CONCENTRATION UNITS:Number TICs found: 0 (-g/L or ug/Kg) UG/KG

CAS NUMBER

1 .2.3 .4 .5 .6.7.8 .9 .10.1 1 .12 .13 .14 .15 .16.17.18.19 .20.21 .22 .23 .24.25 .26.27.28 .29 .30.

COMPOUND NAME

*

RT EST. CONC.

ARSONS

Q

Q Q3Q

246FORM I VOA-TIC 1/87 Rev.

2CWATER SEMIVOLATILE SURROGATE RECOVERY

Lab Name: NET C o n t r a c t : 68D90031


123456789101 112131415161718192021222324252627282930

EPASAMPLE NO.

SBLKW1CCB12CCB13CAU93CAU93MSCAU93MSDCAU94CAU96CAU99

SI(NBZ)*

9392

1019510285953491

S2(FBP)*

898680868875917982

S3(TPH)*

917679

109941009396102

S4(PHL)*

86718397 «

— T9~139089100 *

S5(2FP)*

756479907979798197

S6(TBP)*_ _ _ _ _ _1211051 1 11211151231231 171 18

OTHER TOTOUT

000100001

QC LIMITSSI (NBZ) - Nitrobenzene-d5 (35-114)S2 (FBP) - 2-Fluorobiphenyl (43-116)S3 (TPH) - Terphenyl-d!4 (33-141)S4 (PHL) - Phenol-d6 (10- 94)S5 (2FP) =• 2-Fluorophenol (21-100)S6 (TBP) - 2,4,6-Tribromophenol (10-123)

* Column to be used to flag recovery values

» Values outside of contract required QC l i m i t s

D Surrogates d i l u t e d out c i «J

page 1 of 1

3CWATER SEMIVOLATILE MATRIX S P I K E / M A T R I X S P I K E DUPLICATE RECOVERY



M a t r i x S p i k e - EPA Sample No.: CAU93

COMPOUND

Phenol2-Chl or opheno 11 , 4 - Di chl o r obenzene ___N-Ni troso-di-n-prop.(l)1 ,2 ,4-Trichlorobenzen e_4-Chloro-3-methylphenolAcenaphthene4-Ni t rop henol2,4-Dinitrotol uene _____Pentachl oroohenolPy r ene

SP IKEADDED(UG/L )

200.200.100.100.100.200.100.200.100.200.100.

SAMPLECONCENTRATION

(UG/L )

0.0.0.0.0.0.0.0.0.0.0.

'

MSCONCENTRATION

(UG/L )-------------

163.157.79.94.91 .177.84.146.79.

190.83.

MS\

REC *

8279799491888473799583

QCL I M I T SREC.

12- 8927-1 2336- 9741-11639- 9823- 9746-1 1810- 8024- 969-10326-121

COMPOUND

Phenol2-Chl orophenol1 , 4 - Di chl orobenzene ___N-Ni troso-di -n-prop. (1)1,2,4-Trichl orobenzene__4-Chl oro-3 -me thy! phenolAcenaphthene4-N i t r ophenol2,4-Dini trotol uene ____Pentachl orophenolPy r ene

SPIKEADDED(UG/L )

---------200.200.100.100.100.200.100.200.100.200.100.

MSDCONCENTRATION

(UG/L )-------------

124.162.61 .88.68.

147.70.

178.77.

196.86.

MSD%REC *

------62816188687470 ,

, 89 *• -7-?- '9886

%RPD *

273

26. T--H

' 29 »~TT~"

k 1820233

QC LRPD

424028

- 3828423150385031

[HITSREC .

12- 8927-1 2336- 974 1 - 1 1 639- 9823- 9746-1 1810- 8024- 969-103

26-1 27I(1) N-Nitroso-di-n-propy1 amine

* Column to be used to flag recovery and RPO values with an asterisk

* Values outside of QC l i m i t s AR3G260Q

RPO: 1 out of 11 outside l i m i t sSpike Recovery: 1 out of 22 outside l i m i t s

COMMENTS:

3DSOIL S E M I V O L A T I L E MATRIX SPIKE/MATRIX S P I K E DUPLICATE RECOVERY

Lab Name: NET Contract:68D90031


M a t r i x S p i k e - EPA Sample No.: CAU97 Leve 1 :(1ow/med) LOW

COMPOUND

Phenol2-Chl orophenol1 , 4-Di chl orobenzeneN-Nitroso-di-n-prop.(l)1 ,2,4-Trichlorobenzene_4-Ch1oro-3-methylphenolAcenaphthene4-Ni t r ophenol2,4-Dinitrotol uene ____Pen tachl or ophenol _______Pyrene

SPIKEADDED(UG/KG)

20994.20994.10497.10497.10497.20994.10497.20994.10497.20994.10497.

SAMPLECONCENTRATION

(UG/KG)

0.0.0.0.0.0.0.0.0.0.

1416.

MSCONCENTRATION

(UG/KG)

20003.19060.7967.9999.8806.20226.8245 .22863.9162.22167.9087.

MS

REC *--------

95 »9176958496791098710673

QCLIMITSREC.------26- 9025-10228-10441-12638-10726-10331-1 371 1 - 1 1 428- 8917-10935-142

COMPOUND——— .....-....„-.--*.>--Phenol2-Chl orophenol1 , 4 - Di ch 1 orobenzene _____N-Nitroso-di-n-prop.(l)1 ,2,4-Trichlo robenzene_4 -Chl oro -3 -me thy! phenolAcenaphthene4 -N i trophenol2,4-Dinitrotol uen« ____Pen tachl or ophenol ____Pyrene

SPI K EADDED(UG/KG)

20994.20994.10497.10497.10497.20994.10497.20994.10497.20994.10497.

MSDCONCENTRATION

(UG/KG)

15977.14809.6333.8763 .7338.

13416.771 1 .

21221.9248.19623.8683.

MSD%REC *

76716083708873

101889369

%RPD *

22252313189771

125 •

QC LRPD

3550273823331950474736

[HITSREC .

26- 9025-10228-10441-12638-10726-10331-1371 1 - 1 1 428- 8917-10935-142

(1) N- N i t r o s o - d i - n - p r o p y 1 amine

* Column to be used to fla g recovery and RPD values with an asterisk

(Values outside of QC l i m i t s AR3Q26Q1

RPD: 0 out of 11 outside l i m i t sSpike Recovery: 1 out of 22 outside l i m i t s 276

COMMENTS:

FORM II I SV-2 I/87 R

78SEMIVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: NET Contract:68D90031

Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93*

Instrument ID: DARYD C a l i b r a t i o n Date: 2/ 8/91 Time: 8:27

Lab F i l e ID: D8568 I n i t . C a l i b . Date(s): 2/ 7/91 2/ 7/91

Min RRF50 for SPCC(*) • .050 Max %D for CCC(*) - 25.0%

COMPOUND | RRF

Phenol_______________________« 1.452bis(2-Chloroethyl)ether ___| 1.1712-Chl orophenol_____________| 1.3071 , 3-Dichlorobenzene ______| 1.6381,4-Dichlorobenzene ______* 1.640Benzyl alcohol_____________| .7571 ,2-Dichlorobenzene _______| 1.5332-Methyl phenol_____________| 1.116bi s(2-chloroi sopropyl)ether| 2.0214-Methyl phenol_____________| 1.072N-Ni troso-di-n-propylami ne_* .943Hexachl or oe thane__________| .687Nitrobenzene _ _ _ _ _ _ _ _ ____. . I .538

RRF50 | %0

1.461 .6 *1 . 149 1.9 |1 .251 4.3 |1.506 8.0 |1.567 4.5 *.727 3.9 |

1.456 .5.0|1.061 5.0 |1.949 3.6 |1.021 4.8 |.923 2.2 *.642 6.5 |.557 3.6 |.781 5.2 ||Isophorone_________________| .823

j 2 - N i t r o p h e n o l _____________* .235| .230| 2.3| 2 , 4-Di me thy! phenol_________| .385) .381) .9| B « n z o i c aci d________________ | .238J .227| 4.8|bis(2-Chloroethoxy )me t hane__| .474| 2 , 4-Di chl or ophenol_________* .364| 1 , 2 , 4-Tr i chl or obenzene_____| .448(Naphthalene _______________| 1.069|4-Chloroani1ine __________| .266| Hexachlorobutadiene _______* .296| 4-Chloro-3-methy1 phenol ___* .324|2-Methylnaphtha!ene _______| .895| H e x a c h 1orocyclopentadi ene _* .463| 2,4,S-Trichlorophenol ____* .492| 2 , 4,5-Trichl orophenol ____| .529j2-Chloronaphthalene ________\ 1.070| 2-Ni troani 1 ine____________| .426| Dimethyl phthal ate __________\ 1.423| Acenaphthyl ene_____________| 1.491| 2 , 6-Di ni trotol uene_________| .400| 3-Ni troani 1 i ne______________\ .233| Acenaphthene________________* 1.205|2,4-Dinitrophenol ________# .210|4-Nitrophenol _____________* .181

.457 3.5

.345 5.4

.410 8.41 .054 1 .4.315 18.2.282 4.5.324 .1.873 2.5.463 .1.502 2.1.539 1.9

1.088 1 .7.471 10.4

1.405 1.31.947 30,6..381 4.6.137 "41.2

1.204 .1 *.197 6.5 *.173 4.8 *—— —W302602

FORM VII SV-1 1/87 Rev.

7CS E M I V O L A T I L E CONTINUING CALIBRATION CHECK

Name: NET Contract: 68090031


Instrument ID: DARYD C a l i b r a t i o n Date: 2/ 8/91 Time: 8:27

Lab F i l e ID: D8568 I n i t . C a l i b . Date(s): 2/ 7/91 2/ 7/91

Min RRF50 for SPCC(*) - .050 Max %0 for CCC(«) - 25.0%

(1) Cannot be separated from Diphenylamine

COMPOUND

Dibenzofuran2.4-DinitrotolueneDi ethyl p h t h a l ate4-Chl orophenyl -phenyl ether_Fluorene4-Ni troani 1 ine4 , 6-Di ni tro-2-methyl phenol _N -N i t r osodi phen y 1 ami n e (1) _4 -B r omophen y 1 -pheny 1 e t her _Hexachl orobenzenePentachl orophenol ^Phenan threneAnthraceneDi - n - b u t y l p h t h a l ateF 1 uoran thenePyreneB u t y l b e n z y l p h t h a l a t e3 .3'-DichlorobenzidineBenzo(a)anthraceneC hr y senebis(2- Ethyl hexyl)phthal at e_Di -n-octylphthalateBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(a)pyr ene *Indeno(l,2, 3-cd)pyr ene ______Di ben z.( a. h) anthraceneBenzo(q.h.i )perylene

Ni trobenzene-d52-Fluorobip heny 1Terpheny 1 -d 1 4P henol -d62 - Fl uo r ophenol2 . 4,6-Tribromophenol

RRF

1 .720.564.899. 686

1 .375. 192. 169

* .451. 266.386

» .2511.1161 .0581 . 440

» 1 .3241.411. 694. 224

1 .3701 . 266.978

• 1.6511.5101 . 031

> 1 . 1761 .055.947.897

. 4141 .2611 . 0841 .3551.135.374

1RRF50 |--- —— (•1.611|.522|.818|.642 |

1 .329). 184 |. 1 67 |.428 |.252).376).243|

1 .062 |1 .049|1 .333 |1.213|1 .380 |.633|. 180 |

1.32311 . 196|.909|

1 .392|1.252|.948 |

1 .094|,957|.923|.950 |

.425 |1 .305 |1 .039 |1 .344 |1.110|.3721

1

%D

6.37.59.06.43.34. 11 .45. 1 •5.52.53.5 *4.9 |.9

7.58.4 *2.28.8

19.63.45.57.015.7 *17.18.17.0 *9.32.5 .6.0

2.73.54. 1.8

2.2.5

HR302603

544FORM VII SV-2 1/87 Rev.

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

I| SBLKW1










i u Q y 3 £H 1-44-4----

541-73-1----106-46-7----100-51-6----95-50-1 ----95-48-7----108-60-1----106-44-5----621-64-7----67-72-1----o ~y? 3

O O / 3 3

105-67-9----65-85-0----

1 1 1-91-1----120-83-2----120-82-1----91-20-3----106-47-8----O / D O J

59-50-7----91-57-6----77-47-4----< J O U O t

95-95-4----91 K Q _ *7 _ .

88-74-4----131-1 1-3----_ C U O ; J O o

606-20-2----

- --Phenol•---bi s(2-Chloroethyl )ether ___-- -2-Chl or ophenol

•---1 ,3-Dichlorobenzene•---1 , 4-Di chl orobenzene•---Benzyl alcohol---1 ,2-Dichlorobenzene•---2-Methylphenol---bi s(2-chloroi sopropyl)ether---4-Methylphenol---N-Ni troso-di -n-propyl ami ne __•---Hexachl oroethane---Ni trobenzene• - - - I sophor one•---2-Ni trophenol•---2,4-Dimethyl phenol- - -Benzoi c acid•---bi s( 2-Chl o roe thoxy )me t hane __---2,4-Diehlorophenol

•---1 ,2,4-Trichl orobenzene•---Naphtha! ene.---4-Chl oroani 1 ine•---Hexachl orobutadi ene•- --4-Chl or o-3-met hyl pheno 1 ____---2-Methylnaphthalene

• - - -He xac hi oroc y c ! open t ad i ene __---2, 4 , 6-Tri chl orophenol•---2,4,5-Trichloropheno!---2-Chl oronaphthal ene•---2-Nitroani line- --Di me thy Iphthalate•---Acenaphthylene•---2. 6-Dini trotoluene

10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.10.50.10.10.10.

1|U|UIU|UIUIUIUIU|UIU|U|UI«JIUJU|U|U|U|UIU|UIU|UIUIU|U|U

AFJJ026IUIUIU1

*

m ii 5581

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE N0-I ——'——

ab Nam«: NET Contract: 68D90031 | S8LKW1


M a t r i x : (soil/water) WATER Lab Sflmp1e j - .

Sample wt/vol: 1000.0 (g/mL) ML Lab F,-, e IQ. D8558

Level: (low/med) LOW Datft Rccttiv<>d. 0/ Q/ Q



GPC Cleanup: (Y/N) N pH: .0 Dilution Factor: 1.00

fAf un CONCENTRATION UNITS:CAS N0- COMPOUND (ug/L or ug/Kg) UG/L Q

83-32-9----51-28-5----100-02-7----132-64-9----121-14-2----84-66-2----

7005-72-3----86-73-7----100-01-6----S'34-52-1 ---•J v —r -J £. i

86-30-6----101-55-3----1 18-74-1 ----O / O O v

O 9 U 1 - o - —120-12-7----84-74-2----

4 U O ** H U

129-00-0----

91-94-1----56-55-3----

_ l O w 1 j

117-81-7----117-84-0----205-99-2----4 U / U O 3

50-32-8----193-39-5----53-70-3----191-24-2----

•---3-Ni troani 1 ine----Acenaphthene•---2,4-Dinitrophenol•---4-Ni trophenol•---Di benzofuran•---2,4-Dini trotoluene•---Di ethylphthalate•---4-Chlorophenyl -phenyle ther _•---Fl uorene•---4-Ni troaniline•---4, 6-Dini tro-2-methyl phenol __•-- -N -N i t ro sodi phenyl ami ne (1) __• -- -4- Br omopheny 1 -pheny 1 e t he r __•---Hexachl orobenzene•---Pentachlorophenol•---Phenanthrene• - - -An thr acene•---Di -n-butyl phthal ate•---Fluoranthene• ---Py r ene•---Butylbenzylphthal ate•---3,3'-Dichlorobenzidine•---Benzo(a)anthracene• - --Ch r y sene•---bis(2-Ethylhexyl)phthalat e __•---Di -n-octylphthalate•---8enzo(b)fl uoranthene----8enzo(k )fluoranthene•---Benzo(a)pyrene-~--Indeno(l,2.3-cd)pyrene•---Di benz (a . h) anthracene----8enzo(g.h.i )perylene

50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10.10.20.10.10.

10.10.10.10.10.

!Sfl

i uuuuuuuuuuuuuuuuuuuuuuuuJ

uuuu

*$G261

>559

(1) - Cannot be separated from di p h e n y l a m i n e

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

b Name: NET Contract: 68D90031


M a t r i x S p i k e - EPA Sample No.: CAU93

COMPOUND

GAMMA-BHCHEPTACHLORALORINDIELDRINENORIN4.4 '-DOT

S P I K EADDED(UG/L )

. 20

.20

.20

.50

.50

.50

SAMPLECONCENTRATION

(UG/L )

.00

. 00

.00

.00

.00

.00

MSCONCENTRATION

(UG/L )

. 10

.09

. 10

.27

.28

.30

MS%

REC *

v. 51 •'T3-52545760

QC |L IMITS!REC. |—— ...|56-1 23)40-131 |40-120)52-126)56-121 |38-127)

1

COMPOUND

GAMMA-BHCHEPTACHLORALDRINDIELDRINENDRIN4.4 '-DOT

SPIKEADDED(UG/L )

.20

.20

.20

.50

.50

.50

MSDCONCENTRATION

(UG/L )

. 14

. 1 1

. 14

. 36

.37

.46

MSD%

REC *

685768717492

%RPD *

29 •29 »28 *28 •27 *43 »

QC LRPD

152022132127

IMITSREC.

56-1 2340-13140-1 2052-1 2656-12138-127

* Column to be used to flag recovery and RPO values with an asterisk

* Values outside of QC l i m i t s

RPD: 6 out of 6 outside l i m i t sSpike Recovery: 1 out of 12 outside l i m i t s

COMMENTS:

HR302&II 6FORM III PEST-1 1/87 Rev.

8DPESTICIDE EVALUATION STANDARDS SUMMARY



Instrument ID: SYA1 GC Column ID: DB-608

Dates of Analyses: 2/20/91 to 2/21/91

E v a l u a t i o n Cheek for L i n e a r i t y

PESTICIDE

ALDRINENDRIN4.4'-DDTDBC

| CALIBRATION| FACTOR| EVAL MIX A

| 4066134.| 2171500.| 2645825.| 2602540.1

CALIBRATIONFACTOR

EVAL MIX B

4031834.2649667.2837950.2532530.

CALI BRATIONFACTOR

EVAL MIX C

4368400.2954067.3137994.2546010.

| %RSD

| 10.0%)|. .....1 4^I -'Ts . 2 .1 i.'s1

(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.

E v a l u a t i o n Check for 4,4'-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)

11(.. ..........| INITIAL

1 | EVAL MIX B2| EVAL MIX B3| EVAL MIX B415161718191

10111 11 211 3 1141

1

DATEANALYZED

2/20/912/20/912/21/91

. . .'

TIMEANALYZED

1 1 :2323:438:26

, ,

ENDRIN

8.49100.0012.84

?•

4,4 '-DOT

.00

.0014.81

COMBINED(2) |

--"--"I1

3.687.90 |13.87 |

(1)

(2) See Form instructions AR3026I2683

FORM VII I PEST-l 1/87 Rev,

80PESTICIDE EVALUATION STANDARDS SUMMARY

ab Name: NET Contract: 68D90031


Instrument ID: SYA1 GC Column ID: 08-608

Dates of Ana l y s e s : 2/20/91 to 2/21/91

Evaluation Check for L i n e a r i t y

PESTICIDE

A L D R I NENDRIN4 ,4 '-DOT ____DBC

CALIBRATIONFACTOR

EVAL MIX A

4066134.2171500.2645825 .2602540.

CAL IBRATIONFACTOR

EVAL MIX B————————————

4031834.2649667.2837950.2532530.

CAL IBRATIONFACTOR

EVAL MIX C

4368400.2954067.3137994.2546010.

%RSD

10.0%)

4-rS--UL_2-8.61 .5

(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.

Evaluation Check for 4,4 '-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)

1234567891011121314

INITIALEVAL MIX BEVAL MIX BEVAL MIX B

DATEANALYZED----------

2/20/912/20/912/21/91

•TIMEANALYZED

11 :2323:438:26

-

ENDRIN

8.49100.0012.84

4,4 '-DOT

.00

.0014.81

COMBINED(2)

3.687.90

13.87

(1)

(2) See Form instructions. Hn3026f3

685FORM V I I I PEST-l 1/87 Rev.

8EPESTICIDE EVALUATION STANDARDS SUMMARY

E v a l u a t i o n of Retention Time Shift for D i b u t y 1 c h l o r e n d a t e



Instrument ID: SYA2 GC Column ID: OB-5

Dates of Ana l y s e s : 2/20/91 to 2/21/91

1234561891011121314151 617181920212223242526272829303132333435363738

EPASAMPLE NO.

EVALAEVAL8EVALCINDAINDBTOXAPHAR1016AR1221AR1232AR1242AR1248AR1254AR1260ZZZZZZZZZZZZZZZZZZZZZZZZZE V A L B 0ZZZZZZZZZZZZZZZZZZZZPBLKS1INDA 01CAU97CAU97MSCAU97MSDCAU98EVALBINDA 02INDB 01

LAB SAMPLEID

DATEANALYZED

2/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/91

TIMEANALYZED

10:401 1 :2312:0712:5013:3414:1815:0115:4516:2817:1217:5518:3919:2220:0620:4921:3322:1623:0023:430:271:111 :542:383:214:054:485:326: 156:598:269:09

. 9:52

%D .

.0

. 1

. 1

.2

.2

.2

.2

. 1

. 1

. 1

. 1

. 1

.1

. I

. 1

. 1

.1

. 1

.2

. 1

. 1

. 1

. 1

. 1

.2

. 1

.1

. 1

.1

. 1

.0

. 1

•"-

1

* Values outside of QC l i m i t s (2.0% for packed col un&S,3 0 2 6 f 0.3% for c a p i l l a r y columns)

page 1 of 1FORM V I I I PEST-2 1/87 Rev,

8EPESTICIDE EVALUATION STANDARDS SUMMARY

E v a l u a t i o n of Retention Time Shift for D i b u t y 1 c h l o r e n d a t e

b Name: NET Contract: 68D90031


Instrument ID: SYA2 • GC Column ID: DB-5

Dates of A n a l y s e s : 2/20/91 to 2/21/91

12345678910111213141516171 81920212223242526272829303132333435363738

EPASAMPLE NO.

EVALAEVALBEVALCINDAINDBTOXAPHAR1016AR1 221AR1 232AR1242AR1248AR1254AR1260PBLKW1CC812CCB13CAU93CAU94EVALB 0CAU93MSCAU93MSDCAU96CAU99ZZZZZINDA 01HillZZZZZZZZZZZZZZZEVALB 0INDA 02INDB 01

LAB SAMPLEID

| DATE| ANALYZED|..- —— ——— -I 2/20/91

2/20/912/20/912/20/912/20/912/20/91

| 2/20/91| 2/20/91

2/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/91

TIMEANALYZED

10:401 1 :2312:0712:5013:3414:1815:0115:451 6 :-2 817:1217:5518:3919:2220:0620:4921 :3322: 1623:0023:430:271:111 :542:383:214:054:485:326: 156:598:269:099:52

%D -

.0

. 1

. 1

.2

.2

.2

.2

.1

. 1

. 1

. 1

. 1

.1

. 1

. 1

. 1

. 1

. 1

.2

. 1

. 1

. 1

.1

. 1

.2

.1

. 1

. 1

. 1

. 1

.0

. 1

•

* Values outside of QC l i m i t s (2.0% for packed c o 1 uftiDsO fl O £ I C0.3% for c a p i l l a r y columns) ' »fvOU_:OlO 683

>age 1 of 1FORM V I I I PEST-2 1/87 Rev.

9PESTICIDE/PCS STANDARDS SUMMARY

Lab Name: NET Contract: 68090031


Instrument ID: SYA2 GC Column ID: D8-5

COMPOUND

ALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHC ___HEPTACHLOR ___ALDRINH«pt . Epox i deENDOSULFAN I_DIELDRIN4.4'-DD£ENDRINENDOSULFAN II4,4'-OOD ____Endo . sulfate4.4 '-DOTMETHOXYCHLOR_ENDRIN KETONEa . Chl ordaneg . Chl ordaneTOXAPHENEAROCLOR-1016AROCLOR-1 221AROCLOR-1232AROCLOR-1242AROCLOR-1248AROCLOR-1 254AROCLOR-1260

DATE(S) OF FROM: 2/20/91A N A L Y S I S TO: 2/20/91TIME(S) OF FROM: 12:50ANALYSIS TO: 13:22

FRT WIls

FROM

9.85 9.7810.67 10.5911.57 11.4910.81 10.7313.04 12.9414.15 14.0515.55 15.4316.77 16.6517.69 17.5617.80 17.6718.41 18.2718.77 18.6319.27 19.1320.31 20.1520.60 20.4422.76 22.5921 .88 21 . 7116.37 16.2416.90 16.7821.77 21.6113.61 13.519.90 9.83

12.63 12.5412.63 12.5415.94 15.8218.03 17.8920.74 20.58

{TIDOW

TO

9.9310.751 1 .6610.8913.1414.2615.6616.9017.8217.9418.5518.9119.4220.4620.7522.9322.0416.4917.0321 .9313.719.9712.7212.7216.0618. 1720.90

1

CALIBRATIONFACTOR

2607700.1613675.2192075.2440650.2629150.2792550.2828450.2466725.2386775.2231950.1969000.2494650.2048775.2624400.1564700.881155 .3097300.2860225.2871750.

61756.187812.74043.80043.165279.293013.202870.240293 .

DATE OF ANALYSIS 2/21/91TIME OF ANALYSIS 9 :09EPA SAMPLE NO.(STANDARD) INDA 02

RT

10.8113.0514. 1715.5616.7917.71

18.80

I20.6322.79

1

CALIBRATIONFACTOR

2383500.2555950.2552700.2785200.2410275 .2311625.

2443300.

1285250.777785 .

1

1QNTY/N

yY\e

y

Y

YYYw

YYYvYYYYYYYYYYYY

%0

2.32.89.61 .52.33. l'

=al- —— 4

\ \1

1

Under QNT Y/N: enter Y if quantitation was performed, N if not performed.%D must be less than or equal to 15.0% for quantitation, and less thanor equal to 20.0% for confirmation.

Note: Determining that no compounds were found above the CRQL is a form ofquantitation, and therefore at least one column must meet the 15.0% c r i t e r i a

For mu1ticomponent analytes, the largest single peak that is characteristicof the component should be used to establish retention time aflf?^?19K j f\Identification of such analytes is based p r i m a r i l y on pattern recognition.

page 2 of 3FORM IX PEST 1/87 Rev

9PESTICIDE/PCS STANDARDS SUMMARY

Name: NET Contract: 68D90031

ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93

nstrument ID: SYA2 GC Column ID: D8-5

COMPOUND

ALPHA-BHCBETA-8HCDELTA-BHCGAMMA-BHC ___HEPTACHLOR ___| ALDRIN| Hep t . Epoxi deIENOOSULFAN I_| DIELDRIN»4'-DDE

DRINDOSULFAN II

4T4'-DDOEndo. sulfate4.4 '-DOTMETHOXYCHLOR_ENDRIN KETONEa. Chlordaneg. ChlordaneTOXAPHENEAROCLOR-1016_AROCLOR-1 221AROCLOR-t 232AROCLOR-1 242AROCLOR-l 248AROCLOR-1 254| AROCLOR-1 260

DATE(S) OF FROM: 2/20/91A N A L Y S I S TO: 2/20/91TIME(S) OF FROM: 12:50ANALYSIS TO: 19:22

fRT Wlf

FROM

9 .8510.671 1 .5710.8113 .0414.1515.5516.7717.6917.8018.4118.7719 .2720.3120.6022.7621 .8816.3716.9021 .7713.619.90

12.6312.6315.9418.0320.74

9.7810.591 1 .4910. 7312.9414.0515.4316. 6517.5617.6718. 2718 . 6319.1320. 1520. 4422.5921 .7116. 2416.7821 .6113.519.83

12.5412.5415.8217.8920.58

RTJDOW

TO

9.9310.751 1 .6610.8913.1414.2615.6616.9017.821 7.9418.5518.9119.4220. 4620.7522.9322.04.16.4917.0321 .9313.719.97

12.7212.7216.0618.1720.90

1

CALIBRATIONFACTOR

-----------2607700.1613675.2192075.2440650.2629150.2846150.2828450.2466725.2386775.2231950.1969000.2494650.2048775 .2624400.1564700.881 155 .3097300.2860225 .2871750.

61756.187812.74043.80043 .165279.293013.202870.240293.

DATE OF A N A L Y S I S 2/21/91TIME OF ANALYSIS 9:09EPA SAMPLE NO.(STANDARD) INDA 02

RT

10 .8113 .0514.1715 .5616.7917,71

18 .80

20 .6322.79

CALIBRATION QNTFACTOR |Y/N

2383500.2555950.2552700.2785200.2410275.2311625.

2443300 .

1285250.777785.

YYYYYYYYYYYYYYYYYYYYYYYYYYY

%0

2. 32.8

10.31 .52.33. 1

2 . 1

.- ——— 1LJ_?.9

11.7

—————

—————

Under QNT Y/N: enter Y if quantitation was performed, N if not performed.%D must be less than or equal to 15.0% for q u a n t i t a t i o n , and less thanor equal to 20.0% for confirmation.

Note: Determining that no compounds were found above the CRQL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.0% c r i t e r i a .

r mu 1 ticomponent analytes, the largest single peak that is characteristicthe component should be used to establish retention time an^f^>30 2 6 1.7t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognitno^jC

page 2 of 3FORM IX PEST 1/87 Rev.

Appendix ETelephone Log

8R3026I8

Lib

Contact:

Call WtUt«^ By: __

In rtf«rerKt to d*t» fcr th«

-9

(1) '.w Cooy, (,} ftt^

In Jtftfts'vm to

ContractRZGK UUVLA-50RATORY COWMVNICATKN SYSTEM

T«kphone R«cord

Date o. C*il: :f

Laboratory Na/n«: ____/I/? TLab Contact: __

f SContact: ^

Call Wtiat«

Oa:«AR302620

Oi.:.-.outicr>: (:; ',10 Copy, (2; R^jon Ccpy, ij) <MO C:cy

tfviiTW, ,

R_£.

NETSEMjY:.NET MJDWEST_______: 5-28-91 : 15:53 ; NETJ>_Jm£TT- 3014173

NiT MMw»«t Ine.MATIDWAI 8«ft'f<t otvl*toflINMI IWIN/AI. 850 WMt rt ,ENVIRONMENTAL *•«•«• «•601MTESTING, INC. w

F«x: (708) 289-5445

FAX TRANSMISSION NOTICE

To: 77*",? -7~/»p £6**? ______________Company: ________________ PAX NO: /- / ' VX ?• ' 2 */ f>

Sender: fflt /&**?. A/T faictr.** f 22+ < _________" " ~~~ — "

You should receiv* panes / including thi* notic«. If youdon't receive all pages, please call the sender immediately.This transmission includes:

letter/memootherproject notes (Project ID: _________ _______ .)analytic*! report (s) t

Sanple No(s)i ________ _______ ________

CCS

f n 30262I J

15:54 :

IEV O L A T I L E ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

TI« : NET Contract: 68D90031

ode: NET Case No.: 15741 SAS No.: $DG Ne.: CAU93

ix: (soil/water) WATER Lab Sample ID:

i p l e wt/vol: 5.0 (g/mL) ML L»b F i l e ID: F3699

•vel: (1ow/m«d) LOW Date R e c e i v e d : 1/24/91

'•, Moisture: not dec. 100. Date Analysed: 1/29/91

Column: (pack/cap) CAP D i l u t i o n Factor: 1,00

CONCENTRATION UNITS:Number TICt found: 1 (ug/L or -jg/Kg) UG/L

CAS NUMBER

1 . 75-13-12.3.4.5.6.7.8.9 .10.11 .12.13.14.IS.16.17.18.19.20.21 .

. 22.23 .24.25.2G.27.29.23.30.

COMPOUND NAME

Ethane, !,l,2-trieh1oro-l,2,

-... , ,.., ... ...

RT

4.31

»

FST. CONC.

40.

*

JH3Q2&;

iQj

l

— ii

1,-, 17 2 |(e

FORM I VOA-TIC 1/87

ab302502 - records collections · mcdp 87, and # 15536 sdgs mcdp 80 and ccboo. the validation for...

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