1. Soil pH and SMP Buffer pH methodologies Time for SMP buffer to set in soil-water slurry

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Soil pH and buffer pH methodology: water and SMP/Sikora buffer reaction time with soil and a laboratory survey. 1. Soil pH and SMP Buffer pH methodologies Time for SMP buffer to set in soil-water slurry b. Conditions on LabFit for soil pH and Sikora buffer pH - PowerPoint PPT Presentation

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1. Soil pH and SMP Buffer pH methodologiesTime for SMP buffer to set in soil-water slurryb. Conditions on LabFit for soil pH and Sikora buffer pH2. Laboratory survey on pH and lime recommendationsprepared for SERA-6 conferenceJune 4-5, 2007F.J. SikoraUniversity of KentuckySoil pH and buffer pH methodology:water and SMP/Sikora buffer reaction timewith soil and a laboratory surveyVariations in methods for determining 1:1 soil:water pH Reference pubQuantity of soilStirring (or mixing) time after adding waterStanding time before determining pHStirring during/before pH measurementSPAC, Inc.4.25 cm3, 5 g, or 10 cm3Stir for 5 sec10 minstir during pH measurementSouthern10 cm3Mix for 5 sec30 minstir soil suspension by swirling the cup slightly just prior to reading pHNortheasternScoop 5 cm3 or weigh 5 gStir vigorously for 15 sec30 minplace electrodes in the slurry, swirl carefully and read pH immediatelyNorth Central4.25 cm3(5 g scoop)Stir vigorously for 5 sec10 minplace electrodes in the slurry, swirl carefully and read pH immediatelyWestern5 0.1 gStir thoroughly for 5 sec15 minplace electrodes in the slurry, swirl carefully and read pH immediatelyVariations in SMP methods for determining buffer pHReference pubQuantity of soilVolume of buffer added to soil pH slurry and shaking timeOscillations/minStanding time before determining pHSPAC, Inc.4.25 cm3 or 5 g10 mL buffer, shake for 10 min (or 15 min)>18030 min (or 15 min)SouthernNortheasternScoop 5 cm3 or weigh 5 g10 mL buffer, shake for 10 min (or 15 min)25030 min (or 15 min)North Central4.25 cm3(5 g scoop)10 mL buffer, shake for 10 min (or 15 min)25030 min (or 15 min)Western5 0.1 g10 mL buffer, stir every 5 minutes for 20 min20 minMclean, Eckert, Reddy, and Trierweiler. 1978. An improved SMP soil lime requirement method incorporating double-buffer and quick-test features. SSSAJ 42:311-316. excerpt from1975 North Central publicationon soil test methods.Table in the current North Central region publication on soil test methods.SMP Buffer pH 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2 s- 3 s+ 3 s+ 2 sSMP buffermeanSikora bufferDays after Jan 1, 2005Buffer pHLexington Quality Control Sample 41082110Date_OutIDPH_DBU_D01/04/054.0021105.266.2901/04/054.0021105.246.2501/07/057.0021105.266.2601/07/057.0021105.196.2801/11/0511.0021105.156.2601/11/0511.0021105.046.2801/14/0514.0021105.156.1701/14/0514.0021105.126.2501/21/0521.0021105.256.3201/25/0525.0021105.076.2201/25/0525.0021104.996.301/25/0525.0021105.156.2701/28/0528.0021105.126.3202/01/0532.0021105.126.2502/03/0534.0021105.046.2802/03/0534.0021105.26.302/04/0535.0021105.116.2902/08/0539.0021105.126.2802/10/0541.0021105.096.3702/10/0541.0021105.096.2902/11/0542.0021105.156.302/11/0542.0021105.126.3302/15/0546.0021105.156.302/15/0546.0021105.136.2602/16/0547.0021105.26.2702/17/0548.0021105.26.2602/17/0548.0021105.116.2402/18/0549.0021105.156.3302/18/0549.0021105.166.2402/22/0553.0021105.056.2802/22/0553.0021105.066.3602/23/0554.0021105.136.2802/24/0555.0021105.16.1702/24/0555.0021105.246.3402/25/0556.0021105.076.2402/25/0556.0021105.196.2702/25/0556.0021105.36.3803/01/0560.0021105.166.3203/01/0560.0021105.266.2703/02/0561.0021105.136.3403/02/0561.0021105.176.2403/03/0562.0021105.046.2703/04/0563.0021105.096.3403/04/0563.0021105.086.2403/07/0566.0021105.16.2903/07/0566.0021105.076.2903/08/0567.0021105.136.2803/09/0568.0021105.176.303/09/0568.0021105.146.3703/09/0568.0021105.216.2603/09/0568.0021105.266.2203/09/0568.0021105.116.2803/10/0569.0021105.136.2403/10/0569.0021105.16.3303/10/0569.0021105.146.403/11/0570.0021105.36.403/11/0570.0021105.196.2203/11/0570.0021105.246.2703/14/0573.0021105.056.1903/14/0573.0021105.176.2703/15/0574.0021105.256.2603/15/0574.0021105.216.2703/15/0574.0021105.086.2703/17/0576.0021105.086.2803/17/0576.0021105.046.2603/17/0576.0021105.196.2703/18/0577.0021105.016.3203/18/0577.0021105.216.1703/21/0580.0021105.216.2103/21/0580.0021105.086.2503/21/0580.0021105.086.2403/21/0580.0021105.166.203/22/0581.0021105.116.2703/22/0581.0021105.326.4503/22/0581.0021105.126.2403/23/0582.0021105.016.2103/23/0582.0021105.146.2503/23/0582.0021105.26.2203/24/0583.0021105.176.2403/24/0583.0021105.596.2303/24/0583.0021106.787.0503/24/0583.0021105.176.2603/25/0584.0021105.126.2203/25/0584.0021105.286.2503/25/0584.0021105.236.2903/25/0584.0021105.216.1903/29/0588.0021105.366.2703/29/0588.0021105.146.2303/29/0588.0021105.096.2503/30/0589.0021105.046.2503/30/0589.0021105.056.1703/30/0589.0021105.026.2503/31/0590.0021105.086.2503/31/0590.0021105.126.2403/31/0590.0021105.016.2503/31/0590.0021105.046.2603/31/0590.0021105.026.2303/31/0590.0021105.036.1904/01/0591.0021105.046.204/01/0591.0021105.166.1904/05/0595.0021105.096.2704/05/0595.0021105.036.2104/06/0596.0021105.116.2404/06/0596.0021105.066.2504/07/0597.0021105.256.2104/07/0597.0021105.36.2704/07/0597.0021105.216.2504/08/0598.0021105.126.2804/08/0598.0021105.176.2604/08/0598.0021105.286.2504/08/0598.0021105.026.1804/11/05101.0021105.176.1804/11/05101.0021105.046.3304/11/05101.0021105.176.1304/11/05101.0021105.086.2304/12/05102.0021105.166.2804/12/05102.0021105.046.1904/12/05102.0021105.16.2404/12/05102.0021105.136.3804/14/05104.0021105.026.2604/14/05104.0021105.046.204/14/05104.0021105.086.304/14/05104.0021105.126.2404/15/05105.0021105.066.3204/18/05108.0021105.086.2404/18/05108.0021105.216.304/19/05109.0021105.126.3204/19/05109.0021105.076.2404/19/05109.0021105.16.304/19/05109.0021105.086.2204/20/05110.0021105.066.1804/20/05110.0021105.136.2504/20/05110.0021105.066.1904/20/05110.0021105.126.1504/21/05111.0021105.186.3304/21/05111.0021105.016.4904/21/05111.0021105.076.2504/22/05112.0021107.286.1404/22/05112.0021105.116.1304/25/05115.0021105.16.1604/25/05115.0021105.136.2604/26/05116.0021105.156.104/26/05116.0021105.056.1604/28/05118.0021105.226.1904/28/05118.0021105.076.304/28/05118.00211056.1304/29/05119.00211056.2404/29/05119.0021105.156.2404/29/05119.0021105.256.2104/29/05119.0021105.136.2404/29/05119.0021105.146.1905/02/05122.0021105.16.3405/02/05122.0021105.236.1805/05/05125.0021105.216.2905/05/05125.0021105.226.2905/05/05125.0021105.156.2205/05/05125.0021105.136.2405/10/05130.0021105.046.2105/10/05130.0021105.126.2505/10/05130.0021105.096.2505/10/05130.0021105.086.2405/11/05131.0021105.176.2605/12/05132.0021105.086.1805/16/05136.0021105.086.1605/16/05136.0021105.136.1905/16/05136.0021105.066.1905/18/05138.0021105.16.305/20/05140.0021105.026.1805/20/05140.0021105.126.305/20/05140.0021105.046.4105/24/05144.0021105.116.1805/25/05145.0021105.136.1905/25/05145.0021105.056.2505/26/05146.0021105.136.2605/26/05146.0021105.286.2705/27/05147.0021105.176.2505/27/05147.0021105.16.2105/27/05147.0021105.086.2406/03/05154.0021105.26.2306/03/05154.0021105.216.1906/07/05158.0021105.066.2406/09/05160.0021105.056.2906/09/05160.0021105.216.2806/09/05160.0021105.136.2606/13/05164.0021105.16.3206/13/05164.0021105.086.2606/13/05164.0021105.16.2706/14/05165.0021105.26.3206/15/05166.0021105.086.2606/16/05167.0021105.196.2406/20/05171.0021105.266.2706/21/05172.0021105.066.2206/21/05172.0021105.136.2306/23/05174.0021105.036.2106/23/05174.0021105.066.2306/23/05174.0021105.16.2906/23/05174.0021105.126.2406/24/05175.0021105.016.2406/29/05180.0021105.046.2506/29/05180.0021105.086.2607/05/05186.0021105.216.2307/05/05186.0021105.156.2307/08/05189.0021105.356.1607/08/05189.0021105.316.2507/08/05189.0021105.166.2507/08/05189.0021105.126.3707/13/05194.0021105.136.3607/13/05194.0021105.146.2907/15/05196.0021105.246.3807/15/05196.0021105.196.3207/15/05196.0021105.056.2607/19/05200.0021105.056.2307/19/05200.0021105.056.3207/19/05200.0021105.136.2907/21/05202.0021105.076.2507/27/05208.0021105.176.2507/27/05208.0021105.026.2508/03/05215.0021105.066.3208/03/05215.0021105.086.3208/05/05217.0021105.056.2308/09/05221.0021105.056.3408/09/05221.0021105.136.2708/09/05221.0021105.16.3308/11/05223.0021105.446.308/12/05224.0021105.086.308/12/05224.0021105.216.2308/16/05228.0021105.346.2608/19/05231.0021105.176.5408/23/05235.0021105.16.2708/30/05242.0021105.166.16211000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000daysbuPH4108avg=6.60777251182s=0.14839461296.62047904196.6012std=0.07419730653s=0.22259191940.07663721750.0723359962167275Date_OutIDPH_DBU_Davgavg-2*stdavg+2*stdavg-3*stdavg+3*std04-Jan-054.0041085.266.616.60777251186.45937789896.75616712486.38518059246.830364431307-Jan-057.0041085.336.496.60777251186.45937789896.75616712486.38518059246.830364431307-Jan-057.0041085.496.676.60777251186.45937789896.75616712486.38518059246.830364431311-Jan-0511.0041085.336.76.60777251186.45937789896.75616712486.38518059246.830364431311-Jan-0511.0041085.316.586.60777251186.45937789896.75616712486.38518059246.830364431314-Jan-0514.0041085.336.626.60777251186.45937789896.75616712486.38518059246.830364431321-Jan-0521.0041085.256.666.60777251186.45937789896.75616712486.38518059246.830364431325-Jan-0525.0041085.366.726.60777251186.45937789896.75616712486.38518059246.830364431325-Jan-0525.0041085.216.696.60777251186.45937789896.75616712486.38518059246.830364431325-Jan-0525.0041085.226.636.60777251186.45937789896.75616712486.38518059246.830364431328-Jan-0528.0041085.46.376.60777251186.45937789896.75616712486.38518059246.830364431301-Feb-0532.0041085.366.586.60777251186.45937789896.75616712486.38518059246.830364431303-Feb-0534.0041085.316.66.60777251186.45937789896.75616712486.38518059246.830364431309-Feb-0540.0041085.266.646.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-0541.0041085.36.666.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-0541.0041085.376.686.60777251186.45937789896.75616712486.38518059246.830364431311-Feb-0542.0041085.366.666.60777251186.45937789896.75616712486.38518059246.830364431315-Feb-0546.0041085.276.646.60777251186.45937789896.75616712486.38518059246.830364431315-Feb-0546.0041085.386.576.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-0547.0041085.496.76.60777251186.45937789896.75616712486.38518059246.830364431317-Feb-0548.0041086.156.636.60777251186.45937789896.75616712486.38518059246.830364431318-Feb-0549.0041085.346.666.60777251186.45937789896.75616712486.38518059246.830364431318-Feb-0549.0041085.176.646.60777251186.45937789896.75616712486.38518059246.830364431322-Feb-0553.0041085.446.66.60777251186.45937789896.75616712486.38518059246.830364431323-Feb-0554.0041085.346.716.60777251186.45937789896.75616712486.38518059246.830364431324-Feb-0555.0041085.466.726.60777251186.45937789896.75616712486.38518059246.830364431324-Feb-0555.0041085.386.746.60777251186.45937789896.75616712486.38518059246.830364431325-Feb-0556.0041085.376.676.60777251186.45937789896.75616712486.38518059246.830364431325-Feb-0556.0041085.416.756.60777251186.45937789896.75616712486.38518059246.830364431325-Feb-0556.0041085.26.666.60777251186.45937789896.75616712486.38518059246.830364431301-Mar-0560.0041085.346.76.60777251186.45937789896.75616712486.38518059246.830364431301-Mar-0560.0041085.346.696.60777251186.45937789896.75616712486.38518059246.830364431302-Mar-0561.0041085.426.676.60777251186.45937789896.75616712486.38518059246.830364431302-Mar-0561.0041085.426.676.60777251186.45937789896.75616712486.38518059246.830364431303-Mar-0562.0041085.386.686.60777251186.45937789896.75616712486.38518059246.830364431304-Mar-0563.0041085.346.666.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-0567.0041085.366.686.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-0567.0041085.266.546.60777251186.45937789896.75616712486.38518059246.830364431309-Mar-0568.0041085.496.496.60777251186.45937789896.75616712486.38518059246.830364431309-Mar-0568.0041085.386.876.60777251186.45937789896.75616712486.38518059246.830364431309-Mar-0568.0041085.416.716.60777251186.45937789896.75616712486.38518059246.830364431309-Mar-0568.0041085.276.426.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-0569.0041085.416.66.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-0569.0041085.276.676.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-0569.0041085.216.476.60777251186.45937789896.75616712486.38518059246.830364431311-Mar-0570.0041085.286.646.60777251186.45937789896.75616712486.38518059246.830364431311-Mar-0570.0041085.456.716.60777251186.45937789896.75616712486.38518059246.830364431314-Mar-0573.0041085.296.846.60777251186.45937789896.75616712486.38518059246.830364431315-Mar-0574.0041085.256.696.60777251186.45937789896.75616712486.38518059246.830364431315-Mar-0574.0041085.336.766.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-0576.0041085.316.766.60777251186.45937789896.75616712486.38518059246.830364431318-Mar-0577.0041085.296.546.60777251186.45937789896.75616712486.38518059246.830364431318-Mar-0577.0041085.456.566.60777251186.45937789896.75616712486.38518059246.830364431318-Mar-0577.0041085.226.696.60777251186.45937789896.75616712486.38518059246.830364431321-Mar-0580.0041085.266.686.60777251186.45937789896.75616712486.38518059246.830364431321-Mar-0580.0041085.36.626.60777251186.45937789896.75616712486.38518059246.830364431322-Mar-0581.0041085.366.566.60777251186.45937789896.75616712486.38518059246.830364431322-Mar-0581.0041085.246.566.60777251186.45937789896.75616712486.38518059246.830364431323-Mar-0582.0041085.436.586.60777251186.45937789896.75616712486.38518059246.830364431324-Mar-0583.0041085.346.626.60777251186.45937789896.75616712486.38518059246.830364431324-Mar-0583.0041085.246.76.60777251186.45937789896.75616712486.38518059246.830364431324-Mar-0583.0041085.346.676.60777251186.45937789896.75616712486.38518059246.830364431325-Mar-0584.0041085.496.676.60777251186.45937789896.75616712486.38518059246.830364431325-Mar-0584.0041085.296.666.60777251186.45937789896.75616712486.38518059246.830364431325-Mar-0584.0041085.346.576.60777251186.45937789896.75616712486.38518059246.830364431325-Mar-0584.0041085.316.686.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-0588.0041085.316.616.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-0588.0041085.46.666.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-0588.0041085.36.66.60777251186.45937789896.75616712486.38518059246.830364431330-Mar-0589.0041085.296.526.60777251186.45937789896.75616712486.38518059246.830364431330-Mar-0589.0041085.466.586.60777251186.45937789896.75616712486.38518059246.830364431330-Mar-0589.0041085.376.666.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-0590.0041085.216.566.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-0590.0041085.286.626.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-0590.0041085.256.696.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-0590.0041085.486.766.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-0590.0041085.236.596.60777251186.45937789896.75616712486.38518059246.830364431301-Apr-0591.0041085.36.616.60777251186.45937789896.75616712486.38518059246.830364431301-Apr-0591.0041085.286.616.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-0595.0041085.516.746.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-0595.0041085.256.546.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-0595.0041085.246.566.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-0596.0041085.416.586.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-0596.0041085.326.546.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-0596.0041085.316.626.60777251186.45937789896.75616712486.38518059246.830364431307-Apr-0597.0041085.36.626.60777251186.45937789896.75616712486.38518059246.830364431307-Apr-0597.0041085.336.646.60777251186.45937789896.75616712486.38518059246.830364431308-Apr-0598.0041085.86.596.60777251186.45937789896.75616712486.38518059246.830364431308-Apr-0598.0041085.336.546.60777251186.45937789896.75616712486.38518059246.830364431308-Apr-0598.0041085.266.636.60777251186.45937789896.75616712486.38518059246.830364431308-Apr-0598.0041085.386.76.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-05101.0041085.286.686.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-05101.0041085.276.496.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-05101.0041085.256.656.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-05101.0041085.416.676.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-05101.0041085.386.626.60777251186.45937789896.75616712486.38518059246.830364431312-Apr-05102.0041085.256.696.60777251186.45937789896.75616712486.38518059246.830364431312-Apr-05102.0041085.266.76.60777251186.45937789896.75616712486.38518059246.830364431312-Apr-05102.0041085.266.66.60777251186.45937789896.75616712486.38518059246.830364431312-Apr-05102.0041085.366.716.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-05104.0041085.326.686.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-05104.0041085.426.776.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-05104.0041085.296.726.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-05104.0041085.316.716.60777251186.45937789896.75616712486.38518059246.830364431315-Apr-05105.0041085.266.76.60777251186.45937789896.75616712486.38518059246.830364431318-Apr-05108.0041085.336.646.60777251186.45937789896.75616712486.38518059246.830364431318-Apr-05108.0041085.416.646.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-05109.0041085.286.666.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-05109.0041085.326.656.60777251186.45937789896.75616712486.38518059246.830364431320-Apr-05110.0041085.336.716.60777251186.45937789896.75616712486.38518059246.830364431320-Apr-05110.0041085.236.56.60777251186.45937789896.75616712486.38518059246.830364431320-Apr-05110.0041085.336.636.60777251186.45937789896.75616712486.38518059246.830364431321-Apr-05111.0041085.36.556.60777251186.45937789896.75616712486.38518059246.830364431321-Apr-05111.0041085.266.546.60777251186.45937789896.75616712486.38518059246.830364431322-Apr-05112.0041085.346.526.60777251186.45937789896.75616712486.38518059246.830364431322-Apr-05112.0041085.336.546.60777251186.45937789896.75616712486.38518059246.830364431325-Apr-05115.0041085.446.656.60777251186.45937789896.75616712486.38518059246.830364431325-Apr-05115.0041085.346.596.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-05116.0041085.446.546.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-05116.0041085.336.66.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-05118.0041085.236.556.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-05118.0041085.276.576.60777251186.45937789896.75616712486.38518059246.830364431329-Apr-05119.0041085.216.56.60777251186.45937789896.75616712486.38518059246.830364431329-Apr-05119.0041085.296.576.60777251186.45937789896.75616712486.38518059246.830364431329-Apr-05119.0041085.46.556.60777251186.45937789896.75616712486.38518059246.830364431329-Apr-05119.0041085.216.566.60777251186.45937789896.75616712486.38518059246.830364431302-May-05122.0041085.326.556.60777251186.45937789896.75616712486.38518059246.830364431302-May-05122.0041085.36.586.60777251186.45937789896.75616712486.38518059246.830364431305-May-05125.0041085.276.546.60777251186.45937789896.75616712486.38518059246.830364431305-May-05125.0041085.336.536.60777251186.45937789896.75616712486.38518059246.830364431305-May-05125.0041085.356.586.60777251186.45937789896.75616712486.38518059246.830364431310-May-05130.0041085.376.576.60777251186.45937789896.75616712486.38518059246.830364431310-May-05130.0041085.456.586.60777251186.45937789896.75616712486.38518059246.830364431310-May-05130.0041085.456.446.60777251186.45937789896.75616712486.38518059246.830364431310-May-05130.0041085.336.526.60777251186.45937789896.75616712486.38518059246.830364431311-May-05131.0041085.416.646.60777251186.45937789896.75616712486.38518059246.830364431312-May-05132.0041085.266.626.60777251186.45937789896.75616712486.38518059246.830364431316-May-05136.0041085.226.546.60777251186.45937789896.75616712486.38518059246.830364431316-May-05136.0041085.386.666.60777251186.45937789896.75616712486.38518059246.830364431318-May-05138.0041085.36.556.60777251186.45937789896.75616712486.38518059246.830364431320-May-05140.0041085.336.626.60777251186.45937789896.75616712486.38518059246.830364431324-May-05144.0041085.256.546.60777251186.45937789896.75616712486.38518059246.830364431325-May-05145.0041085.316.636.60777251186.45937789896.75616712486.38518059246.830364431326-May-05146.0041085.376.616.60777251186.45937789896.75616712486.38518059246.830364431327-May-05147.0041085.386.596.60777251186.45937789896.75616712486.38518059246.830364431301-Jun-05152.0041085.266.516.60777251186.45937789896.75616712486.38518059246.830364431303-Jun-05154.0041085.266.596.60777251186.45937789896.75616712486.38518059246.830364431303-Jun-05154.0041085.246.636.60777251186.45937789896.75616712486.38518059246.830364431307-Jun-05158.0041085.296.566.60777251186.45937789896.75616712486.38518059246.830364431309-Jun-05160.0041085.326.576.60777251186.45937789896.75616712486.38518059246.830364431309-Jun-05160.0041085.426.576.60777251186.45937789896.75616712486.38518059246.830364431309-Jun-05160.0041085.376.596.60777251186.45937789896.75616712486.38518059246.830364431309-Jun-05160.0041085.336.586.60777251186.45937789896.75616712486.38518059246.830364431313-Jun-05164.0041085.486.636.60777251186.45937789896.75616712486.38518059246.830364431314-Jun-05165.0041085.386.596.60777251186.45937789896.75616712486.38518059246.830364431320-Jun-05171.0041085.26.716.60777251186.45937789896.75616712486.38518059246.830364431320-Jun-05171.0041085.346.596.60777251186.45937789896.75616712486.38518059246.830364431321-Jun-05172.0041085.486.676.60777251186.45937789896.75616712486.38518059246.830364431323-Jun-05174.0041085.256.456.60777251186.45937789896.75616712486.38518059246.830364431323-Jun-05174.0041085.36.626.60777251186.45937789896.75616712486.38518059246.830364431323-Jun-05174.0041085.26.636.60777251186.45937789896.75616712486.38518059246.830364431324-Jun-05175.0041085.26.636.60777251186.45937789896.75616712486.38518059246.830364431328-Jun-05179.0041085.26.636.60777251186.45937789896.75616712486.38518059246.830364431329-Jun-05180.0041085.226.666.60777251186.45937789896.75616712486.38518059246.830364431329-Jun-05180.0041085.376.476.60777251186.45937789896.75616712486.38518059246.830364431329-Jun-05180.0041085.426.656.60777251186.45937789896.75616712486.38518059246.830364431330-Jun-05181.0041085.336.656.60777251186.45937789896.75616712486.38518059246.830364431305-Jul-05186.0041085.216.546.60777251186.45937789896.75616712486.38518059246.830364431308-Jul-05189.0041085.126.656.60777251186.45937789896.75616712486.38518059246.830364431313-Jul-05194.0041085.36.656.60777251186.45937789896.75616712486.38518059246.830364431315-Jul-05196.0041085.126.566.60777251186.45937789896.75616712486.38518059246.830364431319-Jul-05200.0041085.246.496.60777251186.45937789896.75616712486.38518059246.830364431321-Jul-05202.0041085.086.666.60777251186.45937789896.75616712486.38518059246.830364431327-Jul-05208.0041085.346.596.60777251186.45937789896.75616712486.38518059246.830364431327-Jul-05208.0041085.216.526.60777251186.45937789896.75616712486.38518059246.830364431303-Aug-05215.0041085.126.586.60777251186.45937789896.75616712486.38518059246.830364431305-Aug-05217.0041085.216.56.60777251186.45937789896.75616712486.38518059246.830364431305-Aug-05217.0041085.256.76.60777251186.45937789896.75616712486.38518059246.830364431309-Aug-05221.0041085.236.566.60777251186.45937789896.75616712486.38518059246.830364431312-Aug-05224.0041085.166.576.60777251186.45937789896.75616712486.38518059246.830364431318-Aug-05230.0041085.196.66.60777251186.45937789896.75616712486.38518059246.830364431323-Aug-05235.0041085.166.596.60777251186.45937789896.75616712486.38518059246.830364431326-Aug-05238.0041085.816.846.60777251186.45937789896.75616712486.38518059246.830364431326-Aug-05238.0041085.156.636.60777251186.45937789896.75616712486.38518059246.830364431330-Aug-05242.0041085.166.496.60777251186.45937789896.75616712486.38518059246.830364431330-Aug-05242.0041085.236.526.60777251186.45937789896.75616712486.38518059246.830364431301-Sep-05244.0041085.336.756.60777251186.45937789896.75616712486.38518059246.830364431302-Sep-05245.0041085.296.626.60777251186.45937789896.75616712486.38518059246.830364431302-Sep-05245.0041085.296.746.60777251186.45937789896.75616712486.38518059246.830364431302-Sep-05245.0041085.26.596.60777251186.45937789896.75616712486.38518059246.830364431308-Sep-05251.0041085.216.636.60777251186.45937789896.75616712486.38518059246.830364431308-Sep-05251.0041085.246.686.60777251186.45937789896.75616712486.38518059246.830364431308-Sep-05251.0041085.36.736.60777251186.45937789896.75616712486.38518059246.830364431308-Sep-05251.0041085.346.566.60777251186.45937789896.75616712486.38518059246.830364431308-Sep-05251.0041085.36.756.60777251186.45937789896.75616712486.38518059246.830364431312-Sep-05255.0041085.366.716.60777251186.45937789896.75616712486.38518059246.830364431313-Sep-05256.0041085.266.666.60777251186.45937789896.75616712486.38518059246.830364431313-Sep-05256.0041085.336.676.60777251186.45937789896.75616712486.38518059246.830364431314-Sep-05257.0041085.256.626.60777251186.45937789896.75616712486.38518059246.830364431315-Sep-05258.0041085.326.626.60777251186.45937789896.75616712486.38518059246.830364431315-Sep-05258.0041085.296.716.60777251186.45937789896.75616712486.38518059246.830364431316-Sep-05259.0041085.386.676.60777251186.45937789896.75616712486.38518059246.830364431316-Sep-05259.0041085.376.586.60777251186.45937789896.75616712486.38518059246.830364431320-Sep-05263.0041085.26.76.60777251186.45937789896.75616712486.38518059246.830364431322-Sep-05265.0041085.216.626.60777251186.45937789896.75616712486.38518059246.830364431323-Sep-05266.0041085.336.546.60777251186.45937789896.75616712486.38518059246.830364431323-Sep-05266.0041085.426.636.60777251186.45937789896.75616712486.38518059246.830364431326-Sep-05269.0041085.216.656.60777251186.45937789896.75616712486.38518059246.830364431327-Sep-05270.0041085.296.686.60777251186.45937789896.75616712486.38518059246.830364431303-Oct-05276.0041085.246.456.60777251186.45937789896.75616712486.38518059246.830364431303-Oct-05276.0041085.346.576.60777251186.45937789896.75616712486.38518059246.830364431305-Oct-05278.0041085.36.686.60777251186.45937789896.75616712486.38518059246.830364431305-Oct-05278.0041085.346.636.60777251186.45937789896.75616712486.38518059246.830364431305-Oct-05278.0041085.466.646.60777251186.45937789896.75616712486.38518059246.830364431306-Oct-05279.0041085.256.646.60777251186.45937789896.75616712486.38518059246.830364431306-Oct-05279.0041085.36.676.60777251186.45937789896.75616712486.38518059246.830364431306-Oct-05279.0041085.286.76.60777251186.45937789896.75616712486.38518059246.830364431306-Oct-05279.0041085.336.526.60777251186.45937789896.75616712486.38518059246.830364431313-Oct-05286.0041085.446.556.60777251186.45937789896.75616712486.38518059246.8303644313113-Oct-05286.0041085.416.66.60777251186.45937789896.75616712486.38518059246.8303644313513-Oct-05286.0041085.386.586.60777251186.45937789896.75616712486.38518059246.8303644313913-Oct-05286.0041085.336.636.60777251186.45937789896.75616712486.38518059246.8303644313225-Oct-05298.0041085.386.716.60777251186.45937789896.75616712486.38518059246.83036443131025-Oct-05298.0041085.46.716.60777251186.45937789896.75616712486.38518059246.8303644313526-Oct-05299.0041085.346.586.60777251186.45937789896.75616712486.38518059246.8303644313726-Oct-05299.0041085.36.626.60777251186.45937789896.75616712486.38518059246.8303644313126-Oct-05299.0041085.286.726.60777251186.45937789896.75616712486.38518059246.8303644313226-Oct-05299.0041085.416.86.60777251186.45937789896.75616712486.38518059246.8303644313726-Oct-05299.0041085.246.646.60777251186.45937789896.75616712486.38518059246.8303644313728-Oct-05301.0041085.366.716.60777251186.45937789896.75616712486.38518059246.8303644313731-Oct-05304.0041085.376.646.60777251186.45937789896.75616712486.38518059246.8303644313631-Oct-05304.0041085.296.666.60777251186.45937789896.75616712486.38518059246.83036443131031-Oct-05304.0041085.346.536.60777251186.45937789896.75616712486.38518059246.8303644313401-Nov-05305.0041085.346.626.60777251186.45937789896.75616712486.38518059246.8303644313901-Nov-05305.0041085.326.636.60777251186.45937789896.75616712486.38518059246.8303644313301-Nov-05305.0041085.246.646.60777251186.45937789896.75616712486.38518059246.8303644313502-Nov-05306.0041085.396.426.60777251186.45937789896.75616712486.38518059246.83036443131003-Nov-05307.0041085.346.636.60777251186.45937789896.75616712486.38518059246.8303644313903-Nov-05307.0041085.296.66.60777251186.45937789896.75616712486.38518059246.8303644313509-Nov-05313.0041085.336.626.60777251186.45937789896.75616712486.38518059246.8303644313609-Nov-05313.0041085.276.626.60777251186.45937789896.75616712486.38518059246.8303644313309-Nov-05313.0041085.446.686.60777251186.45937789896.75616712486.38518059246.8303644313810-Nov-05314.0041085.256.736.60777251186.45937789896.75616712486.38518059246.8303644313310-Nov-05314.0041085.396.76.60777251186.45937789896.75616712486.38518059246.8303644313410-Nov-05314.0041085.456.716.60777251186.45937789896.75616712486.38518059246.8303644313314-Nov-05318.0041085.36.676.60777251186.45937789896.75616712486.38518059246.8303644313814-Nov-05318.0041085.416.636.60777251186.45937789896.75616712486.38518059246.8303644313114-Nov-05318.0041085.276.66.60777251186.45937789896.75616712486.38518059246.83036443131014-Nov-05318.0041085.446.536.60777251186.45937789896.75616712486.38518059246.83036443131015-Nov-05319.0041085.446.626.60777251186.45937789896.75616712486.38518059246.8303644313415-Nov-05319.0041085.366.596.60777251186.45937789896.75616712486.38518059246.8303644313415-Nov-05319.0041085.46.616.60777251186.45937789896.75616712486.38518059246.8303644313216-Nov-05320.0041085.286.516.60777251186.45937789896.75616712486.38518059246.8303644313316-Nov-05320.0041085.256.716.60777251186.45937789896.75616712486.38518059246.8303644313617-Nov-05321.0041085.376.766.60777251186.45937789896.75616712486.38518059246.83036443131018-Nov-05322.0041085.216.666.60777251186.45937789896.75616712486.38518059246.8303644313823-Nov-05327.0041085.356.556.60777251186.45937789896.75616712486.38518059246.8303644313223-Nov-05327.0041085.216.626.60777251186.45937789896.75616712486.38518059246.8303644313623-Nov-05327.0041085.266.656.60777251186.45937789896.75616712486.38518059246.83036443131023-Nov-05327.0041085.326.676.60777251186.45937789896.75616712486.38518059246.8303644313929-Nov-05333.0041085.216.696.60777251186.45937789896.75616712486.38518059246.8303644313629-Nov-05333.0041085.246.696.60777251186.45937789896.75616712486.38518059246.8303644313629-Nov-05333.0041085.386.676.60777251186.45937789896.75616712486.38518059246.8303644313201-Dec-05335.0041085.256.536.60777251186.45937789896.75616712486.38518059246.8303644313201-Dec-05335.0041085.386.636.60777251186.45937789896.75616712486.38518059246.8303644313901-Dec-05335.0041085.276.526.60777251186.45937789896.75616712486.38518059246.8303644313606-Dec-05340.0041085.216.636.60777251186.45937789896.75616712486.38518059246.8303644313108-Dec-05342.0041085.266.66.60777251186.45937789896.75616712486.38518059246.8303644313109-Dec-05343.0041085.246.756.60777251186.45937789896.75616712486.38518059246.8303644313409-Dec-05343.0041085.266.66.60777251186.45937789896.75616712486.38518059246.8303644313416-Dec-05350.0041085.346.616.60777251186.45937789896.75616712486.38518059246.8303644313616-Dec-05350.0041085.346.556.60777251186.45937789896.75616712486.38518059246.8303644313420-Dec-05354.0041085.256.696.60777251186.45937789896.75616712486.38518059246.8303644313720-Dec-05354.0041085.386.676.60777251186.45937789896.75616712486.38518059246.8303644313304-Jan-06369.0041085.446.726.60777251186.45937789896.75616712486.38518059246.830364431306-Jan-06371.0041085.346.696.60777251186.45937789896.75616712486.38518059246.830364431312-Jan-06377.0041085.36.656.60777251186.45937789896.75616712486.38518059246.830364431317-Jan-06382.0041085.356.56.60777251186.45937789896.75616712486.38518059246.830364431317-Jan-06382.0041085.286.626.60777251186.45937789896.75616712486.38518059246.830364431319-Jan-06384.0041085.226.596.60777251186.45937789896.75616712486.38518059246.830364431320-Jan-06385.0041085.46.546.60777251186.45937789896.75616712486.38518059246.830364431323-Jan-06388.0041085.486.586.60777251186.45937789896.75616712486.38518059246.830364431323-Jan-06388.0041085.296.596.60777251186.45937789896.75616712486.38518059246.830364431326-Jan-06391.0041085.126.566.60777251186.45937789896.75616712486.38518059246.830364431326-Jan-06391.0041085.186.626.60777251186.45937789896.75616712486.38518059246.830364431327-Jan-06392.0041085.196.676.60777251186.45937789896.75616712486.38518059246.830364431327-Jan-06392.0041085.296.656.60777251186.45937789896.75616712486.38518059246.830364431327-Jan-06392.0041085.336.476.60777251186.45937789896.75616712486.38518059246.830364431330-Jan-06395.0041085.46.686.60777251186.45937789896.75616712486.38518059246.830364431302-Feb-06398.0041085.256.636.60777251186.45937789896.75616712486.38518059246.830364431302-Feb-06398.0041085.46.636.60777251186.45937789896.75616712486.38518059246.830364431302-Feb-06398.0041085.366.616.60777251186.45937789896.75616712486.38518059246.830364431302-Feb-06398.0041085.266.636.60777251186.45937789896.75616712486.38518059246.830364431302-Feb-06398.0041085.346.526.60777251186.45937789896.75616712486.38518059246.830364431306-Feb-06402.0041085.286.676.60777251186.45937789896.75616712486.38518059246.830364431306-Feb-06402.0041085.456.586.60777251186.45937789896.75616712486.38518059246.830364431306-Feb-06402.0041085.236.566.60777251186.45937789896.75616712486.38518059246.830364431306-Feb-06402.0041085.216.596.60777251186.45937789896.75616712486.38518059246.830364431307-Feb-06403.0041085.356.666.60777251186.45937789896.75616712486.38518059246.830364431307-Feb-06403.0041085.276.636.60777251186.45937789896.75616712486.38518059246.830364431309-Feb-06405.0041085.346.696.60777251186.45937789896.75616712486.38518059246.830364431309-Feb-06405.0041085.36.566.60777251186.45937789896.75616712486.38518059246.830364431309-Feb-06405.0041085.376.576.60777251186.45937789896.75616712486.38518059246.830364431309-Feb-06405.0041085.286.616.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-06406.0041085.386.526.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-06406.0041085.36.526.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-06406.0041085.386.496.60777251186.45937789896.75616712486.38518059246.830364431310-Feb-06406.0041085.456.686.60777251186.45937789896.75616712486.38518059246.830364431313-Feb-06409.0041085.336.666.60777251186.45937789896.75616712486.38518059246.830364431313-Feb-06409.0041085.326.596.60777251186.45937789896.75616712486.38518059246.830364431313-Feb-06409.0041085.286.66.60777251186.45937789896.75616712486.38518059246.830364431313-Feb-06409.0041085.226.616.60777251186.45937789896.75616712486.38518059246.830364431314-Feb-06410.0041085.386.636.60777251186.45937789896.75616712486.38518059246.830364431314-Feb-06410.0041085.366.556.60777251186.45937789896.75616712486.38518059246.830364431314-Feb-06410.0041085.266.666.60777251186.45937789896.75616712486.38518059246.830364431314-Feb-06410.0041085.246.646.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-06412.0041085.296.546.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-06412.0041085.256.596.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-06412.0041085.216.536.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-06412.0041085.346.476.60777251186.45937789896.75616712486.38518059246.830364431316-Feb-06412.0041085.236.536.60777251186.45937789896.75616712486.38518059246.830364431317-Feb-06413.0041085.226.656.60777251186.45937789896.75616712486.38518059246.830364431317-Feb-06413.0041085.386.546.60777251186.45937789896.75616712486.38518059246.830364431317-Feb-06413.0041085.246.626.60777251186.45937789896.75616712486.38518059246.830364431317-Feb-06413.0041085.286.76.60777251186.45937789896.75616712486.38518059246.830364431320-Feb-06416.0041085.366.626.60777251186.45937789896.75616712486.38518059246.830364431320-Feb-06416.0041085.346.76.60777251186.45937789896.75616712486.38518059246.830364431321-Feb-06417.0041085.416.586.60777251186.45937789896.75616712486.38518059246.830364431321-Feb-06417.0041085.226.576.60777251186.45937789896.75616712486.38518059246.830364431321-Feb-06417.0041085.366.576.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.336.596.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.416.646.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.336.626.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.286.536.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.396.636.60777251186.45937789896.75616712486.38518059246.830364431327-Feb-06423.0041085.216.576.60777251186.45937789896.75616712486.38518059246.830364431328-Feb-06424.0041085.386.56.60777251186.45937789896.75616712486.38518059246.830364431328-Feb-06424.0041085.386.546.60777251186.45937789896.75616712486.38518059246.830364431302-Mar-06426.0041085.216.56.60777251186.45937789896.75616712486.38518059246.830364431302-Mar-06426.0041085.386.566.60777251186.45937789896.75616712486.38518059246.830364431302-Mar-06426.0041085.396.516.60777251186.45937789896.75616712486.38518059246.830364431303-Mar-06427.0041085.446.76.60777251186.45937789896.75616712486.38518059246.830364431306-Mar-06430.0041085.46.596.60777251186.45937789896.75616712486.38518059246.830364431306-Mar-06430.0041085.36.586.60777251186.45937789896.75616712486.38518059246.830364431306-Mar-06430.0041085.386.586.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-06432.0041085.376.556.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-06432.0041085.346.716.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-06432.0041085.296.546.60777251186.45937789896.75616712486.38518059246.830364431308-Mar-06432.0041085.376.626.60777251186.45937789896.75616712486.38518059246.830364431309-Mar-06433.0041085.376.626.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-06434.0041085.266.596.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-06434.0041085.316.696.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-06434.0041085.226.516.60777251186.45937789896.75616712486.38518059246.830364431310-Mar-06434.0041085.216.626.60777251186.45937789896.75616712486.38518059246.830364431313-Mar-06437.0041085.296.536.60777251186.45937789896.75616712486.38518059246.830364431313-Mar-06437.0041085.446.516.60777251186.45937789896.75616712486.38518059246.830364431313-Mar-06437.0041085.356.516.60777251186.45937789896.75616712486.38518059246.830364431315-Mar-06439.0041085.46.466.60777251186.45937789896.75616712486.38518059246.830364431315-Mar-06439.0041085.456.556.60777251186.45937789896.75616712486.38518059246.830364431315-Mar-06439.0041085.246.516.60777251186.45937789896.75616712486.38518059246.830364431316-Mar-06440.0041085.256.666.60777251186.45937789896.75616712486.38518059246.830364431316-Mar-06440.0041085.456.746.60777251186.45937789896.75616712486.38518059246.830364431316-Mar-06440.0041085.366.556.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.426.546.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.346.666.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.216.536.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.376.576.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.336.576.60777251186.45937789896.75616712486.38518059246.830364431317-Mar-06441.0041085.336.696.60777251186.45937789896.75616712486.38518059246.830364431320-Mar-06444.0041085.276.56.60777251186.45937789896.75616712486.38518059246.830364431320-Mar-06444.0041085.386.596.60777251186.45937789896.75616712486.38518059246.830364431320-Mar-06444.0041085.326.676.60777251186.45937789896.75616712486.38518059246.830364431321-Mar-06445.0041085.346.556.60777251186.45937789896.75616712486.38518059246.830364431321-Mar-06445.0041085.386.566.60777251186.45937789896.75616712486.38518059246.830364431321-Mar-06445.0041085.346.56.60777251186.45937789896.75616712486.38518059246.830364431322-Mar-06446.0041085.446.526.60777251186.45937789896.75616712486.38518059246.830364431322-Mar-06446.0041085.426.526.60777251186.45937789896.75616712486.38518059246.830364431323-Mar-06447.0041085.46.676.60777251186.45937789896.75616712486.38518059246.830364431323-Mar-06447.0041085.46.516.60777251186.45937789896.75616712486.38518059246.830364431323-Mar-06447.0041085.326.586.60777251186.45937789896.75616712486.38518059246.830364431324-Mar-06448.0041085.446.526.60777251186.45937789896.75616712486.38518059246.830364431324-Mar-06448.0041085.246.636.60777251186.45937789896.75616712486.38518059246.830364431327-Mar-06451.0041085.386.586.60777251186.45937789896.75616712486.38518059246.830364431327-Mar-06451.0041085.286.516.60777251186.45937789896.75616712486.38518059246.830364431327-Mar-06451.0041085.346.486.60777251186.45937789896.75616712486.38518059246.830364431328-Mar-06452.0041085.446.636.60777251186.45937789896.75616712486.38518059246.830364431328-Mar-06452.0041085.386.596.60777251186.45937789896.75616712486.38518059246.830364431328-Mar-06452.0041085.296.516.60777251186.45937789896.75616712486.38518059246.830364431328-Mar-06452.0041085.326.626.60777251186.45937789896.75616712486.38518059246.830364431328-Mar-06452.0041085.276.556.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-06453.0041085.426.696.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-06453.0041085.286.556.60777251186.45937789896.75616712486.38518059246.830364431329-Mar-06453.0041085.346.716.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-06455.0041085.326.526.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-06455.0041085.266.666.60777251186.45937789896.75616712486.38518059246.830364431331-Mar-06455.0041085.476.696.60777251186.45937789896.75616712486.38518059246.830364431303-Apr-06458.0041085.286.66.60777251186.45937789896.75616712486.38518059246.830364431303-Apr-06458.0041085.286.566.60777251186.45937789896.75616712486.38518059246.830364431303-Apr-06458.0041085.366.666.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-06460.0041085.236.596.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-06460.0041085.386.676.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-06460.0041085.456.516.60777251186.45937789896.75616712486.38518059246.830364431305-Apr-06460.0041085.376.596.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-06461.0041085.366.466.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-06461.0041085.296.516.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-06461.0041085.386.566.60777251186.45937789896.75616712486.38518059246.830364431306-Apr-06461.0041085.356.516.60777251186.45937789896.75616712486.38518059246.830364431307-Apr-06462.0041085.376.486.60777251186.45937789896.75616712486.38518059246.830364431310-Apr-06465.0041085.256.516.60777251186.45937789896.75616712486.38518059246.830364431310-Apr-06465.0041085.456.596.60777251186.45937789896.75616712486.38518059246.830364431310-Apr-06465.0041085.456.626.60777251186.45937789896.75616712486.38518059246.830364431310-Apr-06465.0041085.346.666.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-06466.0041085.336.666.60777251186.45937789896.75616712486.38518059246.830364431311-Apr-06466.0041085.426.596.60777251186.45937789896.75616712486.38518059246.830364431313-Apr-06468.0041085.286.556.60777251186.45937789896.75616712486.38518059246.830364431313-Apr-06468.0041085.216.596.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-06469.0041085.216.576.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-06469.0041085.346.646.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-06469.0041085.386.486.60777251186.45937789896.75616712486.38518059246.830364431314-Apr-06469.0041085.326.446.60777251186.45937789896.75616712486.38518059246.830364431317-Apr-06472.0041085.386.576.60777251186.45937789896.75616712486.38518059246.830364431317-Apr-06472.0041085.336.636.60777251186.45937789896.75616712486.38518059246.830364431317-Apr-06472.0041085.376.636.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-06474.0041085.446.646.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-06474.0041085.316.516.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-06474.0041085.346.626.60777251186.45937789896.75616712486.38518059246.830364431319-Apr-06474.0041085.456.666.60777251186.45937789896.75616712486.38518059246.830364431321-Apr-06476.0041085.256.566.60777251186.45937789896.75616712486.38518059246.830364431321-Apr-06476.0041085.366.516.60777251186.45937789896.75616712486.38518059246.830364431324-Apr-06479.0041085.276.586.60777251186.45937789896.75616712486.38518059246.830364431324-Apr-06479.0041085.386.596.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-06481.0041085.376.56.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-06481.0041085.36.616.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-06481.0041085.446.596.60777251186.45937789896.75616712486.38518059246.830364431326-Apr-06481.0041085.286.526.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-06483.0041085.246.546.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-06483.0041085.396.516.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-06483.0041085.336.656.60777251186.45937789896.75616712486.38518059246.830364431328-Apr-06483.0041085.376.536.60777251186.45937789896.75616712486.38518059246.830364431302-May-06487.0041085.346.556.60777251186.45937789896.75616712486.38518059246.830364431302-May-06487.0041085.326.556.60777251186.45937789896.75616712486.38518059246.830364431304-May-06489.0041085.416.436.60777251186.45937789896.75616712486.38518059246.83036443134108000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000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2 s- 3 s+ 3 s+ 2 sSMP buffermeanSikora bufferDays after Jan 1, 2005Buffer pHLexington Quality Control Sample 4108P008avg=6.01909090912s=0.1875084212std=0.09375421063s=0.2812626319DATE_OUTIDpHBupHavgavg-2*stdavg+2*stdavg-3*stdavg+3*std20-Jan-0520.00PA084.35.986.01909090915.83158248796.20659933035.73782827726.300353540920-Jan-0520.00PB084.336.026.01909090915.83158248796.20659933035.73782827726.300353540903-Feb-0534.00P0084.2566.01909090915.83158248796.20659933035.73782827726.300353540903-Feb-0534.00P0084.246.026.01909090915.83158248796.20659933035.73782827726.300353540914-Feb-0545.00P0084.316.066.01909090915.83158248796.20659933035.73782827726.300353540914-Feb-0545.00P0084.316.086.01909090915.83158248796.20659933035.73782827726.300353540923-Feb-0554.00P0084.215.96.01909090915.83158248796.20659933035.73782827726.300353540923-Feb-0554.00P0084.245.896.01909090915.83158248796.20659933035.73782827726.300353540928-Feb-0559.00P0084.516.116.01909090915.83158248796.20659933035.73782827726.300353540928-Feb-0559.00P0084.56.156.01909090915.83158248796.20659933035.73782827726.300353540904-Mar-0563.00P0084.566.146.01909090915.83158248796.20659933035.73782827726.300353540904-Mar-0563.00P0085.136.156.01909090915.83158248796.20659933035.73782827726.300353540909-Mar-0568.00P0084.516.126.01909090915.83158248796.20659933035.73782827726.300353540909-Mar-0568.00P0084.556.156.01909090915.83158248796.20659933035.73782827726.300353540915-Mar-0574.00P0084.486.086.01909090915.83158248796.20659933035.73782827726.300353540915-Mar-0574.00P0084.536.096.01909090915.83158248796.20659933035.73782827726.300353540916-Mar-0575.00P0084.476.16.01909090915.83158248796.20659933035.73782827726.300353540916-Mar-0575.00P0084.496.086.01909090915.83158248796.20659933035.73782827726.300353540921-Mar-0580.00P0084.4966.01909090915.83158248796.20659933035.73782827726.300353540921-Mar-0580.00P0084.496.046.01909090915.83158248796.20659933035.73782827726.300353540922-Mar-0581.00PB084.46.16.01909090915.83158248796.20659933035.73782827726.300353540922-Mar-0581.00PA084.396.026.01909090915.83158248796.20659933035.73782827726.300353540923-Mar-0582.00P0084.335.976.01909090915.83158248796.20659933035.73782827726.300353540923-Mar-0582.00P0084.365.936.01909090915.83158248796.20659933035.73782827726.300353540928-Mar-0587.00P0084.45.916.01909090915.83158248796.20659933035.73782827726.300353540928-Mar-0587.00P0084.335.966.01909090915.83158248796.20659933035.73782827726.300353540929-Mar-0588.00P0084.335.996.01909090915.83158248796.20659933035.73782827726.300353540929-Mar-0588.00P0084.355.956.01909090915.83158248796.20659933035.73782827726.300353540901-Apr-0591.00P0084.366.126.01909090915.83158248796.20659933035.73782827726.300353540901-Apr-0591.00P0084.386.116.01909090915.83158248796.20659933035.73782827726.300353540906-Apr-0596.00P0084.235.856.01909090915.83158248796.20659933035.73782827726.300353540906-Apr-0596.00P0084.275.856.01909090915.83158248796.20659933035.73782827726.300353540912-Apr-05102.00P0084.35.96.01909090915.83158248796.20659933035.73782827726.300353540912-Apr-05102.00P0084.255.916.01909090915.83158248796.20659933035.73782827726.300353540915-Apr-05105.00P0084.326.026.01909090915.83158248796.20659933035.73782827726.300353540915-Apr-05105.00P0084.2666.01909090915.83158248796.20659933035.73782827726.300353540920-Apr-05110.00P0084.155.956.01909090915.83158248796.20659933035.73782827726.300353540920-Apr-05110.00P0084.195.856.01909090915.83158248796.20659933035.73782827726.300353540929-Apr-05119.00P0084.295.996.01909090915.83158248796.20659933035.73782827726.300353540929-Apr-05119.00P0084.265.886.01909090915.83158248796.20659933035.73782827726.300353540910-May-05130.00PA084.316.016.01909090915.83158248796.20659933035.73782827726.300353540910-May-05130.00PB084.396.126.01909090915.83158248796.20659933035.73782827726.300353540926-May-05146.00P0084.316.146.01909090915.83158248796.20659933035.73782827726.300353540926-May-05146.00P0084.386.156.01909090915.83158248796.20659933035.73782827726.300353540920-Jun-05171.00P0084.316.16.01909090915.83158248796.20659933035.73782827726.300353540920-Jun-05171.00P0084.316.16.01909090915.83158248796.20659933035.73782827726.300353540915-Jul-05196.58P0084.376.16.01909090915.83158248796.20659933035.73782827726.300353540915-Jul-05196.58P0084.366.146.01909090915.83158248796.20659933035.73782827726.300353540908-Aug-05220.49P0084.726.136.01909090915.83158248796.20659933035.73782827726.300353540908-Aug-05220.49P0084.526.126.01909090915.83158248796.20659933035.73782827726.300353540923-Aug-05235.57P0084.296.056.01909090915.83158248796.20659933035.73782827726.300353540923-Aug-05235.57P0084.256.136.01909090915.83158248796.20659933035.73782827726.300353540909-Sep-05252.74P0084.355.926.01909090915.83158248796.20659933035.73782827726.300353540909-Sep-05252.74P0084.3466.01909090915.83158248796.20659933035.73782827726.300353540915-Sep-05258.66P0084.25.946.01909090915.83158248796.20659933035.73782827726.300353540915-Sep-05258.66P0084.295.976.01909090915.83158248796.20659933035.73782827726.300353540928-Sep-05271.39P0084.125.926.01909090915.83158248796.20659933035.73782827726.300353540928-Sep-05271.39P0084.195.916.01909090915.83158248796.20659933035.73782827726.300353540903-Oct-05276.59P0084.125.996.01909090915.83158248796.20659933035.73782827726.300353540903-Oct-05276.59P0084.136.016.01909090915.83158248796.20659933035.73782827726.300353540906-Oct-05279.45P0084.076.116.01909090915.83158248796.20659933035.73782827726.300353540906-Oct-05279.45P0083.945.976.01909090915.83158248796.20659933035.73782827726.3003535409P008000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000- 2 s- 3 s+ 3 s+ 2 sSMP buffermeanSikora bufferDays after Jan 1, 2005Buffer pHPrinceton Quality Control Sample P008Sheet3DATE_OUTFMIDpHBupH28-Sep-05P0084.125.9228-Sep-05P0084.195.9103-Oct-05P0084.125.9903-Oct-05P0084.136.0106-Oct-05P0084.076.1106-Oct-05P0083.945.97LEXINGTON LABPRINCETON LABstirring time for buffer in soiltime buffer set in soil prior to measurementLabFit method with Sikora buffer0.33 min.0.1137 min.41.5 hrsfor 3 trays(n=120)Method for adding water to soilEach sample stirred with stir rod and let set for 30 min.Sikora Buffer pH, LabFit instrumentSoil pH, LabFit instrumentSoil pH, NAPT medianSMP Buffer pH, NAPT medianSoil pHBuffer pH1:1 lineregression lineChart35.725.97.857.855.275.66.456.47.518.017.898.015.295.176.946.957.458.288.387.587.727.437.475.395.457.957.97.227.45.695.736.346.55.815.77.827.867.387.67.9485.855.76.46.346.76.725.845.957.026.88.18.274.574.85.375.555.685.75.75.84.264.275.285.326.416.575.7864.774.946.326.47.67.76.556.68.058.17.978.096.246.425.085.375.625.797.88.027.678.247.97.928.588.788.17.687.767.998.17.797.867.858.025.725.34.624.726.296.345.275.56.416.56.87.026.746.786.76.756.126.37.888.058.068.165.225.547.897.817.317.736.96.856.9975.635.635.925.746.736.787.387.76.246.45.125.15.986.265.795.917.767.94.654.666.526.15.516.16.086.035.545.59.229.366.376.56.226.26.466.487.427.66.116.16.816.835.765.855.865.86.026.196.276.435.8967.327.568.468.526.396.497.857.95.715.845.775.88.18.246.957.15.345.524.924.827.587.95.325.915.685.385.635.767.397.47.657.76.326.486.15.97.237.765.75.855.65.647.587.857.617.94.54.557.787.765,10water pH, old waywater pH, new instr120+ Pri Farmer SamplesWater with soil-water pH was not hand-stirred for each sample. They were tray swirled.There isan issue with the last couple rows of the last tray in the group of 3 having erratic data for water pH because the tray wasn't set level. The probes probably didn't get fully immersed.The problem is proved because the erratic data at low water pH does not appear in the 5/120 timing where a set of 2 tray was run then a 1 tray was run.5/30avg0.127875-1.30031251.049610389630/30avg0.0834375-1.9881.43552631585/600.0913125-1.3141251.551153846230/600.0961875-1.40606251.94844155845/1200.0785-1.25381252.499480519530/1200.0595625-1.1066252.3629487179std0.21014037692.71291841320.1546697224std0.20700635573.15071496330.12672538740.11899009992.76385711420.16033819720.12175277492.82238515860.16471059930.10208024962.73864399070.3746262490.13483904632.57797928950.4609866249*notice the switching of 30/120 and 5/120 so time could be in orderLab# for Lex analysisNew Lab #Original Lab #Sample #Original pHOriginal BufferpH_2**Buffer_2**delta pHdelta BupHT1WT1BT2BT3BpH_1*Buffer_1*delta pHdelta BupHT1WT1BT2BT3BpH_4****Buffer_4****delta pHdelta BupHT1WT1BT2BT3BpH_3***Buffer_3***delta pHdelta BupHT1WT1BT2BT3BpH_6^^Buffer_6^^delta pHdelta BupHT1WT1BT2BT3BpH_5^Buffer_5^delta pHdelta BupHT1WT1BT2BT3BSETTINGTimeSetLagDiffTIMETIMETimewoLagstdevR2avg diffstd diff1900016238516016.46.876.590.19-6.876.550.15-6.876.620.22-6.876.650.25-6.876.580.18-6.876.440.04-6.87(sec)(sec)(sec)(min)(min)2900026238616026.436.886.490.06-6.886.41-0.02-6.886.277.06-0.160.181.356.38-0.05-6.886.347.1-0.090.222.756.247.07-0.190.192.355/303528631.050.60.130.7940.1278750.21014037693900036238716036.787.056.63-0.15-7.050.826.820.04-7.051.236.80.02-7.051.356.850.07-7.051.756.77-0.01-7.052.756.72-0.06-7.052.3730/306026.486.41.440.990.150.8030.08343750.20700635574900046238816046.556.946.560.01-6.940.826.560.01-6.941.236.610.06-6.941.356.790.24-6.941.756.740.19-6.942.756.580.03-6.942.375/606528931.551.10.160.9350.09131250.11899009995900056238916056.757.046.790.04-7.040.886.960.21-7.041.236.940.19-7.041.326.950.2-7.041.776.910.16-7.042.776.820.07-7.042.3530/6090271171.951.50.160.9360.09618750.12175277496900066239016066.6876.790.11-70.886.810.13-71.236.790.11-71.326.930.25-71.776.780.1-72.776.730.05-72.35*30/120150-8.4141.62.361.910.460.920.05956250.13483904637900076239116076.787.056.77-0.01-7.050.826.880.1-7.051.256.910.13-7.051.356.80.02-7.051.756.73-0.05-7.052.776.68-0.1-7.052.35*5/120125251502.52.050.370.9570.07850.10208024968900086239216086.97.116.85-0.05-7.110.826.930.03-7.111.256.920.02-7.111.356.990.09-7.111.756.84-0.06-7.112.776.81-0.09-7.112.359900096788517016.316.896.630.32-6.890.976.730.42-6.891.26.630.32-6.891.656.610.3-6.891.876.450.14-6.893.086.440.13-6.892.68For next run of samples add a shorter time and drop one of the longer times10900106788617026.276.936.710.44-6.930.976.810.54-6.931.26.530.26-6.931.656.660.39-6.931.876.490.22-6.933.086.490.22-6.932.685/10, 5/30, 30/30, 5/60, 30/60, 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Settings for pH_1 & Buffer_1** Settings for pH_2 & Buffer_2^ Settings for pH_5 & Buffer_5File Name 0130.rckFile Name #4 0130 71305.rckFile Name 1120 JULY192005.RCKSample delay time 30Sample delay time 5Sample delay time 30# rdgs for stability 45# rdgs for stability 45# rdgs for stability 45pH stability 0.01pH stability 0.01pH stability 0.01Maximum sample time 30Maximum sample time 30Maximum sample time 120* Buffer did not get stirred- stirrer came out*** Settings for pH_3 & Buffer_3****Settings for pH_4 & Buffer_4^ ^Settings for pH_6 & Buffer_6File Name 0160 July 13 2005.rckFile Name 0160 JULY142005.RCKFile Name JULY182005 1120.RCK & 1121 71805.RCKSample delay time 30Sample delay time 5Sample delay time 5# rdgs for stability 45# rdgs for stability 45# rdgs for stability 45pH stability 0.01pH stability 0.01pH stability 0.01Maximium sample time 60Maximum sample time 60Maximum sample time 120120+ Pri Farmer Samples0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr120+Pri Farmer Samples woL2Rows0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,60int ND 0slope ND 1water pH, old waywater pH, new instrSamplesFromLex0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instrLexSoilData0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,60SMP buffer pH, old wayKY buffer pH, new instrLexSoilData (2)0.7940.1278750.21014037690.8030.08343750.20700635570.9350.09131250.11899009990.9360.09618750.12175277490.920.05956250.13483904630.9570.07850.1020802496manualReadings6.446.46.246.436.726.786.586.556.826.756.736.686.686.786.816.96.446.316.496.276.376.196.386.146.656.416.235.956.516.326.616.236.556.546.36.236.56.56.516.356.496.466.356.246.586.446.666.56.065.946.096.045.975.956.276.236.26.076.096.056.356.365.945.885.895.836.0766.126.056.055.975.85.725.815.715.675.755.565.475.435.45.645.545.975.876.356.226.426.316.296.175.825.775.895.775.865.866.326.36.126.16.026.025.645.616.286.246.076.096.286.226.216.226.216.116.036.015.795.685.895.886.096.025.75.645.645.535.325.295.735.635.685.626.46.36.396.316.276.1565.975.765.725.585.55.85.85.835.85.755.65.955.96.226.16.216.26.035.96.176.15.835.86.0266.065.95.765.75.825.75.255.25.425.35.225.25.665.65.95.86.486.56.476.46.496.46.16.15.885.86.115.96.136.025.945.845.935.86.0766.015.895.875.736.065.896.095.996.055.786.196.096.115.935.695.35.685.375.875.535.815.485.745.145.725.275.825.646.046.16.126.186.156.145.945.75.825.316.26.345.745.85.455.635.895.565.054.855.755.765.775.995.635.715.185.364.684.955.615.795.684.885.545.845.565.634.966.054.664.884.854.755.174.774.495.275.474.830,120water pH, old waywater pH, new instrNAPTsoils6.966.826.996.86.946.867.116.96.986.876.827.076.926.986.826.886.827.016.876.926.886.986.866.856.766.886.756.776.726.826.716.76.666.766.696.796.787.026.96.96.96.966.866.796.746.866.756.886.857.046.896.946.927.036.896.886.847.066.876.966.917.066.917.026.917.036.896.956.886.866.86.866.856.936.856.796.736.826.76.726.676.836.766.716.696.936.936.936.936.986.876.876.816.966.856.816.86.96.96.8776.9676.9477.0577.017.17.0377.0376.976.96.926.97.0176.856.96.96.96.686.76.776.76.666.76.786.86.836.96.96.96.96.96.96.96.9376.926.96.9476.987.056.886.976.937.046.987.066.9376.886.976.967.036.957.026.9376.947.026.967.016.736.826.86.796.826.886.856.856.76.796.776.766.766.847.037.027.047.127.037.016.856.926.816.816.966.926.986.96.886.857.016.916.476.426.76.656.816.796.836.796.766.746.496.396.936.957.067.046.896.956.956.996.696.776.886.926.526.726.636.736.196.56.226.326.776.816.956.996.796.826.266.296.836.867.016.996.786.856.96.876.746.847.087.016.46.326.316.286.376.336.496.446.616.66.396.296.436.466.76.566.86.816.246.1530,120SMP buffer pH, old wayKY buffer pH, new instrNAPTsoils (2)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30water pH, old waywater pH, new instrNAPT&LEX_rouSet000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30SMP buffer pH, old wayKY buffer pH, new instrelapsedTime_template00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60water pH, old waywater pH, new instrSheet1000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60SMP buffer pH, old wayKY buffer pH, new instr6.586.46.346.436.776.786.746.556.916.756.786.686.736.786.846.96.456.316.496.276.426.196.496.146.626.416.225.956.556.326.666.236.566.546.326.236.56.56.516.356.426.466.426.246.566.446.716.56.085.946.16.046.085.956.326.236.146.076.076.056.446.365.985.885.885.836.0866.146.056.075.975.865.725.855.715.645.755.65.475.485.45.715.5465.876.416.226.426.316.316.175.915.775.915.775.875.866.356.36.166.16.066.025.75.616.316.246.096.096.316.226.256.226.256.116.056.015.795.685.945.886.16.025.715.645.665.535.365.295.745.635.75.626.46.36.446.316.336.156.055.975.785.725.615.55.825.85.865.85.755.65.995.96.266.16.266.26.065.96.236.15.855.86.0366.135.95.865.75.845.75.275.25.475.35.265.25.685.65.955.86.496.56.556.46.516.46.126.15.895.86.095.96.136.025.915.845.865.86.1365.995.895.835.736.025.896.115.995.945.786.166.096.025.935.425.35.485.375.765.535.675.485.265.145.385.275.755.646.266.16.326.186.286.145.745.75.475.316.226.425.816.015.375.875.945.725.124.955.835.825.816.15.615.695.215.434.95.055.655.835.594.895.565.795.575.665.026.074.614.924.944.795.154.744.495.265.54.825,120water pH, old waywater pH, new instr76.827.036.86.976.867.146.97.016.87.036.826.926.927.036.826.926.827.066.876.986.887.026.866.886.766.96.756.826.726.886.716.756.666.846.696.856.786.96.96.96.97.016.866.846.746.956.756.926.857.096.897.016.927.066.896.926.847.096.877.036.917.16.917.056.917.086.896.996.886.936.86.916.8576.856.866.736.876.76.766.676.886.766.86.696.936.936.936.937.056.876.916.817.016.856.866.86.976.96.947777.0277.177.067.17.0877.0776.996.96.966.97.0576.926.96.936.96.726.76.816.76.736.76.846.86.886.96.96.96.96.96.96.96.9576.946.96.9977.067.056.956.9777.047.027.066.9876.926.977.017.036.987.02776.987.0277.016.766.826.856.796.846.886.886.856.746.796.796.766.796.847.047.027.087.127.087.016.886.926.856.816.966.926.96.96.896.857.026.916.476.426.696.656.836.796.846.796.776.746.486.396.926.957.077.046.896.956.956.996.76.776.876.926.536.726.646.736.186.56.316.326.796.816.946.996.796.826.276.296.816.867.016.996.796.856.926.876.776.847.17.016.386.326.326.286.396.336.476.446.646.66.416.296.446.466.716.566.816.816.286.155,120SMP buffer pH, old wayKY buffer pH, new instrWater with soil-water pH was not hand-stirred for each sample. They were tray swirled.There is an issue with the last couple rows of the last tray in the group of 3 having erratic data for water pH because the tray wasn't set level. The probes probably didn't get fully immersed.The problem is proved because the erratic data at low water pH does not appear in the 5/120 timing where a set of 2 tray was run then a 1 tray was run.The orig Buff pH for5/30avg0.1146428571-1.48151.049610389630/30avg0.0760714286-1.77007142861.43552631585/600.0797857143-1.49421428571.551153846230/600.0822142857-1.59921428571.94844155845/1200.0716428571-1.43114285712.499480519530/1200.0367142857-1.25757142862.3629487179water pH>6.44 are calculated values MAXIMUM SAMPLE TIME WAS REALIZEDavg0.7084745763avg1.0771186441avg0avg1.4627118644avg0avg2.866779661SamNumpHBupHT1WT1BT2BT3Bstd0.0936407676std0.127461083std0std0.0812894061std0std0.325405418910015.795.58-9-91.45-95/105/105/305/305/605/6030/3030/30manual30/6030/6030/12030/120910027.267.59-9-91.45-9Original NAPT#SamNumOriginal pHOriginal 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pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instrEVERYTHING HAND STIRRED EXCEPT FOR ONE SET1.4166666667TRAY SWIRLEDwater pHbuf pHavg0.6116949153avg0.7745762712avg0.7350847458avg1.5772881356avg1.4898305085avg0avg2.866779661testavg timestdR2R2std0.1474124691std0.1565255451std0.1224866695std0.1187085853std0.1354005331std0std0.325405418# readings from stability = 3, pH stability = 0.01# readings from stability = 7, pH stability = 0.01# readings from stability = 7, pH stability = 0.01# readings from stability = 45, pH stability = 0.01# readings from stability = 22, pH stability = 0.01# readings from stability = 45, pH stability = 0.012/50.61169491530.14741246910.93070.9453SamNumpHBupHT1WT1BT2BT3B2/52/55/105/105/105/105/605/6030/3030/3030/6030/6030/12030/1205/100.77457627120.15652554510.97630.9607900015.736.15-9-91.03-9Original NAPT#SamNumOriginal pHOriginal 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pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000002, 5water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000002, 5SMP buffer pH, old wayKY buffer pH, new instr0000000000water pHbuffer pHtime to measure one water pH sample, minR2NAPT soils, hand stirred0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10 tray swilredwater pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10 tray swilredSMP buffer pH, old wayKY buffer pH, new instrTest of Routine setting for NAPT and LexRunning 3 trays takes about 1.5 hrshand stirred and tray swirledHAND STIRREDTRAY SWIRLEDHAND STIRREDTRAY SWIRLEDavg0.8881355932avg0.9133898305avg0.8403389831avg0.8416949153SamNumpHBupHT1WT1BT2BT3Bstd0.1535057512std0.1900662068std0.1724629637std0.1657219641900016.53-9# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02900025.16.13-9-91.12-9SamNumpHBupHT1WT1BT2BT3B5/605/605/605/60LEX soils5/605/605/605/60900036.791.28900015.736.15-9-91.03-9Original NAPT#SamNumOriginal pHOriginal BufferpHBupHT1WT1BT2BT3BpHBupHT1WT1BT2BT3BNew Lab #Original Lab #Original pHOriginal BufferpHBupHT1WT1BT2BT3BpHBupHT1WT1BT2BT3B900045.886.641.280.580.6847.6900027.777.48-9-91.03-998118910015.96.45.726.181.155.696.171.171176856.767.046.536.56900056.660.47900035.416.440.450.520.7242.9298119910027.857.57.717.481.157.797.511.172176875.336.165.16.131.125.166.171900066.440.47900046.477.160.450.520.7242.9298120910035.66.85.226.380.970.50.850.775.466.51.070.571.251.853177746.877.16.791.286.70.97900076.176.491.320.551.2746.12900057.117.40.450.50.6742.7798123910046.47.26.437.140.970.50.850.776.367.21.070.571.251.854177776.6775.886.641.280.580.6847.66.036.650.970.70.7347.93900085.236.431.320.551.2746.12900067.747.480.450.50.6742.7799101910058.017.517.717.390.850.530.7250.557.77.410.730.520.7551.675177796.727.026.660.476.660.48900094.645.910.850.580.6746900075.356.490.470.50.7342.5399101910068.017.517.857.490.850.530.7250.557.867.520.730.520.7551.676177806.77.016.440.476.470.48900104.565.990.850.580.6746900087.027.070.470.50.7342.5399106910075.16.365.366.490.730.650.8350.255.316.50.720.580.7851.47177836.226.556.176.491.320.551.2746.126.166.561.320.530.9346.7900114.555.881.120.530.745.88900096.947.130.750.50.7242.3299108910086.947.16.987.070.730.650.8350.256.987.110.720.580.7851.48177865.376.495.236.431.320.551.2746.125.256.41.320.530.9346.7900126.81.12900108.147.50.750.50.7242.3299110910097.457.36.487.130.970.580.8350.076.977.160.970.530.7751.229177884.75.944.645.910.850.580.67464.685.9910.80.8346.4900135.946.740.680.50.7545.67900117.527.281.030.480.7242.199111910108.387.568.137.510.970.580.8350.078.197.530.970.530.7751.2210177894.715.964.565.990.850.580.67464.596.0310.80.8346.4900146.580.68900127.267.171.030.480.7242.199115910117.727.397.497.281.150.520.7349.927.547.321.170.470.7750.9811177904.6264.555.881.120.530.745.884.555.9410.620.7346.47900155.246.450.80.520.8345.33900135.446.070.720.480.741.8899116910127.477.37.227.141.150.520.7349.927.137.211.170.470.7750.9812177916.897.116.81.126.741900166.890.8900147.857.480.720.480.741.8899117910135.456.35.546.040.80.580.7549.685.476.111.20.580.7250.7313177926.186.835.946.740.680.50.7545.675.936.780.730.720.546.58900175.776.541.270.770.8545900157.27.150.670.50.7341.6399118910147.97.57.917.490.80.580.7549.687.937.521.20.580.7250.7314177935.276.376.580.685.346.510.730.720.546.58900185.816.811.270.770.8545900165.726.330.670.50.7341.6399119910157.47.277.267.150.720.631.0249.257.237.160.750.570.8550.4715177956.697.015.246.450.80.520.8345.336.461900196.360.67900176.336.90.730.520.741.4399120910165.736.365.756.40.720.631.0249.255.756.410.750.570.8550.4716177986.897.116.890.86.731900205.936.660.670.520.7844.98900185.837.040.730.520.741.43101910176.576.396.930.830.670.9348.956.366.920.780.650.9350.117178026.016.465.776.541.270.770.85455.96.520.930.730.7345.7900214.955.720.70.520.744.8900197.677.450.720.50.7241.23102910185.77.195.917.090.830.670.9348.955.817.120.780.650.9350.118178116.086.775.816.811.270.770.85455.946.780.930.730.7345.7900226.970.7900207.317.450.720.50.7241.23103910197.867.57.687.450.830.50.7548.877.767.480.770.521.149.6519178136.596.966.360.676.390.83900235.085.990.750.50.7744.55900217.837.460.720.50.7241.02104910207.67.57.327.450.830.50.7548.877.347.470.770.521.149.6520178255.956.615.936.660.670.520.7844.985.926.610.830.630.8545.58900246.990.75900225.887.160.720.50.7241.021059102187.57.897.470.730.520.8848.487.917.490.770.50.7349.4321178305.055.994.955.720.70.520.744.84.95.690.730.520.7745.45900256.116.660.830.530.7344.32900236.376.850.70.50.7540.77106910225.77.165.827.120.730.520.8848.485.87.150.770.50.7349.4322178316.757.046.970.77.060.73900266.390.83900246.667.10.70.50.7540.77107910236.346.96.416.870.750.550.9248.086.396.90.720.551.0348.923178325.196.055.085.990.750.50.7744.555.155.890.50.520.7345.23900276.380.85900255.946.510.730.520.7340.53108910246.727.196.687.10.750.550.9248.086.687.10.720.551.0348.924178576.957.146.990.757.050.5900286.196.710.850.620.7844.07900266.997.330.730.520.7340.53109910255.956.625.886.541.020.530.9547.685.846.540.850.60.9748.4825178606.486.96.116.660.830.530.7344.326.136.610.870.530.7545900296.046.580.780.50.843.88900277.937.460.70.50.7340.32110910266.87.256.977.321.020.530.9547.687.037.360.850.60.9748.4826178736.466.896.390.836.410.87900305.446.590.780.50.843.88900284.566.430.70.50.7340.32111910278.277.527.797.430.930.551.1247.18.037.490.930.550.948.1827178786.496.916.380.856.40.73900315.596.410.70.620.7343.65900296.327.160.720.50.7240.1112910284.86.684.566.480.930.551.1247.14.516.430.930.550.948.1828178796.386.646.196.710.850.620.7844.076.236.670.730.50.7544.78900325.826.60.70.620.7343.65900305.687.060.720.50.7240.1113910295.557.136.317.150.750.580.7346.925.467.081.10.620.7547.9829178806.296.756.046.580.780.50.843.886.116.540.850.530.8844.4900336.420.77900315.826.850.720.470.7539.85114910305.77.175.537.060.750.580.7346.925.537.121.10.620.7547.9830179135.596.65.446.590.780.50.843.885.416.570.850.530.8844.4900346.066.70.770.550.8243.45900326.847.460.720.470.7539.85115910315.86.925.836.820.880.521.0746.435.726.830.730.471.1547.4531179845.856.545.596.410.70.620.7343.655.626.410.770.520.844.139/16/05900355.266.390.730.630.9343.07900335.376.390.750.520.7239.6116910324.276.30.880.521.0746.434.286.260.730.471.1547.4532179855.976.65.826.60.70.620.7343.655.816.550.770.520.844.13Good comparison of data with the settings of sample delay time = 5, # rdgs for stability=10, pH stability=0.02, max sample time = 60. (data above)900365.666.60.730.630.9343.07900346.566.960.750.520.7239.6117910335.326.365.346.430.920.571.0545.95.336.371.030.571.146.8233179946.336.836.420.776.470.73No difference between hand stirring and tray swirling.900376.056.90.780.680.7242.98900355.786.340.730.50.7339.38119910346.577.046.556.960.920.571.0545.96.456.91.030.571.146.8234179986.386.556.066.70.770.550.8243.456.116.70.730.550.7843.87There was also no difference between hand stirring and tray swirling for delay time = 5, # rdgs stability=7, pH stability=0.01, and max sample time = 10. (data not shown)900385.036.050.780.680.7242.98900364.796.420.730.50.7339.381209103566.595.786.340.950.60.9245.555.786.350.970.630.8346.5535180085.466.525.266.390.730.630.9343.075.26.380.750.550.943.52The differences observed between hand stirring and tray swirling in the NAPT samples with GA settings are due to just a couple of errant data. (data not shown)900395.826.570.80.520.7742.9900376.296.760.730.470.7539.131101910364.946.64.746.420.950.60.9245.554.746.440.970.630.8346.5536181745.666.595.666.60.730.630.9343.075.666.550.750.550.943.52I suggest moving to the setting in the first line above for routine analysis of soil with tray swirling. With this setting, 3 trays of 40 (120 samples) can be done in 1.5 hours.900406.530.8900387.517.450.730.470.7539.131102910376.46.916.36.791.120.580.8745.286.296.820.90.580.9346.2537181786.296.956.056.90.780.680.7242.986.046.870.750.70.743.37900415.316.50.730.50.9542.47900396.5970.720.521.0738.531103910387.77.57.617.461.120.580.8745.287.627.490.90.580.9346.2538181805.166.155.036.050.780.680.7242.985.056.050.750.70.743.37900426.296.540.730.50.9542.47900407.917.50.720.521.0738.531104910396.67.16.516.970.730.581.0844.786.557.010.750.751.1245.7239181966.126.635.826.570.80.520.7742.95.786.560.880.520.7843.289004356.190.820.850.8542.12900417.777.450.750.480.6738.381105910408.17.528.027.50.730.581.0844.788.047.530.750.751.1245.7240183096.957.146.530.86.570.88900445.816.410.820.850.8542.12900426.347.040.750.480.6738.381106910418.097.57.877.451.070.520.7344.637.917.481.150.480.7245.7541183105.316.655.316.50.730.50.9542.475.216.480.80.720.9242.88900455.366.270.930.530.742.27900435.16.520.720.480.6738.21107910426.4276.317.011.070.520.7344.636.237.031.150.480.7245.7542183146.376.636.296.540.730.50.9542.476.296.620.80.720.9242.88900466.237.390.930.530.742.27900445.87.090.720.480.6738.21108910435.376.615.16.541.050.581.3543.85.066.551.10.60.7345.543183165.046.2756.190.820.850.8542.1256.20.780.50.942.7900474.8260.720.650.7542.05900457.767.360.730.480.7537.931109910445.797.15.657.131.050.581.3543.85.617.121.10.60.7345.544183296.026.415.816.410.820.850.8542.125.876.440.780.50.942.7900485.566.270.720.650.7542.05900467.777.560.730.480.7537.931110910458.027.497.727.360.920.570.7543.637.887.40.830.60.7345.3745183305.496.255.366.270.930.530.742.275.346.20.90.50.8342.37900494.775.970.770.620.7241.98900477.817.470.750.430.7337.681111910468.247.597.737.550.920.570.7543.637.817.570.830.60.7345.3746183325.266.140.930.530.742.275.216.150.90.50.8342.37900505.476.410.770.620.7241.98900488.337.580.750.430.7337.681112910477.927.547.787.460.870.50.7743.437.857.490.930.50.7345.2347183405.126.224.8260.720.650.7542.054.825.990.70.50.7542.12900516.620.95900497.917.471.070.450.7237.41113910488.77.68.317.550.870.50.7743.438.517.60.930.50.7345.2348183475.766.385.566.270.720.650.7542.055.476.260.70.50.7542.12900525.176.560.950.680.741.9900507.557.451.070.450.7237.41114910498.17.547.887.461.080.520.7343.27.927.491.120.530.734549183495.056.054.775.970.770.620.7241.984.765.980.780.680.741.92900535.376.280.850.520.7741.82900517.917.470.670.470.7337.121115910507.767.477.557.461.080.520.7343.27.67.491.120.530.734550185025.626.295.476.410.770.620.7241.985.526.420.780.680.741.92900545.936.670.850.520.7741.82900527.737.370.670.470.7337.121116910518.17.517.897.460.730.480.7842.937.957.50.720.520.9544.5851185096.6776.620.956.670.92900555.786.590.70.480.941.43900537.717.460.670.480.6736.921117910527.867.497.747.40.730.480.7842.937.747.410.720.520.9544.5852185235.426.635.176.560.950.680.741.95.246.490.920.570.7341.87900564.746.030.70.480.941.43900545.86.830.670.480.6736.921118910538.027.57.687.441.350.520.7342.687.847.480.730.520.7544.3553185615.586.395.376.280.850.520.7741.825.46.270.90.570.7341.7900576.116.490.750.750.7841.13900554.76.430.750.470.7836.621119910545.36.75.746.811.350.520.7342.685.666.830.730.520.7544.3554185636.066.735.936.670.850.520.7741.825.966.680.90.570.7341.7900585.286.140.750.750.7841.13900566.36.960.750.470.7836.621120910554.726.64.616.40.750.551.2841.924.666.390.730.551.2343.6355185665.836.595.786.590.70.480.941.435.86.580.830.550.8741.4900595.876.480.720.550.7341.15900575.2960.730.50.736.382101910566.347.096.266.970.750.551.2841.926.287.010.730.551.2343.6356185694.926.24.746.030.70.480.941.434.746.040.830.550.8741.4900605.636.290.720.550.7341.15900586.417.080.730.50.736.382102910575.56.055.265.950.770.530.7841.685.256.010.730.580.7343.4557185726.216.556.116.490.750.750.7841.136.146.450.750.720.8341.12900615.696.430.70.620.8540.85900596.786.90.720.480.7236.172103910586.57.116.397.060.770.530.7841.686.417.10.730.580.7343.4558185795.96.675.286.140.750.750.7841.135.356.280.750.720.8341.12900626.136.590.70.620.8540.85900606.687.030.720.480.7236.172104910597.027.126.786.890.730.530.7841.436.786.910.730.530.8543.1859187125.916.485.876.480.720.550.7341.155.926.490.70.520.7741.07900636.246.670.770.50.8240.65900616.666.990.730.50.7235.932105910606.787.196.687.020.730.530.7841.436.687.050.730.530.8543.1860187135.816.295.636.290.720.550.7341.155.656.320.70.520.7741.07900646.276.740.770.50.8240.65900626.27.250.730.50.7235.932106910616.757.156.676.980.780.470.8741.16.770.950.630.8842.8361187165.736.345.696.430.70.620.8540.855.696.360.730.531.3840.2900655.696.470.90.580.7240.43900637.837.420.670.480.7535.682107910626.37.326.217.240.780.470.8741.16.177.280.950.630.8842.8362187186.336.536.136.590.70.620.8540.856.186.60.730.531.3840.2900665.126.450.90.580.7240.43900647.97.530.670.480.7535.682108910638.057.477.817.40.730.50.9340.637.917.450.750.50.942.5763187196.36.656.246.670.770.50.8240.656.316.70.730.480.839.93900676.176.90.780.471.0839.93900655.776.420.780.480.735.472109910648.167.57.887.530.730.50.9340.638.027.550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00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPTtray swilredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPTtray swirledSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPThand stirredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPThand stirredSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXtray swirledwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXtray swirledSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXhand stirredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXhand stirredSMP buffer pH, old wayKY buffer pH, new instrtimeelapsed timedayssecs11:18:50117:40:1811:18:50227:40:1811:20:04337:41:390:01:210.0009378111:20:04447:41:390:01:210.0009378111:21:18557:42:580:01:190.0009147911:21:18667:42:580:01:190.0009147911:22:33777:44:190:01:210.0009388111:22:33887:44:190:01:210.0009388111:23:45997:45:580:01:390.0011469911:23:4510107:45:580:01:390.0011469911:25:0211117:47:190:01:210.0009388111:25:0212127:47:190:01:210.0009388111:26:1613137:48:370:01:180.0009037811:26:1614147:48:370:01:180.0009037811:27:2915157:49:580:01:210.0009388111:27:2916167:49:580:01:210.0009388111:28:4317177:51:230:01:250.0009848511:28:4318187:51:230:01:250.0009848511:30:0019197:52:430:01:200.0009268011:30:0020207:52:430:01:200.0009268011:31:1321217:54:180:01:350.001100950:27:01time elapsed for a tray of water pH (40 samples)11:31:1322227:54:180:01:350.001100950:04:42time elapsed for a tray of buffer pH11:32:2623237:55:380:01:200.0009268011:32:2624247:55:380:01:200.000926801.55average min11:33:4025257:57:040:01:260.000995861.57average min11:33:4026267:57:040:01:260.0009958611:34:5127277:58:230:01:190.0009147911:34:5128287:58:230:01:190.0009147911:36:0529297:59:420:01:190.0009147911:36:0530307:59:420:01:190.0009147911:37:1731318:01:010:01:190.0009147911:37:1732328:01:010:01:190.0009147911:38:4933338:02:410:01:400.00115710011:38:4934348:02:410:01:400.00115710011:40:1735358:04:140:01:330.0010769311:40:1736368:04:140:01:330.0010769311:41:4737378:05:470:01:330.0010769311:41:4738388:05:470:01:330.0010769311:43:1739398:07:190:01:320.0010659211:43:1740408:07:190:01:320.0010659211:44:471418:09:000:01:410.00116910111:44:472428:09:000:01:410.00116910111:46:163438:10:350:01:350.0011009511:46:164448:10:350:01:350.0011009511:47:445458:12:090:01:340.0010889411:47:446468:12:090:01:340.0010889411:49:137478:13:420:01:330.0010769311:49:138488:13:420:01:330.0010769311:50:419498:15:220:01:400.00115710011:50:4110508:15:220:01:400.00115710011:52:0911518:16:540:01:320.0010659211:52:0912528:16:540:01:320.0010659211:53:3613538:18:270:01:330.0010769311:53:3614548:18:270:01:330.0010769311:55:0415558:20:010:01:340.0010889411:55:0416568:20:010:01:340.0010889411:56:3317578:21:420:01:410.00116910111:56:3318588:21:420:01:410.00116910111:58:0219598:23:170:01:350.0011009511:58:0220608:23:170:01:350.0011009511:59:2821618:24:500:01:330.0010769311:59:2822628:24:500:01:330.0010769312:00:5523638:26:240:01:340.0010889412:00:5524648:26:240:01:340.0010889412:02:2325658:28:050:01:410.00116910112:02:2326668:28:050:01:410.00116910112:03:5227678:29:400:01:350.0011009512:03:5228688:29:400:01:350.0011009512:05:2029698:31:140:01:340.0010889412:05:2030708:31:140:01:340.0010889412:06:4731718:32:490:01:350.0011009512:06:4732728:32:490:01:350.0011009512:08:1733738:34:300:01:410.00116910112:08:1734748:34:300:01:410.00116910112:09:4635758:36:050:01:350.0011009512:09:4636768:36:050:01:350.0011009512:11:1437778:37:380:01:330.0010769312:11:1438788:37:380:01:330.0010769312:12:4339798:39:140:01:360.0011119612:12:4340808:39:140:01:360.0011119612:14:421818:41:450:02:310.00174815112:14:422828:41:450:02:310.00174815112:16:103838:43:220:01:370.0011239712:16:104848:43:220:01:370.0011239712:17:395858:44:570:01:350.0011009512:17:396868:44:570:01:350.0011009512:19:087878:46:320:01:350.0011009512:19:088888:46:320:01:350.0011009512:20:389898:48:120:01:400.00115710012:20:3810908:48:120:01:400.00115710012:22:0511918:49:470:01:350.0011009512:22:0512928:49:470:01:350.0011009512:23:3213938:51:220:01:350.0011009512:23:3214948:51:220:01:350.0011009512:25:0115958:52:560:01:340.0010889412:25:0116968:52:560:01:340.0010889412:26:3117978:54:370:01:410.00116910112:26:3118988:54:370:01:410.00116910112:28:0119998:56:120:01:350.0011009512:28:01201008:56:120:01:350.0011009512:29:28211018:57:310:01:190.0009147912:29:28221028:57:310:01:190.0009147912:30:56231038:59:060:01:350.0011009512:30:56241048:59:060:01:350.0011009512:32:27251059:00:470:01:410.00116910112:32:27261069:00:470:01:410.00116910112:33:57271079:02:220:01:350.0011009512:33:57281089:02:220:01:350.0011009512:35:26291099:03:570:01:350.0011009512:35:26301109:03:570:01:350.0011009512:36:55311119:05:300:01:330.0010769312:36:55321129:05:300:01:330.0010769312:38:25331139:07:110:01:410.00116910112:38:25341149:07:110:01:410.00116910112:39:54351159:08:480:01:370.0011239712:39:54361169:08:480:01:370.0011239712:41:21371179:10:210:01:330.0010769312:41:21381189:10:210:01:330.0010769312:42:50391199:11:560:01:350.0011009512:42:50401209:11:560:01:350.0011009512:51:46buffbegins1219:19:290:07:330.00524345312:51:46261229:21:010:09:050.00630854512:53:01271239:22:310:03:020.00210618212:53:01281249:22:310:01:300.0010429012:54:17291259:23:510:01:200.0009268012:54:17301269:23:510:01:200.0009268012:55:32321279:25:120:01:210.0009388112:55:32331289:25:120:01:210.0009388112:56:48341299:26:310:01:190.0009147912:56:48351309:27:570:02:450.00191016512:58:04361319:27:570:01:260.0009958612:58:04371329:29:170:01:200.0009268012:59:19381339:29:170:01:200.0009268012:59:19391349:30:370:01:200.000926801:00:34401359:30:370:01:200.000926801:00:3411369:31:580:01:210.000937811:01:5021379:31:580:01:210.000937811:01:5031389:33:250:01:270.001007871:03:0561399:33:250:01:270.001007871:03:0571409:34:450:01:200.000926801:04:1981419:36:050:02:400.0018521601:04:1991429:37:250:02:400.0018521601:05:33101439:37:250:01:200.000926801:05:33111449:38:490:01:240.000972841:06:49121459:38:490:01:240.000972841:06:49131469:40:090:01:200.000926801:08:04141479:40:090:01:200.000926801:08:04151489:41:290:01:200.000926801:09:19161499:41:290:01:200.000926801:09:19171509:42:500:01:210.000937811:10:33181519:42:500:01:210.000937811:10:33191529:44:150:01:250.000984851:11:49201539:44:150:01:250.000984851:11:49211549:45:350:01:200.000926801:13:04221559:45:350:01:200.000926801:13:04231569:46:560:01:210.000937811:14:18241579:46:560:01:210.000937811:14:18251589:48:160:01:200.000926801:15:33261599:48:160:01:200.000926801:15:33271609:49:430:01:270.001007871:16:50301619:49:430:01:270.001007871:16:50311629:51:040:01:210.000937811:18:06321639:52:230:02:400.0018521601:18:06331649:53:440:02:400.0018521601:19:21341659:53:440:01:210.000937811:19:21351669:55:090:01:250.000984851:20:37361679:55:090:01:250.000984851:20:37371689:56:300:01:210.000937811:21:54381699:56:300:01:210.000937811:21:54391709:57:430:01:130.000845731:23:10401719:57:430:01:130.000845731:23:1011729:58:530:01:100.000810701:24:2521739:58:530:01:100.000810701:24:25317410:00:190:01:260.000995861:25:41417510:00:190:01:260.000995861:25:41517610:01:390:01:200.000926801:26:58617710:01:390:01:200.000926801:26:58717810:02:580:01:190.000914791:28:14817910:02:580:01:190.000914791:28:14918010:04:190:01:210.000937811:29:301018110:04:190:01:210.000937811:29:301118210:05:460:01:270.001007871:30:451518310:05:460:01:270.001007871:30:451618410:07:070:01:210.000937811:32:021718510:08:330:02:470.0019331671:32:021818610:08:330:01:260.000995861:33:171918710:09:580:01:250.000984851:33:172018810:09:580:01:250.000984851:34:332118910:11:180:01:200.000926801:35:492219010:11:180:01:200.000926801:35:492319110:12:370:01:190.000914791:37:062419210:12:370:01:190.000914791:37:062519310:14:380:02:010.0014001211:38:212619410:14:380:02:010.0014001211:38:212719510:16:050:01:270.001007871:39:372819610:16:050:01:270.001007871:39:372919710:17:250:01:200.000926801:40:523019810:17:250:01:200.000926801:40:523119910:19:430:02:180.0015971381:42:383220010:19:430:02:180.0015971381:42:383320110:21:000:01:170.000891771:43:533420210:21:000:01:170.000891771:43:533520310:22:260:01:260.000995861:45:093620410:22:260:01:260.000995861:45:093720510:23:470:01:210.000938811:46:263820610:23:470:01:210.000938811:46:263920710:25:010:01:140.000856741:47:434020810:25:010:01:140.000856741:47:4310:26:221:48:5810:26:221:48:5810:32:181:50:141:50:141:50:141:50:141:51:291:51:291:51:291:51:290000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000elapsed time (secs)30,60 setting602171121711123171231723125231251625611.030.9712411811.030.972666217171717171172323123223232323131313131131621.0310.971241.0310.97Soil pH, LabFit instrumentSoil pH, LabFit instrumentSoil pH, NAPT medianSoil pH, NAPT medianEach sample stirred with stir rod for 5 sec and let set for 30 min.Tray swirled for 5 sec. and let set for 30 min.1:1 lineregression lineSoil pHChart55.735.97.777.855.415.66.476.47.118.017.748.015.355.17.026.946.947.458.148.387.527.727.267.475.445.457.857.97.27.45.725.736.336.55.835.77.677.867.317.67.8385.885.76.376.346.666.725.945.956.996.87.938.274.564.86.325.555.685.75.825.84.274.275.375.326.566.575.7864.794.946.296.47.517.76.596.67.918.17.778.096.346.425.15.375.85.797.768.027.778.247.817.928.338.77.918.17.557.767.918.17.737.867.718.025.85.34.74.726.36.345.295.56.416.56.787.026.686.786.666.756.26.37.838.057.98.165.775.547.787.817.227.736.836.856.9675.715.635.915.746.686.787.117.76.266.45.015.15.986.265.785.917.627.94.64.666.596.15.686.16.066.035.555.59.239.366.466.56.236.26.446.487.417.66.116.16.746.835.865.855.985.866.196.296.435.967.237.568.388.526.416.497.757.95.765.845.735.87.988.246.847.15.625.524.864.827.67.95.445.915.85.385.525.767.357.47.467.76.36.486.155.97.167.765.715.855.575.647.497.857.557.94.564.557.627.765,10 tray swilredwater pH, old waywater pH, new instr120+ Pri Farmer SamplesWater with soil-water pH was not hand-stirred for each sample. They were tray swirled.There isan issue with the last couple rows of the last tray in the group of 3 having erratic data for water pH because the tray wasn't set level. The probes probably didn't get fully immersed.The problem is proved because the erratic data at low water pH does not appear in the 5/120 timing where a set of 2 tray was run then a 1 tray was run.5/30avg0.127875-1.30031251.049610389630/30avg0.0834375-1.9881.43552631585/600.0913125-1.3141251.551153846230/600.0961875-1.40606251.94844155845/1200.0785-1.25381252.499480519530/1200.0595625-1.1066252.3629487179std0.21014037692.71291841320.1546697224std0.20700635573.15071496330.12672538740.11899009992.76385711420.16033819720.12175277492.82238515860.16471059930.10208024962.73864399070.3746262490.13483904632.57797928950.4609866249*notice the switching of 30/120 and 5/120 so time could be in orderLab# for Lex analysisNew Lab #Original Lab #Sample #Original pHOriginal BufferpH_2**Buffer_2**delta pHdelta BupHT1WT1BT2BT3BpH_1*Buffer_1*delta pHdelta BupHT1WT1BT2BT3BpH_4****Buffer_4****delta pHdelta BupHT1WT1BT2BT3BpH_3***Buffer_3***delta pHdelta BupHT1WT1BT2BT3BpH_6^^Buffer_6^^delta pHdelta BupHT1WT1BT2BT3BpH_5^Buffer_5^delta pHdelta BupHT1WT1BT2BT3BSETTINGTimeSetLagDiffTIMETIMETimewoLagstdevR2avg diffstd diff1900016238516016.46.876.590.19-6.876.550.15-6.876.620.22-6.876.650.25-6.876.580.18-6.876.440.04-6.87(sec)(sec)(sec)(min)(min)2900026238616026.436.886.490.06-6.886.41-0.02-6.886.277.06-0.160.181.356.38-0.05-6.886.347.1-0.090.222.756.247.07-0.190.192.355/303528631.050.60.130.7940.1278750.21014037693900036238716036.787.056.63-0.15-7.050.826.820.04-7.051.236.80.02-7.051.356.850.07-7.051.756.77-0.01-7.052.756.72-0.06-7.052.3730/306026.486.41.440.990.150.8030.08343750.20700635574900046238816046.556.946.560.01-6.940.826.560.01-6.941.236.610.06-6.941.356.790.24-6.941.756.740.19-6.942.756.580.03-6.942.375/606528931.551.10.160.9350.09131250.11899009995900056238916056.757.046.790.04-7.040.886.960.21-7.041.236.940.19-7.041.326.950.2-7.041.776.910.16-7.042.776.820.07-7.042.3530/6090271171.951.50.160.9360.09618750.12175277496900066239016066.6876.790.11-70.886.810.13-71.236.790.11-71.326.930.25-71.776.780.1-72.776.730.05-72.35*30/120150-8.4141.62.361.910.460.920.05956250.13483904637900076239116076.787.056.77-0.01-7.050.826.880.1-7.051.256.910.13-7.051.356.80.02-7.051.756.73-0.05-7.052.776.68-0.1-7.052.35*5/120125251502.52.050.370.9570.07850.10208024968900086239216086.97.116.85-0.05-7.110.826.930.03-7.111.256.920.02-7.111.356.990.09-7.111.756.84-0.06-7.112.776.81-0.09-7.112.359900096788517016.316.896.630.32-6.890.976.730.42-6.891.26.630.32-6.891.656.610.3-6.891.876.450.14-6.893.086.440.13-6.892.68For next run of samples add a shorter time and drop one of the longer times10900106788617026.276.936.710.44-6.930.976.810.54-6.931.26.530.26-6.931.656.660.39-6.931.876.490.22-6.933.086.490.22-6.932.685/10, 5/30, 30/30, 5/60, 30/60, 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Settings for pH_1 & Buffer_1** Settings for pH_2 & Buffer_2^ Settings for pH_5 & Buffer_5File Name 0130.rckFile Name #4 0130 71305.rckFile Name 1120 JULY192005.RCKSample delay time 30Sample delay time 5Sample delay time 30# rdgs for stability 45# rdgs for stability 45# rdgs for stability 45pH stability 0.01pH stability 0.01pH stability 0.01Maximum sample time 30Maximum sample time 30Maximum sample time 120* Buffer did not get stirred- stirrer came out*** Settings for pH_3 & Buffer_3****Settings for pH_4 & Buffer_4^ ^Settings for pH_6 & Buffer_6File Name 0160 July 13 2005.rckFile Name 0160 JULY142005.RCKFile Name JULY182005 1120.RCK & 1121 71805.RCKSample delay time 30Sample delay time 5Sample delay time 5# rdgs for stability 45# rdgs for stability 45# rdgs for stability 45pH stability 0.01pH stability 0.01pH stability 0.01Maximium sample time 60Maximum sample time 60Maximum sample time 120120+ Pri Farmer Samples0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr120+Pri Farmer Samples woL2Rows0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,60int ND 0slope ND 1water pH, old waywater pH, new instrSamplesFromLex0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instrLexSoilData0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,60SMP buffer pH, old wayKY buffer pH, new instrLexSoilData (2)0.7940.1278750.21014037690.8030.08343750.20700635570.9350.09131250.11899009990.9360.09618750.12175277490.920.05956250.13483904630.9570.07850.1020802496manualReadings6.446.46.246.436.726.786.586.556.826.756.736.686.686.786.816.96.446.316.496.276.376.196.386.146.656.416.235.956.516.326.616.236.556.546.36.236.56.56.516.356.496.466.356.246.586.446.666.56.065.946.096.045.975.956.276.236.26.076.096.056.356.365.945.885.895.836.0766.126.056.055.975.85.725.815.715.675.755.565.475.435.45.645.545.975.876.356.226.426.316.296.175.825.775.895.775.865.866.326.36.126.16.026.025.645.616.286.246.076.096.286.226.216.226.216.116.036.015.795.685.895.886.096.025.75.645.645.535.325.295.735.635.685.626.46.36.396.316.276.1565.975.765.725.585.55.85.85.835.85.755.65.955.96.226.16.216.26.035.96.176.15.835.86.0266.065.95.765.75.825.75.255.25.425.35.225.25.665.65.95.86.486.56.476.46.496.46.16.15.885.86.115.96.136.025.945.845.935.86.0766.015.895.875.736.065.896.095.996.055.786.196.096.115.935.695.35.685.375.875.535.815.485.745.145.725.275.825.646.046.16.126.186.156.145.945.75.825.316.26.345.745.85.455.635.895.565.054.855.755.765.775.995.635.715.185.364.684.955.615.795.684.885.545.845.565.634.966.054.664.884.854.755.174.774.495.275.474.830,120water pH, old waywater pH, new instrNAPTsoils6.966.826.996.86.946.867.116.96.986.876.827.076.926.986.826.886.827.016.876.926.886.986.866.856.766.886.756.776.726.826.716.76.666.766.696.796.787.026.96.96.96.966.866.796.746.866.756.886.857.046.896.946.927.036.896.886.847.066.876.966.917.066.917.026.917.036.896.956.886.866.86.866.856.936.856.796.736.826.76.726.676.836.766.716.696.936.936.936.936.986.876.876.816.966.856.816.86.96.96.8776.9676.9477.0577.017.17.0377.0376.976.96.926.97.0176.856.96.96.96.686.76.776.76.666.76.786.86.836.96.96.96.96.96.96.96.9376.926.96.9476.987.056.886.976.937.046.987.066.9376.886.976.967.036.957.026.9376.947.026.967.016.736.826.86.796.826.886.856.856.76.796.776.766.766.847.037.027.047.127.037.016.856.926.816.816.966.926.986.96.886.857.016.916.476.426.76.656.816.796.836.796.766.746.496.396.936.957.067.046.896.956.956.996.696.776.886.926.526.726.636.736.196.56.226.326.776.816.956.996.796.826.266.296.836.867.016.996.786.856.96.876.746.847.087.016.46.326.316.286.376.336.496.446.616.66.396.296.436.466.76.566.86.816.246.1530,120SMP buffer pH, old wayKY buffer pH, new instrNAPTsoils (2)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30water pH, old waywater pH, new instrNAPT&LEX_rouSet000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30SMP buffer pH, old wayKY buffer pH, new instrelapsedTime_template00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60water pH, old waywater pH, new instrSheet1000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60SMP buffer pH, old wayKY buffer pH, new instr6.586.46.346.436.776.786.746.556.916.756.786.686.736.786.846.96.456.316.496.276.426.196.496.146.626.416.225.956.556.326.666.236.566.546.326.236.56.56.516.356.426.466.426.246.566.446.716.56.085.946.16.046.085.956.326.236.146.076.076.056.446.365.985.885.885.836.0866.146.056.075.975.865.725.855.715.645.755.65.475.485.45.715.5465.876.416.226.426.316.316.175.915.775.915.775.875.866.356.36.166.16.066.025.75.616.316.246.096.096.316.226.256.226.256.116.056.015.795.685.945.886.16.025.715.645.665.535.365.295.745.635.75.626.46.36.446.316.336.156.055.975.785.725.615.55.825.85.865.85.755.65.995.96.266.16.266.26.065.96.236.15.855.86.0366.135.95.865.75.845.75.275.25.475.35.265.25.685.65.955.86.496.56.556.46.516.46.126.15.895.86.095.96.136.025.915.845.865.86.1365.995.895.835.736.025.896.115.995.945.786.166.096.025.935.425.35.485.375.765.535.675.485.265.145.385.275.755.646.266.16.326.186.286.145.745.75.475.316.226.425.816.015.375.875.945.725.124.955.835.825.816.15.615.695.215.434.95.055.655.835.594.895.565.795.575.665.026.074.614.924.944.795.154.744.495.265.54.825,120water pH, old waywater pH, new instr76.827.036.86.976.867.146.97.016.87.036.826.926.927.036.826.926.827.066.876.986.887.026.866.886.766.96.756.826.726.886.716.756.666.846.696.856.786.96.96.96.97.016.866.846.746.956.756.926.857.096.897.016.927.066.896.926.847.096.877.036.917.16.917.056.917.086.896.996.886.936.86.916.8576.856.866.736.876.76.766.676.886.766.86.696.936.936.936.937.056.876.916.817.016.856.866.86.976.96.947777.0277.177.067.17.0877.0776.996.96.966.97.0576.926.96.936.96.726.76.816.76.736.76.846.86.886.96.96.96.96.96.96.96.9576.946.96.9977.067.056.956.9777.047.027.066.9876.926.977.017.036.987.02776.987.0277.016.766.826.856.796.846.886.886.856.746.796.796.766.796.847.047.027.087.127.087.016.886.926.856.816.966.926.96.96.896.857.026.916.476.426.696.656.836.796.846.796.776.746.486.396.926.957.077.046.896.956.956.996.76.776.876.926.536.726.646.736.186.56.316.326.796.816.946.996.796.826.276.296.816.867.016.996.796.856.926.876.776.847.17.016.386.326.326.286.396.336.476.446.646.66.416.296.446.466.716.566.816.816.286.155,120SMP buffer pH, old wayKY buffer pH, new instrWater with soil-water pH was not hand-stirred for each sample. They were tray swirled.There is an issue with the last couple rows of the last tray in the group of 3 having erratic data for water pH because the tray wasn't set level. The probes probably didn't get fully immersed.The problem is proved because the erratic data at low water pH does not appear in the 5/120 timing where a set of 2 tray was run then a 1 tray was run.The orig Buff pH for5/30avg0.1146428571-1.48151.049610389630/30avg0.0760714286-1.77007142861.43552631585/600.0797857143-1.49421428571.551153846230/600.0822142857-1.59921428571.94844155845/1200.0716428571-1.43114285712.499480519530/1200.0367142857-1.25757142862.3629487179water pH>6.44 are calculated values MAXIMUM SAMPLE TIME WAS REALIZEDavg0.7084745763avg1.0771186441avg0avg1.4627118644avg0avg2.866779661SamNumpHBupHT1WT1BT2BT3Bstd0.0936407676std0.127461083std0std0.0812894061std0std0.325405418910015.795.58-9-91.45-95/105/105/305/305/605/6030/3030/30manual30/6030/6030/12030/120910027.267.59-9-91.45-9Original NAPT#SamNumOriginal pHOriginal 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pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instrEVERYTHING HAND STIRRED EXCEPT FOR ONE SET1.4166666667TRAY SWIRLEDwater pHbuf pHavg0.6116949153avg0.7745762712avg0.7350847458avg1.5772881356avg1.4898305085avg0avg2.866779661testavg timestdR2R2std0.1474124691std0.1565255451std0.1224866695std0.1187085853std0.1354005331std0std0.325405418# readings from stability = 3, pH stability = 0.01# readings from stability = 7, pH stability = 0.01# readings from stability = 7, pH stability = 0.01# readings from stability = 45, pH stability = 0.01# readings from stability = 22, pH stability = 0.01# readings from stability = 45, pH stability = 0.012/50.61169491530.14741246910.93070.9453SamNumpHBupHT1WT1BT2BT3B2/52/55/105/105/105/105/605/6030/3030/3030/6030/6030/12030/1205/100.77457627120.15652554510.97630.9607900015.736.15-9-91.03-9Original NAPT#SamNumOriginal pHOriginal 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pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,30SMP buffer pH, old wayKY buffer pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120water pH, old waywater pH, new instr00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000030,120SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000002, 5water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000002, 5SMP buffer pH, old wayKY buffer pH, new instr0000000000water pHbuffer pHtime to measure one water pH sample, minR2NAPT soils, hand stirred0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60water pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,60SMP buffer pH, old wayKY buffer pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10 tray swilredwater pH, old waywater pH, new instr0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000005,10 tray swilredSMP buffer pH, old wayKY buffer pH, new instrTest of Routine setting for NAPT and LexRunning 3 trays takes about 1.5 hrshand stirred and tray swirledHAND STIRREDTRAY SWIRLEDHAND STIRREDTRAY SWIRLEDavg0.8881355932avg0.9133898305avg0.8403389831avg0.8416949153SamNumpHBupHT1WT1BT2BT3Bstd0.1535057512std0.1900662068std0.1724629637std0.1657219641900016.53-9# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02# readings from stability = 10, pH stability = 0.02900025.16.13-9-91.12-9SamNumpHBupHT1WT1BT2BT3B5/605/605/605/60LEX soils5/605/605/605/60900036.791.28900015.736.15-9-91.03-9Original NAPT#SamNumOriginal pHOriginal BufferpHBupHT1WT1BT2BT3BpHBupHT1WT1BT2BT3BNew Lab #Original Lab #Original pHOriginal BufferpHBupHT1WT1BT2BT3BpHBupHT1WT1BT2BT3B900045.886.641.280.580.6847.6900027.777.48-9-91.03-998118910015.96.45.726.181.155.696.171.171176856.767.046.536.56900056.660.47900035.416.440.450.520.7242.9298119910027.857.57.717.481.157.797.511.172176875.336.165.16.131.125.166.171900066.440.47900046.477.160.450.520.7242.9298120910035.66.85.226.380.970.50.850.775.466.51.070.571.251.853177746.877.16.791.286.70.97900076.176.491.320.551.2746.12900057.117.40.450.50.6742.7798123910046.47.26.437.140.970.50.850.776.367.21.070.571.251.854177776.6775.886.641.280.580.6847.66.036.650.970.70.7347.93900085.236.431.320.551.2746.12900067.747.480.450.50.6742.7799101910058.017.517.717.390.850.530.7250.557.77.410.730.520.7551.675177796.727.026.660.476.660.48900094.645.910.850.580.6746900075.356.490.470.50.7342.5399101910068.017.517.857.490.850.530.7250.557.867.520.730.520.7551.676177806.77.016.440.476.470.48900104.565.990.850.580.6746900087.027.070.470.50.7342.5399106910075.16.365.366.490.730.650.8350.255.316.50.720.580.7851.47177836.226.556.176.491.320.551.2746.126.166.561.320.530.9346.7900114.555.881.120.530.745.88900096.947.130.750.50.7242.3299108910086.947.16.987.070.730.650.8350.256.987.110.720.580.7851.48177865.376.495.236.431.320.551.2746.125.256.41.320.530.9346.7900126.81.12900108.147.50.750.50.7242.3299110910097.457.36.487.130.970.580.8350.076.977.160.970.530.7751.229177884.75.944.645.910.850.580.67464.685.9910.80.8346.4900135.946.740.680.50.7545.67900117.527.281.030.480.7242.199111910108.387.568.137.510.970.580.8350.078.197.530.970.530.7751.2210177894.715.964.565.990.850.580.67464.596.0310.80.8346.4900146.580.68900127.267.171.030.480.7242.199115910117.727.397.497.281.150.520.7349.927.547.321.170.470.7750.9811177904.6264.555.881.120.530.745.884.555.9410.620.7346.47900155.246.450.80.520.8345.33900135.446.070.720.480.741.8899116910127.477.37.227.141.150.520.7349.927.137.211.170.470.7750.9812177916.897.116.81.126.741900166.890.8900147.857.480.720.480.741.8899117910135.456.35.546.040.80.580.7549.685.476.111.20.580.7250.7313177926.186.835.946.740.680.50.7545.675.936.780.730.720.546.58900175.776.541.270.770.8545900157.27.150.670.50.7341.6399118910147.97.57.917.490.80.580.7549.687.937.521.20.580.7250.7314177935.276.376.580.685.346.510.730.720.546.58900185.816.811.270.770.8545900165.726.330.670.50.7341.6399119910157.47.277.267.150.720.631.0249.257.237.160.750.570.8550.4715177956.697.015.246.450.80.520.8345.336.461900196.360.67900176.336.90.730.520.741.4399120910165.736.365.756.40.720.631.0249.255.756.410.750.570.8550.4716177986.897.116.890.86.731900205.936.660.670.520.7844.98900185.837.040.730.520.741.43101910176.576.396.930.830.670.9348.956.366.920.780.650.9350.117178026.016.465.776.541.270.770.85455.96.520.930.730.7345.7900214.955.720.70.520.744.8900197.677.450.720.50.7241.23102910185.77.195.917.090.830.670.9348.955.817.120.780.650.9350.118178116.086.775.816.811.270.770.85455.946.780.930.730.7345.7900226.970.7900207.317.450.720.50.7241.23103910197.867.57.687.450.830.50.7548.877.767.480.770.521.149.6519178136.596.966.360.676.390.83900235.085.990.750.50.7744.55900217.837.460.720.50.7241.02104910207.67.57.327.450.830.50.7548.877.347.470.770.521.149.6520178255.956.615.936.660.670.520.7844.985.926.610.830.630.8545.58900246.990.75900225.887.160.720.50.7241.021059102187.57.897.470.730.520.8848.487.917.490.770.50.7349.4321178305.055.994.955.720.70.520.744.84.95.690.730.520.7745.45900256.116.660.830.530.7344.32900236.376.850.70.50.7540.77106910225.77.165.827.120.730.520.8848.485.87.150.770.50.7349.4322178316.757.046.970.77.060.73900266.390.83900246.667.10.70.50.7540.77107910236.346.96.416.870.750.550.9248.086.396.90.720.551.0348.923178325.196.055.085.990.750.50.7744.555.155.890.50.520.7345.23900276.380.85900255.946.510.730.520.7340.53108910246.727.196.687.10.750.550.9248.086.687.10.720.551.0348.924178576.957.146.990.757.050.5900286.196.710.850.620.7844.07900266.997.330.730.520.7340.53109910255.956.625.886.541.020.530.9547.685.846.540.850.60.9748.4825178606.486.96.116.660.830.530.7344.326.136.610.870.530.7545900296.046.580.780.50.843.88900277.937.460.70.50.7340.32110910266.87.256.977.321.020.530.9547.687.037.360.850.60.9748.4826178736.466.896.390.836.410.87900305.446.590.780.50.843.88900284.566.430.70.50.7340.32111910278.277.527.797.430.930.551.1247.18.037.490.930.550.948.1827178786.496.916.380.856.40.73900315.596.410.70.620.7343.65900296.327.160.720.50.7240.1112910284.86.684.566.480.930.551.1247.14.516.430.930.550.948.1828178796.386.646.196.710.850.620.7844.076.236.670.730.50.7544.78900325.826.60.70.620.7343.65900305.687.060.720.50.7240.1113910295.557.136.317.150.750.580.7346.925.467.081.10.620.7547.9829178806.296.756.046.580.780.50.843.886.116.540.850.530.8844.4900336.420.77900315.826.850.720.470.7539.85114910305.77.175.537.060.750.580.7346.925.537.121.10.620.7547.9830179135.596.65.446.590.780.50.843.885.416.570.850.530.8844.4900346.066.70.770.550.8243.45900326.847.460.720.470.7539.85115910315.86.925.836.820.880.521.0746.435.726.830.730.471.1547.4531179845.856.545.596.410.70.620.7343.655.626.410.770.520.844.139/16/05900355.266.390.730.630.9343.07900335.376.390.750.520.7239.6116910324.276.30.880.521.0746.434.286.260.730.471.1547.4532179855.976.65.826.60.70.620.7343.655.816.550.770.520.844.13Good comparison of data with the settings of sample delay time = 5, # rdgs for stability=10, pH stability=0.02, max sample time = 60. (data above)900365.666.60.730.630.9343.07900346.566.960.750.520.7239.6117910335.326.365.346.430.920.571.0545.95.336.371.030.571.146.8233179946.336.836.420.776.470.73No difference between hand stirring and tray swirling.900376.056.90.780.680.7242.98900355.786.340.730.50.7339.38119910346.577.046.556.960.920.571.0545.96.456.91.030.571.146.8234179986.386.556.066.70.770.550.8243.456.116.70.730.550.7843.87There was also no difference between hand stirring and tray swirling for delay time = 5, # rdgs stability=7, pH stability=0.01, and max sample time = 10. (data not shown)900385.036.050.780.680.7242.98900364.796.420.730.50.7339.381209103566.595.786.340.950.60.9245.555.786.350.970.630.8346.5535180085.466.525.266.390.730.630.9343.075.26.380.750.550.943.52The differences observed between hand stirring and tray swirling in the NAPT samples with GA settings are due to just a couple of errant data. (data not shown)900395.826.570.80.520.7742.9900376.296.760.730.470.7539.131101910364.946.64.746.420.950.60.9245.554.746.440.970.630.8346.5536181745.666.595.666.60.730.630.9343.075.666.550.750.550.943.52I suggest moving to the setting in the first line above for routine analysis of soil with tray swirling. With this setting, 3 trays of 40 (120 samples) can be done in 1.5 hours.900406.530.8900387.517.450.730.470.7539.131102910376.46.916.36.791.120.580.8745.286.296.820.90.580.9346.2537181786.296.956.056.90.780.680.7242.986.046.870.750.70.743.37900415.316.50.730.50.9542.47900396.5970.720.521.0738.531103910387.77.57.617.461.120.580.8745.287.627.490.90.580.9346.2538181805.166.155.036.050.780.680.7242.985.056.050.750.70.743.37900426.296.540.730.50.9542.47900407.917.50.720.521.0738.531104910396.67.16.516.970.730.581.0844.786.557.010.750.751.1245.7239181966.126.635.826.570.80.520.7742.95.786.560.880.520.7843.289004356.190.820.850.8542.12900417.777.450.750.480.6738.381105910408.17.528.027.50.730.581.0844.788.047.530.750.751.1245.7240183096.957.146.530.86.570.88900445.816.410.820.850.8542.12900426.347.040.750.480.6738.381106910418.097.57.877.451.070.520.7344.637.917.481.150.480.7245.7541183105.316.655.316.50.730.50.9542.475.216.480.80.720.9242.88900455.366.270.930.530.742.27900435.16.520.720.480.6738.21107910426.4276.317.011.070.520.7344.636.237.031.150.480.7245.7542183146.376.636.296.540.730.50.9542.476.296.620.80.720.9242.88900466.237.390.930.530.742.27900445.87.090.720.480.6738.21108910435.376.615.16.541.050.581.3543.85.066.551.10.60.7345.543183165.046.2756.190.820.850.8542.1256.20.780.50.942.7900474.8260.720.650.7542.05900457.767.360.730.480.7537.931109910445.797.15.657.131.050.581.3543.85.617.121.10.60.7345.544183296.026.415.816.410.820.850.8542.125.876.440.780.50.942.7900485.566.270.720.650.7542.05900467.777.560.730.480.7537.931110910458.027.497.727.360.920.570.7543.637.887.40.830.60.7345.3745183305.496.255.366.270.930.530.742.275.346.20.90.50.8342.37900494.775.970.770.620.7241.98900477.817.470.750.430.7337.681111910468.247.597.737.550.920.570.7543.637.817.570.830.60.7345.3746183325.266.140.930.530.742.275.216.150.90.50.8342.37900505.476.410.770.620.7241.98900488.337.580.750.430.7337.681112910477.927.547.787.460.870.50.7743.437.857.490.930.50.7345.2347183405.126.224.8260.720.650.7542.054.825.990.70.50.7542.12900516.620.95900497.917.471.070.450.7237.41113910488.77.68.317.550.870.50.7743.438.517.60.930.50.7345.2348183475.766.385.566.270.720.650.7542.055.476.260.70.50.7542.12900525.176.560.950.680.741.9900507.557.451.070.450.7237.41114910498.17.547.887.461.080.520.7343.27.927.491.120.530.734549183495.056.054.775.970.770.620.7241.984.765.980.780.680.741.92900535.376.280.850.520.7741.82900517.917.470.670.470.7337.121115910507.767.477.557.461.080.520.7343.27.67.491.120.530.734550185025.626.295.476.410.770.620.7241.985.526.420.780.680.741.92900545.936.670.850.520.7741.82900527.737.370.670.470.7337.121116910518.17.517.897.460.730.480.7842.937.957.50.720.520.9544.5851185096.6776.620.956.670.92900555.786.590.70.480.941.43900537.717.460.670.480.6736.921117910527.867.497.747.40.730.480.7842.937.747.410.720.520.9544.5852185235.426.635.176.560.950.680.741.95.246.490.920.570.7341.87900564.746.030.70.480.941.43900545.86.830.670.480.6736.921118910538.027.57.687.441.350.520.7342.687.847.480.730.520.7544.3553185615.586.395.376.280.850.520.7741.825.46.270.90.570.7341.7900576.116.490.750.750.7841.13900554.76.430.750.470.7836.621119910545.36.75.746.811.350.520.7342.685.666.830.730.520.7544.3554185636.066.735.936.670.850.520.7741.825.966.680.90.570.7341.7900585.286.140.750.750.7841.13900566.36.960.750.470.7836.621120910554.726.64.616.40.750.551.2841.924.666.390.730.551.2343.6355185665.836.595.786.590.70.480.941.435.86.580.830.550.8741.4900595.876.480.720.550.7341.15900575.2960.730.50.736.382101910566.347.096.266.970.750.551.2841.926.287.010.730.551.2343.6356185694.926.24.746.030.70.480.941.434.746.040.830.550.8741.4900605.636.290.720.550.7341.15900586.417.080.730.50.736.382102910575.56.055.265.950.770.530.7841.685.256.010.730.580.7343.4557185726.216.556.116.490.750.750.7841.136.146.450.750.720.8341.12900615.696.430.70.620.8540.85900596.786.90.720.480.7236.172103910586.57.116.397.060.770.530.7841.686.417.10.730.580.7343.4558185795.96.675.286.140.750.750.7841.135.356.280.750.720.8341.12900626.136.590.70.620.8540.85900606.687.030.720.480.7236.172104910597.027.126.786.890.730.530.7841.436.786.910.730.530.8543.1859187125.916.485.876.480.720.550.7341.155.926.490.70.520.7741.07900636.246.670.770.50.8240.65900616.666.990.730.50.7235.932105910606.787.196.687.020.730.530.7841.436.687.050.730.530.8543.1860187135.816.295.636.290.720.550.7341.155.656.320.70.520.7741.07900646.276.740.770.50.8240.65900626.27.250.730.50.7235.932106910616.757.156.676.980.780.470.8741.16.770.950.630.8842.8361187165.736.345.696.430.70.620.8540.855.696.360.730.531.3840.2900655.696.470.90.580.7240.43900637.837.420.670.480.7535.682107910626.37.326.217.240.780.470.8741.16.177.280.950.630.8842.8362187186.336.536.136.590.70.620.8540.856.186.60.730.531.3840.2900665.126.450.90.580.7240.43900647.97.530.670.480.7535.682108910638.057.477.817.40.730.50.9340.637.917.450.750.50.942.5763187196.36.656.246.670.770.50.8240.656.316.70.730.480.839.93900676.176.90.780.471.0839.93900655.776.420.780.480.735.472109910648.167.57.887.530.730.50.9340.638.027.550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00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPTtray swilredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPTtray swirledSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPThand stirredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, NAPThand stirredSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXtray swirledwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXtray swirledSMP buffer pH, old wayKY buffer pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXhand stirredwater pH, old waywater pH, new instr000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000rout setting, LEXhand stirredSMP buffer pH, old wayKY buffer pH, new instrtimeelapsed timedayssecs11:18:50117:40:1811:18:50227:40:1811:20:04337:41:390:01:210.0009378111:20:04447:41:390:01:210.0009378111:21:18557:42:580:01:190.0009147911:21:18667:42:580:01:190.0009147911:22:33777:44:190:01:210.0009388111:22:33887:44:190:01:210.0009388111:23:45997:45:580:01:390.0011469911:23:4510107:45:580:01:390.0011469911:25:0211117:47:190:01:210.0009388111:25:0212127:47:190:01:210.0009388111:26:1613137:48:370:01:180.0009037811:26:1614147:48:370:01:180.0009037811:27:2915157:49:580:01:210.0009388111:27:2916167:49:580:01:210.0009388111:28:4317177:51:230:01:250.0009848511:28:4318187:51:230:01:250.0009848511:30:0019197:52:430:01:200.0009268011:30:0020207:52:430:01:200.0009268011:31:1321217:54:180:01:350.001100950:27:01time elapsed for a tray of water pH (40 samples)11:31:1322227:54:180:01:350.001100950:04:42time elapsed for a tray of buffer pH11:32:2623237:55:380:01:200.0009268011:32:2624247:55:380:01:200.000926801.55average min11:33:4025257:57:040:01:260.000995861.57average min11:33:4026267:57:040:01:260.0009958611:34:5127277:58:230:01:190.0009147911:34:5128287:58:230:01:190.0009147911:36:0529297:59:420:01:190.0009147911:36:0530307:59:420:01:190.0009147911:37:1731318:01:010:01:190.0009147911:37:1732328:01:010:01:190.0009147911:38:4933338:02:410:01:400.00115710011:38:4934348:02:410:01:400.00115710011:40:1735358:04:140:01:330.0010769311:40:1736368:04:140:01:330.0010769311:41:4737378:05:470:01:330.0010769311:41:4738388:05:470:01:330.0010769311:43:1739398:07:190:01:320.0010659211:43:1740408:07:190:01:320.0010659211:44:471418:09:000:01:410.00116910111:44:472428:09:000:01:410.00116910111:46:163438:10:350:01:350.0011009511:46:164448:10:350:01:350.0011009511:47:445458:12:090:01:340.0010889411:47:446468:12:090:01:340.0010889411:49:137478:13:420:01:330.0010769311:49:138488:13:420:01:330.0010769311:50:419498:15:220:01:400.00115710011:50:4110508:15:220:01:400.00115710011:52:0911518:16:540:01:320.0010659211:52:0912528:16:540:01:320.0010659211:53:3613538:18:270:01:330.0010769311:53:3614548:18:270:01:330.0010769311:55:0415558:20:010:01:340.0010889411:55:0416568:20:010:01:340.0010889411:56:3317578:21:420:01:410.00116910111:56:3318588:21:420:01:410.00116910111:58:0219598:23:170:01:350.0011009511:58:0220608:23:170:01:350.0011009511:59:2821618:24:500:01:330.0010769311:59:2822628:24:500:01:330.0010769312:00:5523638:26:240:01:340.0010889412:00:5524648:26:240:01:340.0010889412:02:2325658:28:050:01:410.00116910112:02:2326668:28:050:01:410.00116910112:03:5227678:29:400:01:350.0011009512:03:5228688:29:400:01:350.0011009512:05:2029698:31:140:01:340.0010889412:05:2030708:31:140:01:340.0010889412:06:4731718:32:490:01:350.0011009512:06:4732728:32:490:01:350.0011009512:08:1733738:34:300:01:410.00116910112:08:1734748:34:300:01:410.00116910112:09:4635758:36:050:01:350.0011009512:09:4636768:36:050:01:350.0011009512:11:1437778:37:380:01:330.0010769312:11:1438788:37:380:01:330.0010769312:12:4339798:39:140:01:360.0011119612:12:4340808:39:140:01:360.0011119612:14:421818:41:450:02:310.00174815112:14:422828:41:450:02:310.00174815112:16:103838:43:220:01:370.0011239712:16:104848:43:220:01:370.0011239712:17:395858:44:570:01:350.0011009512:17:396868:44:570:01:350.0011009512:19:087878:46:320:01:350.0011009512:19:088888:46:320:01:350.0011009512:20:389898:48:120:01:400.00115710012:20:3810908:48:120:01:400.00115710012:22:0511918:49:470:01:350.0011009512:22:0512928:49:470:01:350.0011009512:23:3213938:51:220:01:350.0011009512:23:3214948:51:220:01:350.0011009512:25:0115958:52:560:01:340.0010889412:25:0116968:52:560:01:340.0010889412:26:3117978:54:370:01:410.00116910112:26:3118988:54:370:01:410.00116910112:28:0119998:56:120:01:350.0011009512:28:01201008:56:120:01:350.0011009512:29:28211018:57:310:01:190.0009147912:29:28221028:57:310:01:190.0009147912:30:56231038:59:060:01:350.0011009512:30:56241048:59:060:01:350.0011009512:32:27251059:00:470:01:410.00116910112:32:27261069:00:470:01:410.00116910112:33:57271079:02:220:01:350.0011009512:33:57281089:02:220:01:350.0011009512:35:26291099:03:570:01:350.0011009512:35:26301109:03:570:01:350.0011009512:36:55311119:05:300:01:330.0010769312:36:55321129:05:300:01:330.0010769312:38:25331139:07:110:01:410.00116910112:38:25341149:07:110:01:410.00116910112:39:54351159:08:480:01:370.0011239712:39:54361169:08:480:01:370.0011239712:41:21371179:10:210:01:330.0010769312:41:21381189:10:210:01:330.0010769312:42:50391199:11:560:01:350.0011009512:42:50401209:11:560:01:350.0011009512:51:46buffbegins1219:19:290:07:330.00524345312:51:46261229:21:010:09:050.00630854512:53:01271239:22:310:03:020.00210618212:53:01281249:22:310:01:300.0010429012:54:17291259:23:510:01:200.0009268012:54:17301269:23:510:01:200.0009268012:55:32321279:25:120:01:210.0009388112:55:32331289:25:120:01:210.0009388112:56:48341299:26:310:01:190.0009147912:56:48351309:27:570:02:450.00191016512:58:04361319:27:570:01:260.0009958612:58:04371329:29:170:01:200.0009268012:59:19381339:29:170:01:200.0009268012:59:19391349:30:370:01:200.000926801:00:34401359:30:370:01:200.000926801:00:3411369:31:580:01:210.000937811:01:5021379:31:580:01:210.000937811:01:5031389:33:250:01:270.001007871:03:0561399:33:250:01:270.001007871:03:0571409:34:450:01:200.000926801:04:1981419:36:050:02:400.0018521601:04:1991429:37:250:02:400.0018521601:05:33101439:37:250:01:200.000926801:05:33111449:38:490:01:240.000972841:06:49121459:38:490:01:240.000972841:06:49131469:40:090:01:200.000926801:08:04141479:40:090:01:200.000926801:08:04151489:41:290:01:200.000926801:09:19161499:41:290:01:200.000926801:09:19171509:42:500:01:210.000937811:10:33181519:42:500:01:210.000937811:10:33191529:44:150:01:250.000984851:11:49201539:44:150:01:250.000984851:11:49211549:45:350:01:200.000926801:13:04221559:45:350:01:200.000926801:13:04231569:46:560:01:210.000937811:14:18241579:46:560:01:210.000937811:14:18251589:48:160:01:200.000926801:15:33261599:48:160:01:200.000926801:15:33271609:49:430:01:270.001007871:16:50301619:49:430:01:270.001007871:16:50311629:51:040:01:210.000937811:18:06321639:52:230:02:400.0018521601:18:06331649:53:440:02:400.0018521601:19:21341659:53:440:01:210.000937811:19:21351669:55:090:01:250.000984851:20:37361679:55:090:01:250.000984851:20:37371689:56:300:01:210.000937811:21:54381699:56:300:01:210.000937811:21:54391709:57:430:01:130.000845731:23:10401719:57:430:01:130.000845731:23:1011729:58:530:01:100.000810701:24:2521739:58:530:01:100.000810701:24:25317410:00:190:01:260.000995861:25:41417510:00:190:01:260.000995861:25:41517610:01:390:01:200.000926801:26:58617710:01:390:01:200.000926801:26:58717810:02:580:01:190.000914791:28:14817910:02:580:01:190.000914791:28:14918010:04:190:01:210.000937811:29:301018110:04:190:01:210.000937811:29:301118210:05:460:01:270.001007871:30:451518310:05:460:01:270.001007871:30:451618410:07:070:01:210.000937811:32:021718510:08:330:02:470.0019331671:32:021818610:08:330:01:260.000995861:33:171918710:09:580:01:250.000984851:33:172018810:09:580:01:250.000984851:34:332118910:11:180:01:200.000926801:35:492219010:11:180:01:200.000926801:35:492319110:12:370:01:190.000914791:37:062419210:12:370:01:190.000914791:37:062519310:14:380:02:010.0014001211:38:212619410:14:380:02:010.0014001211:38:212719510:16:050:01:270.001007871:39:372819610:16:050:01:270.001007871:39:372919710:17:250:01:200.000926801:40:523019810:17:250:01:200.000926801:40:523119910:19:430:02:180.0015971381:42:383220010:19:430:02:180.0015971381:42:383320110:21:000:01:170.000891771:43:533420210:21:000:01:170.000891771:43:533520310:22:260:01:260.000995861:45:093620410:22:260:01:260.000995861:45:093720510:23:470:01:210.000938811:46:263820610:23:470:01:210.000938811:46:263920710:25:010:01:140.000856741:47:434020810:25:010:01:140.000856741:47:4310:26:221:48:5810:26:221:48:5810:32:181:50:141:50:141:50:141:50:141:51:291:51:291:51:291:51:290000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000elapsed time (secs)30,60 setting602171121711123171231723125231251625611.030.9712411811.030.972666217171717171172323123223232323131313131131621.0310.971241.0310.97A Mid-Atlantic Soil Testing and Plant Analysis Work Group survey on methods for soil pH, buffer pH and lime recommendations Objectives are to assess:1. variation in lab methods being used.2. effect of method variation on intra- and interlaboratory error.3. variation in how lime recommendations are made.& SERA6Soil pH MAD values in the NAPT programChart30.10.130.080.160.080.070.090.10.110.150.10.050.110.090.120.090.070.10.140.060.10.060.130.10.10.10.120.140.050.10.10.070.10.10.070.10.10.10.090.090.080.10.060.20.110.090.10.070.090.060.070.080.080.080.110.10.10.090.080.080.090.080.160.080.170.10.110.10.090.10.080.090.090.060.10.080.080.040.050.080.120.120.10.080.060.090.10.060.080.10.10.080.110.090.10.090.10.10.070.080.130.130.10.080.10.10.070.070.090.110.080.070.10.080.10.10.120.090.090.10.10.080.10.190.130.070.10.10.080.10.090.070.10.080.10.090.090.10.090.090.110.090.10.10.130.080.060.090.110.090.10.10.10.0850.0750.0750.10.110.130.080.060.090.080.10.10.090.10.110.110.10.120.1pHavg=1.0891022835-0.927avg=1.416850444avg=0.5561509966stdev=0.46489606617.2stdev=0.4585365836stdev=0.350677445Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVW PH CVAE pH CV981137.9427.520.10.07981148.26417.550.130.05981156.714670.080.07981165596.650.160.15981174.86450.080.2981185.9636.40.070.1981197.85387.50.090.04981205.6636.80.10.1981216.9467.080.110.08981228.2367.550.150.05981236.4547.20.10.1981245.15646.50.050.14991018.017.517.837.887.50.110.050.030.66577896140.238235BinFrequency1.37328339580.3831417625991025.796.787.575.826.690.090.080.041.17994100290.914945.2501.55440414510.5284015852991036.987.087.697.097.070.120.080.021.12994350280.636845.45.201.71919770770.2600780234991047.77.37.757.597.250.090.030.010.41095890410.43295.65.401.16883116880.1290322581991057.647.357.687.67.330.070.050.030.68027210880.386555.85.610.91623036650.390625991065.16.367.455.016.30.10.130.062.04402515721.3042865.801.96078431370.8053691275991076.486.77.56.876.860.140.10.031.49253731340.98916.2602.16049382720.4991086.947.17.656.977.10.060.090.081.26760563380.61836.46.210.86455331411.0457516349910987.517.828.027.550.10.050.040.66577896140.238236.66.481.250.5115089514991107.457.37.777.577.290.060.060.050.82191780820.43296.86.630.80536912750.6435006435991118.38537.567.898.217.630.130.060.060.79365079370.1918876.861.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238237.27101.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451447.47.2191.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868597.67.4101.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349477.6261.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.4329More01.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35990.91743119271.1142061281991187.9607.57.837.80.10.050.010.66666666670.24751.26582278480.1277139208991197.4607.277.737.70.10.070.020.96286107290.460711.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304281.22164048870.8241758242_001016.55877.646.570.10.070.0510.711Jan 2005 to June 20051.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.53487IDSMP buffer pHCVn1.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.247521077.26677725120.69055413642110.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.247521106.25522613070.91735297311991.31578947370.630517024_001058587.57.858.17.50.10.040.060.53333333330.247521156.79510526321.03484115231901.250.7643312102_001065.7677.167.85.67.20.10.060.030.83798882680.5626821166.79040462430.85478369521731.75438596490.3846153846_001076.34676.97.486.46.90.090.10.031.44927536230.803741086.62066265061.16049183851661.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.53487P0016.44651162791.1553321806431.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326P0026.89952380951.026837191421.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.47925P0036.693751.0924216278401.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.22896P0047.329250.2536371304400.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.00764P0056.493251.0626376821404.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.59049P0067.09050.5879950257401.9819819820.7682458387_001145.7657.177.815.77.10.090.070.060.97629009760.55341P0076.956250.5306315565401.57894736840.7682458387_001155.8656.927.635.86.80.10.080.061.15606936420.78516P0086.019751.623930658401.7241379310.7863695937_001164.27686.37.344.26.30.070.150.042.3809523811.3599P0096.621751.3057857362401.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428P0106.91444444440.6490363471361.69172932331.8641810919_001185.65687.27.825.57.20.060.090.011.250.52561.06194690270.1278772379_001196.57687.047.626.57.10.070.060.020.85227272730.673921.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.091071.33333333330.9446693657_011014.94706.67.656.40.080.10.041.51515151521.08181.61943319840.5263157895_011026.4706.917.636.56.80.080.10.061.44717800290.794431.250.7863695937_011037.7707.57.87.70.110.070.040.93333333330.24751.42857142860.5128205128_011046.6707.17.696.67.10.10.080.051.12676056340.61831.51515151520.6501950585_011058.1707.527.868.20.10.050.030.6648936170.228961.23456790120.3816793893_011068.09417.57.848.17.530.090.070.010.93333333330.24751.11248454880.1275510204_011076.424177.656.637.090.080.10.051.42857142860.7111.2461059190.6535947712_011085.37416.617.515.516.660.080.10.071.51285930411.072531.48975791430.9320905459_011095.79417.17.815.777.170.090.10.021.40845070420.61831.55440414510.2560819462_011108.02417.497.828.317.50.080.090.021.20160213620.256770.99750623440.2557544757_011118.24377.597.918.197.540.160.090.021.1857707510.164071.94174757280.2528445006_011127.92377.547.797.967.540.080.050.040.66312997350.210421.01010101010.513478819_011138.7377.67.958.927.570.170.060.030.78947368420.15481.95402298850.3773584906_011148.1377.547.858.157.530.10.060.010.79575596820.210421.23456790120.127388535_011157.76377.477.897.837.450.110.070.020.937081660.275311.41752577320.2534854246_011168.1417.517.868.137.510.10.060.030.79893475370.238231.23456790120.3816793893_011177.86417.497.827.927.480.090.060.030.80106809080.256771.14503816790.3836317136_011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.3773584906_011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.8064516129_011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021066.75627.157.686.67.10.040.060.030.83916083920.571950.59259259260.39062520021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021136.85457.27.76.697.260.060.040.030.55555555560.52560.87591240880.389610389620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021176.78667.27.76.657.20.080.040.030.55555555560.52561.17994100290.389610389620021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021196.4666.927.726.626.860.10.080.041.15606936420.785161.56250.51813471520021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031066.1707.01117.65.826.950.10.080.041.14122681880.701731.63934426230.526315789520031076.03707117.585.986.950.070.050.060.71428571430.7111.16086235490.791556728220031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031146.1657.04147.666.197.070.10.060.040.85227272730.673921.63934426230.522193211520031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451421.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364811.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835691.24416796270.642673521920031206697.02157.655.877.080.070.080.041.13960113961.16666666670.52287581720041017.56437.35147.617.47.280.10.060.030.81632653061.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878121.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872341.26582278480.639386189320041055.84436.72147.535.966.830.120.080.071.19047619052.05479452050.929614873820041065.8656.7157.525.766.730.090.080.071.19402985071.55172413790.930851063820041078.24657.53157.778.287.540.090.060.040.7968127491.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444441.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397881.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364813.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646732.41635687730.382165605120041145.76716.7207.515.646.630.070.10.041.49253731341.21527777780.532623169120041157.4717.46207.817.47.40.10.040.020.53619302951.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533691.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936421.23456790121.041666666720041185.9517.1147.785.97.080.10.050.070.70422535211.69491525420.899742930620041197.76517.5147.97.717.470.090.030.060.41.15979381440.759493670920041205.85516.74147.545.86.850.070.060.060.89020771511.19658119660.795755968220050015.64736.40.10.132.031251.773049645420050027.85737.570.080.030.39630118891.019108280320050037.9737.520.10.030.39893617021.265822784820050044.55736.20.090.11.61290322581.97802197820050057.76737.510.090.050.66577896141.159793814420050067.8517.50.10.040.53333333331.282051282120050078.127.550.090.050.66225165561.108374384220050087.837.50.090.040.53333333331.149425287420050096.877.160.110.060.83798882681.601164483320050107.216.910.090.091.30246020261.248266296820050117.8677.50.10.030.41.282051282120050126.37.10.10.070.9859154931.587301587320050137.37.40.130.070.94594594591.780821917820050147.097.20.080.081.11111111111.128349788420050155.056.30.060.11.58730158731.188118811920050165.69666.420.090.091.40186915891.581722319920050177.587.50.110.060.81.451187335120050185.56.350.090.091.41732283461.636363636420050196.486.840.10.111.60818713451.543209876520050207.87.50.10.050.66666666671.282051282120060018.36537.590.10.091.1857707511.196172248820060027.377.330.0850.070.95497953621.153324287720060037.837.430.0750.070.94212651410.957854406120060047.137.30.0750.070.95890410961.051893408120060058.47.520.10.060.79787234041.190476190520060068.36517.50.110.040.53333333331.315789473720060076.16.60.130.131.96969696972.13114754120060087.857.460.080.040.53619302951.019108280320060095.766.890.060.081.16110304791.041666666720060107.017.250.090.050.68965517241.283880171220060114.38676.550.080.152.29007633591.826484018320060128.367.50.10.050.66666666671.1961722488200601387.490.10.050.66755674231.2520060146.116.740.090.0650.96439169141.4729950920060158.47.560.10.060.79365079371.190476190520060168.2547.510.110.081.06524633821.341463414620060178.387.60.110.081.05263157891.3126491647200601866.490.10.091.38674884441.666666666720060198.357.50.120.081.06666666671.437125748520060208.37.50.10.081.06666666671.2048192771Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHpH0.66577896140.69055413641.17994100290.91735297311.12994350281.03484115230.41095890410.85478369520.68027210881.16049183852.04402515721.15533218061.49253731341.0268371911.26760563381.09242162780.66577896140.25363713040.82191780821.06263768210.79365079370.58799502570.66577896140.53063155651.09890109891.6239306581.90336749631.30578573620.81190798380.64903634711.36986301372.06349206350.66666666670.96286107291.729559748411.25173852570.66666666670.80.53333333330.83798882681.44927536230.55632823371.20845921450.68965517240.39893617021.34730538920.98176718090.97629009761.15606936422.3809523811.5723270441.250.85227272731.36570561461.51515151521.44717800290.93333333331.12676056340.6648936170.93333333331.42857142861.51285930411.40845070421.20160213621.1857707510.66312997350.78947368420.79575596820.937081660.79893475370.80106809080.53333333331.34328358211.51515151521.12834978841.32231404961.26582278480.98314606740.83449235050.83916083921.09289617490.53547523430.66666666671.56250.40.67567567570.55555555560.99857346651.32158590311.30434782610.55555555560.53120849931.15606936423.07971014491.15606936421.56250.79575596821.92616372390.85106382981.14122681880.71428571431.49253731341.18421052630.84033613450.84507042250.85227272730.80213903740.85227272730.83333333331.12994350281.6442451421.28755364810.84985835691.13960113960.81632653060.77519379841.46842878121.3297872341.19047619051.19402985070.7968127490.69444444441.48760330581.66666666670.53050397881.28755364811.11265646731.49253731340.53619302950.80862533691.15606936420.70422535210.40.8902077151SMP buffer pHCoefficient of Variation (%)y = -0.837 x + 7.00r 2 = 0.658pH_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)PK_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Soil Description0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000Sheet2min=37max=71This was the graph used in the publication to represent interlab erroraverage=58.7816091954avg=1.1252495213-0.927However, the regression coefficient for all samples was kept in definingavg=1.4798714341avg=0.5942695862median=64stdev=0.45794372377.2error bars (-0.837, 7.00). The difference wasn't deemed great enough tostdev=0.4312774603stdev=0.3982478394Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVrecalculate error bars in other graphs.W PH CVAE pH CV991118.38537.567.898.217.630.130.060.060.79365079370.191885BinFrequency1.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238235.2501.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451445.45.201.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868595.65.401.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349475.85.611.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.432965.801.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35996.2600.91743119271.1142061281991197.4607.277.737.70.10.070.020.96286107290.460716.46.211.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304286.66.481.22164048870.8241758242_001016.55877.646.570.10.070.0510.7116.86.631.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.5348776.861.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.24757.27100.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.24757.47.2191.31578947370.630517024_001076.34676.97.486.46.90.090.10.031.44927536230.80377.67.4101.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.534877.6261.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326More01.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.479251.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.228960.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.007644.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.590491.9819819820.7682458387_001164.27686.37.344.26.30.070.150.042.3809523811.3599Jan 2005 to June 20052.5*CV w2.5*CV wo1.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428IDSMP buffer pHCVnSMP buf pHAlldups1.69172932331.8641810919_001196.57687.047.626.57.10.070.060.020.85227272730.6739221077.26677725120.690554136421164.9454.9831.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.0910721106.25522613070.91735297311996.24.52654.570551.33333333330.944669365720011014.94706.67.656.40.080.10.041.51515151521.081821156.79510526321.03484115231906.44.1084.15811.61943319840.526315789520011026.4706.917.636.56.80.080.10.061.44717800290.7944321166.79040462430.85478369521736.63.68953.745651.250.786369593720011037.7707.57.87.70.110.070.040.93333333330.247541086.62066265061.16049183851666.83.2713.33321.42857142860.512820512820011046.6707.17.696.67.10.10.080.051.12676056340.6183P0016.44651162791.15533218064372.85252.920751.51515151520.650195058520011076.424177.656.637.090.080.10.051.42857142860.711P0026.89952380951.026837191427.22.4342.50831.2461059190.653594771220011085.37416.617.515.516.660.080.10.071.51285930411.07253P0036.693751.0924216278407.42.01552.095851.48975791430.932090545920011095.79417.17.815.777.170.090.10.021.40845070420.6183P0047.329250.2536371304407.61.5971.68341.55440414510.256081946220011108.02417.497.828.317.50.080.090.021.20160213620.25677P0056.493251.0626376821400.99750623440.255754475720011118.24377.597.918.197.540.160.090.021.1857707510.16407P0067.09050.5879950257401.94174757280.252844500620011127.92377.547.797.967.540.080.050.040.66312997350.21042P0076.956250.5306315565401.01010101010.51347881920011138.7377.67.958.927.570.170.060.030.78947368420.1548P0086.019751.623930658401.95402298850.377358490620011157.76377.477.897.837.450.110.070.020.937081660.27531P0096.621751.3057857362401.41752577320.253485424620011177.86417.497.827.927.480.090.060.030.80106809080.25677P0106.91444444440.6490363471361.14503816790.383631713620011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.377358490620011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.806451612920011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451420.998371.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364810.720271.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835690.655381.24416796270.642673521920041017.56437.35147.617.47.280.10.060.030.81632653060.386551.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.025020.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878120.887131.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872340.228961.26582278480.639386189320041078.24657.53157.778.287.540.090.060.040.7968127490.219691.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444440.52561.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.591651.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.6381.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397880.210421.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364810.720273.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646730.534872.41635687730.382165605120041157.4717.46207.817.47.40.10.040.020.53619302950.284581.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533690.321661.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936420.785161.23456790121.041666666720041197.76517.5147.97.717.470.090.030.060.40.24751.15979381440.7594936709Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSheet2000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000SMP buffer pHCoefficient of Variation (%)Sheet3000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Values are in units of mg/kguse ICP-P in these columnswhen it is reported in 2001Sample IDn for M3KM3KM3K MADM3K CVn for M3PM3PM3P MADM3P CV99101795415.15723270448689.302325581499102328267.926829268315418.111.7532467532991038156.172839506244.83.88.48214285719910427371866.7957617831385956.859205776299105627386.060606060663.37.912.480252764699106223146.2780269058101109.9009900999910710187.9207920792406.616.59910846428.76.1853448276363.59.722222222299109782719.07928388758578.23529411769911010776.5420560748292.68.96551724149911142171019011.111111111142735.98.08219178089911242800779.6254289910.11235955069911342535.29.81132075474212214.511.8852459016991144210476.73076923084212.52.52099115429599.47368421054261.626.66666666679911634721638.737864077737282.38.2142857143991173418394.918032786937203159911934140139.28571428573717211.76470588249912034346174.9132947977376845.8823529412_001013512497.258064516143323.912.1875_00102353183811.94968553464333515.1515151515_001033543227.16.2731481481433438.8235294118_0010435228198.33333333334357.67.913.7152777778_0010742456275.92105263164556.54.57.9646017699_001084274345.56.123822341945272.710_0010942402174.228855721445263.212.3076923077_0011042378266.87830687834526134.613.2567049808_0011138871112.6436781609384.22.559.5238095238_00112383126.45161290323859.33.86.4080944351_001133823520.88.85106382983876.111.515.111695138_0011643186147.52688172044350918_00117439410.611.27659574474319.67.638.7755102041_0011943249124.8192771084433937.6923076923_0012043225146.22222222224340.55.914.56790123462001101461651911.51515151523251.87.414.28571428572001102467157610.62937062943225.23.915.4761904762200110346645456.97674418632543.97.2222222222200110446732567.65027322432342.88.23529411762001107492473413.765182186235956.16.421052631620011084958813.79310344833591.516.66666666672001109492422610.7438016529353339.0909090909200111049277238.3032490975354149.756097561200111145304.515346.62.131.8181818182200111245538387.0631970263444.93.98.685968819620011134511414.812.98245614043412.71.29.4488188976200111545312288.9743589744341119.28.28828828832001117491792815.64245810063425.54.517.647058823520011184921322.610.610328638534404.611.520011194910798.4112149533342.50.936200112049141128.510638297934577.412.9824561404200210151252166.3492063492376957.2463768116200210251356267.30337078653775.55.67.4172185432002103511021312.745098039237145149.6551724138200210451957616.374085684437676629.17159763312002105511119857.59606791783792.910.110.8719052745200210749646.19.5312537223.114.090909090920021084919116.58.638743455537171.810.5882352941200210949125129.63719210.52631578952002110492172511.52073732723761.26.510.6209150327200211150484357.23140495873692.66.67.127429805620021125013101199.08396946563698.27.87.9429735234200211450254218.2677165354368.31.720.48192771082002115501531711.11111111113695.18.58.93796004212002116524014210.47381546133816.11.911.80124223620021185274076.510.337837837838604.882002120521672213.17365269463810311.511.16504854372003101467679.2105263158349.51.313.68421052632003102469210.811.73913043483452.6611.406844106520031034646932.46.9083155653439.54.310.8860759494200310446254207.8740157483448.7510.266940451720031054696810210.53719008263453.26.311.84210526322003108492983210.73825503363619913.36.6834170854200310949449439.57683741653633.36.720.1201201201200311049166169.63855421693644.94.19.131403118200311152332216.3253012048404536.666666666720031125212512.19.68403239.3752003113522182210.09174311934080.57.28.9440993789200311552258176.58914728684035.62.46.74157303372003116488889.090909090937211.57.1428571429200311748296289.4594594595376569.2307692308200311848969.29.583333333337111.110200311948144128.333333333337236208.4745762712200410146639467.19874804383460.74.26.919275123620041024649130.76.252545824834207167.72946859920041034620719.79.51690821263446.56.814.623655914200410446468326.83760683763439127.16.9309462916200410746461378.026030368837624.77.58064516132004108461829.55.219780219837424.210200410946364.813.3333333333373.91.128.205128205120041104637513.51351351353713.9214.3884892086200411151429429.790209790241545.710.555555555620041125124528.511.63265306124130.85.116.5584415584200411351421.534.98.27995255044131.63.611.3924050633200411551484489.917355371941159159.4339622642200411649440409.090909090939195157.6923076923200411749123016813.6585365854391852513.513513513520041194913601349.8529411765392092110.047846892005101521612012.42236024844237.83.810.0529100529200510252103675.27.2586872587421179.17.7777777778200510352659426.3732928684227.83.412.2302158273200510452244.619.16666666674291.314.4444444444200510552294196.462585034421001010200510752429327.459207459243303102005109523474512.96829971184329.62.79.12162162162005110522212712.2171945701431732413.8728323699000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3K, mg/kgCV, %000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3P, mg/kgCV, %99-111CozadFluventic HaplustollFluventicHaplustoll99-112LaurenCalcic HaploxerollCalcicHaploxerollc99-113ToccaTypic UdifluventTypicUdifluvent99-114LousivilleTypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)99-115SagcoveONTARIO99-116Pay PointXeric HaplargidXericHaplargid99-117PeelerUstic GlossocryalfUsticGlossocryalf99-118KoenigCalcic HaploxerollCalcicHaploxerollc99-119Belle MinaAL99-120Fort EllisTypic ArgiustollTypicArgiustoll00-101WhitewaterMN00-102KeenesburgUstic HaplargidUsticHaplargidl00-103BensonVertic TorrifluventVerticTorrifluvent00-104OrchardTypic HaplargidTypicHaplargidNM00-105KidmanCalcic HaploxerollCalcicHaploxerollc00-106BlairUstic HaplargidUsticHaplargidl00-107AmsterdamTypic HaplustollTypicHaplustoll00-108AshdosVitritorrandic ArgixerollVitritorrandicArgixeroll00-109WyorAquertic ArgiudollAquerticArgiudoll00-110Bresser IIAridic ArgiustollAridicArgiustoll00-111ShiloUstic TorriorthentUsticTorriorthentmJun-0000-112LignumAquic HapludultAquicHapludult00-113ZenithLamellic HaplustalfLamellicHaplustalf00-114WeldUstic HaplargidUsticHaplargidl00-115Monona IITypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)00-116TellerUdic ArgiustollUdicArgiustollOK00-117GrosecloseTypic HapludultTypicHapludult00-118FrancamUstic HaplargidUsticHaplargidl00-119BrookingsCalcic HapludollCalcicHapludoll00-120AmesAquic HapludollAquicHapludoll01-101O'NeilTypic UstipsammentTypicUstipsamment01-102HastingsUdic ArgiustollUdicArgiustollCO01-103OwngatePachic ArgiustollPachicArgiustoll01-104BrandonAridic ArgiustollAridicArgiustoll01-105TokieUstic TorriorthentUsticTorriorthentmMar-0101-106NikkolaUstic TorriorthentUsticTorriorthentmMar-0101-107NittanyTypic HapludalfTypicHapludalfPA01-108ProvidenceTypic FragiudalfTypicFragiudalfcollected in LA01-109HaxtunPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times01-110ColumbiaXeric HaplocambidXericHaplocambid01-111SonomaUltic HaploxerollUlticHaploxerollCA01-112KoshareUstic HaplocambidUsticHaplocambid01-113PascoXeric TorripsanmmentXericTorripsanmment01-114MaureUstic TorriorthentUsticTorriorthentmMar-0101-115Multi-BlendBLEND01-116EatonUstic TorriorthentUsticTorriorthentmMar-0101-117FairmontMollic FluvaquentMollicFluvaquentr01-118RoseTypic PsammaquentTypicPsammaquent01-119ClemsonTypic KanhapludultTypicKanhapludult01-120EwingEntic HaplustollEnticHaplustoll02-101White WaterMN02-102MarshanTypic EndoaquollTypicEndoaquoll02-103OrangeburgTypic KandiudultTypicKandiudult02-104JewelVertic EndoaquollVerticEndoaquollIowa02-105AscalonAridic ArgiustollAridicArgiustollb02-106AscalonAridic ArgiustollAridicArgiustollb02-107DarcoGrossarenic PaleudultGrossarenicPaleudult02-108HasselPachic HapludollPachicHapludoll02-109WasatchVertic EndoaquollVerticEndoaquollUT02-110KennanHaplic GlossudalfHaplicGlossudalf02-111MaderaTypic HaplocambidTypicHaplocambid02-112RandallUdic PellustertUdicPellustertj02-113AdamsAridic ArgiustollAridicArgiustollb02-114KenomaVertic ArgiudollVerticArgiudoll02-115AthensArenic KandiudultArenicKandiudultcollected by Kissel02-116Monona CTypic HapludollTypicHapludollhsampled by Miller 2 different times (sampled Aug 2002)02-117AdamsAridic ArgiustollAridicArgiustollb02-118BakersfieldTypic ToriorthentTypicToriorthent02-119PhillipsPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times02-120North CarolinaTypic UmbraquultTypicUmbraquult03-101St HelenaTypic HaplustultTypicHaplustult03-102Eagle RiverAK03-103Casa GrandeAZ03-104PerkinsUltic HaplustalfUlticHaplustalf03-105AntonVertic GlossudalfVerticGlossudalfoJan-0303-106BrushVertic GlossudalfVerticGlossudalfoJan-0303-107ArmarilloUdic PellustertUdicPellustertj03-108ThorndikeLithic HaplorthodLithicHaplorthod03-109AirportAquic NatrixerollAquicNatrixeroll03-110PrincetonTypic HapludalfTypicHapludalfIL03-111LelandMS03-112BelmondIA03-113CrestonMT03-114LindonVertic GlossudalfVerticGlossudalfoJan-0303-115GriffyTypic HaplargidTypicHaplargidWY03-116CaptinaTypic FragiudalfTypicFragiudalfeAR03-117Little Flat TopsCO03-118RosettaIL03-119McBrideMI03-120PlatnerVertic GlossudalfVerticGlossudalfoJan-0304-101CassND04-102OteroUstic TorriorthentUsticTorriorthent04-103Del RayAquic ArgiudollAquicArgiudoll04-104GenolaXeric TorrifluventXericTorrifluvent04-105NettieTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-106HarryTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-107MaricopaTypic NatrargidTypicNatrargid04-108Baton RougeLA04-109MatanuskaAK04-110GeorgetownDE04-111Hutton LakeUstic NatrargidUsticNatrargid04-112StewartMN04-113WagramArenic KandiudultArenicKandiudultcollected by Hardy04-114CharlesTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-115San LuisCO04-116UtneMIX04-117MoscowUltic HaploxerollUlticHaploxerollID04-118AltheimerTypic FragiudultTypicFragiudulteAR04-119WahlukeDuric TorriorthentDuricTorriorthent04-120NelsonTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)05-101Parmasilt loamIL05-102Fairburysilt loamID05-103Three Cornerssilt loamWY05-104Immokaleesandy loamFL05-105Alderdalesilt loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-106Hermistonsandy loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-107Pinalsandy clay loamTypicNatrargidAZ05-108Pilot Grovesilty clay loamMollicFluvaquentrMN05-109SacrasheloamLithicHaploxerandCA05-110Linneussilt loamDystricEutrudeptMEspacepricexyu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper1.32627.931.53372.1613.20360.02711.312128.699634.36771.39133.533.67082.160.02920.00991.236630.999736.341911920.81522.163.29490.24062.028116.434625.19581.5423138.63552.1658.30080.00261.203336.036341.23470.73518.912.10232.1646.20870.57082.79486.065518.13911.44438.335.41342.168.33260.00221.201132.819138.00771.7964546.98672.163.94700.09331.569543.596650.37681.7743.546.13192.166.92670.07811.514342.861149.40271.70841.544.09342.166.72560.04731.395741.078747.10811.52935.538.20812.167.33360.00151.197935.620740.79552.23465.561.38762.1616.91160.55272.758355.429667.34561.60748.5540.77262.1660.48770.01361.253138.065943.47931.64841.542.12062.160.38520.02481.302339.307744.93361.60846.540.80552.1632.42740.01381.254138.096643.51441.021821.47282.1612.06010.22141.974317.208325.7372SUMMARY OUTPUTRegression StatisticsMultiple R0.9387807757R Square0.8813093449Adjusted R Square0.8721792945Standard Error4.6124802757Observations15ANOVAdfSSMSFSignificance FRegression12053.6396675182053.63966751896.52842063110.0000002208Residual13276.574665815421.2749742935Total142330.2143333333CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept-12.06361686655.1282445036-2.35238722690.0350696645-23.1425134182-0.9847203147-23.1425134182-0.9847203147X Variable 132.87880190523.34648115239.82488781770.000000220825.649170308640.108433501925.649170308640.1084335019000000000000000000000000000000000000000000000000000000000000xySMP Buffer pHCVu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper7.510.66577896140.70991.980.00190.12480.08680.53800.88186.781.17994100291.32121.980.02000.14190.06311.19621.44637.081.12994350281.07001.980.00360.00590.02311.02431.11577.30.41095890410.88581.980.22540.02050.04860.78960.98197.350.68027210880.84391.980.02680.03740.05730.73040.95746.362.04402515721.67301.980.13770.63470.14261.39061.95536.71.49253731341.38821.980.01090.20850.07791.23401.54247.11.26760563381.05331.980.04590.00320.02341.00691.09967.510.66577896140.70991.980.00190.12480.08680.53800.88187.30.82191780820.88581.980.00410.02050.04860.78960.98197.560.79365079370.66801.980.01580.16270.09630.47740.85867.510.66577896140.70991.980.00190.12480.08680.53800.88187.281.09890109890.90251.980.03860.01520.04520.81310.99196.831.90336749631.27941.980.38940.10670.05421.17211.38677.390.81190798380.81041.980.00000.05440.06450.68260.93827.31.36986301370.88581.980.23440.02050.04860.78960.98196.32.06349206351.72321.980.11580.73390.15421.41792.02857.50.66666666670.71831.980.00270.11790.08490.55010.88657.270.96286107290.91091.980.00270.01280.04350.82480.99706.361.72955974841.67301.980.00320.63470.14261.39061.9553711.13701.980.01880.02450.02801.08151.19257.191.25173852570.97791.980.07500.00110.03140.91571.04007.50.66666666670.71831.980.00270.11790.08490.55010.88657.50.80.71831.980.00670.11790.08490.55010.88657.50.53333333330.71831.980.03420.11790.08490.55010.88657.160.83798882681.00301.980.02720.00000.02780.94801.05806.91.44927536231.22071.980.05220.06590.04221.13711.30447.190.55632823370.97791.980.17770.00110.03140.91571.04006.621.20845921451.45521.980.06090.28800.09291.27131.63927.250.68965517240.92761.980.05660.00870.04020.84801.00737.520.39893617020.70151.980.09160.13200.08870.52590.87726.681.34730538921.40501.980.00330.22720.08161.24341.56667.130.98176718091.02811.980.00210.00070.02500.97861.07767.170.97629009760.99461.980.00030.00020.02890.93741.05186.921.15606936421.20401.980.00230.05600.03901.12671.28136.32.3809523811.72321.980.43260.73390.15421.41792.02856.361.5723270441.67301.980.01010.63470.14261.39061.95537.21.250.96951.980.07870.00190.03270.90471.03437.040.85227272731.10351.980.06310.01360.02451.05511.15196.591.36570561461.48031.980.01310.32110.09861.28511.67566.61.51515151521.47201.980.00190.30990.09671.28051.66346.911.44717800291.21241.980.05510.06080.04061.13191.29287.50.93333333330.71831.980.04620.11790.08490.55010.88657.11.12676056341.05331.980.00540.00320.02341.00691.09967.520.6648936170.70151.980.00130.13200.08870.52590.87727.50.93333333330.71831.980.04620.11790.08490.55010.886571.42857142861.13701.980.08500.02450.02801.08151.19256.611.51285930411.46361.980.00240.29880.09481.27591.65137.11.40845070421.05331.980.12620.00320.02341.00691.09967.491.20160213620.72671.980.22560.11110.08310.56220.89117.591.1857707510.64291.980.29470.18780.10190.44100.84487.540.66312997350.68481.980.00050.14690.09250.50170.86797.60.78947368420.63451.980.02400.19650.10390.42890.84027.540.79575596820.68481.980.01230.14690.09250.50170.86797.470.937081660.74341.980.03750.09820.07930.58630.90057.510.79893475370.70991.980.00790.12480.08680.53800.88187.490.80106809080.72671.980.00550.11110.08310.56220.89117.50.53333333330.71831.980.03420.11790.08490.55010.88656.71.34328358211.38821.980.00200.20850.07791.23401.54246.61.51515151521.47201.980.00190.30990.09671.28051.66347.091.12834978841.06161.980.00450.00440.02321.01581.10756.051.32231404961.93261.980.37241.22470.20261.53152.33367.111.26582278481.04491.980.04880.00220.02380.99781.09207.120.98314606741.03651.980.00280.00130.02430.98841.08467.190.83449235050.97791.980.02060.00110.03140.91571.04007.150.83916083921.01141.980.02970.00000.02670.95851.06437.321.09289617490.86901.980.05010.02670.05200.76600.97207.470.53547523430.74341.980.04320.09820.07930.58630.90057.50.66666666670.71831.980.00270.11790.08490.55010.88656.41.56251.63951.980.00590.57250.13491.37231.90667.50.40.71831.980.10130.11790.08490.55010.88657.40.67567567570.80201.980.01600.05920.06640.67060.93347.20.55555555560.96951.980.17140.00190.03270.90471.03437.010.99857346651.12861.980.01690.02150.02701.07521.18206.811.32158590311.29611.980.00060.12020.05771.18181.41046.91.30434782611.22071.980.00700.06590.04221.13711.30447.20.55555555560.96951.980.17140.00190.03270.90471.03437.530.53120849930.69321.980.02620.13940.09060.51380.87256.921.15606936421.20401.980.00230.05600.03901.12671.28135.523.07971014492.37641.980.49462.67870.30551.77152.98146.921.15606936421.20401.980.00230.05600.03901.12671.28136.41.56251.63951.980.00590.57250.13491.37231.90667.540.79575596820.68481.980.01230.14690.09250.50170.86796.231.92616372391.78181.980.02080.85870.16771.44982.11397.050.85106382981.09511.980.05960.01140.02391.04781.14247.011.14122681881.12861.980.00020.02150.02701.07521.182070.71428571431.13701.980.17870.02450.02801.08151.19256.71.49253731341.38821.980.01090.20850.07791.23401.54247.61.18421052630.63451.980.30210.19650.10390.42890.84027.140.84033613451.01981.980.03220.00030.02580.96871.07087.10.84507042251.05331.980.04330.00320.02341.00691.09967.040.85227272731.10351.980.06310.01360.02451.05511.15197.480.80213903740.73501.980.00450.10450.08120.57430.89587.040.85227272731.10351.980.06310.01360.02451.05511.15197.20.83333333330.96951.980.01850.00190.03270.90471.03437.081.12994350281.07001.980.00360.00590.02311.02431.11576.691.6442451421.39661.980.06130.21780.07981.23871.55456.991.28755364811.14541.980.02020.02780.02921.08761.20317.060.84985835691.08671.980.05610.00930.02351.04031.13327.021.13960113961.12021.980.00040.01870.02601.06881.17177.350.81632653060.84391.980.00080.03740.05730.73040.95747.740.77519379840.51731.980.06650.34030.13060.25860.77596.811.46842878121.29611.980.02970.12020.05771.18181.41047.521.3297872340.70151.980.39470.13200.08870.52590.87726.721.19047619051.37151.980.03280.19070.07421.22461.51836.71.19402985071.38821.980.03770.20850.07791.23401.54247.530.7968127490.69321.980.01070.13940.09060.51380.87257.20.69444444440.96951.980.07570.00190.03270.90471.03436.051.48760330581.93261.980.19801.22470.20261.53152.333661.66666666671.97441.980.09471.33790.21221.55422.39477.540.53050397880.68481.980.02380.14690.09250.50170.86796.991.28755364811.14541.980.02020.02780.02921.08761.20317.191.11265646730.97791.980.01820.00110.03140.91571.04006.71.49253731341.38821.980.01090.20850.07791.23401.54247.460.53619302950.75181.980.04650.09200.07750.59840.90517.420.80862533690.78531.980.00050.06930.07000.64660.92406.921.15606936421.20401.980.00230.05600.03901.12671.28137.10.70422535211.05331.980.12180.00320.02341.00691.09967.50.40.71831.980.10130.11790.08490.55010.88656.740.89020771511.35471.980.21580.17360.07051.21521.4943SUMMARY OUTPUTRegression StatisticsMultiple R0.8113950016R Square0.6583618485Adjusted R Square0.65546661Standard Error0.2530855852Observations120ANOVAdfSSMSFSignificance FRegression114.565155315914.5651553159227.39468000450Residual1187.55817298470.0640523134Total11922.1233283006CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept6.99907439920.393927628217.767411826306.2189912967.77915750246.2189912967.7791575024X Variable 1-0.83743973920.0555345703-15.0796114010-0.9474131882-0.7274662902-0.9474131882-0.7274662902000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000SMP Buffer pH MAD values in the NAPT programChart10.070.050.070.150.20.10.040.10.080.050.10.140.050.080.080.030.050.130.10.090.050.060.060.050.080.130.060.10.130.050.070.110.070.090.050.060.040.060.10.040.080.050.030.090.070.070.080.150.10.090.060.090.10.10.070.080.050.070.10.10.10.090.090.050.060.060.070.060.060.040.090.10.080.080.090.070.060.060.080.040.050.10.030.050.040.070.090.090.040.040.080.170.080.10.060.120.060.080.050.10.090.060.060.060.060.060.060.080.110.090.060.080.060.060.10.10.080.080.060.050.090.10.040.090.080.10.040.060.080.050.030.060.130.030.030.10.050.040.050.040.060.090.030.070.070.080.10.090.060.090.110.050.090.070.070.070.060.040.130.040.080.050.150.050.050.0650.060.080.080.090.080.08pHavg=1.0891022835-0.927avg=1.416850444avg=0.5561509966stdev=0.46489606617.2stdev=0.4585365836stdev=0.350677445Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVW PH CVAE pH CV981137.9427.520.10.07981148.26417.550.130.05981156.714670.080.07981165596.650.160.15981174.86450.080.2981185.9636.40.070.1981197.85387.50.090.04981205.6636.80.10.1981216.9467.080.110.08981228.2367.550.150.05981236.4547.20.10.1981245.15646.50.050.14991018.017.517.837.887.50.110.050.030.66577896140.238235BinFrequency1.37328339580.3831417625991025.796.787.575.826.690.090.080.041.17994100290.914945.2501.55440414510.5284015852991036.987.087.697.097.070.120.080.021.12994350280.636845.45.201.71919770770.2600780234991047.77.37.757.597.250.090.030.010.41095890410.43295.65.401.16883116880.1290322581991057.647.357.687.67.330.070.050.030.68027210880.386555.85.610.91623036650.390625991065.16.367.455.016.30.10.130.062.04402515721.3042865.801.96078431370.8053691275991076.486.77.56.876.860.140.10.031.49253731340.98916.2602.16049382720.4991086.947.17.656.977.10.060.090.081.26760563380.61836.46.210.86455331411.0457516349910987.517.828.027.550.10.050.040.66577896140.238236.66.481.250.5115089514991107.457.37.777.577.290.060.060.050.82191780820.43296.86.630.80536912750.6435006435991118.38537.567.898.217.630.130.060.060.79365079370.1918876.861.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238237.27101.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451447.47.2191.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868597.67.4101.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349477.6261.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.4329More01.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35990.91743119271.1142061281991187.9607.57.837.80.10.050.010.66666666670.24751.26582278480.1277139208991197.4607.277.737.70.10.070.020.96286107290.460711.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304281.22164048870.8241758242_001016.55877.646.570.10.070.0510.711Jan 2005 to June 20051.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.53487IDSMP buffer pHCVn1.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.247521077.26677725120.69055413642110.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.247521106.25522613070.91735297311991.31578947370.630517024_001058587.57.858.17.50.10.040.060.53333333330.247521156.79510526321.03484115231901.250.7643312102_001065.7677.167.85.67.20.10.060.030.83798882680.5626821166.79040462430.85478369521731.75438596490.3846153846_001076.34676.97.486.46.90.090.10.031.44927536230.803741086.62066265061.16049183851661.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.53487P0016.44651162791.1553321806431.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326P0026.89952380951.026837191421.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.47925P0036.693751.0924216278401.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.22896P0047.329250.2536371304400.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.00764P0056.493251.0626376821404.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.59049P0067.09050.5879950257401.9819819820.7682458387_001145.7657.177.815.77.10.090.070.060.97629009760.55341P0076.956250.5306315565401.57894736840.7682458387_001155.8656.927.635.86.80.10.080.061.15606936420.78516P0086.019751.623930658401.7241379310.7863695937_001164.27686.37.344.26.30.070.150.042.3809523811.3599P0096.621751.3057857362401.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428P0106.91444444440.6490363471361.69172932331.8641810919_001185.65687.27.825.57.20.060.090.011.250.52561.06194690270.1278772379_001196.57687.047.626.57.10.070.060.020.85227272730.673921.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.091071.33333333330.9446693657_011014.94706.67.656.40.080.10.041.51515151521.08181.61943319840.5263157895_011026.4706.917.636.56.80.080.10.061.44717800290.794431.250.7863695937_011037.7707.57.87.70.110.070.040.93333333330.24751.42857142860.5128205128_011046.6707.17.696.67.10.10.080.051.12676056340.61831.51515151520.6501950585_011058.1707.527.868.20.10.050.030.6648936170.228961.23456790120.3816793893_011068.09417.57.848.17.530.090.070.010.93333333330.24751.11248454880.1275510204_011076.424177.656.637.090.080.10.051.42857142860.7111.2461059190.6535947712_011085.37416.617.515.516.660.080.10.071.51285930411.072531.48975791430.9320905459_011095.79417.17.815.777.170.090.10.021.40845070420.61831.55440414510.2560819462_011108.02417.497.828.317.50.080.090.021.20160213620.256770.99750623440.2557544757_011118.24377.597.918.197.540.160.090.021.1857707510.164071.94174757280.2528445006_011127.92377.547.797.967.540.080.050.040.66312997350.210421.01010101010.513478819_011138.7377.67.958.927.570.170.060.030.78947368420.15481.95402298850.3773584906_011148.1377.547.858.157.530.10.060.010.79575596820.210421.23456790120.127388535_011157.76377.477.897.837.450.110.070.020.937081660.275311.41752577320.2534854246_011168.1417.517.868.137.510.10.060.030.79893475370.238231.23456790120.3816793893_011177.86417.497.827.927.480.090.060.030.80106809080.256771.14503816790.3836317136_011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.3773584906_011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.8064516129_011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021066.75627.157.686.67.10.040.060.030.83916083920.571950.59259259260.39062520021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021136.85457.27.76.697.260.060.040.030.55555555560.52560.87591240880.389610389620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021176.78667.27.76.657.20.080.040.030.55555555560.52561.17994100290.389610389620021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021196.4666.927.726.626.860.10.080.041.15606936420.785161.56250.51813471520021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031066.1707.01117.65.826.950.10.080.041.14122681880.701731.63934426230.526315789520031076.03707117.585.986.950.070.050.060.71428571430.7111.16086235490.791556728220031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031146.1657.04147.666.197.070.10.060.040.85227272730.673921.63934426230.522193211520031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451421.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364811.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835691.24416796270.642673521920031206697.02157.655.877.080.070.080.041.13960113961.16666666670.52287581720041017.56437.35147.617.47.280.10.060.030.81632653061.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878121.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872341.26582278480.639386189320041055.84436.72147.535.966.830.120.080.071.19047619052.05479452050.929614873820041065.8656.7157.525.766.730.090.080.071.19402985071.55172413790.930851063820041078.24657.53157.778.287.540.090.060.040.7968127491.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444441.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397881.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364813.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646732.41635687730.382165605120041145.76716.7207.515.646.630.070.10.041.49253731341.21527777780.532623169120041157.4717.46207.817.47.40.10.040.020.53619302951.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533691.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936421.23456790121.041666666720041185.9517.1147.785.97.080.10.050.070.70422535211.69491525420.899742930620041197.76517.5147.97.717.470.090.030.060.41.15979381440.759493670920041205.85516.74147.545.86.850.070.060.060.89020771511.19658119660.795755968220050015.64736.40.10.132.031251.773049645420050027.85737.570.080.030.39630118891.019108280320050037.9737.520.10.030.39893617021.265822784820050044.55736.20.090.11.61290322581.97802197820050057.76737.510.090.050.66577896141.159793814420050067.8517.50.10.040.53333333331.282051282120050078.127.550.090.050.66225165561.108374384220050087.837.50.090.040.53333333331.149425287420050096.877.160.110.060.83798882681.601164483320050107.216.910.090.091.30246020261.248266296820050117.8677.50.10.030.41.282051282120050126.37.10.10.070.9859154931.587301587320050137.37.40.130.070.94594594591.780821917820050147.097.20.080.081.11111111111.128349788420050155.056.30.060.11.58730158731.188118811920050165.69666.420.090.091.40186915891.581722319920050177.587.50.110.060.81.451187335120050185.56.350.090.091.41732283461.636363636420050196.486.840.10.111.60818713451.543209876520050207.87.50.10.050.66666666671.282051282120060018.36537.590.10.091.1857707511.196172248820060027.377.330.0850.070.95497953621.153324287720060037.837.430.0750.070.94212651410.957854406120060047.137.30.0750.070.95890410961.051893408120060058.47.520.10.060.79787234041.190476190520060068.36517.50.110.040.53333333331.315789473720060076.16.60.130.131.96969696972.13114754120060087.857.460.080.040.53619302951.019108280320060095.766.890.060.081.16110304791.041666666720060107.017.250.090.050.68965517241.283880171220060114.38676.550.080.152.29007633591.826484018320060128.367.50.10.050.66666666671.1961722488200601387.490.10.050.66755674231.2520060146.116.740.090.0650.96439169141.4729950920060158.47.560.10.060.79365079371.190476190520060168.2547.510.110.081.06524633821.341463414620060178.387.60.110.081.05263157891.3126491647200601866.490.10.091.38674884441.666666666720060198.357.50.120.081.06666666671.437125748520060208.37.50.10.081.06666666671.2048192771Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHpH0.66577896140.69055413641.17994100290.91735297311.12994350281.03484115230.41095890410.85478369520.68027210881.16049183852.04402515721.15533218061.49253731341.0268371911.26760563381.09242162780.66577896140.25363713040.82191780821.06263768210.79365079370.58799502570.66577896140.53063155651.09890109891.6239306581.90336749631.30578573620.81190798380.64903634711.36986301372.06349206350.66666666670.96286107291.729559748411.25173852570.66666666670.80.53333333330.83798882681.44927536230.55632823371.20845921450.68965517240.39893617021.34730538920.98176718090.97629009761.15606936422.3809523811.5723270441.250.85227272731.36570561461.51515151521.44717800290.93333333331.12676056340.6648936170.93333333331.42857142861.51285930411.40845070421.20160213621.1857707510.66312997350.78947368420.79575596820.937081660.79893475370.80106809080.53333333331.34328358211.51515151521.12834978841.32231404961.26582278480.98314606740.83449235050.83916083921.09289617490.53547523430.66666666671.56250.40.67567567570.55555555560.99857346651.32158590311.30434782610.55555555560.53120849931.15606936423.07971014491.15606936421.56250.79575596821.92616372390.85106382981.14122681880.71428571431.49253731341.18421052630.84033613450.84507042250.85227272730.80213903740.85227272730.83333333331.12994350281.6442451421.28755364810.84985835691.13960113960.81632653060.77519379841.46842878121.3297872341.19047619051.19402985070.7968127490.69444444441.48760330581.66666666670.53050397881.28755364811.11265646731.49253731340.53619302950.80862533691.15606936420.70422535210.40.8902077151SMP buffer pHCoefficient of Variation (%)y = -0.837 x + 7.00r 2 = 0.658pH_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)PK_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Soil Description0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000Sheet2min=37max=71This was the graph used in the publication to represent interlab erroraverage=58.7816091954avg=1.1252495213-0.927However, the regression coefficient for all samples was kept in definingavg=1.4798714341avg=0.5942695862median=64stdev=0.45794372377.2error bars (-0.837, 7.00). The difference wasn't deemed great enough tostdev=0.4312774603stdev=0.3982478394Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVrecalculate error bars in other graphs.W PH CVAE pH CV991118.38537.567.898.217.630.130.060.060.79365079370.191885BinFrequency1.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238235.2501.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451445.45.201.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868595.65.401.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349475.85.611.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.432965.801.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35996.2600.91743119271.1142061281991197.4607.277.737.70.10.070.020.96286107290.460716.46.211.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304286.66.481.22164048870.8241758242_001016.55877.646.570.10.070.0510.7116.86.631.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.5348776.861.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.24757.27100.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.24757.47.2191.31578947370.630517024_001076.34676.97.486.46.90.090.10.031.44927536230.80377.67.4101.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.534877.6261.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326More01.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.479251.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.228960.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.007644.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.590491.9819819820.7682458387_001164.27686.37.344.26.30.070.150.042.3809523811.3599Jan 2005 to June 20052.5*CV w2.5*CV wo1.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428IDSMP buffer pHCVnSMP buf pHAlldups1.69172932331.8641810919_001196.57687.047.626.57.10.070.060.020.85227272730.6739221077.26677725120.690554136421164.9454.9831.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.0910721106.25522613070.91735297311996.24.52654.570551.33333333330.944669365720011014.94706.67.656.40.080.10.041.51515151521.081821156.79510526321.03484115231906.44.1084.15811.61943319840.526315789520011026.4706.917.636.56.80.080.10.061.44717800290.7944321166.79040462430.85478369521736.63.68953.745651.250.786369593720011037.7707.57.87.70.110.070.040.93333333330.247541086.62066265061.16049183851666.83.2713.33321.42857142860.512820512820011046.6707.17.696.67.10.10.080.051.12676056340.6183P0016.44651162791.15533218064372.85252.920751.51515151520.650195058520011076.424177.656.637.090.080.10.051.42857142860.711P0026.89952380951.026837191427.22.4342.50831.2461059190.653594771220011085.37416.617.515.516.660.080.10.071.51285930411.07253P0036.693751.0924216278407.42.01552.095851.48975791430.932090545920011095.79417.17.815.777.170.090.10.021.40845070420.6183P0047.329250.2536371304407.61.5971.68341.55440414510.256081946220011108.02417.497.828.317.50.080.090.021.20160213620.25677P0056.493251.0626376821400.99750623440.255754475720011118.24377.597.918.197.540.160.090.021.1857707510.16407P0067.09050.5879950257401.94174757280.252844500620011127.92377.547.797.967.540.080.050.040.66312997350.21042P0076.956250.5306315565401.01010101010.51347881920011138.7377.67.958.927.570.170.060.030.78947368420.1548P0086.019751.623930658401.95402298850.377358490620011157.76377.477.897.837.450.110.070.020.937081660.27531P0096.621751.3057857362401.41752577320.253485424620011177.86417.497.827.927.480.090.060.030.80106809080.25677P0106.91444444440.6490363471361.14503816790.383631713620011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.377358490620011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.806451612920011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451420.998371.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364810.720271.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835690.655381.24416796270.642673521920041017.56437.35147.617.47.280.10.060.030.81632653060.386551.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.025020.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878120.887131.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872340.228961.26582278480.639386189320041078.24657.53157.778.287.540.090.060.040.7968127490.219691.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444440.52561.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.591651.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.6381.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397880.210421.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364810.720273.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646730.534872.41635687730.382165605120041157.4717.46207.817.47.40.10.040.020.53619302950.284581.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533690.321661.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936420.785161.23456790121.041666666720041197.76517.5147.97.717.470.090.030.060.40.24751.15979381440.7594936709Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSheet2000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000SMP buffer pHCoefficient of Variation (%)Sheet3000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Values are in units of mg/kguse ICP-P in these columnswhen it is reported in 2001Sample IDn for M3KM3KM3K MADM3K CVn for M3PM3PM3P MADM3P CV99101795415.15723270448689.302325581499102328267.926829268315418.111.7532467532991038156.172839506244.83.88.48214285719910427371866.7957617831385956.859205776299105627386.060606060663.37.912.480252764699106223146.2780269058101109.9009900999910710187.9207920792406.616.59910846428.76.1853448276363.59.722222222299109782719.07928388758578.23529411769911010776.5420560748292.68.96551724149911142171019011.111111111142735.98.08219178089911242800779.6254289910.11235955069911342535.29.81132075474212214.511.8852459016991144210476.73076923084212.52.52099115429599.47368421054261.626.66666666679911634721638.737864077737282.38.2142857143991173418394.918032786937203159911934140139.28571428573717211.76470588249912034346174.9132947977376845.8823529412_001013512497.258064516143323.912.1875_00102353183811.94968553464333515.1515151515_001033543227.16.2731481481433438.8235294118_0010435228198.33333333334357.67.913.7152777778_0010742456275.92105263164556.54.57.9646017699_001084274345.56.123822341945272.710_0010942402174.228855721445263.212.3076923077_0011042378266.87830687834526134.613.2567049808_0011138871112.6436781609384.22.559.5238095238_00112383126.45161290323859.33.86.4080944351_001133823520.88.85106382983876.111.515.111695138_0011643186147.52688172044350918_00117439410.611.27659574474319.67.638.7755102041_0011943249124.8192771084433937.6923076923_0012043225146.22222222224340.55.914.56790123462001101461651911.51515151523251.87.414.28571428572001102467157610.62937062943225.23.915.4761904762200110346645456.97674418632543.97.2222222222200110446732567.65027322432342.88.23529411762001107492473413.765182186235956.16.421052631620011084958813.79310344833591.516.66666666672001109492422610.7438016529353339.0909090909200111049277238.3032490975354149.756097561200111145304.515346.62.131.8181818182200111245538387.0631970263444.93.98.685968819620011134511414.812.98245614043412.71.29.4488188976200111545312288.9743589744341119.28.28828828832001117491792815.64245810063425.54.517.647058823520011184921322.610.610328638534404.611.520011194910798.4112149533342.50.936200112049141128.510638297934577.412.9824561404200210151252166.3492063492376957.2463768116200210251356267.30337078653775.55.67.4172185432002103511021312.745098039237145149.6551724138200210451957616.374085684437676629.17159763312002105511119857.59606791783792.910.110.8719052745200210749646.19.5312537223.114.090909090920021084919116.58.638743455537171.810.5882352941200210949125129.63719210.52631578952002110492172511.52073732723761.26.510.6209150327200211150484357.23140495873692.66.67.127429805620021125013101199.08396946563698.27.87.9429735234200211450254218.2677165354368.31.720.48192771082002115501531711.11111111113695.18.58.93796004212002116524014210.47381546133816.11.911.80124223620021185274076.510.337837837838604.882002120521672213.17365269463810311.511.16504854372003101467679.2105263158349.51.313.68421052632003102469210.811.73913043483452.6611.406844106520031034646932.46.9083155653439.54.310.8860759494200310446254207.8740157483448.7510.266940451720031054696810210.53719008263453.26.311.84210526322003108492983210.73825503363619913.36.6834170854200310949449439.57683741653633.36.720.1201201201200311049166169.63855421693644.94.19.131403118200311152332216.3253012048404536.666666666720031125212512.19.68403239.3752003113522182210.09174311934080.57.28.9440993789200311552258176.58914728684035.62.46.74157303372003116488889.090909090937211.57.1428571429200311748296289.4594594595376569.2307692308200311848969.29.583333333337111.110200311948144128.333333333337236208.4745762712200410146639467.19874804383460.74.26.919275123620041024649130.76.252545824834207167.72946859920041034620719.79.51690821263446.56.814.623655914200410446468326.83760683763439127.16.9309462916200410746461378.026030368837624.77.58064516132004108461829.55.219780219837424.210200410946364.813.3333333333373.91.128.205128205120041104637513.51351351353713.9214.3884892086200411151429429.790209790241545.710.555555555620041125124528.511.63265306124130.85.116.5584415584200411351421.534.98.27995255044131.63.611.3924050633200411551484489.917355371941159159.4339622642200411649440409.090909090939195157.6923076923200411749123016813.6585365854391852513.513513513520041194913601349.8529411765392092110.047846892005101521612012.42236024844237.83.810.0529100529200510252103675.27.2586872587421179.17.7777777778200510352659426.3732928684227.83.412.2302158273200510452244.619.16666666674291.314.4444444444200510552294196.462585034421001010200510752429327.459207459243303102005109523474512.96829971184329.62.79.12162162162005110522212712.2171945701431732413.8728323699000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3K, mg/kgCV, %000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3P, mg/kgCV, %99-111CozadFluventic HaplustollFluventicHaplustoll99-112LaurenCalcic HaploxerollCalcicHaploxerollc99-113ToccaTypic UdifluventTypicUdifluvent99-114LousivilleTypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)99-115SagcoveONTARIO99-116Pay PointXeric HaplargidXericHaplargid99-117PeelerUstic GlossocryalfUsticGlossocryalf99-118KoenigCalcic HaploxerollCalcicHaploxerollc99-119Belle MinaAL99-120Fort EllisTypic ArgiustollTypicArgiustoll00-101WhitewaterMN00-102KeenesburgUstic HaplargidUsticHaplargidl00-103BensonVertic TorrifluventVerticTorrifluvent00-104OrchardTypic HaplargidTypicHaplargidNM00-105KidmanCalcic HaploxerollCalcicHaploxerollc00-106BlairUstic HaplargidUsticHaplargidl00-107AmsterdamTypic HaplustollTypicHaplustoll00-108AshdosVitritorrandic ArgixerollVitritorrandicArgixeroll00-109WyorAquertic ArgiudollAquerticArgiudoll00-110Bresser IIAridic ArgiustollAridicArgiustoll00-111ShiloUstic TorriorthentUsticTorriorthentmJun-0000-112LignumAquic HapludultAquicHapludult00-113ZenithLamellic HaplustalfLamellicHaplustalf00-114WeldUstic HaplargidUsticHaplargidl00-115Monona IITypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)00-116TellerUdic ArgiustollUdicArgiustollOK00-117GrosecloseTypic HapludultTypicHapludult00-118FrancamUstic HaplargidUsticHaplargidl00-119BrookingsCalcic HapludollCalcicHapludoll00-120AmesAquic HapludollAquicHapludoll01-101O'NeilTypic UstipsammentTypicUstipsamment01-102HastingsUdic ArgiustollUdicArgiustollCO01-103OwngatePachic ArgiustollPachicArgiustoll01-104BrandonAridic ArgiustollAridicArgiustoll01-105TokieUstic TorriorthentUsticTorriorthentmMar-0101-106NikkolaUstic TorriorthentUsticTorriorthentmMar-0101-107NittanyTypic HapludalfTypicHapludalfPA01-108ProvidenceTypic FragiudalfTypicFragiudalfcollected in LA01-109HaxtunPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times01-110ColumbiaXeric HaplocambidXericHaplocambid01-111SonomaUltic HaploxerollUlticHaploxerollCA01-112KoshareUstic HaplocambidUsticHaplocambid01-113PascoXeric TorripsanmmentXericTorripsanmment01-114MaureUstic TorriorthentUsticTorriorthentmMar-0101-115Multi-BlendBLEND01-116EatonUstic TorriorthentUsticTorriorthentmMar-0101-117FairmontMollic FluvaquentMollicFluvaquentr01-118RoseTypic PsammaquentTypicPsammaquent01-119ClemsonTypic KanhapludultTypicKanhapludult01-120EwingEntic HaplustollEnticHaplustoll02-101White WaterMN02-102MarshanTypic EndoaquollTypicEndoaquoll02-103OrangeburgTypic KandiudultTypicKandiudult02-104JewelVertic EndoaquollVerticEndoaquollIowa02-105AscalonAridic ArgiustollAridicArgiustollb02-106AscalonAridic ArgiustollAridicArgiustollb02-107DarcoGrossarenic PaleudultGrossarenicPaleudult02-108HasselPachic HapludollPachicHapludoll02-109WasatchVertic EndoaquollVerticEndoaquollUT02-110KennanHaplic GlossudalfHaplicGlossudalf02-111MaderaTypic HaplocambidTypicHaplocambid02-112RandallUdic PellustertUdicPellustertj02-113AdamsAridic ArgiustollAridicArgiustollb02-114KenomaVertic ArgiudollVerticArgiudoll02-115AthensArenic KandiudultArenicKandiudultcollected by Kissel02-116Monona CTypic HapludollTypicHapludollhsampled by Miller 2 different times (sampled Aug 2002)02-117AdamsAridic ArgiustollAridicArgiustollb02-118BakersfieldTypic ToriorthentTypicToriorthent02-119PhillipsPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times02-120North CarolinaTypic UmbraquultTypicUmbraquult03-101St HelenaTypic HaplustultTypicHaplustult03-102Eagle RiverAK03-103Casa GrandeAZ03-104PerkinsUltic HaplustalfUlticHaplustalf03-105AntonVertic GlossudalfVerticGlossudalfoJan-0303-106BrushVertic GlossudalfVerticGlossudalfoJan-0303-107ArmarilloUdic PellustertUdicPellustertj03-108ThorndikeLithic HaplorthodLithicHaplorthod03-109AirportAquic NatrixerollAquicNatrixeroll03-110PrincetonTypic HapludalfTypicHapludalfIL03-111LelandMS03-112BelmondIA03-113CrestonMT03-114LindonVertic GlossudalfVerticGlossudalfoJan-0303-115GriffyTypic HaplargidTypicHaplargidWY03-116CaptinaTypic FragiudalfTypicFragiudalfeAR03-117Little Flat TopsCO03-118RosettaIL03-119McBrideMI03-120PlatnerVertic GlossudalfVerticGlossudalfoJan-0304-101CassND04-102OteroUstic TorriorthentUsticTorriorthent04-103Del RayAquic ArgiudollAquicArgiudoll04-104GenolaXeric TorrifluventXericTorrifluvent04-105NettieTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-106HarryTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-107MaricopaTypic NatrargidTypicNatrargid04-108Baton RougeLA04-109MatanuskaAK04-110GeorgetownDE04-111Hutton LakeUstic NatrargidUsticNatrargid04-112StewartMN04-113WagramArenic KandiudultArenicKandiudultcollected by Hardy04-114CharlesTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-115San LuisCO04-116UtneMIX04-117MoscowUltic HaploxerollUlticHaploxerollID04-118AltheimerTypic FragiudultTypicFragiudulteAR04-119WahlukeDuric TorriorthentDuricTorriorthent04-120NelsonTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)05-101Parmasilt loamIL05-102Fairburysilt loamID05-103Three Cornerssilt loamWY05-104Immokaleesandy loamFL05-105Alderdalesilt loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-106Hermistonsandy loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-107Pinalsandy clay loamTypicNatrargidAZ05-108Pilot Grovesilty clay loamMollicFluvaquentrMN05-109SacrasheloamLithicHaploxerandCA05-110Linneussilt loamDystricEutrudeptMEspacepricexyu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper1.32627.931.53372.1613.20360.02711.312128.699634.36771.39133.533.67082.160.02920.00991.236630.999736.341911920.81522.163.29490.24062.028116.434625.19581.5423138.63552.1658.30080.00261.203336.036341.23470.73518.912.10232.1646.20870.57082.79486.065518.13911.44438.335.41342.168.33260.00221.201132.819138.00771.7964546.98672.163.94700.09331.569543.596650.37681.7743.546.13192.166.92670.07811.514342.861149.40271.70841.544.09342.166.72560.04731.395741.078747.10811.52935.538.20812.167.33360.00151.197935.620740.79552.23465.561.38762.1616.91160.55272.758355.429667.34561.60748.5540.77262.1660.48770.01361.253138.065943.47931.64841.542.12062.160.38520.02481.302339.307744.93361.60846.540.80552.1632.42740.01381.254138.096643.51441.021821.47282.1612.06010.22141.974317.208325.7372SUMMARY OUTPUTRegression StatisticsMultiple R0.9387807757R Square0.8813093449Adjusted R Square0.8721792945Standard Error4.6124802757Observations15ANOVAdfSSMSFSignificance FRegression12053.6396675182053.63966751896.52842063110.0000002208Residual13276.574665815421.2749742935Total142330.2143333333CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept-12.06361686655.1282445036-2.35238722690.0350696645-23.1425134182-0.9847203147-23.1425134182-0.9847203147X Variable 132.87880190523.34648115239.82488781770.000000220825.649170308640.108433501925.649170308640.1084335019000000000000000000000000000000000000000000000000000000000000xySMP Buffer pHCVu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper7.510.66577896140.70991.980.00190.12480.08680.53800.88186.781.17994100291.32121.980.02000.14190.06311.19621.44637.081.12994350281.07001.980.00360.00590.02311.02431.11577.30.41095890410.88581.980.22540.02050.04860.78960.98197.350.68027210880.84391.980.02680.03740.05730.73040.95746.362.04402515721.67301.980.13770.63470.14261.39061.95536.71.49253731341.38821.980.01090.20850.07791.23401.54247.11.26760563381.05331.980.04590.00320.02341.00691.09967.510.66577896140.70991.980.00190.12480.08680.53800.88187.30.82191780820.88581.980.00410.02050.04860.78960.98197.560.79365079370.66801.980.01580.16270.09630.47740.85867.510.66577896140.70991.980.00190.12480.08680.53800.88187.281.09890109890.90251.980.03860.01520.04520.81310.99196.831.90336749631.27941.980.38940.10670.05421.17211.38677.390.81190798380.81041.980.00000.05440.06450.68260.93827.31.36986301370.88581.980.23440.02050.04860.78960.98196.32.06349206351.72321.980.11580.73390.15421.41792.02857.50.66666666670.71831.980.00270.11790.08490.55010.88657.270.96286107290.91091.980.00270.01280.04350.82480.99706.361.72955974841.67301.980.00320.63470.14261.39061.9553711.13701.980.01880.02450.02801.08151.19257.191.25173852570.97791.980.07500.00110.03140.91571.04007.50.66666666670.71831.980.00270.11790.08490.55010.88657.50.80.71831.980.00670.11790.08490.55010.88657.50.53333333330.71831.980.03420.11790.08490.55010.88657.160.83798882681.00301.980.02720.00000.02780.94801.05806.91.44927536231.22071.980.05220.06590.04221.13711.30447.190.55632823370.97791.980.17770.00110.03140.91571.04006.621.20845921451.45521.980.06090.28800.09291.27131.63927.250.68965517240.92761.980.05660.00870.04020.84801.00737.520.39893617020.70151.980.09160.13200.08870.52590.87726.681.34730538921.40501.980.00330.22720.08161.24341.56667.130.98176718091.02811.980.00210.00070.02500.97861.07767.170.97629009760.99461.980.00030.00020.02890.93741.05186.921.15606936421.20401.980.00230.05600.03901.12671.28136.32.3809523811.72321.980.43260.73390.15421.41792.02856.361.5723270441.67301.980.01010.63470.14261.39061.95537.21.250.96951.980.07870.00190.03270.90471.03437.040.85227272731.10351.980.06310.01360.02451.05511.15196.591.36570561461.48031.980.01310.32110.09861.28511.67566.61.51515151521.47201.980.00190.30990.09671.28051.66346.911.44717800291.21241.980.05510.06080.04061.13191.29287.50.93333333330.71831.980.04620.11790.08490.55010.88657.11.12676056341.05331.980.00540.00320.02341.00691.09967.520.6648936170.70151.980.00130.13200.08870.52590.87727.50.93333333330.71831.980.04620.11790.08490.55010.886571.42857142861.13701.980.08500.02450.02801.08151.19256.611.51285930411.46361.980.00240.29880.09481.27591.65137.11.40845070421.05331.980.12620.00320.02341.00691.09967.491.20160213620.72671.980.22560.11110.08310.56220.89117.591.1857707510.64291.980.29470.18780.10190.44100.84487.540.66312997350.68481.980.00050.14690.09250.50170.86797.60.78947368420.63451.980.02400.19650.10390.42890.84027.540.79575596820.68481.980.01230.14690.09250.50170.86797.470.937081660.74341.980.03750.09820.07930.58630.90057.510.79893475370.70991.980.00790.12480.08680.53800.88187.490.80106809080.72671.980.00550.11110.08310.56220.89117.50.53333333330.71831.980.03420.11790.08490.55010.88656.71.34328358211.38821.980.00200.20850.07791.23401.54246.61.51515151521.47201.980.00190.30990.09671.28051.66347.091.12834978841.06161.980.00450.00440.02321.01581.10756.051.32231404961.93261.980.37241.22470.20261.53152.33367.111.26582278481.04491.980.04880.00220.02380.99781.09207.120.98314606741.03651.980.00280.00130.02430.98841.08467.190.83449235050.97791.980.02060.00110.03140.91571.04007.150.83916083921.01141.980.02970.00000.02670.95851.06437.321.09289617490.86901.980.05010.02670.05200.76600.97207.470.53547523430.74341.980.04320.09820.07930.58630.90057.50.66666666670.71831.980.00270.11790.08490.55010.88656.41.56251.63951.980.00590.57250.13491.37231.90667.50.40.71831.980.10130.11790.08490.55010.88657.40.67567567570.80201.980.01600.05920.06640.67060.93347.20.55555555560.96951.980.17140.00190.03270.90471.03437.010.99857346651.12861.980.01690.02150.02701.07521.18206.811.32158590311.29611.980.00060.12020.05771.18181.41046.91.30434782611.22071.980.00700.06590.04221.13711.30447.20.55555555560.96951.980.17140.00190.03270.90471.03437.530.53120849930.69321.980.02620.13940.09060.51380.87256.921.15606936421.20401.980.00230.05600.03901.12671.28135.523.07971014492.37641.980.49462.67870.30551.77152.98146.921.15606936421.20401.980.00230.05600.03901.12671.28136.41.56251.63951.980.00590.57250.13491.37231.90667.540.79575596820.68481.980.01230.14690.09250.50170.86796.231.92616372391.78181.980.02080.85870.16771.44982.11397.050.85106382981.09511.980.05960.01140.02391.04781.14247.011.14122681881.12861.980.00020.02150.02701.07521.182070.71428571431.13701.980.17870.02450.02801.08151.19256.71.49253731341.38821.980.01090.20850.07791.23401.54247.61.18421052630.63451.980.30210.19650.10390.42890.84027.140.84033613451.01981.980.03220.00030.02580.96871.07087.10.84507042251.05331.980.04330.00320.02341.00691.09967.040.85227272731.10351.980.06310.01360.02451.05511.15197.480.80213903740.73501.980.00450.10450.08120.57430.89587.040.85227272731.10351.980.06310.01360.02451.05511.15197.20.83333333330.96951.980.01850.00190.03270.90471.03437.081.12994350281.07001.980.00360.00590.02311.02431.11576.691.6442451421.39661.980.06130.21780.07981.23871.55456.991.28755364811.14541.980.02020.02780.02921.08761.20317.060.84985835691.08671.980.05610.00930.02351.04031.13327.021.13960113961.12021.980.00040.01870.02601.06881.17177.350.81632653060.84391.980.00080.03740.05730.73040.95747.740.77519379840.51731.980.06650.34030.13060.25860.77596.811.46842878121.29611.980.02970.12020.05771.18181.41047.521.3297872340.70151.980.39470.13200.08870.52590.87726.721.19047619051.37151.980.03280.19070.07421.22461.51836.71.19402985071.38821.980.03770.20850.07791.23401.54247.530.7968127490.69321.980.01070.13940.09060.51380.87257.20.69444444440.96951.980.07570.00190.03270.90471.03436.051.48760330581.93261.980.19801.22470.20261.53152.333661.66666666671.97441.980.09471.33790.21221.55422.39477.540.53050397880.68481.980.02380.14690.09250.50170.86796.991.28755364811.14541.980.02020.02780.02921.08761.20317.191.11265646730.97791.980.01820.00110.03140.91571.04006.71.49253731341.38821.980.01090.20850.07791.23401.54247.460.53619302950.75181.980.04650.09200.07750.59840.90517.420.80862533690.78531.980.00050.06930.07000.64660.92406.921.15606936421.20401.980.00230.05600.03901.12671.28137.10.70422535211.05331.980.12180.00320.02341.00691.09967.50.40.71831.980.10130.11790.08490.55010.88656.740.89020771511.35471.980.21580.17360.07051.21521.4943SUMMARY OUTPUTRegression StatisticsMultiple R0.8113950016R Square0.6583618485Adjusted R Square0.65546661Standard Error0.2530855852Observations120ANOVAdfSSMSFSignificance FRegression114.565155315914.5651553159227.39468000450Residual1187.55817298470.0640523134Total11922.1233283006CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept6.99907439920.393927628217.767411826306.2189912967.77915750246.2189912967.7791575024X Variable 1-0.83743973920.0555345703-15.0796114010-0.9474131882-0.7274662902-0.9474131882-0.7274662902000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000extra slidesChart50.66577896140.69055413641.17994100290.91735297311.12994350281.03484115230.41095890410.85478369520.68027210881.16049183852.04402515721.15533218061.49253731341.0268371911.26760563381.09242162780.66577896140.25363713040.82191780821.06263768210.79365079370.58799502570.66577896140.53063155651.09890109891.6239306581.90336749631.30578573620.81190798380.64903634711.36986301372.06349206350.66666666670.96286107291.729559748411.25173852570.66666666670.80.53333333330.83798882681.44927536230.55632823371.20845921450.68965517240.39893617021.34730538920.98176718090.97629009761.15606936422.3809523811.5723270441.250.85227272731.36570561461.51515151521.44717800290.93333333331.12676056340.6648936170.93333333331.42857142861.51285930411.40845070421.20160213621.1857707510.66312997350.78947368420.79575596820.937081660.79893475370.80106809080.53333333331.34328358211.51515151521.12834978841.32231404961.26582278480.98314606740.83449235050.83916083921.09289617490.53547523430.66666666671.56250.40.67567567570.55555555560.99857346651.32158590311.30434782610.55555555560.53120849931.15606936423.07971014491.15606936421.56250.79575596821.92616372390.85106382981.14122681880.71428571431.49253731341.18421052630.84033613450.84507042250.85227272730.80213903740.85227272730.83333333331.12994350281.6442451421.28755364810.84985835691.13960113960.81632653060.77519379841.46842878121.3297872341.19047619051.19402985070.7968127490.69444444441.48760330581.66666666670.53050397881.28755364811.11265646731.49253731340.53619302950.80862533691.15606936420.70422535210.40.8902077151SMP buffer pHCoefficient of Variation (%)y = -0.837 x + 7.00r 2 = 0.658pHavg=1.0891022835-0.927avg=1.416850444avg=0.5561509966stdev=0.46489606617.2stdev=0.4585365836stdev=0.350677445Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVW PH CVAE pH CV981137.9427.520.10.07981148.26417.550.130.05981156.714670.080.07981165596.650.160.15981174.86450.080.2981185.9636.40.070.1981197.85387.50.090.04981205.6636.80.10.1981216.9467.080.110.08981228.2367.550.150.05981236.4547.20.10.1981245.15646.50.050.14991018.017.517.837.887.50.110.050.030.66577896140.238235BinFrequency1.37328339580.3831417625991025.796.787.575.826.690.090.080.041.17994100290.914945.2501.55440414510.5284015852991036.987.087.697.097.070.120.080.021.12994350280.636845.45.201.71919770770.2600780234991047.77.37.757.597.250.090.030.010.41095890410.43295.65.401.16883116880.1290322581991057.647.357.687.67.330.070.050.030.68027210880.386555.85.610.91623036650.390625991065.16.367.455.016.30.10.130.062.04402515721.3042865.801.96078431370.8053691275991076.486.77.56.876.860.140.10.031.49253731340.98916.2602.16049382720.4991086.947.17.656.977.10.060.090.081.26760563380.61836.46.210.86455331411.0457516349910987.517.828.027.550.10.050.040.66577896140.238236.66.481.250.5115089514991107.457.37.777.577.290.060.060.050.82191780820.43296.86.630.80536912750.6435006435991118.38537.567.898.217.630.130.060.060.79365079370.1918876.861.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238237.27101.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451447.47.2191.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868597.67.4101.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349477.6261.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.4329More01.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35990.91743119271.1142061281991187.9607.57.837.80.10.050.010.66666666670.24751.26582278480.1277139208991197.4607.277.737.70.10.070.020.96286107290.460711.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304281.22164048870.8241758242_001016.55877.646.570.10.070.0510.711Jan 2005 to June 20051.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.53487IDSMP buffer pHCVn1.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.247521077.26677725120.69055413642110.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.247521106.25522613070.91735297311991.31578947370.630517024_001058587.57.858.17.50.10.040.060.53333333330.247521156.79510526321.03484115231901.250.7643312102_001065.7677.167.85.67.20.10.060.030.83798882680.5626821166.79040462430.85478369521731.75438596490.3846153846_001076.34676.97.486.46.90.090.10.031.44927536230.803741086.62066265061.16049183851661.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.53487P0016.44651162791.1553321806431.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326P0026.89952380951.026837191421.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.47925P0036.693751.0924216278401.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.22896P0047.329250.2536371304400.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.00764P0056.493251.0626376821404.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.59049P0067.09050.5879950257401.9819819820.7682458387_001145.7657.177.815.77.10.090.070.060.97629009760.55341P0076.956250.5306315565401.57894736840.7682458387_001155.8656.927.635.86.80.10.080.061.15606936420.78516P0086.019751.623930658401.7241379310.7863695937_001164.27686.37.344.26.30.070.150.042.3809523811.3599P0096.621751.3057857362401.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428P0106.91444444440.6490363471361.69172932331.8641810919_001185.65687.27.825.57.20.060.090.011.250.52561.06194690270.1278772379_001196.57687.047.626.57.10.070.060.020.85227272730.673921.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.091071.33333333330.9446693657_011014.94706.67.656.40.080.10.041.51515151521.08181.61943319840.5263157895_011026.4706.917.636.56.80.080.10.061.44717800290.794431.250.7863695937_011037.7707.57.87.70.110.070.040.93333333330.24751.42857142860.5128205128_011046.6707.17.696.67.10.10.080.051.12676056340.61831.51515151520.6501950585_011058.1707.527.868.20.10.050.030.6648936170.228961.23456790120.3816793893_011068.09417.57.848.17.530.090.070.010.93333333330.24751.11248454880.1275510204_011076.424177.656.637.090.080.10.051.42857142860.7111.2461059190.6535947712_011085.37416.617.515.516.660.080.10.071.51285930411.072531.48975791430.9320905459_011095.79417.17.815.777.170.090.10.021.40845070420.61831.55440414510.2560819462_011108.02417.497.828.317.50.080.090.021.20160213620.256770.99750623440.2557544757_011118.24377.597.918.197.540.160.090.021.1857707510.164071.94174757280.2528445006_011127.92377.547.797.967.540.080.050.040.66312997350.210421.01010101010.513478819_011138.7377.67.958.927.570.170.060.030.78947368420.15481.95402298850.3773584906_011148.1377.547.858.157.530.10.060.010.79575596820.210421.23456790120.127388535_011157.76377.477.897.837.450.110.070.020.937081660.275311.41752577320.2534854246_011168.1417.517.868.137.510.10.060.030.79893475370.238231.23456790120.3816793893_011177.86417.497.827.927.480.090.060.030.80106809080.256771.14503816790.3836317136_011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.3773584906_011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.8064516129_011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021066.75627.157.686.67.10.040.060.030.83916083920.571950.59259259260.39062520021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021136.85457.27.76.697.260.060.040.030.55555555560.52560.87591240880.389610389620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021176.78667.27.76.657.20.080.040.030.55555555560.52561.17994100290.389610389620021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021196.4666.927.726.626.860.10.080.041.15606936420.785161.56250.51813471520021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031066.1707.01117.65.826.950.10.080.041.14122681880.701731.63934426230.526315789520031076.03707117.585.986.950.070.050.060.71428571430.7111.16086235490.791556728220031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031146.1657.04147.666.197.070.10.060.040.85227272730.673921.63934426230.522193211520031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451421.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364811.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835691.24416796270.642673521920031206697.02157.655.877.080.070.080.041.13960113961.16666666670.52287581720041017.56437.35147.617.47.280.10.060.030.81632653061.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878121.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872341.26582278480.639386189320041055.84436.72147.535.966.830.120.080.071.19047619052.05479452050.929614873820041065.8656.7157.525.766.730.090.080.071.19402985071.55172413790.930851063820041078.24657.53157.778.287.540.090.060.040.7968127491.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444441.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397881.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364813.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646732.41635687730.382165605120041145.76716.7207.515.646.630.070.10.041.49253731341.21527777780.532623169120041157.4717.46207.817.47.40.10.040.020.53619302951.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533691.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936421.23456790121.041666666720041185.9517.1147.785.97.080.10.050.070.70422535211.69491525420.899742930620041197.76517.5147.97.717.470.090.030.060.41.15979381440.759493670920041205.85516.74147.545.86.850.070.060.060.89020771511.19658119660.795755968220050015.64736.40.10.132.031251.773049645420050027.85737.570.080.030.39630118891.019108280320050037.9737.520.10.030.39893617021.265822784820050044.55736.20.090.11.61290322581.97802197820050057.76737.510.090.050.66577896141.159793814420050067.8517.50.10.040.53333333331.282051282120050078.127.550.090.050.66225165561.108374384220050087.837.50.090.040.53333333331.149425287420050096.877.160.110.060.83798882681.601164483320050107.216.910.090.091.30246020261.248266296820050117.8677.50.10.030.41.282051282120050126.37.10.10.070.9859154931.587301587320050137.37.40.130.070.94594594591.780821917820050147.097.20.080.081.11111111111.128349788420050155.056.30.060.11.58730158731.188118811920050165.69666.420.090.091.40186915891.581722319920050177.587.50.110.060.81.451187335120050185.56.350.090.091.41732283461.636363636420050196.486.840.10.111.60818713451.543209876520050207.87.50.10.050.66666666671.282051282120060018.36537.590.10.091.1857707511.196172248820060027.377.330.0850.070.95497953621.153324287720060037.837.430.0750.070.94212651410.957854406120060047.137.30.0750.070.95890410961.051893408120060058.47.520.10.060.79787234041.190476190520060068.36517.50.110.040.53333333331.315789473720060076.16.60.130.131.96969696972.13114754120060087.857.460.080.040.53619302951.019108280320060095.766.890.060.081.16110304791.041666666720060107.017.250.090.050.68965517241.283880171220060114.38676.550.080.152.29007633591.826484018320060128.367.50.10.050.66666666671.1961722488200601387.490.10.050.66755674231.2520060146.116.740.090.0650.96439169141.4729950920060158.47.560.10.060.79365079371.190476190520060168.2547.510.110.081.06524633821.341463414620060178.387.60.110.081.05263157891.3126491647200601866.490.10.091.38674884441.666666666720060198.357.50.120.081.06666666671.437125748520060208.37.50.10.081.06666666671.2048192771Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHpHSMP buffer pHCoefficient of Variation (%)y = -0.837 x + 7.00r 2 = 0.658pH_woDupswater pHCoefficient of Variation (%)PK_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Soil DescriptionSheet2min=37max=71This was the graph used in the publication to represent interlab erroraverage=58.7816091954avg=1.1252495213-0.927However, the regression coefficient for all samples was kept in definingavg=1.4798714341avg=0.5942695862median=64stdev=0.45794372377.2error bars (-0.837, 7.00). The difference wasn't deemed great enough tostdev=0.4312774603stdev=0.3982478394Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVrecalculate error bars in other graphs.W PH CVAE pH CV991118.38537.567.898.217.630.130.060.060.79365079370.191885BinFrequency1.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238235.2501.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451445.45.201.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868595.65.401.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349475.85.611.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.432965.801.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35996.2600.91743119271.1142061281991197.4607.277.737.70.10.070.020.96286107290.460716.46.211.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304286.66.481.22164048870.8241758242_001016.55877.646.570.10.070.0510.7116.86.631.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.5348776.861.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.24757.27100.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.24757.47.2191.31578947370.630517024_001076.34676.97.486.46.90.090.10.031.44927536230.80377.67.4101.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.534877.6261.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326More01.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.479251.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.228960.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.007644.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.590491.9819819820.7682458387_001164.27686.37.344.26.30.070.150.042.3809523811.3599Jan 2005 to June 20052.5*CV w2.5*CV wo1.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428IDSMP buffer pHCVnSMP buf pHAlldups1.69172932331.8641810919_001196.57687.047.626.57.10.070.060.020.85227272730.6739221077.26677725120.690554136421164.9454.9831.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.0910721106.25522613070.91735297311996.24.52654.570551.33333333330.944669365720011014.94706.67.656.40.080.10.041.51515151521.081821156.79510526321.03484115231906.44.1084.15811.61943319840.526315789520011026.4706.917.636.56.80.080.10.061.44717800290.7944321166.79040462430.85478369521736.63.68953.745651.250.786369593720011037.7707.57.87.70.110.070.040.93333333330.247541086.62066265061.16049183851666.83.2713.33321.42857142860.512820512820011046.6707.17.696.67.10.10.080.051.12676056340.6183P0016.44651162791.15533218064372.85252.920751.51515151520.650195058520011076.424177.656.637.090.080.10.051.42857142860.711P0026.89952380951.026837191427.22.4342.50831.2461059190.653594771220011085.37416.617.515.516.660.080.10.071.51285930411.07253P0036.693751.0924216278407.42.01552.095851.48975791430.932090545920011095.79417.17.815.777.170.090.10.021.40845070420.6183P0047.329250.2536371304407.61.5971.68341.55440414510.256081946220011108.02417.497.828.317.50.080.090.021.20160213620.25677P0056.493251.0626376821400.99750623440.255754475720011118.24377.597.918.197.540.160.090.021.1857707510.16407P0067.09050.5879950257401.94174757280.252844500620011127.92377.547.797.967.540.080.050.040.66312997350.21042P0076.956250.5306315565401.01010101010.51347881920011138.7377.67.958.927.570.170.060.030.78947368420.1548P0086.019751.623930658401.95402298850.377358490620011157.76377.477.897.837.450.110.070.020.937081660.27531P0096.621751.3057857362401.41752577320.253485424620011177.86417.497.827.927.480.090.060.030.80106809080.25677P0106.91444444440.6490363471361.14503816790.383631713620011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.377358490620011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.806451612920011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451420.998371.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364810.720271.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835690.655381.24416796270.642673521920041017.56437.35147.617.47.280.10.060.030.81632653060.386551.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.025020.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878120.887131.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872340.228961.26582278480.639386189320041078.24657.53157.778.287.540.090.060.040.7968127490.219691.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444440.52561.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.591651.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.6381.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397880.210421.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364810.720273.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646730.534872.41635687730.382165605120041157.4717.46207.817.47.40.10.040.020.53619302950.284581.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533690.321661.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936420.785161.23456790121.041666666720041197.76517.5147.97.717.470.090.030.060.40.24751.15979381440.7594936709Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSheet2000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000SMP buffer pHCoefficient of Variation (%)Sheet3000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Values are in units of mg/kguse ICP-P in these columnswhen it is reported in 2001Sample IDn for M3KM3KM3K MADM3K CVn for M3PM3PM3P MADM3P CV99101795415.15723270448689.302325581499102328267.926829268315418.111.7532467532991038156.172839506244.83.88.48214285719910427371866.7957617831385956.859205776299105627386.060606060663.37.912.480252764699106223146.2780269058101109.9009900999910710187.9207920792406.616.59910846428.76.1853448276363.59.722222222299109782719.07928388758578.23529411769911010776.5420560748292.68.96551724149911142171019011.111111111142735.98.08219178089911242800779.6254289910.11235955069911342535.29.81132075474212214.511.8852459016991144210476.73076923084212.52.52099115429599.47368421054261.626.66666666679911634721638.737864077737282.38.2142857143991173418394.918032786937203159911934140139.28571428573717211.76470588249912034346174.9132947977376845.8823529412_001013512497.258064516143323.912.1875_00102353183811.94968553464333515.1515151515_001033543227.16.2731481481433438.8235294118_0010435228198.33333333334357.67.913.7152777778_0010742456275.92105263164556.54.57.9646017699_001084274345.56.123822341945272.710_0010942402174.228855721445263.212.3076923077_0011042378266.87830687834526134.613.2567049808_0011138871112.6436781609384.22.559.5238095238_00112383126.45161290323859.33.86.4080944351_001133823520.88.85106382983876.111.515.111695138_0011643186147.52688172044350918_00117439410.611.27659574474319.67.638.7755102041_0011943249124.8192771084433937.6923076923_0012043225146.22222222224340.55.914.56790123462001101461651911.51515151523251.87.414.28571428572001102467157610.62937062943225.23.915.4761904762200110346645456.97674418632543.97.2222222222200110446732567.65027322432342.88.23529411762001107492473413.765182186235956.16.421052631620011084958813.79310344833591.516.66666666672001109492422610.7438016529353339.0909090909200111049277238.3032490975354149.756097561200111145304.515346.62.131.8181818182200111245538387.0631970263444.93.98.685968819620011134511414.812.98245614043412.71.29.4488188976200111545312288.9743589744341119.28.28828828832001117491792815.64245810063425.54.517.647058823520011184921322.610.610328638534404.611.520011194910798.4112149533342.50.936200112049141128.510638297934577.412.9824561404200210151252166.3492063492376957.2463768116200210251356267.30337078653775.55.67.4172185432002103511021312.745098039237145149.6551724138200210451957616.374085684437676629.17159763312002105511119857.59606791783792.910.110.8719052745200210749646.19.5312537223.114.090909090920021084919116.58.638743455537171.810.5882352941200210949125129.63719210.52631578952002110492172511.52073732723761.26.510.6209150327200211150484357.23140495873692.66.67.127429805620021125013101199.08396946563698.27.87.9429735234200211450254218.2677165354368.31.720.48192771082002115501531711.11111111113695.18.58.93796004212002116524014210.47381546133816.11.911.80124223620021185274076.510.337837837838604.882002120521672213.17365269463810311.511.16504854372003101467679.2105263158349.51.313.68421052632003102469210.811.73913043483452.6611.406844106520031034646932.46.9083155653439.54.310.8860759494200310446254207.8740157483448.7510.266940451720031054696810210.53719008263453.26.311.84210526322003108492983210.73825503363619913.36.6834170854200310949449439.57683741653633.36.720.1201201201200311049166169.63855421693644.94.19.131403118200311152332216.3253012048404536.666666666720031125212512.19.68403239.3752003113522182210.09174311934080.57.28.9440993789200311552258176.58914728684035.62.46.74157303372003116488889.090909090937211.57.1428571429200311748296289.4594594595376569.2307692308200311848969.29.583333333337111.110200311948144128.333333333337236208.4745762712200410146639467.19874804383460.74.26.919275123620041024649130.76.252545824834207167.72946859920041034620719.79.51690821263446.56.814.623655914200410446468326.83760683763439127.16.9309462916200410746461378.026030368837624.77.58064516132004108461829.55.219780219837424.210200410946364.813.3333333333373.91.128.205128205120041104637513.51351351353713.9214.3884892086200411151429429.790209790241545.710.555555555620041125124528.511.63265306124130.85.116.5584415584200411351421.534.98.27995255044131.63.611.3924050633200411551484489.917355371941159159.4339622642200411649440409.090909090939195157.6923076923200411749123016813.6585365854391852513.513513513520041194913601349.8529411765392092110.047846892005101521612012.42236024844237.83.810.0529100529200510252103675.27.2586872587421179.17.7777777778200510352659426.3732928684227.83.412.2302158273200510452244.619.16666666674291.314.4444444444200510552294196.462585034421001010200510752429327.459207459243303102005109523474512.96829971184329.62.79.12162162162005110522212712.2171945701431732413.8728323699000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3K, mg/kgCV, %000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3P, mg/kgCV, %99-111CozadFluventic HaplustollFluventicHaplustoll99-112LaurenCalcic HaploxerollCalcicHaploxerollc99-113ToccaTypic UdifluventTypicUdifluvent99-114LousivilleTypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)99-115SagcoveONTARIO99-116Pay PointXeric HaplargidXericHaplargid99-117PeelerUstic GlossocryalfUsticGlossocryalf99-118KoenigCalcic HaploxerollCalcicHaploxerollc99-119Belle MinaAL99-120Fort EllisTypic ArgiustollTypicArgiustoll00-101WhitewaterMN00-102KeenesburgUstic HaplargidUsticHaplargidl00-103BensonVertic TorrifluventVerticTorrifluvent00-104OrchardTypic HaplargidTypicHaplargidNM00-105KidmanCalcic HaploxerollCalcicHaploxerollc00-106BlairUstic HaplargidUsticHaplargidl00-107AmsterdamTypic HaplustollTypicHaplustoll00-108AshdosVitritorrandic ArgixerollVitritorrandicArgixeroll00-109WyorAquertic ArgiudollAquerticArgiudoll00-110Bresser IIAridic ArgiustollAridicArgiustoll00-111ShiloUstic TorriorthentUsticTorriorthentmJun-0000-112LignumAquic HapludultAquicHapludult00-113ZenithLamellic HaplustalfLamellicHaplustalf00-114WeldUstic HaplargidUsticHaplargidl00-115Monona IITypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)00-116TellerUdic ArgiustollUdicArgiustollOK00-117GrosecloseTypic HapludultTypicHapludult00-118FrancamUstic HaplargidUsticHaplargidl00-119BrookingsCalcic HapludollCalcicHapludoll00-120AmesAquic HapludollAquicHapludoll01-101O'NeilTypic UstipsammentTypicUstipsamment01-102HastingsUdic ArgiustollUdicArgiustollCO01-103OwngatePachic ArgiustollPachicArgiustoll01-104BrandonAridic ArgiustollAridicArgiustoll01-105TokieUstic TorriorthentUsticTorriorthentmMar-0101-106NikkolaUstic TorriorthentUsticTorriorthentmMar-0101-107NittanyTypic HapludalfTypicHapludalfPA01-108ProvidenceTypic FragiudalfTypicFragiudalfcollected in LA01-109HaxtunPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times01-110ColumbiaXeric HaplocambidXericHaplocambid01-111SonomaUltic HaploxerollUlticHaploxerollCA01-112KoshareUstic HaplocambidUsticHaplocambid01-113PascoXeric TorripsanmmentXericTorripsanmment01-114MaureUstic TorriorthentUsticTorriorthentmMar-0101-115Multi-BlendBLEND01-116EatonUstic TorriorthentUsticTorriorthentmMar-0101-117FairmontMollic FluvaquentMollicFluvaquentr01-118RoseTypic PsammaquentTypicPsammaquent01-119ClemsonTypic KanhapludultTypicKanhapludult01-120EwingEntic HaplustollEnticHaplustoll02-101White WaterMN02-102MarshanTypic EndoaquollTypicEndoaquoll02-103OrangeburgTypic KandiudultTypicKandiudult02-104JewelVertic EndoaquollVerticEndoaquollIowa02-105AscalonAridic ArgiustollAridicArgiustollb02-106AscalonAridic ArgiustollAridicArgiustollb02-107DarcoGrossarenic PaleudultGrossarenicPaleudult02-108HasselPachic HapludollPachicHapludoll02-109WasatchVertic EndoaquollVerticEndoaquollUT02-110KennanHaplic GlossudalfHaplicGlossudalf02-111MaderaTypic HaplocambidTypicHaplocambid02-112RandallUdic PellustertUdicPellustertj02-113AdamsAridic ArgiustollAridicArgiustollb02-114KenomaVertic ArgiudollVerticArgiudoll02-115AthensArenic KandiudultArenicKandiudultcollected by Kissel02-116Monona CTypic HapludollTypicHapludollhsampled by Miller 2 different times (sampled Aug 2002)02-117AdamsAridic ArgiustollAridicArgiustollb02-118BakersfieldTypic ToriorthentTypicToriorthent02-119PhillipsPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times02-120North CarolinaTypic UmbraquultTypicUmbraquult03-101St HelenaTypic HaplustultTypicHaplustult03-102Eagle RiverAK03-103Casa GrandeAZ03-104PerkinsUltic HaplustalfUlticHaplustalf03-105AntonVertic GlossudalfVerticGlossudalfoJan-0303-106BrushVertic GlossudalfVerticGlossudalfoJan-0303-107ArmarilloUdic PellustertUdicPellustertj03-108ThorndikeLithic HaplorthodLithicHaplorthod03-109AirportAquic NatrixerollAquicNatrixeroll03-110PrincetonTypic HapludalfTypicHapludalfIL03-111LelandMS03-112BelmondIA03-113CrestonMT03-114LindonVertic GlossudalfVerticGlossudalfoJan-0303-115GriffyTypic HaplargidTypicHaplargidWY03-116CaptinaTypic FragiudalfTypicFragiudalfeAR03-117Little Flat TopsCO03-118RosettaIL03-119McBrideMI03-120PlatnerVertic GlossudalfVerticGlossudalfoJan-0304-101CassND04-102OteroUstic TorriorthentUsticTorriorthent04-103Del RayAquic ArgiudollAquicArgiudoll04-104GenolaXeric TorrifluventXericTorrifluvent04-105NettieTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-106HarryTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-107MaricopaTypic NatrargidTypicNatrargid04-108Baton RougeLA04-109MatanuskaAK04-110GeorgetownDE04-111Hutton LakeUstic NatrargidUsticNatrargid04-112StewartMN04-113WagramArenic KandiudultArenicKandiudultcollected by Hardy04-114CharlesTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-115San LuisCO04-116UtneMIX04-117MoscowUltic HaploxerollUlticHaploxerollID04-118AltheimerTypic FragiudultTypicFragiudulteAR04-119WahlukeDuric TorriorthentDuricTorriorthent04-120NelsonTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)05-101Parmasilt loamIL05-102Fairburysilt loamID05-103Three Cornerssilt loamWY05-104Immokaleesandy loamFL05-105Alderdalesilt loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-106Hermistonsandy loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-107Pinalsandy clay loamTypicNatrargidAZ05-108Pilot Grovesilty clay loamMollicFluvaquentrMN05-109SacrasheloamLithicHaploxerandCA05-110Linneussilt loamDystricEutrudeptMEspacepricexyu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper1.32627.931.53372.1613.20360.02711.312128.699634.36771.39133.533.67082.160.02920.00991.236630.999736.341911920.81522.163.29490.24062.028116.434625.19581.5423138.63552.1658.30080.00261.203336.036341.23470.73518.912.10232.1646.20870.57082.79486.065518.13911.44438.335.41342.168.33260.00221.201132.819138.00771.7964546.98672.163.94700.09331.569543.596650.37681.7743.546.13192.166.92670.07811.514342.861149.40271.70841.544.09342.166.72560.04731.395741.078747.10811.52935.538.20812.167.33360.00151.197935.620740.79552.23465.561.38762.1616.91160.55272.758355.429667.34561.60748.5540.77262.1660.48770.01361.253138.065943.47931.64841.542.12062.160.38520.02481.302339.307744.93361.60846.540.80552.1632.42740.01381.254138.096643.51441.021821.47282.1612.06010.22141.974317.208325.7372SUMMARY OUTPUTRegression StatisticsMultiple R0.9387807757R Square0.8813093449Adjusted R Square0.8721792945Standard Error4.6124802757Observations15ANOVAdfSSMSFSignificance FRegression12053.6396675182053.63966751896.52842063110.0000002208Residual13276.574665815421.2749742935Total142330.2143333333CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept-12.06361686655.1282445036-2.35238722690.0350696645-23.1425134182-0.9847203147-23.1425134182-0.9847203147X Variable 132.87880190523.34648115239.82488781770.000000220825.649170308640.108433501925.649170308640.1084335019000000000000000000000000000000000000000000000000000000000000xySMP Buffer pHCVu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper7.510.66577896140.70991.980.00190.12480.08680.53800.88186.781.17994100291.32121.980.02000.14190.06311.19621.44637.081.12994350281.07001.980.00360.00590.02311.02431.11577.30.41095890410.88581.980.22540.02050.04860.78960.98197.350.68027210880.84391.980.02680.03740.05730.73040.95746.362.04402515721.67301.980.13770.63470.14261.39061.95536.71.49253731341.38821.980.01090.20850.07791.23401.54247.11.26760563381.05331.980.04590.00320.02341.00691.09967.510.66577896140.70991.980.00190.12480.08680.53800.88187.30.82191780820.88581.980.00410.02050.04860.78960.98197.560.79365079370.66801.980.01580.16270.09630.47740.85867.510.66577896140.70991.980.00190.12480.08680.53800.88187.281.09890109890.90251.980.03860.01520.04520.81310.99196.831.90336749631.27941.980.38940.10670.05421.17211.38677.390.81190798380.81041.980.00000.05440.06450.68260.93827.31.36986301370.88581.980.23440.02050.04860.78960.98196.32.06349206351.72321.980.11580.73390.15421.41792.02857.50.66666666670.71831.980.00270.11790.08490.55010.88657.270.96286107290.91091.980.00270.01280.04350.82480.99706.361.72955974841.67301.980.00320.63470.14261.39061.9553711.13701.980.01880.02450.02801.08151.19257.191.25173852570.97791.980.07500.00110.03140.91571.04007.50.66666666670.71831.980.00270.11790.08490.55010.88657.50.80.71831.980.00670.11790.08490.55010.88657.50.53333333330.71831.980.03420.11790.08490.55010.88657.160.83798882681.00301.980.02720.00000.02780.94801.05806.91.44927536231.22071.980.05220.06590.04221.13711.30447.190.55632823370.97791.980.17770.00110.03140.91571.04006.621.20845921451.45521.980.06090.28800.09291.27131.63927.250.68965517240.92761.980.05660.00870.04020.84801.00737.520.39893617020.70151.980.09160.13200.08870.52590.87726.681.34730538921.40501.980.00330.22720.08161.24341.56667.130.98176718091.02811.980.00210.00070.02500.97861.07767.170.97629009760.99461.980.00030.00020.02890.93741.05186.921.15606936421.20401.980.00230.05600.03901.12671.28136.32.3809523811.72321.980.43260.73390.15421.41792.02856.361.5723270441.67301.980.01010.63470.14261.39061.95537.21.250.96951.980.07870.00190.03270.90471.03437.040.85227272731.10351.980.06310.01360.02451.05511.15196.591.36570561461.48031.980.01310.32110.09861.28511.67566.61.51515151521.47201.980.00190.30990.09671.28051.66346.911.44717800291.21241.980.05510.06080.04061.13191.29287.50.93333333330.71831.980.04620.11790.08490.55010.88657.11.12676056341.05331.980.00540.00320.02341.00691.09967.520.6648936170.70151.980.00130.13200.08870.52590.87727.50.93333333330.71831.980.04620.11790.08490.55010.886571.42857142861.13701.980.08500.02450.02801.08151.19256.611.51285930411.46361.980.00240.29880.09481.27591.65137.11.40845070421.05331.980.12620.00320.02341.00691.09967.491.20160213620.72671.980.22560.11110.08310.56220.89117.591.1857707510.64291.980.29470.18780.10190.44100.84487.540.66312997350.68481.980.00050.14690.09250.50170.86797.60.78947368420.63451.980.02400.19650.10390.42890.84027.540.79575596820.68481.980.01230.14690.09250.50170.86797.470.937081660.74341.980.03750.09820.07930.58630.90057.510.79893475370.70991.980.00790.12480.08680.53800.88187.490.80106809080.72671.980.00550.11110.08310.56220.89117.50.53333333330.71831.980.03420.11790.08490.55010.88656.71.34328358211.38821.980.00200.20850.07791.23401.54246.61.51515151521.47201.980.00190.30990.09671.28051.66347.091.12834978841.06161.980.00450.00440.02321.01581.10756.051.32231404961.93261.980.37241.22470.20261.53152.33367.111.26582278481.04491.980.04880.00220.02380.99781.09207.120.98314606741.03651.980.00280.00130.02430.98841.08467.190.83449235050.97791.980.02060.00110.03140.91571.04007.150.83916083921.01141.980.02970.00000.02670.95851.06437.321.09289617490.86901.980.05010.02670.05200.76600.97207.470.53547523430.74341.980.04320.09820.07930.58630.90057.50.66666666670.71831.980.00270.11790.08490.55010.88656.41.56251.63951.980.00590.57250.13491.37231.90667.50.40.71831.980.10130.11790.08490.55010.88657.40.67567567570.80201.980.01600.05920.06640.67060.93347.20.55555555560.96951.980.17140.00190.03270.90471.03437.010.99857346651.12861.980.01690.02150.02701.07521.18206.811.32158590311.29611.980.00060.12020.05771.18181.41046.91.30434782611.22071.980.00700.06590.04221.13711.30447.20.55555555560.96951.980.17140.00190.03270.90471.03437.530.53120849930.69321.980.02620.13940.09060.51380.87256.921.15606936421.20401.980.00230.05600.03901.12671.28135.523.07971014492.37641.980.49462.67870.30551.77152.98146.921.15606936421.20401.980.00230.05600.03901.12671.28136.41.56251.63951.980.00590.57250.13491.37231.90667.540.79575596820.68481.980.01230.14690.09250.50170.86796.231.92616372391.78181.980.02080.85870.16771.44982.11397.050.85106382981.09511.980.05960.01140.02391.04781.14247.011.14122681881.12861.980.00020.02150.02701.07521.182070.71428571431.13701.980.17870.02450.02801.08151.19256.71.49253731341.38821.980.01090.20850.07791.23401.54247.61.18421052630.63451.980.30210.19650.10390.42890.84027.140.84033613451.01981.980.03220.00030.02580.96871.07087.10.84507042251.05331.980.04330.00320.02341.00691.09967.040.85227272731.10351.980.06310.01360.02451.05511.15197.480.80213903740.73501.980.00450.10450.08120.57430.89587.040.85227272731.10351.980.06310.01360.02451.05511.15197.20.83333333330.96951.980.01850.00190.03270.90471.03437.081.12994350281.07001.980.00360.00590.02311.02431.11576.691.6442451421.39661.980.06130.21780.07981.23871.55456.991.28755364811.14541.980.02020.02780.02921.08761.20317.060.84985835691.08671.980.05610.00930.02351.04031.13327.021.13960113961.12021.980.00040.01870.02601.06881.17177.350.81632653060.84391.980.00080.03740.05730.73040.95747.740.77519379840.51731.980.06650.34030.13060.25860.77596.811.46842878121.29611.980.02970.12020.05771.18181.41047.521.3297872340.70151.980.39470.13200.08870.52590.87726.721.19047619051.37151.980.03280.19070.07421.22461.51836.71.19402985071.38821.980.03770.20850.07791.23401.54247.530.7968127490.69321.980.01070.13940.09060.51380.87257.20.69444444440.96951.980.07570.00190.03270.90471.03436.051.48760330581.93261.980.19801.22470.20261.53152.333661.66666666671.97441.980.09471.33790.21221.55422.39477.540.53050397880.68481.980.02380.14690.09250.50170.86796.991.28755364811.14541.980.02020.02780.02921.08761.20317.191.11265646730.97791.980.01820.00110.03140.91571.04006.71.49253731341.38821.980.01090.20850.07791.23401.54247.460.53619302950.75181.980.04650.09200.07750.59840.90517.420.80862533690.78531.980.00050.06930.07000.64660.92406.921.15606936421.20401.980.00230.05600.03901.12671.28137.10.70422535211.05331.980.12180.00320.02341.00691.09967.50.40.71831.980.10130.11790.08490.55010.88656.740.89020771511.35471.980.21580.17360.07051.21521.4943SUMMARY OUTPUTRegression StatisticsMultiple R0.8113950016R Square0.6583618485Adjusted R Square0.65546661Standard Error0.2530855852Observations120ANOVAdfSSMSFSignificance FRegression114.565155315914.5651553159227.39468000450Residual1187.55817298470.0640523134Total11922.1233283006CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept6.99907439920.393927628217.767411826306.2189912967.77915750246.2189912967.7791575024X Variable 1-0.83743973920.0555345703-15.0796114010-0.9474131882-0.7274662902-0.9474131882-0.7274662902000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000Chart61.37328339581.55440414511.71919770771.16883116880.91623036651.96078431372.16049382720.86455331411.250.80536912751.55131264921.251.53846153851.85185185191.55440414511.87416331990.91743119271.26582278481.35135135141.22164048871.53846153851.75438596490.89058524171.31578947371.251.75438596491.41955835961.33928571431.34453781511.47058823530.72551390574.16666666671.9819819821.57894736841.7241379311.63934426231.69172932331.06194690271.06544901071.33333333331.61943319841.251.42857142861.51515151521.23456790121.11248454881.2461059191.48975791431.55440414510.99750623441.94174757281.01010101011.95402298851.23456790121.41752577321.23456790121.14503816791.2468827931.50943396231.9067796611.41955835961.09090909091.53846153851.13960113961.17994100290.59259259260.79365079370.99378881991.47058823532.16606498191.28040973111.03492884860.87591240881.28571428571.77619893431.04529616721.17994100291.29870129871.56251.5686274511.75718849841.52284263961.26582278481.93133047211.63934426231.63934426231.16086235491.45454545451.388888888921.61290322581.23456790121.31578947371.63934426231.02489019031.19658119661.55172413791.77705977381.24416796271.16666666671.32275132280.93896713621.54083204931.26582278482.05479452051.55172413791.09223300971.40845070421.81159420291.65975103731.26582278483.21489001692.41635687731.21527777781.35135135141.29870129871.23456790121.69491525421.15979381441.1965811966water pHCoefficient of Variation (%)pHavg=1.0891022835-0.927avg=1.416850444avg=0.5561509966stdev=0.46489606617.2stdev=0.4585365836stdev=0.350677445Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVW PH CVAE pH CV981137.9427.520.10.07981148.26417.550.130.05981156.714670.080.07981165596.650.160.15981174.86450.080.2981185.9636.40.070.1981197.85387.50.090.04981205.6636.80.10.1981216.9467.080.110.08981228.2367.550.150.05981236.4547.20.10.1981245.15646.50.050.14991018.017.517.837.887.50.110.050.030.66577896140.238235BinFrequency1.37328339580.3831417625991025.796.787.575.826.690.090.080.041.17994100290.914945.2501.55440414510.5284015852991036.987.087.697.097.070.120.080.021.12994350280.636845.45.201.71919770770.2600780234991047.77.37.757.597.250.090.030.010.41095890410.43295.65.401.16883116880.1290322581991057.647.357.687.67.330.070.050.030.68027210880.386555.85.610.91623036650.390625991065.16.367.455.016.30.10.130.062.04402515721.3042865.801.96078431370.8053691275991076.486.77.56.876.860.140.10.031.49253731340.98916.2602.16049382720.4991086.947.17.656.977.10.060.090.081.26760563380.61836.46.210.86455331411.0457516349910987.517.828.027.550.10.050.040.66577896140.238236.66.481.250.5115089514991107.457.37.777.577.290.060.060.050.82191780820.43296.86.630.80536912750.6435006435991118.38537.567.898.217.630.130.060.060.79365079370.1918876.861.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238237.27101.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451447.47.2191.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868597.67.4101.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349477.6261.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.4329More01.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35990.91743119271.1142061281991187.9607.57.837.80.10.050.010.66666666670.24751.26582278480.1277139208991197.4607.277.737.70.10.070.020.96286107290.460711.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304281.22164048870.8241758242_001016.55877.646.570.10.070.0510.711Jan 2005 to June 20051.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.53487IDSMP buffer pHCVn1.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.247521077.26677725120.69055413642110.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.247521106.25522613070.91735297311991.31578947370.630517024_001058587.57.858.17.50.10.040.060.53333333330.247521156.79510526321.03484115231901.250.7643312102_001065.7677.167.85.67.20.10.060.030.83798882680.5626821166.79040462430.85478369521731.75438596490.3846153846_001076.34676.97.486.46.90.090.10.031.44927536230.803741086.62066265061.16049183851661.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.53487P0016.44651162791.1553321806431.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326P0026.89952380951.026837191421.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.47925P0036.693751.0924216278401.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.22896P0047.329250.2536371304400.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.00764P0056.493251.0626376821404.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.59049P0067.09050.5879950257401.9819819820.7682458387_001145.7657.177.815.77.10.090.070.060.97629009760.55341P0076.956250.5306315565401.57894736840.7682458387_001155.8656.927.635.86.80.10.080.061.15606936420.78516P0086.019751.623930658401.7241379310.7863695937_001164.27686.37.344.26.30.070.150.042.3809523811.3599P0096.621751.3057857362401.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428P0106.91444444440.6490363471361.69172932331.8641810919_001185.65687.27.825.57.20.060.090.011.250.52561.06194690270.1278772379_001196.57687.047.626.57.10.070.060.020.85227272730.673921.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.091071.33333333330.9446693657_011014.94706.67.656.40.080.10.041.51515151521.08181.61943319840.5263157895_011026.4706.917.636.56.80.080.10.061.44717800290.794431.250.7863695937_011037.7707.57.87.70.110.070.040.93333333330.24751.42857142860.5128205128_011046.6707.17.696.67.10.10.080.051.12676056340.61831.51515151520.6501950585_011058.1707.527.868.20.10.050.030.6648936170.228961.23456790120.3816793893_011068.09417.57.848.17.530.090.070.010.93333333330.24751.11248454880.1275510204_011076.424177.656.637.090.080.10.051.42857142860.7111.2461059190.6535947712_011085.37416.617.515.516.660.080.10.071.51285930411.072531.48975791430.9320905459_011095.79417.17.815.777.170.090.10.021.40845070420.61831.55440414510.2560819462_011108.02417.497.828.317.50.080.090.021.20160213620.256770.99750623440.2557544757_011118.24377.597.918.197.540.160.090.021.1857707510.164071.94174757280.2528445006_011127.92377.547.797.967.540.080.050.040.66312997350.210421.01010101010.513478819_011138.7377.67.958.927.570.170.060.030.78947368420.15481.95402298850.3773584906_011148.1377.547.858.157.530.10.060.010.79575596820.210421.23456790120.127388535_011157.76377.477.897.837.450.110.070.020.937081660.275311.41752577320.2534854246_011168.1417.517.868.137.510.10.060.030.79893475370.238231.23456790120.3816793893_011177.86417.497.827.927.480.090.060.030.80106809080.256771.14503816790.3836317136_011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.3773584906_011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.8064516129_011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021066.75627.157.686.67.10.040.060.030.83916083920.571950.59259259260.39062520021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021136.85457.27.76.697.260.060.040.030.55555555560.52560.87591240880.389610389620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021176.78667.27.76.657.20.080.040.030.55555555560.52561.17994100290.389610389620021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021196.4666.927.726.626.860.10.080.041.15606936420.785161.56250.51813471520021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031066.1707.01117.65.826.950.10.080.041.14122681880.701731.63934426230.526315789520031076.03707117.585.986.950.070.050.060.71428571430.7111.16086235490.791556728220031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031146.1657.04147.666.197.070.10.060.040.85227272730.673921.63934426230.522193211520031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451421.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364811.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835691.24416796270.642673521920031206697.02157.655.877.080.070.080.041.13960113961.16666666670.52287581720041017.56437.35147.617.47.280.10.060.030.81632653061.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878121.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872341.26582278480.639386189320041055.84436.72147.535.966.830.120.080.071.19047619052.05479452050.929614873820041065.8656.7157.525.766.730.090.080.071.19402985071.55172413790.930851063820041078.24657.53157.778.287.540.090.060.040.7968127491.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444441.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397881.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364813.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646732.41635687730.382165605120041145.76716.7207.515.646.630.070.10.041.49253731341.21527777780.532623169120041157.4717.46207.817.47.40.10.040.020.53619302951.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533691.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936421.23456790121.041666666720041185.9517.1147.785.97.080.10.050.070.70422535211.69491525420.899742930620041197.76517.5147.97.717.470.090.030.060.41.15979381440.759493670920041205.85516.74147.545.86.850.070.060.060.89020771511.19658119660.795755968220050015.64736.40.10.132.031251.773049645420050027.85737.570.080.030.39630118891.019108280320050037.9737.520.10.030.39893617021.265822784820050044.55736.20.090.11.61290322581.97802197820050057.76737.510.090.050.66577896141.159793814420050067.8517.50.10.040.53333333331.282051282120050078.127.550.090.050.66225165561.108374384220050087.837.50.090.040.53333333331.149425287420050096.877.160.110.060.83798882681.601164483320050107.216.910.090.091.30246020261.248266296820050117.8677.50.10.030.41.282051282120050126.37.10.10.070.9859154931.587301587320050137.37.40.130.070.94594594591.780821917820050147.097.20.080.081.11111111111.128349788420050155.056.30.060.11.58730158731.188118811920050165.69666.420.090.091.40186915891.581722319920050177.587.50.110.060.81.451187335120050185.56.350.090.091.41732283461.636363636420050196.486.840.10.111.60818713451.543209876520050207.87.50.10.050.66666666671.282051282120060018.36537.590.10.091.1857707511.196172248820060027.377.330.0850.070.95497953621.153324287720060037.837.430.0750.070.94212651410.957854406120060047.137.30.0750.070.95890410961.051893408120060058.47.520.10.060.79787234041.190476190520060068.36517.50.110.040.53333333331.315789473720060076.16.60.130.131.96969696972.13114754120060087.857.460.080.040.53619302951.019108280320060095.766.890.060.081.16110304791.041666666720060107.017.250.090.050.68965517241.283880171220060114.38676.550.080.152.29007633591.826484018320060128.367.50.10.050.66666666671.1961722488200601387.490.10.050.66755674231.2520060146.116.740.090.0650.96439169141.4729950920060158.47.560.10.060.79365079371.190476190520060168.2547.510.110.081.06524633821.341463414620060178.387.60.110.081.05263157891.3126491647200601866.490.10.091.38674884441.666666666720060198.357.50.120.081.06666666671.437125748520060208.37.50.10.081.06666666671.2048192771Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHpHSMP buffer pHCoefficient of Variation (%)y = -0.837 x + 7.00r 2 = 0.658pH_woDupswater pHCoefficient of Variation (%)PK_woDups000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Soil DescriptionSheet2min=37max=71This was the graph used in the publication to represent interlab erroraverage=58.7816091954avg=1.1252495213-0.927However, the regression coefficient for all samples was kept in definingavg=1.4798714341avg=0.5942695862median=64stdev=0.45794372377.2error bars (-0.837, 7.00). The difference wasn't deemed great enough tostdev=0.4312774603stdev=0.3982478394Sample IDSoil pH (1:1)n for SMPSMP Buffer pHn for Adams-EvansAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSMP CVrecalculate error bars in other graphs.W PH CVAE pH CV991118.38537.567.898.217.630.130.060.060.79365079370.191885BinFrequency1.55131264920.7604562738991128537.517.878.157.610.10.050.040.66577896140.238235.2501.250.5082592122991136.5537.287.876.357.350.10.080.031.09890109890.451445.45.201.53846153850.3811944091991145.4536.837.585.246.890.10.130.031.90336749630.868595.65.401.85185185190.3957783641991157.72537.397.767.497.460.120.060.040.81190798380.349475.85.611.55440414510.5154639175991167.47607.37.767.40.140.10.021.36986301370.432965.801.87416331990.2577319588991175.45606.37.185.46.20.050.130.082.06349206351.35996.2600.91743119271.1142061281991197.4607.277.737.70.10.070.020.96286107290.460716.46.211.35135135140.2587322122991205.73606.367.285.86.30.070.110.061.72955974841.304286.66.481.22164048870.8241758242_001016.55877.646.570.10.070.0510.7116.86.631.53846153850.6544502618_001025.7587.197.8467.10.10.090.041.25173852570.5348776.861.75438596490.5102040816_001037.86587.57.777.67.50.070.050.030.66666666670.24757.27100.89058524170.3861003861_001047.6587.57.937.97.40.10.060.050.80.24757.47.2191.31578947370.630517024_001076.34676.97.486.46.90.090.10.031.44927536230.80377.67.4101.41955835960.4010695187_001086.72677.197.696.77.20.090.040.020.55632823370.534877.6261.33928571430.2600780234_001095.95676.627.3866.80.080.080.021.20845921451.06326More01.34453781510.27100271_001106.8677.257.766.87.30.10.050.020.68965517240.479251.47058823530.2577319588_001118.27657.527.868.20.060.030.040.39893617020.228960.72551390570.5089058524_001124.8656.687.635.16.50.20.090.081.34730538921.007644.16666666671.0484927916_001135.55657.137.815.570.110.070.060.98176718090.590491.9819819820.7682458387_001164.27686.37.344.26.30.070.150.042.3809523811.3599Jan 2005 to June 20052.5*CV w2.5*CV wo1.63934426230.5449591281_001175.32686.367.515.36.40.090.10.141.5723270441.30428IDSMP buffer pHCVnSMP buf pHAlldups1.69172932331.8641810919_001196.57687.047.626.57.10.070.060.020.85227272730.6739221077.26677725120.690554136421164.9454.9831.06544901070.2624671916_001206686.597.4166.70.080.090.071.36570561461.0910721106.25522613070.91735297311996.24.52654.570551.33333333330.944669365720011014.94706.67.656.40.080.10.041.51515151521.081821156.79510526321.03484115231906.44.1084.15811.61943319840.526315789520011026.4706.917.636.56.80.080.10.061.44717800290.7944321166.79040462430.85478369521736.63.68953.745651.250.786369593720011037.7707.57.87.70.110.070.040.93333333330.247541086.62066265061.16049183851666.83.2713.33321.42857142860.512820512820011046.6707.17.696.67.10.10.080.051.12676056340.6183P0016.44651162791.15533218064372.85252.920751.51515151520.650195058520011076.424177.656.637.090.080.10.051.42857142860.711P0026.89952380951.026837191427.22.4342.50831.2461059190.653594771220011085.37416.617.515.516.660.080.10.071.51285930411.07253P0036.693751.0924216278407.42.01552.095851.48975791430.932090545920011095.79417.17.815.777.170.090.10.021.40845070420.6183P0047.329250.2536371304407.61.5971.68341.55440414510.256081946220011108.02417.497.828.317.50.080.090.021.20160213620.25677P0056.493251.0626376821400.99750623440.255754475720011118.24377.597.918.197.540.160.090.021.1857707510.16407P0067.09050.5879950257401.94174757280.252844500620011127.92377.547.797.967.540.080.050.040.66312997350.21042P0076.956250.5306315565401.01010101010.51347881920011138.7377.67.958.927.570.170.060.030.78947368420.1548P0086.019751.623930658401.95402298850.377358490620011157.76377.477.897.837.450.110.070.020.937081660.27531P0096.621751.3057857362401.41752577320.253485424620011177.86417.497.827.927.480.090.060.030.80106809080.25677P0106.91444444440.6490363471361.14503816790.383631713620011188.02417.57.958.167.530.10.040.030.53333333330.24751.2468827930.377358490620011195.3416.77.445.26.730.080.090.061.34328358210.98911.50943396230.806451612920011204.72416.67.584.776.670.090.10.051.51515151521.08181.9067796610.659630606920021016.34657.097.746.427.080.090.080.041.12834978840.627571.41955835960.516795865620021025.5656.057.195.526.090.060.080.071.32231404961.591651.09090909090.973574408920021036.5657.117.776.567.10.10.090.041.26582278480.609031.53846153850.514800514820021047.02657.127.697.057.120.080.070.030.98314606740.599761.13960113960.390117035120021056.78657.197.696.687.180.080.060.040.83449235050.534871.17994100290.520156046820021076.3627.327.926.27.260.050.080.031.09289617490.414360.79365079370.378787878820021088.05627.477.878.057.390.080.040.030.53547523430.275310.99378881990.381194409120021098.16627.57.887.440.120.050.040.66666666670.24751.47058823530.512820512820021105.54626.47.45.426.320.120.10.071.56251.26722.16606498190.945945945920021117.81457.57.857.737.550.10.030.020.40.24751.28040973110.254777070120021127.73457.47.567.787.440.080.050.020.67567567570.34021.03492884860.264550264620021147457.017.56.97.080.090.070.040.99857346650.701731.28571428570.533333333320021155.63456.817.645.636.890.10.090.041.32158590310.887131.77619893430.523560209420021165.74666.97.615.776.940.060.090.041.30434782610.80371.04529616720.525624178720021187.7667.537.737.597.510.10.040.040.53120849930.219691.29870129870.517464424320021205.1665.527.025.295.740.080.170.173.07971014492.082961.5686274512.421652421720031016.26646.92127.596.266.90.110.080.021.15606936420.785161.75718849840.263504611320031025.91646.4127.256.096.40.090.10.051.56251.26721.52284263960.689655172420031037.9647.54127.857.957.510.10.060.050.79575596820.210421.26582278480.636942675220031044.66646.23127.224.656.050.090.120.121.92616372391.424791.93133047211.662049861520031056.1647.05127.625.886.940.10.060.050.85106382980.664651.63934426230.65616797920031085.5706.7117.525.746.730.080.10.071.49253731340.98911.45454545450.930851063820031099.36707.6117.899.317.560.130.090.041.18421052630.15481.38888888890.506970849220031106.5707.14117.786.737.160.130.060.030.84033613450.5812220.385604113120031116.2657.1147.796.17.050.10.060.040.84507042250.61831.61290322580.51347881920031126.48657.04147.676.527.030.080.060.020.85227272730.673921.23456790120.26075619320031137.6657.48147.887.347.460.10.060.040.80213903740.266041.31578947370.507614213220031156.83657.2147.736.747.160.070.060.030.83333333330.52561.02489019030.388098318220031165.85697.08157.775.897.010.070.080.031.12994350280.636841.19658119660.386100386120031175.8696.69157.585.926.70.090.110.061.6442451420.998371.55172413790.791556728220031186.19696.99157.76.247.020.110.090.041.28755364810.720271.77705977380.519480519520031196.43697.06157.786.77.060.080.060.050.84985835690.655381.24416796270.642673521920041017.56437.35147.617.47.280.10.060.030.81632653060.386551.32275132280.39421813420041028.52437.74147.848.447.690.080.060.040.77519379840.025020.93896713620.510204081620041036.49436.81147.536.46.910.10.10.051.46842878120.887131.54083204930.664010624220041047.9437.52147.827.887.510.10.10.051.3297872340.228961.26582278480.639386189320041078.24657.53157.778.287.540.090.060.040.7968127490.219691.09223300970.514800514820041087.1657.2157.747.157.230.10.050.040.69444444440.52561.40845070420.516795865620041095.52656.05157.065.576.070.10.090.161.48760330581.591651.81159420292.266288951820041104.82656157.274.855.910.080.10.051.66666666671.6381.65975103730.687757909220041117.9717.54207.877.767.480.10.040.020.53050397880.210421.26582278480.254129606120041125.91716.99207.75.866.90.190.090.031.28755364810.720273.21489001690.389610389620041135.38717.19207.855.397.110.130.080.031.11265646730.534872.41635687730.382165605120041157.4717.46207.817.47.40.10.040.020.53619302950.284581.35135135140.256081946220041167.7517.42147.817.647.410.10.060.030.80862533690.321661.29870129870.384122919320041176.48516.92147.686.487.010.080.080.081.15606936420.785161.23456790121.041666666720041197.76517.5147.97.717.470.090.030.060.40.24751.15979381440.7594936709Sample IDSoil pH (1:1)SMP Buffer pHAdams-Evans Buf pHOur Water pH (1:1)Our SMP Buffer pHMAD soil pH (1:1)MAD SMP Buffer pHMAD Adams-Evans Buffer pHSheet2000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000SMP buffer pHCoefficient of Variation (%)Sheet3000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)000000000000000000000000000000000000000000000000000000000000000000000000000000000000000water pHCoefficient of Variation (%)Values are in units of mg/kguse ICP-P in these columnswhen it is reported in 2001Sample IDn for M3KM3KM3K MADM3K CVn for M3PM3PM3P MADM3P CV99101795415.15723270448689.302325581499102328267.926829268315418.111.7532467532991038156.172839506244.83.88.48214285719910427371866.7957617831385956.859205776299105627386.060606060663.37.912.480252764699106223146.2780269058101109.9009900999910710187.9207920792406.616.59910846428.76.1853448276363.59.722222222299109782719.07928388758578.23529411769911010776.5420560748292.68.96551724149911142171019011.111111111142735.98.08219178089911242800779.6254289910.11235955069911342535.29.81132075474212214.511.8852459016991144210476.73076923084212.52.52099115429599.47368421054261.626.66666666679911634721638.737864077737282.38.2142857143991173418394.918032786937203159911934140139.28571428573717211.76470588249912034346174.9132947977376845.8823529412_001013512497.258064516143323.912.1875_00102353183811.94968553464333515.1515151515_001033543227.16.2731481481433438.8235294118_0010435228198.33333333334357.67.913.7152777778_0010742456275.92105263164556.54.57.9646017699_001084274345.56.123822341945272.710_0010942402174.228855721445263.212.3076923077_0011042378266.87830687834526134.613.2567049808_0011138871112.6436781609384.22.559.5238095238_00112383126.45161290323859.33.86.4080944351_001133823520.88.85106382983876.111.515.111695138_0011643186147.52688172044350918_00117439410.611.27659574474319.67.638.7755102041_0011943249124.8192771084433937.6923076923_0012043225146.22222222224340.55.914.56790123462001101461651911.51515151523251.87.414.28571428572001102467157610.62937062943225.23.915.4761904762200110346645456.97674418632543.97.2222222222200110446732567.65027322432342.88.23529411762001107492473413.765182186235956.16.421052631620011084958813.79310344833591.516.66666666672001109492422610.7438016529353339.0909090909200111049277238.3032490975354149.756097561200111145304.515346.62.131.8181818182200111245538387.0631970263444.93.98.685968819620011134511414.812.98245614043412.71.29.4488188976200111545312288.9743589744341119.28.28828828832001117491792815.64245810063425.54.517.647058823520011184921322.610.610328638534404.611.520011194910798.4112149533342.50.936200112049141128.510638297934577.412.9824561404200210151252166.3492063492376957.2463768116200210251356267.30337078653775.55.67.4172185432002103511021312.745098039237145149.6551724138200210451957616.374085684437676629.17159763312002105511119857.59606791783792.910.110.8719052745200210749646.19.5312537223.114.090909090920021084919116.58.638743455537171.810.5882352941200210949125129.63719210.52631578952002110492172511.52073732723761.26.510.6209150327200211150484357.23140495873692.66.67.127429805620021125013101199.08396946563698.27.87.9429735234200211450254218.2677165354368.31.720.48192771082002115501531711.11111111113695.18.58.93796004212002116524014210.47381546133816.11.911.80124223620021185274076.510.337837837838604.882002120521672213.17365269463810311.511.16504854372003101467679.2105263158349.51.313.68421052632003102469210.811.73913043483452.6611.406844106520031034646932.46.9083155653439.54.310.8860759494200310446254207.8740157483448.7510.266940451720031054696810210.53719008263453.26.311.84210526322003108492983210.73825503363619913.36.6834170854200310949449439.57683741653633.36.720.1201201201200311049166169.63855421693644.94.19.131403118200311152332216.3253012048404536.666666666720031125212512.19.68403239.3752003113522182210.09174311934080.57.28.9440993789200311552258176.58914728684035.62.46.74157303372003116488889.090909090937211.57.1428571429200311748296289.4594594595376569.2307692308200311848969.29.583333333337111.110200311948144128.333333333337236208.4745762712200410146639467.19874804383460.74.26.919275123620041024649130.76.252545824834207167.72946859920041034620719.79.51690821263446.56.814.623655914200410446468326.83760683763439127.16.9309462916200410746461378.026030368837624.77.58064516132004108461829.55.219780219837424.210200410946364.813.3333333333373.91.128.205128205120041104637513.51351351353713.9214.3884892086200411151429429.790209790241545.710.555555555620041125124528.511.63265306124130.85.116.5584415584200411351421.534.98.27995255044131.63.611.3924050633200411551484489.917355371941159159.4339622642200411649440409.090909090939195157.6923076923200411749123016813.6585365854391852513.513513513520041194913601349.8529411765392092110.047846892005101521612012.42236024844237.83.810.0529100529200510252103675.27.2586872587421179.17.7777777778200510352659426.3732928684227.83.412.2302158273200510452244.619.16666666674291.314.4444444444200510552294196.462585034421001010200510752429327.459207459243303102005109523474512.96829971184329.62.79.12162162162005110522212712.2171945701431732413.8728323699000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3K, mg/kgCV, %000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000M3P, mg/kgCV, %99-111CozadFluventic HaplustollFluventicHaplustoll99-112LaurenCalcic HaploxerollCalcicHaploxerollc99-113ToccaTypic UdifluventTypicUdifluvent99-114LousivilleTypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)99-115SagcoveONTARIO99-116Pay PointXeric HaplargidXericHaplargid99-117PeelerUstic GlossocryalfUsticGlossocryalf99-118KoenigCalcic HaploxerollCalcicHaploxerollc99-119Belle MinaAL99-120Fort EllisTypic ArgiustollTypicArgiustoll00-101WhitewaterMN00-102KeenesburgUstic HaplargidUsticHaplargidl00-103BensonVertic TorrifluventVerticTorrifluvent00-104OrchardTypic HaplargidTypicHaplargidNM00-105KidmanCalcic HaploxerollCalcicHaploxerollc00-106BlairUstic HaplargidUsticHaplargidl00-107AmsterdamTypic HaplustollTypicHaplustoll00-108AshdosVitritorrandic ArgixerollVitritorrandicArgixeroll00-109WyorAquertic ArgiudollAquerticArgiudoll00-110Bresser IIAridic ArgiustollAridicArgiustoll00-111ShiloUstic TorriorthentUsticTorriorthentmJun-0000-112LignumAquic HapludultAquicHapludult00-113ZenithLamellic HaplustalfLamellicHaplustalf00-114WeldUstic HaplargidUsticHaplargidl00-115Monona IITypic HapludollTypicHapludollpsampled by Miller 2 different times (June 99)00-116TellerUdic ArgiustollUdicArgiustollOK00-117GrosecloseTypic HapludultTypicHapludult00-118FrancamUstic HaplargidUsticHaplargidl00-119BrookingsCalcic HapludollCalcicHapludoll00-120AmesAquic HapludollAquicHapludoll01-101O'NeilTypic UstipsammentTypicUstipsamment01-102HastingsUdic ArgiustollUdicArgiustollCO01-103OwngatePachic ArgiustollPachicArgiustoll01-104BrandonAridic ArgiustollAridicArgiustoll01-105TokieUstic TorriorthentUsticTorriorthentmMar-0101-106NikkolaUstic TorriorthentUsticTorriorthentmMar-0101-107NittanyTypic HapludalfTypicHapludalfPA01-108ProvidenceTypic FragiudalfTypicFragiudalfcollected in LA01-109HaxtunPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times01-110ColumbiaXeric HaplocambidXericHaplocambid01-111SonomaUltic HaploxerollUlticHaploxerollCA01-112KoshareUstic HaplocambidUsticHaplocambid01-113PascoXeric TorripsanmmentXericTorripsanmment01-114MaureUstic TorriorthentUsticTorriorthentmMar-0101-115Multi-BlendBLEND01-116EatonUstic TorriorthentUsticTorriorthentmMar-0101-117FairmontMollic FluvaquentMollicFluvaquentr01-118RoseTypic PsammaquentTypicPsammaquent01-119ClemsonTypic KanhapludultTypicKanhapludult01-120EwingEntic HaplustollEnticHaplustoll02-101White WaterMN02-102MarshanTypic EndoaquollTypicEndoaquoll02-103OrangeburgTypic KandiudultTypicKandiudult02-104JewelVertic EndoaquollVerticEndoaquollIowa02-105AscalonAridic ArgiustollAridicArgiustollb02-106AscalonAridic ArgiustollAridicArgiustollb02-107DarcoGrossarenic PaleudultGrossarenicPaleudult02-108HasselPachic HapludollPachicHapludoll02-109WasatchVertic EndoaquollVerticEndoaquollUT02-110KennanHaplic GlossudalfHaplicGlossudalf02-111MaderaTypic HaplocambidTypicHaplocambid02-112RandallUdic PellustertUdicPellustertj02-113AdamsAridic ArgiustollAridicArgiustollb02-114KenomaVertic ArgiudollVerticArgiudoll02-115AthensArenic KandiudultArenicKandiudultcollected by Kissel02-116Monona CTypic HapludollTypicHapludollhsampled by Miller 2 different times (sampled Aug 2002)02-117AdamsAridic ArgiustollAridicArgiustollb02-118BakersfieldTypic ToriorthentTypicToriorthent02-119PhillipsPachic ArgiustollPachicArgiustolldsampled by Miller 2 different times02-120North CarolinaTypic UmbraquultTypicUmbraquult03-101St HelenaTypic HaplustultTypicHaplustult03-102Eagle RiverAK03-103Casa GrandeAZ03-104PerkinsUltic HaplustalfUlticHaplustalf03-105AntonVertic GlossudalfVerticGlossudalfoJan-0303-106BrushVertic GlossudalfVerticGlossudalfoJan-0303-107ArmarilloUdic PellustertUdicPellustertj03-108ThorndikeLithic HaplorthodLithicHaplorthod03-109AirportAquic NatrixerollAquicNatrixeroll03-110PrincetonTypic HapludalfTypicHapludalfIL03-111LelandMS03-112BelmondIA03-113CrestonMT03-114LindonVertic GlossudalfVerticGlossudalfoJan-0303-115GriffyTypic HaplargidTypicHaplargidWY03-116CaptinaTypic FragiudalfTypicFragiudalfeAR03-117Little Flat TopsCO03-118RosettaIL03-119McBrideMI03-120PlatnerVertic GlossudalfVerticGlossudalfoJan-0304-101CassND04-102OteroUstic TorriorthentUsticTorriorthent04-103Del RayAquic ArgiudollAquicArgiudoll04-104GenolaXeric TorrifluventXericTorrifluvent04-105NettieTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-106HarryTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-107MaricopaTypic NatrargidTypicNatrargid04-108Baton RougeLA04-109MatanuskaAK04-110GeorgetownDE04-111Hutton LakeUstic NatrargidUsticNatrargid04-112StewartMN04-113WagramArenic KandiudultArenicKandiudultcollected by Hardy04-114CharlesTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)04-115San LuisCO04-116UtneMIX04-117MoscowUltic HaploxerollUlticHaploxerollID04-118AltheimerTypic FragiudultTypicFragiudulteAR04-119WahlukeDuric TorriorthentDuricTorriorthent04-120NelsonTypic HapludollTypicHapludollhsampled by Miller 2 different times (sample Aug 2003)05-101Parmasilt loamIL05-102Fairburysilt loamID05-103Three Cornerssilt loamWY05-104Immokaleesandy loamFL05-105Alderdalesilt loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-106Hermistonsandy loamXeric TorriorthentXericTorriorthentqORdata shows these as same but they are given different texture classification?05-107Pinalsandy clay loamTypicNatrargidAZ05-108Pilot Grovesilty clay loamMollicFluvaquentrMN05-109SacrasheloamLithicHaploxerandCA05-110Linneussilt loamDystricEutrudeptMEspacepricexyu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper1.32627.931.53372.1613.20360.02711.312128.699634.36771.39133.533.67082.160.02920.00991.236630.999736.341911920.81522.163.29490.24062.028116.434625.19581.5423138.63552.1658.30080.00261.203336.036341.23470.73518.912.10232.1646.20870.57082.79486.065518.13911.44438.335.41342.168.33260.00221.201132.819138.00771.7964546.98672.163.94700.09331.569543.596650.37681.7743.546.13192.166.92670.07811.514342.861149.40271.70841.544.09342.166.72560.04731.395741.078747.10811.52935.538.20812.167.33360.00151.197935.620740.79552.23465.561.38762.1616.91160.55272.758355.429667.34561.60748.5540.77262.1660.48770.01361.253138.065943.47931.64841.542.12062.160.38520.02481.302339.307744.93361.60846.540.80552.1632.42740.01381.254138.096643.51441.021821.47282.1612.06010.22141.974317.208325.7372SUMMARY OUTPUTRegression StatisticsMultiple R0.9387807757R Square0.8813093449Adjusted R Square0.8721792945Standard Error4.6124802757Observations15ANOVAdfSSMSFSignificance FRegression12053.6396675182053.63966751896.52842063110.0000002208Residual13276.574665815421.2749742935Total142330.2143333333CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept-12.06361686655.1282445036-2.35238722690.0350696645-23.1425134182-0.9847203147-23.1425134182-0.9847203147X Variable 132.87880190523.34648115239.82488781770.000000220825.649170308640.108433501925.649170308640.1084335019000000000000000000000000000000000000000000000000000000000000xySMP Buffer pHCVu(hat)t(y-u(hat))^2Sxxvar^1/2lowerupper7.510.66577896140.70991.980.00190.12480.08680.53800.88186.781.17994100291.32121.980.02000.14190.06311.19621.44637.081.12994350281.07001.980.00360.00590.02311.02431.11577.30.41095890410.88581.980.22540.02050.04860.78960.98197.350.68027210880.84391.980.02680.03740.05730.73040.95746.362.04402515721.67301.980.13770.63470.14261.39061.95536.71.49253731341.38821.980.01090.20850.07791.23401.54247.11.26760563381.05331.980.04590.00320.02341.00691.09967.510.66577896140.70991.980.00190.12480.08680.53800.88187.30.82191780820.88581.980.00410.02050.04860.78960.98197.560.79365079370.66801.980.01580.16270.09630.47740.85867.510.66577896140.70991.980.00190.12480.08680.53800.88187.281.09890109890.90251.980.03860.01520.04520.81310.99196.831.90336749631.27941.980.38940.10670.05421.17211.38677.390.81190798380.81041.980.00000.05440.06450.68260.93827.31.36986301370.88581.980.23440.02050.04860.78960.98196.32.06349206351.72321.980.11580.73390.15421.41792.02857.50.66666666670.71831.980.00270.11790.08490.55010.88657.270.96286107290.91091.980.00270.01280.04350.82480.99706.361.72955974841.67301.980.00320.63470.14261.39061.9553711.13701.980.01880.02450.02801.08151.19257.191.25173852570.97791.980.07500.00110.03140.91571.04007.50.66666666670.71831.980.00270.11790.08490.55010.88657.50.80.71831.980.00670.11790.08490.55010.88657.50.53333333330.71831.980.03420.11790.08490.55010.88657.160.83798882681.00301.980.02720.00000.02780.94801.05806.91.44927536231.22071.980.05220.06590.04221.13711.30447.190.55632823370.97791.980.17770.00110.03140.91571.04006.621.20845921451.45521.980.06090.28800.09291.27131.63927.250.68965517240.92761.980.05660.00870.04020.84801.00737.520.39893617020.70151.980.09160.13200.08870.52590.87726.681.34730538921.40501.980.00330.22720.08161.24341.56667.130.98176718091.02811.980.00210.00070.02500.97861.07767.170.97629009760.99461.980.00030.00020.02890.93741.05186.921.15606936421.20401.980.00230.05600.03901.12671.28136.32.3809523811.72321.980.43260.73390.15421.41792.02856.361.5723270441.67301.980.01010.63470.14261.39061.95537.21.250.96951.980.07870.00190.03270.90471.03437.040.85227272731.10351.980.06310.01360.02451.05511.15196.591.36570561461.48031.980.01310.32110.09861.28511.67566.61.51515151521.47201.980.00190.30990.09671.28051.66346.911.44717800291.21241.980.05510.06080.04061.13191.29287.50.93333333330.71831.980.04620.11790.08490.55010.88657.11.12676056341.05331.980.00540.00320.02341.00691.09967.520.6648936170.70151.980.00130.13200.08870.52590.87727.50.93333333330.71831.980.04620.11790.08490.55010.886571.42857142861.13701.980.08500.02450.02801.08151.19256.611.51285930411.46361.980.00240.29880.09481.27591.65137.11.40845070421.05331.980.12620.00320.02341.00691.09967.491.20160213620.72671.980.22560.11110.08310.56220.89117.591.1857707510.64291.980.29470.18780.10190.44100.84487.540.66312997350.68481.980.00050.14690.09250.50170.86797.60.78947368420.63451.980.02400.19650.10390.42890.84027.540.79575596820.68481.980.01230.14690.09250.50170.86797.470.937081660.74341.980.03750.09820.07930.58630.90057.510.79893475370.70991.980.00790.12480.08680.53800.88187.490.80106809080.72671.980.00550.11110.08310.56220.89117.50.53333333330.71831.980.03420.11790.08490.55010.88656.71.34328358211.38821.980.00200.20850.07791.23401.54246.61.51515151521.47201.980.00190.30990.09671.28051.66347.091.12834978841.06161.980.00450.00440.02321.01581.10756.051.32231404961.93261.980.37241.22470.20261.53152.33367.111.26582278481.04491.980.04880.00220.02380.99781.09207.120.98314606741.03651.980.00280.00130.02430.98841.08467.190.83449235050.97791.980.02060.00110.03140.91571.04007.150.83916083921.01141.980.02970.00000.02670.95851.06437.321.09289617490.86901.980.05010.02670.05200.76600.97207.470.53547523430.74341.980.04320.09820.07930.58630.90057.50.66666666670.71831.980.00270.11790.08490.55010.88656.41.56251.63951.980.00590.57250.13491.37231.90667.50.40.71831.980.10130.11790.08490.55010.88657.40.67567567570.80201.980.01600.05920.06640.67060.93347.20.55555555560.96951.980.17140.00190.03270.90471.03437.010.99857346651.12861.980.01690.02150.02701.07521.18206.811.32158590311.29611.980.00060.12020.05771.18181.41046.91.30434782611.22071.980.00700.06590.04221.13711.30447.20.55555555560.96951.980.17140.00190.03270.90471.03437.530.53120849930.69321.980.02620.13940.09060.51380.87256.921.15606936421.20401.980.00230.05600.03901.12671.28135.523.07971014492.37641.980.49462.67870.30551.77152.98146.921.15606936421.20401.980.00230.05600.03901.12671.28136.41.56251.63951.980.00590.57250.13491.37231.90667.540.79575596820.68481.980.01230.14690.09250.50170.86796.231.92616372391.78181.980.02080.85870.16771.44982.11397.050.85106382981.09511.980.05960.01140.02391.04781.14247.011.14122681881.12861.980.00020.02150.02701.07521.182070.71428571431.13701.980.17870.02450.02801.08151.19256.71.49253731341.38821.980.01090.20850.07791.23401.54247.61.18421052630.63451.980.30210.19650.10390.42890.84027.140.84033613451.01981.980.03220.00030.02580.96871.07087.10.84507042251.05331.980.04330.00320.02341.00691.09967.040.85227272731.10351.980.06310.01360.02451.05511.15197.480.80213903740.73501.980.00450.10450.08120.57430.89587.040.85227272731.10351.980.06310.01360.02451.05511.15197.20.83333333330.96951.980.01850.00190.03270.90471.03437.081.12994350281.07001.980.00360.00590.02311.02431.11576.691.6442451421.39661.980.06130.21780.07981.23871.55456.991.28755364811.14541.980.02020.02780.02921.08761.20317.060.84985835691.08671.980.05610.00930.02351.04031.13327.021.13960113961.12021.980.00040.01870.02601.06881.17177.350.81632653060.84391.980.00080.03740.05730.73040.95747.740.77519379840.51731.980.06650.34030.13060.25860.77596.811.46842878121.29611.980.02970.12020.05771.18181.41047.521.3297872340.70151.980.39470.13200.08870.52590.87726.721.19047619051.37151.980.03280.19070.07421.22461.51836.71.19402985071.38821.980.03770.20850.07791.23401.54247.530.7968127490.69321.980.01070.13940.09060.51380.87257.20.69444444440.96951.980.07570.00190.03270.90471.03436.051.48760330581.93261.980.19801.22470.20261.53152.333661.66666666671.97441.980.09471.33790.21221.55422.39477.540.53050397880.68481.980.02380.14690.09250.50170.86796.991.28755364811.14541.980.02020.02780.02921.08761.20317.191.11265646730.97791.980.01820.00110.03140.91571.04006.71.49253731341.38821.980.01090.20850.07791.23401.54247.460.53619302950.75181.980.04650.09200.07750.59840.90517.420.80862533690.78531.980.00050.06930.07000.64660.92406.921.15606936421.20401.980.00230.05600.03901.12671.28137.10.70422535211.05331.980.12180.00320.02341.00691.09967.50.40.71831.980.10130.11790.08490.55010.88656.740.89020771511.35471.980.21580.17360.07051.21521.4943SUMMARY OUTPUTRegression StatisticsMultiple R0.8113950016R Square0.6583618485Adjusted R Square0.65546661Standard Error0.2530855852Observations120ANOVAdfSSMSFSignificance FRegression114.565155315914.5651553159227.39468000450Residual1187.55817298470.0640523134Total11922.1233283006CoefficientsStandard Errort StatP-valueLower 95%Upper 95%Lower 95.0%Upper 95.0%Intercept6.99907439920.393927628217.767411826306.2189912967.77915750246.2189912967.7791575024X Variable 1-0.83743973920.0555345703-15.0796114010-0.9474131882-0.7274662902-0.9474131882-0.7274662902000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000Variations in methods for Mehlich III extractable nutrients Reference pubQuantity of soilVolume of Mehlich IIIMixing time and methodSPAC, Inc.5 cm350 mL5 min on reciprocating shakerSouthern2.5 cm325 mL5 min on reciprocating shakerNortheasternScoop 2.5 cm3or 2.5 g(references orig. method on 10:1 ratio based on vol.)25 mL5 min on reciprocating shaker at 200 epmNorth Central1.7 cm3(2 g scoop)20 mL5 min on shaker at 200 or more epm between 24 to 27oCWestern2 0.05 g20 mL5 min on reciprocating shaker

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